ML20207B844

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Core Labs Analytical Rept for Job Number 940637
ML20207B844
Person / Time
Site: 07003073
Issue date: 05/10/1994
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080264
Download: ML20207B844 (8)
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Text

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ESE WESTERN ATLAS Core Laboratories l

'C O R E -' L A B O R A T O R I E S ANA-LYTICAL R E P O R.T Job Number: '940637

. Prepared'For:

i KERR-McGEE" CORPORATION-JEFF OSTMEYER l

P.O. BOX 89 CUSHING, OK. 74023 Date:

05/10/94 i

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Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor l

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w a sirm a n ATLAS Core Laboratories LAB 0RATORY TESTS RESULTS 05/10/94 JOB NUMBER: 940637 CUSTOMER: KERR-McGEE CORPORATION ATTN: JEFF OSTMEYER CLIENT 1.D.........: BLOCK 12-E14-5 0 LABORATORY I.D...: 940637-0001 DATE SAMPLED.......: 03/25/94 DATE RECE!VED....: 04/04/94 TIME SAMPLED.......: 15:30 TIME RECE!VED....: 10:00 WORK DESCRIPTION...: CU1-65 011 REMARKS..........: WATER TEST DESCRIPTION -

FINAL RESULT DETECT!DN LIMIT UNITS OF MEASURE TEST METHOD DATE TECHNICIAN Tharlum 230, total ND pCl/l 05/02/94 JG Thorium 230, total, error, +/-

0.1 pcl/l 05/02/94 JG thorium 230, total, LLD 0.4 pCi/l 05/02/94 JG Thori m 232, total ND pCi/l 05/02/94 JG Thorium 232, total, error, +/-

0.1 pCi/l 05/02/94 JG Thori m 232, total, LLD 0.2 pCi/l 05/02/94 JG Uranium 234, total 1.3 pCi/l 04/29/94 PLJ Uranium 234, total, error, +/-

0.3 pCi/l 04/29/94 PLJ Uranium 234, total, LLD 0.2 pC1/l 04/29/94 PLJ Urtnium 235, total ND pCi/l EPA 901.1 04/29/94 PLJ Urtni m 235, total, error, +/-

0.1 pci/l 04/29/94 PLJ Urtni m fji, total, LLD 0.2 pCi/l 04/29/94 PLJ Urani m 238, total 0.9 pCi/l 04/29/94 PLJ Uranium 238, total, error, +/-

0.3 pci/l 04/29/94 PLJ Urtnium 238, total, LLD 0.2 pci/l 04/29/94 PLJ Thorium 228, total 0.3 pcl/l 05/02/94 JG Thorium 228, total, error, +/-

0.2 pCi/l 05/02/94 JG Thorium 228, total, LLD 0.3 pci/l 05/02/94 JG i

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420 West First Street i

Casper, WY 82601 (307) 235-5741

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EERE wasunn ATLAS Core Laboratories QUALITY CONTROL REPORT 05/10/94 J0S. NUMBER: 940637:

CUSTOMER: KERR-McGEE CORPORATION ATTN: JEFF OSTMEYER ANALYS!$

DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSl$

ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS-TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bl}

VALUE RECOVERY VALUE ADDED-RECOVERY PARAMETER:Uranlun 234, total' DATE/ TIME ANALYZED:04/29/94 10:55 QC BATCH NUMBER:150616 REPORTING LIMIT /DF UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:PLJ BLANK MB M811UO414 0.1 BLANK MB M821UO414 ND STANDARD LCS LC11UO414 6.5 6.6 98 STANDARD LCS ST11UD414 6.7 6.6 102 SPIKE MS 940631 1 11.3 2.4 8.2 109 DUPLICATE MD 940634-1 4.1 3.3 22 PARAMETER:Urantun 235i total i

REPORTING 1!MIT/DFs UNITS pCf/t

. DATE/ TIME ANALYZED:04/29/94 11:18 QC BATCH NUMBER:150622 METHOD REFERENCE : EPA 901.1 TECHNICIAN:PLJ BLANK M8 M811UO414 ND BLANK MS M821UO414 ND DUPLICATE MD 940634 1 ND 0.1 0

PARAMETER:Uranlun 238, total -

DATE/ TIME ANALYZED:04/29/94 11:28 QC BATCH NUMBER:150625 REPORTING LIMIT /DF:

UNITS:pCl/l

.' METHOD REFERENCE 6

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TECHNICIAN:PLJ BLANK MB MB11U0414 ND BLANK M8 MB21UO414 ND STANDARD LCS LC11UO414 7.3 6.9 106 STANDARD LCS ST11U0414 6.9 6.9 100 SPIKE MS 940631 1 10.8 1.3 8.6 110 i

DUPLICATE MD 940634-1 1.4 1.5 7

PARAMETER:Thortun 228, total -

DATE/ TIME ANALYZED:05/02/94 15:03 QC BATCH NUMBER:150693 REPORTING LIMIT /DF

' UNITS:pCf/L METHOD REFERENCE :

TECHNICIAN:JG BLANK MB MB370415 ND BLANK

- kB MB470415 0.1 STANDARD LCS ST2T0415 4.7 4.0 118 STANDARD LCS LC270415 3.7 4.0 92 SPIKE MS 940637-1 4.9 0.3 4.0 115 DUPLICATE MD 940633-1 0.5 0.6 18 PARAMETER:Thortun 230, total DATE/ TIME ANALYZED:05/02/94 15:10 QC BATCH NUMBER:150697 REPCTING LIMIT /DF:

UNITS:pci/l METHOD REFERENCE :

