Text

Restoration Project - Final Status Survey Release Record, Area Far South of Switchyard Survey Unit 10219A - Final Report - Phase 1, Revision 1
	ML19178A100
Person / Time
Site:	Zion File:ZionSolutions icon.png
Issue date:	06/20/2019
From:	Yetter R; ZionSolutions
To:	; Office of Nuclear Material Safety and Safeguards
Shared Package
MML19178A106	List: ML19178A098; ML19178A100; ML19178A101; ML19178A102; ML19178A103; ML19178A104; ML19178A105; ML19178A107; ML19178A108; ZS-2019-0043, Transmittal of Revised Final Status Survey Report - Phase 1;
References
	ZS-2019-0043
	Download: ML19178A100 (255)
	v • d • e

=ZION SOLUTIONS LLC-An EnergySo/utions Company

=11+++ ()=1 1 3.630 ()+ 0.002 3.095 ()=3.622 / ()=1 1 1.091 ()+180.45914.458 ()=0.898 /

()=1 0.012 0.898 ()+0.00001 1.733+ 0.988 3.622 ()=3.494 /

10/4/21, . -1 :05:36PM ~~~pex-Gamma Analysis Report for 04-0ct-16-10008 L3-10219A-FRGS-001 SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 04-0ct-16-10008

L3-10219A-FRGS-001SS

1 L 130G Soil Sample 1.303E+03 grams : Default : 9/27/2016 1:30:00PM

10/4/2016 12:41:54PM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.17 % : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16021 PEAK WITH NID REPORT Peak Analysis Performed on 10/4/2016 12:47:00PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of7 10/4/201'.

1:05:36PM Page 2 of7 Analysis Report for 04-0ct-16-10008 L3-10219A-FRGS-001 SS Peak Energy ROI No. (keV) start 1 2 38.57 949 -2 351.84 1403 -3 582.78 2326 -4 1460.52 5835 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 962 1415 2336 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.78 4.87E+Ol 18.84 2.85E+Ol 1407.55 4.84E+O l 14.77 5.20E+OO 2330.90 l.98E+Ol 1 0.30 6.38E+OO 5843.04 6.49E+Ol 1 6.41 2.25E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 0.99 1460.82 Tl-208 0.99 583.19 Bi-211 0. 96 351.07 Pb-212 1. 00 115 .18 2 38.63 300.09 Pb-214 0.51 2 41.99 2 95.22 351.93 785. 96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 10.66 85.00 13.02 0.60 43.60 3.30 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. Activity (pCilgrams)

o. llE+OO 1.38E-01 1.40E+OO 3.30E-01 5.13E-0 1 Activity Uncertainty 1.63E+OO 7.37E-02 4.84E-01 l.38E-01 l.77E-01 Tentative Nuclide Pb-212 Pb-214 Bi-211 Tl-208 K-40 Coinc Corr miss 0.932 miss free free 10/4/201', 1 :05:36PM Analysis Report for 04-0ct-16-10008 L3-10219A-FRGS-OO 1 SS INTERFERENCE CORRECTED REPORT ? ? Nuclide Name K-40 Tl-208 Bi-211 Pb-21 2 Pb-214 Nuclide Id Confidence 0.994 0.990 0. 964 1.000 0. 513 ? = nuclid e is part of an undetermined solution X = nuclid e rejected by the interference analysis Wt mean Activity (pCilgrams) 6.llE+OO l.38E-01 l.40E+OO 3.30E-01 5 .13E-Ol @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma wt mean Activity Uncertainty l.63E+OO 7.37E-0 2 4.84E-01 l.38E-Ol l.77E-01 Page 3 of7 Comments 10/4/20h.

1 :05:36PM Page 4 of7 Analysis Report for 04-0ct-16-10008

+ + + + + + + + + L3-10219A-FRGS-001 SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/4/2016 12:47:00PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LJB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

Corr K-40 1460.82

10.66 6.llE+OO 7.38E-01 7.38E-01 miss Cr-5 1 320.08 9.9 1 -2.99E-01 3.14E-01 3.14E-01 free Mn-54 834.85 99.98 8 .11E-03 7.49E-02 7.49E-02 miss Co-58 810.76 99.45 2.41E-03 8.68E-02 8.68E-02 1.000 1674.73 0.52 O.OOE+OO 6.lOE+OO 1. 0 2 4 Co-60 1173.23 99.85 1. 27E-0 2 7.30E-02 1. lOE-01 0.947 13 32.49 99.98 9.92E-03 7.30E-0 2 0.947 Nb-94 702.65 99.81 1. 38E-02 8.04E-02 8.49E-02 0.944 871.09 99.89 4.98E-03 8.04E-02 0.944 Ag-108m 79.13 6.60 6.71E-02 5.07E-0 2 2.41E+OO miss 433.94 90.50 -5.46E-04 5.07E-02 0.887 614.28 89.80 9.80E-03 7.53E-02 0.886 7 22.94 90.80 9.0lE-03 1.0lE-01 0.887 Sn-113 2 55.1 3 2.11 2.51E-Ol 8.59E-02 2.65E+OO free 391.70 64.97 4. 72E-03 8.59E-02 free Cs-134 475.36 1. 48 -1.59E-01 2.26E-02 3.82E+OO miss 5 63. 2 5 8.34 4.2 4E-02 9.27E-01 0. 896 569.33 15.37 7.02E-02 4.20E-01 0.888 604. 72 97.62 -l.22E-03 5.67E-02 0.931 10/4/201v 1:05:36PM P age 5 of7 Analysis Report for 04-0ct-16-10008 L3-10219A-FRGS-001SS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Cain e Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Corr Cs-134 7 95.86 85.46 O.OOE+OO 2.26 E-02 2.26E-02 0.933 801.95 8.69 1. 72E-01 7.98E-01 0.898 1038.61 0.99 2.78E+OO 1.03E+Ol 0.943 1167.97 1. 79 -1.59E-01 4.14E+OO 1. 081 1365.19 3.0 2 5.64E-01 2.62E+OO 1.1 2 8 + Cs-137 661.66 85.10 9.07E-02 1. 43E-0 1 1.43E-01 miss + Eu-152 121.78 2 8.67 2.52E-02 l.58E-Ol 2.33E-01 0.936 244.70 7.61 -8.79E-03 7.94E-01 0.935 295.94 0.45 1.89E+OO 1. 61E+Ol miss 344.2 8 26.60 -8.78E-0 2 1.58E-01 0.957 367.79 0.86 -1.43E-01 6.71E+OO 0.884 411.1 2 2.24 -1.2 3E+OO l.93E+OO 0.908 443.96 2.83 O.OOE+OO 1.81E+00 0.934 488.68 0.42 5.29E-01 1.22E+Ol miss 563.99 0.49 -1.32E+OO 1.38E+Ol 0.934 586.26 0.46 1.74E+OO 1.16E+Ol 0.94 2 678. 62 0.47 -3.80E+OO 1.05E+Ol 0.887 688.67 0.86 -3.58E-01 5.26E+OO 0.980 719.35 0.28 -4.63E+OO 2.67E+Ol miss 778.90 12. 96 O.OOE+OO 3.93E-01 0.945 810.45 0.32 -5.65E+OO 1.85E+Ol 1. 050 867.3 7 4.26 O.OOE+OO 4.81E-01 0.928 919.33 0.43 1.75E+OO 1.62E+Ol 0.981 964. 08 14.65 2.57E-01 7.12E-01 1. 022 1085.87 10.2 4 3.03E-01 1.03E+OO 1.018 1089.74 1. 73 5.46E-01 5.3 7 E+0 0 0.952 111 2. 07 13.69 1.31E-01 8.03E-01 0.992 1212.95 1. 43 -4.75E-01 7.16E+OO 0.929 1249.94 0.19 -1.08E+Ol 4.02E+Ol 1. 097 1299.14 1. 63 -4.2 9E-01 6.47E+OO 0.944 1408.01 2 1.07 4. 72E-0 2 4.38E-01 0.98 3 1457.64 0.50 -2.39E+Ol 2.79E+Ol 1.076 1528.10 0.2 8 -1.05E+OO 2.70E+Ol 1. 007 + Eu-154 123.07 40.40 -2. 72E-02 1.50E-0 1 l.50E-01 0.934 247.93 6.89 8.68E-02 8.92E-01 0.92 8 591.76 4.95 O.OOE+OO 3.2 5E-0 1 0.915 692.4 2 1. 78 3.03E-01 3.38E+OO 0.936 723. 3 0 20.0 6 4.70E-0 2 3.99E-01 0.935 756.80 4.5 2 3.02E-01 1.67E+OO 0.915 873.18 12.08 1.83E-01 7.54E-01 0.93 2 996. 29 10.48 -1.27E-02 7.06E-01 0.971 1004.76 18.01 O.OOE+OO 3.25E-01 0.978 1274.43 34.80 1.90E-02 1. 96E-0 1 0.981 1596.48 1. 80 O.OOE+OO 1.38E+OO 1.175 + Eu-155 45.30 1. 31 1. 95E+01 3.1 9E-01 5 .13E+Ol 0.99 9 60.01 1. 22 -6.66E-01 3.87E+Ol 1. 000 86.55 30.70 1.66E-02 3.69E-01 free 105.31 2 1.10 -9.59E-03 3.19E-01 1. 000 + Tl-208 583.19

85.00 1.38E-01 7.60E-02 7.60E-02 0.932 + Bi-211 351.07

13.02 1.40E+OO 3.14E-01 3.14E-01 mi ss + Pb-211 404.85 3.78 -5.85E-01 l.03E+OO 1.03E+OO miss 10/4/201, 1:05: 36PM Page 6 of7 Analysis Report for 04-0ct-16-10008 L3-10219A-FRGS-001 SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCl/grams) (pCi/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 -9.84E-0 2 1.03E+OO 2.2 9E+OO miss 832.01 3.52 -2.91E-01 1.80E+OO miss + Bi-212 39.86 1. 06 -5.83E+OO 1.34E+OO 3.80E+Ol 0.998 727.33 6.67 4.90E-01 1.34E+OO 0.982 785.37 1.10 1. llE+OO 9.49E+OO 0.944 1 620.50 1. 47 O.OOE+OO 1.99E+OO 1.006 + Pb-212 115 .18 0.60 O.OOE+OO 1.59 E-01 1.08E+01 miss 23 8.63 43.60 3.30E-01 1.59E-01 free 300.09 3.30 -3.03E-01 1.55E+OO free + Pb212-XR 74.8 2 10.28 8.46E-01 1.17E+OO 2.00E+OO miss 77 .11 17.10 5.90E-01 1.17E+OO miss 87.35 3.97 1. 73E+OO 3.02E+OO miss 89.78 1. 46 3. llE-01 6.38E+OO miss + Bi-211 609.32 45.49 3.98E-01 3.68E-0 1 3.68E-01 0.948 768.36 4.89 3.75E-01 1.69E+OO 0.94 2 806.18 1. 2 6 1.86E+OO 6.89E+OO 0.92 3 934.0 6 3.11 -3.36E-0 1 3.03E+OO 0.944 1120.2 9 14. 9 2 4.2 3E-01 9.88E-01 0.944 1155.2 1 1. 63 O.OOE+OO 1. 50E+OO 0.943 1238.12 5.83 -3.30E-01 1.94E+OO 0.944 128 0.98 1. 43 O.OOE+OO 1.82E+OO 0.944 1377. 67 3.99 6.68E-02 1. 72E+OO 1. 030 1385. 31 0.79 7.36E-01 9.48E+OO 0.945 1401.52 1. 33 3.32E-01 5.70E+00 0.945 1 407.99 2.39 4.32E-0 1 4.0lE+OO 0.945 1 509.2 1 2 .13 2.55E+OO 6.67E+OO 0.950 1 661.27 1. 05 2.65E-01 7.79E+OO 1. 001 1729.59 2.88 1.07E+OO 3.83E+OO 1.119 1 764.49 15.30 3.04E-01 9.12E-01 1. 001 1 847.43 2.03 5.56E-01 4.09E+00 1.06 3 > 2118. 51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 2 41.99 7.25 -2.57E-03 1.15E-01 7.73E-01 1. 000 2 95.22 18.42 3.18E-01 4.41E-01 1. 000 351.93

35.60 5.13E-01 1.15E-01 free 785.96 1. 06 1.61E+OO 9.32E+OO 1. 000 + Pb214-XR 74.82 5.80 1.50E+OO 2.07E+OO 3.55E+OO mis s 77 .11 9.70 l.04E+OO 2.07E+OO mis s 87.35 2.24 3.06E+OO 5.35E+OO miss 89.7 8 0.82 5.54E-01 l.14E+Ol miss + Ra-2 2 6 1 86.2 1 3.64 4.90E-01 l.81E+OO 1.81E+OO free + Ac-2 2 8 129.0 7 2.42 7.15E-01 4.48E-01 2.86E+OO 0.944 209.25 3.89 4.lOE-01 1. 51E+00 0.978 270.24 3.46 5.22E-01 1.88E+OO 0.955 328.00 2.95 5.29E-01 2.33E+OO 0.955 338.32 11. 27 3.30E-02 5.74E-01 0.992 4 0 9.46 1. 92 7.09E-01 3.51E+OO 0.937 463.00 4.40 2.58E-01 1.68E+OO 0.933 794.95 4.2 5 O.OOE+OO 4.48E-01 0.942 911.2 0 25.80 2.02E-01 4.52E-01 0.990 964.77 4.99 6.44E-01 2.1 8E+OO 0.981 968.97 15.80 3.68E-01 7.69E-01 0.990 10/4/20 , _ 1:05:36PM Page 7 of7 Analysis Report for 04-0ct-16-10008 L3-10219A-FRGS-001 SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCl/grams)

Corr Ac-2 2 8 1588.20 3.22 O.OOE+OO 4.48E-01 8.99E-01 1. 00 2 + Pa-231 27.36 10.3 0 -6.0lE-01 2.08E+OO 5.22E+OO 0.998 283.69 1. 70 4.48E-01 3.07E+OO 1. 000 300.0 7 2.47 -4.05E-01 2.08E+OO 1. 000 302.65 2.20 5.2 5 E-01 2.83E+OO 1. 000 330.0 6 1. 40 5.48E-01 3.89E+OO 1. 000 + Th-234 92. 38 2.13 -2. 91E-0 2 6.30E+OO 6.30E+OO free 92.80 2.10 2. 96E+OO 6.73E+OO free 112. 81 0.2 1 1.03E+Ol 4.2 1E+Ol free + U-235 143.76 10. 96 -3.0BE-0 3 1.2 1E-01 4.95E-01 free 163.33 5.08 -1.70E-0 1 8.22E-01 free 185.71 57.20 4.71E-02 1.21E-01 free 202 .11 1. 08 3.16E-01 4.21E+OO miss 205.31 5.01 8.83E-02 1.lOE+OO free + Am-241 59.54 35.90 4.21E-01 1.54E+OO 1. 54E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed. free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

VI ...... C: :::s 60-55 50 45 40 35 8 30 25 1000 2000 3000 0000016021.

