ML20207B766
| ML20207B766 | |
| Person / Time | |
|---|---|
| Site: | 07003073 |
| Issue date: | 12/29/1997 |
| From: | External (Affiliation Not Assigned) |
| To: | |
| Shared Package | |
| ML20207B577 | List:
|
| References | |
| NUDOCS 9903080232 | |
| Download: ML20207B766 (27) | |
Text
.
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THERMO NUtech mt rw Amaxan Hwy NE Atuguergue, NM 87109 ISOS 345 3461 fus(505) 761-5410 Kerr McGee Corp. Data Package Work Order # 97 10-277I
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THERMO NUTECH KERR MCGEE SDG/Ver 9710277I Client Kerr McGee Contact Marv Kamoss Contract Shionina #971022212 i
Case no I
SUMMARY
DATA SECTION TABLE OF C0NTENTS Data Sheets 1
Method Blanks 2
Lab Control Samples 3
Duplicates 4
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S DC/Ver sion 9710277T Client /Caso no Ferr McGee Contact Mary Famous Contract Shippino 9971022212 bMle]i nv47 q l
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+%.i Lab sample id 9710277-09 Client sample id CU3-41-011 Dept sample id Location / Matrix WATER Received 10/24/97 Collected / Volume / Basis 10/20/97 16:00 4163 ML t moisture Custody /SAS no/ Level l
l RESULT 2e ERR NDA RDL QUALI-ANALYTE CAS 50 pC1/1 (TOTAL) pC1/1 pCi/1 FIERS TEST l
i Gross Alpha 33 15 14' GA Gross Beta 25 10 14 GB Radium 228 4.3 2.0 2.8 3.0 RA28 Radium 226 2.2 0.36 0.11 0.50 R226 Uranium 233/234 2.6 0.34 0.062 0.10 8
U j
Uranium 235 0.10 0.050 0.038 U
Uranium 238 1.6 0.24 0.048 0.10 U
Thorium 228 2s 1 0.29 0.11 TH Thorium 230 1.2 0.19 0.054 0.10 TH Thorium 232 1.3 0.20 0.038 0.10 TH TEST PLABCERT SUFFIE SY1BLD ANALTERD BY KETROD RE FE RENCE GA 100 11/17/97 FP EPA-600 900.0 GB 100 11/17/97 EP EPA-6u0 900.0 RA28 80 12/09/97 EP EPA, 1980b R226 79 12/19/97 KP EPA 1980, 903.1 U
93 12/04/97 NJ DOE 1990, HASL-300 U-02 TH 83 12/04/97 NJ LANL 1986, ER200 Lab id HUTFCH ABO Protocol -
DATA SHEETS Version 1 Page 1 Form DVD-DS SUNNARY DATA SECTION Version 3.08 Page 1 Report date 12/29/97
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9711033-02 method Blank METHOD BLANK SDC/ Version 97102771 Client /Caso no Ferr McGee Contact Mary Famoes Contract Shippina 9971022212 Lab sample id 9711033-02 Client sample id Method Blank Dept sample id Material /Matfix WATER
% moisture SAS no i
RESULT 20 ERR NDA RDL QUALI-ANALYTE CAS 50 PC1/1 (TOTAL) pC1/1 pC1/1 FIERS TEST Gross Alpha
=0.15 1.3 2.6 U
CA cross Beta 0.037 1.4 2.5 U
CB Radium 228
-1.2 0.51 0.95 3.0 U
RA28 Radium 226 0.080 0.066 0.11 0.50 U
R226 Uranium 233/234 0.047 0.030 0.029 0.10 J
U Uranium 235
-0.008 0.016 0.043 U
U Uranium 238 0.012 0.014 0.011 0.10 J
U Thorium 228 0.030 0.011 0.11 UK TH Thorium 230
'0.007 0.026 0.049 0.10 U
TH Thorium 232 0.007 0.015 0.027 0.10 U
TH TEST PLABCBET SUFFII 8 YIELD ANALTEED BY KETEOD RE FE RENCE GA 100 11/17/97 KP EPA-600 900.0 GB 100 11/17/97 KP EPA-600 900.0 RA28 87 12/09/97 KP EPA, 1980b l
R226 89 12/19/97 KP EPA 1980, 903.1 U
89 12/04/97 NJ DOE 1990, HASL-300 U-02 TH 67 12/05/97 NJ LANL 1986 ER200 l
Lab id NUTECH ABO Protocol -
KETEOD Bt.AERS Version 1 Page 1 Form DVD-DS SUMKARY DATA SECTION Version 3.08 Page 2 Report date 12/29/97 l
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THERM 3 CUTDCE 6
xBRA meaEE
'9711033-02 ~
Imb Coetzel sample.
