ML16294A190

Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix G, Part 1 of 11

ML16294A190
Person / Time
Site:	West Valley Demonstration Project, P00M-032
Issue date:	08/22/2016
From:	MJW Technical Services
To:	Office of Nuclear Material Safety and Safeguards, State of NY, Energy Research & Development Authority, Office of Nuclear Reactor Regulation
Shared Package
ML16293A155	List: ML16293A130 ML16293A131 ML16293A132 ML16293A133 ML16293A134 ML16293A135 ML16293A136 ML16293A137 ML16293A139 ML16293A140 ML16293A141 ML16293A142 ML16293A143 ML16293A178 ML16293A179 ML16293A180 ML16293A181 ML16293A182 ML16293A183 ML16293A184 ML16293A185 ML16293A186 ML16293A187 ML16293A278 ML16293A279 ML16293A281 ML16293A282 ML16293A364 ML16293A365 ML16293A366 ML16293A367 ML16293A368 ML16293A389 ML16293A391 ML16293A392 ML16293A393 ML16293A394 ML16293A674 ML16293A675 ML16293A676 ML16293A677 ML16293A678 ML16293A808 ML16293A809 ML16293A810 ML16293A811 ML16293A812 ML16293A843 ML16293A844 ML16293A846 ... further results
References
Download: ML16294A190 (35)

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{{#Wiki_filter:Appendix G-Area Certificates of Analysis

Appendix G-Area 1 -COA

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 ~ (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: MJW Corporation Address: l 5 .Hazelwood Drive Suite I 12 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

     . ... -* *- -* *- ... *-* .. -- .......... ***** ..              ... -****      ...... .

Client Sample ID: I. l.C I Project MJWCOOI 15 Sample ID: 385101005 Client ID: MJ\VCOOI Matrix: Soil Collect Date: 22-0CT-15 !"0:05 Receive Date: 05-NOV-15 Collector: Client Moisture: 32% Parameter MDC RL Units_. . .... i?.f.__~-~~~ys_t __!)ate Time Batch. !\-1~thod_ Gravimetric Solids ASTM D 22 ! 6 % Moisture "As Received" Moisture 32 0 percent LYTI 11110/15 0955 1521927 Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Actmium-227 !J -0.598 +/-lJ 511 0703 pCi!g RXF2 12!03/l:'i 0825 1522386 2 r\ntimony-125 u 0.143 +/-0 176 .ii 346 pCi.'g Ccsium-137 3.64 +/-0 256 0 108 0.[()0 pC1/g Cobalt-60 ll fl.Oii -r/-0.-0535 0.112 pCi/g Europium-154 l! 00401 +/-0 155 0.31_6 pC1/g Protacumum-231 lJ -0.936 +/-0.826 I 27 jJC1/g Radium-226 074(! +/-0 216 0.200 pCilg Radium-228 0 777 +/-0 275 0.308 pC1/g Tin- 126 l.l 0 0572 +/-0 l 74 0. 191 pC1/g Rad Gas Flow Proportional Counting GFPC, Gross A/B. solid "Dry Weight Corrected" l\.l1Jh.a 12.6 +1-3 93 3.89 4 00 pCilg JXB7 12/02115 1412 152576% 3 Beta 25.5 +/-3.89 3 57 IIJ.O pCi/g !l1e_ f<>.~l.t>.w.!~~- P.r~p .~1.~t_l:o~~--~\.'~r7_ P:e.~~<>.rr_n_~<;I:_ .. Method Description Analyst Date Time Prep Batch br-Y So1i Prep... ... . *- .... "or): Soii"Prcp GL-kA°D~A-(i.ii . . . ... -..... . L)'Ti .. . 0955

                                                                                                                                                                                          *****152f927"""-*-*** ............ **- .. ***-*-* **-

.!.h.~-f?.11?\~*.in_~ -~-~-alY.ti_ci:t_l_ l\~~tl1~~~ w.er.e._ pe_~r~rI?~d: .. . . ..... . .. .. ..... . . .. . . .. . . .. ... .. .. . (\W~o-~_ ... . .. _p~scr,ipti911_____ ......... *****--- .................... ___ .. -** *-****** .......... _.. AnaJyst.(o~in<,:)1t~ ........ . [ ASTM D 2216 (Modified) 2 DOE HASL 300, 4 5 2.3iGa-lll-R EPA 900.0iSW846 9310.iSM 71 JOB Modified Notes: Counting Uncertainty is calculated at the 95% confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: MJW Corporation* Address: 15 Hazelwood Drive Suite l 12 Buffalo. New York ! 4228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

  ...................                                           . -**** ....... -*           - ... . ... . ..

Client Sample ID: l.2.CJ Project: MJWC001 l5 Sample ID: 38.5101006 Client ID: MJWCOOI l\!latri.x: Soil Collect Date: 22-0CT-15 !0:55 Rec*eive Date: 05-NOV-15 Collector: Client Moisture: 24%

 ~~r~!n.~t~r . . .. .                   ......... .9~.a~fier      -~e_s.~il~ ___U_n.c.e~~int.J.:. _ . _ -~1.I?S .           ... RL Gravimetric Solids ASTM D 2216 %i Moisture "As Received" Mrnslure                                                                24 0                                                                          percent                        l. YTI     11110115 0955 I 521927 Rad Gamma Spec Analysis Gammaspec. Gamma, Solid Dry Weight Corrected" Aclmium-227                                                ll      -0.0837           -t/-0 370                 0.680                                    pCifg                        RXF2. 12iU3115 0826 1522386                                       2 Antimony-12.5                                              [.l       00215           +/-0.151                  () 281                                   p('iig Ccsium-137                                                              2 52          +/-ll.198                () 102             0 IOtl                pC1!g Cobalt-60                                                  u         0.0114         +l-0 .04(15              0 0856                                     pC1/g Europtum-154                                               u       -0.0436           +/-0 13 3                 0245                                     p(."':'1/g

• Protactimum-231 L' U.537 .,-/.1) 730 I 32 pC1/g Radium-22.6 {) 909 ...,.() 223 0201 pCilg Radium-228 0 595 +/.().287 0.350 pCilg Tin-126 U -00136 +/-0 166 0262 pC1/g Rad Gas Flow Proportional Counting GFPC'. Gross AIB, solid "Dry Weight Corrected" Alpha 7 52 +/-3.29 3.92 400 pC1/g JXB7 12102/15 \412 1525768 3 BS ~5 +1-3.81 3 69 10 0 pCi/g Th.~. f<?!.1.()~Y.i~~ Pr~P... 1\.'!t:t~.od_s _we1:~ p_e1/()1:llll!d.:_

Method Description Analyst Date Time Prep Batch ory**so~rpr*ef; ** **-*-**-*-- **-*******-**or): So1f'Pre*p*GL~R:Ao.:A:o:ff **-***-***-****** * . -****- . **-*** *"l>i'fl * ............... f1ii.nii5 * .. l)955 ***i si 19ii". *** ................. ** ***** -*** -* * **-** _:r1~e 1~~)?~!.~~--f\~~IY.ti~~l '.':~~~~o_ct: ."."'~~- ~:.r!?.~~-~-: ..... _......... __ ........ -*- _-*** ........ . . ......... ***-***---* Methqtj .. . . .D_e~cripti{)n. .. . . .. .. . .......... _ .. ... . .... . . _An11.J.l'st ~Ql)l,JJJe.11ts.... . .. _.. . ASTM D2216(Mod1ITcd) 2 DOE HASL 300, 4523fGa-01-R 3 EPA 900. OiSWS46 93 IOjSM 71 IOB Mod 1ficd Notes: Counting Uncertainty is calculated at the 95% confidence level fl .96-sigma). 11

                                                                                                                                                                                           -

GEL LAB ORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Rcpon Dote: December 17, 2015

Contact:

Ms. Lourie Losey Project: Soil Radioisotopes Client Sample ID: 1.1.C l Project: l\-UWCOOJ 15 Sample ID: 3&5101005 Client ID: MJWCOOI Matrix: Soi! Collect Date: 22-0CT-15 Receive Date: 05*NOV- J5 Col!ector: Client Moisture: 32%

                                                                                                                                                             .........     *- ..                     . ...... .

P:u---.unete r Result L)tcert:ti!l!Y ________ :Vl_D( __ . --~c __ __ . _ _Trr. _____ . . RL,_ Units _ Df_ -~~~~y~t- ___ _I>atc___Ti1t1e. J3'.lt~-~-- --~ltd:_ Gravimi:tric Solitls

 .-IS1JJ D 2216 % MoislUre "As Rt:cei1*ed" Mo1s1ure                                                           J2_0                                                                                             percent             LYTl   11/\ll/15 0955    1521927 R11d Gam1t1a Spec Alrnlysh Gammpspec. Gamma. Sofid "Dry Weigh! Corrected" Actmmm-227              '                          U          -(l.598          +1-0511                0.703         () 328         +1*0.585                          pC1/g              RXF2   12103115 0825     1522386         2 Antunony-125                                       U             0 143         +1-0 176               () 34&        0.162          +i-0 188                          pC1/g Bismuth-212                                        U             0.236         +l-0.678                  !J3        0591           +1-0.687                          pCi/g Bismuth-214                                                      0.740         +/-cl 216              0.200      D.ll9Q(,          +/-0_226                          pCtlg Ccsmm-137                                                          JM           +/-ti 256             0 108         (l 049         +/-tl-416           () 1(1{)      pCilg Cobalr-60                                          U             !i tl1 I     +/-0 05J5               {) 112     0.0476           +1-0.0538                          pCilg Europium-15-1                                      U           O 040 !         +/-0 155               (1.316        0.135          -<-/-0 \56                        pC1/g Lcad-212                                                         0.615         +/-0.142               () 155     O_ll724           ~1-0_ 152                         pCilg.

Lead-214 0.910 +/-0 196 0403 II 193 i-/-0.212 pCt!g Potassium-40 I0.4 +/-1.92 0.958 0-396 +/-2.12 pC1/g Protacumum-231 u -0 936 +/-0 826 I 27 0-589 -t-/-0. 952 pCi/g Radium-226 0.740 f.().2]6 0200 00906 +f-0.226 pCi/g Rad111m-228 0.777  ;./.Q 275 "308 0.132 +/-0 Jlll) p('1/g Thallium-208 0.121 +/-0.102 IW96R l)_[).\36. +/-0.102 p('ilg Tin-126 tJ 00572 +/-0-17-1 0 191 0.0904 +/-0 175 pC1/g Rad Gas .Flow Proportional Counting GFPC G1*oss A.B. solid "D1:1* Weigh! Cprrec1ed" Alphil 12 6 +/-3-93 3-89 1.57 +/.4_62 400 pCi!g JXB7 12102115 1412 1525768 3 Reta 25.5 +/-3.89 3-57 1 61 +l-5 31 100 pCilg ~:~c _foll~\~i_ng_Pi:_ep_ l\-leth_ii.~s. '\er.~ _p~rforn,i_~~ . . . .. . **-** -- . ... -*-*-**. **- Method Description Analyst  !>ate Time Prep Batch

                                                  . .. . ******                                            ................            ......... --***-* -*******-**-**** -***-* .... .... ...

