ML20207B947

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Amended Rept for Core Labs Analytical Rept for Job Number 951921
ML20207B947
Person / Time
Site: 07003073
Issue date: 02/08/1996
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903080298
Download: ML20207B947 (15)
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CORE LABORATORIES AMENDED REPORT TCORE$IABORATORI5S1

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LJob Number: 1E95192ii iPrepared?For:

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KERR McGEE1 CORPORATION <

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Name: Rondalynn Mull Core Laboratories, Inc.

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i FINAL REPORT DISTRIBUTION 02/08/96 JOB NUMBER: 951921 COMPMY MAME.l COMPMY MAILING ADDRESS -

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SCUSTftlER d EERR McGEE CORPORATIONS

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2 CLIENT I.D.........: ANNUAL ENVIRONMENTAL CMW 9.2 LABORATORY I.D...: 951921 0001 DATE SAMPi f%...... : 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPf..J.......:

TIME RECEIVED....: 10:08 WORE DESCRIPTION...: CU2-26-020 REMARES..........: WATER TEST DESCRIPTION 1 FINAL,RESULTx DETECTION LIMIT.

UNITS OF MEASURE)

TEST METHOD DATE]

{TECNNICIAN Gross Alpha, total 36.4 pC1/1 EPA 900.0 08/30/95 NRF Gross Alpha, total, error, +/-

24.4 pcl/l 08/30/95 NRF Crosa Alpha, total, LLD 28.1 pCf/t 08/30/95 NRF Gross Beta, tota 1 ND pci/l EPA 900.0 08/30/95 NaF Cross Beta, total, error, */-

24.4 pcl/t 08/30/95 NRF Gross Beta, total, LLD 41.0 pCf/t 08/30/95 NRF Thortun 232, total 0.92 pcl/t 09/25/95 DW Thorium 232, total, error, +/-

0.5 pcl/l 09/25/95 DW Th:rlun 232, total, LLD 0.4 pCf/t 09/25/95 DW Urantun 234, total (ISO U) 6.6 pCl/t CA CLR R405 09/26/95 DW Urantun 234, total, error, +/-

1.3 pcl/t 09/26/95 DW Uranlun '.34, total, LLD 0.3 pCl/l 09/26/95 DW t

Uranlun 235, total (ISO U) 0.2 pCl/t CA GLR-R405 09/26/95 DW Uranlun 235, total, error, +/-

0.2 pCl/l 09/26/95 DW Uranlun 235, total, LLD 0.3 pcl/t 09/26/95 DW Uranium 238, total (ISO U) 2.7 pCl/l CA GLR R405 09/26/95 DW Uranlun 238, total, error, +/-

0.8 pCl/l 09/26/95 DW

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Uranium 238, total, LLD 0.3 pcl/t 09/26/95 DW Thortus 228, totat 0.35 pCl/t 09/26/95 DW Thoriun 228, total, error, +/-

0.5 pCl/l 09/26/95 DW Thortua 228, total, LLD 1.1 pCI/t 09/26/95 DW 420 West First Street i

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QUALIFY CONTROL REPORT i

02/08/96 JQsIMSERQ951921S

{CUSMMER:fKERR'Mc0EECORPORATIONE

[ ATTN 2JEFF OSTMEYERL ANALYSIS DUPLICt.TES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SP!KE PERCENT TTPE SUS TYPE I.D.

VALUE (A)

VALUE (s)

(lAsl)

VALUE RECOVERY VALUE ADDED REC 0WERY PARAMETER: Gross Alpha,1 tota,l4.. _.....