LAB CONTROL SAMPLE SD3/ Version 9710277T Client / Case no serr McGee Contact Mary samoso Contract shinoina #971022212 Lab sample id 9711033-03 Client sample id Lab control samole Dept sample id Material / Matrix WAMR._
t moisture SAs no I
RESULT 2e 3RR 3Enh RDL QUALI-ADDED 2o ERR RSC 3e 1 Jets PR050CuL ANALTTE pC1/1 (20EAL) pC1/1 pCi/1 FIERS TEST pCi/1 pCi/1 (10EhL) LIMITS cross Alpha 100 24
- 2.0 GA 75.2 2.3 133 52-140 Cross Seta 110 18 2.0 GB 99.1 4.5 Ill 72-128 Radium 220 15 3.1 0.84 3.0 X
RA2e 19.0 0.82 79 75-125 Radium 226 14 2.1 0.079 0.50 R226 11.9 1.1 110 70-130 Uranium 233/234 9.4 0.98 0.052 0.10 0
9.71 0.07 97 80-120 Uranium 235 0.41 0.094 0.040 U
Uranium 238 9.9 1.0 0.012 0.10 B
U 9.71 0.87 102 00-120 Thorium 22B 0.031 0.062 0.11 U
T5 Thorium 230
'4.9 0.54 0.031 8.10 T5 5.18 0.22 95 03-117 i
Thorium 232
-0.026 0.021 0.052 0.10 U
TB 1
l sur-Trzra j
TEST PLANCENT FII t ANALTERD BY METBOD RzFERENCE GA 100 11/17/97 KP EPA-600 900.0 GB 100 11/17/97 KP EPA-600 900.0 RA20 28 12/09/97 KP EPA, 1940b I
R226 et 12/19/97 EP EPA 1980, 903.1 U
84 12/04/97 NJ DOE 1990, RAEL-300 U-02 TE 87 12/05/97 NJ IANL 1986, ER200 l
Lab id NUTECR ABQ Protocol -
t LAB CONTROL SAMPLES Version 1 Page 1 Form DVD-trS l
SUMMARY
DATA SECTION Version 3.06 Page 3 Report date 12/29/97 I.
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THERMO NUTECH EERm McGER l
9711033'.01 CU3 41 003.
DUPLICATE I
SDG/ Version 97102771 Client /Caso no Kerr McGee Contact Mary Ramoes contract Shinoing #971022212 DUPLICATE ORIGIEAL Lab esaple id 9711033-01 Lab sample id 9710271 01 Client sample id cu3-41 003 Dept sample id Dept sample id Incation/Matria WATER cli:nt samp id Received 10/24/97 Collected / Volume /Laele 10/20/97 13:00 4145 ea, t moistute t moisture custody /SAS no/ Level DUPLICATE 2e ERA gen RDL QUALI-ORIGINAL 2e ERA ash QUALI-RPD So DER ANALTTE pC1/1 (TURAL) pC1/1 pC1/1 FIERS TEST pCi/1 (total) pCi/1 FIERS t
ST/T e
Drcaium 233/234 4.4 0.54 0.064 0.10 U
5.9 0.63 0.041 8
21 23 2.6 Ursaium 235 0.077 0.040 0.033 U
0.33 0.046 0.010 51 89 1.7 UrInium 238 2.6 0.23 0.055 0.10 U
3.9 0.44 0.041 J
26 M Thirium 220 0.60 0.12 0.000 TE 0.44 0.11 0.061 4
37 0.5 Thorium 230 0.33 0.072 0.032 0.10 TE 0.30 0.065 0.026 10 46 0.6 Thirium 232 0.55 0.098 0.022 0.10 TE 0.54 0.094 0.020 2
37 0.1 i
DUPLICATE SUF= TIEID ORIGINAL SUF-YIIIb 1TST P!JWCIET FIE 4 ANALTIED BY FIAseCERT FII 4
