ML20207B818

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Core Labs Analytical Rept for Job Number 940636
ML20207B818
Person / Time
Site: 07003073
Issue date: 05/10/1994
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080256
Download: ML20207B818 (8)
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WESTERN ATLAS Core Laboratories I

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1 CORE LABORATORIES.

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' ANALYTICAL REPORT 1

Job Number:

940636 Prepared For:

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KERR-McGEE CORPORATION

'JEFF OSTMEYER P.O. BOX 89 CUSHING, OK 74023 Date:

05/10/94 l

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Signature Date:

Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor i

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JOS NUMBER: 940636 CUSTOMER: KERR-McGEE CORPORATION-'

-ATTN: 'JEFF OSTMEYER CLIENT I.D.........: BLOCK-104-E12-S-86 LABORATORY 1.D...: 940636-0001 DATE SAMPLED.......: 03/28/94 DATE RECE!VED....: 04/04/94 TIME SAMPLED.......: 10:00 TIME RECE!VED....: 10:00 WORK DESCRIPTION...: CU1*65 010 REMARKS..........: WATER TEST DESCRIPTION FINAL RESULT DETECTION LIMIT UNITS OF MEASURE TEST METHOD DATE TECHNICIAN Thoriun 230, total 1.0 pCl/t 05/02/94 JG

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i Thoriun 230, total, error, +/-

0.3 pcl/t 05/02/94 JG Thirium 230, total, LLD 0.5 pCi/l 05/02/94 JG Thirlun 232, total 0.6 pci/t 05/02/94 JG Thiriun 232, total, error, +/-

0.3 pct /t 05/02/94 JG Thortun 232, total, LLD 0.3 pCi/t 05/02/94 JG Vrcniun 234, total 1.4 pCf/t 04/29/94 PLJ Uraniun 234, total, error, +/-

0.4 pcl/l 04/29/94 PLJ Uranlun 234, total, LLD 0.2 pct /l 04/29/94 PLJ Uranlun 235, total ND pCf/t EPA 901.1 04/29/94 PLJ Urtniun 235, total, error, +/-

0.1 pCi/t 04/29/94 PLJ l

Urtniun 235, total, LLD 0.1 pCf/t 04/29/94 PLJ Uraniun 238, totat 0.5 pCi/l 04/29/94 PLJ Urtniun 238, total, error, +/-

0.2 pCi/L 04/29/94 PLJ l

Urtniun 238, total, LLD 0.2 pCi/l 04/29/94 PLJ l

Thoriun 228, total 0.9 pci/t 05/02/94 JG Thorlun 228, total, error, +/-

0.3 pCl/t 05/02/94 JG 1

Thortun 228, total, LLD 0.3 pCi/l 05/02/94 JG l

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BERE ATLAS Core Laboratories QUALITT C0NTR0L REP 0RT 05/10/94 JOB NUMBER: 1 940636 -

CUST0h2R: -KERR-McGEE CORPORATION:

ATTN: JEFF OSTMEYER-ANALYSIS DUPLICATES

- REFERENCE STANDARDS MATRIX SP!KES ANALYSIS ANALYS!$

ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SP!KE PERCENT TYPE SUS TYPE I.D.

VALUE (A)

VALUE (B)

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VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Urani a 234,. total DATE/ TIME' ANALYZED:04/29/94 -10:55 QC BATCH NUMBER:150616 REPORTING LIMIT /DF:

UNITS:pci/l METHOD REFERENCE :

TECHNICIAN:PLJ Bu.NK MB M811UO414 0.1 BLANK Me M821UO414 ND STANDARD-LCS LC11UO414 6.5 6.6 98 STANDARD-LCS ST11U0414 6.7 6.6 102 SPIKE MS 940631 1 11.3 2.4 8.2 109 DUPLICATE-ND 940634 1 -

441 3.3 22 PARAMETER:Uranim 235, total DATE/ TIME ANALYZED:04/29/94 11:18 QC BATCH NUM8ER:150622 REPORTING LIMIT /DF:.

