ML20207C006

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Amended Rept for Core Labs Analytical Rept for Job Number 951925
ML20207C006
Person / Time
Site: 07003073
Issue date: 02/08/1995
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080314
Download: ML20207C006 (7)
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Text

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bY WM CORE LABORATORIES AMENDED REPORT 4

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CORE 9 IABORATORIES7 i

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.? Job Numbers 951925

PreparedXFor: 1
KERR McGEE CORPORATION-JEFF OSTMEYER P.O.-BOX'89

. CUSHING; OK1 74023 Date:- 02/08/96:

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Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor 9903000314 991106

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KERR McGEE CORPORATION P.O. BOX 89 CUSHING OK 74023 JEFF OSTIEYER i

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N WRU CORE LABORATORIES l

LABORATORY TESTS RESULTS 02/08/96 l J05 INalBEtti. 951925j

? CUSTOMER:..KERRMcGEECORPORATION l ATTN. JEFF OSTMEYER-l CLIENT I.D.........: ANNUAL ENVIRONMENTAL CMW 19.1 LABORATORY I.D...: 951925-0001 DATE SAMPLED.......: 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 WORK DESCRIPTION...: CU2-26-024 REMARKS..........: WATER TEST DESCRIPTIONO FINAL RESULT!

DETECTION LIMIT UNITS OF MEASURE 1 TESTMETHOD)

DATEL TECHNICIAN Gross Alpha, total 136 pcl/l EPA 900.0 08/30/95 NRF l Gross Alpha, total, error, +/-

45.3 pcl/t 08/30/95 NRF l 8ross Alpha, total, LLD 37.1 pci/t 08/30/95 NRF l

l cross seta, total 135 pci/L EPA 900.0 08/30/95 NRF Gross Beta, total, error, +/-

35.1 pcl/t 08/30/95 NRF Gross Beta, total, LLD 48.3 pct /L 08/30/95 NRF Thortus 232, total 0.89 pcl/t 09/25/95 DW Thortus 232, total, error, +/-

0.6 pci/t 09/25/95 DW Thortun 232, total, LLD 0.7 pct /L 09/25/95 DW Uranius 234, total (150 U) 3.9 pcl/l cA GLR R405 09/26/95 DW uraniun 234, total, error, +/-

0.9 pct /t 09/26/95 DW Uranium 234, total, LLD 0.3 pcl/l 09/26/95 UW Uranium 235, total (ISO U) 0.1 pcl/l CA-GLR-R405 09/26/95 DW Uranium 235, total, error, +/-

0.2 pct /t 09/26/95 DW

Uranlun 235, total, LLD 0.2 pcl/l 09/26/95 DW Uranlue 238, total (ISO U) 2.0 pcl/L CA-GLR R405 09/26/95 DW Uranlun 238, total, error, +/-

0.7 pci/t 09/26/95 DW Uranium 238, total, LLD 0.2 pcl/t 09/26/95 DW Thorfua 228, total 0.59 pci/t 09/26/95 DW Thortun 228, totat, error, +/-

0.6 pct /t 09/26/95 DW Thorlue 228, tota (, LLD 1.2 pci/t 09/26/95 DW 420 West First Street casper, WY 82601 (307) 235-5741 PAGE:2 no eu.. -.r

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}nLAB CORE LABORATORIES QUALITY CONTR0L REPORT 02/08/96 JOB IBmBER s951925I

?CUBTOMEtti G RR Mc0EE CORPORATIONi SATTNNJEFFOBTMEYERE ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES

'NALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIE PERCENT TYPE SUB-TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bl}

VALUE RECOVERY VALUE ADDED RECOVERY 2ARMTER:GrossAlphedtoteln..........<

% DATE/ TIME ~ ANALYZED:08/30/95s 14:05; tGC'BATCN IRSIDER 170093 IEPWTING LIMIT /DFF ' 6tallTS:ptt/lM L DETHW REFERENCEp

  • EPA 900.0 s nTECMICIAN:NRF IL M MB MB2AB0829 ND iTANDARD LCS LCIA0829 22.4 25.5 88 3 PIE MS 951963 1 124 10.0 128 89 XJPLICATE e

951963 1 10.0 14.6 37

'ARMTER Gross' Bete,l totet:{

?DATE/ TIME ANALYZED 08/30/95! 14:14e fOC BATCH NUMBER 170097 tEPORTING LIMIT /DF:y iUNITS pCf/li NETHOD' REFERENCE 5* EPA'900.0J TECM ICIAN:NRF 3L M MB MB2AB0829 0.4 STANDARD LCS LC180829 23.9 22.0 109 iPIKE MS 951963 1 144 5.0 110 126 XJPLICATE e

951963 1 5.0 8.8 55

>AAAMETER:Thorfim 232f totet!

