ML20207B806

From kanterella
Jump to navigation Jump to search
Core Labs Analytical Rept for Job Number 940631
ML20207B806
Person / Time
Site: 07003073
Issue date: 05/06/1994
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080250
Download: ML20207B806 (16)
v • d • e


Text

.

F4RE waarnase ATLAS Core Laboratories CORE L.3 ORATORIES T

ANALYTICAL REPORT Job Number:

940631 Prepared For:

KERR-McGEE CORPORATION JEFF OSTMEYER P.O. BOX 89 CUSHING, OK 74023.

Date:

05/06/94 s

l fl W

. S., ;,; /,;,,

Signature Date:

Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor 9903000250 981106 3

PDR ADOCK 07003073 1 B

PDR ;

RECENED "E I COPY y

we ms lawn gJortest W Ca6 a_

00fs Lat7alone6. nouewer segnames fu reesumeduely arts manos se WWraney y wipemenesh0R4 espou y stped at 5 phe POthsChW4p FFJup Oportreft W P0htdDmM84 W F4 08 945 Eue et

- ethes stators reporgy est y tens e garm one eme$ aucfi saport e assee F M espOR lor erg seence emettoeven Fhe segnA she not he reipenuand estant e 45 esusesy ominiA the setten apparsi W Core Labo'ahwes J

+

EE M wasunse ATLAS Core Laboratories LA80 RAT 0RT TESTS RESULTS 05/06/94 JOB NUMBER:- 940631 CUSTOMER: KERR McGEE CORPORATION ATTN: JEFF OSTMEYER CLIENT 3.D.........: BLOCK 63 E54-S 98 LABORATORY I.D...: 940631-0001 DATE SAMPLED.......: 03/26/94 DATE RECEIVED..... 04/04/94 TIME SAMPLED.......: 10:00 TIME RECEIVED....: 10:00 WORK DESCRIPTION...: CU1-65-004 REMARKS..........: WATER TEST R*SCRIPTION FINAL RESULT DETECT!DN LIMIT UNITS OF MEASURE TEST METH00 DATE TECHNICIAN Thsrium 230, total 0.1 pCi/l 05/02/94 JG Thiriun 230, total, error, +/-

0.2 pCi/t 05/02/94 JG Thortun 230, total, LLD 0.4 pCi/t 05/02/94 JG Th:riun 232, totat 0.1 pCi/t 05/02/94 JG Thortun 232, total, error, +/-

0.1 pCi/l 05/02/94 JG Thorium 232, total, LLD 0.1 pCi/t 05/02/94 JG Uranium 234, total 2.4 pCi/t 04/29/94 PLJ Uranlun 234, total, error, +/-

0.6 pCi/t 04/29/94 PLJ Uranium 234, total, LLD 0.1 pC1/l 04/29/94 PLJ Urrnium 235, total 0.1 pC1/L EPA 901.1 04/29/94 PLJ Uranium 235, total, error, +/-

0.1 pCi/l 04/29/94 PLJ Urtnium 235, total, LLD 0.1 pCf/t 04/29/94 PLJ uranium 238, total 1.3 pCi/t 04/29/94 Uranium 238, total, error, +/-

0.4 pCi/t 04/29/94 PLJ Urtnium 238, total, LLD 0.1 pCi/l 04/29/94 PLJ Thoriun 228, totat 0.4 pCi/t 05/02/94 JG Thoriun 228, total. error, +/-

0.2 pci/l 05/02/94 Jr Thorium 228, total, LLD 0.2 pC1/t 05/02/94 J.

420 West first Street Casper, WY 82601 (307) 235-5741 PAGE:1

w. -

n.at,

..ne-si u.s.w e.

w

n. n, n n

..m.sa

.ern M tellpaarnent Of C089 Lelastetwas Casp Latforegenest Scae.e' enmuret

. and mance no ortenly O' 8808~

. spent W 4'4p.sl en Ab Ihm PeOuCE*WW PapeN ofiPresunt p P "

-_ W M4 a. gas cshy y ofNp n.see Pepsfly men es tar.m gennergen egh pene ed sogen a n,nar! y go.e5 utlin apt 884.aaer eNptes.et the suguNq sw stol be sapronusse essasP e en enhemy spinaut the eastem emprove, p L4pe 1,horaltwen

_~ ~-

=- --- -

~. __

NRW wasume ATLAS Core I aboratories i

r QUALITY CONTROL REPORT 05/06/94 i

JOB NUMBERt. 940631 CUSTOMER: KERR-McGEE CORPORATION ATTN: JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALYS!$

ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE 1.D.