ANAL 15ED BY METWOD REFERENCE U
79 12/04/97 NJ 98 12/03/97 NJ DOE 1990, EASL-300 U-C2 TE 89 12/05/97 NJ 89 12/04/97 NJ LANL 1986, ER200 Lab ad NUTECN ABO l
Protocol -
DUPLICATIS Vereson 1 Page 1 Form DVD-DUP SUMetARY DATA SECTION Version 3.09 Page 4 Report date 12/29/97
f' THERMS NUTECH EERR meaEE
< 9711031-01.-
CU3 41 008 DUPLICATE SDG/ Version 97102771 Client / Case no Ferr McGee contact Mary Famees contract shiocino #97102??12 DUPLIt. ATE ORIGIMAL Lab sample id 9711033 01 Lab semple id 9710277-06 Client sample id cul-41-Ooe Dept sample id Dept sample id Location / Matrix WATER Clitat samp id Received 10/24/97 Collected / volume /Sasio 10/20/97 15:00 4261 ML t moisture 4 moisture Custody /SAS no/Lovel i
1 i
DUPLICATE 2a ERR 8Eh4 RDL QUALI-ORIGINAL 2e ERR 8Eh4 QUALI. RPO 30 DER AEALYTE pC1/1 (TwfAL) pCi/1 pCi/1 FIERS TEST Ki/1 (TUFAL)
PC1/1 FIERS 4
TUF o
Radium 226 0.93-0.10 0.13 0.50 R226 1.3 0.22 0.095 33 30 2.6 DUPLICATE SUF= TIE!D ORIGINAL SUF-TIEID TBET PLANCERT FIE t ANALYSED BY FIANCERT I.1 4. 4ALf1ED BY METHOD REFERENCE R226 07 12/19/97 EP S3 12/19/97 EP EPA 1980, 903.1 l
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lab id NtTITCB ABO Protocol -
DUPLICATES Version 1 Page 2 Form DVD-DUP EUMMARY DATA SBCTION Version 3,08 Page 5 Report date 12/29/97 i
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THERMO NUTECH i
KERa seccEE l
'9711033-01' CU3-41-009 DUPLICATE SDC/ Version 97102771 C11ont/ Case no Earr McGee Contact Mary Ramoso contract Shineine #971022212 DUPLICATE ORIGINAL Lab sample id 9711033-01 Lab sample id 9710277-07 Client sample id CU3-41-009 l
Dept sample id Dept sample id Location / Matrix WATER l
Clim t samp id Received 10/24/97 Collected / Volume /Saale 10/20/97 15:30 4236 ML t moistare 4 moisture Custody /SAS no/ Level 1
1 I
I 1
DUPLICATE 20 ERE 88)A RDL QUALI-ORIGINAL 20 ERA SEE QUALI-RFD 30 DER ANALTTE PCi/1 (SUTAL)
PCi/1 pC1/1 FIERS TEST pC1/1 (TOTAL) p:i/1 FIERS 4
TUT o
l Radium 228 150 23 7.9 3.0 RA28 170 26 6.5 13 32 1.2 l
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l DUPLICATE SUF-TIRID ORICIMAL SUF-YIE1D TEST FIADCENT FII t ANALYSED ST FIANCENT FIE t
AMALYEED ST METWOD REFERENCE RA28 60 12/08/97 EP 59 12/09/97 EP EPA, 1990b l
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THERM 3 NUTECH KEmR mCGEE 9711033.ca.
