ML20207B935

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Amended Rept for Core Labs Analytical Rept for Job Number 951919
ML20207B935
Person / Time
Site: 07003073
Issue date: 02/08/1996
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080296
Download: ML20207B935 (15)


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CORE LABORATORIES AMElNDED REPORT

CORE LIABORATORIES '

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m Jbb! Nitaber:i. : 951919;.

i Prepared ? For::

l KERR McGEE CORPORATION 1

- JEFFE; OSTMEYER :

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CUSHING,,OK: -.74023-

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ggRD CORE LA : ORATORIES FINAL REP 0RT DI$TRIBUTION 02/08/ %

c-JOB NUMBER: 951919 COMPANY.NAME:I COMPANY MAILING ADDRESS -

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LAB 0 RAT 0RY TESTS RESULTS 02/08/M J05' NUMBER'3951919/

f CUSTOMER:[KERR Mc0EE 'c0RPORATION :I i ATTNS JEFF OSTHEYER:

CLIENT !.D.........: ANNUAL ENVIRONMENTAL CMW 1.1 LABORATORY 1.D...: 951919-0001 DATE SAMPLED.......: 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPfl0N... CU2 26-018 REMARKS..........: WATER TEST DESCRIPfl0N;?

FINAL RESULT.

DETECTION LIMIT.

UNITS OF MEASURE TEST METHOD, DATE-

~ TECHNICIAN Gross Alpha, total 72.9 pcl/l EPA 900.0 08/30/95 NRF l

Gross Alpha, total, error, +/-

19.5 pci/l 08/30/95 NRF 1

l Cross Alpha, total, LLD 13.8 pcl/l 08/30/95 NRF 1

l Gross Beta, total 46.0 pcf/l EPA 900.0 08/30/95 NRF Gross Beta, total, error, +/-

14.1 pcl/l 08/30/95 NRF Gross Beta, total, LLD 19.9

Cf/t 08/30/95 NRF l

Thorium 232, total 1.88 pcl/t 09/25/95 DW Thorium 232, total, error, +/-

0.8 pci/l 09/25/95 DW l

l Thorium 232, total, LLD 0.6 pct /t 09/25/95 DW Uranlun 234, total (ISO U) 4.5 pci/L cA GLR R405 09/26/95 DW Uranlun 234, total, error, +/-

1.0 pcl/t 09/26/95 DW Uranfun 234, total, LLD 0.4 pcl/l 09/26/95 DW Uranium 235, total (150 U) 0.2 pcl/l cA-GLR R405 09/26/95 DW Uranium 235, total, error, +/-

0.2 pci/l 09/26/95 DW Uranlun 235, total, LLD 0.2 pc!/t 09/26/95 DW i

Uranlun 238, total (150 U) 2.3 pci/L cA GLR R405 09/26/95 DW I !

Uraniun 238, total, error, +/-

0.7 pci/L 09/26/95 DW lUranium 238, total, LLD 0.2 pct /L 09/26/95 DW Thoriun 228, tota 1 0.67 pc1/L 09/26/95 DW Thortun 228, totat, error, +/-

0.5 pcl/l 09/26/95 DW l

Thoriun 228, total, LLD 0.7 pcl/l 09/26/95 DW l

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g CORE LABORATORIES QUAL 17Y CONTROL REPORT 02/08/96 J05 NLMBERtF9519192 iCUSTOMER IKERR'McGEE CORPORAT!0N-ATTN: EJEFF OSTMEYER-ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SP!KE PERCENT TYPE SUS TTP!

I.D.

VALUE (A)

VALUE (B)

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VALUE RECOVERY VALUE ADDED RECOVERY i

PARAMETER: Gross Alphaj totat-DDATE/TIMEANALYZED:08/30/95'14:05

' QC BATCM NLMBER 170093 REPORTING LIMIT /DFs:

. UNITS:pCl/lo s METHOD REFERENCE : EPA 900.0:

TECHNICIAN:NRF BLANK MB MB2AB0829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963-1 124 10.0 128 89 DUPLICATE MD 951963-1 10.0 14.6 37

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PARAMETER: Gross Beta, total ~.