VALUE (A)

VALUE (B)

(lA-Bj)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Urani m 234, total DATE/ TIME ANALYZED:04/29/94 10:55.

QC BATCH NUMBER 150616 REPORTING LIMIT /DF UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:PLJ BLANK MB MB11UO414 0.1 BLANK MB M823U0414 ND STANDARD LCS LC11UO414 6.5 6.6 98 STANDARD LCS ST11UO414 6.7 6.6 102 SPIKE MS 940631-1 11.3 2.4 8.2 109 9UPLICATE MD 940634 1 4.1 3.3 22 PARAMETER:Urani m 235, total DATE/ TIME ANALYZED:04/29/94 11:18 QC BATCH NUMBER:150622 REPORTING LIMIT /DFs UNITS:pCl/l METHOD REFERENCE : EPA 901.1 TECHNICIAN:PLJ BLANK MB MB11UO414 ND BLANK MB MB21UO414 ND DUPLICATE MD 940634-1 ND 0.1 0

PARAMETER: Uranium 238, total DATE/ TIME ANALYZED 04/29/94 11:28 QC BATCH NUMBER:150625 REPORTING LIMIT /DF.

UNITS:pCl/t METHOD REFERENCE :

TECHNICIAN:

BLANK MB MB11U0414 ND BLANK MB MB21UO414 ND STANDARD LCS LC11UD414 7.3 6.9 106 STANDARD LCS ST11UO414 6.9 6.9 100 l

SP!KE MS 940631 1 10.8 1.3 8.6 110 DUPLICATE MD 940634-1 1.4 1.5 7

PARAMETER: Thorium 228, total DATE/ TIME ANALYZED:05/02/94 15:03 QC BATCH NUMBER:150693 REPORVING LIMIT /DF UNITS:pci/t METHOD REFERENCE :

TECHNICIAN:JG BLANK MB MB3T0415 ND BLANK MB MB4T0415 0.1 STANDARD LCS ST2TD415 4.7 4.0 118 STANDARD LCS LC2T0415 3.7 4.0 92 SPIKE MS 940637-1 4.9 0.3 4.0 115 DUPLICATE MD 940633 1 0.5 0.6 18 PARAMETER: Thorium 230, total DATE/ TIME ANALYZED:05/02/94 15:10 QC BATCH NUMBER:150697 REPORTING LIMIT /DF:

UNITS:pci/l METHOD REFERENCE '

TECHNICIAN:JG BLACK MB MB3T0415 0.1 BLANK MB MB4T0415 ND STANDARD LCS ST3T0415 2.0 1.7 118 STANDARD LCS LC370415 1.8 1.7 106 SPIKE MS 940632-1 2.3 0.2 1.7 124 DUPLICATE MD 940633 1 0.5 0.3 50 l

1 420 West First Street i

Casper, WY 82601 (307) 235-5741 PAGE:1 l

~.,

=== i== = e ca. (

ca ten.

a w no..e.e. =,.,.

. nn a a io m m.co ev.

a.,r

..w.-

een,o om me.

ethat.mspe pop.rgy e. eens e 'spmer.se op a.eph essen eng pt. gase s.ese uglen 8. ant etori tuhel.ou.es lhet.open shap mot to poluanusale esteDI e as eni.est e.goul gh. emil.n espro.& of ca. n.JDoratorch I

E l

e l

l l

EERE I

WESTERN l

ATLAS l

Core 1.aboratories QUALITY C0NTROL REPORT 05/06/94 JOB NUMBER: 940631 CUSTOMER: KERR-McGEE CORPORATION ATTN: JEFF OSTMEYER l

ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYS!$

ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS-TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bl}

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Thortun 232,, total DATE/ TIME ANALYZED:05/02/94 15:27 QC BATCH NUMBER:150701 REPORTING LIMIT /DFs UNITS:pci/l METHOD REFERENCE :

TECHNICIAN JG BLANK M8 MS3T0415 ND BLANK MS MB4T0415 ND STANDARD LCS ST2T0415 4.5 4.0 112 STANDARD LCS LC270415 4.2 40 105 SPIKE MS 940637-1 4.4 ND 4.0 110 DUPLICATE MD 940633 1 0.2 0.2 0

420 West First Street Casper, WY 82601 (307) 235 5741 PAGE:2 tae e au.w. e ewpame= awwise e m espan me na ee een anaevemas me mane + w e, we casa== e ee..cnn.ve ne annienne. ine wie encon na. eu.a maa.

