ML20207B837

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Core Labs Analytical Rept for Job Number 940632
ML20207B837
Person / Time
Site: 07003073
Issue date: 05/10/1994
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080261
Download: ML20207B837 (9)
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WESTERN ATLAS 1

Core Laboratories l

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ANALYTICAL REPORT i

Job Number:

940632 Prepared For-KERR-McGEE CORPORATION JEFF OSTMEYER PeOeBOX 89 CUSHING, OK 74023 i

Date:

05/10/94 l

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Name: Rondalynn Mull Core Laboratories, Inc.

I 420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor 9903000261 981106

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l NERE wastasus ATLAS Cure I aboratories LABORATORY TEST $

RESULTS 05/10/94 JOB NUMBER:,940632 CUSTOMER: KERR-McGEE CORPORAfl0N ATTN ' JEFF OSTMEYER 1

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!.D.........: BLOCK 48-E70-$ 50 LABORATORY 1.D...: 940632-0001 DATE SAMPLED.......: 03/25/94 DATE RECEIVED..... 04/04/94 TIME SAMPLED.......: 13:30 TIME RECrlVED....: 10:00 l

WORK DESCRIPflod...: CU1 65-007 REMARKS..........: WATER

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TEST DESCRIPTION FINAL RESULT DETECTION LIMIT UNITS OF MEASURE TEST METHOD DATE TECHNICIAN Thoriun 230, total 0.2 pCi/l 05/02/94 JG i

Thoriun 230, total, error, +/-

0.3 pCl/l 05/02/94 JG Thoriun 230, total, LLD 0.5 pCl/l 05/02/94 JG Thoriun 232, total 0.1 pCi/l 05/02/94 JG Thortun 232, total, error, +/-

0.1 pcl/l 05/02/94 JG Thortun 232, total, LLD 0.2 pCi/l 05/02/94 JG urani n 234, total 7.4 pcl/l 04/29/94 PLJ Urtnf un 234, total, error, +/-

1.4 pci/l 04/29/94 PLJ Urmiun 234, total, LLD 0.5 pCi/l 04/29/94 PLJ Uraniua 235, total 0.1 pCi/l EPA 901.1 04/29/94 PLJ Urtniun 235, total, error, +/-

0.1 pCi/l 04/29/94 PLJ Uraniun 235, total, LLD 0.3 pCi/l 04/29/94 PLJ uraniun 238, total 4.1 pci/l 04/29/94 PLJ Uraniun 238, total, error, +/-

0.9 pCl/l 04/29/94 PLJ uraniun 238, total, LLD 0.4 pCi/l 04/29/94 PLJ Thoriun 228, total -

1.0 pCl/l 05/02/94 JG Thoriun 228, total, error, +/-

0.3 pCi/l 05/02/94 JG Thoriun 228, total, LLD 0.3 pCi/l 05/02/94 JG 420 West First Street Casper, WY 82601 l

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LABORATORY TESTS RESULTS 05/10/94 JOS NUM8ER: 940632 CUSTOMER: KERR-McGEE CORPORATION ATTN JEFF OSTMEYER CLIENT I.D.........: BLOCK 48-E55-S-5 LABORATORY 1.D...: 940632 0002 DATE SAMPLED.......: 03/26/94 DATE RECE!VED..... 04/04/94 TIME SAMPLED.......: 11:00 TIME RECEIVED....: 10:00 WORK DESCRIPTION...: CU1 65-009 REMARKS..........: WATER I

TEST DESCRIPTION FINAL RESULT.

DETECTION LIMIT UNITS OF MEASURE TEST METHOD DATE TECHNICI Alu Thoriun 230, total 0.5 pCl/l 05/02/94 JG Thorium 230, total, error, +/-

0.3 pCi/l 05/02/94 JG Thorium 230, Mtat, LLD 0.4 pCi/l 05/02/94 JG Thoriun 232, total 0.2 pCi/l 05/02/94 JG Thortun 232, total, error, +/-

0.1 pCl/l 05/02/94 JG Thoriun 232, total, LLD 0.1 pCi/l 05/02/94 JG Urcniun 234, total 6.9 pcl/l 04/29/94 PLJ Urtniun 234, total, error, +/-

1.3 pCi/l 04/29/94 PLJ Urentun 234, total, LLD 0.3 pci/t 04/29/94 PLJ Urrniun 235, total ND pCi/l EPA 901.1 04/29/94 PLJ Urtniun 235, total, error, +/-

0.1 pCi/l 04/29/94 PLJ i

Urtniun 235, total, LLD 0.2 pCi/t 04/29/94 PLJ l

j Uraniun 238, total 3.1 pCi/l 04/29/94 PLJ l

Urtniun 238, total, error, +/-

0.8 pCi/l 04/29/94 PLJ Urtniun 238, total, LLD 0.3 pCl/l 04/29/94 PLJ l

Thoriun 228, totat 0.4 pCi/l 05/02/94 JG j

Thoriun 228, tot at, error, +/-

0.2 pCi/t 05/02/94 JG Thoriun 228, to'tal, LLD 0.4 pCi/t 05/02/94 JG 1

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QUALITY C0NTROL REPORT 05/10/94 JOB NUMBER:- 940632 CUSTOMER: KERR-McGEE CORPORATION ATTN JEFF OSTMEYER i

ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SP!KES I

ANALYSIS ANALYSIS ANALYS!$

ANALYZED OUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS-TYPE I.D.