-UNITS:pci/l METHOD REFERENCE : EPA 901.1 TECHNICIAN:PLJ BLANK MS M81!UO414 ND BLANK MB M821U0414 ND DUPLICATE MD 940634 1 ND 0.1 0

l PARAMETER: Uranium 238, total DATE/ TIME ANALY2E0:04/29/94 11:28

'QC BATCH NUMBER:150625 REPORTING LIMIT /DF:

. UNITS:pCi/L.

METHOD REFERENCE :

TECHNICIAN:PLJ BLANK' MB M811UO414 ND BLANK MB M821UO414 ND

..6.9 106 STANDARD LCS LC11UO414 7.3 STANDARD LCS ST11UO414 6.9 6.9 100 SPIKE MS 940631 1 10.8 1.3 8.6 110 DUPLICATE MD 940634-1 1.4 1.5 7

PARAMETER: Thorium 228, total-DATE/ TIME ANALYZED:05/02/94 15:03 QC BATCH NUMBER:150693 REPORTING LIMIT /DF:

. UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:JG BLANK MB MR3T0415 WD BLANK MB MB4T0415 0.1 STANDARD LCS ST210415 4.7 4.0 118 STANDARD LCS LC2T0415 3.7 4.0 92 SPIKE MS 940637-1 4.9 0.3 4.0 115 i

DUPLICATE MD 940633 1 0.5 0.6 18 i

PARAMETER Thorita 230, total.

DATE/ TIME ANALY2ED:05/02/94 15:10 QC BATCH NUMBER:150697 REPORTING LIMIT /DFs UNITS:pci/l

. METHOD REFERENCE :

TECHNICIAN:JG BLANK MB ~

M83T0415 0.1 BLANK MS M64T0415 ND STANDARD LCS' ST3T0415 2.0 1.7 118 STAND.'RD LCS LC3T0415 1.8 1.7 106 SPIKE MS 940632-1 2.3 0.2 1.7 124 DUPLIC ATE MD '

940633 1 0.5 0.3 50 420 West First Street Casper, WY 82601 (307) 235-5741 PAGE:2

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wastame ATLAS Core Laboratories QUALITY CONTROL REPORT 05/10/94 JOB NUMBER: 940636

' CUSTOMER: KERR-McGEE CORPORATION-ATTN: JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALYSIS ANALYS!$

ANALYZED DUPLICATE RPD or TRLE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS-TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bl}

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Thoriun 232, total DATE/ TIME ANALYZED:05/02/94 15:27 QC BATCH NUMBER:150701 REPORTING LIMIT /DF:

UNITS:pci/t.

METHOD REFERENCE :

TECHNICIAN:JG BLANK MB MB3T0415 ND BLANK M8 M84T0415 ND STANDARD LCS ST2T0415 4.5 4.0 112 STANDARD LCS LC2T0415 4.2 4.0 105 SPIKE MS 940637-1 4.4 ND 4.0 110 DUPLICATE Mo 940633-1 0.2 0.2 0

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MRW wasvann ATLAS Core Laboratories QUAUTY CONTROL FOOTER METHOD REFERENCES (l) EPA 600/4-79-020, Methcds for Chemical Analysis of Water and Wastes, March 1993 (3) EPA SW-846. Tcat Methods for Evaluating Solid Waste, T,iird Edstaan. Novernber 1990 and July 1992 update j

(3) Standard Methods for the Exanunauen of Water and Wastewater.17th.1989 (4) EPA 600 4-80432, Prescnbed Proudures for Measurement of Radaoactivity in Dnnking Water, August 1980 (9) Federal Register. Fnda). October 26.1984 (40 CFR Part 136)

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(6) ETA 600'8 78417. Miaubsological Methods fw Monitanng the Environment, December 1978 l

COMMENTS (l) N data in the laboratory Test Results Report may ddfer from the data in the QC Report due to calculatsons sur sanple preparauon and or diluuons (2) N " Time Anahzed"in the QC Report may not reflect the actual time of each analysis. The "Date Analyzed" is the actual date of analysis.

