ML20207B982
| ML20207B982 | |
| Person / Time | |
|---|---|
| Site: | 07003073 |
| Issue date: | 09/28/1995 |
| From: | Mull R CORE LABORATORIES, INC. |
| To: | |
| Shared Package | |
| ML20207B577 | List:
|
| References | |
| NUDOCS 9903080308 | |
| Download: ML20207B982 (9) | |
Text
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CORE LABORATORIES l
i CORE:IABORATORIES.
A1 N 2 A LL Y T I C: A L -
REPORT l
~ Job Number: ^ 951924-Prepared For:
KERR McGEE CORPORATION JEFF'OSTMEYER P.O.
BOX 89.
CUSHING, OK-74023' l
Date:
09/27/95 g,rLM 9625D OME. '7 ic.
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Name: Rondalynn Mull Core Laboratories, Inc.
420 West First Street Casper, WY 82601
Title:
LADORATORY SUPERVISOR 9903080308 981106 _
PDR ADOCK 07003073 B
PDR_
per'F.IVCD OCT 0 21995 Safety & Environ Cusning
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1 1"MLAB gym CORE LABORATORIES 1
FINAL REPORT DI37RIBUTION i
09/27/95 l
l JOB NUMBER: 951924 COMPANY NAME COMPANY MAILING ADDRESS COMPARY CITY' STATE COMPANY ZIP CODE KERR McGEE CORPORATION P.O. BOK 89 CUSHING OK 74023 JEFF OSTMEYER l
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CORE LABORATORIES 1
l LABORATORY TESTS RESULTS 09/27/95 i
JOB NLmsER:. 951924-CUSTOMER: KERR McGEE CORPORATION-ATTN JEFF OSTMEYER-CLIEN) 4.0.........: ANNUAL ENVIRONMENTAL CMW 16.3 LABORATORT I.D...: 951924 0001 i
DATE SAMPLED.......: 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPLED.......:
TIME RECEIVED....: 10:08 WORK DESCRIPTION...: CU2-26-023 REMARKS..........: WATER TEST DESCRIPTION' FINAL RESULT DETECTION LIMIT' UNITS OF MEASURE TEST DETHOD DATE' TECHNICIAN
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Gross Alpha, total 248 pCl/l EPA 900.0 08/30/95 NRF Gros 3 Alpha, total, error, +/-
70.5 pcl/l 08/30/95 NRF Gross Alpha, total, LLD 51.9 pCf/l 08/30/95 NRF Gross Seta, total 346 pCl/l EPA 900.0 08/30/95 NRF Gross teta, total, error, +/-
54.0 pCf/l 08/30/95 NRF Gross Beta, total, LLD 65.0 pcl/l 08/30/95 NRF l
Thorlun 232, total 0.5 pCi/l 09/25/95 DW
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Thorlue 232, total, error, +/-
0.4 pCl/l 09/25/95 DW i
Thorium 232, total, LLD 0.6 pCl/l 09/25/95 DW Uranium 234, total (ISO U) 6.1 pCf/L CA GLR-R405 09/26/95 DW Uranium 234, total, error, +/-
1.4 pCf/l 09/26/95 DW Uranlun 234, total, LLD 0.7 pCl/l 09/26/95 DW Urantun 235, total (ISO U) 0.0 pCf/t CA-GLR R405 09/26/95 DW Uranium 235, total, error, +/-
0.2 pCf/l 09/26/95 DW Urantun 235, total, LLD 0.5 pCi/l 09/26/95 DW Uranlue 238, total (ISO U) 4.0 pci/l CA-GLR-R405 09/26/95 DW Uranium 238, total, error, +/-
1.0 pCl/l 09/26/95 DW Uranlun 238, total, LLD 0.5 pcl/l 09/26/95 DW i
Thoriun 228, total 1.1 pcl/l 09/26/95 DW i
Thortun 228, total, error, +/-
0.6 pCf/l 09/26/95 DW Thorius 228, total, LLD 0.7 pCf/l 09/26/95 DW 420 West First Strc-et Casper, WY 82601 (307) 235 5741 PAGE:2
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CORE LABORATORIES QUALITY CONTROL REPORT 09/27/95 JOE WlMBER: 951924, QJST(MER: KERR McGEE CORPORAT!0N ATTN JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS NATRIK SPIKES AN,dVS!$
ANALYS!$
ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS-TYPE I.D.
VALUE (A)
VALUE (B)
(lABl}
VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER Gross Alpha, totalt DATE/ TIME ANALYZED:08/30/95 14:05
.QC BATCN NUMSER 170093 REPORTING LIMIT /DF:
" UNITS:pCl/LL METHOD REFERENCE : EPA 900.0
- TECHNICIAN:NRF BLANK Ms Ms2AB0829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963-1 124 10.0 128 89 DUPLICATE MD 951963 1 10.0 14.6 37 PARAMETER Gross Beta, total
'DATE/ TIME ANALYZED 08/30/95 14:14 QC BATCH NUMBER 2170097 REPORTING LIMIT /DFs UNITS pCf/l METHOD REFERENCE EPA 900.0 TECHNICIAN:NRF BLANK Ms M82A80829 0.4 STANDARD LCS LC180829 23.9 22.0 109 SPIKE MS 951963 1 144 5.0 110 126 DUPLICATE e
951963 1 5.0 8.8 55 PARAMETER Thorlun 232, total:....