Dry*S(11J Prep Dry S(lll Prep GL-RAD*A-02 I L'lTI 11/IOflS 0955 1521927 Tbe __f.0J_ll)~-~1_!~_A!1_~_lyti_ca,I __ i\~_et_ho~~- ~\*er,~ p~r_f~ ~lll~c!- _ ...... ... . . ******** .............. ******-* ***-**** *****-**** Method Description ASTM D 2216 (Modified) 2 DOE l\ASL 300, 4 5 2 J/Ga-0!-R 3 EPA 900_0/SW846 93 !0ISM 7\ IOB Modified Surrogateffraccr Recovery Test Batch m ReCO\'Cry% Acccp!ablc Limits

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -www.gel.com Certificate of Analysis

  . Company:        M.IW Corporation Address:        15 Hazelwood Dri\*e Suite 112 Bu!Tnlo. New York 14228                                                                                                           Report Date:      December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 1.1.C I Project: MJWCOOI 15 Sample ID: 385101005 Client ID: MJWC_OO ! Par~mctcr .. .Qu,nlilfcr. ...... R.!~u_U_ ..... ~~n-~ert;a_i!J.IY. ...... ~:l_l)C ........ _l~c__ .... __ .. Tr..L ....... ll~ ...~'{lits... .Df. ~\n_aly~t. l)at~. l}l_tlc __ B~tc_h_. ~t.!.1~ Sur1*ogatc/Traccr Recovery Test Batch ID Recovery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2*040 Savage Road Charleston SC 29407 - {843} 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Huzelwoo<l Drive Suite 112 Buffalo. New York 14228 Report Date: January 2.0, 2016

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 1.1.C.2 Project: MJWC00115 Sample ID: 388092001 Client ID: MJWCOOl Matrix: Soil Collect Date: 22-0CT-15 Receive Date: 23-DEC-15 Collector; Client Moisture: 17.8% Parameter ...... 911.al_ilil'.'.. -* MDC Le TPl' RJ, l'nits... f>.~. ::.\n'.11.Ys.t .. Date Time Batch Mttl. Gravimetric Solids 1JSTM D 2.216 % Moisture "As Received" Mornturc 17.8 pcrc~nt LYTI 12124115 0703 1533555 Rad Gamma Spec Analysis Gammaspec, Gum ma. Solid "DIJ' H'eighr .Corrected" Actmmm-227 lJ 0.039 +/-0.193 0.355 0 \69 +l-0 \94 pC1/g MJB I 12i29/15 1154 1533562 2 Antm1011y-!25 ll -0.0086 +/-0 072 0 134 0.0626 +l-0 0721 pCi/g Bi~muth-212 UI 0 OU  ;./.(l 40') 0.824 0.385 ..f.tJ.471 pC1/g Bi~muth-214 0.599 +/-0l12 00%(> 00448 +/-0 123 pC1/g Cl.lS\UID-137 0.182 +1-0.0431 00264 IU)l 12 +/-0.0458 0.1()0 p('1/g Cob~lt-60 u -000744 +1-0.0317 0 0.575 0.0256 +/-0.0319 pC1fg Emopium-154. u 00456 +/-0.0908 0 180 . 0.08l3 +/-0 0932 . pCilg 1.cau-212 0.522 H-0 !04 0. !06 (). 0513 +/-0 113 pCi/g Lead-214 () 878 +/-0 14(, 0106 00498 +/-0 164 p(.'1lg Potassium-40 9 so +/-I 00 0 601 0 269 +/-1 30 pCifg ProUictimum-231 lJ 0 00 +1-0561 0.599 0 281 +1-0 592 pCi!g Radium-226 0599 +/.() l 12 O.ll%(1 0 0448 +1-0 123 pC1/g Radium-228 0.6f>3 +/-0.230 l) 169 () n759 +/-0.250 pC1tg Thall1um*20& 0 248 +/-Q.0628 0.0465 \10215 +/-0.0663 pCi/g Tm-!26 u 0 0313 +l-0 0955 0 130 0063 +/-0.0964 pCi/g Rad Gas Flow Prupurticmal Co!lntin~ CiFPC, Gross A:B. solid 11D1:1' Weight Carn!l'ted'1 Alplla 9 22 +/-l.49 l 62 () 748 +/-2.31 4 00 p('ilg JXB7 01/11/16 1859 1534760 3 Beta 14 3 +./-! 24 1.28 0614 +1-2.34 10 0 pCi.1g

}l.1_c:_ ff!ll_ow_i_ng_P.~_e.p ~l~t~ods "'-cr.e_pcr..form_e_d ....

Method Description Analyst Date Time Prep Blitch Dry Soil Prep Dry Sml Prep GL-RAD-A-02 l LYTI 12/24-115 11703 1533555

1:~':! ft_il_ID'Y.~n.g An:J:lyt~t:~l _:V,l!:!~~odS'_Ytr~ pcrforl!le.~..

VIethod Description ASTM D 2216 (Modil1ed) 2 DOE HASI. 300, 4.5.2JiGa-01-R EPA 900.0!S\V846 93l0/SM 71 lOB Modified Surrogatc/frncer Recovery Test Batch ID Reco,*c1j% Acceptable Limits

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -{843) 556-8171 -WWW.!;jel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 1!2 BufTalo. New York 14228 Report Dare; January 20. 2016

Contact:

Ms. Laurie Lo~ey Project: Soil Radioi~otopes Client Sample ID: l. l.C.2 Project: MJWCOO I 15 Sample ID: 388092001 Client JD: MJWCOOI Parameter Qualifier .......R.csu_lt .... l'nc.er..ta_inty ......MDC......I:c . Surrogateffraeer Recovery Test Batch ID Recovcry 0k Acceptable Lin1its Notes: TPU and Counting Uncertainty arc calculated at the 95% confidence level (1.96-sigma).

-....;::;-'",

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Ha:;o;clwood Drive Suite 112 Buffalo, New York 14228 Report Date: January 20. 20 I 6

Contact:

Ms. Lallrie Losey Project: Soil Radioisotopes Client Sample ID: 1.1.C.2 Project: MJWCOOJJS Sample JD: 388092011 Client ID: MJWCOOJ Matrix: Soil Collect Date: 22-0CT-15 Receive Date: 23-DEC-l 5 Collector: Clieut Moisture: l 7.8~o Pa ram etc.- Le TPl' RL ll11its Rad Gmnma Spec Analysis c;ammaspec, Gamma, Solid "D1:v H-'eiglu Corrected" Acumum-227 l~ 0 189 +/-(J.366 0420 0.196 +/.() 37} pCi/g MJHI 01118116 1)627 I 534020 Anmnony-125 u ().()0955 +f-0.0883 0 168 0 0769 +/-0 0884 pCilg Bismuth-212 Ul 0 00 +/.] 04 1 31 0.607 +/-1 25 pCil~ Bismuth-214 {) 814 +l-1) 159 0 l19 0.0536 +l-0 173 pCilg Ce~mm-137 0.150 +/-0.0613 1).(1615 0.{]274 +/-0.0625 0.100 pCl/g Cobalt-60 ll 0.00777 +/-0 0336 00701 0 0.298 +/-0.0338 pC1/g Europium-154 !J -II U0312 +/-0 l !3 0.220 0.0958 +1-0 113 pCi/.g Lead-2!2 0646 +/-0 I \9 0.0981 00461 +J-!l 148 pCi/g Lead-2\4 0.946 +1-0.168 n.296 0 143 +1-0 I'll pC1lg l'otassmm-40 9.18 +/-1.34 tl.716 llJl2 +I-I 57 pCi/g Prota~trmum-231 UI 000 +1-0.454 0 626 0.284 +/-0.473 pC1/g Ratlium-226 08l4 .,./.(1 [59 0.119 0.0536 +1-0.173 pCllg Radium-228 06&5 +/-0.271 0.223 0 0972 t-1-0291 pCill! Thallium-208 0. 191 +/-0 0609 ll.0636 (J 0288 +/-0 063 pCi/g Tm-126 UI 0.00 +l-00805 ll0794 0 0375 +/-0 0823 pC1fg.

!!.if:!_ foll()wing. l'rcp. ~!.c.t.~oi!~_\vere P.cr~~i:n.11:1.tl . , .,............. .                                                                    . .. .. .. . . ***-*

Method Description Analyst Date Time Prep Balch

                                                                                                   . *-***                                 ..... -** ...

Dry Soll Prep Dry Soil Prep GL-RAD-A-021 LYTI *!2124/l.5 0703 1533924 !_h1:..f.1J!l~~':!l!~l!\~!1:1Y.1!.~.'11.~1c1.h.o<J.:s 'Y.e1*e. p~~.f.~.r~e(~ Method Description DOE HASL 300.4.5.2 3/Ga-01-R Surro~111e/Tracer Re<:overy Test Batch ID Recovery% Ac:ceptable Limit~

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8i71 -www.gel.com Certificate of Analysis Company: MJ\\' Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Report Date: January 20. 20 l6

Contact:

Ms. Laurie Losey Project: Soil Radioisotapes Client Sample 10: 1..1.C'.2 Project: MJWC00115 Sample ID: 388092011 Client ID: MJWCOOI ..... .. . . ...... ******** P:ir:imeter ...... Q'!ali~_e!'. Result ... _l'n~ert:tinty .  !\-'IJ)C Le ........ T..f:'.l! ......... _l_lL .... l:n.ils.. ll.F. -~"lll):'st .. _[)i:i_t~ .'!:.i.1_n~ .~atc.h .. M.ttL Surroii,atcffraccr Recovery Test Batch ID Recovery% Ae~eptablc Limits Notes: TPU and Counting Uncertainty arc calculated at the 95% confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Ce.-tificate of Analysis Company: MJW Corporation Address: 15 HaLelwood Drive Suite 112 Buffalo, New York 14228 Report Date: December 17. 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample fD: 1.2.C 1 Project: MJWCOOl 15 Sample ID: 385101006 Client lD: MJWCOOI Matnx: Solt Collect Date: 22-0CT-tS Receive Date: 05-NOV-i5 Collector: Client Moisture: 24% Parameter Le

• 000****

TPC

                                                                                                                                  >O* ** OOHO 0 M >O 0  0 0   0 RL                 (:nits OF Analvst 00000 0 . . . . . 00 0 Date Time Batch :VHd.
                                                                                                                                                                                                      ****** ~ * * *

• 00 . , 00 *** 0 00 0 ., 0 0 00 0 ... 0 Gravimetric Solids ASTJf D 2216 % Moi11ture '~4s Received