CU3-41-011 DUPLICATE SDC/ version 9710277T cliset/Caso na Farr McGee Contact Mary Femoes Contract Shionine #971022222 DUPLICATE ORICIEAL Lab sample id 9711033-01 Lab semple id 9710277-09 Client semple id CU3-41-011 Dept sample id Dept sample id Incation/Matriz WATER Clitat samp id Received 10/24/97 Collected / Volume /Sa.sie 10/20/97 16:00 416) %
4 meisture 4 moisture Custody /SAs ne/ Level DUPL1CATE 20 ERR SEE ADL QUALI.
ORIGIRAL 20 EAR DEE QUALI. RPD 3a DER AEALYTu pC1/1 (torAL) pC1/1 pC1/1 FIERs TsET pci/1 (19tAL) pCi/1 FIERS t
TUT e
Croes Alpha S3 23 22 GA 33 15 14 47 96 1.5 Groes tota 32 12 17 CB 25 10 14 25 83 0.9 DUPLICATE SUP-TIEIb ORIGIRAL SUP-TIE 1D TERT PIANCERT FIE 4 ANALYSED B?
PIANCERT
- PIE 4
ANALYSED ST METHOD REFERENCE GA 100 11/17/97 KP 100 11/17/97 KP EPA-600 900.0 GB 10C 11/17/97 KP 100 11/17/97 KP EPA-600 900.0 Lab id trUTECH ABC Protocol -
DUPLICATES Version 1 Page 4 Para D~.D-DUP
SUMMARY
DATA SECTIOR Version 3.08 Page 7 Report date 12/29/97
ACKNOWLEDGEMENT OF SAMPLE RECEIPT i
! Thormo NUtech Albuquerque lab has received-samples to be analyzed as follows:
1-9-WATER SAMPLES FOR ISOTOPIC URANIUM, ISOTOPIC THORIUM, GROSS ALPHA /DETA,, RADIUM-226, RADIUM-228 ANALYSIS We received the samples 10/24/97 Our projected completion date is 11/24/97 Samples have been assigned to work order 97-10-277 Please contact PRODUCTION CONTROL at (505) 345-3461 with any changes or questions involving the analysis to be performed.
The invoice will be mailed to the address below:
KERR McGEE CORP.
ROUTE 4, BOX 2323 CUSHING, OK 74023 Attention TERRIE GIBSON Under purchase order: Please provide The report will be mailed to the address b elow:
KERR McCEE CORP.
ROUTE 4, BOX 2323 CUSHING, OK 74023 Attention ROBERT POUNDS RETURN ORIGINAL COC WITH REPORT PER TELECON WITH TERRI GIBSON 11/14/96(C. BALES)
--n era -
1 0 1997 o
Please contact ADMINISTRATIVE SUPPORT at (505) 345-3461 with any changes or questions involving address information.
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REGUIRED ANALYSIS REPORT icros Nutech ORDER
- 97-10-277 CLIENT KERR_MCGEE_C ME JOB #-
- 57600200 WORK ID
- SHIP. # 971022204 THRU 212 4TCH/ SET /tGNTACT
- 9710277 SAMPLE. TYPE: WATER ETURN ORIGINAL COC WITH REPORT PER TELECON WITH TERRI GIBSON
- /14/96(C. DALES) t DATE TOTAL i
\\MP-SAMPLE DESCRIPTION COLLECTED V/W ANALYSES'REGUIRED L
..U3-41-003 10/20/97 4145MLS_EST GROSS ALPHA / BETA
!B RADIUM 228
'. C RADIUM 226 BY RADON EMANATION
'b ISOTOPIC URANIUM
!C RADIUM 226 BY RADON EMANATION
!D ISOTOPIC URANIUM
!E ISOTOPIC THORIUM IA CU3-41-OO3 10/21/97 4236MLS_EST GROSS ALPHA / BETA IB RADIUM 228 IC RADIUM 226 BY RADON EMANATION ID ISOTOPIC URANIUM IE ISOTOPIC THORIUM IA CU3-41-OO6 10/20/97 4100MLS_EST GROSS ALPHA / BETA l
Ir RADIUM 228 IL RADIUM 226 BY RADON EMANATION ID ISOTOPIC URANIUM IE ISOTOPIC THORIUM iA CU3-41-OO7 10/20/97 4172MLS_EST GROSS ALPHA / BETA 3B RADIUM 228 i
3C RADIUM 226 BY RADON EMANATION iD ISOTOPIC URANIUM IE ISOTOPIC THORIUM
>A CU3-41-OOB 10/20/97 4261MLS_EST GROSS ALPHA / BETA 2B RADIUM 228 WC RADIUM 226 BY RADON EMANATION 2D ISOTOPIC URANIUM
>E ISOTOPIC THORIUM i
.. =
REGUIRED ANALYSIS REPORT ictma Nutech ORDER
- 97-10-277.
