ML20207B812

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Core Labs Analytical Rept for Job Number 940634
ML20207B812
Person / Time
Site: 07003073
Issue date: 05/10/1994
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080254
Download: ML20207B812 (7)
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MRE WESTERN ATLAS Core Laboratories CORE LABORATORIES ANALYTICAL R E'P O R T Job Number:

940634 Prepared For:

KERR-McGEE CORPORATION JEFF OSTMEYER P.O. BOX 89 CUSHING, OK 74023 Date:

05/10/94 4

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Signature Date:

Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor l

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We5 wasman ATLAS i

Core Laboratories LABORATORY TE$TS RESULTS 05/10/94 i

JOS NUMBER: 940634 CUSTOMER: KERR-McGEE CORPORATION,

. ATTN: JEFF OSTMETER CLIENT 3.D.........: SLOCK-140-E37-S 78 LABORATORY 1.D...: 940634-0001 DATE SAMPLED.......: 03/26/94 DATE RECEIVED....a 04/04/96 TIME SAMPLED.......: 11:00 TIME RECE!VED....: 10:00 WORK DESCRIPil0N...: CU1-65 006 REMARKS..........: VATER TEST DESCRIPT!0W FINAL RESULT DETECTION LIMIT Uti!TS OF MEASURE TEST METHOD CATE TECHNICIAN Thorium 230, total 0.6 pCl/l 05/02/94 JG Thorim 230, total, error, +/-

0.3 pCl/l 05/02/94 JG Thirim 230, total, LLD 0.5 pcl/l 05/02/94 JG Thiriun 232, total 0.4 pcl/l 05/02/94 JG Th:rium 232, total, error, +/-

0.2 pcl/l 05/02/94 JG Thorium 232, total, LLD 0.1 pcl/l 05/02/94 JG Urtnium 234, total 4.1 pCi/l 04/29/94 PLJ Urtnium 234, total, error, +/-

0.7 pCf/t 04/29/94 PLJ Uranium 234, total, LLD 0.2 pCl/l 04/29/94 PLJ j

Uranium 235, total ND pCi/l EPA 901.1 04/29/94 PLJ Uranium 235, total, error, +/-

0.1 pcl/l 04/29/94 PLJ l

Urtnium 235, total, LLO 0.2 pCi/l 04/29/94 PLJ Urantun 238, total 1.4 pCl/l 04/29/94 PLJ Urtnium 238, total, error, -/-

0.4 pCi/l 04/29/94 PLJ Uranium 238, total, LLD 0.2 pCi/l 04/29/94 PLJ Thorium 228, total 1.1 pCi/l 05/02/94 JG 1

Thorium 228, total, error, +/-

0.3 pCl/l 05/02/94 JG Thorium 228, total, LLD 0.1 pcl/l 05/02/94 JC I

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. Core Laboratories 0UALITY C0NTR0L REPORT 05/10/94 JOB NUMBER: 940634.

CUSTOMER: KERR McGEE CORPORATION.

ATTN: JEFF OSTMEYER ANALYSIS DUPLICATES.

REFERENCE STANDARDS MATRIX SP!KES ANALYS!$

ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUB-TYPE I.D.

VALUE (A)

VALUE (B)

(lABl}

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETIR:Urantun 234, total.

LAIE/ TIME ANALYZED:04/29/94 10:55 QC BATCH NUMBER:150616 REPORTING LIMIT /DF:

UNITS:pC1/l-METHOD REFERENCE :

TECHNICIAN:PLJ BLANK MB MB11UO414 0.1 BLANK MB M821UO414 ND STANDARD LC:

LC11UO414 6.5 6.6 98 STANDARD LCS ST11UO414 6.7 6.6 102 CPIKE MS 940631 1 11.3 2.4 8.2 109 DUPSICATE MD 940634 1 4.1 3.3 22 PARAMETER:Uranlun 235, total DATE/ TIME ANALYZED:04/29/94 11:18 QC BATCH NUMBER:150622 REPORTING LIMIT /DFs UNITS:pCi/l METHOD REFERENCE : EPA 901.1 TECHNICIAN:PLJ BLANK MB MB11UO414 ND BLANK MB M821UO414 ND DUPLICATE MD 940634-1 ND 0.1 0

