ML20207C027

From kanterella
Jump to navigation Jump to search
Core Labs Analytical Rept for Job Number 951926
ML20207C027
Person / Time
Site: 07003073
Issue date: 09/28/1995
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080322
Download: ML20207C027 (9)
v • d • e


Text

- - -

4 J

l 1}LAR W

CORE LABORATORIES LABORATORY TESTS RESULTS 02/08/96 l

~~ 951926s

'(USTOMER:.KERR McGEE CORPORATION

' ATTN ' JEFF OSTMETER l

J0" IRMBER 1

1 CLIENT 1.D.........

ANNUAL ENVIRONMCNTAL CMW 20.2 LABORATORY I.D...: 951926-0001 DATE SAMPLED.......: 08/23/95 OATE RECE!VED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPTION...: CU2-26 025 REMARKS..........: WATER l

TEST DESCRIPTION FINAL RESULT DETECTION LINIT UNITS OF EASURE -

TEST PETHOD DATE TECHNICIAN Gross Alpha, total 70.3 pCl/l EPA 900.0 08/30/95 NRF Gross Alpha, total, error, +/-

36.4 pCl/t 08/30/95 NRF Gross Alpha, total, LLD 37.7 pCi/l 08/30/95 NRF Gross Beta, total 55.6 pcl/l EPA 900.0 08/30/95 NRF Gross Bate, total, error, +/-

33.8 pCf/t 08/30/95 NRF Gross Beta, total, LLD 52.1 pct /t 08/30/95 NRF Thoriun 232, total 1.48 pCl/l 09/25/95 DW j

Thoriun 232, total, error, +/-

0.6 pCi/l 09/25/95 DW Thortun 232, total, LLD 0.3 pCl/t 09/25/95 DW uranlun 234, total (ISO U) 0.8 pCi/t CA GLR-R405 09/26/95 DW uraniun 234, total, error, +/-

0.3 pCi/L 09/26/95 DW Uraniun 234, total, LLD 0.3 pC1/1 09/26/95 DW uranlun 235, total (ISO U) 0.0 pCl/l CA-GLR R405 09/26/95 DW Uranlun 235, total, error, +/-

0.1 pCl/t 09/26/95 DW uranlun 235, total, LLD 0.3 pCf/l 09/26/95 DW uranlun 238, total (ISO't) 0.3 pCi/L CA-GLR-R405 09/26/95 DW Uranlun 238, total, error, +/-

0.3 pCI/l 09/26/95 DW uraniun 238, total, LLD 0.2 pCl/l 09/26/95 DW l

Th:rfun 228, total 1.7 pCi/t 09/26/95 DW l

Thoriun 228, total, error, +/-

0.7 pCf/t 09/26/95 DW Thiriun 228, total, LLD 0.7 pCl/l 09/26/95 DW l

1

~

420 West First street 9903080322 981106 t

PDR ADOCK 07003073 Casper, Wy 82601 B

PDR (307) 235 5741 PAGE:2 v--..e.....,,n..,_.4......

is.m...,...-..

._,-_.<._e__-..__._....,._....-.._,__.._._-_....

eth.e II.n.e4,sup. tty e OF rgi ist teMst.i:1.ph $det sensch.AM e s(t a l#s.43 (4 F.wi.g3 gggW tw arig e...gp> pndt.eev.e I986 8.gleM.hdM RW II f.tworgia

.ssJs.1 et 16..I.qy $^hd l'n WHHe,6 m.8m.'.8 00'. L $0* 1f0".s l

7 Y

WIW CORE LABORATORIES QUALITY CONTROL REPORT 02/08/96 JOB IMIBER 4 951926i CUBTOMER:-1EERR Mc0EE CORPORATION-ATTN JEFF OSTMEYER'.

ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS AllALYSIS ANALYSIS ANALYZED DUPLICATE RPO or TRUE PERCENT ORIGINAL SPIKE PERCENT TTPE BUS TYPE I.D.

VALUE (A)

VALUE (B)

(lABl}

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Groaa'Alphe, totalt,

DATE/ TIME ANALYZED 08/30/955 14:05-

,0C BATCN IMIBER:170093 REPORTIIIG LIMIT /DFs- ' -UNITS:pCf/l.

