ML20207D137

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Core Labs Analytical Rept for Job Number 940633
ML20207D137
Person / Time
Site: 07003073
Issue date: 05/10/1994
From: Mull R
CORE LABORATORIES, INC.
To:
Shared Package
ML20207B577 List:
References
NUDOCS 9903090239
Download: ML20207D137 (8)
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Text

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Wm WA. J WESTERN l

I ATLAS Core Laboratories l

i CORE LABORATORIES ANALYTICAL REPORT Job Number:

940633 Prepared For:

KERR-McGEE' CORPORATION JEFF OSTMEYER P.O. BOX 89 CUSHING, OK 74023 Date:

05/10/94 j

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i Name: Rondalynn Mull Core Laboratories, Inc.

420 West First Street Casper, WY 82601

Title:

Laboratory Supervisor 1

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LAB 0 RAT 0RY TE$TS RESULTS 05/10/94 JOB IRMBER:" 940633' CUSTOMER: KERR-McGEE CORPORATION ATTN JEFF OSTMEYER i

CLIENT

!.D........: BLOCK 75 E25.S 80 LABORATORY 1.D...: 940633 0001 DATE SAMPLED.......: 03/26/94 DATE RECEIVED....: 04/04/94 TIME SAMPLED.......: 10:30 TIME RECEIVED....: 10:00 WORK DESCRIPTION... CU1-65-005 REMAR:'S.......... t WATE R TEST DESCRIPTION FINAL RESULT DETECTION LIMIT UNITS OF MEASURE TEST METHOD-DATE

' TECHNICIAN Thiriun 230, total 0.5 pCi/l 05/02/94 JG Thiriun 230, total, error, +/-

0.3 pCi/l 05/02/94 JG Thiriun 230, total, LLD 0.4 pCi/l 05/02/94 JG Thiriun 232, total 0.2 pci/l 05/02/94 JG Th:riun 232, total, error, +/-

0.1 pCi/l 05/02/94 JG Thirium 232, total, LLD 0.2 pCf/l 05/02/94 JG Uranlun 234, total 7.9 pcl/l 04/29/94 PLJ Uranium 234, total, error, +/-

1.3 pCi/l 04/29/94 PLJ l

Uranlun 234, total, LLD 0.3 pCf/l 04/29/94 PLJ Urantun 235, total 0.1 pCi/l EPA 901.1 04/29/94 PLJ Uranlun 235, total, error, +/-

'O.1 pCl/l 04/29/94 PLJ Ur:niun 235, total, LLD 0.3 pCi/l 04/29/94 PLJ Urantun 238, total 3.7 pcl/l 04/29/94 PLJ Urtniun 238, total, error, +/-

0.8 pCi/l 04/29/94 PLJ Urtniun 238, total, LLD 0.2 04/29/94 FLJ Thoriun 228, total 0.5 pci/l 05/02/94 JG Thoriun 228, total, error, +/-

0.2 pCi/l 05/02/94 JG Thorium 228, total, LLD 0.4 pCi/l 05/02/94 JG l

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0UAL17Y C0NTR0L REPQRT 05/10/94 JOB NUMBER: 940633 CUSTOMER: KERR McGEE CORPORATION ATTN JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARJS MATRIX SPIKES ANALYS!$

ANALYSIS ANALYS!$

ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUB* TYPE I.D.

VALUE (A)

VALUE (B)

(lA-Bj)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Uranlun 234.' total '

DATE/ TIME ANALYZED:04/29/94 10:55 QC BATCH NUMBER:150616 REPORTING LIMIT /DFs UNITS:pti/t METHOD REFERENCE :

TECHNICIAN:PLJ l

BLANK MB MB11UO414 0.1 BLANK MB MB21UO414 ND l

STANDARD LCS LC11UO414 6.5 6.6 98 STANDARD LCS ST1!UO414 6.7 6.6 102 SP!KE MS 940631 1 11.3 2.4 8.2 109 DUPLICATE MD 940634 1 4.1 3.3 22 FARAMETER:Uranlun 235, total DATE/ TIME ANALYZED:04/29/94 11:18 QC BATCH NUMBER:150622 REPORTING LIMIT /DF:

UNITS:pCl/l METHOD REFERENCE : EPA 901.)

