ML20207B831

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Core Labs Analytical Rept for Job Number 940635
ML20207B831
Person / Time
Site: 07003073
Issue date: 05/10/1994
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080258
Download: ML20207B831 (8)
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KRW wasvunn ATLAS Core Laboratories CORE LABORATORIES A N A L Y T I C'A L' REPORT Job Number:

940635 Prepared For:

KERR-McGEE CORPORATION JEFF OSTMEYER P.O. BOX 89 CUSHING, OK 74023 Date:

05/10/94 n c/

Signature Date:

Name: Rondalynn Mull Core Laboratories, Ince 420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor 9903000258 981106 3

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Core Laboratories LAB 0 RAT 0RY TESTS RESULTS 05/10/94 JOB NUMBER: 940635 CUSTOMER: KERR-McGEE CORPORATION ATTN: JEFF OSTMEYER k

i CLIENT I.D......... : BLOCK 47-E80-S-18 LABORATORY I.D...: 940635-0001 DATE SAMPLED.......: 03/25/94 DATE RECEIVED....: 04/04/94 1

TIME SAMPLED.......: 15:00 TIME RECEIVED....: 10:00 WORK DESCRIPTION...: CU1-65-006 REMARKS..........: WATER I

l TEST DESCRIPil0N, FINAL RESULT DETECTION LIMIT UNITS OF MEASURE TEST METHOD DATE TECHNICIAN Thoriun 230, total -

0.4 pcl/l 05/02/94 JG Therium 230, totat,' error, +/-

0.3 pCl/l 05/02/94 JG Thorium 230, totst, LLD 0.5 pCi/l 05/02/94 JG ihorium 232, total 0.4 pCf/l 05/02/94 JG Th rium 232, total, error, +/-

0.2 pcl/l 05/02/94 JG Thorium 232, total, LLD 0.2 pCi/l 05/02/94 JG Urantun 234, total 5.7 pCi/l 04/29/94 PLJ Uranium 234, total, error, +/-

0.9 pCi/l 04/29/94 PLJ Uraniun 234, total, LLD 0.2 pcl/l 04/29/94 PLJ Uranium 235, total 0.2 pCi/l EPA 901.1 04/29/94 PLJ Uranium 235, total, error, +/-

0.1 pcl/l 04/29/94 PLJ Urcnium 235, total, LLD 0.2 pCi/l 04/29/94 PLJ Uranium 238, total 2.6 pC1/:

04/29/94 PLJ Urenium 238, total, error, +/-

0.5 pCi/l 04/29/94 PLJ

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i Urenium 238, total, LLD 0.2 pcl/l 04/29/94 PLJ Thorium 228, total 0.7 pci/l 05/02/94 JG i

i Thoriun 228, total,crror, +/-

0.2 pCi/l 05/02/94 JG Thorium 228, total, LLD 0.3 pcl/l 05/02/94 JG i

l 420 West First Street Casper, WY 82601 1

(307) 235-5741 4

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I BERE wasmuss ATLAS Core Laboratories QUAL!TY C0NTR0L REPORT 05/10/94 J08 NUMBER: 940635 CUSTOMER: KERR-McGEE CORPORATION ATTN JEFF OSTMEYER ANALTSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALYSl$

ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUB TYPE I.D.

VALUE (A)

VALUE (B)

(lABj)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Urani m 234, total DATE/ TIME ANALYZED:04/29/94 10:55 QC BATCH NUMBER:150616 REPORTING LIMIT /DF:.