M THOD REFERENCE : EPA 900.0L

. TECHillCIM:llRF BLAllK MB MB2A80829 ND STANDARD LCS LCIA0029 22.4 25.5 88 SPIKE MS 951963 1 124 10.0 128 89 DUPLICATE e

951963 1 10.0 14.6 37 PARAE TER Gross Sita, totato DATE/ TIME ANALYZED 08/30/95 ~ 14:14 GC BATCilIMIBER 170097 REPORTIIIG LIMIT /DFs UNITS:pCf/l

' METIES REFERENCE : EPA 900.0 TECHNICIAN:NRF BLANK MB MB2AB0829 0.4 STANDARD LCS LC150829 23.9 22.0 109 SP!KE MS 951963 1 144 5.0 110 126 DUPLICATE fe 951963 1 5.0 8.8 55 PARAMETER: Thorium 232,1 total DATE/T!ME AIIALY2ED:09/25/95.16:49 -

OC 4ATCN IMIBER:171053 REPORTIIIG LIMIT /DF:

UIIITSepCI/1 s E THOD REFERENCE :
TECalulCIAN:DW BLAllK MB M55T0906 0.47 BLANK MB MB6T0906 0.95 STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101 SP!rE MS 951921 1 16.3 0.92 14.0 110 DUPLICATE sc 951922 1 0.61 0.89 37 PARAMETER Thortun 228, total DATE/ TIME ANALY2ED:09/26/95 08:19 QC BATCH NUMBER 171058 REPORTING LIMIT /DFs UNITS:pCf/t

- METHOD REFERENCE :

TECHNICIAN DW BLANK MB M55T0906 0.18 BLAIIK MB MB6T0906 0.01 STANDARD LCS ST3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 4

SPIKE MS 951921 1 18.0 0.35 14.0 126 DU*LICATE MD 951922-1 0.74 0.86 15 PARAETER:Uranlun 234, totel' (ISO U)

DATE/ TIME ANALYZED:09/26/95 10:46 GC BATCH IMIBER 171081 REPORTING LIMIT /DFs Jf!TS:pci/t.

'IEETHOD REFERENCE :CA GLR R405 TECHNICIAN.DW BLA81K MB MB1UO906 0.2 BLANK MB MB2UO906 0.3 STANDARD LCS ST100906 6.6 6.6 100 STANDARD LCS LC1UD906 6.5 6.6 98 J

DUPLICATE MD 952012-2 107 110 3

l PARAETER: Uranium 235, total - -(ISO U)

DATE/ TIME ANALYZED:09/26/95 11:13 GC BATCH llUMBER:171088 REPORTIleG LIMIT /DFs UNITS _:pci/l -

METHOD REFERENCE. CA GLR R405 TECHNICIAll:DW BLANK MB MB1UO906 0.0 i

A20 West First Street Casper, WY 82601 (307) 235-5741 FAGE:3

%w.,..,m.o.w.~,i..-.-..-,,

iH Ld'. B.ata.ra he. C.08. L.ats etorw. h g s a gm

,1. e.603res.*4v.81. %e.

d e.ftnesy er pr.

d. tea..s..e GP m.IWeil 8. In.e yes.ra bwWy estupeN lat.wreennit.' D'tehl stuen.sS et.seg dw gn n 4 o*

sut sw h.gt.

r

.,.wi, w

w

.... r.,

,..a u t a

,y.

t l

l WIW CORE LABORATORIES QUALITY CONTROL REPORT 02/08/96 1

1 JOB IM eER:1 951926

EUSTOMER
( KERR Mc0EE' CORPORATION ATTN JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS NATRIX SPIKES ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUB TYPE I.D.

VALUE (A)

VALUE (B)

(lABl}

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER: Uranium 235, total...!(180 U)-

.DATE/ TIME ANALYZED:09/26/95 11:13 :

oC BATCH lu mER 171088 REPORTIINI LIMIT /DFs :

UNITb,'aCl/l METHOD REFERENCE SCA GLR-R405 TECHNICIAN:DW SLANK MS M82UO906 0.0 DUPLICATE MD 952012-2 4.5 5.0 11 PARAMETER:Uranita 238/ tr.,tal J(ISO U)-

.DATE/ TIME ANALIZED 09/26/95 11:19 DC BATCH NUMBER 171092 REPORTJWG LIMIT /DF2 ~

UNITS pCl/l METHOD REFERENCE :CA GLR R405 TECHNICIAN:DW SLANK

- Ms MB1UO906 0.1 i

BLANK Ms MS2UO906 0.1 l

STANDARD LCS ST100906 6.2 6.0 103 STANDARD LCS LC1UO906 6.7 6.0 112 D'JPLICATE IC 952012-2 48.2 48.2 0

420 West First Street Casper, WY 82601 (307) 235 5741 l

PAGE:4 l

%4

  • m..nin i e. ceaien.s c

. n,i m, m.m a n, ie, e = iin e.m.

u

.,= an.45,m.

ir m.