?DATE/ TIME ANALYZED:09/25/95?16:495 GC BATCM IRsIDER 171053

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tEPW TING LIMIT /DF:l h lal!TS:pCf /lN:

1 METHOD REFERENCE--:

' TECMICI AN:DW BL M MB MB5T0906 0.47 3 LANK W

MB6T0906 0.95 STANDARD LCS ST3T0906 7.59 7.0 108 3TANDARD LCS LC3T0906 7.1 7.0 101 iPIKE MS 951921 1 16.3 0.92 14.0 110 1

XJPLICATE 2

951922 1 0.61 0.89 37 2ARAMETEC:Thselus' 228i.totali.

.'DATE/ TIME ANALYZED:09/26/95f 08:19.

OC BATCH ltatBER 171058 tEPORTING LIMIT /DF:

? UNITS:pCf/l

' METHOD REFERENCE. :

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TECMICIAN:DW 3 LANK M3 MB5T0906 0.18 3 LANK MB M56T0906 0.01 iTANDARD LCS ST3T0906 7.0 7.0 100 3TANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921 1 18.0 0.35 14.0 126 XJPLICATE e

951922 1 0.74 0.86 15 2ARAMETER:Uranlue 234,jotel. (!$0 U);

DATE/ TIME ANALYZED:09/26/95 10:46 QC BATCH NUMBE; 171081 4FPORTING LIMIT /DF24

UNITS:pci/l -

~ METHOD REFERENCE :CA GLR R405 TECHNICIAN:0W 3L M MB M1UO906 0.2 3L M MB MR2UO906 0.3 STANDARD' LCS ST1UO906 6.6 6.6 100 3TANDARD LCS LC1UO906 6.5 6.6 98 XIPLICATE -

MD 952012 2 107 110 3

2ARAMETER: Uranium 235,;totalJ (ISO U)1 l DATE/ TIME. ANALYZED:09/26/95 11:13 OC BATCH NUMBER 171088 4EPORTilIG LIMIT /DF '

UNITS
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METHOD REFERENCE :. CA-GLt R405 TECNNICIAN:DW 3 LANK MB MB1UO906 0.0 420 West First Street Casper, WY 82601 (307) 235-5741 PAGE:3 r - -.

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}WLAB CORE LABORATORIES QUAL 17Y CON 7ROL REPORT i

02/08/96

! os IRm0ER 4951925>

sCUSTOMER -IKERR McGEE CORPORATION

'ATTW: 'JEFF OSTMEYERt J

ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIES IANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIE PERCENT l TYPE SUB TYPE I.D.

VALUE (A)

VALUE (B)

(lABl}

VALUE RECOVERY YALUE ADDED RECLWERT PARAMETER:Urantun 235f totalt j (Ito U) -.

? DATE/ TIME. ANALYZED:09/26/95 311:13 :

OC BATCN IRatgERt171088 REPORTING LIMIT /DFs [ ' tUNITS
pC1/1i L METHOD REFERENCE : CA-GLR R405.

= TEclut!CIAN:DW

>SLANK Ms MB2UO906 0.0

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952012-2 4.5 5.0 11 l

PARAMETER: Uranium 238,1 total 4 (ISO U):

-DATE/ TIME ANALYZED 09/26/95"11:19-L OC BATCH NUMs!R 171092

, REPORT!IeGLIMIT/DF2}

iUNITSapC1/1" 9 METHOD REFERENCE' :CA GLR R405" TECHNICIAN DW BLANK MB Ms1UO906 0.1

BLANK Ms Ms2UO906 0.1 STANDARD LCS ST1UO906 6.2 6.0 103 STANDARD LCS LC1UO906 6.7 6.0 112 DUPLICATE m

952012-2 48.2 48.2 0

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C SAMPLE NU'tBER:C001 DATE RECEIVED:P8/24/95 TIME RECEIVED:10:08 SAMPLE DATE:08/23/95 SAMPLE T!f1E:

DUE DATE:09/21/95 PROJECT ID: ANNUAL ENVIRDNMENTAL CMW 19.1 SAMPLE ID:CU2-26-024 REI: WATER L O MDTES:114 L CUBE 2.lRT 10:

BIN NUMBER:L 6

CDDE TEST DESCRIPT10M TEST LIMITS UNITS OF MEASURE TEST METHDD CDMMENTS R000 UNAT CHECK FOR ISD U R513 Gross Alpha, total PCi/l EPA 900.0 R$14 Gross Alpha, total, error, f/-

pCi/l R515 Gross Alpha, total, LLD 4.,

pC1/1 r.