UNITS:pCf/t METHOD REFERENCE :

TECHNICIAN:PLJ BLANK MS M811UO414 0.1 BLANK MS M821UO414 ND STANDARD LCS LC11UO414 6.5 6.6 98 i

$7ANDARD LCS ST1!UO414 6.7 6.6 102 SP!KE MS 940631-1 11.3 2.4 8.2 109 DUPLICATE MD 940634 1 4.1 3.3 22 PARAMETER:Urani a 235, total DATE/ TIME ANALYZED:04/29/94 11:18 QC BATCH NUMBER:150622 REPOR71NG LIMIT /DF:

UNITS:pci/l METHOD REFERENCE : EPA 901.1 TECHNICIAN:PLJ lMB M811UO414 ND BLANK BLANK M8 M821UO414 ND DUPLICATE MD 940634 1 ND 0.1 0

PARAMETER:Urani m 238, total DATE/ TIME ANALYZED:04/29/94 11:28 QC BATCH NUMBER:150625 REPONTING LIMIT /DF:

L'illTS:pCl/l METHOD REFERENCE :

TECHNICIAN:PLJ BLANK M4 M811UO414 ND BLANK M8 M821UO414 ND STANDARD LCS LC11UO414 7.3 6.9 106 STANDARD LCS ST1!UO414 6.9 6.9 100 SPIKE MS 940631 1 10.8 1.3 8.6 110 DUPLICATE MD 940634 1 1.4 1.5 7

PARAMETER:Thori m 228, total DATE/ TIME ANALYZED:05/02/94 15:03 QC BATCH NUMBER:150693 j

REPORTING LIMIT /DF:

UNITS:pci/l METHOD REFERENCE :

TECHNICIAN:JG I

BLANK MB MB3T0415 ND BLANK MB MB4T0415 0.1 STANDARD LCS ST2TD415 4.7 4.0 118 STANDARD LCS LC270415 3.7 4.0 92 SPIKE MS 940637-1 4.9 0.3 4.0 115 DUPLICATE MD 940633-1 0.5 0.6 18 i

PARAMETER:Thori m 230, total DATE/ TIME ANALYZED:05/02/94 15:10 QC BATCH NUMBER:150697 REPORi'ING LIMIT /DF:

UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:JG j

BLANK MB MB3T0415 0.1 BLANK MB MB4T0415 ND SVANDARD LCS ST3T0415 2.0 1.7 118 STANDARD LCS LC3T0415 1.8 1.7 106 SPIKE MS 940632 1 2.3 0.2 1.7 124 DUPLICATE MD 940633-1 0.5 0.3 50 i

420 West First Street Casper, WY 82601 (307) 235-5741 l

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ATLAS Core Laboratories 0UALaTY C0NTR0L REP 0RT 05/10/94 JOB NUMBER:. 940635 CUSTOMER: KERR-McGEE CORPORAfl0N ATTN: -JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRlX SP!KES ANALYS1$

ANALYSIS ANALYSIS ANALYZED DUPLICATE 'RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE.

SUS TYPE I.D.

VALUE (A)

VALUE (B)

(lA-8l)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Thortun 232, total DATE/ TIME ANALYZED:05/02/94 15:27 QC BA1CH NUMBER:150701 REPORTING LIMIT /DF: '

UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:JG BLANK MS M83T0415 ND r

BLANK MS M84T0415 ND STANDARD LCS ST270415 4.5 4.0 112 STANDARD LCS LC2T0415 4.2 4.0 105 SPIKE MS 940637-1 4.4 ND 4.0 110 DUPLICATE MD 940633 1 0.2 0.2 0

420 West First Street i

I Casper, WY 82601 l

(307) 235-5741 PACE:3

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l wasnes ATLAS Core Laboratories QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600,4-79 020. Methods for Chemical Analysis of Water and Wastes, March 1983 1

(2) EPA SW-846, Test Methods for Evaluatmg Solid Waste, nird Edinon, November 1990 and July 1992 update l

(3) Standard Me' hods for the Exanunanon of Water and Wastewater,17th,1989 (4) EPA 600/4-80-032. Presenbed Procedures for Measurement of Ra&oactivity ui Dnnking Water, August 1980

($) Federal Register. Friday, October 26.1984 (40 CFR Part 136)

(6) EPA 600478417, Microbiological Methods for Morutonng the Environment. December 1978 i

COMMENTS (1) The data in the Laboratory Test Results Report rnay difTer from the data si the QC Report due to calculations for sampic preparauon and or &lu6ans.