.a.,,3

., <>,,%,ig.....

mesal W.W bett qualgtestt Of LO8e & M.10994 (A89 L. Des 4testet Dueever.%un'en sec..

a'W Praeus ne estess ty of stepsesarmJter>% miepive or.regs-gso ag sc st.ep aptmmMy p* Wast Narr.3 r n te e**u es'.a* y a" G.as a

e atenge seinsvge gartporty esp gr g.pid,P CfpFIRgK]IDF et$ ofMCS EnsEf1199001IS WGSO.If. hell Wpun IDEentry esAton ehgl.gyggr lasg fggpspe grig mee en sygegggys yg pasgpt sp Ag ympygy gyrt%gg grg e W,e agruvJ g, 6his4'ia38e

l n

CORE LABORATORIES QUALITY CONTROL FOOTER l

i METHOD REFERENCES (I) EPA 600 4 79-020. Methods for Chemical Analvsis of Water and Wastes. March 19?)

(3) i PA SW H46. Test Methods for Evaluatmg Solid Wasie. Third Edition. November 1990 and July 1992 update (3) Standard Methods for the Exammauon of Water and Wastewater.17th.1989 (4) EPA 600 440-032. Presenhed Procedures for Measurement of Radioastmty m DruAing Water. August 1980 (5) Fcderal Register.1nday.(h.tober 26.19N4 (40 CFR Part 136)

(6) EPA 600 R.78-017. Microbiologwal Methods for Morutonng the Environment. December 1978 COMMENTS (1) ne data m the laboraturv Test Results Report mas difier from the data in the QC Report due to calculations for sample preparauon and or dilutiorm (2) The " Time Analvred" m the QC Report may not reflect the actual time of each analwis. The "Date Analped"is the actual date of anajpis (3) Soil and sludge samples are reported on a wet basis or on an "as received" basis unless otherwise mdicated.

(4) The data m this repast are withm the hmits of urwertamtv specified m the referenced method unless otheruisc mdicated.

(5) Anahses performed in a subeuntract laborstars are indicated wnh an estensk and associated code m the "Techmcian" data field.

j i

Subcontract LaboratoneS Code Core tab-: ones. Anaheun CA

  • AN Cs, s aborsione. Aurura. CO
  • AU Core bboratona. Casper, WY

'CA Core bhorntones. Corpus Chnste. TX

  • CC Core Laboratones. Hnuston. TX

' HP Core Laburatones. Lake Charlen. LA

  • If Core Laboratones. bng Beach. CA
  • LB Other Subonntract laboratones
  • XX PEFINITIONS (1) NC = Not Calculable due to salues lower than the reporting knut.

(2) ND - Not Detected above the reportmg Imut.

OC SAMPLE IDENTIFICATIONS BLANKS SPIKES MB - Method 13 tank (also referred to as a preparation blank)

MS = Matna Spika RH - Reagent Blank MSD = Maann Spas Duphcate ll)

Instrument Hlank PDS = Post Digesuon Spike ICl3 Innial Calibration Hlank BS

  • Blank Spike (also referred to na a method spike)

CCB = Conimums Cahbranon Blank SS = Surrognae Sp&e fin a iloidmg 13 tank (also referred to as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = Cahbrauon Standard MSD - Matnx Spike Duphcate RS = Reference Standard (also referred to as an cyternal reference standard)

MD Method Duphcate ICV = innsa!Cahbrauan Venficauon CCV = Casassoms Cahbrauon Vertficauon trS = LaboratoryControlSample 420 West First Stat Casper,WY 82601 (307) 235 5741

. m.,,,,,,,,..-..e--.r,.,,,,,,-a.,..e%..

n.-....-..

testa 'Pse bege udt33mesm g4 04 peg Lampratapeg CONp L ADWMO8994 floseve' Ashmes MO fe400sneaba4y Sftp ma.pt np weregnty or 4ppstr artialagnt Warent Or tPP(bued.41(r RW StfithKfively 98MWfuseer.36 arm ti p'rnfit teppnergs at is 9 als fi 4

  1. 4. N.81ste $NM354y Well er 64stG $ CO'"tecteert mesh es.r# tasta segun 4 natted 088th4EI iAB06 GBt emy suggen yttatgopost treet espelft oftar 800 D. 8sitreaGut op est usW WL d4 edbretty govtboist I'+ eritterti JWess<t* Ett i tr'e t,esliu'3*enet

1} LAB gg CORE LABORATORIES i

J CORE IABORATORIES -

j A N A:L'~Y T I'C:A L-REP' ORT i

Job Number:.951926 Prepared;For:

KERR McGEE CORPORATION JEFF OSTMEYER P.O.

