ML20207C033

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Core Labs Analytical Rept for Job Number 951927
ML20207C033
Person / Time
Site: 07003073
Issue date: 09/27/1995
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080326
Download: ML20207C033 (9)
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A-N"A'L'Y T I C A L R E P O-R T

' Job Number:

951927' 3

-Prepared For:

KERR McGEE CORPORATION JEFF OSTMEYER P;O. BOX 89 CUSHING, OK 74023 Date:

09/27/95 82.c.

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Signature Date:

Nazne: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

LABORATORY SUPERVISOR 1

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OCT 0 21995 COPY Safetv & Environ Cushinc 9903080326 981106 PDR ADOCK 07003073 B

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1 FINAL REPORT DISTRIBUTION 09/27/95 JOB NUMSER: 951927 i

COMPANY NAME COMPANY MAILING ADDRESS COMPANY CITY STATE COMPANY ZIP CODE KERR McGEE CORPORATION P.O. BOX 89 CUSHING OK 74023 JEFF OSTMEYER l

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CORE LABORATORIES LAB 0 RAT 0RY TESTS RESULTS 09/27/95 JOB NUMSER - 951927 (DSTOMER: ' KERR McGEE CORPORATION -

ATTN JEFF OSTMEYER CLIENT 1.D.........: ANNUAL ENVIRONMENTAL CNW 26.1 LARORATORT I.D...: 951927 0001 DATE $AMPLED.......: 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPTION...: CU2*26-026 REMARKS..........: WATER TEST DESCRIPTION FINAL RESULT DETECTION LIMIT UNITS OF MEASURE TEST METHOD DATE'

' TECHNICIAN Gross Alpha, total 53.8 pcl/l EPA 900.0 08/30/95 NRF Gross Alpha, total, error, +/-

18.2 pCI/l 08/30/95 NRF Gross Alpha, total, LLD 15.1 pCf/L 08/30/95 NRF Gros 3 Beta, total 40.7 pCf/l EPA 900.0 08/30/95 NRF Gross Beta, tote', error, +/-

14.2 pCf/t 08/30/95 NNF Gross Beta, for LLD 20.5 pCl/l 08/30/95 NRF Thorita 232, ts 0.62 pC1/l 09/25/95 DW Thori a 232, u t, error, +/-

0.5 pCf/l 09/25/05 DW Thorita 232, total, LLD 0.7 pCf/L 09/25/95 DW Uranita 234, total (150 U) 2.8 pCf/l CA-GLR R405 D9/26/95 DW Uranita 234, total, error, +/-

0.8 pCf/t 09/26/95 DW Uranita 234, total, LLD 0.5 pCi/l 09/26/95 DW Uranita 235, total (ISO U) 0.1 pCf/l CA GLR R405 09/26/95 DW Uranita 235, total, error, +/-

0.1 pCf/l 09/26/95 DW Uranita 235, total, LLD 0.2 pCf/l 09/26/95 DW Uranita 238, total (Iso U) 1.2 pCi/l CA GLR R405 09/26/95 DW Uranite 238, total, error, +/-

0.5 pct /l 09/2//95 DW Uranita 238, total, LLD 0.2 pct /l 09/26/95 DW Th: rite 228, total 0.72 pCf/l 09/26/95 DW Thorita 228, total, error, +/-

0.6 pCf/l 09/26/95 DW Th:rita 228, total, LLD 0.8 pCf/l 09/26/95 DW 420 West First street Casper, WY 82601 (307) 235-5741 PAGE 2

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CORE LABORATORIES QUALITY CONTROL REPORY I

09/27/95 JOB NUMBER: - 951927.

CUSTOMER: KERit McQEE CORPORATION ATTN: JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES I

ANALYSIS ANALYCIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SP!KE PERCENT TYPE SUB TYPE I.D.

VALUE (A)

VALUE (B)

(lABl)

VALUE RECOVERY VALUE ADDED

. RECOVERY PARAMETER: Cross Alpha, totaln..

DATE/ TIME ANALYZED:08/30/95 14:05 DC BATCM NUMBER 170093 REPORTING LIMIT /DFs

- UNITS pCl/l METHOD REFERENCE : EPA 900.0 TECHNICIAN NRF BLANK MB Ms2AB0829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963 1 124 10.0 128 89 DUPLICATE MD 951963 1 10.0 14.6 37 PARAMETER Gross Beta, total.

