ML20207B973

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Amended Rept for Core Labs Analytical Rept for Job Number 951924
ML20207B973
Person / Time
Site: 07003073
Issue date: 02/08/1996
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080305
Download: ML20207B973 (6)
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.bY WW1UJ CORE LABORATORIES p.NU.NDED REPORT l

...... 1 CORE;IABORATORIES-l A NiA L'Y.T..I C ALL1 lR E P O R T.

Job Number:;- 951924" Prepared For:

l KERR McGEE CORPORATION I

1 JEFF OSTMEYER P.0;' BOX 89' CUSHING,-OK.74023

.Date:-

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Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

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Laboratory Supervisor l

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FINAL REPORT DISTRIBUTIOP 02/08/96 JOB NUMBER: 951924 COMPANY WAME" COMPANY MAILING ADDRESS' COMPANY CITY' STATE COMPANY ZIP CODE KERR R GEE COPp00LT10N P.O. BOK 89 CUSNING OK 74023 JEFF OST5 EYER l

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nlW CORE LABORATORIES LABORATORY TESTS RESULTS 02/08/96 JOS IRaletR E951924)

CUBTOMERai KERR'Nc0EE CORPORATION-

? ATTN 1 JEFF OSTMEYER CLIENT I.D.........

ANNUAL ENVIRONMENTAL CMW 16.3 LABORATORY I.D...: 951924-0001 DATE SAMPLED.......: 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPil0N... CU2 26-023 REMARKS..........: WATER TEST DESCRIPTIONJ flNAL RESULT ~

DETECTION LIMIT UNITS OF MEASUREi TEST METHOD DATE TECHNICIAN Gross Alpha, total 248 pCl/l EPA 900.0 08/30/95 NRF Gross Alpha, total, error, +/-

70.5 pCl/l 08/30/95 NRF Gross Alpha, total, LLD 51.9 pCf/L 08/30/95 NRF Gros) Beta, total 346 pCf/1

[PA 900.0 08/30/95 NRF Gross seta, total, error, +/-

54.0 pCf/t 08/30/95 NRF Gross Seta, total, LLD 65.0 pC1/t 08/30/95 NRF Thorium 232, total 0.5 pcl/l 09/25/95 DW Thortun 232, total, error, +/-

0.4 pCl/l Ov,'M/95 DW Thorium 232, total, LLD 0.6 pCl/l 09/25/95 DW Urantun 234, total (150 U) 5.1 pCf/t CA GLR R405 09/26/95 DW Uranium 234, total, error, +/-

1.2 pCf/l 09/26/95 DW Uranlun 234, total, LLD 0.6 pCf/t 09/26/95 DW Uranluu 235, total (ISO U) 0.0 pCl/l CA-GLR-R405 09/26/95 DW Uranlun 235, total, error, +/-

0.2 pC1/l 09/26/95 DW Uranlun 235, total, LLD 0.4 pCl/l 09/26/95 DW Uranlun 238, total (ISO U) 3.4 pCi/l CA-CLR R405 09/26/95 DW Uranlun 238, total, error, +/-

0.8 pCI/l 09/26/95 DW Uranium 238, total, LLD 0.4 pCf/t 09/26/95 DW Thortun 228, total 1.1 pCf/t 09/26/95 DW Thortun 228, totat, error, +/-

0.6 pCf/t 09/26/95 DW Thorium 228, total, LLD 0.7 pci/l 09/26/95 DW 420 West First Street Casper, WY 82601 (307) 235 5741 PAGE:2 l

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CORE LABORATORIES QUALITY CONTROL REPORT 02/08/96 JOB IRmgER: i 951924 ;

CUSTOMER: KERR McGEE CORPORATION ATTN JEFF OSTMEYER-ANALYS!$

DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bl)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER: Gross Alpha, totst-(DATE/ TIME ANALYZED:08/30/95' 14:05 GC SATCH NUMBER:170093 REPORTING LIMIT /DFt.--

~ UNITS pCl/l METHOD REFERENCE : EPA 900.0 TECHNICIAN:NRF SLANK Ms Ms2As0829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963-1 124 10.0 128 89

' DUPLICATE 2

951963 1 10.0 14.6 37 PARAMETER: Gross Bets, total..

DATE/ TIME ANALYZED:08/30/95 14:14 GC BATCH Wlm0ER 170097 REPORTING LIMIT /DFs-UNITS pCf/t' METHOD REFERENCE EPA 900.0 TECHNICIAN:NRF BLANK MB Ms2As0829 0.4 STANDARD LCS LC180829 23.9 22.0 109 SPIKE MS 951963 1 144 5.0 110 126 DUPLICATE e

951963 1 5.0 8.8 55 PARAMETER:Thorius 232,. total

. DATE/ TIME ANALYZED:09/25/95 16:49 GC RATCN MlmBER:171053 REPORTING LIMIT /DFs UNITS pcl/l METM00 REFERENCE :

TECHNICIAN:DW BLANC MS Me5T0906 0.47 BLANC MB M86T0906 0.95 STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101 4

SPIKE MS 951921 1 16.3 0.92 14.0 110 l

DUPLICATE MD 951922-1 0.61 0.89 37 PARAMETER:Thorius 228, total DATE/ TIME ANALYZED:09/26/95 08:19 DC BATCH NUMBER:171058 REPORTING LIMIT /DF UNITS pci/l:

METHOD REFERENCE :

TECHNICIAN:DW BLANC MB Ms5T0906 0.18 BLANC MB MB6T0906 0.01 STANDARD LCS ST3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921 1 18.0 0.35 14.0 126 DUPLICATE MD 951922 1 0.74 0.86 15 PARAMETER:Uranius 234, total (!$0 U)

DATE/ TIME ANALYZED:09/26/95 10:46 DC BATCN NUMBER:171081 REPORTING LIMIT /DFs UNITS:pCl/l-METHOD REFERENCE :CA-GLR-R405-TECHNICIAN:DW SLANK Ms Ms1UO906 0.2 BLANC MS Ms200906 0.3 STANDARD LCS ST1UO906 6.6 6.6 100 STANDARD LCS LC1UO906 6.5 6.6 98 DUPLICATE MD 952012-2 107 110 3

CARAMETER: Uranium 235, total (ISO U)

DATE/ TIME ANALYZED:09/26/95 11:13 DC SATCH NUMBER 171088 REPORTING LIMIT /DF UNITS:pCl/l-METHOD REFERENCE :CA GLR R405 TECHNICIAN:DW BLANC MS MB1UO906 0.0 4

1 420 West First Street Casper, WY 8260)

(307) 235-5741 i

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bY nlW CORE LABORATORIES QUAL 17Y CONTROL REPORT 02/08/96 JOB IRMBER:/ 951924-CUSTOMER: KERR Mc0EE CORPORATION-ATTW: JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALY$lt ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE I.D.

VALUE (A)

VALUE (B)

(lA8l)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER: Uranium 235, total (ISO U)

' DATE/ TIME ANALYZED:09/26/95 11:13 BC BATCH NUMBER 171088 REPORTING LIMIT /DFs-

. UNITS pcl/l,

. METHOD REFERENCE ~ CA GLR R405.

TECHNICIAN:DW BLANC Me MB2UO906 0.0 DUPLICATE MD 952012-2 4.5 5.0 11 PARAMETER: Uranium 238, total - (ISO U)-

DATE/ TIME ANALYZED:09/26/95 11:19 QC BATCH NUMBER 171092 REPORTING LIMIT /DF2 UNITS:pCf/L METHOD REFERENCE :CA GLR-R405 TECHNICIAN:DW BLANC MB MB1UO906 0.1 SLANC Ms MB2UO906 0.1 STANDARD LCS ST1UO906 6.2 6.0 103 STANDARD LCS LC100906 6.7 6.0 112 DUPLICATE MD 952012 2 48.2 48.2 0

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CORE LABORATORIES QUALITY CONTROL FOOTER 1

METHOD REFERENCES l

(1) EPA 600 4 79420. Methods for Chemical Analnas of Water and Wastes. March 1983 (2) F PA SW N46. Test Methods for Evaluatmg Sohd Waste. Bird Editiort November 1990 and July 1992 update I

(3) Standard Methods for the Esammation of Water and Wastewater.17 tit 1989 (4) EPA f40 4 RO-012. Presenhed Procedures for Measurement of Ra&oacuvity m Dnnking Water. August 1980 (5) f ederal Repster.1ndayJAtober 26.19X4 (40 CFR Part 136)

(6) EPA 600 R 78-017. Microbiok>gwal Methods for Monitonna the Environment. December 1978 COMMENTS (1) the data m the Laboratorv Test Results Report mav differ from the data in the QC Report due to calculanons for sample preparauon and,or dilutions.

j (2) The " Time Analvred" m the UC Report mav not reflect the actual tune of each analna The

  • Data Analyzed"is the actual date of analpa (3 ) Soil and sludge samples are reported on a wet basis or on an "as received" basis unless otherwise mdicated.

(4) The data m this report are mthm the limits of uncertamty specified in the referenced method unless otherutse m&cated.

(5) Analyses pertormed by a subcontract laborators are mdicated with an astensk and associated code m the "Techrucian" data field.

Subcontract Laboratones C.giq Core laboratones. Anaheint CA

  • AN Core tahorntones-Aurora.CO

'AU Core tahorntones. Casper, WY

  • CA Core Lahorntones. Corpus Chnsti. TX

'CC Core !.aboratones. iloustort TX

  • HP Core taburatoi s. I.ake Charles. LA
  • If Core Laboratones 12mg Beacit CA
  • LB Other Subantract Laboratones
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DEFINITIONS (1) NC = Not Calculable due to salues lower than the reportmg lumt.

(3) ND - Not Detected above the reportmg linut.

OC SAMPLE IDENTIFICATIONS BLANKS SPUG S MB - Methud Blank (also referred to as a preparatiori blanh MS = Matna Spika RB - Reagent Blank MSD = Mainx Spike Duphcate IB Instrument Blank PDS = Post Digestion Spike ICD - InmalCahbration Blank BS = Blank Spike (also referred to as a method spike)

CCB - Conimums Cahbration Blank SS = Surrogate Spike llD - Holdmg Diank talso referred to as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = Calibration Standard MSD = \\fatna Spike Duphcate R5 - Referena Standard (also referred to an an external reference standard)

MD Methud Duplwate ICV = InitialCahbrauon Verificasson CCV = CoramumsCahbraison Venficauan l

LIS = laboratory Control Sample i

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