BOX 89 CUSHING, OK - 74023-Date:

09/27/95 ap W gf.

..n

,,. ne q -p

'i

/

/

.,,/

s _../ /

i /

-m, Signature Date:

Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

LABORATORY SUPERVISOR a pr:.P N "

OCT 0 21995

~~~

COPY L~ h-,.-~ -.. - - -. -.........-..-.

.....~ - ~,- - -. -..

e6f IPe Ibg89f glryttEDM OfE,"4W ( DIM J.BW9% Yt fi 4.d40' yl F W

' 2&yr J. I-.eP6 '*858W '@ uP'4 MW 4*E A' 38#5"'

t" I' AV W 3ppsDWng 4.st' g gayepo gp dB" G

e f.e psigfs trylg y.ne 4e%gflp

  1. jef.N.1 WrW $ We

'** f 19hiflW 4 $8@fg Seja gs 6 (elg #

n'"nge(MM $ ffi $44 0 segpf M g y gyrf gr aptgggl ger3$ lLtAMg W. g'J38tWstWiggypt )y ts[grgq) b/Nif IbP89(ph]fIiA.08fl $E og f'.lm FiddWig $ fli

.I l' #e ' "@

b& JEW 4W $

'40 taftf" llut*W D 8

__4__a w

es a

a-9

+a.J L

+

e e a

I i

1"l LAB gg CORE LABORATORIES FINAL REP 0RT 01STRI8UTION 09/27/95 JOB NUMBER: 951926 COMPANY NAME' COMPANY MAILING ADDRESS (XMPANY CITY STATE COMPANY ZIP CODE KERR McGEE CCRPORATION P.O. BOK 89 CUSHING OK 74023 JEFF OSTMEYER I

PAGE 1 i

,o,.~,.~.--,--.w.,.,.-,

,-.o.--.m-n,.e.~.....,o-,s...,.u...

~.e.,*,...-...

O'?8 If a %k'n' 4,rkYttep#8 & ( t. '. k IDDf MS b4Bf8 L MIOf 8808859 84f4WWWU' 4%W flC RIP 9W.R* Sk ID 38 @ Mte.i 8t(13 ttf amt W r.0'erMfi'44'd*4.sp.'4 tp 'Milb*It b ks Fgt sp'WB.d t W4y pr 19t*' 44p.8 94W'9 & 4W'Ot*1.W4 til 48V 4D' S 13 s.

c

4 t

rw-m 8'efter e c'f eeng w rt 4NS e testreIICMPt W@ 9%ur'm ast 'ptuvi e i4*sitt W tesest5 sv 'c' er% a..,was. achitosassegue b a repuff 48W r4-8 terp8asths.esd ess og r ett.%fmv estNonal Itty esittier ainyttes de Ldi.1.steue tttvists

}WLAB CORE LABORATORIES LA80 RAT 0RY TE$TS RESULTS 09/27/95 JOS NUMBER:- 951926 CUSTOMER: KERR Mc0EE CCAPORATION ATTW: JEFF OSTMEYER CLIENT 1:9.........: ANNUAL ENVIRONMENTAL CMW 20.2 LABORATORY 1.D...: 951926-0001 DATE SAMPLED.......: 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPTION...: CU2-26 025 REMARKS..........: WATER TEST DESCRIPfl0N FINAL RESULT-DETECTION LIMIT UNITS OF MEASURE TEST K THOD DATE TECHNICIAN Gross Alpha, totat 70.3 pcl/l EPA 900.0 08/30/95 NRF Gross Alpha, total, error, +/-

36.4 pcl/l 08/30/95 NRF Gross Alpha, total, LLD 37.7 pCl/l 08/30/95 MRF Gros) Seta, total 55.6 pCl/l EPA 900.0 08/30/95 NRF Gross Seta, total, error, +/-

33.8 pCf/l 08/30/95 NRF Gross Beta, total, LLD 52.1 pcl/l 08/30/95 NRF Thortun 232, total 1.48 pCf/l 09/25/95 DW Thoriun 232, total, error, +/-

0.6 pCf/l 09/25/95 DW Thoritsa 232, total, LLD 0.3 pCf/l 09/25/95 DW i

Uranlun 234, total (150 ll) 0.9 pCl/l CA GLR R405 09/26/95 DW Uranlun 234, total, error, +/-

0.4 pct /t 09/26/95 DW Uranlun 234, total, LLD 0.4 pcl/t 09/26/95 DW Uraniun 235, total (150 U) 0.0 pcl/l CA-GLR-R405 09/26/95 DW Uraniun 235, total, error, +/-

0.0 pCI/l 09/26/95 DW Urantun 235, totst, LLD 0.3 pCf/t 09/26/95 DW Uranitsn 238, total (ISO U) 0.4 pCi/l CA-GLR R405 09/26/95 DW Uranium 238, total, error, +/-

0.3 pcl/l 09/26/95 DW Uranlun 238, total, LLD 0.2 pCl/l 09/26/95 OW Thoriun 228, total 1.7 pCl/l 09/26/95 DW Thiriun 2c8, total, error, +/-

0.7 pCi/l 09/26/95 DW Thortun 228, total, LLD 0.7 pcl/l 09/26/95 DW 420 West First Street Casper, WY 82601 (307) 235-5741 PAGE:2

,, ~,..

m. ~m ~,

..n

-a.~~.=~a.m

. =,*~ w.w~..