VALUE (A)

VALUE (8)

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VALUE RECOVERY VALUE ADDED RECOVERY I

?ARAMETER:Urani a 234, total DATE/ TIME ANALYZED:04/29/94 10:55 QC BATCH NUMBER:150616 i

REPORTING LIMIT /DF:

UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN PLJ BLANK M8 M811UO414 0.1 BLANK MB M821UO414 ND STANDARD LCS LC11UO414 6.5 6.6 98 STANDARD LCS ST11UO414 6.7 6.6 102 SP!KE MS 940631 1 11.3 2.4 8.2 109 DUPLICATE MD 940634-1 4.1 3.3 22 i

j PARAMETER:Uranlun 235, total DATE/ TIME ANALYZED:04/29/94 11:18 QC BATCH NUMBER:150622 REPORTING LIMIT /DFs UNITS:pCf/l METHOD REFERENCE : EPA 901.1 TECHNICIAN:PLJ BLA~K MB M811UO414 ND BLANK MB M821UO414 ND DUPLICATE MD 940634-1 ND 0.1 0

PARAMETER:Uranlun 238, total DATE/ TIME ANALYZED:04/29/94 11:28 cc BATCH NUMBER:150625 j

REPOR?!NG LIMIT /DF:

UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:PLJ BLANK M8 M811UO414 ND I

BLANK MB M82!UO414 ND STANDARD LCS LC11UO414 7.3 6.9 106 SVANDARD LCS ST11UO414 6.9 6.9 100 j

SP!KE MS 940631-1 10.8 1.3 8.6 110 DUPLICATE MD 940634-1 1.4 1.5 7

PARAMETER: Thorium 228, total DATE/ TIME ANALY2ED:05/02/94 15:03 QC BATCH NUMBER:150693 i

REPOR71NG LIMIT /DF:

UNITS:p 1/l METHOD REFERENCE :

TECHNICIAN:JG BLANK MB MB3T0415 ND BLANK MB MB4T0415 0.1 SVANDARD LCS ST2T0415 4.7 4.0 118 j

STANDARD LCS LC270415 3.7 4.0 92

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SP!KE MS 940637-1 4.9 0.3 4.0 115 2

i DUPLICATE MD 940633 1 0.5 0.6 18 l

PARAMETER:Thartum 230, total DATE/ TIME ANALY2ED:05/02/94 15:10 oC BATCH NUMBER:150697 REPCQVING LIMIT /DFs UNITS:pCi/l METHOD REFERENCE :

TECHNICIAN:JG fM8 MB3T0415 0.1 SLANK BLACK M8 M84T0415 ND STANDARD LCS ST3T041$

1.7 118 STAC9ARD LCS LC3T0415 1.7 106 SPIKE MS 940632-1 0.2 1.7 124 DUPLICATE MD 940633 1 0.3 50 l

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1 QUAL!TY CONTROL REPORT J

05/10/94 JOB NUMBER: 940632 CUSTOMER: KERR-McGEE CORPORATION ATTN: JEFF OSTMEYER l

ANALYS!$.

DUPLICATES REFERENCE STAND MDS MATRIX SPIKES l

ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE I.D.

VALUE (A)

VALUE (8)

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VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER Thorita 232, total DATE/ TIME ANALYZED:05/02/94 15:27 QC BATCH NUMBER:150701 REPORTING LIMIT /DF:

UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN JG BLANK MS M83T0415 ND BLANK-MB M64T0415 ND STANDARD LCS ST2T0415 4.5 4.0 112 i

STANDARD LCS LC2TD415 4.2 4.0 105 SP!KE MS 940637 1 4.4 ND 6.0 110 DUPLICATE MD 940633-1 0.2 0.2 0

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wastsaw ATLAS

' Core Laboratories QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600/4-79420. Methods for Chenu6al Analysis of Water and Wastes, March 1983 (2) EPA SW-846. Test Methods for Ewiusting Solid Waste, Third Ednion, November 1990 and July 1992 up$ ate (3) Standard Methods for the Exanunation of Water and W* stewater,17th,1989 (4) EPA 600'4-80 032. Prescnbod Procedures for Measurement of Radioacuvity in Dnnking Water, August 1980 (5) Federal Register, Fnday, Octaher 26,1984 (40 CFR Part 136)

(6) EPA 600'8 78417, Microtnological Methods for Marutonns the Environment. December 1978 COMMENTS (I) The data in the 1.aboratory Test Resuha Report may differ from the data in the QC Report due to calculations for sample preparation and or dilutions.

l (2) The " Tune Analped"in the QC Report may not refleet the actual time of each analysis. The "Date Analyzed" is the actual date of analysis.