Moisture 240 percent LYTI 11/lQ.1150955 1521917 Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry /Yei~hl Corrected" Actmium-227 \J -0.0837 **/-0 370 0.680 0 322 +1-0 373 pCi/g RXF2 l 2103.115 0826 152:;!386 2 Anlimony-125 IJ 00215 +/.() \51 0 281 0131 +1-0 151 pC1/g Bismuth-212 u 0.529 +/-0 674 I 36 0619 +1-tl 717 pCilg Bismuth-214 0.909 +/.().223 ()201 0.0931 +/-0 236 pCi/g Ccsium-137 2 52 +/-0.198 0 102 0.0465 +/-0.286 () 100 pC1/g Cobalt*60 u 00114 +/-0.0405 0.085<- () 0363 +/-{) 0409 pCt/g Europium-154 LT -0.0436 +l*O 133 0.245 0 l05 +l-0 JJ4 pCi/g Lead-212 0.621 +/-0 130  !) 153 () 0727 t-/.() 139* pCi/g Lead-214 0.926 +/-0.244 0205 0.0%3 +f-0 255 pC1/g Potassrnm-40 11 7 +/-1 50 0 645 () 257 +/-1 82 pC1/g Prolactmrum-231 u 0 S37 +/-0 730 132 0.621 "'-/-0 778 pCi/g Radium-226 0.909 +/-0 223 0 201 () 0931 +f-0.136 pCt/g Radium-228 0.595 +/-0.287 0 350 0.157 +1-0.298 pCi!g Thallium-208 0246 +/-0 090 0 094(, OJJ434 +1-0.tl924 p('i/g Tin-12(> LI -0.0136 +/-0.1()6 n.2n2 0.126 +!-016.6 pCi!g, Rad Gas Flow Proportional Counting GFPC. Gross :J.B. solid Dry Weight Corrected" Alplia 7.52 +/-3 29 3. 92 I SY +/-3 63 4*00 pCt/g .JX!l7 ~2!02115 1412 1525768 3 Beta 24.5 ~t-3.81 3 69 1.68 +1-5.17 100 pCt!g Jh.i: f.o_l_Io_l.v.i!ll,1 ~.'.:..".P. M~~~<l..d.s_1'."cr.e pc_rforlJl~<.1.. ... .... -*-*

!\1ctho<l                           Description                                                               Analyst                     Date                                Time            Prep Batch
. . .. .. ..... **- .. -*-**..   -* . **-. ***-- **--*-*-* ..    -* ......                                                                 -* . . .

Ory Soil Prep Dry Soil Prep U L-RAD-A-021  !.YTl I III 1)/15 0955 1521927 "_fb~ f[Jll(J1Vill,f,{ A1rn!r.t!c:1l :\-!ctlil)~.~ _'.\'.t:'.:.e_ r.e_r~nrnu!~

\1ctb11d Description

                                 .....

ASTM D 22 I6 (Mo<l1Jicd) 2 DOE HASL 300. 4 5.2.J.'Ga-01-R 3 EPA 900 O!SWS46 9310/SM 71 lOB Modified Surrogaterrracer Reco1*cry Test Batch ID Recovery% Acceptable I,imits

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843} 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drh:e Suite 112 13uffalo, New York 14228 Report Date: December 17, 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 1.2.Cl Project: MJWCOOl 15 Sample ID: 385101006 Client ID: MJWCOOl __........ *****-* ............... -*-*--**.. --***** ..-***-- ***-*-*.. *-** -*-* .... **-****** ..... - ........ -****** **-*** ..... ***- *- . .......... . **-**-** **-*******-***** ..................................... - .. , ..... ' ..

                                                                                                                                                                                                                               '**

-~iu:_~_rn.~!.cT _.. ____ . _____ ..Q_11i~i.f!~~- .. ,, _ _l~e_s~tlt_.... -~'.!l~C._t:t:tin!Y. _.... ,~1.J?.~~ .... Le JJ'.l~. _. __ }ll,;.____Lt11.i1!1.. ll.1'.'.. ~!lalyM_ __()~te JilJI~. _Bnt~h.. :\f~~: Surrogalcffraccr Recovery Test Batch ID Reco\'ery% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - W"Ww.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 !*Ia:i:eh\ood Drive Suite 112 Buffalo, New York 14228 Report Date: January 20. 2016

Contact:

Ms. Laurie Losey Project; Soil Radioisotopes Client Sample ID: 1.2.C.2 Project: MJWCOOl 15 Sample ID; 388092002 Client !D: MJWCOOl Matrix: Soil Collect Date: 22-0CT-l 5 Receive Date: 23-DEC-15 Collector: Client Moisture: 15.8% Result Le ... TPJ'.. RL l'.nits Dr< Analnt

                                                                                                                                ....................................... ****' '* .......Date
                                                                                                                                                                                        ~

Time

                                                                                                                                                                                          '* ............... .

Batch :\-1td. GraYimch'ic Solids i!STM D 2216 % Mois/l/re "As Rect'iw:d" Moisture 15.S percent LYTI 12124115 0703 1533555 Rud Gamma Spec Anal)*sis Gommaspec. Gamma. Solid "DI')' lFl!ight Corrected" Actinium-227 U  !}.()35 +1-0.176 11343 0.163 +1-0.177 p('1lg MJH I 12/29115 1154 1533562 2 Antmiony-125 ll U.033 +/-0 0658 0.128 00601 +1*0.0675 pCi!g l31smuth-212 lJ IJ 00 +f-0 523 0.&52 0400 +1-0.843 pC1!g Bismuth-214 0 605 +t-O 120 ()(1912 00422 +/-() 136 pCilg Cesmm-137 0 139 +!-0 0437 0.05\ 0.0236 +/-0.0452 0 100 pCi/g Cobalt-60 lJ (I 0124 +f-0.03Q 0.()606 0.0273 +/.(l.0305 pC1ig

• Europmm-154 lJ 0.{1494 +f-0 128 0 tSO 0()818 +1-0.130 pCi/g Lead-212 0.715 +l-ll,132 00806 00385 +i-0.14(1 pCi/g Lead-214 0 812 +/-0 114 0.200 0 0972 +J-0 133 pC'i/g Pornssmm-40 13 n +/-1 ()6 0.348 0 144 +/-1 53 pC'1/g Protactmium-231 ll 0.110 +l-0 388 iJ5J(I 0248 +1-0.431 pCl/g Rmhum-226 n 605 +f-0 126 00912 0.0422 H-0.1311 pC1!g

. Radium-228 0 456 +/-0 233 () 1~9 00711 +1-0 24() pCi/g Tbalhum-208 0.226 +/.().0531 00445 0.0205 +/-U.0563 pC1/g Tin-126 UI 000 +f.JJ lll7 () 129 0U625 +l-0 107 pC1/g Rad Gns Flo1~ Proportional Counting GFPC. Gross A. B, solid D1J* Weight Corrected"

                                                                                 +/-1.68          2 2')            +/-2 09                    pCiig                                 Olil 1/16 1859             1534760
 ~*                                                            ~D                                          1 08                    4.00                             JXB7                                                 3 Bc1<1                                                          170              +1-145            l.tW   0 818    +/-2.77         10.0       pCilg T~c fo_ll()Wi_n_g __P_:r.e.p ~I~!~~d..:~.l\:~1:c.J.lC!:fo_rll\£d. .....
 .\1ethod                   Description                                                                 Analyst        Date                 Time            Prep Batch
                                                                                                                                                  .. ******* .............. .

Dry Soil Prep Dry Sotl Prep GL-RAD-A-021 I.YT! 12/24115 0703 1533555 The following Anal)iical Methods W!;rC 11crformed

~:1~th-~d* ** **** * * *iics.ci*i!>!iiiii * *** * ** ** -* ** *** * ****** **

ASTM D 2216 [:>.fod1fied) DOE HAS!. 30G, 4.5.2 3/Ga-01-R EPA 900 OISW846 9310iSM 7! lOB Modified Surrc>gatc/Tracer Recovery Test Batcll JO Recovery% Acceptable Limits

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112

                    ~uffalo, New York 1.:/.228                                                                           Report Onie:        January 20. 2016 Contact         Ms. Laurie Losey Project:        Soil Radioisotopes Client Sample ID:    1.2.C.2                                                                  Project             MJWC00115 Sample ID:           388092002                                                                Client ID:          MJWCOO l l'arnmeter                                                              Le         .... 'f P.t:. _. *-* *- _RL.. _~'.nhs_. _D.f A11a_lyst___ 0.!lt.~ _Time ..B~tc~ .. ~I_td:

Surrogatcn'racer Recovery Test Batch ID Rccm*cry% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( ! .96-sigma).

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228 Report Date: Jan11ary 20. 2016

Contact:

M~. Laurie Losey Project: Soil Radioisotopes Client Sample IO: 1.2.C.2 Project: MJWCOOl 15 Sample ID: 388092012 Client JD: MJWCOOI Matrix: Soi I Collect Date: 22-0CT- l 5 Receive Date: 23-DEC-15 Collector: Client Moisture: 15.8% Parameler .Le Rad Gamma Spec Aualysis Gamma:;pec. Gamma. Solid "Dry 1-Veight Corrected Acnrnum-227 u 0017 +/-0 253 D 495 0 231 +1-0.253 pC1/1; MJHI 01/18116 0627 1534020 Antimony-125 ur 0 00 +/-0 0944 . 0 200 (J 092 +1-0.106 pC'l/g Bismuth-212 u 0.557 +1-U.587 1n 0.562 +1-!i.641 pC1/g Bismuth-214 D.730 +/-0 170 I) 131 0.059 +i-0 183 pCi/g Ces!um-137 () l43 +/-() 063() 0.0815 (}.(1372 +/-0 0649 U.10(1 pC1tg Cohalt-6(1 u -0.00831 +/-<i 0387 0 0741 (}.()313 +/-0 03&9 pC1/g Europium-154 u -00202 +1*0.147 0.276 0 123 +/-0. 147 pCi!g Lead-212 0891 +1-0126 fJ.l 17 0055.J. +1-0 148 pCilg Lead-214 1 03 +l-0 209 ll 13 l 0060 +/-0.228 pCi/g Poiassi um-40 l4.7 +i-1 52 0.67() 0.27'J +l-1 97 p('i/g Protacl1111um-231 IJ -0.189 ..,.{) 521 11.MJ 0 38.9 +1-0.529 p('1lg Radmm-226 0 730 +/-0 170 0 131 0059 +1-0 183 pCi/g Radmiri-228 0932 +/-0 262 ll 295 0.132 +/-0.298 pC!fg

'Ilml\mm-208                                             0.185            +/-0 030      00679      00307    +/-0 0817               pCilg Tm-126.                                     lJ         ()0471             +/-0.140         0 161   (}07&8    +1-0 14]               pC1/g

r~~ foll.ov;ing J11~e]?_i';.l!'.~~~ds .w~:r~ r.~rro.i:111cl}

Method Description Anal)'St Date Time Prep Batch D1J Soil Prep D0* Soil Prep GL-RAD-A-021 LYTl 12124/15 0703 1533924 !h.c. foll1J,w.i.ng A.na.lyti~a l}\l~.t~o'l.s .:w.c1:~-P.~.r.fo.r_mc.d ...

\fotl!od Description DOE HASL 300. 4 5 2 3/Ga-Ol*R Sllrrogateffracer Recovery Test Barch JD Rcc1n*cry% Acceptable Limits

                                                                                                                                                    .       ...