CNF 4000 channel 5000 Live Time :300.000 sec Real Time :300.500 sec start: 1: -0.l(kev) stop : 8192: 2047 .O(kev) Acq. start :Tue oct 04 12:41:54 2016 6000 7000 8000 10/4/~.., .J 1 :45:01 PM ~pex-Gamma Analysis Report for 04-0ct-16-10009 L3-10219A-FRGS-002SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real lime Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 04-0ct-16-10009

L3-10219A-FRGS-002SS

1 L 130G Soil Sample 1.686E+03 grams : Default : 9/27/2016 1:35:00PM

10/4/2016 1:21:42PM

130G 1 L Soil Sample : HTomlin : P40818B : 130G S oil : 300.0 seconds : 300.5 seconds : 0.17 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16023 PEAK WITH NID REPORT Peak Analysis Performed on 10/4/2016 1 : 26: 44PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of7 10/4/2(J IV* 1:45:01PM Page 2 of7 Analysis Report for 04-0ct-16-10009 L3-10219A-FRGS-002SS Peak Energy ROI No. (keV) start 1 185.8 3 740 -2 238.28 949 -3 609.2 8 2432 -4 1460.49 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigrna ROI end 747 958 2442 5850 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 743.98 l.OlE+Ol 11. 68 2.39E+Ol 953.62 2.06E+Ol 16.87 4.2 8E+Ol 2 436.85 1.94E+Ol 11. 89 1.51E+Ol 5842.94 6.98E+Ol 17.02 2.38E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

10.66 5.08E+OO 1.32E+OO Pb-212 0.99 115 .18 0.60 23 8.63 -,': 43.60 1.08E-01 8.99E-0 2 30 0.0 9 3.30 Bi-21 4 0.82 609.32

45.49 1.97E-01 1.2 3E-01 768.36 4.89 806.18 1.2 6 934.06 3.11 1120.29 14.92 1155.21 1. 63 1238.12 5.33 1280.98 1. 43 1377.67 3.99 1385. 3 1 0.79 1 401.52 1. 33 1407.99 2.39 1509.21 2.1 3 1661.27 1. 05 1729.59 2.88 1764.49 15.30 1847.4 3 2.03 2118.5 1 1.16 Ra-22 6 0.99 1 86.21

3.64 5.62E-01 6.58E-01 Tentative Nuclide ~5 Ra-226 Pb-212 Bi-214 K-40 /t1'.?" Coinc Corr miss free 0.948 free Analysis Report for 04-0ct-16-10009 L3-10219A-FRGS-002SS Nuclide Id Energy Name Confidence (keV) U-235 0.99 143.76 163.33 185. 71 2 02.11 205.31 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required. Yield(%) 10.96 5.08 57.20 1. 08 5.01 miss = Nuclide energy was not found in the coincidence library. 10/4/2v, -1 :45:01 PM Page 3 of7 Activity Activity Coinc (pC/lgrams)

Uncertainty Corr 3.57E-02 4.1 9E-02 free INTERFERENCE CORRECTED REPORT ? ? Nuclide Name K-40 Pb-21 2 Bi-214 Ra-226 u-~ fl, 1,~1,)-t, Nuclide Id Confidence 0.993 0.993 0.825 0.991 0~9 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCl/grams) 5.08E+O O 1.08E-0 1 1.97E-0 1 5.62E-0 1 3.~02 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 1.32E+OO 8.99E-02 1. 2 3E-01 6.58E-01 4.1~2 10/4/20 , v 1 :45:01 PM Page 4 of7 Analysis Report for 04-0ct-16-10009

+ + + + + + + + + L3-10219A-FRGS-002SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/4/2016 1:26:44PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\

R oot\Default\Library

\Z ION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Coinc Mame (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr K-40 1460.82

10.6 6 5.08E+OO 5.86E-01 5.86E-01 miss Cr-51 320.08 9.91 4.95E-02 4.66E-01 4.66E-01 free Mn-54 834.85 99.98 1.19E-02 5.79E-02 5.79E-02 miss Co-58 810.76 99.45 -1.68E-02 6.02E-02 6.02E-02 1.000 1674.73 0.52 1.74E+OO 1.2 8E+Ol 1. 024 Co-60 1173.23 99.85 O.OOE+OO 1. 91E-02 1.91E-02 0.947 1 332.49 99.98 1. 09E-03 7.12E-02 0.947 Nb-94 702.65 99.81 1.67E-03 5.36E-02 5.39E-02 0.944 871.09 99.89 6.73E-03 5.36E-02 0.944 Ag-108m 79.13 6.60 5.09E-01 4.3 9E-02 1.86E+OO miss 433.94 90.50 -7.87E-03 4.54E-02 0.887 614.28 89.80 1.70E-0 2 6.5 0E-02 0.886 722.94 90.80 3.98E-0 3 4.39E-02 0.887 Sn-113 255 .13 2.11 -1. 4 7E-02 6.08E-02 2.05E+OO free 391. 70 64.9 7 2.02E-03 6.08E-02 free C s-13 4 475.36 1. 48 -6.39E-01 3.47E-02 2.28E+OO miss 563.25 8.34 -6.56E-02 5.07E-01 0. 896 569.33 15.37 3.0lE-03 3.62E-01 0.888 604. 72 97.62 -5*. 66E-0 3 3.47E-02 0.931 10/4/2(., Ov 1:45:01PM Page 5 of7 Analysis Report for 04-0ct-16-10009 L3-10219A-FRGS-002SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCUgrams) (pCi/grams) (pC//grams)

Corr Cs-134 7 95. 8 6 85.46 6.47E-03 3.47E-02 4.76E-02 0. 93.3 801.95 8.69 8.58E-02 7.98E-01 0.898 1038.61 0.99 O.OOE+OO 1.79E+OO 0.94 3 1167.97 1. 79 1. 3 8E+OO 4.14E+OO 1. 081 1365 .19 3.0 2 O.OOE+OO 5.90E-01 1.12 8 + Cs-137 661.66 85.10 2.22E-0 2 8.45E-02 8.45E-0 2 miss + Eu-15 2 121.78 28.67 6.51E-02 1.28E-01 1.94E-01 0.936 244.70 7.61 2.2 6E-02 5.43E-01 0.935 295.94 0.45 8.89E+OO 1.25E+Ol miss 344.2 8 2 6.60 -3.03E-02 1.48E-01 0.957 367.79 0.86 -1.58E-02 5.19E+OO 0.884 411.12 2.24 -1. 21E-01 1.93E+OO 0.908 443. '.:l6 2.8 3 -5.21E-02 l.40E+OO 0.934 488.68 0.4 2 -5.26E-0 1 6.45E+OO miss 563.99 0.49 -1.15E+OO 8.22E+OO 0.934 586.2 6 0.46 -1.54E+OO 8.94E+OO 0.94 2 678.62 0.47 -7.3 4E-01 1.19E+Ol 0.887 688.67 0.86 O.OOE+OO 1.50E+OO 0.980 719.35 0.2 8 1. 72E+OO 1.26E+Ol miss 778. 90 12. 96 -2.75E-02 3.04E-01 0.945 810.45 0.3 2 -l.46E+00 1.66E+O l 1.050 867.3 7 4.26 O.OOE+OO 1.2 8E+OO 0.928 919.33 0.43 5.80E+OO 1.77E+01 0.981 964.08 14.65 8.46E-02 4.69E-01 1. 0 22 1085.87 10.24 -1.86E-01 5.64E-01 1. 018 1089.74 1. 73 -1.16E+OO 3.58E+OO 0.952 1112. 07 13.69 O.OOE+OO 1.28E-01 0.992 1212.95 1. 43 7.34E-02 3.78E+OO 0. 929 1249.94 0.19 2.39E+OO 2.46E+Ol 1. 097 1299.14 1. 63 4.65E-01 4.31E+OO 0.944 1408.01 21.07 1.09E-01 3.93E-01 0.983 1457.64 0.50 O.OOE+OO 2.2 7E+Ol 1. 076 1528.1 0 0.28 O.OOE+OO 7.67E+OO 1. 007 + Eu-154 123.07 40.40 -5.34E-02 1. 08E-01 1.08E-01 0.934 247.93 6.89 -1.60E-02 5.81E-01 0.928 591.76 4.95 2.78E-01 9.98E-01 0.915 692.4 2 1. 78 6.87E-01 3.02E+OO 0.93 6 7 23. 3 0 20.06 -8.55E-03 1.89E-01 0.93 5 756.80 4.52 -4.60E-01 8.82E-01 0.91 5 873.18 1 2.08 -1.13E-01 3.57E-01 0.93 2 996.29 10.48 O.OOE+OO 1.59E-01 0.971 1004.76 18.01 6.45E-02 3.68E-01 0.978 1274.43 3 4.80 4.61E-02 2.22E-01 0.981 1596.48 1. 80 O.OOE+OO l.07E+OO 1.175 + Eu-155 45.3 0 1. 31 -4.22E-01 3.00E-0 1 2.68E+Ol 0.999 60.01 1. 22 5. 72E+OO 3.55E+O l 1. 000 86.55 30.70 1.30E-01 3.00E-01 free 105.31 2 1.10 7.97E-0 2 3.19E-01 1.000 + Tl-208 583.19 85.00 7.19E-02 1.09E-01 1.09E-01 0.93 2 + Bi-211 351.07 13.02 2.74E-01 5.92E-01 5.92E-01 miss + Pb-211 404.85 3.78 6.83E-02 1. 03E+OO 1.03E+00 miss 10/4/2l, .~ 1:45:01PM Page 6 of7 Analysis Report for 04-0ct-16-10009 L3-10219A-FRGS-002SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCi/grams) (pCl/grams)

Corr Pb-211 427.09 1. 76 8.65E-01 1.03E+OO 3.02E+OO miss 832.01 3.5 2 -8.33E-03 1.61E+OO miss + Bi-21 2 39.86 1. 06 -1.39E+OO l.17E+OO 3.47E+Ol 0.998 727. 33 6.67 4.54E-01 1.17E+OO 0.98 2 785.37 1.10 -1.87E+00 4.53E+OO 0.944 1620.50 1. 47 O.OOE+OO 1.54E+OO 1. 006 + P b-212 115 .18 0.60 -6.70E-01 l.36E-01 7.53E+OO miss 238.63

43.60 1.08E-0 1 1.36E-01 free 300.09 3.30 4.00E-03 1.05E+OO free + Pb212-XR 74.8 2 10.28 5.81E-01 8.65 E-01 1.63E+OO miss 77 .11 17.10 2.33E-01 8.65E-01 miss 87.35 3.97 4.30E-01 2. llE+OO miss 89.78 1. 46 1.69E+OO 5.54E+OO miss + Bi-2 1 4 609.32

45.49 1.97E-01 1.57E-01 l.57E-01 0.948 768.36 4.89 2.35E-01 1. 30E+OO 0.942 806.18 1. 2 6 5.17E-01 4.77E+OO 0.92 3 934.06 3 .11 5.36E-01 2.75E+OO 0.944 1120.2 9 14.9 2 1.75E-01 6.00E-01 0.944 1155.2 1 1. 63 -3.05E-01 3.15E+OO 0.94 3 1238.12 5.83 -4.83E-0 1 9.2 1E-01 0.944 1280.98 1. 43 7.44E-02 4.83E+00 0.944 1377.67 3.99 -3.lOE-01

1. 33E+OO 1. 030 1385.31 0.79 -4.2 7E-01 7.32E+00 0.945 1401.52 1. 33 l.80E+OO 6.44E+00 0.945 1407.99 2.39 1.00E+OO 3.59E+OO 0.945 1509.2 1 2 .13 3.93E-01 2.90E+OO 0.950 1661.2 7 1. 05 8.19E-01 6.02E+OO 1.001 1 72 9.59 2.88 O.OOE+OO 7.43E-01 1.119 1764.49 15.30 O.OOE+OO 1.59E-01 1. 001 1847.43 2.03 O.OOE+OO l.16E+OO 1. 063 > 2 118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + P b-2 14 241.99 7.2 5 2.19E-01 2.45E-01 7.79E-01 1. 000 295.22 18.42 9.42E-02 2.94E-01 1.000 351. 93 35.60 2.40E-01 2.45E-01 free 785. 96 1. 06 -6.39E-01 5.16E+OO 1. 000 + Pb214-XR 74.82 5.80 1. 03E+OO l.53E+OO 2.89E+OO miss 77.11 9.70 4.lOE-01 1.53E+OO miss 87.35 2.24 7.62E-01 3.75E+OO miss 89.78 0.82 3.02E+OO 9.87E+OO miss + Ra-226 186.21

