ML20207B788

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Core Labs Analytical Rept for Job Number 940630
ML20207B788
Person / Time
Site: 07003073
Issue date: 05/06/1994
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080243
Download: ML20207B788 (9)
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e F5kW WESTERN ATLAS Core Laboratories CORE LABORATORIES ANALYTICAL REPORT Job Number:

9406 0 4

Prepared For:

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KERR-McGEE CORPORATION JEFF OSTMEYER P.O. BOX 89 CUSHING, OK 74023 Date:

05/06/94 i

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i Signature Date:

Name: Rondalynn Mull Core Labcsratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor RECEIVED MAY 121994 Env0ps Cusning 9903000243 981106

'I PDR ADOCK 07003073 $

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BERE wSSman ATLAS Core Laboratories LAB 0 RAT 0RT TESTS RESULTS 05/06/94 l

JOB NUMBER: 940630 CUSTOMER: KERR-McGEE CORPORATION ATTN JEFF OSTMETER d

CLIENT 1.D.........: BLOCK 39 E30 $40 LABORATORY 1.D...: 940630-0001 DATE SAMPLED.......: 03/26/94 DATE RECEIVED....: 04/04/94 TIME SAMPLED.......: 09:00 TIME RECEIVED....: 10:00 WORK DESCRIPTION...: CU1-65-003 REMARKS..........: WATER TEST DESCRIPTION -

FINAL RESULT DETECTION LIMIT UNITS OF MEASURE' TEST METHOD DATE.

~ TECHNICIAN Thiriun 230, total 0.3 pcl/l 05/02/94 JG Thoriun 230, total, error, +/-

0.3 pCi/l 05/02/94 JG Thorlum 230, total, LLD.

0.5 pCl/l 05/02/94 JG Thtriun 232, totat 0.3 pCl/l 05/02/94 JG Thoriun 232, total, error, +/-

0.2 pCl/l 05/02/94 JG Thortun 232, total, LLD 0.2 pcl/l 05/02/94 JG Uranium 234, total 4.3 pCi/l 04/29/94 PLJ Uraniun 234, total, error, +/-

0.8 pci/l 04/29/94 PLJ Urantun 234, total, LLD 0.3 pcl/l 04/29/94 PLJ Urtnian 235, total 0.1 pCi/l EPA 901.1 04/29/94 PLJ Uraniun 235, total, error, +/-

0.1 pCi/l 04/29/94 PLJ Ureniun 235, total, LLD 0.1 pcl/l 04/29/94 PLJ Urtniun 238, total 2.4 pCi/l 04/29/94 Urtniun 232, total, error, +/-

0.1 pCi/l 04/29/94 PLJ Urenf un 238, total, LLD 0.2 pCi/l 04/29/94 PLJ Thoriun 228, total 0.4 pCi/l 05/02/94 JG Thoriui 228, total, error, +/-

0.3 pCi/l 05/02/94 JG thortun 228, total, LLD 0.2 pCi/l 05/02/94 JG 420 West First Street Casper, WY 82601 (307) 235-5741 n.:

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ATLAS i

Core Laboratories QUALITY CONTROL REPORT 05/06/94 JOB NUMBER: 940630:

CUSTOMER: KERR McGEE CORPORATION ATTN JEFF OSTMEYER i

ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES i

i ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bj)

VALUE RECOVERY VALUE ADDED RECOVERY

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i PARAMETER:Uranlun 234, total DATE/ TIME ANALYZED:04/29/94 10:55 oc SATCH NUMBER:150616 I

REPORTI:'C LIMIT /DFs -

UNITS pCl/l METHOD REFERENCE :

TECHNICIAN:PLJ SLANK MB M811UO414 0.1 BLA:K MB M821U0414 ND STANDARD.