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Bu!Talo. New York 14228 Report Dute: January 20. 2016

Contact:

Ms. Laurie Losey Prnject: Soil Radioisotopes Client Sample ID: 1.2.C .2 Project: MJWCOOJ 15 Sample ID: 388092012 Client ID: MJWCOOI .l'.'.1.ra~~-te~**-**- ....... -*** .... 9.1!.?.l_ifi.~.r. ...... ~es!l_lt.. _l'n_cc.rtain1_v . *-* .. :\:IT)C_ .. J,c TPt:

                                                                                                                      ... -*****- -     R~. C1t!t~ ... IJ_f'. 1~11alyst_ . D_a~_e.Yilile _B_at.c_h_ ..~~td.

Sui*l'Ogate!fracer Recovery Test Batch ID Recovery% Acceptable Lirnits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company: MJ\V Corporation Address: 15 Haze!wo.od Drive Suite 112 BuffaioT New York . 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

           .. ..  . . ..                 **-* ...
                     *client Sample ID:                     1.3.CI                                                                                   Project:              MJWCOOll5 Sample ID:                            385101007                                                                                Client ID:            MJWCOO!

Matrix: Soil Collect Date: 21-0CT-15 09:35 Receive Date: 05*NOV-15 Collector: Client Moisture: 39.2% Parameter Qualifier MDC RL

-** *****-** **-* ........ -**** *****-* .............. ***-* ... .

Gravimetric Solids ASTh1D2216 % Moisture "As Received" Moisture 392 Rad Gamma Spec Analysis Gatnmaspec. Gamma, Solid "Dry Weight Corrected" Actmium-227 u -0 01U9 +/-() 316 Antimony-l 25 ll 0.156 +/-0152 Cesium-l37 0.406 +/-0.144 Cobalt-60 ll 0.0075 +f-0 0663 Europ1um-l54 u 0 165 +/-0.187 Protaclimum-231 u 0.635 +/.rJ.752 Radium-226 ll.802 +/-0.242 Radium-228 \.03 +/-0 402 Tin-l26 Ul 0 00 ...,_() 0942 Rad. Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight CotTected" ~~ 7M +/-3,45 Beta  :!5 6 +/-3 77 T.liefoll.~w!ng Prep .Me~l!ol:J~ ..\1V~.r.e pe.r.f:'a.i:m.e.d.: ... Method Description Analyst Date Time Prep Batch bi):so~*1prcp*- ***** **-****** ....... _"Dr}*s*oii.PiePGL~*RAb-A'~*oii * ** *'L~*~:ri .......... * -* * 't"1/i-Oils*** ***** - -*6;i55 ........ ***1'5ii9i7 .. ............ ***-*****- . *

 !.~~- ~~.ll_():Vi!lg; ~~~l~t.i_~.~1. ~f~.tll.?.~.s \V.e.ri:yer.f?.rn.1ed.: _ ..... _. ................_ ... *-............................... *- ..... _. .. ..... .                      .. .

.M~t.h9.<l _ ............. -**. De.si:,rip~ior.i ....... _................ -* . .... ........... .. . .. .At!~!yst.C:9n1me:1.lt~ *-. .. .. .. ASTM D 2216 (Modified) 2 DOE HASL 300, 4.5.2.3iGa-01-R 3 EPA 900 OISW846 9310/SM 71 lOB Modified Notes: Countrng Uncertainty is calculated at the 95%, confidence level ( l .96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: !VUW Corporation Address: 15 Haiclwood Drive Suite 112 Buffalo. New York. 14228 Report Date: December 17, 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes ClientSampleID: 1.3.CI Project: MJWCOOll5 Sample ID: 385l01007 Client ID: MJWCOOI Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 39.2% Parameter ... 9.ua_li_~~'." . . Result Le Gravimetric Solids ASTM D 2216 % !'doislure "As Received" Momure 39.2 percent LYTI 11/10115 0955 1521927 Rad Gamma Spc~ Anal~*sis GammasjJec. Gamma, Solid "Dry Weight Corrected" Actinium-227 u -Q.0109 +f-0 316 0 586 0 27{) +/-0.316 pC1/g RXF2 t:\103/!5 0826 1522386 2 Antimony-125 ur 000 +/-0.152 03!4 (J 145 +1-0 \()8 pCi/g B1smuth*212 U1 000 +/-!DB 2.21 I 01 +(-1 24 pCt/g !3ismuth-214 0.802 +l-0 242 0.194 0.0856 +l-0 251 pCtlg Ce~ium-137 0406 +/-0 144 0. I09 0 0478 *-1-0.148 0.!00 pC1/g Cobalt-60 ti 00075 .../-0.0663 () 136 00569 +/-0.0664 pCt/g Europium-154 u 0 165 +/-0 187 n.429 (l 184 +l-0 202 pCt/g Lead-210 3 71 /-0.987 0.993 0.467 +/-I 04 4.00 pCi/r; Lead-212 0.879 +/-0 ]37 0 156 0.0733 +l-0 168 pCi/g Lead-il4 0.930 -i-/-0 237 0222 0.103 +/-() 25\ pC1lg Pota5S1um-40 f.j 3 -r/-2.24 (} 9{).1 () .140 +/-2.58 pCilg Pr(llactinium-231 Ul ().IJ(I +/~0 752 1.33 0.1>2() +/-0.8\7 p(i/g Radium-226 0 802 +/-0 242 0.194 ().()851* +/-0 25 [ pCilg Radium-228 I 03 +/-0.402 0434 0.187 +/-0 423 pCi!g Thallium-208 0369 +/.() 107 () 104 0.0465 +/-0 ! I! pCrlg Tin-126 lll 0.00 -'-f-0.0.942 0 106 () 0501 +/-00958 pC1/g Rad Ga~ Flaw Proportirrnal Counting GFPC, Gross A-*B, solid "Di)' Weigllt Corrected" Alpha 784 +/-3.45 J 97 1.60 +/-3.81 4 00 pClig JXB7 12'02/ l 5 1420 1525 768 3 Beta 25 6 +/-3. 77 3 05 l 35 +t-S 21 ]{) 0 pCilg !h~fo~lowing_P_~(!P -~~_tl10ds_ w~rc _pc_r,f()rl11~~.

Vlei hod Description Analyst Date Time Prep !latch

                                                                                  ... __ ................................... .

Dry Soil Prep Dry Soil l'rcp GL-RAD-A-021 LVTl l l/10!15 0955 1521927 ~:he.f.ollowf11_g 1.\!J.lllyt_i~_al_M~~l!t,!d_s_~\:eE~..r.erfo_~lll_c~... Method Description ASTM D22\6 (Modified) 2 DOE HASL 300,4.5.2 J/Ga-()1-R 3 EPA 90().0!SW846 93 IOISM 71 !0B Modified Surrogate{fracer Recovery Test Batch ID Recover}*% Acceptable Li111its

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive

                    *Suite 112 Buffalo, New York 14228                                                                        Report Date:         December 17. 2015 Co11tact:        Ms. Laurie Losey Project:         Soil Radioisotopes Client Sample ID:      1.3.Cl                                                             Project:          MJWCOOl 15 Sample !D:             385101007                                                          Clien1 JD:        MJWCOO\

P:ir:tmcter .. .Qu~li.fi.e.r....... _Result .. {P:C..cr.tai1_1h* .. Jvl_J!(. Le TPl' RL.....~:n.1t.~ ... D_F__A11!1l:p_t ___ [)!l~~.!il_llc_)lj\tC~ :\:ltcL Surrogatefl.'racer Recovery Test Batch ID Re~ovcry% Accc1>tabfc Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 * (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York !4228 Report Date: January 20. 20 ! 6 Contact Ms. Laurie: Lose)' Project Soil Radioisotopes Client Sample ID: 1.3.C.2 Project: MJWCOOl 15 Sample ID: 388092013 Cllent lD: MJWCOOl Matrix: Soil Colh'lct Date: 21-0CT-15 Receive Date: 23-D EC -15 Collector: Client

• Moisture: 21.6%

Parameter Le RL . l:'n [t.s....I:>.F.: Analys_t ...1)1_1 le_ Ti.r.nc .. Batch.. :\1t.~ .. Rad Gamma Spec Analysis Gammaspec. Gamma. Solid "Dry Wei1?111 Corrected" Actmium-227 u 0 166 +/-OJI I 0.595 0280 +/-0.321 pCi.lg MJHI 01/18/16 0705 1534020 Antimony-125 u *0.0396 +/*O.l 16 *0203 0.0928 +/.().118 pC1/g Bismuth-2 l2 UI 0 00 +i-107 1 59 0742 +I-I 68 pCi!g Bismuth-214 I 08 +/-0 170 () 152 0.06&9 .../-0.192 pCi/g Ccsium-137 0.482 +1-0 []947 l) 0637 0.0279 +/-0.102 0 JOO pC!lg Cobalt-60 u (I 0129 .,.1-0.0444 0.0907 0 ()393 +1-li 0448 pCi/g f,urcp*um-154 u 0.0122 +/-0 138 (l.268 O.l 18 +/-0. 138 pC1/g LeHd-212 1.07 +/-0 J3B () 126 () 0594 .,./-0 162 pC'ili; Lead-214 I 31 +/-0211 0.388 0.1&8 +/../,) 234 pCi/g Potassmm-40 14.2 f/-1 72 0.877 0.379 +1-2 15 pC!!g Protnct1111um-23 l \JI 0.00. +/-fl 623 l 05 0,+90  :..1.0 632 pC)/g Radium-226 I 03 +/-0.170 0 152 006S9 -+/-0. \92 pC1/g Radiuni-228 . I 02 +/-0 272 0.309 0.138 ~*/-ll.306 pCilg Thalhum-208 0 360 +l-0 093B ti 0771 0.035 .,.f-0.0985 pCi!g Tin-121i lJI 000 +/-0.130 0.209 0 IOI +1-0 \31 pCtlg Th_~ f~!.l<l~~*i!lz. r.i:i:.e..JV!ethods_ w.~.**.c pi:rro~~c_d____ ... Method .Description *Analyst Date "Time Prep Batch

                                                                                                                                       -*-*- . . .. . ..... .... ... - .... . . ...          ***-* ....... - ..... ... . ........ .

DI)' Soil Prep Dry Soil Prep GL-RAD-A-021  !,YTI 12/24f15 U703 1533924 "t.he..f~l~~~v~~g :':\n_i:il~ica_l_l\11~.t~~-~s .~l'~r~..J?.crfoE~l(!~ _.. . ..... .. .. .... .. . ... ... . ...... __ . Method Description DOE HASL 300. 4.5.2 3/Ga--01-R Surrogateffracer Recovery Test Batch JD Recovery% Acceptable Limits

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843} 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: l 5 I!azelwood. Drive Suite 112 Buffalo. New York 14228 Report Date: January 20, 2016

Contact:

Ms. Laurie Losey Project: Soil Radioi5otopcs Client Sample JD: 1.3.C.2 Project: MJWCOOl 15 Sample ID: 3&8092013 Client ID: MJWCOO 1

  .... "  . .......... .. . ........................ --** ....... - . .... ......... ...... .   .. , ............................................ - ......., .. , ................, .. , .. .
 !'a.:a."..1d.~r........ _ .... . . ,quAli~cr ...... -~~c~1:1I~ .. -... l'.nce.rta.i11t.v ...... i>l!)C......L~ ...... -* ~P,l.!                   RL**-*
                                                                                                                                           ............ l;nils      IW r\ni1lvst
                                                                                                                                                          ,. . . .. . . .. .. - ... ~-      .. . . .. Time
                                                                                                                                                                                       . . Dale        ........B1ttch   Mtll.
                                                                                                                                                                                                                , . ........ .