(3) Soil and aludge samples are reported on a wet basis or on an "as received" basis unless otherwise indscated (4) The data m Gus report are mtlun the imuts of uncertainty specified in the referenced method unless othermse indicated.

(5) Analyses performed by a subcontract laboratory are indicated with an astensk and associated code m the "Techrucian" data field.

j Subcontract Laboratories Code Corelaboratorica. Anahein CA

  • AN Core Laboratones Aurora.CO

'AU Core Laboratones. Casper, WY

'CA Cae laboratones. Corpus Chnsta, TX

  • CC Core Laboratones. Houston. TX
  • HP 1

Core Laboratones. lake Charles, LA

  • 14 Core laboratones - Long Beach, CA

Other Sutantract laboratonsa

  • U pfFINITIONS (1) WC = Not Calculable due to s alues lower than the reportmg Imut.

(2) ND = Not Detected above the reportmg hnut.

OC SAMPLE IDENTIFICATIONS BLANKS EL};ES MB = Method Blank (also refened to as a preparation blank)

MS - Matnx Spike RB = Reagent Blank MSD = Mainz Spike Duplicate IB = Instrument Blank PDS = Post Digesuon Spike ICB = buttalCalibrabon Blank BS = Blank Spike (also referred to as a method spike)

CCB = Contmuing Calibraton Blank SS = Surrogate Spike HB = Iloiding Blank (also referred to as as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = Calibration Standard MSD = Mainx Spike Duplicate RS = Reference Standard (also refened to as an extemal reference standard)

MD Method Dupheate ICV = 1rutial Calibration Verificatmn

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I CCV = ConunumgCahbrauonCahbrsuon IIS = Laburatory Control Sample 420 West First Street Casper.WY 82601 I

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cn Adme p.o Sample Receipt Acknowledgment e

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Customer ID Remarks mt

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THIS iS NOT AN INVOICE Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please cortact laboratory immediately, if any discrepancies are observed.

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SAMPLE NUMBER 0001 DATE CECEIVED:04/04/94 TIME RECEIVED 10:00 SAMPLE DATE:03/28/94 SAMPLE TIME:10:00 DUE DATE:05/02/94 PROJECT ID: BLOCK-104-E12-s-86 SAMPLE ID:CU1-65-010 REM: WATER LAS NOTES 114L CUBE SHORT ID:

SIN NUMBER:0 CIDE TEST DESCRIPTION TEST LIMITS UNITS OF MEASURE TEST METHOD C010eENTS R552 Thorfun 230, total pcl/l R553 Thortun 230, total, error, +/-

pCi/t R554 Thoriun 230, total, LLD pCi/t 4555 Thorium 232, total pCi/t R$% Thorium 232, total, error, +/-

pcl/l R557 Thortun 232, total, LLD pct /t' R%1 Urantun 234, total pcl/t R562 Uranlun 234, total, error, +/-

pCi/t R563 Urantun 234, total, LLD pcl/l i

R%4 Uranlun 235, total pCl/l EPA 901.1 R565 Urantun 235, total, error, +/-

pCi/1 R%6 Urani m 235, total, LLD pCf/t RM7 Uranlun 238, total pCf/L RS68 Urantun 238, total, error, +/-

pcl/l RS69 Urantun 238, total, LLD pCl/l l

R570 Thoriun 228, total pCi/l R571 Thortun 228, total, error, +/-

pcl/l R572 Thoriun 228, total, LLD pcl/l 1

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CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST bOf C bct8 5 cotAPANY NARAE:

ANALYSIS REQUEST CORAPANY ADDRESS:

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Note: Do not comanne Spectet Doctecton TNs sample meets at M

Bill & Report to:

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appropriate radiological.

Jeff Ostmeyer Note: Time of analysis & tech's these results with um :

name must be recorded on other Chain of requirements.

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