PARAMETER:Uranlun 238, total DATE/ TIME ANALYZED:04/29/94 11:28 QC BATCH NUMBER:150625 REPORT!NC LIMIT /DF; UNITS:pci/l METHOD REFERENCE :

TECHNICIAN:PLJ BLANK MB HB11U0414 ND BLANK MB MB21U0414 ND STANDARD LCS-LC11UO414 7.3 6.9 106

$7ANDARD LCS

$1sIUO414 6.9 6.9 100 SPIKE MS 940631-1 10.8 1.3 8.6 110 PUPLICATE MD 940634-1 1.4 1.5 7

2ARAMETER:Thoriun 228, total DATE/ TIME ANALYZED:05/02/94 15:03 QC BATCH NUMBER:150693 REPORTING LIMIT /DFs UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:JG.

BLA"K MB MB3T0415 ND BLANK MB MB4T0415 0.1 STANDARD LCS ST2T0415 4.7 4.0 118 STANDARD LCS LC2T0415 3.7 4.0 92 SP!KE.

MS 940637-1 4.9 0.3 4.0 115 DUPLICATE ~ jMD 940633 1 0.5 0.6 18 PAR AMETER:T5oriun 230, total DATE/ TIME ANALYZED:05/02/94 15:10 QC BATCH NUMBER:150697 REPORTING LIMIT /DF:

UNITS pC(/l METHOD REFERE::CE :

TECHNICIAN JG BLANK MB M83T0415 0.1 BLANK' MB MB4T0415 ND STANDARD LCS ST3T0415 2.0 1.7 118 STANCARD LCS LC3T0415 1.8 1.7 106 SPIKE MS 940632 1 2.3 0.2 1.7 124 DUPLICATE MD 940633-1 0.5 0.3 50 420 West First Street Casper, WY 82601 (307) 235-5741 PAGE:2 w

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l wasman ATLAS Core Laboratories QUAL 1TY CONTROL REPORT 05/10/94 JOB NUMBER: 940634 CUSTOMER:.KERR McGEf CORPORATIONv Af iP JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES l

ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT I

TYPE SUB-TYPE

!.D.

VALUE (A)

VALUE (B)

(lA-Bj)

VALUE RECOVERY VALUE ADDED RECOVERY l

PARAMETER:Thoriun 232, total '

DATE/ TIME ANALYZED:05/02/94 15:27 QC BATCN NUMBER:150701 REPORTING LIMIT /DF:

UNIT $rpCi/l METHOD REFERENCE :

TECHNICIAN!JG BLANK MB MB3T0415 ND BLANK MB MB4T0415 ND STANDARD LCS ST2TD415 4.5 4.0 112 SVANDARD LCS LC2T0415 4.2 4.0 105 SPIKE MS 940637-1 4.4 ND 4.0 110-

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DUPLICATE MD 940633-1 0.2 0.2 0

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BERJ wastmius ATLAS Core Laboratories QUALITY CONTROL FOOTER f

METHOD REFERENCES (1) EPA 600/4-79 020. Methods for Chenucal Analysts of Water and Wasca, March 1983 (2) EPA SW.846. Test Methods for Evaluating Sohd Wame, nird Edition, November 1990 and July 1992 update (3) Standard Methods for the Exanunation of Water and Wamewater.17th,1989 (4) EPA 600/4-80-032. Presenbed Procedures for Measurement of Radaoacuvny in Drinkmg Water, Aaigust 1980

($) Federal Register, Friday, October 26,1984 (40 CFR Part 136)

(6) EP A 600 ~8-78-017, Microbiological Methods for Morutorms the Environment December 1978 COMMENTS (1) ne data in the Laboratory Test Resuhs Report snay ddrer froen the data in the QC Report due to calculatiam for sample preparatson and or ddutions.

(2) De " Time Analped"in the QC Report may not reflect the actual tune ofeuh a alysis. The "Date Analyzed"is the actual date of analysis.

(3) Soil and sludge samples are reported on a wet basis or on an "as received" basis unless otherwise mdicated.

(4) ne data in tius report are wnhin the knuts of uncenauty specified m the referenced method unless otherwne indicated.

($) Analyses perfxmed try a subcontred laboratory are indicated with an amerisk and associated code in the "Tcchrucian" data facid.