(2) The " Time Analyzed" m the QC Report may not reflect the actual tune of each analpis ne "Date Analvud" is the actual date of analysis.

(3) Soil and sludge samples are reported on a wet basis or on an "as received" basis unless otherwise m&cated (4) ne data m this report are within the limits of uncertamty specified in the referenced method unless otherwise in&cated.

(5) Analyses performed by a subcontract laboratory are in&cated with an astensk and associated code in the "Techrucian" data field Sutcontract Latsratories Cgds Care laboratones. Anaheim,CA

  • AN Core Laboratones. Aurora,CO
  • AU Core Laboratones. Casper. WY
  • CA Core Laboratones. Corpus Christa. TX
  • CC Core taboratones. Houston. TX
  • HP Ccre laborazones. Lake Charles, LA
  • LC Core laboratones. Long Beach, CA
  • LB Other Subcontract Laboratones
  • XN, i

DEFINITIONS (1) NC > Not Calculable due to values lower than the reportmg lumt.

(2) ND = Not lktected above the reportang limrt j

OC SAMPLE IDENTIFICATIONS BLANKS SPIKES j

MB - Method Blank (also referred to as a preparation blank)

MS = Matns Snike RB = Reagent Blank MSD = Mainx Spar Duphcate IB Instrument Blank PDS = Post Digesuon Spike

=

ICB = trutialCalilwauan Blank BS = Diank Spike (also referred to as a method spike)

CCB = Contmuing Calibrauon Blank SS = Surrogate Spike HB = Holding Blank (also referred to as as a storage blank)

REFERENCE STANDARDS DUPLICATES CS = Calibration Standard MSD

  • Matnx Spike Duphcate RS = Reference Standartkatso referred to as an external reference standard) i MD Method Duphcate ICV = Initial Calibration Venfication

=

CCV = Conunuing Cahbrauon Cahbrauon j

IIS = laboratory Control Sample 420 West First Street Casper, WY 82601 I

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CORE LABORATORIES Wootern Atdee l

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Customer ID Remarks

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THIS IS NOT AN INVOICE Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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l LOG lN job REPOR7 04/08/94 JOS NUMBER:940635 CUSTOMER (KE0001) KERR-McGEE CORPORATION CONTACT:JEFF OSTMEiER PHONE:(

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SAMPLE NUMBER:0001 DATE RECEIVED:04/04/94 TIME RECEIVED:10:00

$ AMPLE DATE:03/25/94 SAMPLE TIME:15:00 DUE DATE:05/02/94 i

PROJECT ID:5 LOCK 47-E80-S 18 SAMPLE 1D:CU1-65 008 REM: WATER l

LAB NOTES:134L CUBE SHORT ID:

BIN NUMBER:0 l

CODE TEST DESCRIPfl0N TEST LIMITS UNITS OF MEAStNtE TEST METHOD COMENTS I

R552 Thortun 230, total pCf/t R553 - Thorius 230, total, error, +/-

pCf/l l

R554 Thorium 230, total, LLD pCf/1 l

R555 Thorfun 232, total pCf/t R556 Thortun 232, total, error, +/-

pcl/l l

R$57 Thortun 232, total, LLD pCf/t R561 Urantun 234, total pcl/t R562 Uranlun 234, total, error, +/-

pCi/t R563 Urantun 234, total, LLD pCI/l R564 Uranfun 235, total pct /t EPA 901.1 R565 Uranium 235, total, error, +/-

pCf/1 RS66 Uraniun 235, total, LLD pCi/t RS67 Uranius 238, total pCf/;

RS68 Uranlun 238, total, error, +/-

pCi/l R569 Uranlun 238, total, LLD pCi/t R570 Thoriun 228, total pci/t R571 Thorlun 228, total, error, +/-

pCi/t R572 Thoriun 228, total, LLD pci/t l

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SHIP TO:

CHAIN OF CUSTODY RECORD AND ANALYSIS REGUEST.

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Jeff Ostmeyer Note: Time of analysis & tech's these results with Limits:

name must be recorded on other Chain of requirements.

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