ML20207C038

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Amended Rept for Core Labs Analytical Rept for Job Number 951927
ML20207C038
Person / Time
Site: 07003073
Issue date: 02/08/1996
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080331
Download: ML20207C038 (6)
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LJob-Number:0 L951927 Prepared 1For:-

KERR'McGEE'CORPORATIONc JEFF OSTMEYER-

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BOX;89

. CUSHING, OK:.74023

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Signature Date:

Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor l

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1}LM gg CORE LABORATORIES l

FINAL REPORT DlSTRIBUTION l

02/08/96 JOB NUMBER: 951927 1

COMPAllY MNE J COMPANY MAILING ADDRESS-COMPANY CITY STATE COMPANY ZIP CODE l

KERR McGEE CORPORATION P.O. BOX 89 CUSHING OK 74023 JEii OSTMEYER l

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LAK nRD CORE LA: ORATORIES LABDRAT0RY TESTS RESULTS 02/08/96 JOS NUMart: '951927 CUSTOMER:; KERR McGEE CORPORATION :

ATTN JEFF OSTMEYER CLIENT !.D.........h ANNUAL ENVIRONMENTAL CMW 26.1 LABORATORY I.D...: 951927-0001 DATE SAMPLED.......: 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPTION...: CU2 26 026 REMARKS..........: WATER 1

I TEST DESCRIPTION FINAL RESULT DET[cTION LIMIT UNITS OF MEASURE TEST METHOP DATE

--TECHNICIAN Gros:s Alpha, total 53.5 pcl/l EPA 900.0 08/30/95 NRF j

Gr:ss Alpha, total, error, +/-

18.2 pcl/l 08/30/95 WRF Gross Alpha, total, LLD 15.1 pcl/l 08/30/95 WRF Gross Beta, total 40.7 pcl/l EPA 900.0 08/30/95 NRF l

Gross Beta, total, error, +/-

14.2 pcl/l 08/30/95 NRF Gross Beta, total, LLD 20.5 ocl/l 08/30/95 NRF Thoriun 232, total 0.62 pCl/l 09/25/95 DW Thortun 232, total, error, +/-

0.5 pCi/l 09/25/95 DW Th:Irium 232, total, LLD 0.7 pct /l 09/25/95 DW Uranlun 234, total (ISO U) 2.4 pcl/l CA ctR-R405 09/26/95 DW Uraniun 234, total, error, +/-

0.7 pci/l 09/26/95 DW Uranlun 234, total, LLD 0.4 pcl/l 09/26/95 DW Uraniun 235, total (ISO U) 0.1 pcl/l CA-GLR-R405 09/26/95 DW Uranlun 235, total, error, +/-

0.1 pcl/l 09/26/95 DW Uranlun 235, total, LLD 0.2 pcl/l 09/26/95 DW Uranlun 238, total (ISO U) 1.0 pcl/l CA-GLR-R405 09/26/95 DW Uranlun 238, total, error, +/-

0.4 pci/l 09/26/95 DW Uranlun 238, total, LLD 0.2 pcl/l 09/26/95 DW Thorfun 228, totat 0.72 pci/l 09/26/95 DW Thoriun 228, total, error, +/-

0.6 pci/l 09/26/95 DW Thirius 228, total, LLD 0.8 Wiit 09/26/95 DW l

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l 420 West First Street casper, WY 82601 (307) 235-5741 i

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QUALITY CONTROL REPORT 02/08/96 JW ItaIBER:; 9519271 fCUBTOMER: KERR'McGEE CORPORATIONS ATTNV JEFF 087MEYER :

ANALYSIS DUPLICATES REFERENCE STANDARDS NATRIX SPIKES ANALYSIS ANALYSIS ANALYSIS ANAL" ZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SP!KE PERCENT TYPE BUB TYPE I.D.

VALUE (A)

VALUE (B)

(lABl)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMkTER Groes'Alphe,: totals..

TDATE/TIMEANALY2ED:04/30/95114:051 ec BATCet NUMBER:170093 REPORTING LIMIT /DFs E ~ UNITS:pcl/LF

! MTNOD REFERENCE G EPA 900.0i

-TECINilCIAN NRF BLANK MB MB2AB0829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 95196L1 124 10.0 128 89 DUPLICATE MD 951963 1 10.0 14.6 37 PARAMEMR Gross Sete,; totetJ

-;DATE/ TIME ANALY2ED:08/30/95 '14:14; OC BATCH NLBIBER 170097 REPORT %G L?MIT/DF ' ' : UNITS pCf/t-DETHOD REFERENCE : EPA 900.0 TECHNICIAN:NRF BLANK MB MB2AB0829 0.4 I

STANDARD LCS LC180829 23.9 22.0 109 SPIKE MS 951963-1 144 5.0 110 126 DUPLICATE MD 951963 1 5.0 8.8 55 PARAMETERThorita 232, total"....,

.' METHOD REFERENCE'.

TECINilCIAN DW

~DATE/ TIME ANALY2ED:09/25/95: 16:49 oC BATCN NUMBER:171053 REPORTING LIMIT /DFs:

UNITS pCl/t!