~~~~-~~a-o---

- =~~ - **"+-

pme epig gyg,gt gaggqyges, et ( my (,ylpur y p-

. Arm pga og balppuppew Awam.tS-..gmmhy 4ei6 e ases e gass 4My.* wgs'as sepM.t! @,

puWest w 4M d"beMFWI y FM & F "4 M C -

  1. MW @ 8h l'

-tOer SPMt.4 $ EFf(IpN19 pee W R Ytd S ( F ** id. IPeM'Pe4 h dusDiaPI 4 gwtf G' se>=seG bgr.m In* Hit t=#-P s#.%#v1.wpa JN ryggf8 s p etft'P4 ryg38419ds af6 p5?&lH # itt M8MD WN? t'$ 9'418511#6 4

s4.W $'lHW4

  • 4 8 4 TMB g

CORE LABORATORIES QUALITY C0NTR0L REP 0RT 09/27/95 JOB NUMBER: 951926' CUSTOMER: KERR McGEE CORPORATION ATTMs JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS NATRIX SPIKES ANALYS!$

ANALYSIS ANALYS!$

ANALYZED ir L ICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE 1.D.

VALUE (A)

VALUE (B)

(\\ABj)

VALUE RECOVERY VALUE ADDEL RECOVERY PARAMETER: Gross Alpha, totat

. DATE/ TIME ANALYZED 08/30/95 14:05 QC BATCH NUMBER 170093 REPORTING LIMIT /DF UNIT 5:pCl/t METHOD REFERENCE : EPA 900.0 TECHNICIAN:NRF BLANK MB M82A80829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963-1 124 10.0 128 89 DUPLICATE MD 951963 1 10.0 14.6 37 PARAMETER: Gross Beta, total DATE/TI,1E ANALYZED 08/30/95'14:14 QC BATCH NLMBER 170097 REPORTING LIMIT /DFs UNITS:pCf/t METHOD REFERENCE EPA 900.0 TECHNICIAN:NRF BLANK MS Ms2A80829 0.4 STANDARD LCS t.C1s0829 23.9 22.0 109 SPIKE MS 951963 1 144 5.0 110 126 DUPLICATE MD 951963 1 5.0 8.8 55 PARAMETER Thori a 232, total-DATE/ TIME ANALYZED:09/25/95. 16:49 QC BATCH NUMBER 171053 REPORTING LIMIT /DFs UNIT 5 pci/1 METHOD REFERENCE

. TECHNICIAN:DW BLANK Ms Me5T0906 0.47 BLANK Ms MS6T0906 0.95 STANDARD LCl ST3T0906 7.59 7.C 108 STANDARD LCS LC3T0906 7.1 7.0 101 SPIKE MS 951921 1 16.3 0.92 14.0 110 DUPLICATE MD 951922-1 0.61 0.89 37 TARAMETER:Thori m 228, total DATE/ TIME ANALYZED 09/26/95 08:19 OC BATCH NUM8ER:171058 REPORTING LIMIT /0F:

UNITS pCi/t METHOD REFERENCE :

TECHNICIAN:DW BLANK Me Me5TD906 0.18 BLANK MS M86T0906 0.01 STANDARD LCS ST3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921 1 18.0 0.35 14.0 126 DUPLICATE MD 951922-1 0.74 0.86 15 PARAMETER:Urani a 234, total (ISO U)

DATE/ TIME ANALYZED 09/26/95 10:46 QC BATCH NUMBER 171081 REPORTING LIMIT /DF UNITS:pci/l METHOD REFERENCE 2CA GLR-R405 TECHNICIAN:DW BLANK MS M81UO906 0.2 BLANK MB M82UO906 0.4 STANDARD LCS ST1UO906 7.8 7.8 100 STANDARD LCS LC1UO906 7.7 7.8 99 DUPLICATE MD 952012 2 127 131 3

PARAMETER:Urani m 235, total (ISO U).