METN00. REFERENCE /
EPA 900.0' lTEC MICIAN NRF iDATE/ TIME ANALY2ED:08/30/95 114:057

.;0C BATCM IM SER 170093 s

REPORTING LIMIT /DFa? ~ iUNITSpCl/th BLANK MB M82A80829 ND STANDARD LCS LC1A0829 22.4 25.5 88 SPIKE MS 951963 1 124 10.0 128 89 DUPLICATE MD 951963 1 10.0 14.6 37 ARAMETER Gross sete',: total 4

DATE/ TIME ANALYZED
08/30/95.14:14

'OC BATCH NLaeER 170097 REPORTING LIMIT /DFs;

. UNITS pCf/Li LNETHOD REFERENCE-EPA'900.0' TECHNICIAN:NRF j

i BLANK Ms Ms2A80829 0.4 STANDARD LCS LC180829 23.9 22.0 109 SPIKE MS 951963 1 144 5.0 110 126 DUPLICATE MD 951963 1 5.0 8.8 55 PARAMETERThorita 232, total?..

1DATE/ TIME ANALYZED 09/25/95? 16:497 1 0C BATCH lu eER:171053 REPORTING LIMIT /DFs- ' ? UNITS:pcl/l; JMETHOD REFERENCE L ?

DTECNNICIAN DW SLANK MB Ms5T0906 0.47 BLANK MS M86T0906 0.95 STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101 SPIKE MS 951921 1 16.3 0.92 14.0 110 DUPLICATE MD 951922-1 0.61 0.89 37 PARAMETER: Thorium 228, totst' DATE/ TIME ANALYZED:09/26/95 ~ 08:19

QC BATCH NLaeER:171058 REPORTING LIMIT /DFs UNITS:pCl/l

' METHOD REFERENCE :

TECHNICIAN:DW BLANK Ms Ms5T0906 0.18 BLANK MS M86T0906 0.01 STANDARD LCS ST3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921 1 18.0 0.35 14.0 126 DUPLICATE MD 951922-1 0.74 0.86 15 PARAMETER: Uranium 234, totalH (ISO U)

DATE/ TIME ANALYZED:09/26/95'~10:46 QC BATCH NLeeERi171081 REPORTING LIMIT /DF:

UNITS pcl/l METHOD REFERENCE :CA GLR-R405 TECHNICIAN:DW SLANK Ms Ms1UO906 0.2 BLANK MS M62UO906 0.3 STANDARD LCS ST100906 6.6 6.6 100 STANDARD LCS LC1UO906 6.5 6.6 98 DUPLICATE MD 952012 2 107 110 3

PARAMETER: Uranium 235,'. total -

(ISO U)L

..DATE/ TIME ANALYZED:09/26/95 11:13 QC BATCH NUMBER 171088 REPORTlWG LIMIT /DFs.

UNITS:pCf/t:

LMr.THOD REFERENCE ^:CA GLR-R405 TECHNICIAN:DW BLANK Ms Ms100906 0.0 420 Uest First Street Casper, WY 82601 1

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ANAL 1 SIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES j

ANALYSIS ANALYdl$

ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE I.D.

VALUE (A)

VALUE (B)

(lABj)

VALUE RECOVERY VALUE ADDED RECOVERY PARAME1ERUranita 235, toteLK s(ISO U).:.

'DATE/ TIME ANALY2ED:09/26/95? 11:13:

0C BATCH E81BER:171008 i

REPORTING LIMIT /DF:'

xUNITS:pCl/ty

NETHOD REFERENCE. :CA GLR-R405:

1 TECHNICIAN:DW i

BLANK MB MB2UO906 0.0 DUPLICATE MD 952012 2 4.5 5.0 11 4

PARAMETER:Uranlurs 238, totati: (!$0 U)

DATE/ TIME ANALYZED:09/26/9$ 11:19-

'QC BATCH NUMBER:171092 l

REPORTING LIMIT /DF --

.: IMITS:pCl/ t '

METHOD REFERENCE' :CA GLR-R405 TECMICI AN:DW SLANK MB MB1UO906 0.1 8 LANK MB MB2UO906 0.1 STANDARD LCS ST1UO906 6.2 6.0 103 STANDARD LCS LC1UO906 6.7 6.0 112 DUPLILATE MD 952012 2 48.2 48.2 0

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QUALITY CONTROL FOOTER 1

METHOD REFERENCES 1

1 (1) EPA 600/4 79 020. Methods for Chemical Analysis of Water and Wastes March 1983 I