3.64 5.62E-01 1.05E+OO 1. 05E+00 free + Ac-228 129.07 2.42 -6.00E-02 3.lOE-01 2.05E+OO 0.944 2 09.25 3.89 2.78E-01 1.06E+OO 0.978 2 70.24 3.46 1.63E-02 1.19E+OO 0.955 328.00 2.95 -4.29E-02 1.40E+OO 0.955 338.32 11. 27 2.34E-01 4.62E-01 0.99 2 409.46 1. 92 -2.41E-0 2 1.95E+00 0.937 463.00 4.40 1.1 7E-01 l.13E+OO 0.933 794.95 4.2 5 1.49E-01 l.19E+OO 0.942 911.20 2 5.80 8.93E-02 3.lOE-01 0.990 964.77 4.99 -7.96E-02 l.2 9E+OO 0.981 968.97 15.80 8.74E-02 5.2 8E-01 0.990 10/4/2(,. _ 1:45:01PM Page 7 of7 Analysis Report for 04-0ct-16-10009 L3-10219A-FRGS-002SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pC//grams)

Corr A.c-22 8 1588.2 0 3.22 O.OOE+OO 3.lOE-01 6.95E-01 1. 002 + Pa-23 1 27.36 10.30 -2.29E-01 1.40E+OO 3.73E+OO 0.998 2 83.69 1. 70 -8.24E-0 2 1.96E+OO 1. 000 300.07 2.47 5.3 4E-03 l.40E+OO 1.000 302.65 2.2 0 3.77E-02 1.91E+OO 1. 000 330.06 1. 40 2.86E-01 3. OlE+OO 1. 000 + Th-234 92.38 2.13 -~.16E+OO 3.68E+OO 3.68E+OO fre e 92.80 2.10 -1.48E+00 4.llE+OO fre e 112.81 0.21 -6.87E+00 2.90E+O l fre e + U-235 143.76 10. 96 -4.2 0E-0 3 6.69E-0 2 4.16E-01 free 163.33 5.08 2.40E-01 9.20E-01 free 185. 71

57.2 0 3.57E-02 6.69E-02 free 2 02 .11 1. 08 9.16E-01 4.17E+OO miss 2 05.31 5.01 -1.86E-01 7.07E-01 free + Am-241 59.54 35.90 O.OOE+OO 1.2 3E+OO l.23E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 1000 2000 3000 0000016023.CNF 4000 channel 5000 Live Time 300.000 sec Real Time 300.520 sec start: 1 -0.l(kev)

Stop : 8192 2047. O(kev) Acq. start Tue Oct 04 13: 21: 42 2016 6000 7000 8000 10/4/_ J 3:08:30PM

.~§~p ex-Gamma

Analysis Report for 04-0ct-16-10010 L3-10219A-FRGS-003SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Un i t Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 04-0ct-16-10010

L3-10219A-FRGS-003SS

1 L 130G Soil Sample 1.207E+03 grams : Default : 9/27/2016 1:50:00PM

10/4/2016 2:45:09PM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.4 seconds : 0.15 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16024 PEAK WITH NID REPORT Peak Analysis Performed on 10/4/2016 2:50:11PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 10/4/2(. 3:08: 30PM Page 2 of8 Analysis Report for 04-0ct-16-10010 L3-10219A-FRGS-003SS Peak Energy ROI No. (keV) start 1 77.00 304 -2 238.58 950 -3 351.89 1 400 -4 609.02 2430 -5 1460.48 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 313 959 1415 2441 5854 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 309.07 1.87E+Ol 1 8.12 4.66E+Ol 954.83 5.25E+Ol 17. 96 2.50E+Ol 1407.75 6.63E+Ol 1 6.86 3.45E+OO 2435.84 3.67E+Ol 12.60 2.55E+OO 5842.87 l .11E+02 21.34 2.67E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

10.66 l.13E+Ol 2.38E+OO Bi-211 0.95 351.07

13. 02 2.08E+OO 6.25E-01 Pb-212 1. 00 115.18 0.60 238.63

43.60 3.84E-0 1 1.45E-01 300.09 3.30 Pb212-XR 1. 00 74.82 10.28 77 .11

17.10 1. OlE+OO 1.00E+OO 87.35 3.97 89.78 1. 46 Bi-214 0.99 609.32

45.49 5.2 0E-01 1.89E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 11 2 0.2 9 1 4.92 1155. 2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 140 1.52 1. 33 1407.99 2.39 Tentative Nuclide Pb214-XR Pb212-XR Pb-212 Pb-214 Bi-211 Bi-214 K-40 Coinc Corr miss miss free miss 0.948 Analysis Report for 04-0ct-16-10010 L3-10219A-FRGS-003SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1509.21 1661.27 1729.59 1764.49 1847.43 2 118.51 Pb-214 0.51 2 41.99 2 95.22 351.93 785. 96 Pb2 1 4-XR 1. 00 74.82 77 .11 87.35 89.78 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2.1 3 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 5.80 9.70 2.24 0.82 miss = Nuciide energy was not found in ihe coincidence library. 10/4/20. 3:08:30PM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 7.59E-01 2.28E-01 free 1.79E+OO 1. 78E+OO miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pC/lgrams)

Uncertainty K-40 0.993 1.13E+Ol 2.38E+OO ? Bi-211 0.959 2.08E+OO 6.25E-01 Pb-212 1. 000 3.84E-01 1. 45E-01 ? Pb212-XR 1. 000 1.0lE+OO 1. OOE+OO Bi-214 0.998 5.20E-0 1 1.89E-0 1 ? Pb-214 0.5 1 3 7.59E-0 1 2.28E-01 ? Pb214-XR 1. 000 l.79E+O O 1.78E+OO Analysis Report for 04-0ct-16-10010 L3-10219A-FRGS-003SS

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/4/20 .. 3:08:30PM Page 4 of8 10/4/20 , . 3:08: 30PM Page 5 of8 Analysis Report for 04-0ct-16-10010

+ + + + + + + + + L3-10219A-FRGS-003SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/4/2016 2: 50:11PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuc li de Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCilgrams) (pCl!grams)

Corr K-40 1 460.82

1 0.66 1.13E+Ol 8.68E-0 1 8.68E-01 miss Cr-5 1 320.08 9.9 1 -7.70E-02 6.51E-01 6.51E-01 free Mn-54 834.85 99.98 5.0lE-03 9.02E-02 9.02E-02 miss Co-58 810.76 99.45 -6. 51E-03 5.75E-02 5.75E-02 1.000 1 674.73 0.52 O.OOE+OO 6.59E+OO 1. 024 Co-60 1173.23 99.85 2.81E-03 9.94E-02 1.06E-01 0.947 13 32.49 99.98 1.07E-02 9.94E-02 0.947 Nb-94 702.65 99.8 1 O.OOE+OO 7.52E-0 2 7.52E-02 0.944 871. 09 99.89 -4.48E-04 8.68E-0 2 0.944 Ag-108m 79.13 6.60 7.lOE-01 7.74E-02 2.67E+OO miss 433.94 90.50 -1.18E-03 8.85E-02 0.887 614.28 89.80 -3.02E-03 8.13E-02 0.886 7 2 2.94 90.80 -8.34E-03 7.74E-02 0.887 Sn-113 255.13 2 .11 -4.33E-01 1.0 6E-01 2.98E+OO free 391.70 64.97 1.31E-02 1. 06E-01 free Cs-134 475.36 1. 48 -2.61E+OO 6.12E-02 3.19E+OO miss 563.25 8.34 1.83E-02 1.00E+OO 0.89 6 569.33 1 5.37 -1.91E-01 5.93E-01 0.888 604. 72 97.62 2.64E-03 6.12E-02 0.931 10/4/20, _ 3:08: 30PM Page 6 of8 Analysis Report for 04-0ct-16-10010 L3-10219A-FRGS-003SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pC//grams)

Corr Cs-13 4 795.86 85.46 2. 59E-02 6.12E-02 1. 27E-01 0.933 801.95 8.69 1.86E-01 8.62E-01 0.898 1038.61 0.99 1.00E+OO 8.58E+OO 0.943 1167.97 1. 79 -1.51E+OO 4.47E+OO 1. 081 1365.19 3.0 2 5.80E-01 3.28E+OO 1.128 + Cs-137 661.66 85.10 6.87E-02 1.30E-01 1.30E-01 miss + Eu-152 121.78 2 8.67 9.55E-02 2.23E-01 2.83E-01 0.936 244.70 7.61 -1.06E-01 7.59E-01 0.935 295.94 0.45 7.70E+OO 2.12E+01 miss 344.28 26.60 -2.63E-02 2.23E-01 0.957 367.79 0.86 -2.38E+OO 5.13E+OO 0.884 411.12 2.24 -6.73E-01 3.37E+OO 0.908 443.96 2.83 5.82E-01 2.39E+00 0.9 34 488.68 0.42 1.96E+OO l.14E+Ol rniss 563.99 0.49 -6.06E+OO 1.49E+01 0.934 586.26 0.46 -5.92E+OO l.25E+01 0.94 2 678.62 0.47 -1.15E+OO 1.43E+Ol 0.887 688.67 0.86 6.69E-01 1.0lE+Ol 0.980 719.3 5 0.28 8.33E+OO 3.38E+Ol miss 778.90 12. 96 9.61E-02 5.35E-01 0.945 810.45 0.32 -5.3eE+00 1.58E+Ol 1. 050 867.37 4.26 3.20E-02 1.78E+OO 0.928 919.33 0.43 7.79E+OO 2.47E+Ol 0.981 964. 08 14.65 l.71E-01 7.69E-01 1.022 1085.87 10.2 4 -6.06E-02 9.13E-01 1.018 1089.74 1. 7 3 6.53E-01 6.46E+OO 0.952 1112. 07 13. 69 2.59E-01 8.67E-01 0.992 1212.95 1. 43 O.OOE+OO 1.94E+OO 0.929 1249.94 0.19 l.14E+Ol 6.13F+Ol 1. 097 1299.14 1. 63 3.2 4E+OO 8.51E+OO 0.944 1408.01 21. 07 7.2 8E-0 3 3.75E-01 0.983 1457.64 0.50 -1.06E+Ol 3.34E+Ol 1. 076 1 528.10 0.28 O.OOE+OO 1.07E+Ol 1. 007 Eu-154 123.07 40.40 -2.88E-02 1.67E-01 1.67E-01 0.934 247.93 6.89 2.66E-01 9.2 7E-01 0.928 ~91.76 4.95 9.39E-01 2.06E+OO 0.915 692.42 1. 78 O.OOE+OO 1.06E+OO 0.936 723.30 2 0.06 -8.96E-0 2 2.64E-01 0.935 756.80 4.52 -4.47E-01 2.0lE+OO 0.915 873.18 12.08 -6.2 1E-02 6.2 9E-01 0. 33 2 996.29 10.48 5.47E-02 8.84E-01 0.971 1004.76 18.01 5.57E-02 5.14E-01 0.978 12 74.43 34.80 -4. llE-03 2.12E-01 0.98 1 1596.48 1. 80 O.OOE+OO 1.49E+OO 1.1 75 + Eu-155 45.30 1. 3 1 -8.llE+OO 3.57E-01 3.93E+01 0.999 60.01 1. 22 -1.26E+O l 4.1 7E+Ol 1. 000 86.55 3 0.70 2.13E-01 4.58E-01 free 105.31 2 1.10 -4.90E-02 3.57E-01 1.000 + Tl-208 583.19 85.00 1.16E-01 1.64E-01 1.64E-01 0.93 2 + Bi-211 351.07

13. 0 2 2.08E+00 3.09E-01 3.09E-01 miss + Pb-211 404.85 3.78 7.15E-02 1.68E+OO 1.68E+OO miss 10/4/20 I -3:08:30PM Page 7 of8 Analysis Report for 04-0ct-16-10010 L3-10219A-FRGS-003SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

Corr Pb-2 11 427.0 9 1. 76 6.91E-01 1.68E+OO 2.86E+OO mis s 832.01 3.52 5.50E-01 2.52E+OO mis s + Bi-212 39.86 1. 06 -2.2 6E+Ol 1. 87E+OO 3.13E+Ol 0.998 727. 33 6.67 6.58E-01 l.87E+OO 0.982 785.37 1.10 3.79E-02 7.34E+OO 0.944 1 62 0.50 1. 47 9.44E-01 7.38E+OO 1. 006 + Pb-212 115 .18 0.60 5.74E+OO 1. 4 7E-01 l.36E+Ol miss 23 8.63

43.60 3.84E-01 1.47E-0 1 free 30 0.0 9 3.30 -4.59E-02 2.2 5E+OO fre e + Pb212-XR 74.82 1 0.28 1. 03E+OO 1.56E+OO 2.5 9E+OO miss 77 .11

1 7.10 l.OlE+OO l.56E+OO miss 87.35 3.97 4.76E-01 3.47E+OO miss 89.78 1. 46 -7.63E-01 7.74E+OO miss + Bi-21 4 609.32