DATE/ TIME ANALYZED:09/26/95. 11:13 OC BATCH NUMBER 171088 REPORTING LIMIT /DFs UNITS:pci/t METHOD REFERENCE :CA-GLR-R405 TECHNICIAN:DW BLANK MS M51UO906 0.0 420 West first Street Casper, WY 82601 (307) 235-5741 PAGE:3

.4,

-.,-.w

,-.,n.u-,-~.-m.om.,_.,.,,,,,,,m,.,,,m,.i,.....,-,.,.M,.

    • tte th. Ig.gf gg'qy'emagens g6 (apg L,tfe'r'.l'"'

.c "* 4 41'.Ifflh.E 4t##WrI8 esMar t.a Itp 1.igan'tq4 petty.stel fp th.g rtsj W.gF.tnts t. 9.pu r>,.nf Ttsm..sgs.st. IpfMLan gtp i4Agg Py p+'igag h.it, (p speww,nrge w" se pw'p.ngr%t W 3+1 Q pi e

se e

  1. Wf % Pane,tl(W35b.89y pun ger m.ggnig * '"' s.ber' FM WN p %K't Ierts019 et nah.$ 418.6dS4P ed.On 10' Jfly '. Item WP/I4dmetf8 ItM WOO 99 491 W. rtre' ts, f.p*allt..ql su segW tit.P. 't "g g pipwisj1 %..*sqte" 3plFtat.I'Jf 1 Diss & ltaus FD8 et

i i

gdD CORE LABORATORIES I

1 l

QUALITY CONTROL REPORT 09/27/95 JOB NUMBER: 951926 CUSTOMER: KERR McGEE CORPORATION ATTN: JEFF OSTMEYER l

l ANALYSIS DUPLICATES REFERENCE STANDARDS NATRIX SPIKES ANALYSIS ANALYS!$

ANALYSl$

ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE I.D.

VALUE (A)

VALUE (B)

(lABl}

VALUE RECOVERY VALUE ADDED RECOWRY l

PARAMETER:Uranita 235, total (ISO U).

- DATE/ TIME ANALYZED 09/26/95 11:13 QC BATCH lutBER 171088 l

REPORTING LIMIT /DF.

. UNITS:pCl/l-METHOD REFERENCE 3CA GLR R405'

-TECHNICIAN:DW l

BLANK Ms Ms2UO906 0.0 l

DUPLICATE MD 952012 2 5.4 6.0 11

[

PARAMETER:Uranita 238,' total - (ISO U)'

DATE/ TIME ANALYZED:09/26/95 '11:19 oC BATCH NUMBER 171092 REPORTING LIMIT /DFs UNITS pCl/l METHOD REFEREN E' :CA GLR *R405 TECHNICIAN DW j

j BLANK MS M51UO906 0.1 BLANK Ms M82UO906 0.1 STANDARD LCS ST1UO906 7.4 7.2 103 STANDARD LCS LC100906 8.0 7.2 111 DUPLICATE MD 952012-2 57.4 57.4 0

l d

420 West First Street Casper, WY 82601 (307) 235 5741 PAGE:4 2,

o~

. ~

.. e.m.a e.,..-, i o..-. - n. - % r, a.e. ~.

. o w

.,o..,,,,.. s

,e-.

o.---e-...

-.o,-~4.w.

.e p#w gnarv 6dfttl'9tE"'I.' let'8tf ( ADW Gffledt*- ( J't a.bOfibl10s@4 ft' h e Wr'59 %IM 41*(rP" O' % 4fT Nt IRM PR e a" 1ety Os tesgatesettl 31

-4 e psy *. tv.7 p.pd3 tr 1.s qYg pehuld $str49 gespen.Magt thrWi% 0.9 prML 4thWH#' i (18.m. W 14.'

r e

d at sensuma Wi pffismit'W A8W Gr Settid II' f.4%'serse W4f5$9m.r D 4

e c' dgigin3 0+ 't-we9 A P J 4 =g e stets er'.tf%)psy* I felttsrl &P.& st& tbsedety t:ftse.e4 te st ep0 cr. t-yrhq. ef tiV PEMs erstferte 3D6#8th D' 88 d.

