ML20207B965

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Amended Rept for Core Labs Analytical Rept for Job Number 951923
ML20207B965
Person / Time
Site: 07003073
Issue date: 02/08/1996
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080302
Download: ML20207B965 (15)
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N ggM CORE LABORATORIES AMENDED REPORT

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.... ! CORE' IABORATORIES S T N A>LLYJ.T.:ITC~AELD R1E1P;O:RiT!

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KERR Mu EE
CORPORATION JEFF-OSTMEYERE xP.O. BOX"89 L CUSHING,:' OK ; L 74 023 :-

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Signature Date:

i Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor 9903080302 981106

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FINAL REPORT DISTRIBUTION 02/08/96 i

JOB NUMBER: 951923 CtBIPANY.MAME)

(XNIPANY MAILING ADDRES$'

COMPANY CITY STATE COMPANY ZIP CODE l

KERR McGEE CORPORATION Pe0s BOK 89 CUSHING OK 74023

' JEFF OSTMEYER 1

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CORE LABORATORIES LABORATORY TE$TS RESULTS 02/08/96 JOS NUMBERS.. 951923-.

CUSTOMER: KERR Mc0EE CORPORATION

-ATTN: 'JEFF OSTMEYER-CLIENT I.D.........: ANNUAL ENVIRONMENTAL CMW 14.2 LABORATORY I.D...: 951923-0001 0 ATE SAMPLED.......: 08/23/95 DATE RECE!VED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPTION... CU2 26 022 RENARKS..........: WATER TEST DESCRIPTION' FINAL. RESULT.

DETECTION LIMIT UNITS OF MEASURE TEST METNOD DATE.

afECNNICIAN Gross Alphs, total 135 pcl/l EPA 900.0 08/30/95 NRF Gross Alpha, total, error, +/-

48.0 pcl/l 08/30/95 NRF Gross Alpha, total, LLD 40.7 pcl/l 08/30/95 NRF 1

Gross Bets, total 91.3 pcl/l EPA 900.0 08/30/95 NRF Gross Beta, total, error, +/-

33.8 pci/t 08/30/95 NRF Gross Beta, total, LLD 49.2 pcl/L 08/30/95 NRF Thori a 232, total 0.49

' pci/1 09/25/95 DW Thori a 232, total, error, +/-

0.3 pct /L

' 09/25/95 DW Thoriun 232, total, LLD 0.3 pcl/l 09/25/95 DW Uranlue 234, total (ISO U) 17.7 pcl/l CA GLR R405 09/26/95 DW Uranium 234, total, error, +/-

2.5 pci/l 09/26/95 DW Uranium 234, total, LLD 0.2 pci/l 09/26/95 DW Uranium 235, total (ISO U) 0.4 pci/l CA GLR R405 09/26/95 DW Uranium 235, total, error, +/-

0.3 pcl/l 09/26/95 DW Uranlun 235, total, LLD 0.2 pCi/l 09/26/95 DW Urantun 238, total (!$0 U) 9.1 pCl/l CA-GLR R405 09/26/95 DW Uranium 238, total, error, +/-

1.6 pci/l 09/26/95 DW Uranium 238, total, LLD 0.3 pCl/t 09/26/95 DW Th:riun 228, total 1.3 pcl/t 09/26/95 DW Thoriun 228, total, error, +/-

0.6 pcl/l 09/26/95 DW Thorius 228, total, LLD 0.5 pci/t 09/26/95 DW 420 West First Street Casper, WY 82601 (307) 235-5741 PAGE:2 t.

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I gdD CORE LARORATORIES QUALITY CONTROL REPORT 02/08/96 JOB IRMBER ~ 951923!

CUSTOMER KERR McGEE CORPORATION

-ATTN ~^ JEFF OSTMEYER' l

ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SP!KE PERCENT (lABl}

VALUE RECOVERY VALUE ADDED RECOVERY TYPE SL2 TYPE I.D.

VALUE (A)

VALUE (B) 2 PARAMETER Gross Alpha, total:....