Surrogate!Tr:iccr Recovery Test Butch ID Rccovc~*% Acceptable Limits Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma). L

I GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite l L2 13uffalo, New York 14228 Report Date: January 20. 2016

Contact:

• Ms. Laurie J ,osey Project Soil Radioisotopes Client Sample ID: 1.3.C.1 Project: MJWCOOl 15 Sample ID: 388092003 Client ID: MJWC001 Matrix: Soil Co!lect Date: 21-0CT-15 Receive Date: 23-DEC- l 5 Collector: Client Moisture: 21.6%

Parameter .... <)_uali_(i~r. . RcsuH ___ . J:nc.cr_ta.~11.t:Y ........ MDC Le . ~.Irr... . .. E.~ .....~*_nit~. _DF ..~\n1tl>.:st .... Date. .IJ!l!~ . ~a.~~h. _1\'1!~.'.. G r:ivimctric Solids ASTA-ID 12 J6 % Moisture "As Receivl!d" Mmsture 216 percent LYTI 12i24/l5 0703 1533555 Rail Gamma Spec Analysis Gammaspec, Gamma, Solid "D1:r !Veigf1t Corrected" Actinium-227 U -0.0784 +/-0.231 0.413 0.1% +l-0 234 pCtlg MJHI 12129115 \ 154 1533562 2 Antimony-125 lJ 00254 +/-00997 () 166 0.0782 +/-0 JOO pC1/g Bismutll-212 1.39 +l-0 700 n 852 0.394 +/-0.713 pC1.lg Bismutii-214 0678 +/-0122 (). 114 005:'.l +l-0.134 pCt/g Ccsium-137 0 405 +/-0 067B 0 0658 (I 0306 +1-0 0752 () 100 p('tlg Cobnit-60 U 0.0136 +/-!J.0426 0 0739 00332 +l-0 043 pC11g. l..:uropium-154 U -D.0175 +1-0 121 0.217 ll.098i +l-0 12.l pC1tg Lc~d-212 . *

• I 06 +/.() 104 0.0882 0(142 +/-0.140 pCi/g l.ead-214 0.776 +/-0 142 0.129 00612 +/-0.157 pC11g Potassium-40 15.2 +/-l 34 0.547 0.236 +/-1.R7 pCi/g Protactmium-231 lJ 0.00 +f-0 728 0769 IJ 364 +/-0 762 pC1/g Rarlium-226 0 678 +f-0 122 0l14 0.0531 +l*O 134 pC1lg Radium-228 I 03 +/-0216 () 215 0.0974 +/-0.260 pCi!g Thaltium-208 0.286. +/.() 0695 0 0568 ll.0263 +/-(1.(1735 pCi/g Tm-126 U 0.00 ~i-0\13 0.111 0.0534 +/..{] 115 pCilg Rad Gas Flaw Proportional Counting.

GFPC. Gross A-8. solid "DI')' Ti'eight Corre,*1ed". Alpha 11 I +/-2 15 2.78 I 31 +/-3 06 4 00 pCtlg JXB7 Ol fl 1/16 1859 1534760 3 Beta 212 *-1-1.80 2 19 1.06 +/.J.53 HI Cl pC'1/g.

• T~e- f.nll_~lt\o"i_nA, Pr~p _l\l~~-~~.d.s. 'v4:lr.C:.P.~.r:~or.med .......... _ ... .

 ;\.let hod                   D.escription                                                                   Analyst            Date              Time       Prep Batch
                                                                                         ********-**** --* .......... .

Dry Soil Prep Dry Soil Prep GL*R1\D-A-02 I LYTl 12/24115 0703 1533555 1:h.c f.IJ~ltl_)V_i:rig .A.n_a_~f.ti~~l-~fi:_t~ods_ '~C:r~ pcrfm:n.*_c~ _.. __ ... Method Description ASThl D 2216 (Modified) DOE HASL 300, 4 5.2 3/Ga-01-R 3 EPA 9000.ISW.846 93 IO/SM 71 IOB Modilied Surrogatcffracc .. Recovery Test Batch![) Recovery% Acceptable Limits

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite I 12 Buffalo. New York 14228 Report Date: Januai-y 20, 2016

Contact:

• M~. Lnurie Losey Project: Soil RJldioisolopes Client Sample ID: 1.3.C.2 Project: MJWCOOi 15 Sample ID: 388092003 Client ID: MJWCOOI Parameter Le . ll~~--. Y.*i.its . .D.-1'... :~.!1'.1.1_ys~ .. _D_a_~~..T!!'!e .. ~_:ttc.11 _..l\l,td:.

Surrogate/Tracer Recovery Test Batch ID Reco\*ery% Acceptable Limit~ Notes: TP!J and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.get.com Certificate of Analysis Report Date: December 4. 2015 Company: MJW Corporation Address: 15 Hazelwood Drive Suite I 12 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

• • -*
• H*** *OOOO O*OOO OOOOO*o*****'* 0 H0 . . 0
• Client Sample ID: l.3.C5 Project: MJWC00!15 Sample ID: 385101008 Client ID: MJWCOOl.

Matrix: Soil Collect Date: 2 l-OCT-l5 09:40 Receive Date: 05-NOV-15 Collector: Client Moisture: 39.7% Parameter MDC RL Units Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 39 7 percent L YTI 11/\(}/I S 0955 1521927 Rad Alpha Spec Analysis ASP Plutonium lsotopic, Solid "Dry Weight Corrected" [>lutomum-238 U -0.0042 +/-0 0363 0 084 1 00 pC'1/g HAKB 11/23115 1502 1522517 l f'lutomum-239/240 ll 0 0\47 +/-0 0734 0.147 I 00 pC1!g ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 U 0 0644 +/-0 127 0.225 I OD pc1lg HAKB 1 l/24/15 0851 1522580 Uramum-233i234 0.656 +/-0 320 0.261 I 00 pct.lg Uranium-2351231;i U O 0709 +/-0.121 Cl.106 I 00 pctfg Urnmum-238 0 954 t/-0 367 ll.106 1 on pr:i/g Alphaspec Np237, Solid "D1y Weight Corrected" Neptumwn-237 U -0 146 +/-0 252 0.714 l 00 pCilg HAKB T l/23115 17 fl 1522576 4 Alphaspec Th229 + 228,230.232 Solid "Dry Weight Corrected" Thorium-228 I 40 +/-0 595 CJ.449 I 00 pCrlg HAKfl 11/24/15 11114 1522579 5 Thonum-229 U -0 0406 +/-0 122 ll.344 l 00 pCilg Timrium-230 0 8()3 ../-0.444 0.343 100 pC1lg Thonum-232 0 616 +/-0.381 0.168 1 00 pC1/g Am241, Cm Solid ;'Dry Weight Corrected" Amcncium-241 lJ O 0173 +1-0.0593 011() 1 00 pC1lg HAKB l l/24115 1039 1.522571 6 Curmm-242 U -0.00457 +1-00394 II 0913 t 00 pCilg Curium-2431244 ll -0 0119 +1-0 0359 fLIOl 1 ao pC1/g Cunum-245/246 l: 0 0382 +1-0.0654 () 0573 l (l(I pCilg Liquid Scinl Pu241, Solid Dry Weight Corrected" Plutonium-241 U -\ S2 +/-5.SO 10.l 15.0 pCilg llAKB 11125/15 1739 1522578 7 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" lodine-129 lJ O 130 +/-0 576 (] 92& IUD pC1/g MJHI 12/021!5 1805 1522374 8 Gammaspec, Gamma. Solid "Dry Weight Corrected" Actimum-227 1; 0.18 I -;-/-0 ..293 0 56l! pCtlg RXF2 12/03/15 0827 1522386 9 Antimony-125 l; 0 06D3 +/.() \O\J ll 213 pCilg Ccsium-137 CJ 481 +/-0 110 0.0796 0 100 pCtlg Coball-60 l) -0 00427 +f-Q.0412 0(l7RR pCilg Europium-154 l! * -0.0!18 +/.() 149 0.277 pC1/g Protactimum-~31 U (l 0888 +/-0.620 I (J3 pCilg

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Report Date: December4, 2015

                   *Company:                        MJW Corporation Address:                        15 Hazelwood Drive Suite 112 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

                                                  .. .. ..... .. . -***-*-*- ....... *-**  ..   *-****-**-* .... .

Client Sample ID: 1.3.C5 Project: MJWCOO!l5 Sample ID: 38510100& Client ID: MJWCOO!

                                                                                                                               ... .......... ....
                                                                                                                                                                 ....................

Rad Gamma Spec Analysis

• Gammaspec, Gamma, Solid "D1y Weight Con'Ccted" Radium-226 0 803 +/-0 169 () 156 pC'*lg Ra<lium-228 0 665 +l-ll.382 OJOO pCilg Tm-126 U! 0 00 +/.(). \6J O.IJO pCtlg Rad Gas Flow Proport[onal Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha 9.43 +/-3.61 3.99 400 pCilg JXn7 12f02/l5 1422 1525768 LO Beta 27.0 +1-346 152 ]l),() pCtlg GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 U -0.321 +/-0.8S9 1 76 2 ()() pCi.lg KSDI 12/02/15 1710 1525755 II Rad Liquid Scintiflation Analysis LSC, Tritium Dist, Solid "DI)' Weight Corrected" Tntium t; 2.71 +l-2 71 4.45 I> ()CJ pC1/g TXJI 12!0211 s 1944 1522724 12 Liquid Scint C' l 4, Solid "Dry Weight Corrected" Carbon-14. U -0 459 +/-0 768 1.32 2 00 pC1lg TXJI 12104/15 0357 1522716 13 Liquid Sein.! Tc99, Solid Dry Weight Corrected" Tcchnetium-99 U I 57 +/-2 OIJ 338 5.00 pCilg MY!\11 11/29/15 1349 1522715 14

.I.h~. f.o.ll~.'.N..i"-~.. ~~P...fyie_t!~()9s__>>'..~~~ Eerf~-~.e~.: ......_........ -* Method Description Date Time Prep Batch oi-y soii>rep. ** **** ori sO:ifi>rcii cii.:~R)\b-A-i1i1 .. iiifoh5 (l\155 1521927

GEL LABO RA TORIES LLC

                                                                      *2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4. 2015 Company:                           MJW Corporation Address:                            15 Hazelwood Drive Suite l 12 Buffalo, New York !4228

Contact:

Ms. Laurie Losey

• • -*

Project:

     .... -....................... -

Soil Radioisotopes

                                                    ................... .