45.49 5.20E-01 l.16E-0 1 l.16E-01 0.948 768.36 4.89 1.77E-01 2.14E+OO 0.94 2 806.18 1. 26 9.63E-01 6.66E+OO 0.923 934.06 3.11 9.31E-01 3.84E+OO 0.944 1120.2 9 1 4.92 3.57E-01 1.07E+OO 0.944 1155.21 1. 63 -5.97E-01 7.17E+OO 0.94 3 1238.1 2 5.83 -3.74E-02 2.lOE+OO 0.944 128 0.98 1. 43 -3.12E-01 8.73E+OO 0.944 1377.67 3.99 7.57E-01 2.72E+OO 1.030 1385.31 0.79 l.99E-01 l.02E+Ol 0.945 1401.52 1. 33 4.18E+OO l.lOE+Ol 0.945 1 407.99 2.39 6.66E-02 3.43E+OO 0.945 1 509.21 2 .13 O.OOE+OO 1. 49E+OO 0.950 1 661.27 1. 05 2.2 9E+OO 1.06E+Ol 1. 001 1729.59 2.88 7.67E-01 3.56E+OO 1.119 1764.49 15.30 6.55E-01 1.30E+OO 1. 001 1847.43 2.0 3 2.25E-01 4.42E+OO 1. 0 63 > 2 11 8.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 241.99 7.25 6.54E-01 l .13E-0 1 l.17E+OO 1.000 2 95. 22 18.4 2 6.2 4E-01 6.06E-01 1. 000 351.93

35.60 7.59E-01 l.13E-01 free 785. 96 1. 0 6 1.98E+OO 8.04E+OO 1. 000 + Pb21 4-XR 74.8 2 5.80 1.83E+OO 2.76E+OO 4.59E+OO miss 77 .11 .. 9.70 l.79E+OO 2.76E+OO mi ss 87.35 2.24 8.44E-01 6.15E+OO mi ss 89.78 0.82 -1.36E+OO

1. 38E+Ol miss + Ra-226 1 86.21 3.64 2.86E-01 1.66E+OO 1.66E+OO free + Ac-228 129.07 2.4 2 -3.2 1E-0 1 5.12E-01 2.86E+OO 0.944 209.2 5 3.89 6.97E-02 1.53E+OO 0.978 270.2 4 3.46 6.61E-01 2.16E+OO 0.955 328.00 2.95 -5.26E-01 1.49E+OO 0.955 338.32 11. 2 7 5.55E-01 8.55E-01 0.992 409.46 1. 9 2 1.95E-01 3.79E+OO 0.937 463.00 4.40 -5.18E-01 l.12E+OO 0.93 3 7 94. 95 4.25 4.32E-01 2.52E+OO 0.942 911. 20 2 5.80 2.35E-0 1 5.12E-01 0.990 964.77 4.99 6.03E-01 2.35E+OO 0.981 968.97 1 5.8 0 7.44E-01 1.08E+OO 0.990 Analysis Report for 04-0ct-16-10010

+ + + + + > L3-10219A-FRGS-003SS Nuclide Energy Yield(%) Activity Name (keV) (pCilgrams)

Ac-22 8 1588.2 0 3.22 -1. 34E-01 Pa-231 27.36 10.30 -1.81E-02 2 83.69 1. 70 -2.27E-01 300.07 2.47 -6 .13E-02 302.65 2.2 0 8.42E-02 330.06 1. 40 1.0lE+OO Th-234 92. 38 2.13 -2.3 1E-01 92.80 2.10 -4.52E-01 112. 81 0.21 3.40E+OO U-2 3 5 143.76 10. 96 1.25E-02 163.33 5.08 1.32E-01 185.71 57.2 0 1.59E-02 202 .11 1. 08 9.90E-01 205.31 5.01 -4.48E-01 Am-24 1 59.54 35.90 -2.13E-01 = Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/4/2C., *-NuclideMDA (pCUgrams) 5.12E-01 3.00E+OO 6.36E+OO 1.06E-0 1 l.49E+O O ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed. free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 3:08:30PM Page 8 of8 LineMDA Caine (pC//grams)