.DATE/ TIME ANALYZED 08/30/95 14:141

'QC BATCH NUMBER 170097 REPORTING LIMIT /DF UNITS:pCf/L'-

METHOD REFERENCE

  • EPA 900.0' LTECHNICIAN:NRF BLANK MS M82AB0829 0.4 STANDARD LCS LC180829 23.9 22.0 109 SPIKE MS 951963-1 144 5.0 110 126 DUPLICATE MD 951963 1 5.0 8.8 55 PARAMETERThorium 232i totati.........

~DATE/ TIME ANALY2ED:09/25/95 16:49.

QC BATCN IRMBER 171053 REPORTING LIMIT /DFac
UNITS
pcl/l'

--METHOD REFERENCE :

' TECHNICIAN:DW BLANK MB MB5T0906 0.47 BLANK MB M86T0906 0.95 STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101

SP!KE MS 951921 1 16.3 0.92 14.0 110 DUPLICATE MD 951922-1 0.61 0.89 37 PARAMETER
Thortun 228i total DATE/ TIME ANALYZED:09/26/95 08:19 QC BATCH NUMBER 171058 REPoetTING LIMIT /DFs UNITS:pci/l:

METHOD REFERENCE :

TECHNIC'AN:DW BLANK MB MB5T0906 0.18 BLANK MB MB6T0906 0.01

$TANDARD LCS ST3T0906 7.0 7.0 100 SVANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921-1 18.0 0.35 14.0 126 DUPLICATE MD 951922 1 0.74 0.86 15 PARAMETER:Urantun 234, total? (ISO U) '

DATE/ TIME ANALYZED 09/26/95 10:46 QC BATCH WlMBER:171081 REPORTING LIMIT /DF::

UNITS:pci/t METHOD REFERENCE :CA GLR R405 TECHNICIAN:DW i

! BLANK MB MS1UO906 0.2 BLANK MB MB2UO906 0.3 STANDARD LCS ST1UO906 6.6 6.6 100 STANDARD LCS LC1UO906 6.5 6.6 98 DUPLICATE MD 952012 2 10'.

110 3

PARAMETER:Uranlun 235, total, (ISO U)

DATE/ TIME ANALYZED:09/26/95 11:13 QC BATCH NUMBEW:171088 REPORTING LIMIT /DF:

UNITS:pti/t-METHOD REFERENCE :CA-CLR R405

-TECHNICIAN:DW BLANK MS M01UO906 0.0 420 West First Street Casper, WY 82601 (307) 235-5741 i

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ggRD CORE LABORATORIES QUALITY CONTROL REPORT 02/08/96 JOB NUMBER 1 951919I

CUSTOMER
fKERRMcGEECORPORATION9 ATTN JEFF OSTMEYER ANALYS15 DUPLICATES REFERENCE STANDARDS MATRIX SP!KES i

ANALYSIS ANALYS!$

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VALUE (8)

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-DATE/ TIME ANALY2ED:09/26/95' 11:13

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UNITS pCf/t
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~ ' TECMICI AN:DW BLANK Ms M82UO906 0.0 DUPLICATE MD 952012 2 4.5 5.0 11 PARAMETER:Uranfun 238,' total '(150 U) '

DATE/ TIME ANALYZED 09/26/95' 11:19 OC BATCH lueBER 171092 REEDRTING LIMIT /DFs.

. UNITS:pCl/l.

METHOD REFERENCE :CA GLR R&O5.