' DATE/ TIME ANALYZED:08/30/95.14:05-OC BATCH IRmBER 170093

' REPORTING LIMIT /DFt

~ UNITS pCl/l

' METHOD REFERENCE EPA 900.0 '

TECHNICIAN NRF BLANK Ms Ms2A80829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963-1 124 10.0 128 89 DUPLICATE MD 951963-1 10.0 14.6 37 PARAMETER:Grosa'Seta, totali DATE/ TIME ANALYZED:08/30/95 14:14-OC BATCH IRMBER:170097 REPORTING LIMIT /DF:.

. UNITS pCf/t METHOD REFERENCE : EPA 900.0-iTECHNICIAN:NRF 1

BLANK Ms Ms2AB0829 0.4 STANDARD LCS LC180829 23.9 22.0 109 SPIKE MS 951963 1 144 5.0 110 126 DUPLICATE MD 951963 1 5.0 8.8 55 PARAMETER:Thorita 232,' totalc

DATE/ TIME ANALYZED:09/25/95 16:49 GC BATCH NUMsER 171053

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REPORTING LIMIT /DFs

UNITS:pCl/l'

-METHOD REFERENCE. :

TECHNICIAN:DW BLANK Ms Me5T0906 0.47 i

BLANK MS M86T0906 0.95 i

STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101 SPIKE

'MS 951921 1 16.3 0.92 14.0 110 DUPLICATE MD 951922 1 0.61 0.89 37 PARAMETER: Thorium 228, total DATE/ TIME ANALYZED:09/26/95 08:19 QC BATCH NLMBER:171058

!REPORTINGLIMIT/DFs UNITS:pCl/L' METHOD REFERENCE :

TECHNICIAN:CW BLANK Ms Me5T0906 0.18 BLANK MS Ns6T0906 0.01 STANDARD LCS ST3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 SP!KE MS 951921 1 18.0 0.35 14.0 126 DUPLICATE MD 951922 1 0.74 0.86 15 PARAMETER:Uranque 234,' total (ISO U)

DATE/ TIME ANALYZED:09/26/95 10:46 QC BATCH NUMBER:171081 REPORTING LIMIT /DFs ~

UNITS:pCl/l' METHOD REFERENCE :CA-GLR R405-TECHNICIAN:DW BLANK MB MB100906 0.2 BLANK MB M82UO906 0.3 STANDARD LCS ST1UO906 6.6 6.6 100 STANDARD LCS LC1UO906 6.5 6.6 98 DUPLICATE MD 952012-2 107 110 3

PARAMETER:Uranita 235,. total (ISO U)

'DATE/ TIME ANALYZED:09/26/95: 11:13 -

OC BATCH NUMBER:171088 REPORTING LIMIT /DF:

' UNITS:pCl/t

' METHOD REFERENCE :CA GLR R405' TECHNICIAN:DW BLANK M8 MB1UO906 0.0 420 West First Street Casper, VY 82601 (307) 235-5741 PAGE:3 v

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A'N A-LY T:I'C'A L R E'P O R T.

..' Job-Number:

951923' Prepared For:

KERR McGEE CORPORATION JEFF OSTMEYER P.O.

BOX 89

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Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

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LABORATORY SUPERVISOR at r.c.niv OCT 0 21995 l

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FINAL REPORT CISTRIBUTION 09/27/95 JOB NUMBER: 951923 i

COMPANT MAME COMPANY MAILING ADDRESS COMPANY CITY STATE COMPANY ZIP CODE KERR McGEE CORPORATION P.O. BOX 89 CUSHING OW' T4023 JEFF OSTMEYER 1

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CORE LA: ORATORIES LABORATORY TE$T5 RESULT $

09/27/95 JOB MJMBER: - 951923-CUSTOMER KERR McGEE CORPORATION ATTN: ' JEFF OSTMEYER CLIENT I.D.........: ANNUAL ENVIRONMENTAL cNW 14.2 LABORATORT 1.D...s 951923 0001 DATE SAMPLED.......: 08/23/95 DATE REcEIV20....: 08/24/95 11ME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPTION...: CU2 26-022 REMARKS..........: WATER TEST DESCRIPTION FINAL RESULT DETECTION LIMIT UNITS OF MEASURE TEST METHCD DATE TECHNIC!AN Gross Alpha, total 135 pcl/l EPA 900.0 08/30/95 NRF Gross Alpha, total, error, +/-