Corr 2. 64E+OO 1.002 5.43E+OO 0.998 3.49E+OO 1. 000 3.00E+OO 1. 000 3.05E+OO 1.000 4.20E+OO 1. 000 6.36E+OO fre e 6. 71E+OO fre e 4.79E+Ol fre e 5.82E-01 free l.22E+O O free l.06E-01 free 6.42E+00 miss 1. 03E+OO free l.49E+OO free 60 55 50 45 40 35 1000 2000 3000 0000016024.CNF 4000 channel 5000 Live Time 300.000 sec Real Time 300.440 sec start: 1 -0. l(kev) stop : 8192 2047. O(kev) Acq. Start Tue act 04 14: 45: 09 2016 6000 7000 8000 10/4,~ o 3:34:32PM

~~~pex-Gamma Analysis Report for 04-0ct-16-10011 L3-10219A-FRGS-004SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 04-0ct-16-10011

L3-10219A-FRGS-004SS : 1 L 130G Soil Sample 1.334E+03 grams : Default : 9/27/2016 3:45:00PM

10/4/2016 3:11:09PM

130G 1 L Soil Sample ; HTomlin : P40818B : 130G Soil : 300.0 s econds : 300.5 s econds : 0.18% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16025 PEAK WITH NID REPORT Peak Analysis Performed on 10/4/2016 3:16:12PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB Peak MatchJTol\rjJ-i): 1.000FWHM I lo\'f /11? (._CP~ Page 1 of8 10/4/21., , 3:34:32PM Page 2 of8 Analysis Report for 04-0ct-16-10011 L3-10219A-FRGS-004SS M m Peak Energy ROI No. (keV) start 1 235.10 938 -2 238.57 938 -3 294.77 1175 -4 351.86 1402 -5 609.22 2 430 -6 1 460.52 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 960 1186 1413 2441 5853 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 940.89 8.82E+OO 8.04 1.92E+Ol 954.78 4.42E+Ol 15.59 3.64E+Ol 1179.41 2.71E+Ol 14.96 2.1'7E+Ol 1407.61 4.12E+Ol 15.87 1. 96E+Ol 2436.64 2. 72E+Ol 12.42 9.55E+OO 5843.05 8.93E+Ol 19.56 5.30E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.82

10.66 8.22E+00 1.94E+OO Pb-212 1. 00 115 .18 0.60 238.63

43.60 2.92E-01 1.13E-01 300.09 3.30 Bi-21 4 1. 00 609.32

45.49 3.49E-0 1 1.65E-01 768.36 4.89 806.18 1. 26 934.06 3 .11 1120.2 9 1 4. 92 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1661. 27 1. 05 1729.59 2.88 1764.49 15.30 1847.4 3 2.03 Tentative Nuclide Th-2.27 Pb-21 2 Pb-214 Pb-214 Bi-211 Bi-214 K-40 Coinc Corr miss f r ee 0.948 Analysis Report for 04-0ct-16-10011 L3-10219A-FRGS-004SS Nuclide Id Energy Name Confidence (keV} Bi-214 1. 00 2118.51 Pb-214 0.99 2 41.99 2 95.22 351.93 785. 96 Th-2 2 7 0.98 50 .13 79.69 94.97 2 10.62 235. 96 2 56.23 2 86.09 2 99.98 304.50 329.85 334.37 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

tree = No coincidence correction required.

Yield(%) 1.16 7.25 18.42 35.60 1. 06 8.40 1. 95 0.03 1.25 12.90 7.00 1. 74 2.2 1 1.15 2.90 1.14 miss = Nuclide energy was not found in the coincidence library. 10/4/21. .. 3:34:32PM Page 3 of8 Activity Activity Coinc (pCi/grams)

Uncertainty Corr 4.86E-01 2.79E-01 1. 000 4.2 7E-01 1.78E-0 1 free 1. %E-01 1.84E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.995 8.22E+OO 1.94E+OO X Bi-2 11 0.963 Pb-21 2 1. 000 2.92E-01 1.13E-01 Bi-214 1. 000 3.49E-01 1.65E-01 Pb-214 0.996 4.44E-0 1 1.SOE-01 Th-227 0.986 1. 96E-0 1 1.84E-01 Analysis Report for 04-0ct-16-10011

? X @ = = = L3-10219A-FRGS-004SS nuclide is part of an undetermined solution nuclide rejected by the Interference analysis nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/4/2l, 3:34: 32PM Page 4 of8 10/4/2L . _ 3:34:32PM Analysis Report for 04-0ct-16-10011

+ + + + + + + + + L3-10219A-FRGS-004SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/4/2016 3:16:12PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\CanberraiApex\Root\Defauit\Library\ZION UB-BNL.NLB Nuclide Energy Yield(%.)

Activity NuclldeMDA LineMDA Name (keV) (pCilgrams) (pCltgrams) (pCi!grams)

K-40 1460.82

1 0.66 8.22E+OO 1.0lE+OO l.OlE+OO Cr-51 320.08 9. 91 -5.22E-03 5.89E-01 5.89E-01 Mn-54 834.85 99.98 6.79E-03 7.31E-02 7.31E-0 2 Co-58 810.76 99.45 1.18E-03 6.56E-02 6.56E-02 1674.73 0.52 -2.75E-01 1.62E+Ol Co-60 1173.2 3 99.85 -1.2 3E-0 2 2.G2E-02 9.59E-02 1332.49 99.98 O.OOE+OO 2.62E-02 Nb-94 702.65 99.8 1 8.43E-03 6.77E-02 8.29E-02 871.09 99.89 -2.SSE-02 6.77E-0 2 Ag-108m 79.13 6.60 -9.lOE-01 3.92E-02 2.2 1E+OO 433.94 90.50 -2.03E-02 3.92E-02 614.2 8 89.80 8.SSE-03 8.21E-02 722. 94 90.80 1. 47E-0 2 8.12E-02 Sn-113 2 55.13 2 .11 -3.58E-01 6.89E-02 2.3oE+OO 3 91. 70 64.97 -2.30E-02 6.89E-02 Cs-134 475.36 1. 48 l.66E-01 6.42E-02 3.34E+OO 563.25 8.3 4 -2.76E-02 8.2 9E-01 569.33 15.37 -l.75E-01 3.54E-01 Page 5 of 8 Tolerance Nuclide Coinc Corr miss free miss 1. 000 1. 0 2 4 0.947 0.947 0.944 0.944 miss 0.887 0.88 6 0.887 free free miss 0. 896 0.888 604. 72 97.62 -2.27E-02 6.42E-02 0.931 10/4/2(,.

_ 3:34:32PM Page 6 of8 Analysis Report for 04-0ct-16-10011 L3-10219A-FRGS-004SS Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 3.04E-02 6.42E-02 l.36E-01 0.933 801.95 8.69 2.45E-01 1.0lE+OO 0.898 1038.61 0.99 2.51E+OO 1.00E+Ol 0.943 1167.97 1. 79 6.2 3E-02 4.05E+OO 1. 081 1365.19 3.02 O.OOE+OO 7.46E-01 1.128 + Cs-137 661. 66 85.10 8.18E-02 1. 35E-0 1 1.35E-01 miss + Eu-1 52 121. 78 2 8.67 -7.66E-03 2.15E-01 2.27E-01 0.936 244.70 7.61 4.07E-0 2 9.69E-01 0.935 295.94 0.45 O.OOE+OO 1.77E+Ol miss 344.28 2 6.60 '.2.2 1E-02 2.15E-01 0.957 367.79 0.86 -1.14E+OO 6.56E+OO 0.884 411.12 2.2 4 -3.25E-01 1. 89E+OO 0.908 443. 96 2.83 5.43E-01 2.32E+OO 0.934 488.68 0.4 2 4.43E-01 1.33E+Ol miss 563.99 0.49 2.91E+OO l.47E+Ol 0.934 586.2 6 0.46 -5.3 6E+OO l.3 1E+Ol 0.94 2 678.62 0.47 -1.16E+OO 1.02E+Ol 0.887 688.67 0.86 -5.82E-01 5.14E+OO 0.980 719.35 0.28 -1.63E+OO 2.02E+Ol miss 778.90 12. 96 2.17E-01 7.36E-01 0.945 810.45 0.32 -3.25E-01 l.81E+Ol 1. 050 867.37 4.26 3.19E-01 2.09E+OO 0.92 8 919.33 0.43 -2.84E-01 1.84E+Ol 0.981 964. 08 14.65 1.97E-01 5.93E-01 1. 022 1085.87 10.24 -3.51E-01 5.65E-01 1. 018 1089.74 1. 73 5.56E-01 5.24E+OO 0.952 1112.07 13.69 8.12E-02 7.19E-01 0. 992 1212.95 1. 43 O.OOE+OO 1.76E+OO 0. 92 9 1249.94 0.19 6 , 05E-01 3.93E+Ol 1. 097 1 2 99.14 1. 63 -8.39E-01 4.32E+OO 0.944 1408.01 2 1. 07 l.45E-01 5.54E-01 0. 983 1457.64 0.50 -1.32E+Ol 2.72E+Ol 1. 076 1528.1 0 0.28 2.56E+OO 2.64E+Ol 1.007 + Eu-154 123.07 40.40 2.69E-03 7.05E-02 l.51E-01 0.934 247.93 6.89 -5.39E-01 6.07E-01 0.928 591. 76 4.95 4.69E-0 2 1.41E+OO 0.915 692.42 1. 78 5.92E-02 3.30E+OO 0.936 723.30 2 0.06 5.40E-03 3.0lE-01 0.935 756.80 4.52 O.OOE+OO 2.14E+OO 0.915 873.18 12.08 3.68E-01 8.64E-01 0.932 996.29 10.48 -2.23E-01 6.90E-01 0. 971 1004.76 18.01 3.60E-02 3.18E-01 0.978 1274.43 34.80 O.OOE+OO 7.05E-02 0.981 1596.48 1. 80 O.OOE+OO 1. 35E+OO 1.175 + Eu-155 45.30 1. 31 -l.33E+OO 3.88E-01 3.38E+Ol 0.999 60.01 1. 22 1.66E+Ol 4.75E+O l 1. 000 86.55 30.70 6.61E-02 3.88E-01 free 105.31 2 1.10 -1.15E-01 3.95E-Ol 1.000 + Tl-208 583.19 85.00 1.lOE-01 1.63E-01 1. 63E-01 0.93 2 + Bi-211 351.07

13. 02 l.17E+OO 5.12E-01 5.12E-01 miss + Pb-211 404.85 3.78 5.88E-01 1. 71E+OO 1. 71E+OO miss 10/4/2(.,, 3:34:32PM Page 7 of8 Analysis Report for 04-0ct-16-10011 L3-10219A-FRGS-004SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCl/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 -2.21E-01 1.71E+OO 3.15E+OO miss 83 2.01 3.52 -8.42E-0 2 2.04E+OO miss + Bi-21 2 39.86 1. 06 -4.38E+OO 1.55E+OO 3. 71E+Ol 0.998 7 2 7.33 6.67 7.69E-01 1.55E+OO 0.982 785.37 1.10 l.78E+OO 9.2 7E+OO 0.944 16.'.20.50 L 47 7.19E-01 5.2 9E+OO 1. 006 + Pb-212 115 .18 0.60 1.30E+OO l.49E-01 9.87E+OO miss 238.63

43.60 2.92E-01 1.49E-01 fre e 300.09 3.30 3.76E-01 2.1 5E+OO fre e + Pb21 2-XR 74.82 10.28 l.09E+OO 1.41E+OO ~.43E+OO miss 77 .11 17.10 7.67E-01 l.41E+OO miss 87.35 3.97 5.81E-01 2.95E+OO miss 89.78 1. 46 1.21E+OO 6.82E+OO miss + Bi-214 609.32

45.49 3.49E-01 1. 73E-01 l.73E-Ol 0.948 768.36 4.89 4.03E-01 1.80E+OO 0.942 806.18 1. 2 6 5.60E-01 4.12E+OO 0.923 934.06 3.11 9.53E-01 3.23E+OO 0.944 1120.2 9 14. 9.'.2 2.17E-01 8.69E-01 0.944 1155.21 1. 63 O.OOE+OO l.46E+OO 0.943 1238.12 5.83 l.58E-01 1.90E+OO 0.944 12 80.98 1. 43 O.OOE+OO 1.78E+OO 0.944 1377. 67 3.99 O.OOE+OO 6.18E-01 1. 030 1385. 31 0.79 O.OOE+OO 3.40E+OO 0.945 1 401. 52 1. 33 l.08E-01 7.03E+00 0.945 1 407.99 2.39 l.33E+OO 5.07E+OO 0.945 1509.21 2 .13 4.97E-01 3.66E+OO 0.950 1661. 2 7 1. 05 1.03E+OO 7.61E+OO 1. 001 1729.59 2.88 3.47E-01 2.55E+OO 1.119 1 764.49 15.30 4.39E-01 1. llE+OO 1. 001 1 847.43 2.03 l.31E+OO 5.85E+OO 1. 063 > 2 118. 51 1.16 O.OOE+OO O.OOE+OO 1.041 + Pb-214 241.99 7.25 9.40E-01 1.87E-01 l.16E+OO 1. 000 295.22

18.42 4.86E-01 3.64E-01 1. 000 351.33

35.60 4.27E-01 l.87E-01 free 785.96 1. 06 -1.25E+00 8.55E+OO 1.000 + Pb214-XR 74.82 5.80 l.92E+OO .'.2.49E+OO 4.30E+OO miss ,7 .11 9.70 1. 3 5E+OO 2.49E+OO miss 87.35 2.24 l.03E+OO 5.23E+OO miss 89.78 0.82 2.16E+OO 1. 21E+O l miss + Ra-226 186.2 1 3.64 7.45E-01 1.66E+OO 1.66E+OO free + Ac-228 129.07 2.42 1.82E-01 6.96E-01 2.79E+OO 0.944 209.25 3.89 -1.35E-01

1. 24E+OO 0.978 270.24 3.46 5.33E-01 1.78E+OO 0.955 328.00 2.95 1.17E+OO 2.74E+OO 0.955 338.32 11. 27 5.83E-01 7.90E-01 0.99 2 409.46 1. 92 3.66E-01 3.00E+OO 0.937 463.00 4.40 -7.08E-02

1. 31E+OO 0.933 794.95 4.25 l.48E+OO 3.04E+OO 0.942 911. 20 25.80 5.38E-01 6.96E-01 0.990 964.77 4.99 6.04E-01 1. 81E+OO 0.981 968.97 15.80 6.19E-Ol 9.53E-01 0.990 Analysis Report for 04-0ct-16-1 0011 + + + + + > L3-10219A-FRGS-004SS Nuclide Energy Yield(%) Activity Name (keV) (pCl!grams)

Ac-228 1588.2 0 3.22 O.OOE+OO Pa-231 27.36 10.30 l.38E+OO 2 83.69 1. 70 -9.84E-01 300.07 2.47 5.02E-01 302.65 2.2 0 -7.62E-01 330.06 1. 40 -5.82E-01 Th-234 92.38 2 .13 7.73E-01 92. 80 2.10 3.2 4E+OO 112. 81 0.2 1 -7.00E+OO U-235 143.76 10. 96 5.2 1E-02 163.33 5.08 l.90E-02 185.71 57.20 3.40E-02 202.11 1. 08 -8.03E-01 205.31 5.01 1. 83E-02 Am-241 59.54 35.90 6 .13E-01 = Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/4/2C,.

-NuclideMDA (pCUgrams) 6.96E-01 2.48E+OO 5.61E+OO 1. 05E-01 1. 73E+OO ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 3:34:32PM Page 8 of8 LineMDA Coinc (pCi!grams)

Corr 8.78E-01 1.002 5.77E+OO 0.998 2.48E+OO 1. 000 2.88E+OO 1. 000 2.65E+OO 1. 000 3.04E+OO 1.000 5.61E+OO free 6.33E+OO free 3.54E+Ol free 4.98E-01 free 9.52E-01 free l.OSE-01 free 4.12E+OO miss 9.73E-01 free l.73E+OO free 60 55 50 45 1000 2000 3000 0000016025 .CNF 4000 channel 5000 Live Time :300.000 sec Real Time : 300. 530 sec start: 1: -0.l(kev) stop : 8192: 2047. O(kev) Acq. start :Tue Oct 04 15:11:09 2016 6000 7000 8000 10/6/21.J , .., 6:53:38AM

~§~pex-Gamma Analysis Report for 06-0ct-16-10001 L3-10219A-FRGS-005SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification EnE;irgy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Peak Analysis Performed on Peak Analysi s From Channel Peak Analysi s To Channel : 06-0ct-16-10001

L3-10219A-FRGS-005SS