W l'dt' thWM

1MB g

CORE LABORATORIES QUALITY CONTROL FOOTER METHOD REFERENCE $

(1) EPA 600/4-79420. Methods for Chemical Analysis of Water and Wasten. March 1983 (3) EPA SW-846. Test Methods for Evalualmg Sohd Waste. Third Editiort November 1990 and July 1992 update (3) Standard Methods lir the Exanunauon of Water and Wastewater.17tik 1989 (4) EPA 600/4-R0 032. Prescnhed Procedures for Measurement of Radioacuvity in Dnnking Water. August 1980 (5) f ederal Register. Fnday. October 26,19N4 (40 CFR Part 136)

(6) EPA 600/R.78417. Micruhiological Methods for Morutonns the Environment. December 1978 COMMENTS (I) W data m the Laboratorv Test Results Report may ddrer from the data m the OC Report due to calculanons for sarnple preparauon ardor dduuans.

(3) The ' Time Analvred" in the OC Report may not reflect the actual time of each analms. The "Date Analyzed"is the actual date of analysis.

(3) Sod and sludge samples are reported on a wet basis or on an "as received" basis unkas otherwise mdicated.

(4) The data in this report are withm the hmsts of uncertamry specif id in the refenneed method unless otherwise mdicated (5) Analyses performed by a subcontract laboratory are indwated with an astensk and associated code m the "Techrucian" data field Subcontract Laboratones Cgde Corelaboratones. Anaheim CA

  • AN Core Laboratonca. Aurora.CO

'AU Core Laboratones. Casper, WY

  • CA Core Lahnratones. Corpus Chnstt TX
  • CC Core Laboratones. Houston.1%
  • HP Core laboratones. take Charles. LA
  • If Core Laboratonea. leng Beach. CA
  • LB Other Subonntract Laboratones
  • XX DEFINITIONS (l) NC = Not Calculable due to values lower than the reportmg lumt.

(2) ND

  • Not Deta:ted above the reportmglurut.

OC SAMPLE IDENTIFICATIONS BLANKS SPIKES MB - Method Diank (also referred to as a preparsuon blank)

MS - MainxSpike RD = Reagent Diank MSD = Mainz Spike Duphcase IB. Instrument Blank PDS = Post Digestion Spike ICD - ImtialCahbranon D1snk BS = Blank Spike (also referred to as a rnethod spike)

CCD = Contmums Cahbranon Blank SS = Surrogate Spike llD = Holdmg Diank (also referred to as a storage blank)

REFERENCE STANDARDS DUPLICATES i

CS = Calibrauon Standard MSD = Mainx Spike Duplicate RS = Reference Standard (also refernd to as an external nference standard)

MD < Method Duphate ICV = ImtialCahbrauon Venficauon CCV = Contanums Cahbrauon Venficauon IIS - LaboratoryControlSample 420 West First Street Casper, WY 82601 (307) 235-5741

.~, e.~,

u m.~. 4 W,

.~ --

---e..-~.~..=.--Me.~---

---u+~~-a~~

.M $fty 9

4. g?"'ti,1 MP 4 r f.i.,$NU A..% ( f '. L alWyt*rgpa l'@er.s.f @ w M R$ 9 -pi 4=% 41 #48*.%. W Wg W 558'W" NA NW 4 Y "tM 8 I 4WM4 N WW +WM M 'MN D d D
  • M 8 N W f

e

,~.

.. ~,,.-~. ~ - - -., -.,.

-r

,,,.n,~..,,,

_..,mm.4,...,

)

CORE LABORATORIES, INC.

5295 Holl ster Road h\\d, Houston. Texas 77040 I'a ge : I j

(713) 460-9600 i

i l

Sample Receipt Acknowledgment l

ate M/2$/95 R

t l

e n

p kERR Mc0EE CORPORATION v 3AnE l

o P.O.00X 89 o

' CUSli!Ni, OK 74023 I

t Jfff 051MEYFR c

1 T

T o

o l

' Core Laboratories Customer Estimated Job Number Project ID Completion Date 951976 AhNUAL INVIRChMENTAL Cr:0 til.2 ggf;.1/95 Sample #

Customer ID Remarks i

0001 CU2-24-025 UATE81

.E D En '"'

SEF 0 5 1995 Enviran :t'r9'rio r

safety &

if you have env pestier.s please call Core Laboratories, Casper, bV i307) 135-5741 THIS IS NOT AN INVOICE Order subject to our salos agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

ursi +. c..c.-o, oi....

i-w ra.