) TECHNICIAN:DW BLANK Ms MB1UO906 0.1 BLANK Ms M82UO906 0.1 STANDARD LCS ST1UO906 6.2 6.0 103 STANDARD LCS LC1UO906 6.7 6.0 112 DUPLICATE MD 952012-2 48.2 48.2 0

420 West First street Casper, WY 82601 (307) 235 5741 PAGE 4

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CORE LABORATORIES QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600 4-79 020. Methods for Cherrucal Analms of Water and Wastes. March 1983 (2) t PA 5W 846. Test Methods for Evalualms Sohd Waste. Third Ed:tiert November 1990 and July 1992 update (3) Standard Methods for the Exanunanon of Water and Wastewater.17th.1989 (4) EPA 600 4.R0 032. Prescrihed Procedures for Measurement of Radioacuvity m Dnnkmg Water August 1980

($) i ederal Register. Fnday. October 26.19N4 (40 CFR Part 136)

(6) EPA 600 R 78 017. Mwruhiologwal Methods for Murutonns the Enviraranent. December 1978 GlMMENTS (I) Dw data m the laboraiorv Test Resuha Report may difTer from the data in the QC Report due to calcuiations for sampe preparauon and or dilutions.

(2) Die " Time Analyzed" m the OC Report may not re(lect the actual time of each analysis The "Date Analyzed" is the actual date of analpis.

(3) Soil and sludge samples are reported on a wet basis or on an "as received" basis unless othetwtw mdicated.

(4) Die data m this report are withm the hmits nf uncertainry specified in the referenced method unless otherwise treheated (S) Arthses performed by a subcomract laborators are andwated unh an astensk and associated code m the *Techructan" data field Subcontract Laboratones Cgds Core laboratones. Anahemt CA

  • AN Core lahorntones Aurora.CO

'AU Core Laboratones - Camper. WY

  • CA Core laboratones-Corpus Chnssa. !%
  • CC Core Laboratones. Hmaston. TX
  • HP Core 12hurstones. Lake Charles. LA

'If Core Laboratones Long Beach.CA

  • LB Other Subcontract Laboratones
  • XX DEFINITIONS (l) NC = Not Calculable due to values lower than the reporung lumt.

(2) ND - Not Detected above the reputting knut-OC SAMPLE IDENTIFICATIONS BLANKS SPIKES MB - Method litank (also referred to as a preparauon blank)

MS - Matna Spike RB - Reagent Blank MSD = Matnx Spike Duphcate IB < Instrument Eilank PDS = Post Digeehan Spike ICB Initial Cabhration Blank BS = Blank Spike (also referred to as a methmi upake)

CCB - Continums Cahbration illank SS = Surrogate Spiks 118 = Holdmg Blank (also referred to as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = Cahbrauan Standard MSD = Matnx Spike Duptwate RS = Reference Standard (also referred to as an external reference standard)

MD Method Duphcate ICV = imuelCahbracon Venficauan CCV = Continums Cahbrauon Venficauan ifs = 1.aboratoryControlSample 420 West First Street Casper, WY 82601 (307) 235-5741 m.

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' Job Number:': '951919 Prepared For:-

KERR McGEE CORPORATION

.JEFF OSTMEYER P.O. BOX'89 CUSHING, OK 74023 Date:

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CORE LABORATORIES FINAL REPORT DISTRIBUTION 09/27/95 JOS NLMBER: 951919 COMPANY NAME :

COMPANY MAILING ADDRESS COMPANY' CITY STATE COMPANY ZIP CODE KERR McGEE CORPORATION P.O. BOX 89 CUSHING OK 74023 JEFF OSTMEYER PAGE:1

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CUSTOMER:~- KERR McGEE CORPORATION '

ATTN ' JEFF OSTMEYER LI ENT 1.D......... : ANNUAL ENVIRONMENTAL CMW 1.1 LABORATORY 1.D...: 951919-0001

) ATE SAMPLED.......: 08/23/95 DATE RECEIVED....: 08/24/95 f!ME SAMPLED.......:

TIME RECEIVED....: 10:08 JORK DESCRIPTION...: CU2 26-018 REMARKS..........: WATER TEST DESCRIPTIONt FINAL RESULT :