BLANK MB MB5T0906 0.47 BLANK MB MB6T0906 0.95 STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 1

7.0 101 SPIKE MS 951921 1 16.3 O.92 14.0 110 DUPLICATE MD 951922 1 0.61 0.89 37 PARAMETER:Thorita 228, total

.DATE/ TIME ANALY2ED:09/26/95. 08:19 QC BATCH NUMBCR 171058 REPORTING LIMIT /DFs-UNITS pCl/l' METHOD REFL U NCE :-

TECHNICIAN:DW l

STANK

!MB MOST0906 0.18 J et MB670906 0.U1 aNDARD ST3T0906 7.0 7.9 100

$TANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921 1 16.0 0.35 14.0 126 DUPLICATE MD 951922 1 0.74 0.86 15 l

PARAMETER:Uranita 234, totel- (ISO 4).-

DATE/ TIME AWLYZED:09/26/95' 10:46 GC BATCH NLBIBER 171081 REPORilWG LIMIT /DFs-UNITS:pt /t

- ME1 NOD REFERENCE :CA-GIR R405 TECHNICIAN:DW BLANK MB MB1UO906 0.2 BLANK MB MB2UO906 0.3 STANDARD LCS ST1UO906 6.6 6.6 100 STANDARD LCS LC1UO906 6.5 6.6 98 i

DUPLICATE MD 952012 2 107 110 3

PARAMETER:Uranita 235, total-i 4

. 1(ISO U)

'DATE/ TIME ANALY2ED:09/26/95 11:13 DC BATCH NUMBER:171088 i 'ORTING LIMIT /DFs

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UNITS pCl/l.

NETHOD REFERENCE CA GLR *R405 -

' TECHNICIAN:DW I

kLANK MB MB1UO906 0.0 420 West First Street Casper, WY 82601 (307) 235-5741 i

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l QUALITY CONTROL REPORT 02/08/ %

JOB NUMBERS. 951927' CUSTOMER: KERR McGEE CORPORATION

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'JEFF OSTMEYER ANALYSIS DUPLICATES REFERENT,E STANDARDS NATRIX SP!KES ANALYSIS ANALYSIS ANALYSIS ANI.;.YZED DUPLICATE lRPDor TRUE PERCENT ORIGINAL SP!KE PERCENT TYPE SUS TTPE I.D.

VALUE (A)

VALUE (B) l(lABl}

VALUE RECOVERY VALUE ADDED RECOVERT PARAMETER:Uranius 235,. total? '(ISO U)'

LDATE/ TIME ANALYZED 09/26/95 11:13.

. OC BATCH NUMBER 171088 REPORTING LIMIT /DF:/

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l METHOD REFERENCE :CA GLR R405" TECMICI AN:DW l

BLANK MB M82UO906 0.0 DUPLICATE MD 952012-2 4.5 5.0 11 PARAMETER: Uranium 238,'. total- (ISO U)

DATE/ TIME ANALYZED 09/26/95 11:19 QC BATCN IRmBER 171092 REPORTING LIMIT /DF:

UNITS:pCf/L-METHOD REFERENCE :CA GLR R405 TECHNICIAN:DW BLANK MS MB1UO906 0.1 i

BLANK Ms MS2UO906 0.1 STANDARD LCS ST1UO906 6.2 6.0 103 STANDARD LCS LCiUO906 6.7 f.0 112 i

DUPLICATE MD 952012 2 48.2 48.2 0

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}WMB CORE LA: ORATORIES QUALITY CONTROL FOOTER l

i METHOD REFERENCES 1

(1) LPA 600 4-79420. Methods for Chemwal Analysis of Water and Wastes. March 1983 (2 ) l PA SW-R46. Test Methods for Evaluatmg Sohd Waste. Unrd Ediuort November 1990 and July 1992 update (3i Standard Methods for the baminanon of Water and Wastewater.17t!L 1989 (4) LPA 600 4-80-032. Pressnhed Pnwedures fiw Measurement of Radioacimsy m Dnnkmg Water, August 1980 (5) Irderal Regisser, inday. October 26.19x4 (40 CFR Part 136)

16) EPA #900 R.7n-017. Microbiologwal Metimmh for Monnonne the Environment, December 1978 COMMENTS

(!) nw data m the Lahorsiorv Test Resulta Report mas ddTer from the data in the QC Report due to c4eulanons for sampic preparauon andor ddutions (2) The " Time Analvreu" m the QC Repnt mav not retlect the actual tune of each analysis. The "Daie Analyzed"is the actual date of analpas (3) Sod and sludge samples are reported on a wet basis or on an "as rcceived" basis unless otherwise mdicated.

(4 the data m this repnt are withm the hmits ni urwertamtv specified m the referenced method unless otherwise indacated.

(9) Analvses per1onned by a subsonunct laborahn are indwaned with an astensk and annostated code m the "Techrucian" data licid-1 Subcontract Laboratones Code Core laboratones. Anahemt CA

' AN Core Iahorntones. Aurora.CO

  • AU Core Laboratones. Casper. WY

'CA Core Laboratones. Corpus Chnsta. TX

  • CC Core Laboratones. linustart TX
  • HP Core Laborstones. Lake Charlea. LA
  • If Core Laboratones. Long Beach. CA
  • LB Other Subcontra61 Laboratones
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i DEFINITIONS (1) NC = Not Calculabic due to values lowe than the reponmg lumt.

(2) ND - Not Detected above the reportr.g imut.

OC SA MPLE IDENTIFICATIONS BLANKS SPIKES MB Method Illank (aho refened to as a preparauon blank)

MS = Matnx Spike RH - Reagent Diank MSD = Manna Spike Duplicate III instrument liiank PDS

  • Post Disosson Spike ICH - ImtialCabhration Blank BS = tvank Spike (also referred to as a method spike)

CCD - Conimuing Cahbration illank SS = Surrogene Spike llB lloidmg Blank (also referred io as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = Cahbraban Standard MSD = Matnx spike Duptwate RS = Reference Standara (also refened to as an external reference standard)

MD Methud Duptwate ICV = innialCahbration Venfication CCV = ContumamsCahbrauon Venficauan l

ifs = LaboratoryControlSample l

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