(2) i PA SW 846. Test Methods for Evaluatmg Sohd Waste. Durd Eddiort November 1990 and July 1992 update

(.h Standard Methods fiv the Examination of Water and Wastewater.17dt 1989 (4) EPA 600 4 80 032. Prencnhed Procedures for Measurement of Radioacuvity m Dnnkmg Water. August 1980

($) f ederal Regsster. Fnday. R1oher 26.19N4 (40 CFR Part 136)

(6) EPA 600 8-784117. Mwnhologwal Mediods for Morutonna the Environment. December 1978

)

COMMENTS (1) N data m the Lahoratorv Test Results Report may ddfer from the data m the QC Report due to calculaimns for sMie preparauun and or dilutions.

(2) The " Time Analyzed"in the QC Report nuv not reflect the actual time ofeach analwis. The Date Analyzed"is the actual date of anajpis.

(3) Sad and sludge samples are reported on a wet basis or on an "as received" basis unless otherwise indicated.

(4) W data m this report are withm the hmns of uncertamtv specified m the referenced nwthod unless othermse mdicated.

($) Analyses performed by a subcontract laborators are indicated wnh an antensk and associated sode m the "Technscian" data field.

Subcontract Laboratories Code Corelaboratones Anaheim.CA

'AN Core laboratones. Aurora. CO

  • AU Core Laboratones Casper, WY
  • CA Core Lahoratones - Corpus Chnsta. IX
  • CC Core Laboratones Houston.TX
  • HP Core Laboratones - Laks Charles. LA
  • If Core Laboratones Img Beacit CA
  • !.B other Subcontraci laboratones
  • w DEFINITIONS 1

(1) NC = Not Calculable due to values lower than the reportmg lunit.

(2) ND = Not Detected above the reportmg knut.

OC SAMPLE IDENTIFICATIONS BLANKS SPIKES l

MD - Method Diank (also referred to as a preparauon blank)

MS Manns Spike RB - Reagent Blank MSD = Mainz Spike Duplicate Ill - Instnament litank PDS = Post Digestion Spike ICB - IrutialCahbratmn 1) lank BS Blank Spike (also referred to as a rnethod spike)

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CCD = Contmuing Cahbration Blank SS Surrogate Spike

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110 a iloidmg Blank (also referred to as a storage blank)

REFERENCE STANDARDS DUPLICATES CS Cahbrataan Standard MSD = Matna Spike Dupheate RS Reference Standard (also referred to as an extemal reference standard)

MD Methud Duphcate ICV = InsualCahbraison Venficauon CCV - Contanums Cahhretion Venfwatson ifs = Laboratory Corurol Sample 420 West first Street Casper,WY 82601 0 07) 235-5741

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A~N A:LLY T I'C A:Li

-R E P_O R T Job' Number:.951921

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KERR McGEE CORPORATION-JEFF OSTMEYER P.O.

BOX 89

- CUSHING,.OK' 74023 Date: ~ 09/27/95~

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Title:

LABORATORY SUPERVISOR I

OCT 0 21995 natev & Envuon Cushing

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LABORATORY TE$T$

RESULTS 09/27/95 JOB NUMBER:: 951921' E nlSTOMER: KERR M;0EE CORPORATION -

ATTN: JEFF OSTMEYER l OLIENT I.D.........: ANNUAL ENVIRONMENTAL CMW 9.2 LABORATORY I.D...: 951921-0001

' 3 ATE SAMPLEO.......: 08/23/95 DATE RECEIVED....: 08/24/95 TIME SAMPLED.......:

TIME RECEIVED....: 10:08 JORK DESCRIPTION...: CU2 26-020 REMARKS..........: WATER j

i VEST DESCRIPTION FINAL RESULT' DETECTION LINIT UNITS OF MEASURE TEST NETHOD -

DATE' TECHNICIAN 3ross Alpha, total 36.4 pCl/l EPA 900.0 08/30/95 NRF 1ross Alpha, total, error, +/-