DATE/ TIME ANALYZED:09/25/95 16:49-OC BATCH NUMBER 171053 REPORTING LIMIT /DF:
UNITS:pCl/l'
' METHOD REFERENCE :
TECHNICIAN DW BLANK Ms Ms5T0906 0.47 SLANK Ms M86T0906 0.95 (TANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101 SPIKE MS 951921 1 16.3 0.92 14.0 110 DUPLICATE MD 951922 1 0.61 0.89 37 PARAMETER: Thorium 228,' totat DATE/ TIME ANALYZED:09/26/95 08:19 QC BATCH NUM8ER 171058 REPORTING LIMIT /DFs UNITS:pCf/t' METHOD REFERENCE :
TECHNICIAN:DW BLANK MS M85T0906 0.18 BLANK MS M86T0906 0.01 STANDARD LCS LT3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 SP!KE MS 951921 1 18.0 0.35 14.0 126 DUPLICATE MD 951922 1 0.74 0.86 15 PARAMETER Uranium 234, total (ISO U)
DATE/ TIME ANALYZED:09/26/95 10:46 QC BATCH NUMBER 171081 REPORTING LIMIT /DFs UNITS:pCl/l METHOD REFERENCE :CA-GLR-R405 TECHNICIAN:DW BLANK -
MB Ms1UO906 0.2 BLANK
'Ms Ms2UO906 0.4 STANDARD LCS ST1UO906 7.8 7.8 100 STANDARD LCS LC1UO906 7.7 7.8 99 j
DUPLICATE MD 952012-2 127 131 3
PARAMETER:Urantun 235, total. ~ (ISO U)
DATE/ TIME ANALYZED:09/26/95 11:13-QC BATCN NUMBER:171088 REPORTING LIMIT /DFs UNITS:pCl/l METNOD REFERENCE :CA GLR-R405 TECHNICIAN:DW BLANK MS MB100906 0.0 420 West First Street Casper, WY 82601 (307) 235 5741 PAGE:3
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CORE LABORATORIES QUALITY CONTROL REPORT 09/27/95 JOB NUMBER -~ 951924 CUSTOMER. KERR McGEE CORPORATION :
. ATTN: JEFF OSTMEYER-ANALYSIS DUPLICATES REFERENCE STANDARDS NATRIX SPIKES ANALYSIS ANALYS15 ANALYSIS ANALYZEP DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE 1.D.
VALUE (A)
VALUE (B)
(lABl)
VALUE RECOVERY VALUE ACDED RECOVERY PARAMETER:Urantun 235, total. (ISO U)
DATE/ TIME ANALYZED:09/26/95: 11:13 QC BATCH NUMBER 171088 REPORTING LIMIT /DF:
. UNITS:pCl/t..
METHOD REFERENCE :CA-GLR R405--
1 TECHNICIAN:DW BLANK MB MB2UO906 0.0 DUPLICATE MD 952012-2 5.4 6.0 11 PARAMETER: Uranium 238, total (ISO U)
DATE/ TIE ANALYZED 09/26/95 11:19' QC BATCH NL8tBER:171092 REPfNtTING LIMIT /DF:
UNITS:pC1/I' METHOD REFERENCE -lCA GLR R405 TECHNICIAN:DW BLANK MB MB1UO906 0.1 BLANK MB MB2UO906 0.1 STANDARD LCS ST1UO906 7.4 7.2 103 STANDARD LCS LC1UO906 8.0 7.2 111 DUPLICATE e
952012 2 57.4 57.4 0
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420 West First street Casper, WY 82601 (307) 235 5741 PAGE:4 a,-a.,-v~.,n..~.,.~w,-me~.m~~ame,"~~.e--+-ve~~>~~>~n~~~~~~'~v>-~~~"~-
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CORE LABORATORIES QUAUTY CONTROL FOOTER METHOD REFERENCES (1) EPA 600/4 79 020. Methods for Chenucal Analysis of Water and Wasten. March 1983 (2) FPA SW.846. Test Methods for Evalualms Sohd Weste. Third Edstion. November 1990 and July 1992 update (3) Standard Methods for the Exammauon of Water and Wasiewater.17th.1989 (4) EPA 600/4 80 032. Prescrihed Procedures for M - -
- f Radioacuvity m Drmking Water. August 1980 o
(5) Federal Regisser, Fnday. Odober 26.19N4 (40 CFR Part 136)
(6) Era 600/R.73 017. Microbiological Methods for Marutonng the Environment. December 1978 COMMENTS (l) The data in the Laboratorv Test Resuha Report may differ from the data m the QC Report due to calculauons for sample preparauon and/or dilutions.