LCS LC1]U0414 6.5 6.6 98 STANDARD LCS ST11UD414 6.7 6.6 102 SP!P.E MS 940631 1 11.3 2.4 8.2 109 DUPLICATE MD 940634 1 4.1 3.3 22 PARAMETER: Uranium 235, total DATE/ TIME ANALYZED:0=/29/94 11:18 QC BATCH NUMBER:150622 i

REPORTING LIMIT /DF:

UNITS:pC(/l METHOD REFERENCE : EPA 901.1 TECHNICIAh PLJ BLANK MS MB11U0414 ND BLANK M8 M821UO414 ND i

DUPLICATE MD 940634-1 ND 0.1 0

1 PARAMETER:Uranlun 238, total DATE/ TIME ANALYZED:04/29/94 11:28 oc 8ATCH NUMBER:150625 REPORTING LIMIT /DFs UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:

BLANK MS M811U0414 ND BLANK MB M821U0414 No STANDARD LCS LC11UO414 7.3 6.9 106 STANDARD LCS ST11UO414 6.9 6.9 100 SPIKE MS 940631 1 10.8 1.3 8.6 110 DUPLICATE MD 940634-1 1.4 1.5 7

PARAMETER: Thorium 228, total DATE/ TIME ANALYZED 05/02/94 15:03 QC BATCH NUMBER:150693 REPORTING LIMIT /DF:

UNITS:pCf/t METHOD REFERENCE :

TECHNICIAN:JG BLANK MB MB3T0415 0.0 OLACK MB MB470415 0.1

$7ANDARD LCS 5T270415 4.7 4.0 118 STANDARD LCS LC2iD415 3.7 4.0 92 SPIKE MS 940637-1 4.9 0.3 4.0 115 DUPLICATE MD 940633-1 0.5 0.6 18 PARAMETER: Thorium 230, total DATE/ TIME ANALYZED:05/02/94 15:10 oc BATCH NUMBER:150697 REPORTING LIMIT /DF:

. UNITS:pci/l METHOD REFERENCE :

TECHNICIAN:JG BLANK MB MB3T0415 0.1 BLANK MB MB4T0415 0.0 STANDARD LCS ST3TD415 2.0 1.7 118 STANDARD LCS LC3T0415 1.8 1.7 106 CPIKE MS 940632 1' 2.3 0.2 1.7 124 DUPLICA7E MD 940633 1 0.5 0.3 50 l

420 West First Street Casper, WY 82601 (307) 235 5741 l

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ATLAS i

l Core Laboratories QUALITY C0NTR0L REPORT 05/06/94 i

JOB NUMBER: 940630 CUSTOMER: KERR McGEE CORPORATION ATTN: JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES l

ANALYSIS ANALYSIS ANALYS!$

ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SU8-TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bj)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Thortua 232, total DATE/ TIME ANALYZED:05/02/94 15:27 QC BATCH NUMBER:150701 REPORTING LIMIT /DF:

UNITS:pCl/l

- METHOD REFERENCE.

TECHNICIAN JG BLANK Ms MB3T0415 0.0 8 LANK MB M84T0415 0.0 STANDARD LCS ST2T0415 4.5 4.0 112 STANDARD LCS LC2TD415 4.2 4.0 105 SP!KE MS 940637-1 4.4 0.0 4.0 110 DUPLICATE MD 940633-1 0.2 0.2 0

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l QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600/4 79 020 Methods for Chonucal Analysis of Water and Wastes March 1983 (3) EPA SW.846. Ten Methods for Evaluaung Solid Waste. Third Edition, November 1990 and July 1992 update (3) Standard Methuds for the Exanunahon of Water and Wastewater,17th,1989 (4) EPA 600/4-80432. Presenbod Procedures for Measurement of Radioactmty in Dnnking Water. August 1980 (5) Federal Register, Friday. October 26.1984 (40 CFR Part 136)

(6) EPA 600'8-78-017 Microbiological Methods for Monstonns the Environment, December 1978 COMMENTS j

(1) The data in the Laboratory Tea Resuhs Report may differ from the data in the QC Report due to calculations for sangle preparauon and or dilutions.