= a=rwoman w asmao=.mun =w.

tent $le beti pinpIIe8e & C@e Lappelenpl [.Se Lalerasenog hueever theudhes ac.

, se elemet sin operWy & flereteMLahomE espont y momeO st in we preewchuny Popp evermem es peMaDefett el Fev ed gab 504 y comes enteral papesty eso y aard a garmsween edh east que 8seen 4 eense6 m essen usum kW rey **1 top eNstnever 1848 sueen sheb not que scorqWhate estelp eith endwely e4htmal 98tP e*dlen apprewe et CFo LSMHatWest

m_

-.m-m._

BEM wasman ATLAS Core Laboratories QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600/4-79420, Methods for Chenucal Analysis of Water and Wastes, March 1983 (8) EPA SW-846, Tom Methods for Evaluaung Sohd Waste. Third Ediuon. November 1990 and July 1992 update (3) Standard Methods for the Exanunation of Water and Womewater.17th,1989 (4) EPA 600 4-80432, Pressnbod Pr== hares fur Measurement of Radioacuvny a Dnnking Water August 1980 (5) Federal Register Friday, October 26,1984 (40 CFR Part 136)

(6) EPA 600'8 78 017 Microbiological Methods for Morutoring the Environment. December 1978 COMMENTS (1) The data in the Laboratory Test Results Report may ddfor from the data in the QC Report due to calculations for sample preparauon and or ddutions.

(3) The " Time Analyzed"in the QC Report may not refied the actual tune of each analysa The "Date Analyzed"is the actual date of analysa (3) Sod and sludge samples are reported on a wet basis cr on an "as received" basis unless otherwise uubcated.

(4) The data in this reptwi are withm the 1: nuts of uncertausy specified in the referenced method unless otherwise indicated

(!) Analyws perfonned by a subcontract laboratory are uubcated with an astensk and asaoeisted code in the "Teduucian" data field.

Subcontract Laboratories Code Core Laburmons. Anaheun,CA

  • AN

- Cwe Laboratones. Aurora.CO

  • AU Core Laboratones. Casper, %Y
  • CA

- Core Laburatones. Corpus Chnsti. TX

  • CC Corelaborstor:es. Houston TX

'HP Core Laboratones. Lake Charles, LA

'LC Core taburatones. long Beach, C A

  • IB Other Subcontract Laboratones
  • XX DEFINITIONS (1) NC e Not Calculable due to values lower than the reporting knut (2) ND = Not Detected above the reportmg linut.

OC SAMPLE IDENTIFICATIONS a

BLANKS SPIKES MB = Method Diank (also referred to as a preparation blank)

MS

  • Matnx Spike RB = Reagent Diank MSD = Matnx Spike Duplicate IB = Instrument Blank PDS = Post Digestion Sp ke ICB = Imtsal Cahbrauon Diank BS = Diank Spike (also referred to as a method spike)

CCD = Contmuing Calikation Blank SS = Surrogate Spike HD = Holding Diank (also referred to as as a storage blank)

REFERENCE STANDARDS DUPLICATES i

CS = Calibration Standard l

i MSD = Matnx Spike Duphcate RS = Reference Standankatso referred to as an extemal reference standard)

Method Duphcate ICV = Inst alCalibration Venficatum MD

=

CCV = ContmumgCahbrauonCahbrsuon LCS = !aboratoryControlSample i

420 West First Street i

Casper,WY 82601 (307) 235-5741 w -

in re.

u s.w a,.

n me.~~.

==

e.

in.ne

=>r e.im e

con e i,,i. i u, n

e i.,,

_., -.._ al any as g,gt. gas y tuft Wit tunet psognieri, ed (ese lehmaiefst c0's Ldlueralenet tonover estumqua ne toteenteousy WW manet se eerrancy y taprogeestateg espeta er anglem en to tre pW papse agoraecns er p -

amor seners peliarly ees er tesis e eennotien eilh etWJi taste epon e used IP enen geosi ter any syssean J 1846 resoft t'W Got tis, eup wguten escogs e en avesely edhout Pw e** Men aussovel el COW Ladip8SIO8et L

CORE LABORATORIES Weeramen Atdes W

ALaunsosemmer W

.a..