DATE/ TIME ANALYZED:08/30/95 14:14 QC BATCH NUMBER 170097 REPORTING LIMIT /DF:

. UNITS:pCl/l

= METHOD REFEREWCE EPA 900.0 TECHNICIAN NRF BLANK Me Ms2As0829 0.4 l

STANDARD LCS LC180829 23.9 22.0 109 I

SP!KE MS 951963 1 144 5.0 110 126 DUPLICATE MD 951963-1 5.0 8.8 55 PARAMETER Thorium 232, total a DATE/ TIME ANALYZED 09/25/95 16:49 GC 8ATCH NUMBER 1N053 REPORTING LIMIT /DFs-UNITS:pCl/I' METHOD REFERENCE :-

TECHNICIAN DW l

SLANK Ms Me5T0906 0.47 l

BLANK MS M86T0906 0.95 i

STMDARD LCS ST3T0906 7.59

'0 108 STANDARD LCS LC3T0906 7.1 T.b 101 l

SPIKE MS 951921-1 16.3 0.92 14.0 110 I

DUPLICATE MD 951922 1 0.61 0.89 37 j

I PARAMETER:Thortun 228, total CATE/ TIME ANALYZED 09/26/95 08:19 DC BATCN NUMBER 171058 l

REPORTING L.lMIT/DFs

~ UNITS pci/l METHOD REFERENCE :

TECHNICIAN DW l

BLANK M8 MR5T0906 0.18 BLANK MS M86T0906 0.01 STANDARD LCS ST3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 SP!KE MS 951921 1 18.0 0.35 14.0 126 DUPLICATE MD 951922 1 0.74 0.86 15 l

PARAMETER:Uranlun 234, total. (ISO U)

DATE/ TIME ANALYZED 09/26/95 10:46 GC BATCH NUMBER 171081 l

REPORTING LIMIT /DFs UNITS:pci/l METHOD REFERENCE CA-GLR R405 TECHNICIAN:DW i

BLANK MS M5100906 C.2 j

BLANK MS MB2UO906 0.4 STANDARD LCS ST100906 7.8 7.8 100 i

STANDARD LCS LC1UO906 7.7 7.8 99 DUPLICATE MD 952012-2 127 131 3

PARAMETER:Uranius 235, total (ISO U)

DATE/ TIME ANALYZED:09/26/95 11:13' OC BATCH NUMBER 171088 REPORTING LIMIT /DFs UNITS:pci/l METHOD REFERENCE :CA-GLR R405 -

TECHNICIAN:DW 1

SLANK MS M51UO906 0.0 420 West First Street Casper,'afY 82601 (307) 2',5 5741 PAGE:3

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QUAL 1YY CONTROL REPORT 09/27/95 JOS autBER 1951927 LCUSTOMER: KERR McGEE CORPORATION ATTN JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STAWARDS NATRIN SPIKES ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PENCENT TYPE SUB TYPE 1.D.

VALUE (A)

VALUE (B)

(lA-8l)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Urani a 235,' total'. (ISO U).

DATE/ TIME ANALYZED 09/26/95 11:13-OC BATCH luesER:171088 i

REPORTING LIMIT /DFt UNITBspC1/1 METHOD REFERENCE :CA GLR R405

-TECHNICIAN DW i

BLANK Ms NB200906 0.0 DUPLICATE MD 952012-2 5.4 6.0 11 PARAMETER Urani a 238,' tota; (ISO U)'

- DATE/ TIME ANALYZED:09/26/95. 11:19 BC BATCH NUMBER:171092 REPORTING LIMIT /DFs UNITS pCf/t METHOD REFERENCE :CA GLR 8405 TECHNICIAN DW BLANK Ms M81UO906 0.1 SLANK Me MS2UO906 0.1 STANDARD LCS ST100906 7.4 7.2 103 1

STANDARD LCS LC1UO906 8.0 7.2 111 DUPLICATE e

952012 2 57.4 57.4 0

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420 West First Street Casper, WY 8260)