Client Sample ID: l .3.C5 Project: MJWCOOI 15 Sample ID: 385101008 Client ID: MJWCOOI .Th.~.~o_l_lo_':"in~ _;\~~lrt_i~al. tvle~_hods_ ~e:_c__p~_~f.?!.n~~d_:__ . _.... .......... .. .... . Jyl~t!.1.c.>'f... . .. . .. . .. ... ... .. ... . Q~,'!~riPti Qll_.... . ......... i\STM D 2216 (Modified) 2 DOE EML HASL-300. Pu-I !-RC Modilkd J DOE EML HASL-300, U-02-RC Modilicd 4 ASTM C 1476-00 Modified 5 DOE EML HASL-300. Th-OJ-RC Mod1Jied 6 DOE EML HASL-300. Am-05-RC Modified 7 DOE EML HASL-300. Pu-1 I-RC Modified 8 DOE EML HASL-300J-Ol Modified 9 DOE HAS\. .100, 4 5 23/Ga-Ol*R lO EPA 900 OiSW846 93 !0ISM 7l IOJ3 Mod1f1cd ll EPA 905.0 Mod1ficdiDOE RP501 Rev 1 Modtfi~d 12 EPA 906.0 Modified l3 EPA EERF C-\)1 Modified 14 DOE EML HASL-300. 'fo*U2-RC' Modified ~.u.rro~at~(f r_~::_e!. ~e::?~e_ry Result Test ............................................................................ ***-** _l\j()n~i[]_~l...... ~_e_cg~e.9'.~ -* _'\c_c~_P.-~(l~~~J~i!:ll.it_s_ Plutonium-242 Tr<.icer ASP Plutomum !sotop1c, Solid "Dry Weight 84.:5 (15%-125%) Corrected" llranium-232 Tracer ASP Uiamurn l~otop1c, Solid "Dry Wc1gh! 42 (15%-125%) Corrected" !Jranium-235/236 Tracer ASP Uranium lsotop1c_ Sohd "Dry Weight 64.9 (15%-125%) Corrected"' Amcricmm-243 Tracer Alphaspcc Np237, Solid "Dry Wc1gln Correcccd" 86.2 (15%-125%) Aclmium-22 7 Tracer Alphaspec Th229 + 228,230.232 Sohd Dry 89.2 (15%-125%) Weight Corrected" Americium-243 Trru::cr Am24 I, C't11 Solid "Dry Wcigln Comx:lcd" 88 3 (15%-125%) Plutomum-242 Tracer Liquid Scmt Pu24 l, Solid Dry Weight Correc1cd 84 ..5 (1.5%-125%) Stronlium Carner Gl'l'C, Sr90, solid "Dry Weight Corrected" 86.7 (25%-l2S%} Tcchnctirn11-99m Tracer L1qu1d Scint Tc99, Solid "Dry Weight Corrc~ted" 94 5 (l5%-125%i Notes: Counting Uncet1ainty is calculated at the 95% confidence level ( 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 .. (843) 556-8171 -www.gel.com Certificate of Analysis Compan>*: MJW Corporation Address: 15 Halclwood Drive Suite 112 Buffo.lo. New York 14228 Report Date; December 17, 2015

Contact:

Ms. Laurie Losey Project: Soil Radioisotor-:s Client Sample ID: l .3.C5 Project: MJWCOOJl5 Sample ID: 385101008 Client lD: MJWCOOI Matrix: Soil Collect Date: 21-0CT-15 Receive Date: 05-NOV-15 Collector: Client Moisture: 39.7% Parameter Result _l..'n.ccrt:ii~.IY. . [\-:I.Dr .... J,.c. . . .... .. IP.t.: .. Gravimetric Solids ASTM D 2216 % Moisl!Jre As Received" Moisture 397 percent LYT! I I/10/1 S 0955 15219i7 Rad Alpha Spec Analysis ASP Pi11to11i11111 Isotopic. Solid "Dry Weight Corrected" Plutonium-238 ll -0 0042 +!-0036.3 (I 084 0 0157 i/-0 0363 l 00 pC1lg HAKB 11123115 1502 1522577 2 Plutomum-239/240 u 0.0147 t/-00734 (J t.17 (J0.171 +l-0 0734 I 00 pC'ilg ASP Ura11i11111 Jsotopic, Solid "Dry 1-f'eight Co1*re~*1ed" llranium-232 lJ 00644 +1-0 127 0225 00853 +l-0 128 l.00 pci/g HAKB 11124115 0851 1522580 3 Uranium-:!331234 0.656 +/-0 320 0.261 00777 +/.() 355 l.Oll pc1/g Urnrnum-2351236 007t)<) t/-0.121 0.106 l)I)[) +(-0 123 1.00 pcilg Uramurn-238 () 954 +1~0 367 O.Hl6 0.00 +f-0.429 I 00 pci/g tflphaspec .Vpi37, Solid "D1:1* TVeight Corrected" N~ptunium-237 ll -0.146 '!-/-0.252 0714 0 241 +1-0252 1 00 pCi!g HAKB 11123115 1711 l 522576 4

  .4.fphaspec Tl1229 ;- 228:230.232 Solid "Dr.i* Weighr Corrected" Thonum-228                                          140          ~l-0 595          t'J.449     (\ \38           +/-0.631            I 00   pC1lg        HAKB 11/24115 1014 1522579      5 Thonum-229                             lJ     -0.04011           +-1-0 122         0 344     () ()876           +.'-0.123           1.00   pCi/g Thonum-230                                        0.803         +l-0 444           0.343     00874              +1-045~             I 00   pCi!g Thonum-232                                        ()616         +/-0.381           O. lfi8        000           +1-0 392            ll\O   pC1/g AmUJ, Cm Solid "Dry Weig/it Corl'ected

Amcncium-24 I u 00173 +/-0 0593 (l.l]O 00299 +1-0 0:593 1.00 pC1/g HAKE l 1124115 1039 152257,l 6 Curium-242 u -0 00457 +1-0.0394 0 0913 00171 +1-0 0395 l 00 pCi/g Cunum-243i244 u -ll.0119 +/-0.0359 0 WI 0 025(> +/-0 0359 \ 00 pCslg Curmm-2451246 0.0382 +1-0Q(,54 00573 0.00 +f-0 0656 l.00 pCilg liquid Seim Pit24 I. Solid "Dry Weight Corrected Plutonium-241 ll -1.82 +/-5.80 10.1 4.92 +/-5.80 IS 0 pCi!g HAKB 11125115 1739 1522578 7 Rad Gamma Spec Ane.lysis Gamma I I 29, Solid "Di:v Weight Comxted" lodme-\29 u 0 130 +/-0 576 0.928 0 4::!8 +l-0 576 100 pCilg MHll 12/02/15 1805 1522374 8 Gammaspec. Gamma, Solid "Di:v Weight Corrected" Actmium-227 ll 0 181 +/-0 293 () 568 () 265 +l-0 305 pCi/g IL'XF2 \2/03/15 0827 1522386 9 Anlmwny- 125 ll 0.0603 +/-0.109 0.213 0.0971 +/.() 112 pC1/g Brnmuth-2 J2 1.39 +/-0.906 I 12 0 499 .../.() 916 pCi!g Bismuth-214 0.803 +/-0 169 0 156 00704 +/-0.181 pCilg Cc~ium-137 0.481 +/-0. l 10 *o.u796 0 0354 +/-0.117 0 100 pC1/g Cobalt-60 lJ -0.00427 +-/.() 0412 0.0788 0.0327 +/-0.0412 pC!/g Europmm-154 ll -00118 +l-0 149 0.277 0.120 */-0.149 pCilg Lcad-212 0.928 +/-0 127 0 112 0 0522 +/-0 148 pCt!g Lcad-214 l OS +/-0 188 0 .l84 (J 185 +f-0 :W6 pCs/g

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJ W Corporation Address: 15 Hazelwoml Drive Suite! !2 Buffalo, New York 14228 Report Date: . December 17, 20 l5

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: l.3.C5 Project: MJWCOOJ15 Sample ID: 385101008 Client ID: MJWCOOI Parameter Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "D1:v Weigli! C01*1*ected" Potassium-40 14.2 +/-l.66 0 8C>7 0 336 +/-2.to pC1tg Pmtnctinmm-23 l U 0.0888 +/-0.620 1.03 ll.475 +/-0 621 pCrlg Radium*226 0.803 t/-(l.J 69 0 15(1 () 0704 +l-0 181 pC1lg Radium-22.8 0.665 +l-0 382 030() (J 132 +1-U 393 pC1tg Thallium-208 0.354 +/-0.0817 !Ui70ol [J.(l312 ~/-0 0867 pCi/g Tin-126 U! 000 +/-0.163 0 130 ll.0612 +/-0.165 pC1 11r Rl'ld Gas Flow Proportional Counting M* Bem GFPC.. Gross A-'B. solid "Dry Weig/rt Corrected" 9~

                                                             .27.0
                                                                           +1-3 61
                                                                           +1-3 .i6 3 99 2 52 16!

I 12

                                                                                                                      +/-4.06
                                                                                                                      +/-5.28 400 10 u pCtfg pCi/g JXB7           l2i02f\5 1422 1525768                  IO GFPC. Sr90. solid "Dr,\' Weight Correc1ed" Strontium-90                                  U           -0 321          +/-0.889         1 76       0 7S3          +/-0.889             200        pCilg                   KSDJ            12102115 1710 1525755                  11 Rad Liquid Scintillation Analysis LSC. Tritium Dis1, Solid "Dry Weig/rt Corrected" Tritium                                                        2 71         +1-171          4 45          1.93         *H-2 71              6(1(1     pC'1lg                   TXJI           \2/02/15 1944              1522724     12 liquid Seim Cl 4. Solid "DI')' Weig/It Corrected" Carbon-14                                      U           -0.459                           1.32       0.651          +/-0.768              2.00      pCt/g                    TXJ1           \2i04/\5 0357              1522716     13 liquid Scint Tc99. Solid "Dry WeiRhl Corrected" Techncuurn-99                                  U               1.57         +l-200          3 38          I 63         +1-2 01              5.00      pCi/g                    MYM 11/29115 1349 1522715                             \4 I

Th~-~~l~~~v.i~ILP.F~I? ~lt:l~?~S.:'.cr~. pcz:f~n_r1~.~ . . ............. *-**. .............. . .. ..... -*-**-**-*******"'"'

~1ethod                 Description                                                                  Analyst               Oatc                     Time            Prep B:itch
                                                                                                                         ........ -* .. - .............. **-* *-. -*- *-*********** -** *-**--*-**** -* ... ................. *****

Dry Soil Prep DI}' Sml Prep GL-RJ\D-A-02 l LYTI I 1/l0Jt5 0955 1521927 }11.~ fol'.?l\"~ng_,\n~!Y.tic_al __ !\*~-~th._o~~- l'er~ pl)r_f~rm.~d- _ Method Description ASTM D 2216 (Modified) 2 OOE EML HASLoJOO. Pu-11-RC Modified 3 DOE EML l!ASL-300, U-02-RC Modifi~d 4 ASTM C 1476-00 Modilicd 5 DOE EML HASL-3UU, Th-CH-RC Modified (l DOE E"ML HASL-300. Am-05-RC Modified 7 DOE EML HASL-300, Pu-11-RC Modified 8 DOE EML HASl.-300.l*O I Modified 9 DOE HASL 30(), 4 5 2.3/Ga-01-R 10 EPA 900.0.iSW846 93!0iSM 71 IOB Modified II EPA 905.0 Modified/DOE RP50\ Rev 1 Modified 12 EPA 9{)6 0 Modified 13 EPA f.ERF C-0 I Modified