48.0 pct /l 08/30/95 NRF Gross Alpha, total, LLD 40.7 pci/t 08/30/95 NRF Gross Beta, total 91.3 pci/t EPA 900.0 08/30/95 NRF Gross Beta, total, error, +/-

33.8 pcl/l 08/30/95 NRF Gross Beta, total, LLD 49.2 pci/l 08/30/95 NRF Thortun 232, total 0.49 pcl/l 09/25/95 DW Thorf un 232, total, error, +/-

0.3 pcl/l 09/25/95 DW Thortun 232, total, LLD 0.3 pct /l 09/25/95 DW Uranlun 234, total (!$0 U) 21.1 pcl/t cA-GLR R405 09/26/95 DW Uranlun 234, total, error, +/-

3.0 pci/t 09/26/95 DW Urantun 234, total, LLD 0.2 pci/t 09/26/95 DW Uranius 235, total

(!$0 U) 0.5 pct /t cA-cLR R405 09/26/95 DW Uranium 235, total, error, +/-

0.3 pci/t 09/26/95 DW Uranium 235, total, LLD 0.2 pci/l 09/26/95 DW Uranlun 238, total (ISO U) 10.8 pcl/l cA-cLR R405 09/26/95 DW Urantun 238, total, error, +/-

1.9 pci/l 09/26/95 DW Uranlun 238, total, LLD 0.4 pcl/l 09/26/95 DW Thorium 228, total 1.3 pci/t 09/26/95 DW Thortun 228, totat, error, +/-

0.6 pci/t 09/26/95 DW Thor!un 228, total, LLD 0.5 pcl/l 09/26/95 DW 420 West First Street casper, WY 82601 (307) 235-5741 PAGE22

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I GUALIfY CONTROL REPORT 09/27/95 JOB NUMBER 1 951925-

'CUBTOMER " KERR McGEE CORPORATION '

' ATTN' JEFF OBTMEYER~

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ANALYSIS DUPLICATES REFERENCE STANDARDS MATR!k SPIKES i

ANALYSIS ANALYS!$

ANALYSi$

ANALYZED CUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT j

TYPE BUS TYPE 1.0.

VALUE (A)

VALUE (B)

(lABl}

WALUE RECOVERY VALUE ADDEO RECOWERY

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DATE/ TIME ANALYIED:08/30/95 14:05 GC BATCN NUMBER 170093 PARAMETER Groes Alpha, total;....

REPORTING LIMIT /DFs'

-UNITB pCl/l

. METNOD REFERENCEJ EPA 900.0-TECWICIAN NRF i

BLANK MB MB2AB0829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963-1 124 10.0 128 89 DUPLICATE MD 951963 1 10.0 14.6 37 1

PARAMETER Grosa Geta, total ~

DATE/TIIE! ANALYZED:08/30/95 14:14 GC BATCH NLBIBER:170097 REPORTING LIMIT /DFs ~

1 UNITS:pCf/t METNOD REFERENCE 7: EPA 900.0 TECHNICIAN:NRF BLANK MB MB2AB0829 0.4 i

STAE ARD LCS LC100829 23.9 22.0 109 SPIKE MS 951963 1 144 5.0 110 126 I

DUPLICATE e

951963-1 5.0 8.8 55 PARAMETER Thorium 232f totall

' DATE/TIIE ANALYZED:09/25/95 ~ 16:49 GC BATCH MLBIBER 171053 REPORTING LIMIT /DFsJ '

UNITS pCf/t'

. METNQD REFERENCE 3 TECHNICIAN DW BLANK MB MB5T0906 0.47 BLANK MB Mg670906 0.95 STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101 SPIKE MS 951921 1-16.3 0.92 14.0 110 DUPLICATE e

951922 1 0.61 0.89 37

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PARAMETER:Thoriun 228, total DATE/ TIME ANALYZED:09/26/95 08:19 GC BATCH NUMBER:171058 REPORTING LIMIT /DF HNITS:pci/I METHOD REFERENCE :