Sample Receipt Acknowledgment Date Ji/]7/91 R

I e

n E > il;

    • .C.E. JFJW17.1 14nE V

o r LErv 3 o

r i

C'2DI'4 'rE'.ic OK 7EE3 t

c

.ter T e

T T

o o

Core Laboratories Customer Estimated Job Number Project ID Completion Date a ::s a :

.:,asi; Sample #

Customer ID Remarks

t tt c-a, m ER 1

.r.

n : -! - t THIS IS NOT AN INVO!CE Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediate!y, if any discrepancies are observed.

I usu.,. e..-.

o s.,, o s cun

A

....x.,

~...u 2

.._,.....m u.

-.,o 2

m 4

~

~ ~~~

~~~~ ~

L0G-1N J0B REP 0RT 04/0T/94 3 N E NI411 CUffM56fTrifRR E5fft0RWKYIF C5EfKCfitT5EfKifR Fii5EE:1 3

SAW LE NURIER:0001 DATE RECEIVED:04/04/94 TINE RECEIVED:10:00 SAK'.E CATE:03/26/94 SANPLE TIME:10:00 DUE DATE:05/02/94 P 2 JECT ID:BLDC1 63 E54 5 98 SANPLE ID:CU165-Otr4 REN:NATER LAB NOTES:ll4L CUIE SHORT ID:

BIN NURSER:0 CODE TEST DESCRIPTION TEST LIMITS UNITS OF NEASURE TEST NETHOD CONNENTS R552 Thorius 230, total pCill R553 Thorius 230, total, error, */-

pCi/1 R$54 Thortus 230, total, LLD pCill R555 Thorius 232, total pCill R556 Thorius 232, total, error, +/-

PCill R55T Thorius 232, total LLD pCill RS61 Uranius 234, total pCi/1 R562 Uranius 234, total, error, +/-

pCill R563 Uranius 234, total, LLD pCill RS64 Uranius 235, total PCill EPA 901.1 R565 Uranius 235, total, error, +/-

pCill R566 Uranius 235, total, LLD pCill R567 Uranine 238, total PCill R568 Uranius 238, total, error, +/-

pCill R569 Uranius 238, total, LLD pCill RSTO Thorius 228, total pC1/1 RSTI Thortus 228, total.cfror, +/-

pCill RSTt Thorius !!$, total, LLD PCill I

~

~~

~

PAGE:1

SHIP TO:

CHAIN OF CUSTODY RECORD AND ANALYS13 REIUEST bore kct3 5 COMPANY NAME:

ANALYSIS REQUEST l

COMPANY ADDRESS:

I YW toes} l S$ tee l l'oSpe, qlgeleskt $c9/oOl

}

j r

FROM:

KERR MCGEE CORPORAllON PHONE: 1-918-'225-7753 3

g 2 MILES NORTH OF HWY. JCT 18 & 33 FAX: 1-918-225-7749 h

t-4 4

h 1/2 MILE EAST h

0 0

CUSHING.OKLA. 74023 SHIPPING # fYd329.3 f g

4 arissT THar tus emoren risto sAMetino emocrounts

"" N Q

.Y O

vvens useo pumma TMs coLLECTtON OF THESE SAMPLES.

  1. 1 L K',esped g,b g

@ 9 9 8 g

5 U

PROJECT MANAGER:

c m w. 3.l SAMPLd LOCATION:

g 0

h O

JEFF LLM G( cq ( 3-fgy-5 pf m

n wfNoo h

MATRtX SAMPUNG b

SAMPLE LAB PRESERVED k

I b

l3 se NUMBER USE o

E l l

a g l g l g a l l 3

l

==

=

u a

g ilt 2

2 m

ONLY e

n Q

a

- 1 Cul-/,F-co4 I

N6-7/

10'.0 0 I

I i

I I

I i

i p

Special Reporting requireroents:

Note: Do not comtHne Special Doctecton This sample meets aH M

Big & Report to:

l Note: Time of analysis & tech's these results with umns:

appropriate radiological.

Jeff Ostmeyer l

,p,M M"

requirements.

Hp initial M n-Box 89

[

name must be recorded on other Chain of da'a report.

Custodys.

7/g6 m-7.cr1,1t Cushina. Okla. 74023 l

o w

w 1

n.*=gie 6, se CUSTODY 77Q bu,J 3-ff-99 4 oc> gm

,% _ O bw n1 RECORD

- w

=

i t

bt lura 3 :=,n - 9 bf/

LLSS.

~'"- b i

~

a.

ioco ht~k C~t-e 4Mn n.~*.

( ra:C 0} Y D h $

Retrieved from "https://kanterella.com/w/index.php?title=ML20207B806&oldid=4041103"