1 L 130G Soil Sample 1.201E+03 grams : Default : 9/27/2016 2:00:00PM

10/6/2016 6:30:21AM

130G 1 L Soil Sample : HTomlin : P408188 : 130G Soil : 300.0 seconds : 300.5 seconds : 0.17 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16040 PEAK WITH NID REPORT 10/6/2016 6:35:24AM

120 : 8192 Tentative NID Library Peak Match Toleranc e : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB 1.000FWHM V (..,~ 0 A. *-ref) r,J I re, t, e,_ \\) Page I of7 Analysis Report for 06-0ct-16-10001 L3-10219A-FRGS-005SS Peak Energy ROI No. (keV) start 1 351.81 1402 -2 583.32 2328 -3 609.15 2429 -4 1460.81 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 1413 233 8 2443 5852 10/6/201b 6:53:38AM Peak Net Peak Net Area Centroid Area Uncertainty 1407.42 4.39E+Ol 1 5.15 2333.06 1. 88E+Ol 9.69 2436.33 3.90E+Ol 13. 64 5844.22 8.51E+01 19.19 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 1.21E+Ol Pb-214 Bi-211 4.40E+OO Tl-208 6.00E+OO Bi-214 5.71E+OO K-40 Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 1. 00 1460.82

10.66 8.70E+OO 2.lOE+OO miss Tl-208 0.99 583.19

85.00 1.42E-01 7.53E-02 0.932 Bi-211 0. 96 351.07

13. 02 1.3 8E+OO 5.2 6E-01 miss Bi-214 0.99 609.32

45.49 5.55E-01 2.05E-01 0.948 768.36 4.89 806.18 1. 26 934.06 3.11 1120.2 9 14.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 3 1 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241. 99 7.25 295.22 18.42 Analysis Report for 06-0ct-16-10001 L3-10219A-FRGS-005SS Nuclide Name Pb-214 Id Confidence 0.99 Energy (keV) 351.93

785.96 * = Energy line found In the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/6/2010 6:53:38AM Page 3 of7 Activity (pCi/grams) 5.06E-01 Activity Uncertainty 1.92E-01 Caine Corr free INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Tl-208 ? Bi-211 Bi-214 ? Pb-214 Nuclide Id Confidence

1. 000 0.999 0. 967 0.999 0.999 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 8.70E+OO 1. 42E-01 l.38E+OO 5.55E-01 5.06E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 2.lOE+OO 7.53E-02 5.26E-01 2.05E-01 1.92E-01 10/6/201 6:53:38AM Analysis Report for 06-0ct-16-10001

+ + + L3-10219A-FRGS-005SS Peak Locat e Performed on Peak Locat e From Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/2016 6:35:24AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertain'ly Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keVj (pC/lgrams) (pCilgrams) (pCl/grems)

K-40 1 460.82

10.66 8.70E+OO 1.16E+OO l.16E+OO Cr-51 320.08 9.91 3.02E-02 6.82E-01 6.82E-01 Mn-54 834_85 99.98 2.52E-0 3 9.93E-02 9.93E-02 Page 4 of7 Tolerance Nuclide Coinc Corr miss free miss + Co-58 810.76 99.45 -5.98E-0 3 7.41E-02 7.41E-02 1.000 1 674.73 0.52 O.OOE+OO 6.73E+OO 1. 024 + Co-60 1 173.23 99.85 2.36E-03 1.00E-01 1. 07E-01 0.947 1332.49 99.98 1. OOE-02 1. OOE-01 0.947 + Nb-94 702.65 99.81 -2.34E-02 5.17E-02 5.17E-02 0.944 871.09 99.89 -2.63E-0 2 7.52E-02 0.944 + Ag-108m 79.13 6.60 -3.78E-01 6.3,E-02 1.89E+OO mis s 433.94 90.50 -2.05E-02 6.37E-02 0.887 614.28 89.80 l.95E-02 1.07E-01 0.886 722.94 90.80 5.59E-03 9.02E-0 2 0.887 + Sn-11 3 255 .13 2.1 1 -8.34E-01 1.0lE-01 2. 51E+OO free 391.70 64.97 l.03E-02 1. OlE-01 free + Cs-134 475.36 1. 48 -8.84E-01 7.96E-02 4.53E+OO miss 563.25 8.34 3.93E-0 1 1.15E+OO 0. 896 569.33 15.37 3.39E-02 4.56E-01 0.888 604. 72 97. 62 5.30E-03 7.96E-02 0.931 10/6/2011:l 6:53:38AM Page 5 of7 Analysis Report for 06-0ct-16-10001 L3-10219A-FRGS-005SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr Cs-1 3 4 795.86 85.46 -7. 58E..,.03

7. 96E-02 1.09E-01 0.933 801.95 8.69 -1.87E-01 6.87E-01 0.898 1038.61 0.99 -4.65E-01 8.64E+OO 0.943 1167. 97 1. 79 4.85E-01 3.57E+OO 1. 081 1365.19 3.0 2 4.38E-0 2 2.85E+OO 1.1 2 8 + Cs-137 661.66 85.10 6.lOE-0 2 l.30 E-01 1.30E-01 miss + Eu-15 2 121.78 2 8.67 9.73E-0 3 2.38E-01 2.38E-01 0.936 244.70 7.6 1 -1.14E-02 8.30E-01 0.935 295.94 0.45 1.45E+Ol 2.31E+Ol mi ss 344.28 2 6.60 3.68E-02 2.39E-01 0.957 367.79 0.86 -2.51E+OO 7.28E+OO 0.884 411.12 2.24 -9.02E-0 3 2.96E+OO 0.908 443. 96 2.83 2.56E-01 1.97E+OO 0.934 488.68 0.42 3.63E+OO l.48E+Ol miss 563.99 0.49 1.80E+OO 1.49E+Ol 0.934 586.2 6 0.46 -5.14E+OO 9.95E+OO 0.94 2 678. 62 0.47 -2.83E+00 1.44E+Ol 0.887 688.67 0.86 -7.12E-01 7.21E+OO 0.980 719. 35 0.2 8 5.09E+OO 2.60E+Ol miss 773.90 1 2. 96 5.80E-0~ 4.2 6E-01 0.945 810.45 0.32 -9.0lE-01 2.0lE+Ol 1. 050 867.37 4.26 O.OOE+OO 5.22E-01 0.928 919.33 0.43 3.79E+OO 1.76E+Ol 0.981 964.08 14.65 2.83E-01 7.73E-01 1.02 2 1085.87 10.2 4 -1.22E-02 7.92E-01 1. 018 1089.74 1. 73 l.08E+OO 5.02E+OO 0.952 11 12.07 13.69 4.37E-0 2 8.71E-01 0.992 1212.95 1. 43 -2.17E+OO 5.3 1E+OO 0. 929 1249.94 0.19 1.3 4E+OO 5.06E+Ol 1. 097 1299.14 1. 63 1.12E+OO 6.06E+OO 0.944 1408.01 2 1.07 1.02E-01 4.76E-01 0.983 1457.64 0.50 -2.90E+Ol 3.65E+Ol 1. 076 1528.10 0.2 8 O.OOE+OO 1.08E+Ol 1. 007 + Eu-154 123.07 40.40 3.46E-0 2 7.83E-02 1.68E-01 0.934 247.93 6.89 3.0lE-01 1.03E+OO 0.92 8 591.76 4.95 -2.34E-01 9.58E-Ol 0.915 692.42 1. 78 8.55E-01 4.74E+OO 0.936 723. 30 20.06 4.80E-02 3.88E-Ol 0.935 756.80 4.52 5.89E-01 2.02E+OO 0.915 873.18 12.08 1.48E-01 8.18E-01 0.932 996.2 9 10.48 1.24E-01 7.67E-01 0.971 1004.76 18.01 -4.00E-02 3.53E-01 0.978 1274.43 34.80 O.OOE+OO 7.83E-02 0.981 1596.48 1. 80 5.54E-01 4.08E+OO 1.175 + Eu-155 45.30 1. 31 4.74E+OO 3.66E-01 3.95E+Ol 0.999 60.01 1. 22 1.34E+Ol 4.85E+Ol 1. 000 86.55 30.70 -6.26E-02 3.66E-01 free 105.3 1 2 1.10 1. 27E-0 2 4.18E-01 1. 000 + Tl-208 583.1 9

85.00 1.42E-01 7.22E-02 7.22E-02 0.932 + Bi-211 351.07

13. 02 1. 38E+OO 4.65E-01 4.65E-01 miss + Pb-211 404.85 3.78 3.95E-01 1.90E+OO 1.90E+OO mis s 10/6/2010 6:53:38AM Page 6 of7 Analysis Report for 06-0ct-16-10001 L3-10219A-FRGS-005SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Cain e Name (keV) (pCi/grams) (pCilgrams) (pC/lgrams)

Corr Pb-2 11 427.09 1. 76 -1. 55E+OO 1.90E+OO 2.48E+OO miss 832.01 3.52 6.58E-01 2.53E+OO miss + Bi-2 12

39. 86 1. 06 -1.95E+OO 1.36E+OO 4.12E+01 0.998 727; 33 6.67 3.79E-01 l.36E+OO 0.98 2 785.3"/ 1.10 -l.49E+Oci 5.04E+OO 0.944 1(:)20.50

1. 47 6.99E-01 5.88E+OO 1.006 + Pb-21 2 115 .18 0.60 4.66E+OO 2.89E-01 1.31E+Ol miss 238.63 43.60 3.27E-01 2.89E-01 free 300.09 3.30 5.00E-01 2.04E+OO free + Pb212-XR 74.8 2 10.2 8 4.62E-01 1. 53:E+OO 2.65E+OO miss 77 .11 17.10 6.47E-01 1.53E+OO miss 87 .. 15 3.97 O.OOE+OO 2.80E+OO miss 89.78 1. 46 -4.40E-01 7.15E+OO miss + Bi-214 609.32

45.49 5.55E-01 1.63E-01 1.63E-01 0.948 768.36 4.89 -6.35E-01 l.12E+OO 0.94 2 806.18 1.2 6 -5.18E-0 1 4.58E+OO 0.923 934.06 3.11 1.13E+OO 3.86E+OO 0.944 1120.2 9 14. 92 -1.15E-02 7.72E-01 0.944 1155.2 1 1. 63 -2.23E+OO 5.57E+OO 0.943 1238.12 5.83 8.2 0E-01 3.0oE+OO 0.944 1280.98 1. 43 1.46E+OO 6.79E+OO 0.944 1 377.67 3.99 8.51E-01 3.05E+OO 1. 030 1385. 31 0.79 1.40E+OO 1. 03E+Ol 0.945 14 01. 52 1. 33 8.40E-01 6.18E+OO 0. 945 1 407.99 2.39 9.37E-01 4.35E+OO 0.945 1509.2 1 2.13 O.OOE+OO 1.49E+OO 0.950 1661.2 7 1. 0 5 1.15E+OO 8.46E+OO 1. 00 1 1729,59 2.88 -4.82E-0 2 2.84E+OO 1.119 1764.49 15.30 4.12E-01 1. 08E+00 1. 001 1847.43 2.03 O.OOE+OO 1.63E+OO 1. 063 > 2118. 51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 14 241. 99 7.2 5 4.99E-01 1.70E-0 1 l.16E+OO 1. 000 295.22 1 8.42 4.33E-01 5.86E-01 1.000 351.93

35.60 5.06E-01 1.70E-01 free 785.96 1. 06 -2.2 4E-01 6.25E+OO 1. 000 + Pb214-XR 74.82 5.80 8.19E-01 2.69E+OO 4.69E+OO miss 77.11 9.70 1.14E+OO 2.69E+OO miss 87.35 2.24 O.OOE+OO 4.97E+OO miss 89.78 0.82 -7.84E-Ol l.2 7E+Ol miss + Ra-226 186.21 3.64 7.61E-01 2.00E+OO 2.00E+OO free + Ac-228 129.07 2.42 3.37E-01 5.60E-01 2.79E+OO 0.944 209.25 3.89 5.55E-01 1.64E+OO 0.978 270.24 3.46 4.46E-01 1.90E+OO 0.955 328.00 2.95 4.65E-O l 2.42E+OO 0.955 338.32 11.27 4.53E-02 6.73E-01 0.992 409.46 1. 92 1.52E-01 3.58E+OO 0.937 463.00 4.40 4.12E-01 l.82E+OO 0.933 794.95 4.2 5 -7.48E-02 2.16E+OO 0.942 911.20 25.80 1.70E-01 5.60E-0 1 0.990 964.77 4.99 1.54E-01 2.0lE+OO 0.981 968. 97 15.80 8.09E-01 l.12E+OO 0.990 10/6/201b 6:53:38AM Page 7 of7 Analysis Report for 06-0ct-16-10001 L3-10219A-FRGS-005SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCi/grams) (pCilgrams)

Corr Ac-2 28 1588.2 0 3.22 3.60E-01 5.60E-01 2.65E+OO 1. 00 2 + Pa-2 3 1 27.36 10.30 4.57E+OO 2.54E+OO 7.07E+OO 0.998 2 83.69 1. 70 7.36E-01 3.34E+OO 1.000 300.07 2.47 6.68E-01 2.72E+OO 1. 000 302.65 2.2 0 -2.12E-01 2.54E+OO 1. 000 330.06 1. 40 4.50E-01 4.46E+OO 1. 000 + Th-234 92. 38 2 .13 1.44E+OO 6.87E+OO 6.87E+OO free 92. 80 2.10 1.2 1E+OO 6.92E+OO free 112.8 1 0.2 1 2.2 0E+OO 4.55E+Ol free + U-235 1 43.76 10. 96 1.lOE-01 1.1:E-01 6.42E-01 free 1 63.33 5.08 l.37E-01 1.29E+OO free 185.71 57.2 0 2.04E-02 1.1 7E-01 f r ee 2 02.11 1. 08 -5.66E-01 4.35E+OO miss 205.31 5.01 3.90E-01 1.08E+OO free + Am-241 59.54 35.90 1.14E-01 1. 6:E+OO l.67E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Ill ..... C :::II 60 55 50 45 40 35 B 30 25 ;:;j 1 "' 1000 2000 3000 0000016040.CNF 4000 channel 5000 Live Time :300.000 sec Real Time :300.500 sec Start: 1: -0.l(kev) stop : 8192: 2047 .O(kev) Acq. start :Thu oct 06 06:30:21 2016 6000 7000 8000 Analysis Report for 1 O-Oct-16-10008 L3-10219A-FRGS-006SS 10/10/2016 10:08:11AM GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 10-0ct-16-10008

L3-10219A-FRGS-006SS

1 L 130G Soil Sample 1.311E+03 grams : Default : 10/3/2016 9:10:00AM

10/10/2016 9:44:42AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.16% : 2.80 : 120-8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16064 PEAK WITH NID REPORT Peak Analysis Performed on. 10/10/2016 9:49:49AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce ., }<9 ,,.. ' !I... \J,,... '.,i~ '° I"' I,.,. : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM P age I of7 10/10/2016 10:08:11AM Page 2 of7 Analysis Report for 1O-Oct-16-10008 L3-10219A-FRGS-006SS Peak Energy ROI No. (keV) start 1 238.49 949 -2 351. 7 5 1400 -3 609.18 2431 -4 1460.46 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 961 1413 2442 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.46 3.90E+Ol 20.99 5.40E+Ol 1407.19 3.3 7E+Ol 14.65 1.66E+Ol 2436.45 2.56E+Ol 11.12 4.80E+OO 5842.80 7.68E+Ol 17.84 2.49E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

10.66 7.19E+OO 1.78E+OO Bi-211 0.97 351.07

13.02 9. 72E-01 4.50E-Ol Pb-212 0.99 115 .18 0.60 2 38.63

43.60 2.62E-01 1.47E-Ol 3 00.09 3.30 Bi-2 14 0.99 609.32