TECHNICIAN:JG BLANK MB MB3T0415 0.1 BLACK MB M8410415 ND STANDARD LCS ST3T0415 2.0 1.7 118 STANDARD LCS LC3T0415 1.8 1.7 106 SP!KE MS 940632 1 2.3 0.2 1.7 124 DUPLICATE MD 940633 1 0.5 0.3 50 420 West First Street Casper, WY 82601 (307) 235-5741 l

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0UALITY C0NTR0L REPORT 05/10/94 JOB NUMBER: 940637 CUSTOMER: KERR-McGEE CORPORATION-ATTN JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES 1

ANALYSIS ANALYSIS ANALYSIS ANALY2ED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS-TYPE

!.De VALUE (A)

VALUE (B)

(lA-Bl}

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Thorita 232, total DATE/ TIME ANALYZED:05/02/94' 15:27 QC BATCH NUMBER 150701 REPORTING LIMIT /DFs UNITS:pCf/t METHOD REFERENCE :

TECHNICIAN:JG BLANK MS M83T0415 ND BLANK M8 M84T0415 ND STANDARD LCS ST2T0415 4.5 4.0 112 STANDARD LCS LC2T0415 4.2 4.0 105 SPIKE MS 940637-1 4.4 ND 4.0 110 DUPLICATE MD 940633 1 0.2 0.2 0

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QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600/4-79420, Medxxis for Chemical Analpis of Water and Wastes, March 1983 (2) EPA swr 846, Test Methods for Evaluating Sohd Waste, Third Edition November 1990 and,Iuly 1992 update (3) Standard Methods for the Exanunation of Water and Wutewater,17th,1989 (4) EPA 600/4-80432, Presenbed Procedures for Measuremettz of Radionamty in Dnnking Water, August 1980 (9) Federal Register. Friday, October 26,1984 (40 CFR Part 136)

(6) EPA 600/8-78417, Microbiological Methods for Monitanns the Environment. December 1978 COMMENTS (1) The data m the laboratory Test Resuhs Report may ddfer from the data in the QC Report due to calculations for sample preparation and or ddutions.

(3) The " Time Analyzed" in the QC Report may not reflect the actual tune of each analysis. The "Date Analped"is the actual date of analysis.

(3) Sod and sladge samples are reported on a wet basis or on an "as received" basis unless othermne indicated (4) The data in dus report are within the hnuts of uncertairrty specified in the referenced method unless otherwise indicated.

(5) Analyses performed by a subcontract laboratory are indicated mth an astensk and associated code m the "Techrucian" data field Subcontract Laboratories Gods Core Laboratones Anaheim, CA

  • AN Core Laboratones Aurora, CO
  • AU Core Laboratones Casper WY
  • CA Core Laboratones - Corpus Chnsta, TX

'CC Core laboratones - Houston,TX

  • HP Core laboratones. take Charles, LA
  • If Core laboratones - Long Beach, CA

'LB Other Subcontract laboratones

  • XX DEFINITIONS (1) WC Not Cateulable due to salues lower than the retx< ting hrrut.

(2) ED - Nut Detected above the reportmg knut.

i OC SAMPLE IDENTIFICATIONS l

BLANKS SPIKES MB = Method Blank (also refened to as a preparaison blank)

MS - Matnx Spike RB - Reagent Blank MSD = Mainx Spike Duplicate IB = Instrument Blank PDS - Post Digestion Spike ICB = InitialCahbration Blank BS = Blank Spike (also referred to as a method spike)

CCB = Contmutng Calibtation Blank SS = Surrogate Spike HB = Holdmg Blais (also referred to as as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = Calibration Standard MSD = Matnx Spike Duphcate RS Reference Standardmiso referred to as an extemal reference standard)

Method Duphcate ICV = 1mtial Caldratmn Vei.fication MD

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l THIS IS NOT AN INVOICE Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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l LOG-10 JGB REPORT 04/08/94 JOB NUMOER:940637 CUSTOMER:(KE0001) KERR-McGEE CORPORATION CONTACT:JEFF OSTMEYER PHONES (

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SAMPLE NUMBER:0001 DATE RECEIVED 04/04/94 TIME RECEIVED 10:00 SAMPLE DATE:03/25/94 SAMPLE TIME:15:30 DUE DATE:05/02/94 PROJECT ID: BLOCK 12 E14-5-0 SAMPLE ID:CU1 65 011 REM: WATER LAB WTES:114L CU8E SHORT ID:

BIN NUMBER:0 CODE TEST DESCRIPfl0N TEST LIMITS UNITS OF MEASURE TEST METHOD COMMENTS 1

R552 Thortus 230, total pcl/l R553 Thorium 230, total, error, +/-

pC1/t R554 Thorium 230, total, LLD pCf/l R555 Thortun 232, total pCi/l R$56 Thorium 232, total, error, +/-

pC1/l R557 Thoriun 232, total, LLD pCf/1 R561 Uranium 234, total pCI/t i

R562 Uranlun 234, total, error, +/-

pCl/l R563 Uranlun 234, total, LLD pCl/l R564 Uranlun 235, total pCl/l EPA 901.1 R565 Uranlun 235, total, error, +/-

pCI/l R566 Urantun 235, total, LLD pCl/l R567 Urantun 238, total pCi/l

' R568 Uranlun 238, total, error, +/-

pCi/l R569 Uranlun 238, total, LLD pCl/l R570 Thorius 228, total PCf/t R577 Thorium 228, totat, error, +/-

pcl/l R572 Thorius 228, total, LLD pCl/l PAGE:1

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CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST i

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