DETECTION LIMIT UNIT 5 0F MEASURE TEST METN00 DATE TECNNICIAN 3 rosa Alpha, total 72.9 pCf/l EPA 900.0 08/30/95 NRF iross Alpha, total, error, +/-

19.5 pCi/l 08/30/95 NRF 3roa3 Alpha, total, LLD 13.8 pCl/l 08/30/95 NRF 1ross Beta, total 46.0 pCf/l EPA 900.0 08/30/95 NRF 2 rosa Beta, total, error, +/-

14.1 pCl/l 08/30/95 NRF 3ross Beta, total, LLD 19.9 pCi/l 08/30/95 NRF Thortun 232, total 1.88 pCf/l 09/25/95 DW Thortun 232, total, error, +/-

0.8 pCf/l 09/25/95 DW Thorium 232, tMai, LLD 0.6 pCf/L 09/25/95 DW Jrani>m 234, total (ISO U) 5.4 pCf/t CA-GLR-R405 09/26/95 DW Jrantun 234, total, error, +/-

1.2 pCf/t 09/26/95 DW Jranlun 234, total, LLD 0.5 pCf/l 09/26/95 DW Jrantun 235, total (Iso U) 0.2 pCi/t CA-CLR R405 09/26/95 DW Jranlun.235, total, error, +/-

0.2 pCl/l 09/26/95 DW Jranlun 235, total, LLD 0.2 pCi/l 09/26/95 DW Jranlun 238, total (ISO U) 2.7 pCf/t CA-GLR R405 09/26/95 DW Jrantun 238, total, error, +/-

0.8 pcl/l 09/26/95 DW Jrantuu 238, total, LLD 0.2 pCf/l 09/26/95 DW Thorium 228, total 0.67 pCi/l 09/26/95 DW Thoriun 228, total, error, +/-

0.5 pCf/t 09/26/95 DW

.'hirium 228, total, LLD 0.7 pCi/t 09/26/95 DW i

420 West First Street Casper, WY 82601 (307) 235 5741 l

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CORE LABORATORIES QUALITY COMTROL REPORT 09/27/95 JOB NUMBER:) 951919 CUSTOMER:: KERR McGEE CORPORATION

' ATTN: ~JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES LNALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPO or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS-TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bl}

VALUE RECOVERY VALUE ADDED RECOVERY E'ARAMETER: Gross Alpha,- total:..

DATE/ TIME ANALYZED:08/30/95 14:05 cc BATCH NUMBER 170093 REPORTING LIMIT /DFs UNITS:pCl/l METHOD REFERENCE EPA 900.0-TECHNICIAN NRF BLANK Ms M62AB0829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963-1 124 10.0 128 89 XJPLICATE MD 951963 1 10.0 14.6 37 2ARAMETER: Gross Beta, total DATE/ TIME ANALYZED 08/30/95 14:14 oc BATCN NLmsER 170097 tEPORTING LIMIT /DFs

- UNITS:pci/l-METHOD REFERENCE EPA 900.0 TECHNICIAN NRF BLANK Me Ms2A80829 0.4 STANDARD LCS LC1B0829 23.9 22.0 109 SPIKE MS 951963 1 144 5.0 110 126

)UPLICATE MD 951963 1 5.0 8.8 55 PARAMETER Thorium 232, total-DATE/ TIME ANALYZED:09/25/95 16:49 OC BATCH NUMBER 171053 REPORTlWG LIMIT /DFs UNITS:pCl/l METHOD REFERENCE : -

TECHNICIAN:DW BLANK MB MB570906 0.47 SLANK MB Ms6T0906 0.95 STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101 SPIKE MS 951921 1 16.3 0.92 14.0 110 3UPLICATE MD 951922 1 0.61 0.89 37

'ARAMETER:Thortun 228, total.