45.49 3.34E-01 1.50E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 11 2 0.2 9 14.92 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.2 1 2.13 1661.2 7 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Tentative Nuclide Pb-212 Pb-214 Bi-211 Bi-214 K-40 Caine Corr miss miss free 0.948 Analysis Report for 1 O-Oct-16-10008 L3-10219A-FRGS-006SS Nuclide Id Energy Name Confidence (keV) Pb-214 0.99 241. 99 295.22 351.93 785. 96 " = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

"' 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free "' No coincidence correction required.

Yield(%) 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/10/2016 10:08:11AM Page3 of7 Activity Activity Caine (pCi/grams)

Uncertainty Corr 3.55E-01 1.65E-01 free INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? Bi-211 Pb-21 2 Bi-214 ? Pb-214 Nuclide Id Confidence 0.992 0. 972 0.999 0.999 0.999 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 7.19E+OO 9. 72E-01 2.62E-01 3.34E-01 3.55E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 1.78E+OO 4.50E-01 1.47E-01 1.50E-01 1. 65E-01 10/10/2016 10:08:11AM Page 4 of7 Analysis Report for 10-0ct-16-10008

+ + + + + + + + + L3-10219A-FRGS-006SS Peak Locate Performed on Peak Locate From Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 9:49:49AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCl/grams) (pCilgrams)

Corr K-40 1460.8 2

10.66 7.19E+OO 7.71E-01 7.71E-01 miss Cr-51 320.08 9.9 1 1.46E-01 6.75E-01 6.75E-01 free Mn-54 834.85 99.98 -9.22E-0 3 6.42E-0 2 6.42E-02 miss Co-58 810.76 99.45 -2.40E-03 8.63E-02 8.63E-0 2 1. 000 1 674.73 0.5 2 O.OOE+OO l.65E+Ol 1. 024 Co-60 1173.2 3 99.85 2.07E-02 9.15E-02 9.76E-02 0.947 133 2.49 99.98 -l.27E-02 9.15E-02 0.947 Nb-94 702.65 99.8 1 1.64E-0 2 7.73E-02 7.73E-02 0.944 871. 09 99.89 2.2 3E-02 7.99E-02 0.944 Ag-108m 79.13 6.60 -1.13E-01

1. 88E-02 2.32E+OO miss 433.94 90.50 2.17E-03 6.51E-0 2 0.887 614.28 89.80 O.OOE+OO 1.88E-02 0.886 722.94 90.80 O.OOE+OO 2.08E-02 0.887 Sn-113 255 .13 2 .11 9.46E-03 9.18E-02 2.85E+OO free 391.70 64.97 -5.64E-03 9.18E-02 free Cs-134 475.36 1. 48 1.72E+OO 7.29E-02 4.46E+OO miss 563.25 8.34 -3.37E-01 5.17E-01 0.896 569.33 15.37 -4.65E-02 2.85E-01 0.888 604. 72 97. 62 6.67E-03 7.29E-02 0.931 10/10/2016 10:08:11AM Page5of7 Analysis Report for 10-0ct-16-10008 L3-10219A-FRGS-006SS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coin c Name (keV) (pCl/grams) (pCUgrams) (pCi!grams)

Corr Cs-134 795.86 85.46 1.18E-02 7.2 9E-02 7.73E-02 0.933 801.95 8.69 9.97E-02 9.20E-01 0.898 1 038.61 0.99 -1.13E+OO 6.26E+OO 0.943 1167.97 1. 79 6.33E-0 2 4.12E+OO 1. 08 1 1365.19 3.0 2 O.OOE+OO 7.59E-01 1.128 + Cs-137 661.66 85.10 4.56E-02 1. 09E-01 1. 09E-01 miss + Eu-152 121.78 28.67 -8.2 6E-02 l.5:E-0 1 2.llE-01 0.936 244.70 7.61 7.72E-02 7. 61E-01 0. 935 295.94 0.45 1.71E+OO l.69E+Ol miss 344.2 8 26.60 -6. llE-02 1.57E-01 0.957 367.79 0.86 2.14E+OO 6.67E+OO 0.884 411.12 2.2 4 -5.37E-0 1 2.48E+00 0.908 443.96 2.8 3 -1.44E+OO 1.2 3E+OO 0.934 488.68 0.4 2 2.33E+OO l.2 1E+Ol miss 563.99 0.49 1.44E+OO l.23E+Ol 0.934 586.26 0.46 -3.96E+OO l.33E+Ol 0.94 2 678.62 0.47 O.OOE+OO 3.83E+OO 0.887 688.67 0.86 -1. llE+OO 7.65E+OO 0.980 719.35 0.28 -3.68E-01 l.63E+Ol miss 778.90 1 2. 96 -8.85E-0 2 4.93E-01 0.945 8 10.45 0.32 -8.2 6E+OO l.84E+Ol 1. 050 867.37 4.26 -3.2 4E-01 1.30E+OO 0.928 919.33 0.43 3.76E+OO 2.08E+Ol 0.981 964.08 14.65 2.2 8E-01 6.58E-01 1. 02 2 1085.87 10.24 -1. 34E-*01 7.25E-01 1. 018 1 089.74 1. 73 9.91E-01 5.95E+OO 0.95 2 11 12.07 13.69 O.OOE+OO 1.65E-01 0.99 2 1212.95 1. 43 2.85E+OO 8.67E+OO 0.929 1 2 49.94 0.19 O.OOE+OO l.1 7E+Ol 1. 097 1 2 99.14 1. 63 -4.27E-02 5.55E+OO 0.944 1408.01 2 1. 07 4.69E-02 3.45E-01 0.983 1 457.64 0.50 -1.74E+Ol 2.93E+O l 1. 076 1528.10 0.2 8 3.65E+OO 2.68E+Ol 1.007 + Eu-154 1 2 3.07 40.40 6.60E-02 1.80E-01 l.80E-01 0.934 247.93 6.89 8.24E-0 2 7.07E-01 0.928 591.76 4.95 O.OOE+OO 3.23E-01 0. 915 692.42 1. 78 -5.22E-01 3.89E+OO 0.936 723.30 2 0.0 6 :.75E-02 2.43E-01 0.935 756.80 4.5 2 6.17E-01 1.85E+OO 0.915 873.18 12.08 -5.20E-02 4.59E-01 0.932 996.29 10.48 8.40E-02 8.14E-Ol 0.971 1004.76 18.01 8.30E-0 2 4.73E-01 0.978 1274.43 34.80 1. 51E-0 2 l.95E-01 0.981 1 596.48 1. 80 O.OOE+OO l.37E+OO 1.1 75 + Eu-155 45.30 1. 31 -l.16E+Ol 3.56E-01 2.33E+Ol 0.99~ 60.01 1. 2 2 1.69E+Ol 4.15E+Ol 1.000 86.55 30.70 -9.89E-02 3.56E-01 free 105.31 2 1.10 1.70E-01 4.llE-01 1. 000 + Tl-208 583.19 85.00 1. 33E-01 l.65E-01 l.65E-01 0.932 + Bi-211 351.07

13.02 9.72E-01 5.02E-01 5.02E-01 miss + Pb-2 11 404.85 3.78 2.28E-01 1.44E+OO l.44E+OO miss 10/10/2016 10:08:11AM Page 6 of7 Analysis Report for 10-0ct-16-10008 L3-10219A-FRGS-006SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 5.45E-01 1.44E+OO 3.67E+OO miss 832.01 3.52 4.18E-01 2.32E+OO miss + Bi-212 39.86 1. 06 1.17E+Ol 1.58E+OO 4.66E+Ol 0.998 727. 33 6.67 5.05E-01 1.58E+OO 0.98 2 785.37 1.10 1.19E+OO 6.76E+OO 0.944 1620.50 1. 47 1.83E-01 5.38E+OO 1. 006 + Pb-212 115 .18 0.60 -~.44E+00 2.05E-0 1 9.30E+OO miss 238.63

43.60 2.62E-01 2.05E-01 free 300.09 3.30 7.97E-01 1.94E+OO free + Pb212-XR 74.82 10.28 3.40E-0 2 1. 22E+OO 1.69E+OO miss 77. 11 17.10 6.2 8E-01 1.22E+OO miss 87.35 3.97 1.3 5E+OO 3.00E+OO miss 89.78 1. 46 5.86E+OO 8.46E+OO miss + Bi-214 609.32

45.49 3.34E-01 1.31E-0 1 l.31E-01 0.948 768.36 4.89 1.40E-01 1.50E+OO 0.942 806.18 1. 2 6 O.OOE+OO 1.54E+OO 0.923 934.06 3.11 1. llE-01 2.70E+OO 0.944 1120.29 14.9 2 5.39E-01 1.07E+OO 0.944 1155.2 1 1. 63 -7.07E-01 5.92E+OO 0.943 1238.12 5.83 6.44E-01 2. llE+OO 0.944 1280.98 1. 43 -1.05E+OO 6.22E+OO 0.944 1377. 67 3.99 4.65E-01 2.16E+OO 1. 030 1385. 31 0.79 1.83E-01 9.42E+OO 0.945 1401. 52 1. JJ 7.70E-01 5.67E+OO 0.945 1407.99 2.39 4.29E-01 3.16E+OO 0.945 1509.2 1 2 .13 O.OOE+OO l.37E+OO 0.950 1661.2 7 1. 05 O.OOE+OO 2.85E+OO 1. 001 1729.59 2.88 1.77E+00 4.63E+OO 1.119 1764.49 15.30 4.18E-01 l .13E+OO 1. 001 1 847.43 2.03 5.53E-01 4.07E+OO 1. 063 > 2 118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 14 241.99 7.2 5 4.90E-01 1.84E-01 9.81E-01 1. 000 295.22 18.42 4.25E-01 4.90E-01 1. 000 351.93

35.60 3.55E-01 1.84E-01 free 785.96 1. 06 7.19E-01 6.64E+OO 1. 000 + Pb214-XR 74.8 2 5.80 6.02E-0 2 2.14E+OO 3.00E+OO miss 77 .11 9.70 1. llE+OO 2.14E+OO miss 87.35 2.24 2.40E+OO 5.32E+OO miss 89.78 0.82 1.04E+Ol 1.51E+Ol miss + Ra-226 186.21 3.64 1.16E+OO 1.90E+OO 1.90E+OO free + Ac-228 129.07 2.42 5.91E-01 4.93E-01 2.48E+OO 0.944 209.25 3.89 4.74E-01 1.63E+OO 0.978 270.24 3.46 4.56E-01 2.05E+OO 0.955 328.00 2.95 1.27E-01 1. 53E+OO 0.955 338.32 11. 27 3.43E-01 6.79E-01 0.992 409.46 1. 92 1.22E+OO 3.87E+OO 0.937 463.00 4.40 1.39E-01 1.33E+OO 0.933 794.95 4.25 2.19E-01 1.77E+OO 0.942 911.20 2 5.80 2.65E-01 4.93E-01 0.990 964. 77 4.99 4. 71E-01 2.0lE+OO 0.981 968.97 15.80 2.46E-01 7.2 4E-01 0.990 10/10/2016 10:08:11AM Page 7 of7 Analysis Report for 10-0ct-16-10008 L3-10219A-FRGS-006SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCUgrams) (pCilgrams)

Corr Ac-228 1588.20 3.22 O.OOE+OO 4.93E-01 8.93E-01 1.002 + Pa-231 27.36 1 0.3 0 -l.36E+OO 2.1 9E+OO 4.14E+OO 0.998 283.69 1. 70 -2.41E-01 2.72E+OO 1. 000 300.07 2.47 1.06E+OO 2.59E+OO 1. 000 302.65 2.20 -2.71E-01 2.19E+OO 1. 000 330.06 1. 40 4.55E-01 3.63E+OO 1.000 + Th-234 92.38 2.1 3 ~.90E+OO 5.75E+OO 6.00E+OO free 92. 80 2.10 l.05E+OO 5.75E+OO free 112.81 0.2 1 -8.2 0E+OO 3. 61E+Ol free + U-235 143.76 10.96 -6. 96E-02 l.2 1E-01 5.2 2E-01 free 163.33 5.08 4.55E-01 l.18E+OO free 185.71 57.2 0 7.48E-02 1. 2 1E-Ol free 20 2.11 1. 08 -4.63E-01 3.99E+OO miss 205.31 5.01 -l.36E-02 7.16E-01 free + Am-241 59.54 35.90 -3.56E-01 l.37E+OO 1.37E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Vl C: :=I 60 55 50 45 40 35 8 30 25 1000 2000 3000 0000016064.CNF 4000 channel 5000 Live Time :300.000 sec Real Tille : 300.490 sec start: 1: -0.l(kev) stop : 8192: 2047. O(kev) Acq. Start : Non oct 10 09: 44: 42 2016 6000 7000 8000 10/10/2016 2:47:52PM Analysis Report for 1O-Oct-16-10015 L3-10219A-FRGS-007SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real Time Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Peak Analysis Performed on Peak Analysis From Channel Peak Analysis To Channel : 10-0ct-16-10015

L3-10219A-FRGS-007SS

1 L 130G Soil Sample 1.190E+03 grams : Default : 10/3/2016 9:30:00AM

10/10/2016 2:42:15PM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 300.0 seconds : 300.2 seconds : 0.08% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

6/28/2012

16071 PEAK WITH NID REPORT 10/10/2016 2:47:19PM

120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM

~J<;'{' ... '1=\~-+/-:D \.~ti"LII'-Pagel of7 10/10/2016 2:47:52PM Page 2 of7 Analysis Report for 10-0ct-16-10015 L3-10219A-FRGS-007SS Peak Energy ROI No. (keV) start 1 238.59 948 -2 2 94. 96 1176 -3 352.04 1403 -4 609.2 0 2430 -5 1460.7 3 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1183 1412 2441 5851 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.68 3.08E+Ol 2 0.09 5.24E+Ol 1179.88 7.65E+O O 9.74 1.47E+Ol 1407.94 2.34E+O l 13.46 2.12E+Ol 2435.75 3.33E+Ol 13 .28 9.31E+OO 5842.2 3 9.19E+Ol 20.17 8.26E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

10.66 8.53E+OO 2.0lE+OO Bi-211 0.94 351. 07

13. 02 6.69E-01 3.99E-01 Pb-212 1. 00 115.18 0.60 238.63

43.60 2.03E-0 1 1.36E-01 300.0 9 3.3 0 Bi-214 0.82 609.32

45.49 4.0 lE-0 1 1.67E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 1 12 0.2 9 14.92 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 13 85. 31 0.79 1 401.52 1. 33 1407.99 2.39 1509.2 1 2 .13 166 1.2 7 1. 05 1729.59 2.88 1764.49 1 5.30 Tentative Nuclide Pb-212 Pb-214 Eu-15 2 Pb-21 4 Bi-211 Bi-214 K-40 Caine Corr miss miss miss miss Analysis Report for 10-0ct-16-10015 L3-10219A-FRGS-007SS Nuclide Name Bi-214 Id Confidence 0.82 Energy (keV) 1847.43 2118.51 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2.03 1.16 miss = Nuclide energy was not found in the coincidence library. 10/10/2016 2:47:52PM Page 3 of7 Activity (pCilgrams)

Activity Uncertainty Caine Corr INTERFERENCE CORRECTED REPORT Nuclid e Name K-40 Bi-211 Pb-21 2 Bi-214 Nuclide Id Confidence 0.999 0.944 1. 000 0.824 X Pb-214 0.998 ? X = = nuclide is part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 8.53E+OO 6.69E-0 1 2.03E-01 4.0lE-01 @ = nuclide c ontains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 2.0lE+OO 3.99E-01 l.36E-01 l.67E-01 10/10/2016 2:47:52PM Analysis Report for 1O-Oct-16-10015

+ + + + + + + + + L3-10219A-FRGS-007SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 2 294. 96 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 2:47:19PM

120 : 8192 Peak Size (CPS) 2.55000E-02 Peak CPS(%) Uncertainty Peak Type Tol. NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL. NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi!grams) (pCilgrams) (pCi!grams)