(2) The " Time Analyzed' in the QC Report may not reflect the actualtime of each analysis. The "Date Analy7ed" is the actual date of analpis.

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(3) Soil and sludge samples are reported on a wet basis or on an "as received" basis unless otherwise mdicated.

(4) The data in tius report are within the linuts of uncertainty spectfied in the referenced method unless otherwise indicateii j

(3) Analyses performed by a subcontract laborasary are indicated with an astensk and associated code in the " Technician" data field j

Subcontract Laboratories Code Core Laboratones. Anaheim, CA

  • AN Core Laboratones - Aurora.CO
  • AU Core Laboratones. Casper. WY
  • CA Core Lahmatones Corpus Christi, TX
  • CC Core Laboratones Houmon. TX
  • HP Core laboratones - Lake Charles. LA
  • If Core Laboratones - Long Beach, CA
  • LB Other Subcontract laboratones
  • XX DEFINITIONS (1) NC = Not Calculable due to salues lower than the repswting limit.

(2) ND = Not Detected above the reponmg linut.

OC SAMPLE IDENTIFICATIONS BLANKS SPIKES MB = Method Blank (also referred to as a preparat un blank)

MS = Matnx Spike RB = Reagent Blank MSD = Mainx Spike Duphcate Instnament Blank PDS = Post Digestion Spike IB

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ICB = Initial Cahbration Blank BS = Blank Spike (also referred to as a method spike)

CCB = Contmums Cahbrauon Blank SS = Surrogate Spike HB = Iloidmg Blank (also referred to as as a storage blank)

REFERENCE STANDARDS DUPLICATES -

CS = Calibration Standard MSD - Matrix Spike Duptw. ate RS = Reference Standard (also referred to as an external reference standard)

Method Duphcate -

ICV = InitialCahbration Venficahon MD

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CCV = Contmuing Cahbration Cahbrauon LCS = laboratory Control Sample 420 West First Street Casper, WY 82601 (307) 235 5741 va.

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Sample Receipt Acknowledgment Date

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Core Laboratories Customer Estimated Job Number Project ID Completion Date Sample #

Customer ID Remarks C '.' : +.:3

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.e THIS IS NOT AN INVOICE Order subject to our sales agreement. if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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LOG-IN JOB REPORT 04/08/95

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JOB NUMBER:940630 CUSTOMER (KE0001) KERR McGEE CORPORATION CONTACT JEFF OSTMEYER PHONE:(

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p SAMPLE NUMBER:0001 DATE RECEIVED 04/04/94 TIME RECEIVED 10:00 SAMPLE DATE:03/26/94 SAMPLE TIME:09:00 DUE DATE:05/02/94 PROJECT ID: BLOCK 39 E30-540 SAMPLE ID:CU1 65 003 REM: WATER LAS NOTES:114L CUSE SHORT 10:

BIN NUMBER:0 CODE TEST DESCRIPTION TEST LIMITS UNITS OF MEASURE TEST METHOD COMENTS R552 Thori m 230, total pcl/l R553 Thori m 230, total, error, +/-

pCi/t R554 Thori a 230, total, LLD pCl/l R555 Thori a 232, total pcl/l R556 Thori a 232, total, error, +/-

pCi/t R557 Thori a 232, total, LLD pCi/t R561 Urani m 234, total pCi/t R562 Urani m 234, total, error, +/-

pcl/l R$63 Urani m 234, total, LLD pCl/l R564 Urani m 235, total pCl/l EPA 901.1 RS65 Urani m 235, total, error, +/-

pCl/l R566 Urani a 235, total, LLD pcl/l R567 Urani a 238, total pcl/l R 48 Urani a 238, total, error, +/-

pcl/l i

R 69 Urani a 238, total, LLD pCi/l j

t i70 Thori m 228, total pcl/l

571 Thorim 228, totat, error, +/-

pCi/t R573 Thori m 228, total, LLD pCi/t l

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