DATE/ TIME ANALYZED:09/26/95 08:19 DC BATCH NUMBER:171058 REPORTING LIMIT /DF '

UNITS:pCl/l

- NETHOD REFERENCE :

TECHNICIAN:DW 3 LANK Ms Me5T0906 0.18 3 LANK MS M86T0906 0.01 STANDARD LCS ST3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921-1 18.0 0.35 14.0 126 DUPLICATE MD 951922-1 0.74 0.86 15 1

PARAMETER:Uranion 234, total ? (ISO U)

DATE/ TIME ANALYZED:09/26/95 10:46 GC BATCH NUMBER 171081 REPORTING LIMIT /DF:

UNITS:pci/l METHOD REFERENCE CA-GLR R405 TECHNICIAN:DW BLANK Ms Me100906 0.2 BLANK Ms M82UO906 0.4 STANDARD LCS ST1UO906 7.8 7.8 100 ETANDARD LCS LC1UO906 7.7 7.8 99 DUPLICATE MD 9520*2-2 127 131 3

PARAMETElt: Uranium 235, total

' (ISO U)

DATE/ TIME ANALYZED 09/26/95 11:13 QC BATCH NUMBER 171088 REPORTING LIMIT /DFs UNITS pCl/l METHOD REFERENCE :CA-GLR-R405 TECHNICIAN DW SLANK MS MS100906 0.0 l

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l ANALYSIS DUPLICATES REFERENCE STANDARDS NATRIX SPIKES l

ANALYSIS ANALYSIS ANALY$15 ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUB-TYPE 1.D.

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DATE/ TIME ANALYZED:09/26/95 11:13.

oc BATCH NUMBER 171080

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REPORTING LIMIT /DFs -

. UNITS pCl/l METHOD REFERENCE CA-GLR-R405 TECHNICIAN:DW i

l BLANK MS MB2UO906 0.0 l DUPLICATE MD 952012 2 5.4 6.0 11 1

CARAMETER: Uranium 238," total'(190 U)~

DATE/TIIE ANALYZED 09/26/95 11:19 OC BATCH NLAISER 171092 i

REPORTING LIMIT /DF:.

- UNITS pCl/l METHOD REFERENCE-lCA GLR R405 TECHNICIAN DW BLANK MS MB100906 0.1 i

l BLANK MB Ms2UD906 0.1

! STANDARD LCS ST100906 7.4 7.2 103 STANDARD LCS LC1UO906 8.0 7.2 111 l

DUPLICATE MD 952012-2 57.4 57.4 0

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420 West First Street Casper, WY 82601 (307) 235 5741 PAGE:4

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% LAB gE CORE LABORATORIES QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600/4-79420. Methods for Chenucal Analysis of Water and Wasten. March 1983 (2) EPA SW R46. Test Methods for Evaluatmg Solid Waste. nird Edition. November 1990 and July 1992 update O) Standard Methods for the Exanunanon of Water and Wastewater 17th,1989 (4) EPA 600/4-80 032. Presa hed Pmcedures for Measurement of Radioacuvity in Drinking Water, August 1990 (5) Federal Register. Fnday. October 26.19x4 (40 CFR Part 136)

(6) EPA 600/8-78417. Miachiological Methods for Monstonng the Environment. December 1978 COMMENTS (1) The data in the laboratory Test Results Report may differ frorn the data in the QC Report due to calculanons (ce sample preparantw and,or ddutions.

(2) De " Time Analyzed" in the QC Report may not reflect the actual time ofeach analvsta. & 'Date Analyzed"is the actual date of analysut

0) Soil and sludge samples are reponed on a wet basis or on an "as roccived"Imais unless otherwise mdicated.

(4) h data an this report are withm the limits of uncertamry specified in the referenced method unless otherwise indicated.

(3) Analyses petformed by a subcontract laboratorv are..ubcated with an astensk and associated code in the "Techrucian" data field.