24.4 pcl/l 08/30/95 NRF Gross Alpha, total, LLD 28.1 pcl/t 08/30/95 NRF j

aross Beta, total ND pCi/t EPA 900.0 08/30/95 NRF 2ross Beta, total, error, +/-

24.4 pcl/l 08/30/95 NRF Bross Beta, total, LLD 41.0 pCi/l 08/30/95 NRF Thortun 232, total 0.92 pCf/t 09/25/95 DW Thorius 232, total, error, +/-

0.5 pcl/l 09/25/95 DW thorius 232, total, LLD 0.4 pCf/t 09/25/95 DW Jraniun 234, total (ISO U) 7.8 pcl/l CA GLR R405 09/26/95 DW Jranium 234, total, error, +/-

1.5 pcl/t 09/26/95 DW Jranium 234, total, LLD 0.4 pCi/l 09/26/95 DW Jranlun 235, total (ISO U) 0.2 pci/l CA-GLR-R405 09/26/95 DW Jrantun 235, total, error, +/-

0.2 pcl/l 09/26/95 DW Jranlun 235, total, LLD 0.3 pcl/l 09/26/95 DW Jraniun 238, total (ISO U) 3.2 pCf/l CA-GLR R405 09/26/95 DW Jraniun 238, total, error, +/-

0.9 pci/t 09/26/95 DW Jranlun 238, total, LLD 0.3 pcl/t 09/26/95 DW Thorium 228, total 0.35 pCI/t 09/26/95 DW Thorius 228, total, error, +/-

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OUALITY CONTR0L REPORT 09/27/95 JOB ltseER:4 9519211

' CUBTOMER: F KERR McEE CORPORATION :

ATTN:. JEFF DETMEYER; I

ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SP!KES ANALYSl8 ANALYS!$

ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUB-TYPE 1.D.

VALUE (A)

VALUE (B)

(lA-Bl}

VALUE RECOVERY VALUE ADDED REC 0WERY CARAMETER Gross Alpha,:. total 9

?DATE/ TIME' ANALYZED:08/30/95314:05' OC BATCM NUMBER 17D093 REPORTING LIMIT /DF:'-

. UNITS:pci/L" L NETIND REFERENCE ^ : EPA 900.0 -

TECHNICIAN NRF i

l BLANK MB MB2AB0829 ND

STANDARD LCS LCIA0829 22.4 25.5 88 SPIKE MS 951963-1 124 10.0 128 89 DUPLICATE 4

951963-1 10.0 14.6 37 PARAMETER Gross Sete, totalc.

1 METHOD REFERENCEJ EPA 900.0

. TECHNICIAN:NRF DATE/ TIE ANALYZED:08/30/95' 14:14 GC BATCN NLSSER 170097 REPORTING LIMIT /DFs;

. UNITS:pCI/L.-

BLANK MB IW2AB0829 0.4 l STANDARD LCS LC100B29 23.9 22.0 109 SPIKE M5 951963 1 144 5.0 110 126 DUPLICATE MD 951963 1 5.0 8.8 55 PARAMETER Thori a 232,;totat

~DATE/ TIME ANALYZED:09/25/95 "16:49 GC BATCN IRAGER 171053 REPORTING LIMIT /DFs

! UNITS pct /t+

. METHOD REFERENCE :

TECHNICIAN:DW BLANK MB MB5T0906 0.47 BLANK MB MB6T0906 0.95 i

STANDARD LCS ST3T0906 7.59 7.0 108 STANDARD LCS LC3T0906 7.1 7.0 101 SPIKE MS 951921 1 16.3 0.92 14.0 110 i

DUPLICATE MD V51922-1 0.61 0.89 37 OARAMETER:Thori m 228,-total-DATE/ TIME ANALYZED:09/26/95 08:19 GC BATCH NUMBER 171058 REPORTING LIMIT /DFs UNITS:pCf/L METHOD REFERENCE :