TECHNICIAN:PLJ BLANK MB MJ)1UO414 ND BLANK MB 9821b0414 ND

940634 1 DUPLICATE MD ND 0.1 0

PARAMETER Uranlun 238,' total DATE/ TIME ANALYZED:04/29/94 11:28 QC BATCH NUMBER 150625 REPORTING t!MIT/DFs UNITS:pCl/l-

~ METHOD REFERENCE :

TECHNICIAN:PLJ BLANK MB MB11U0414 ND BLANK MB MB21UO414 ND STANDARD LCS LC11UO414 7.3 6.9 106 STANDARD LCS ST11UO414 6.9 6.9 100 SP!KE MS 940631 1 10.8 1.3 8.6 11D DUPLICATE MD 940634 1 1.4 1.5 7

PARAMETER:Thoriun 228, total

.DATE/ TIME ANALYZED:05/02/94 15:03 QC BATCH NUMBER:150693 REPORTING LIMIT /DFs UNITS pci/l METHOD REFERENCE :

TECHNICIAN:JG CLANK MS MB3T0415 ND BLANK MB MB4T0415 0.1 STAkDARD LCS ST210415 4.7 4.0 118 i

STANDARD LCS LC270415 3.7 4.0 92 SPIKE MS 940637 1 4.9 0.3 4.0 115 DUPLICATE MD 940633 1 0.5 0.6 18 ME ':Thorlun 230, total DATE/ TIME ANALYZED:05/02/94 15:10 QC BATCH NUMBER:150697 REPORTI.

IMIT/DF:

UNITS:pC1/l METHOD REFERENCE :

TECHNICIAN JG BLANK MC310415 0.1 BLACK MB

,MB4T0415 ND STANDARD LCS 0415 2.0 1.7 118 STANDARD LCS LL '.

1.8 1.7 106 SPIKE MS 94063c.

2.3 0.2 1.7 124 DUPLICATE MD 940633-1 0.5 0.3 50 l

420 West First Street i

Casper, WY B2601 (307) 235 5741

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QUAL!TY C0NTR0L REP 0RT 05/10/94 JOS NUWAER: 940633 CUSTOMER: KERR-McGEE CORPORATION ATTN: JEFF OSTMEYER ANALYSIS DUPLICATES REFERENCE STANDARDS MATRIX SPIKES ANALYSIS ANALYSIS ANALYSIS ANALYZED DUPLICATE RPD or TRUE PERCENT ORIGINAL SPIKE PERCENT TYPE SUS TYPE I.D.

VALUE (A)

VALUE (B)

(lABj)

VALUE RECOVERY VALUE ADDED RECOVERY PARAMETER:Thoriun 232, total DATE/ TIME ANALYZED:05/02/94 -15:27

_ C BATCH NUMBER:150701 Q

REPORTING LIMIT /DF:

UNITS:pCl/l METHOD REFERENCE :

TECHNICIAN:JG BLANK M8 MB3T0415 ND BLANK MB MS4T0415 ND STANDARD LCS ST2T0415 4.5 4.0 112 STANDARD LCS LC210415 4.2 4.0 105 SPIKE MS 940637-1 4.4 ND 4.0 110 DUPLICATE MD 940633-1 0.2 0.2 0

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FME wasvaan ATLAS Core Laboratories QUALITY CONTROL FOOTER METHOD REFERENCES (1) EPA 600 4-79-020, Methods for Chemical Analyns of Water and Wastes. Marsh 1983 (3) EPA SW-846. Test Methods for Evaluaung Solid 4'aste, nird Edition, November 1990 and July 1992 update (3) Standard Methods for the Exanunauon of Water and Wastewater 17th,1989 (4) EPA 600 4-80-032, Picscnbod Procedures for Measurement of Radioacuvity in Dnnking Water, August 1980 (9) Federal Register. Fnday October 26.1984 (40 CFR Part i36)

(6) EPA 600'8-78417, Microbiological Methods for Morntonng the Emironment. December 1978 COMMENTS (1) ne data in the Laboratory Test Results Report may ddrer from the data m the QC Report due to calculations for sample preparauon and or diluuans.