Jgbcontract Laboratorig Cgdg Corelaboratones Anahrun,CA

  • AN Core laboratones. Aumra. CO
  • AU Core laboratones. Casper. WY
  • CA Core laboratones. Corpus Chnsti. TX
  • CC Corelaboratones Houston.TX
  • HP Care taburatones lake Charles. LA
  • 1E Core laboratones. lang Beach. CA
  • LB Other Sutuxntract laboratones
  • XX DEFINITIONS (1) NC = Not Calet.lable due to values lower than the reportmg lumt.

(2) ND = Not Detected above the reportmg lirrut J

j OC SAMPLE IDENTIFICATIONS l

BLANKS SPIKES MB = Method Blank (also referred to as a preparauon blank)

MS Matna Spike RD = Reagent Blank MSD = Marna Spike Duphcate ID = Instrument Blank PDS = Post Digestion Spike ICB - Initial Cahbratmn Blank BS Blank Spike (also refermd to as a method spike)

=

CCB = Contmums Cahbration Blank SS Surrogate Spike

=

llB = Holdmg Diank (also referred to as a storage blank)

REFERENCE 'iTANDARDS DUPLICATES CS Calibratson Standard

=

MSD = Matnx Spike Duplicate RS R.eference Standani (also referred to as an extemal reference standnd)

=

MD + Method Duphcste ICV = InstmalCalibration Verification CCV = Contmums Calibration Venfication IIS = 14horntoryControlSample 420 West First Street Casper,WY 82601 (307) 235-5741

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rp ) Jt CORE LABORATORIES, INC.

1 5295 Holkster Road E39' I g"

Houston, Texas 77040 (713)460 9600 Sample Fleceipt Acknowledgment Date 08/25/95 R

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Cors Laboratories Customer Estimated Job Number Project ID Completion Date 951119 ANNUAL INVIRONMENTAL Cnc 1.1 09/2t/95 l

Sample #

Customer ID Remarks 0001 CO2-26-018 WATER i

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i FtEC ElVFri SEP0 5 1995 Safety & Environ Go" If you have any questions pleast call Ccre Laborticries, Cast.cr. Ut (3071 235 5741 THIS IS NOT AN INVOICE Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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SAMPLE NUtiBER:0001 DATE RECE!VED:08/24/55 TIME RECEIVED 10:08 SAMPLE DATE:08/23/95 SAMPLE TIME: -

DUE DATE C9/21/95 PROJECT ID:A W UAL ENVIRONMENTAL CMW 1.1 SAMPLE ID:CU2 26-018 REN: WATER Lf3 NOTES:134L CUBE SHORT 10:

BIN NUMBER:L CDDE TEST DESCRIPTION TEST LIMITS UNITS OF MEASURE TEST METHOD COMENTS

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Rf00 UNAT CHECK FOR ISO U 4

R513 Gross Alpha, total pCi/l EPA 900.0 R514 Gross Alpha, total, error, f/-

pCi/l R515 Gross Alpha, total, LLD s

pCi/l Cl4 Sress Beta, total.

pC1/1 EPA 900.0

~ R517 Gross Beta, total, error, f/-

pCill R$18 Gross Beta, total. LLD pCi/l R$55 Thorius 232, total pCi/l R556 Thorius 232, total, error, +/-

pCi/l R557 Thortus 232, total, LLD pC1/1 R561 Uranium 234, total (ISO Ul pCi/l CA-6LR R405 R562 Uraniue 234, total, error, 4/-

pCi/l R563 Uranius 234, total, LLD pCi/l R564 Uranium 235, total (ISO U) pC1/1 CA-6LR R405 R565 Uranive 235, tc1al error, +/-

pC1/1 R566 Uranium 235, total LLD pCi/l

' R567 Uranive 238, total 1150 Ul pC1/1 CA-SLR R405

~ R568 Urantue 238, total, error, 1/-

pCi/l R569 Uranive 230, total, LLD pC1/1 I

A570 Thorius 228, total pC1/1 R571 Thorius 228, total, error, f/-

PCi/l R572 Thorius 226, total, LLD pC1/1 4

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