(2) The " Time Analyzed"in the OC Report may not reflect the actual tune ofeach analpis.1he *Date Analyzed"is the actual date of analpis.
(3) Soil and sludge samples are reported on a wet basis or on an "as received" basis unless otherwue mdicated.
(o) The data in this report are wnhin the limns of uncertamty specified in the referenced method unless otherwise mdacated.
(9) Analyses performed by a subcontract laboratory are indaeased wnh an assensk and associated code m the "Techrucian" data field.
Subcontract Laboratories Code Core labormiana. Anaheun. CA
- AN Core Labormiona. Aurora. Co
- AU Core Laboratones. Casper. WY
- CA Core Labormiones. Corpus Chnata. TX
- CC Core Laberasones. Houston. TX
' HP Core laborsiones. Lake Charles. LA
- LC Core Laboratones. Long Beach CA
- LB Other Subcontract Laborasones
- XX i
DEFINITIONS (1) NC = Not Calculable due to values lower than the reportmg limit.
(2) ND = Not Detected above the reportmg hrrut.
)
OC SAMPLE IDENTIFICATIONS BLANKS SPIKES 3
MB - Mcthod Diank (also referred to as a preparauon blank)
MS - Mains Spike RD = Reagent Diank MSD = Manna Spike Duplicate IB = Instrurnent Blank PDS = Post Diessuon Spike ICB - InnialCahbrahon Blank BS = Blank Spike (also referred to as a method spike)
CCB =_ ContmumsCalibratson Blank SS = Surrognie Spike IIB = Holdmg Diank (also referred to as a morage blank)
REFERENCE STANDARDS DUPLICATES CS = Calibration Standard i
MSD = Matnz Spike Dupheate RS = Reference Standard (also referred to as an external reference standard) 1 MD = Method Dupheute ICV = InnialCalibrauon Venficauon CCV = Contumaing Calibratiou Venficauan LES = LaborosoryControlSample 420 West first Street Casper, WY 82601 (307) 235 5741 i
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(1Aqbb CORE LABORATORIES, INC.
1 s293 soii re,no.a gg sousion.re.. 77040 o,,e; i (713) 460-9600 Sample Receipt Acknowledgment Date
?>a/25/95 R
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n p KERR-McGEE COGPORA110N v ', 4 n E o P.0 E0X 6?
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' CUSHIN6. OK 74023 t JIFF OsinEYER c
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o Core Laboratories Customer Estimated Job Number Project ID Completion Date 951974 AhNUAL IN'JIROCFNTAt Cr:9 16 3 09/21/95 Sample #
Customer ID Remarks 0001 CU2-26-023 WATER RECE Bien SEP0 5 1995 Safety & Enurc r e r.' a l
I If wu nave anv quertions please call (cre Laderatcries, hsper WY 13076 235-5741 THIS IS NOT AN INVOICE Order subject to our sales agreement. if any.
Otherwise subject to our current terms of sale as shown on reverse side.
l Please contact laboratory immediately, if any discrepancies are observed.
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>TE aECElt EC'."1/2a/i5 TIF,E SECTI'JD 10:C3 IAnotE CATE Ci/2!/M isr.hE iirE COE DATE Gi/21/M EROJECT 10; ANNUAL EhVif.0NMENTAL (MW 16.3 SAMPLE ID:Cu2-26-023 REM: WATER
.63 NOTES:tHL CLEE SJR1 13 illN NUNEER.L CZE TEST DESCRIPT*0N TEST LIrli!
UNIT 3 0F lie 65URE TEST METHOD COMMENTS FG00 uMi (mCCR FOR ISC U
- 513 Gross Alpha, total FC /l EFA 9CD.C R514 Ercss Alpna, total, error, +/-
pCi/l R515 Grcss Alpha, tstal, LLD pC1/1 R5t6 Gross feta, total pCi/1 EPA 900.0 A517 Gross Beta, total, error, +/-
pCi/1 R513 Gross Beta, total, LLD pCi/l F5:5 ibertus 232, tctal pCi/l R336 inorsun 232, total, error, +/-
pCi/l 4557 Thort a 232, total, LLD pCi/l U61 Uranium 234, total (ISD U1 pCi/l (A-6LR-R405 E562 srannus 234, total, errcr, +/-
pCi/l fi3@3 Uranius 234, total. LLD pC /1
%4 L'anium 235, total (130 Ut
- Ci/l CA 6t R-E4' R365 Urantun 235, total, error +/-
pCi/l A566 urania 235, total, LLD 902/1 M67 Uranium 238, total (150 'J:
pCs/l CA-6LR '1405
~56E trantue 233, total, r.rcr 4/-
- Clil R569 Uranium 238, tata', LLD pCi/l a57C T!.crive 223, te.41 pC1/1 R571 Tnortum 228, total, error, +/-
pCi/1 55?2 Ti.criue 229, total, TLC pCi/l pee--
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ISOTCPICS Th232 E Th 228 N
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