(3) The " Time Analyzed" in the QC Report may not reflect the actual tune of each analysis. De "Date Analyzed" is the actual date of analysis.

(3) Sml and sludge samples are reported on a wet basis or on an "as received" basis unless otherwise indicated.

(4) ne data m tius report are wittun the lututs of uncertmuny specdied m the referenced method unless otherwise mdicated.

(5) Analyses performed by a subcontract laboratory are indicated with an astensk and associated code in the "Techrucian" data field

.Si&gontract Laboratories Code Core Laboratories. Anaheun.CA

  • AN Cars Laboratones. Aurora.CO

'AU Core Laboratones - Casper WY

  • CA Core Laborstones. Corpus Chnsti, TX
  • CC Core laboratones. Iloumon. TX
  • !!P Core Laboratones e Lake Charles. IA
  • If Core laboratones - Long Beach, CA
  • LB Other Subcontract laborniones
  • XX DEFINITIONS

'O KC = Not Cakslable due to salues louer than the reportmg linut.

(2) ND = Not Detected above the repertmg lumt.

OC S AMPII IDENTIFICATIONS DLMXS SPIKES MB = Method Blank (also refemd to as a preparatirn blank)

MS = Matrix Spike RB = Reagent Blank MSD = Mainx Spike Duphcate IB = Instrument Blank PDS = Post Digesuon Spike ICB = ImtsalCalibrauon BicA BS = Blank Spike (also referred to ar a method spike)

CCB = Contmums Cabbration Blank SS = Surrogata Spike HB = V dmg Blank (also referred to as as a storage blank)

REFERENCE STANDARDS DUPLICATES CS - Calibranon Standard MSD = Mainx Spike Duphcate RS = Reference Standard (also referred to as an external reference standard) i l

MD = Method Duphcate ICV = Innial Cahbrauon Verificanon I

CCV = Conunumg Cahbrauon Calibrauon 145 = LaboratoryControlSampic 420 West First Street Casper,WY 82601 f 307) 235-5741

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COR~'t LABORATORIES Western Atdem Irvtiernet:lottal ine

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Otherwise subject to our current terms of sale as shown on reverse side.

Please contact laboratory immediately, if any discrepancies are observed.

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L0G-!N J08 REP 0RT 04/08/94 J05 NUMBER:940633 CUSTOMER (KE0001) KERR-McGEE CORPORATION CONTACT JEFF OSTMEYER PHONES (

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SAMPLE NUMBER:0001 I

DATE RECE!VED 04/04/94 TIME RECE!VED:10:00 SAMPLE DATE 03/26/94 SAMPLE TIME:10:30 DUE DATE:05/02/94 PROJECT 10 BLOCK 75-E25-S-60 SAMPLE ID:CU1 65 005 REM: WATER LAB NOTES:1)4L CUSE SNORT 10:

BIN NUMBER:0 CODE TEST DESCRIPTION TEST LIMITS UNITS OF MEASURE TEST METHOD COMMENTS R552 Thorium 230, total pCl/t R553 Thorium 230, total, error, +/-

pCl/t R554 Thorium 230, total, LLD pCf/t R555 Thorium 232, total

'pCf/t R556 Thorium 232, total, error, +/-

pCf/t R557 inorium 232, total, LLD pCf/l RS61 Uranium 234, total pCl/t RS62 Uranium 234, total, error, +/-

pCI/t R563 Uranium 234, total, LLD pCf/t R564 Uranlun 235, total pcl/l EPA 901.1 R565 Uranium 235, total, error, +/-

pCf/t R566 Uranium 235, total, LLD pCi/l RS67 Uranium 238, total pCf/t R568 Uranium 238, total, error, +/-

pCf/t R569 Uranium 238, total, LLD pct /t R570 Thorium 228, total

. pCl/t

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R571 Thorium 228, totat, error, +/-

pCI/l 4

R572 Thorium 228, total, LLD pCi/l j

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SHIP TO:

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST l

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ANALYSIS REQUEST COMPANY ADDRESS:

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KERR MCGEE CORPORATION PHONE: 1918-225-7753 m

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Note: Do not comeme Specia Dooesesion This sample meets ad N

Bill & Report to:

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Note: Time of analysis & tech's these results with Limits:

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Jeff Ostmeyer

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