(307) 235-5741 PAGE:4

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}nMB CORE LABORATORIES QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600/4-7M20. Methods for Chermcal Analysis of Water and Westen. March 1983 (3) EPA SW-846. Test Methods for Evalualmg Solid Waste. Third Edition, November 1990 and July 1992 update (3) Standard Methods for the Emanunation of Water and Wastewater.17th.1989 (4) EPA 600/4-a0 032. Presmhed Procedures for Measurunent of Radioactivity m Druning Water, August 1980 (5) Federal Register. Friday. October 26.1984 (40 CFR Part 136)

(6) EPA 600/8-78 017. Microbiologul Methods for Momtonng the Environment, December 1978 COMMENTS (1) The data sa the laboratorv Test Results Report may ddTer from the data m the QC Report due to calculaunns for sample preparauon anct or dilutions.

(3) The " Time Analyzed" in the QC Report may not reflect the actual tune of each analysis. The "Date Analyzed"is the actual dam of analysm.

(3) Soil and sludge samples are reported on a wet bases or on an "as rccrived" basis unless otherwise indicated.

(4) The data m this report m within the linnts of uncertarity specified m the referenad method unless otherwuc indicated.

(5) Analvses performed by a subcontract laboratory are inciented with an astensk and associated code tu the "Techrucian" data field.

Subcontract Laboratories Code Corelaboratones-Anaheun CA

  • AN Core laboratones. Aurora. CO

'AU Cars imboratones Casper, WY

  • CA Core Lahorntones. Corpus Chnsti. TX
  • CC Core laboratones. Ilouston. TX
  • HP Core Laboratones. Lake Charles 1.A
  • If Core Laboratones long Beeck CA
  • 1.B Other Subcontract Laboratones
  • XX DEFINITIONS (1) NC = Not Calculable due to salues lower than the reportmg lumt.

(3) h!D

  • Not Detected above the reportmgImut.

OC SAMPLE IDENTIFICATIONS BLANKS SPIKES MD - Method litank (also referred to as a preparauon blank)

MS - Mannx Spike RD = Reagent Dlank MSD. Mains Spike Duplicate ID = Instrument Blank PDS - Post Digesuon Spike ICD - ImtsaiCahbration Blank DS = Blank Spike (also referred to as a method spike)

CCD = CornmumgCahbrat.on Blank SS = Surrogate Spike 11D = Iloidmg Blank (also referred to as a storage blank)

REFERENCE STANDARDS DUPLICATES CS - CahbrauonStandard MSD - Matnx Spike Duplicate RS = Referencz Standard (also referred to as en external reference standard)

MD Method Duphcate ICV = imtialCahbration Venficauan CCV = Contmutng Cahbrauon Venficauon j

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if ucu have en, questions citase (41) Cert Locriteries, Casur. VY (307) 135-5741 THIS IS NOT AN INVOICE j

Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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ANNUAL ENVIRDNMENTAL CW 26.1 SAMPLE ID:CU2-26-026 FEM: WATER as h]iES:t;4L COBE In0AT 10 Elk hVMEE.L
GDE TEST DESCRIPTION TEST LIMITS UNITS CF I!Es5URE Test METWDD CDMMEhTS 4 00 ut4T CrECK FOR 153 U l

7513 Gross Alpha, total pCi/l EPA H0.0 R5l4 Gross Alpha, total, error, t'-

pC1/1 D15 Grcss Alpha, total. L3

C /l R$16 Gross Eeta, total pC1/1 EPA 900.0 U17 3rriss Peta, total, errer, /-

pCi/l R51a Gross Beta, total, LLD pC1/1 i355 ibcrti,e 232, tstal pC /l R556 Tnoraus 232, tetal, error, f/-

pCi/l A557 ~ Lorica 232, tetal, LLD pCs/l i

l R561 Urannus 234, total 1150 bl pCa/l CA-6LR-R405 6562 Lrantue 234, total, error, t/-

pC1/1 E!t3 Uranius 234, total, LLD pCi/1 E64 wantur 225, total

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F35 Uranius 235 total, error. +/-

pCi/l Mo w enive 235 tttal, u 0 p(sil R567 Drannus 238, total (150 L) pct /l CA-BLR-R405 R65 waniur 234, total, a rrcr, u -

p;1/1 E519 branium 238, total, LLD pCi/l F570 Thorium 225, total pC1/1 R571 Thortus 228, total, error, t/-

pCi/l 4572 T urive, 228, :stal, iLD C

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