TECHNICIAN:DW j

BLANK MB MB5T0906 0.18 BLANK MB MB6T0906 0.01 STANDARD LCS ST3T0906 7.0 7.0 100 STANDARD LCS LC3T0906 7.01 7.0 100 SPIKE MS 951921 1 18.0 0.35 14.0 126 DUPLICATE MD 951922 1 0.74 0.86 15 j

i PARAMETER:Urani m 234, total (ISO U)-

DATE/ TIME ANALYZED:09/26/95 10:46 OC BATCH WlMBER:171081 REPORTING LIMIT /DFs UNITS:pCI/l METH(2 REFERENCE CA GLR R405 TECHNICIAN:DW BLANK MB MB1UO906 0.2 BLANK MB MB2UO906 0.4 STANDARD LCS ST1UO906 7.8 7.8 100 STANDARD LCS LC1UO906 7.7 7.8 99 DUPLICATE e

952012 2 127 131 3

PARAMETER:Urani m 2354 total-(ISO U)

DATE/ TIME ANALYZED:09/26/95 11:13 QC BATCH NUMBER:171088 REPORTING LIMIT /DF ( '

UNITS:pci/t-METNCD REFERENCE' :CA-GLR R405 TECHICIAN:DW BLANK MB MB1UO906 0.0 420 West First Street Casper, WT 82601 (307) 235-5741 PAGE:3

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'EUSTOMER: ?KERR McGEE CORPORATION ATTN JEFF OSTMEYER -

l ANALYS18 DUPLICATES REFERENCE STANDARDS NATRIX SPIKES l

ANALYS!$

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VALUE (A)

VALUE (B)

(lA-Bl)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER Uranium 235,' total

. (ISO U)1 DATE/ TIME ANALYZED 09/26/95 11:13 GC BATCH NLsIBER:171088 REPORTING LIMIT /DFs

' UNITS:pcl/ls.

METHOD REFERENCE CA-GLR R405 TECHNICIANDW I

I BLANK ME Ms2OO906 0.0 l

DUPLICATE MD 952012-2 5.4 6.0 11 PARAMETER Uranism 238,'totali2(ISO U)'

DATE/ TIME ANALYZED 09/26/95 11:19 OC BATCH MlatBER:171092 REPORTING LIMIT /DFs-UNITS:pC1/L-METHOD REFERENCE 3CA* GLR R405 TECHNICIAN DW SLANK Ms Ms1UO906 0.1 SLANK Ms Ms2UD906 0.1 STANDARD LCS ST1UO906 7.4 7.2 103 STANDARD LCS LC1UO906 8.0 7.2 111 DUPLICATE MD 952012-2 57.4 57.4 0

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l 420 West First Street Casper, WY B2601 (307) 235-5741 PAGE:4

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g CORE LABORATORIES QUALITY CONTROL FOOTER METHOD REFERENCES (I) EPA 600/4 79420. Methods for Chenucal Analysis of Water and Wases. March 1983 (3) EPA SW.846. Test Methods for Evaluatmg Sohd Waste. Bird Edition. November 1990 and July 1992 update (3) Standard Methods far the Exanunaten of Water and Wastewater.17th 1989 (4) EPA 600/4 80 032. prosaihed Proondes for Measurement of P%vity ui Dnnking Water, August 1980 (9) federal Register. Friday. October 26.19R4 (40 CFR Part 136)

(6) EPA 600'R 78417. Mhrohologn:al Metleds for Marutonng the Environrnent. December 1978 COMMENTS (1) N data m the laboratory Test Results Report may difTer from the data in the QC Report due to calculauons for sample preparauon endor dilutsons.

(3) & " Time Analyzed

  • in the OC Report may not reflect the actual time of each analwis. & "Date Analyzed"is the actual date of analpis.

(3) Sod and sludge sampics are reported on a wet basis or on an "as received" basis unicas otherwise indicated.

(4) N data in this report m withm the limits of unecrtamey spectfud in the refenmmd method unicas otherwise indu:ated.

(9) Analyses performed by a subcontract laboratory are mdscated wnh an astensk and associased code in the "Tectuuctan* data field.