CLIENT
- KERR_MCGEE_C.
3E JOB #
- 57600200
. WORK ID SHIP. # 971022204 THRU 212 ITCH / SET / CONTACT 9710277 SAMPLE TYPE: WATER ITURN ORIGINAL COC WITH REPORT PER TELECON WITH TERRI GIBSON t/14/96(C. BALES)
DATE TOTAL d1P SAMPLE DESCRIPTION COLLECTED V/W ANALYSES REGUIRED
'A J3-41-OO9 10/20/97 4236MLS_EST GROSS ALPHA / BETA eB RADIUM 228
'C RADIUM 226 BY RADON EMANATION
'D ISOTOPIC URANIUM
'E ISOTOPIC THORIUM 1A CU3-41-010 10/21/97 4258MLS_EST GROSS ALPHA / BETA IB RADIUM 228 1C RADIUM 226 BY RADON EMANATION 3D ISOTOPIC URANIUM IE ISOTOPIC THORIUM 2A CU3-41-011 10/20/97 4163MLS_EST GROSS ALPHA / BETA 2B RADIUM 228
)C RADIUM 226 BY RADON EMANATION 7D ISOTOPIC URANIUM
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3 5
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TOTAL URANIUM J h j
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m m
m f
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3 F
m ISOTOPIC:ETT.1234 BTJ235 ED238 h
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. 4
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m ISOTOPIC:E'iTh232 [fth 228 0
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r-m ISOTOPIC:IU234 [WU235
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MDA PRm-L i A7 2-N 5 9y O
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t LBS16t1WLowBackgroundOntnMur Syswn -- SmearAna& sis A>ha ene;ency tog no: ro210AB o
Alpha EEciency: 44.74%
Date: 3f29f94 Alpha ac#dy actonlevel(DPM) 10 00 Alpha to Beta Oosstalk: 0 73% ~
Countng Unitid: 1 Beta acIMty actionlevel(DPM) 000 Alpha Bac+ ground (CFM): 0212G Data file name: C1.BXL\\ UNIT 1\\SME1A2MD Certameylowelfor MDA and tags: 95 00%
Balch Ended: af29f94 9 03 High VoRage Setting 1410 Beta efficiency log tiae: SR90AB Qosstak Correcton: Not Applied Beta Ellierency: 54.44%
Application Revision.1 Betairdo Alpha Oosstellr: 0 99%
Application Version Standard Bets Bac& ground (CPM): 1 2875 Batch D: CUSHING ENVIRONMENTAL GROUND WATER SURVEY Alpha Activily Beta Activity Count Alpha Beta Completon Canier DFM o
tags MDA time (rnin)
CPM CPM TOD l
1 1.760 2.46 MA 10 85
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-0.475 1,03 MA 1085 4.98 4 23 AlAL 14 67 1 00
-0 213 2 71 3/29f94 8.55 3
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<MDA 10.85 4.98 4 23 At AL 14 67 1.00
-0 213 2 71 3/29/94 8 56 4
-043 1 03 4ADA 1085
-2.37 2 09 4ADA 14 67 1 00
-0 213
-1 29 3/29/94 8 57 5
-0 c'E 1.03 4ADA 10 85 1.31 3 33 4ADA 14 67 1.00
-0 213 0 71 3/29/94 8 58 i.
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-0.473 1 03 4ADA 1085
-2 37 2 09 4ADA 1467 1 00
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-1 29 3/29/94 8 59 7
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-0213 0 71 3/29f94 902 9
-0 475 1.03 4ADA 10 85
-0.53 2.78 4ADA 14 67 1.00
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