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - {843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW C'orp()ration Address: 15 Hazelwood Drive Suite 112 Buffalo. New York 14228 Report Date: December 17. 2015

Contact:

l\*fa. Laurie Losey Project: Soil RadiC1isotopes Client Sample ID: l.3.C5 Project: MJWCOOl 15 Sample ID: 38510!008 Client ID: MJWCOOI Parnmeter J.c 14 DOE El\IL HASL-300, Tc-02-RC' Modified Sun*ogatcfl"racer Recovery Test Batch ID Recovery% Acceptable Limits Plutonhnn-242 Tracer ASP Plutonium Isotopic. Solid "DI}* Weight Corrected" 1522577 84.5 ( 15%-125%) llranium-232 Trac~r AS!' Uranium Isotopic. Solid "Dry Weight Com.>c!ed" 1522580 42 (15%-125%) Urnniurn-235/236 Tracer ASP Uranium Isotopic. Solid "Dry Weight Corrected" 1522580 64.9 (15%-125%) Americium-243 Tracer Alphaspec Np237. Solid "Dry Weight Corrected" 1522576 86.2 (15%-125%) Actinium-227 Trnccr Alphaspcc Th229 + 228,230,232 Solid "Dry Weight Corrected" 1522579 89.2 (15%-125%} Amcricium-243 Tracer Am24 L Cm Solid "Dry Weight Corrected" 1522571 88.3 (15%-125%) Plutonium-242 Tracer Liquid Sein! Pu24 l. Solid "Di) Weight Corrected" 1522578 84.5 (15%-125%) Strontium Carrier GFPC, Sr90, solid "Dry Weight Corrected" 1525755 86.7 (25%-125%) Technelium-99m Tracer Liquid Scint Tc99. Solid "DI)' Weight Corrected" 1522715 94.5 (15%-125%} Notes:* TPU and Counting Uncertainty are calculated at the 95% confidence level { 1.96-sigma).

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) ~56-8171 -www.geLcom Certificate of Analysis Report Date: December 4, 2015 Company: MJW Corporation Address:  ! 5 Hazelwood Drive Suite 112 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

                                             ..... -**       .

Client Sample ID: 1.3.C6 Project: MJWCOOll5 Sample ID: 385101009 Client JD: MJWCOOJ

• Matrix: Soil Collect Date: 21-0CT-!5 09:55 Receive Date: 05-NOV-15 Collector; Client Moisture: 23.6%

Paramet~r, ................ __ ___9ua!i~~r_ Result UncMainty lVIDC

                                                                ****-**** ***-*-** **-** .... ***-****-* **********.
                                                                                                                     .~L. ..... *- ______l)_n_it~ .... _... !?~- Ana._ly_s~. _J::)ate    Time Batch Method Gravimetric Solids ASTM D 22 l 6 % Moisture "As Received" Moisture                                                   23.6                                                                         percent                    LYTl     11/I0/15    0955 1521927 Rad Alpha Spec Analysis ASP Plutonium Isotopic. Solid "Dry Weight Corrected" Plutomum-238                               lJ         0.00979            . +/-0 0544                    0 !04             I !HJ                                    UAKB 11/23/15        1502 1522577     2 Ptutonirnn-2391240                         U          0.00677              +/-U 0799                    0 168             I 00 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232                                lJ           0.0473.              +/-0.121                   fJ 222            I 00             pci!g                   HAKB l 1124i15       0851  1522580    3 Uranium-2331234                                          0 799*               +1-0 30 I                 0 214             I 00             pcilg IJranmm-2351236                            U            0 0469             /-0 0921                  () 128            I 00             pc1lg Urnnium-238                                                 I 14              +/-0 345                0.0796              I O!J            pc1lg Alphaspec Np237, Solid "Dry Weight Corrected" Ncptunium-237                              U          -0 0342                +/-0 236                   0 575             I 00            pCifg                    HAKB 11123115        !711 1522576     4 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thomim-228                                               0 984                +/-0 482                  0 395             I 00            pC1/g                    HAKB 11124115        IQl4 1522579     5 Thormm-229                                 U             0 131                +/-0 207                  0 287             l.Q{)           pC1lg Thormm-230                                                  l.lti             +!-{l.498                  0 280            I 00            pCi!g Thorium-232                                              0.979                +1-0.452                   0 155            I 00            pC'1/g Am241,.Cm Solid "Dry Weight Con*ected" t\mencium-241                              U            0.0315                +/-0 062                (}.0859             I 00            pC1lg                    HAKB 11124115        1039 1522571     6 C11rium-242                                U               0 00             +/-0 0412                 00613               1.00             pC'1!g Cunum-24 3/244                              U         0 00921               +/-0. 0512                0 098l              I 00             pCt/g.

Curium-2451246 U 0.0361 +/-D 0709 ()()'}83 I 00 pC1/g Liquid Scint Pu241. Solid "Dry Weight Corrected" Plutonmm:241 lJ -2 07 +/*6 40 11 2 150 pCi/g llAKB 11125115 \840 1522578 7 Rad Gamma Spec Analysis Gnmma I129, Solid "Dry Weight Corrected" lodine-129 U 0.214 +/-0.383 0.76') I 00 pCi/g MHll J2i02/15 1806 !522374 8 Gammaspec, Gamma. Solid "Dry Weight Con*ected" Actmium-227 l! -0.478 +/-0 4M 0 775 pCtlg R.XF2 \2i0:>/l 5 0828 1522386 9 Antimony-125 U 0 0263 * +/-0 202 0 361) p('Jlg Cesium-137 O 357 -ti-0. \22 0178 !l 100 pC'ilg Cobalt-60 U -0 0195 t/-(J.081<1 () 153. µCtlg Europium- I 54 U co ()()356 +/-0 241 O46B pCt!~ Prolactinium-231 lJ 0 80 I +/-0 980 I 81 pC1lg

GEL LA BORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 2015 Company : MJW Corporation Address : 15 Hazelwood Drive Suite 112 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

                  **fi*******-** .............. ,. **-*** ... ******** ........                  ............. .

Client Sample ID: l .3.C6 Project: MJWC00! 15 Sample ID: 385101009 Client ID: MJWCOOl Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Dl)* Weight Corrected" Radmm-226 I .08 +/-0 289 () 255 pCi/g Radium-228 0.891 +1-0.403 0 526 pCilg Tin-1215 U 0 143 +/.() 185 0 177 pC1/g Rad Gas Flow Proportional Counting GFPC. Gross AiB, solid "Dry Weight Corrected" Alpha 7 80 +/-3 22 3.91 4.00 pCi/g JXB7 12103115 123<> 1:\25768 lO Beta 18 3 +r-2 99 2.69 100 pC1/g GFPC, Sr90, solid "Dry Weight Corrected" Stronuum-90 U -0 122 -+*l-0 65'1 [ 34 200 pCi!!_! KSOI 12/02il5 1712 1525755 II Rad Liquid Scintillation Analysis LSC. Tritium Dist, Solid "Dry Weight Corrected" Tritium lJ I 95 +/-2.00 3.30 6.00 pC1/g TXJ! 121()2/15 2031 1522724 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 ll -0 833 +/-0.891 1.55 2.UO pC1!g nm 12104r15 0520 1s2271r, 13 Liquid Scint Tc99, Solid "Dry Weight Corrected" Tcchneuum-99 ll 1 60 +/-1.76 2 \15 5.00 pCitg MYMI 11129115 1416 1522715 14 T.h.~ _fo~!~_\\:i!l~ ..P.£ee. ~"..~~-{)~~-'~~e _pert:~1:m~~: ****- .... Method Description Analyst Date Time Pl'ep Batch Dry-Soii f:ire*;i* ...... '[:i[y's{i1f'Pi-~j:iGI ;~RAD~A~02T . *******-******-****** **y:~fc-- i Wib/15 . ... . .. 0955 1521927

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report Date: December 4, 20 I5 Company; MJW Corporation Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228

Contact:

Ms. Laurie Losey Project: Soil Radioisotopes

            *-***--* *-* ....... *-. .. . ........... - . - ........ *******. .. .. ... . .                                                           ...........        ,.

Client Sample ID: l .3.C6 Project: MJWCOOll5 Sample JD: 385101009 Client JD: MJWCOOI The ~°.I to:vi_n~ r.\n_alY.tical M~~~?~.5.. ~e_re_ye_r~?~!~:~.:..... . .. " ......... *****-** .. .. . . - .... -**-**** .. rYl.~tJ:io.cJ.... . ....... .... .P.~~~r.ipti<:JI). ...... ... .... .. .. .... . .. ...... __ ........ _.. *-- .. t.ng[y~t. f ()~ll)l~IJt~- .................... -* *- ....... _ .......... __ r\STM D 2216 (Modified) 2 DOE EML !-!ASL-JOO, Pu-l 1-RC Modified 3 DOE EML HASL-300. tJ-02-RC Modified 4 ASTM C 14 76-00 Modi ficd 5 DOE EML J-IASL-300, *111-0l-RC' Modified 6 OOE EML HASL-300, Am-05-RC" Modilicd 7 DOE EML HASL-300. Pu-11-RC Modified 8 DOB EML HASL-300,1-01 Modified 9 DOE HASL JOO. 4 5.2 JIGn-01-R 10 EPA 900.0iSW8% 93 IO!SM 71 lOB ~fodified II EPA 905 0 Mod11icd/OOE RP50l Rev 1 Mod11led 12 EPA 906.0 Mod1fie<l 13 EPA EERF C-01 Modified 14 DOE EML HASL-300, Tc-02-RC Modilfod ~1:1.'..'..()_~~~:/Tr~_ce~* -~~-~('.)~'.Cl)' . Test Result Pl1aonium-242 Tracer ASP Plutonium Isotopic. Solid Dty Weight 76.6 (15%-125%) Corrected" Uranium-232 Tracer ASP Uranium Isotopic. Sohd Dry Weight 55.9 (IS%-125%} Corrected" Uranium-235/236 Tracer ASP Uranium Isotopic, Solid "IJry We1~11 654 (15%-125%) Corrected" Amcncium-243 Tracer Alphaspec Np237, S<ll1d "OT)* Weight Corrected' 74.8 (15%-125%) Actimum-227 Tracer A!phaspec Th229 + 228.230,232 Solid Dry 88 6 (15%-125%) Weight Correct~d" Amencmm-.243 Tracer Am241,Cm Solid "Dry Weight Corrected 86.4 {15%-125%) Plutomum-242 Tracer Liquid Semi Pu24I, Solid "Dry W~ig.hl Corrected" 76 6 (15%-125%) Strontium C<1mer GFPC', Sr90, ~olid "Dry Weight Corrected" 88 9 {25%-125%) Tcclme!lum-99m Tr~cer L1qmd Scint Tc99, Solid "Dlj' Weight Corrected" 98.4 (!5%-125%) Notes; Counting Uncertainty is calculated at the 95% confidence !eve! ( 1.96-sigma). _j