' TECHNICIAN:DW l

BLANK MB MB570906 0.18 BLANK MB MB6T0906 0.01 STANDARD LCS ET3T0906 7.0 7.0

100, STANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921 1 18.0 0.35 14.0 126 DUPLICATE MD 951922 1 0.74 0.86 15 PARAMETER: Uranium 234,' total < (150 U) -

DATE/ TIME ANALYZED:09/26/95 10:46 0C BATCH NLMBER:171081 REPORTING LIMIT /DF UNITS pCl/l METHOD REFERENCE :CA GLR-R405 TECHNICIAN:DW BLANK MB MB1UO906 0.2 BLANK MB MB2UO906 0.4 j

STANDARD LCS 5T1U0906 7.8 7.8 100 STANDARD LCS LC1UO906 7.7 7.8 99 DUPLICATE MD 952012 2 127 131 3

PARAMETER: Uranium 235, total.-

(Iso U)

DATE/ TIME ANALY2ED:09/2i/95 11:13 GC BATCH NUMBER:171088 i

REPORTING LIMIT /DFs:

UNITS pci/l:

~ METHOD REFERENCE. :CA-Gi.R-R405 TECHNICIAN:DW BLANK MB MB1UO906 0.0 420 West First Street Casper, WY 82601 (307) 235 5741 PAGE33 i

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1 1% LAB nRD CORE LABORATORIES 1

l QUALITY CONTR0L REPORT 09/27/95 JOB NUMBER:' 951923 CUSTOMER: KERR McGEE CORPORATION

~ ATTN: JEFF OSTMEYER ANALYS!$

DUPLICATES REFERENCE STANDARDS NATRIX SP!KES l

ANALYS!$

ANALYS15 ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT VALUE (B)

(lABl)

VALUE RECOVERY VALUE ADDED RECOVERY TYPE SUS TYPE I.D.

VALUE (A)

PARAMETER Urant a 235, total (ISO U).

'DATE/ TIME ANALYZED 09/24/95 11:13 QC SATCH NLMBER 171088 REPORT!kG LIMIT /DFs UNITS pCl/t METHOD REFERENCE :CA GLR R405 TECHNICIAN DW BLANK MS MB2UO906 0.0 DUPLICATE e

952012 2 5.4 6.0 11 l

PARAMETER Urani a 238, total (ISO U)

CATE/ TIME ANALYZED 09/26/95 11:19 QC BATCH NUMBER 171092 REPORTING LIMIT /DFs UNITS:pCl/l-METMOD REFERENCE 2CA GLR *R405 TECHNICIAN DW BLANK MS M81UO906 0.1 BLANK MB M82UO906 0.1 STANDARD LCS ST1UO906 7.4 7.2 103 i

STANDARD LCS LC1UO906 8.0 7.2 til DUPLICATE MD 952012-2 57.4 57.4 0

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QUALITY CONTROL' FOOTER

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METHOD REFERENCES 1

j (1) EPA 600/4.79420. Methods for Chemical Analysis of Water and Wames. March 1983 (3) EPA SW.R46. Test Methods for Evaluatmg Solid Weste. Third Edition, Novemtwr 1990 and July 1992 update (3) Standard Methods for tlw Emanunanon of Water and Wastewater,17th,1989 (4) EPA 600/4-afM)32. Prenathed Pmeeduren for Measurement of Radioacuvay m Drmking Water, August 1980 i

(5) Federal Ragsster. Fnday. October 26.1984 (40 CFR Part 136)

(6) EPA 600/s.78 017. Miaoino6egwal Methods for Monitorms the Environunent. December 1978 l

1 COMMENTS 1

(1) The data in the laboratory Test Resuha Report may ddrer from the data m the QC Report due 10 calculations for sample preparnuon and/or dduuans.