Subcontract Laboratories fadt Corelaboratones. Anaheun.CA

  • AN Core Laboratones. Aurora.CO
  • AU Core Laboratones. Casper, WY
  • CA Core Laboratones. Corpus Chnsti. TX
  • CC Core laborasones. Houston.1%
  • HP Core taboratonen. lake Charian. LA
  • If Core laboratones. tang Beach. CA
  • LB Other Subcontract 14huraterws
  • XX DEFINITIONS (1) WC = Not Calculable due to values lower than the reporting hmit.

(3) ND = Not Detected above the reporting linut.

OC SAMPLE IDENTIFICATIONS BLANKS SMK_EJ MD - Method Blank (also referred to as a preparauon blara)

MS - Matnx Spike RD = Reagent Diank MSD = Mainx Spas Duphcate IB = Instrument Blara PDS = Post Diseason Spike ICD - Imtial Calibration illank BS = Blank Spike (also refened to as a method spike)

CCD = Cuntmums Cahbratmn Blank SS = Sunogase Spas IIB = licidmg Diank (also rtfened to as a storage blank)

REFERENCE STANDARDS DUPLICATES CS - Cahbrauon Standard MSD = Matna Spike Duptu:ste RS = Reference Standard (also referred to as an external reference standard)

MD < Methud Duphs; ate ICV = InsualCahbrauon Venficanon CCV = Corsinums Cahbraaon Venficauon LCS = LaboratoryControlSample 420 West First Street Casper, WY 82601 0 07) 235 5741

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gh)y CORE LABORATORIES, INC.

5295 Holkster Road I

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Hous'.on. Texas 77040 I89'; I l

(713)460 9600 Sample Receipt Acknowledgment Date aa/25/95 R

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p (ERR Mc6tE CORPORAf!ON v 3ANE

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o Coro Laboratories Customer Estimated Job Number Project ID Completion Date 951911 ANNL%l (NVIRONr.Fl6 tat Cf1W 9.2 cg/21/95 Sample #

Customer ID Remarks 000I CU2-26-020 WATER RECEIVED SEP 0 51995 Safety e Environ Cushinc l

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If veu have anv cuestions please call (cre Lateratories, Casper. UV G71 IM-5741 l

THIS IS NOT AN INVOICE Order subject to our sales agreement, if any.

Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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SAnptE NUMBER:0001 DATE RECEIVED:C8/24/95 TIME RECEIVED:10:08 SAMPLE DATE:GB/23/95 SAMPLE TIME:.

DUE DATE:09/21/95 I

PROJECT 10:AMMUAL ENVIRONMEMTAL CMW 9.2 SAMPLE ID:CU2-26-020 REM: WATER LA8 MOTES:114L VATER SHORT 10:

BlN NUMBER:L l

CDDE TEST DESCR!pTION TEST LIMITS UNITS OF MEASURE TEST METHOD COMMEMIS RG00 DMAT CHECK FOR ISO U R313 Gross Alpha, total pCi/l EPA 900.0 R514 Gross Alpha, total, error, f/-

pC1/1 R515 Gross Alpha, total LLD pCi/l R516 Gross geta, total pCi/l epa 900.0 R517 Gross Beta, total, error, f/-

pCi/1 R$18 Gross geta, total, LLD pC1/1 R555 Thorius 232, total pCl/l R556 Thortus 232, total, error, f/-

pCi/l 1

R557 Thorium 232, total, LLD pC1/1 R561 Uranium 234, total (ISO 0) pC1/1 CA-6LR-R405 R362 Uranium 234, total, error, 4/-

P 1/1 C

R563 Uranius 234, total, LLD pCi/l R564 Uranius 235, total (ISO U) pCi/1 CA-6LR R405 R565 Uranive 235, total, error, f/-

pC1/1 R566 Uran 19e 235, total, LLD pCi/l R567 Uranium 238, total !!LO Un pct /l CA-6LR-R405 R568 Urantum 238, total, error, f/-

pC1/1 R569 Uranive 238, total, LLD pCi/l R$70 Thortus 228, total pC1/1 R571 Thortus 228, total, error, f/-

pCi/1 R572 Thortus 228, total, LLD pC1/1 1

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