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: * .! 5 Tfozc:lwood Drive Snite I 12 Bu/T[l)O. New York 14228 Report Date: December 17, 2015

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Ms. La~rie Lo~ey Project: Soil Radioisotopes Client Sample ID: I .3.C6 Project: MJWCOOl 15 Sample ID: 38510 I 009 Client ID: MJWCOOI Matrix: Soil Collect Date; 21-0CT-!5 Receive Date: 05-NOV-15 Collector: Client Moisture: 23.6% Parameter ................... 911~1m.e.~ ..........~i:sult .... ~:n_ccr~?-i!ltY.. ............. t\lDC_, .......Le. R~~... .l 'nits__ ..O..F.. ..~.1~a.IY.SI ... ~.li~l!...!ipc Bate~ . .:vi Id... Gravimetric Solids ASTA!/ D 2216 % Mois1ure "As Received" Moisture 23.6 percent LYTl l \IJOil5 0955 1521927 Rod Alpha Spec Analysis ASP Plutonium Isotopic. Solid "D1:r Weigh/ Corrected" Plutomum-238 lJ 0 00979 +/-0.0544 0 104 0.0239 +/-00545 1.00 rC1lg HAKB 11123115 1502 1522577 2 Plutm1ium-23W240 U 0 00677 +/-0 0799 0 168 0 056 +!-0 0799 1.00 pCi/g ASP Uranium Isotopic. Solid "Dry Weight Corrected" Uronium-232 U (} ()473 +/-ll 121 0222 0 0&21 +/-0121 1.00 pc1/g 1-!AKB 11124115 0851 1522580 3 Un:mfom-2331134 0.799 +f.() 30 I 0214 0.0674 +/-0 347 1.00 pci/g llromum-2351236 00469 +/-[) 0921 0.128 00239 +/-0.0927 l.00 pc1/g Uranium-238 l 14 .,./.() 345 00796 000 +/-0.424 1 00 pc1.lg Alplmspec Xp237. Solid "Dr)' Weight Correaed" Neptunium-237 ti -0.0342 +/-0.236 0.575 0.171 +/-0 236 1.00 pCilg HAKB I l123/l5 1711 1522576 Alphaspec Th229 ~ 2:!8,230.232 Solid "D1y Weight Corrected" Thorium-228 0.9&4 *l-IH&2 0.395 0 117 +1-0505 I 00 pC1/g 1-!AKB I J/24/l5 1014 1522579 Thonum-229 0 13 l +l-0 207 0 2&7 ()0657 +/-0208 1.no pCi/g Thormm-230 t.16 +/-l! 498 0 2~6 0.0656 +1-0 527 1 00 pCiig Thorium-232 0.979 /-[} 452 () 155 000 +/-(}475 l.00 pCi/g A11124 l. Cm Solid "Dry Weight Corrected" Amenciurn-241 0.0315 +l-0 062 0 0859 0 016.1 +1-0.0621 1.00 pCi/g HAKB 11/24115 .1039 1522571 6 Curi u m-242 000 +/-0.0412 0.0613 000 +l-0 0413  !.00 pCi/g Curium-2431244 ti 0.00921 +/-0.0512 0.0981 () 0225 +/-0 0512 1.00 pC1lg Curium-2451246 0 0361 +!-O.o709 0.()*)&3 00184 +/.()()711 100 pC1lg liquid Sein/ Pu:.!41. Solid "Dry Weifdll Con*ected" Plutomum-24l lJ -2.07 +/-6..JO 11 2 H3 +/-6 40 150 pCilg HA.KB ll/25115 1840 1522578 Rall Camma Spec Analysis Gamma 1129. Solid "Dry Weight Corrected" !odinc-129 ll 0.214 +/-ll.383 0 769 0 345 +/-0396 1.00 pCUg MJH I 12102115 1806 1521374 8 Gammaspec. Gamma. Solid "Dry Weight Corrected Acunium-227 ll -0.478 +f-0 464 0 775 () 355 +/-0.517 pCi/g RXF2 12i03/\5 0828 1522386 9 /\ntimony-125 U 1).0263 +f-0.202 !1369 IJ. !69 +/-0 202 pC'i/g Bismuln-212 lI 0.725 +/-I 19 2 35 1 07 +f-1 23 pCi/g Bismu(h-214 I 08 +/-0.289 0.255 () 114 t-/-0 303 pC1/g Cesium-137 0 357 +/-0.122 0.178 IJ.0812 +/-0 126 O. lOO pCi/g Coba!t-60 U -0.0195 +/-00816 0 153 lUl64 +1-0.0821 pC1/g Europium-154 U -0 00356 +/-0.241 0.468 0 200 ~1-0 241 pCi/g Lcad-212 I 34 +/-0. 197 (} 181 l) 0839 't-/-0'236 pC1/g Lcud-214 l.09 +/-0.363 0 5SO 0 279 -rl-0 374 pCiig

GEL LA BORA TORIES LLC 2040 Savage Road Charleston SC 29407-(843) 556-8171 -www.gel.com Certificate of Analysis Company: MJ\V Corporntion Address: 15 Ha:zelwoocl Drive Suite 112 Buffalo, New York 14228 Report Date: December 17. 20 LS

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Ms. Laurie Losey Project: Soil Radioisotopes Client Sample JD: l.3.C6 Project: MJWC001 l5 Sample ID: 385101009 Client ID: MJWCOO! 1':1n1metcr. ................... Qu~_lifi~r. ***- ... ~c_s11I_t___ ... l)1se~!li.!1tV **- ... :VJ.I_).( ........ l.:C: ... . **-* *******-* Tl'F.. **-**-*** Rad Gamma Spee Annl)'sis Gammaspec. Gamma. Solid "Dry Weight CorrecNd Potassium-.40 I3 9 +/-227 1.05 0 402 +/-2.5(;> pCi/g Piatactmium-23! lJ 0 80! +/-0 980 I.St . 0 841 +1-1.06 pC1/g Radium-226 1.08 +/-0.28'1 0.255 0.114 +/-0 303 pC1fg Radmm-228 0.892 +1-0403 0 526 0.229 +/-0415 pCitg Tlmllnun-208 0381 +l-0168 0 131 00584 t-1-0 171 pC1/g Tin-126 UI 0 00 +/.() 185 ll.177 00839 +/-0 185 p('ilg Rat! Gos Flow Proportional Cou11ti11g GPPC. Gross A.* B, solid "Dry Weigltr Corrected" Alpha 7.80 +!-3 22 3.91 1 63 +/-3.56 4 OU pCiig JXl37 12/03!15 1234 1525768 10 Beta 18 3 -+*/-2 99 2 69 \ 20 +/-393 10.0 pC'i/g GFPC. Si*9fJ. solid "D1:i* Weight Corrected" Stromium-90 ll -0.122 +/-0 659 I 34 0.573 +/-0 660 2HO pCifg KSDI I 2i02/l 5 1712 152.5755 II Rad Lic111il.I Scintillation Analysis LSC. Triti11m Dis/, Solid "D1:v Weight f'orracted" Triuum I 95 +/-2.llO 3 30 l 44 +/-2.00 6.00 pCl/g TXJ! 12/02/15 2031 \522724 12 Liquid Seim C/4. Solid "D1:r Weight Corrected" Carbon-14 U -0 833 +/.()~<)\ 1 55 o 1r,2 +i-0.891 2.00 pCifg TXJI I21lW15 0520 1522716 13 Liquid Sein/ Tc99, Solid "D1J-* Wf!ighl Con*ec/ed" Technetium-99 1.60 +l-l.76 2.95 1.42 +1-1 77 5.0(J pCi/g MYM 11129/15 1'116 15227!5 14 I Th.~ (oll!J"'.!ll:g~rcp_~l~tl!o~~ \V.f.!~e.11~rfor111e.d_. . ...... ... **- .......... .... -* *- ....... *****- ... ***** ..... ...... -* ........ .. Method Oescriptio11 Analyst "Date Time Prep Batd1

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Dry Soil Piep Dry Sml Prep GL-RAD-A-021 LYTI I J/J0/15 0955 1521927 Tl1c_ f(}_l~o":i.n_g_:~?.~ly~~cal l\*lt~t~_c!~~- ~~-c!:~ _11crfor111e_q Method Description ASTM D 2216 (Modified) 2 DOE EML HASL-300, Pu-11-RC Modified 3 DOE EML HASL-300, U-02-RC Modified ASTM C 1476-00 Mod1tied 5 DOE EMI. HASL-300, Th-01-RC Modified 6 DOE EML l IASL-300, Am-05-RC Modified 7 DOE liML HASl.-300, Pu-11-RC Modified 8 DOE EMLJ!ASL-300,1-01 Mollified 9 DOE HASL 300, 4 5.2 Ji<la-01-R 10 EPA 900 O.'SW84G 93 lOiSM 71 \OB IV!od1ficd II EPA 905 0 Mod1licd!DOE RP501 Rev l Mod1fi~d 12 EPA 906 0 Modified 13 EPA EERF C-01 Modified

.- 1 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: MJW Corporation Address: 15 Hazelwood Drive Suite 112 13u1Talo, New York 14228 Reporl Date: December 17, 20 l S

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Ms. Laurie Losey Project: Soil Radioisotopes Client Sample lD: 1.3 .C6 Project: MJWCOO! 15 Sample ID: 385!0J009 Client ID: MJWCOO! P:m1mcter .. *-**** _....... 9.ll:tl!fl~E. ***- ___I~c~ull ~!11~er:~a,i!}ty .:\IDC Le 14 DOE EML llASL-300. T,-02-RC Mod1fieJ Surrogate{fraeer Recovery TesI Batch JD Rcc1n*ery% AccertabJc Limits

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Plutonium-242 Tmccr ASP Plutcmium Isotopic. Solid "Dry Weight Corrected" t522'.i77 76.6 (15%-125%) lJranium-232 Tracer ASP Uranium Isotopic. Solid "Dry Weight Corrected" 1522580 55.9 (15%-125%) 1522580 65.4 (15%-125%) lJranium-235/236 Tracer ., ASP Uranium Isotopic, Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspcc Np237, Solid "!Jr)' Weight Corrected" 152257fr 74.8 Cl 5%-125'lol Actiniuin-227 Tracer Alphaspec Th229 + 228.230,232 Solid "Dry Weight Corrected" !522579 88.6 05%-125%) A1m:rici11m*243 Tracer i\m24l. Cm Solid "Dry Weight Corrected 1522571 86.4 (15%-125%) Plutmiium-242 Tracer Liquid Scint Pu24 l. Solid "Dry Weight Corrected" 1522578 76.6 (! 5%-125~0) Strontium Carrier GFPC. Sr90, solid "Dry Weight Corrected" 1525755 88.9 (25%-125%) Tcchnetiurn-99m Tracer Liquid Scint Tc99. Solid "D1y Weight Corrected 1522715 98.4 (15%-125~'<.) Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level ( 1.96-sigma).}}