(8) The " Time Analyzed"in the OC Report may nos reflect the actual time of each analysis. The *Date Analyzed"is the actual date of analysut (3) Sad and sludge samples are reported on a wet basis or on an "as received" basis unicas otherwise mdicrtect (4) The data m this report are within the hmrts of unartamty specified in the referenced methud unless otherwue indicatect (5) Analyses performed by a subcontract laboratorv are indicated wnh an amensk and assocsated code m the "Techrucian" d::: Nid j

Subcontract Laboratories Cgde l

Core laboratones. Anahemt CA

  • AN Cm laboratones. Aurora. CO
  • AU Core laborator:en. Casper. WY
  • CA Core Laboratones. Corpus Chnsti. TX

'CC Core Laboratones Houstort1%

  • HP l

Core taburatones. Lake Charles,IA

  • If Cm Laboratones Long Beach.CA
  • LB Other Subcontrait Lia

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'XX 1

DEFINITIONS (1) RC = Not Calculable due to salues lower than the reporting limst.

(2) ND = Not Detected above the reportmg Imut.

I OC SAMPLE IDENTIFICATIONS BLANKS SPIKES MB - Method Blank (also referred to as a preparation blank)

MS Mstnx Spiko

=

RB = Reagent Blank MSD = Mainx Spike Duplicate ID = Instrument Blank PDS = Post Digestion Spike ICB - InitialCalibration Blank BS Blank Spike (also referred to as a method spike)

=

CCB = Contmums Cahbration Blank SS Sunogate Spike

=

HD = lloidmg Blank (also referred to as a storage blank) 1 REFERENCE STANDARDS DUPLICATES CS Calibration Standard

=

MSD = Matnx Spike Duplicate RS Reference Standard (also referred to as an extemal reference standard)

=

MD Method Duptwate ICV = InrtialCalibrauon Venficauan CCV = ContmumgCalibrauon Venficabon trS = lahorntoryControlSample 420 West First Stn:et Casper.WY 82601 (307) 235-5741

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(713) 460-9600 Sample Receipt Acknowledgment j

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Customer ID Remarks 0001 CU2 26-022 UATER i

I REC EIVED SEP ('5'1995 Safety & Erviron Cushirm l

If you hase any questions please call tore Laboratories, (esper, Wt (307) 735-5741 THIS IS NOT AN INVOICE Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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SAMPLE NUMBER:OCO1 DATE RECEIVEO:08/24/95 TIME RECEIVED: 10:08 SAMPLE DATE.C8/23/95 SAMPLE TlHE:

DUE DATE:09/21/95 PRO KCT ID:AMMUAL ENVIRONMEMTAL CMW 14.2 SAMPLE ID:CU2 26-022 REM: WATER LAB MOTES:ll4L CUIE SHORT 10:

BIN huMBER.L CODE TEST DESCRIPT10M TEST LIMITS UNITS OF MEASURE TEST METHOD COMMENTS s

R000 UNAT CHECK FOR ISO U R513 tross Alpha, total PCi/l EPA 900.0 i

R$14 Gross Alpha, total, error, f/-

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,R$15 Gross Alpha, total, LLO pC1/1

, C16 Gross Beta, total pC1/1 epa 900.0 R$17 Gross Beta, total, error, f/-

pC1/1 R$t8 Gross Beta, total, LLD pC1/1 R555 Thorius 232, total pCi/l R556 Thorius 232, total, error, f/-

pCi/l R557 Thorium 232, tetal, LLO pC1/1 R561 Uranium 234, total (ISO Ul pCi/1 CA-6LR-R405 R562 Uranius 234, total, error, f/-

pCi/l R$63 Uranium 234, total, LLD pC1/1 R564 Uranium 235, total (ISO U) pC1/1 CA-6LR-R405 R563 Uranius 235, to1al, error, f/-

pCi/1 R566 Uranium 235, total LLO pCi/l R$67 Uranius 238, total (!$0 U) pCi/l CA-6LR-R405 R568 Uranius 238, total, error, f/-

pCi/l R569 Uranium 238, total LLD pCi/l R570 Thorius 228, total pCi/l R571 Thorius 228, total, error, f/-

pCi/l R572 Thortus 223, total LLD pCi/1 j

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N WRD CORE LABORATORIES QUALITY CONTROL REPORT 02/08/96 j

Jos IRmett N 951923.