R516 Gross Beta, total pCi/l EPA 900.0 R517 Gross Beta, total, error, f/-

pCi/1 R518 Stoss Beta, total LLD pCi/l R555 Thorius 232, total pCi/l R556 Thorius 232, total, error, t/-

pCi/l R557 Thorium 232, total LLO pCi/l R561 Uranium 234, total (150 U) pCi/1 CA-6LR-R405 R562 Uranius 234, total, error, f/-

pC1/1 R563 Uranius 234, total, LLD pCi/l R564 Uranius 235, total (ISO U) pC1/1 CA-6LR-R405 R565 Uranius 235, total, error, f/-

pCi/l R566 Uranius 235, total, LLO pC1/1 R567 Uranium 23B, total (150 Ul pC1/1 CA-6LR-MD5 R568 Uranius 230 total, error, f/-

pct /l R569 Uranius 238, total, LLD pC1/1 R570 Thortus 228, total pCi/l Rs71 Thorium 228, total, error, f/-

pC1/1 R572 Thortus 228, total, LLD pCi/l 1

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nlW CORE LABORATORIES QUALITY CONTROL FOOTER METHOD REFERENCES (l) EPA 600 4 79 020. Methods for Chenucal Analysis of Water and %stes. March 1983 (2) FPA SW-R46. Test Method. for Evaluatmg Solid Ws Third Edition. November 1990 and July 1992 update (3) Standard Methods ihr the F ummatum of Water and Wastewater.17th.1989 (4) EPA 600 4 80 032. PreeM Piocedures for M<.asurement of Radioactmty m Dnnking Water. August 1980 (5) f ederal Register, f nday. October 26.198t4 (40 CFR Part 136)

(6) EPA 600 E 78 Ol7. M6cndnulogwal Methods for Mosutcrmg the Environment. December 1978 COMMENTS (l) h data m the talmratorv Test Results Report may difTer from the data m the QC Report due to calculations for sample preparauon ancL or dilutions.

(2) The " Time Analyzed" m the QC Report may not reflea the aaual tune of each analysts. The "Date Analyzed"is the actual date of analysis.

(3) Soil and sludge samples are rsported on a. net basis or on an "as rcceived" basis unless otherwise indicated.

(4) The data m this report are withm the hmrts of uncertamey specified m the referenced method unless otherwise ualwated.

(S) Analyses performed by a subcontract laboratory are indecated with an estensk and associated code in tha ' Muunan" data field Subcontract Laboralga_es fads Core 14borstones AnahemtCA

' AN Core laboratones. Aurora. CO

  • AU Core tabarstrtws. Casper. WY

'CA Core laboratones. Corpus Chnsti. TX

  • CC Core Lahnratones Hmston.TX

'HP l

Core laboratones. Lake Charles. LA

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Core Laboratones. Iong Beach, CA

  • LB Other Subcontract Laboratones
  • XX DEFINITIONS (l) NC = Not Calculable due to values lower than the reportmg hmit (2) ND = Not Detected above the reportmg knut OC SAMPLE IDENTi.FICATIONS BLANKS SPIKES MB = Method Blank (also referred to as a preparatmn blank)

MS Matrix Spika a

RB = Reagent Blank MSD = Maena Spike Duplicate IB = Instrunwen Blank PDS = Post Digestmn Spike ICB - ImtialCahbration Blank BS Blank Spike (also referred to as a method spike)

=

CCB = Contmuing Cahbranon Blank SS = Surrogais Spike HB = Holdmg Blank (also referred to as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = CahbrataanStandard MSD = Matnx Spike Dupheane RS = Reference Standard (also referred to as an external refernice standard)

MD Method Dupheate ICV = InnsalCahbrepon Venfication CCV = ContmumsCalibraten Venfication 145 = [AaratoryControlSample 420 West first Street l

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