.::..... =

_..... 7.,.._... y

,,9

.g.y..,.;.g........

c5e25/95

.~E wile *IE~W~~.*ET:iEE~Illl%I"*[4-TEEEET:W G ill5 ^

~~~~'::Efii:I~EIf?ITRlIlf~~~~

i GE7I~~~~~

~~

Buhl N! EER:NO) 0,,TE TECElvE3 08/24/05 Tit;E RECEIVEL 10 00 sal:pLE CATE CS/23/65

? W LE tit 12 QUE CATE Gi/21/H FROJECT ID. ANNUAL ENVIRDhMENTAL CW 20.2 5 AMPLE ID:CU2-26-025 REM: WATER JB e0TES:11&L CLSE 54]RT 13:

i!N b)REER L

0,E TEST DESCRlpTION TEST LIMITS UNIT 3 0F HEASURE TEST NETHOD COMMENTS AC00 USAT CrECE IDR 153 V R513 3ross Alpha, total pCi/l EPA 500.0 1514 Gross Alpha, total, error, +/-

pCi/l F515 Gross sloha, total, LLO pC /l E516 Gross Beta, total pCi/l epa 900.0 R517 Gross Eeta, tctal, error, +/-

pC1/1 R518 6 toss Beta, total, LLD pCi/l A5:5 Thorium 232, total pCi/l R556 Thortus 232, total, error, +/-

pCi/l R557 Thorica 232, total, LLD pCi/l R561 Uranium 234, total (ISO UI pC /l CA-GLR-R405 6562 brantur 274, total, trrer, tr-pCi/l Eb3 Uranium 234, total, LLD pCi/l M64 sranium 2 5, total (150 0) pCul C4-s.R-R405 E5e5 Uranaus 235, tatal, error, t/-

pCi/1

?5(o vrantum 2?5, t tal, J.3 pC2/1 R:67 tranium 23B, total !!SD U1 pCi/l CA-6LR-R405

?560 srannun. 233, total, error, O -

pCa/l R569 Uranius 238, total, LLD pCi/l A570 lhorium 223, tctal pC3/1 R571 TForius 228, total, error, t/-

pti/l 6572 Thcriur 223, t etal, di, pCi/l

_....,p

.2 8..**

80

'***~-

i EEh m

gmy

$ h e

s5 e S

g a

_1 o

85

$ 2 l an m n 3

m-R5

-=

uo m

O ER gE g]

[

-0 casm g5 n_~3 m

{ o1 l

og

=

0

$s a e

E*x

{

s N

D 3

o' ESW Y h W !

m 4

A b5 Pm3E E H El b

h3g5

' 5!

R O i m*

"ES l

l ll l !g!

j E

3 5

m ga

20

$h

  • I E 3!

m

\\

o o

o o

bh T

T T

I 3 :

\\

U C l mt

~

  1. CONTAINEgg g

cr d

1 ul w^m

\\

2 :

g'

\\

SOIL f

g j

AIR l

9 Z I l

8

\\

SLUDGE g

g

{

gpig i

OTHER

$5

{

g,

\\,

og8 N

gg i

g HNO3 f

m

~

n ist m

g, 6 ! sr 8

1

"==

  • %E

\\

ICE em P

Ng a E

'l.

m am g4

]$

2 l\\

NONE i

5g

~0l e

W I Eg M !

li 3]

g gg g

i s

15 R se a

n}

=

e~

I I

I I

]

7 w

m a

a a

6

" ~*

M e

s a

g M

)

W 3

w M

M L

g P

4 m

}(,

\\*1 6

m a

9 l

k Q

g 9

)

5 N

8

=

U

?

h 5

E k

E e!

\\

g g

}

l

\\

l METALS:

O ARSENIC O CADMtuM d

g$

l l

\\

O CHROMlUM CCOPPER 13 3

l l

\\

OLEAD 0 SELENIUM Q ZINC i

m M -Q C.,

zgm l

l

\\

m GROSS ALPHA RADIOACTIVITY EgM l

l

\\

PH Q

9}

l

}

)

SULPHATE M

A 2

i R

K l

l

\\

OIL t. GREASE 2

3 g

3 l

\\

TOTAL URANIUM j

{%

g l

r-ISOTOPIC:t2HJ234 $U235 MU238 n

l j

TOTAL THORIUM Y

g 3

N l

\\

s ISOTOPICd5 Th232 N Th 228 b $

N l

j CLP:

O METAL O SEMI VOA O VOA m

l l

\\

TCLP:

O METALC SEMIVOA O VOA h!p f l

j j

\\

O REACTIVITY O CORROS!VITY 3$ Q R l

l

\\

IGNITABILITY s

j h P N of l

l

.l

\\

FLASH POINT i

y i5 s

> m l

l l

\\

l dress ScTA fadissd;v;fy l

9' I

i i

i l

..

Retrieved from "https://kanterella.com/w/index.php?title=ML20207C027&oldid=4040936"