Subcontract Laboratories Cgdg Core Laboratonen. Anaheun,CA

  • AN Core Laboratones. Aurora, CO
  • AU Core Laboratones Casper.WY

'CA Core Labcretones. Corpus Chnst TX

  • CC Core Laborator.ca. Houmon, TX

' HP Core Laboratones lake Charles, LA

  • If Core Laturatones lmg Beads, CA
  • LB Other Subcoenract laboratones
  • XX DEFINITIONS (1) NC - Not Calculable due to values lower than the reportmg Inmit.

(2) ND = Nn Detected above the reponmg lima.

OC SAMPLE IDENTIFICATIONS DLANKS SPIKES MB e Methud Blank (also referred to as a preparation blank)

MS = Matnx Spike RB = Reagent Blank MSD = Matnx Spike Duphcate IB = Inarument Plank PDS = Post Digesuon Spike ICB = InnialCalibrauon Blank BS = Blank Spike (also referred to as a enethod spike)

CCB = Continuing Catibratson Blank SS = Surrogate Spike HB = Holdmg Blank (also referred to as as a aorage blank)

REFERENCE STANDARDS D1!PLICAlT;S -

CS = Calibration Standard MSD = Mainx Spike Duphcate -

RS = Reference Standard (also referred to as an extemal reference standard)

MD = Method Duplicate ICV = Initial Calibration Venfication CCV = ContmumgCalibrationCahbrauun trS = LaboratoryControlSample 420 West First Street Casper, WY 82601 0 07) 235 5741 n.

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Core Laboratories Customer Estimated j

Job Number Project ID Completion Date AHH LC3-140-EIM-76 C:n2,94 Sample #

Customer ID Remarks 3MI CJ1 s5-D h WATER i

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THIS IS NOT AN INVOICE I

Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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-J08 REP 0RT 04/08/94 JOB NUMBER:940634 CUSTOMER (KE0001) KERR-McGEE CORPORATION CONTACT JEFF OSTMEYER PHONE:(

)

SAMPLE NUMBER:0001 DATE RECEIVED:04/04/94 TIME RECE!VED:10:00 SAMPLE DATE:03/26/94 SAMPLE TIME 11:00 DUE DATE:05/02/94 PROJECT ID: BLOCK-140 E37 5 78 SAMPLE ID:CU1 65-006 REM: WATER LAS NOTES 134L CUSE SHORT ID:

SIN NUMBER:0 CtBE TEST DESCRIPTION TEST LIMITS UNITS OF MEASURE TEST METHOD COMMENTS R552 Thortun 230, total pC1/L R553 Thortun 230, total, error, +/-

PCi/L R554 Thoriun 230, total, LLD pCl/l R555 Thorium 232, total pCi/L R$56 Thortun 232, total, error, */-

PCl/l R$57 Thorium 232, total, LLD pCi/L R561 Uranlun 234, total PCf/1 R562 Uranlun 234, total, error, +/-

PCl/l R563 Uranlun 234, total, LLD pcl/L R564 Urantun 235, total pcl/l EPA 901.1 R565 Uranium 235, total, error, +/-

PCl/l R566 Urantun 235, total, LLD pC1/L R567 Urantun 238, total PCl/t R568 Urantun 238, total, error, +/-

pCl/1 R569 Uranium 238, total, LLD PCl/t R570 Thoriun 228, tetal pcl/l R571 Thoriun 228, totat, error, +/-

pCi/l R572 Thorium 228, total, LLD pcl/l 1

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1 PAGE:1

SHIP TO:

CHAIN OF CUSTODY RECORD AND ANALY2D REE.UEST bot e bcd.5 COMPANY NAME:

ANALYSIS REQUEST COMPANY ADDRESS:

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FROM:

KERR lACGEE CORPORATION PHONE: 1-918-225-7753

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,E 2 MILES NORTH OF HWY. JCT 18 & 33 FAX: 1-918-225-7749 h

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0 CUSHING.OKLA. 74023 SHIPPING d f[dM9 3b 4

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Spedel Reporting requwerdents:

Note: Do not comtune SpecialDeceecean This sample meets a5 W Bill & Report to:

Note: Time of ans!ysis & tech's these results with Limits:

.g appropriate radiological.

Jeff Ostmeyer name must be recorded on other Chain of

" "'I'8I'f6/*L requirements.

Hp initial nt K Box 89 data report.

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