(3) Sod and sludge samples are reported on a wet basis or on an "as received" basis unlesa otherwise mdicated (4) 1he data in tius report are within the Imuts of uncertainty specified in the referenced method unless otherwise indicated j

(5) Analyses performed by a subcontract laboratory are indicated with an astensk and associated code in the " Technician" data field.

Subcontract Laboratories Code Core Laborsione. Anahrun.CA

  • AN

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Cure Laborarones. Aurora.CO

'AU Core Laboratones. Casper, WY

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Core Laboratories. Corpus Chnsti. IX

  • CC i

Core laboratones. Houston. TX

Core Lalmtories. Lake Charles. LA

  • LC Core Laborazones - bng Beach, CA
  • LB Other Subcontract blmtones
  • XX

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DEFINITIONS (1) NC = Not Calculable due to values lower than the repnrting linut.

(2) ND = Not Detected above the reporting hmit.

OC SAMPLE IDENTIFICATIONS I

l BLAhKS SPIKES l

MB. Method Blank (also refened to as a preparation blank)

MS = Matnx Spike l

RB = Reagent Blank MSD = Matnx Spike Duphcate IB = Instrumern Blank PDS = Post Digestion Spike ICB = InitialCalibration Blank BS = Blank Spike (also referred to na a method spike)

CCB = Contuwing Calibration Blank SS = Surrogate Spike HB

  • Holding Blank (also referred to as as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = Calibration Standard i

MSD = Mainx Spike Duphcate RS = Referenu Stardard(also referred to as an external reference stanaard)

MD = Method Duphcate ICV = Initial Calibration Venfication i

CCV = ConunuingCahbrationCahbrauon IIS = Laboratory Control Sample 420 West First Street Casper.WY 82601 i

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CORE LABORATORIES Western Attes interna.tional

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Sample Receipt Acknowledgment Date

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THIS IS NOT AN INVOICE l

Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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o LOG-10 JOB REPORT 04/08/94 J08 WUMBER 940632 CUSTOMER (KE0001) KERR-McGEE CORPORATION CONTACT:JEFF OSTMEYER PHONE:(

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SAMPLE NUMBER:0001 DATE RECEIVED:04/04/94 TIME RECEIVED:10:00 SAMPLE DATE:03/25/94 SAMPLE TIME:13:30 DUE. CAT [ 05/02/94

' PROJECT IP BLOCK 48-E70+S-50 SAYPLE ID:CU1-65-007 REM: WATER LA8 NOTES 134L CUBE SHOCT ID:

SIN NUMBER:0 CODE TEST DESCRIPTION TEST LIMITS UNITS OF MEASURE TEST METHOD COBOqENTS R552 Thori a 230, total pcl/t R553 Thori a 230, total, error, +/-

pcl/l R554 Thori a 230, total, LLD pCi/l R555 Thorium 232, total pcl/l R5% Thori m 232, total, error, +/-

pCf/L R557 Thorium 232, total, LLD pCi/L RM1 Uranim 234, totst pcl/l R562 Urani m 234, total, error, +/-

pcl/l R563 'Urani m 234, total, LLD pCi/l R564 Urani a 235, total pCf/t EPA 901.1 R565 Urani a 235, total, error, +/-

pCl/l R$66 Urani m 235, total, LLD pci/L R567 Urani m 238, total pcl/l R%8 Uranium 238, total, error, +/-

pci/l R569 Urani m 238, total, LLD pCi/l R570 Thori m 228, total pcl/l R571 Thori m 228, total, error, +/-

pCi/t R572 Thori m 228, total, LLD pCi/l SAMPLE NUMBER:0002 DATE RECEIVED:04/04/94 TIME RECEIVED:10:00 SAMPLE DATE 03/26/94 SAMPLE TIME 11:00 DUE DATE:05/02/94 PROJECT ID:8 LOCK 48-E55 5-5 SAMPLE ID:CU1-65-009 REM: WATER LAS NOTES:114L CUSE SHORT ID:

BIN NUMBER 0 CODE VEST DESCRIFil0N TEST LIMITS UNITS OF MEASURE TEST METHOD COMMENTS R552 Thortun 230, total pCf/t l

R553 Thorium 230, total, error, +/-

pCf/l R554 Thoriun 230, total, LLD pCl/l R555 Thori m 232, total pCl/l R556 Thortun 232, total, error, +/-

pCi/t R557 Vhorius 232, total, LLD pCl/l R561 Uranlun 234, total pcl/l R562 Urantun 234, total, error, +/-

pCl/l R563 Urantun 234, total, LLD pcl/l R564 Urantun 235, total pCi/t EPA 901.1 R565 Uranlun 235, total, error, +/-

pCl/l R566 Urantun 235, total, LLD pC1/l R%7 Uraniun 238, total pCl/l R568 Urantun 238, total, error, +/-

pCf/l R569 Uranita 238, total, LLD pC1/1 R570 Thor *un 228, total PC1/l R571 Thorium 228, totat error, +/-

PCl/l R572 Thorium 228, total, LLD pCl/l PAGE 1

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