- INSTOMER: ~ KERR McGEE CORPORATION :

ATTN JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SP!KES ANALYS15 ANALYSIS ANALYS!$

ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUB TYPE I.D.

VALUE (A)

VALUE (8)

(lA-Bl}

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER Uranium 235, totat::. -(190 U)-

DATE/ TIME AEALYZED:09/26/95 11:13'

' OC BATCH IK3GER:171088 REPORT!IM LIMIT /DFs:

UNITS:pC1/l.

- METHOD REFERENCE ' CA GLR-R405 TECHNICIAN:DW sLANK MS M52UO906 0.0 DUPLICATE MD 952012 2 4.5 5.0 11 PARAMETER Uranfue 238,' totet ?-(ISO U)-

DATE/ TIME ANALYZED:09/26/95 11:19 OC BATCH NUMBER 171092 REPORTING LIMIT /0Fs UNITS pCl/L METN00 REFERENCE CA-GLR R405 TECHNICIAN:DW BLANK MS MB1UO906 0.1 BLANK MS Ms2UO906 0.1 STANDARD LCS ST1UO906 6.2 6.0 103 STANDARD LCS LC1UO906 6.7 6.0 112 OUPLICATE MD 952012 2 48.2 48.2 0

420 West First Street Casper, WY 8?601 (307) 235 5741 PAGE:4 v.i.,-.nia.

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CORE LABORATORIES QUALITY CO."eTROL FOOTER METHOD REFERENCES (1) EPA 600 4-79420. Methods for Chemical Analysis of Water and Wastem. March 1983 (2) FPA SW-846. Test Methods for Evalualms Solid Waste. Third E&tson. November 1990 and July 1992 update (h Standard Methods lie the Exammation of Water and Wastewater.17th,1989 (4) EPA 600 4 N0412. Presenhed Procedurn for Measurement of Radaoacuvity m Dnnkmg Water, August 1980 (5) lederal Register. Enday. Ih1ober 26.19N4 (40 CFR Part 136)

(6) EPA 600 R-78417. Mwndnuk>gi6al Meuxxh fur Murutonna the Envirorunent, December 1978 COMMENTS

(!) Ihe data m the laboraturv Test Results Report may diiTer from the data m the QC Report due to calculations for sample preparanon andar dilutaans.

(2) The " Time Analyzed"in the OC Report may not tellect the actual tune of each analwis. The "Date Analyzed"is the actual date of analpis.

(3) Snd and sludge samples are reported on a wet basis or on an "as received" basis unless otherwise indicated.

(4) The data m this report are uithm the hmits of uncertamry speedied in the referenced method unless otherwise mdicated (5) Analyses performed by a subcontrast laborators are mdicated wnh an astensk and asaoetated code m the "Techrucian" data field.

Subcontract Laboratories Code Core labora1ones. Anaheim. CA

  • AN Core Lahorntonen Aurora.CO
  • AU Core Laboratones Casper. WY

'CA Core Lahorntones. Corpus Chruiu. TX

  • CC Core Laboratones Hnuston TX
  • HP Core laboratones L ike Charles. LA

'If Core Laboratones 1ong Beach.CA

  • LB Other Submnaract Laboratones
  • XX DEFINITIONS (1) NC = Not Calculable due to values lower than the reporting lumt.

(2) ND Not Detected above the reporting knut.

OC SAMPLE IDENTIFICATIONS BLANKS SPDGS MB - Method Diank (alm referred to as a preparation blank)

MS = Matna Spike RD - Reagent Diank MSD = Mains Spike Duplicate IB = Instrument Hlank PDS = Post Digestion Spike ICU - Initial Cahbrahon Blank BS - Blank Spike (also referred to as a method spike)

CCB = Conimums Calibration Blank SS = Surrogate Spike HD = Holdmg Diank (also referred to as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = CahbrahonStandard MSD = alatna Spike Duptwate RS = Reference Standard (also referred to as an external reference standard)

MD Method Duptwate ICV = truualCahbracon Venficahon

=

CCV = Conunums Cahbrauon Venficauon 14S = Laboratory Control Sarrele 420 West Ftrst Street Casper.WY 82601 (307) 235 57d1

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