K-40 1460.8 2

10.6 6 8.53E+OO 1.21E+OO l.21E+OO Cr-51 320.08 9.91 l.2 7E-01 5.95E-01 5.95E-01 Mn-54 834.85 99.98 8.02E-03 7.40E-02 7.40E-02 Co-58 810.76 99.45 -2.39E-03 6.64E-02 6.64E-0 2 1674.73 0.52 O.OOE+OO 6.17E+OO Co-60 1173.23 99.85 l.66E-02 2.51E-02 9.18E-02 1332.49 99.98 O.OOE+OO 2.51E-02 Nb-94 702.65 99.81 l.2 1E-02 6.47E-02 6.50E-02 871.09 99.89 -9.2 9E-03 6.47E-02 Ag-108m 79 .13 6.60 l.16E-01 3.51E-0 2 l.42E+OO 433.94 90.50 -1.34E-02 3.51E-02 614.28 89.80 -1. 59E-02 6.59E-02 722. 94 90.80 1. OlE-02 8.12E-02 Sn-113 2 55.13 2.11 -6.13E-01 9.12E-02 2.09E+OO 391. 70 64.97 7.76E-03 9.12E-0 2 Cs-134 475.36 1. 48 -5.02E-01 8.42E-0 2 2.91E+OO Page 4 of7 Tolerance Nuclide Eu-152 Pb-214 Colnc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss 10/10/2016 2:47:52PM Page 5 of7 Analysis Report for 10-0ct-16-10015 L3-10219A-FRGS-007SS Nuclide Energy Yield{%) Activity NuclideMDA LlneMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCl/grams)

Corr Cs-134 563.25 8.34 3.'75E-02 8.42E-02 6.73E-01 miss 569.33 15.37 O.OOE+OO 9.25E-02 miss 604. 72 97. 6 2 3.85E-03 8.42E-02 miss 795.86 85.46 2.55E-0 2 l.16E-01 miss 801. 95 8.69 l.65E-01 9.16E-01 miss 1038.61 0.99 -l.42E+OO 8.58E+OO miss 1167.97 1. 79 6.80E-02 4.42E+00 miss 1365.19 3.0 2 O.OOE+OO 8.49E-01 miss + Cs-137 661.66 85.10 2.34E-02 9.59E-02 9.59E-0 2 miss + Eu-152 121.78 28.67 -2.37E-0 2 l.2 4E-01 l.34E-01 miss 244.70 7.61 7.04E-0 2 5.41E-01 miss 2 95.94 0.45 4.49E-0 1 l.62E+Ol miss 344.2 8 26.60 5.52E-03 l.48E-01 miss 367.79 0.86 -l.87E+OO 3.28E+OO miss 411.12 2.2 4 l.12E-01 l.73E+OO miss 443. 96 2.83 2.79E-01 2.19E+00 miss 488.68 0.42 -2.24E+OO l.34E+Ol miss 563.99 0.49 O.OOE+OO l.14E+Ol miss 586.26 0.46 l.48E+OO l.52E+Ol miss 678.62 0.47 O.OOE+OO 3.38E+OO miss 688.67 0.86 -1. 96E+OO 6.43E+OO miss 719.35 0.2 8 4.39E+OO 2.36E+O l miss 778.90 12. 96 l.50E-01 5.99E-01 miss 810.45 0.32 2.41E+OO 2.2 3E+Ol miss 867.37 4.26 8.15E-01 2.14E+OO miss 919.33 0.43 -8.17E+OO l.24E+Ol miss 964. 08 14.65 l.2 2E-0 1 6.69E-01 miss 1085.87 10.24 -6.76E-02 7.33E-01 miss 1089.74 1. 73 -l.27E+OO 3.45E+OO miss 1112.07 13.69 O.OOE+OO l.62E-01 miss 1212.95 1. 43 4.26E+OO 9.66E+OO miss 1249.94 0.19 4.69E+OO 4.35E+Ol miss 1 2 99.14 1. 63 -4.79E-01 4.12E+OO miss 1403.01 21. 07 O.OOE+OO 1. 24E-01 miss 1457.64 0.50 -5.06E+OO 2.12E+Ol miss 1528.10 0.2 8 -l.66E+Ol 2.68E+Ol miss + Eu-154 123.07 40.40 2.lOE-02 l.05E-01 l.05E-01 miss 247.93 6.89 5.50E-02 6.43E-01 miss 591.76 4.95 6.51E-02 l.17E+OO miss 692.42 1. 78 2.24E-01 3.62E+OO miss 723.30 2 0.06 l.02E-02 3.68E-01 miss 756.80 4.52 5.42E-01 l.84E+OO miss 873.18 12.08 2.39E-01 7.58E-01 miss 996.29 10.48 O.OOE+OO l.97E-01 miss 1004.76 18.01 -9.96E-02 3.14E-01 miss 1274.43 34.80 3.69E-03 l.90E-01 miss 1 596.48 1. 80 O.OOE+OO l.60E+OO miss + Eu-155 45.30 1. 31 1.50E-01 2.34E-01 l.27E+Ol miss 60.01 1. 22 -3.73E-Ol l.62E+Ol miss 86.55 30.70 l.2 9E-01 3.17E-01 miss 105.31 21.10 -3.2 3E-02 2.34E-01 miss 10/10/2016 2:47:52PM Page 6 of7 Analysis Report for 10-0ct-16-10015 L3-10219A-FRGS-007SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCUgrams) (pCi/grams)

Corr + Tl-208 583.19 85.00 6.88E-02 1. 33E-01 l.33E-01 miss + Bi-211 351.07

13.02 6.69E-01 5.17E-01 5.17E-01 miss + Pb-211 404.85 3.78 -6.53E-02 1.1 7E+OO l.1 7E+OO miss 427.09 1. 76 -3.88E-01 2.25E+OO miss 832.01 3.5 2 -1.60E-01 1.41E+OO miss + Bi-212 39.86 1. 06 -4.25E+OO 1.21E+OO 1.03E+Ol miss 727. 33 6.67 2.71E-01 1.2 1E+OO miss 785.37 1.10 -6.87E-01 7.07E+OO miss 1620.50 1. 47 O.OOE+OO l.97E+OO miss + Pb-212 115 .18 0.60 -2.0lE+OO 1.99E-01 7.54E+OO miss 238.63

43.60 2.03E-01 l.99E-01 miss 300.09 3.30 5.57E-01 1.77E+OO miss + Pb212-XR 74.82 10.28 6.83E-01 9.48 E-01 1.54E+OO miss 77 .11 17.10 7.34E-01 9.48E-01 miss 87.35 3.97 7.57E-01 2.2 0E+OO miss 89.78 1. 46 2.40E+OO 5.62E+OO miss + Bi-2 1 4 609.32

45.49 4.0lE-01 1.62E-0 1 l.62E-01 miss 768.36 4.89 -1.67E-01 1.41E+OO miss 806.1 8 1. 2 6 O.OOE+OO 1.41E+OO miss 934.06 3.11 1.34E+00 3.53E+OO miss 1120.29 14.9 2 6.22E-01 l.04E+OO miss 1155.21 1. 63 -2.21E-0 1 6.18E+OO miss 1238.12 5.83 2.15E-02 l.40E+OO m i ss 1280.98 1. 43 -2.24E+OO 5.83E+OO miss 1377. 67 3.99 2.37E-01 1.75E+OO miss 1385. 31 0.79 -1.03E+OO 8.82E+OO miss 140 1. 52 1. 33 O.OOE+OO l.95E+OO miss 1407.99 2.39 O.OOE+OO 1. 09E+OO miss 1509.21 2 .13 O.OOE+OO l.2 9E+OO miss 1661. 27 1. 0 5 O.OOE+OO 2.83E+OO miss 1 729.59 2.88 3.92E-01 2.88E+OO miss 1 764.49 15.30 O.OOE+OO 2.03E-01 miss 1847.43 2.03 7.64E-01 5.41E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-2 14 2 41.99 7.25 1.77E-01 1.89E-01 8.51E-01 miss 2 95.22

18.42 1.37E-01 2.85E-01 miss 351.93

35.60 2.45E-01 1.89E-01 miss 785. 96 1. 06 -3.32E-01 7.36E+OO miss + Pb214-XR 74.8 2 5.80 1.21E+OO 1.67E+OO 2.73E+OO miss 77 .11 9.70 l.29E+OO l.67E+OO miss 87.3 5 2.24 1. 34E+OO 3.90E+OO miss 89. 78 0.82 4.'.2 7E+OO l.OOE+Ol miss + Ra-226 186.21 3.64 3.16E-01 1.43E+OO 1. 43E+OO miss + Ac-2 2 8 129.07 2.42 6.49E-02 5.94E-01 1.95E+OO miss 209.25 3.89 4.95E-01 l.43E+OO miss 270.24 3.46 8.03E-01 l.97E+OO miss 328.00 2.95 2.71E-01 1.44E+OO miss 338.32 11.27 3.27E-01 7.39E-01 miss 409.46 1. 92 1.73E-01 1. 59E+OO miss 463.00 4.40 2.05E-02 l.45E+OO miss 10/10/2016 2:47:52PM Page 7 of7 Analysis Report for 10-0ct-16-10015 L3-10219A-FRGS-007SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Corr Ac-228 794.95 4.25 3.85E-01 5.94E-01 2.02E+OO mis s 911.20 25.80 4.22E-01 5.94E-01 mis s 964.77 4.99 4.99E-0 2 l.80E+OO miss 968.97 15.80 l.58E-01 6.22E-01 miss 1588.20 3.22 9.37E-02 2. 41E+OO miss + Pa-23 1 2 7.36 10.30 O.OOE+OO 3.09E-01 3.09E-01 miss 283.69 1. 70 2.68E-01 2.67E+OO miss 300.07 2.47 7.45E-Ol 2.36E+OO miss 302.65 2.20 8.60E-01 2.43E+OO miss 330.06 1. 40 -8.2 7E-01 2.3 6E+OO mis s + Th-234 92.38 2.1 3 2.61E+OO 5.0 9E+OO 5.09E+OO miss 92.80 2.10 2.80E+OO 5.13E+OO miss 112. 81 0.2 1 -4.62E-01 3.25E+Ol miss + U-23 5 143.76 10.96 2.24E-02 8.2 6E-02 3. 91E-01 miss 163.33 5.08 -9.93E-02 6.3 5E-01 miss 1 85.71 57.2 0 -l.lOE-03 8.2 6E-02 miss 202 .11 1. 08 1.18E+OO 4.58E+OO miss 205.31 5.01 -2. llE-01 7.45E-01 miss + Am-241 59.54 35.90 2.02E-01 6.1 5E-01 6.15E-01 miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V, ..... C: :::J 60 55 50 45 40 35 8 30 25 1000 2000 3000 0000016071.CNF 4000 channel 5000 Live Time :300.000 sec Real Tfae : 300. 240 sec start: 1: -0.2(kev) stop : 8192:2047.4(kev)

Acq. Start :MOn oct 10 1-i:42:15 2016 6000 7000 8000 10/10/2016 3:06:11PM Analysis Report for 10-0ct-16-10016 L3-10219A-FRGS-008SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 10-0ct-16-10016

L3-10219A-FRGS-008SS

1 L 130G Soil Sample 1.161E+03 grams : Default : 10/3/2016 9:55:00AM

10/10/2016 2:42:27PM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.16 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM : 1/27/2016

1/5/2015 : 16072 PEAK WITH NID REPORT Peak Analysis Performed on 10/10/2016 2:47:58PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce "?~" ~o....\~ J:-.D \<:>/\7-(fi., : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of7 A~alysis Report for 10-0ct-16-10016 L3-10219A-FRGS-008SS Peak Energy ROI No. (keV) start 1 238.61 948 -2 294.98 1177 -3 35 1.84 1401 -4 608.94 2429 -5 1460.19 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 959 1184 1411 2441 5850 10/10/2016 3:06:11PM Peak Net Peak Net Area Centroid Area Uncertainty 954.95 5.25E+Ol 18.56 1180. 25 1. 31E+Ol 11. 83 1407.53 3.42E+Ol 14.52 2 435.51 3.14E+Ol 13.74 5841. 72 7.67E+Ol 17.85 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 2.69E+Ol Pb-212 2.18E+Ol Pb-214 Eu-152 l.76E+Ol Pb-214 Bi-211 l.32E+Ol Bi-214 2.52E+OO K-40 Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.97 1460.82

10.66 8.llE+OO 2.0lE+OO miss Pb-212 1. 00 115 .18 0.60 238.63

43.60 3.99E-01 1.55E-01 free 300.09 3.30 Bi-214 0.99 609.32

45.49 4.62E-01 2.lOE-01 0.948 768.36 4.89 806.18 1. 26 934.06 3.11 1120.2 9 14.92 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385.31 0.79 1401.5 2 1. 33 1407.99 2.39 1509.2 1 2.13 1661. 27 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 Analysis Report for 10-0ct-16-10016 L3-10219A-FRGS-008SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 2118. 51 Pb-214 0.99 241. 99 295.22 351.93 785.96 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1.16 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/10/2016 3:06:11PM Page 3 of7 Activity Activity Caine (pCi/grams)

Uncertainty Corr 2.70E-01 2.47E-01 1. 000 4.07E-01 1.85E-01 free INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Nuclide Id Confidence 0.976 X Bi-211 0. 965 ? = X = Pb-212 Bi-214 Pb-214 1. 000 0. 996 0.999 nuclide is part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 8.llE+OO 3.99E-01 4.62E-01 3.58E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 2.0lE+OO 1.55E-01 2.lOE-01 1.48E-01 10/10/2016 3:06:11PM Page 4 of7 Analysis Report for 10-0ct-16-10016

+ + + + + + + + + L3-10219A-FRGS-008SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 2:47:58PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keVj (.oCl/grams) (pCilgrams) (pCl/grams)

Corr K-40 1460.8 2

10.6 6 8.llE+OO 8.76E-01 8.76E-01 miss Cr-51 320.08 9.91 -1.42E-01 6.32E-01 6.32E-01 free Mn-54 834.85 99.98 1. 56E-0 2 7.25E-02 7.25E-02 miss Co-58 810.76 99.45 1.54E-02 8.75E-0 2 8.75E-02 1.000 1674.7 3 0.52 O.OOE+OO 6.86E+OO 1. 024 Co-60 1173.23 99.85 -1.76E-02 9.51E-02 9.51E-0 2 0.947 1332.49 99.98 7.95E-03 1. 03E-01 0.947 Nb-94 702.65 99.81 -9.08E-03 6.75E-02 6.75E-02 0.944 871.09 99.89 2.51E-02 9.02E-02 0.944 Ag-10 8m 79.13 6.60 6.14E-Ol 7.29E-02 2.70E+OO miss 433.94 90.50 2.61E-02 8.64E-02 0.887 614.28 89.80 1.57E-02 7.29E-0 2 0.886 722. 94 90.80 -5.78E-03 9.33E-02 0.887 Sn-113 2 55 .13 2 .11 -1.06E+OO 8.84E-02 2.98E+OO free 391. 70 64.97 -3.02E-02 8.84E-02 free Cs-134 475.36 1. 48 4.64E-01 7.37E-02 4.29E+OO miss 563.25 8.34 3.02E-01 1.12E+OO 0.896 569.33 15.37 -8.75E-0 3 4.06E-01 0.888 604. 72 97.62 7.76E-0 3 7.37E-0 2 0.931 10/10/2016 3:06:11PM P age 5 of7 Analysis Report for 1 O-Oct-16-10016 L3-10219A-FRGS-008SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCUgrams) (pCi/grams)

Corr Cs-134 '"195. 86 85.46 1.67E-02 7.37E-0 2 1.0lE-01 o.~33 80 1.95 8.69 -8.04E-02 7.lOE-01 0.898 1038.61 0.99 O.O OE+OO 2.60E+OO 0.943 116 7.97 1. 79 -1. 79E-01 4.65E+OO 1. 081 1365.1 9 3.0 2 9.50E-01 3.41E+OO 1.128 + Cs-137 661.66 85.10 6.96E-02 1.2 9E-01 1.29E-01 miss + Eu-1 52 121.78 2 8.67 -4.56E-02 l.43E-01 l.94E-01 0.936 244.70 7.61 4.44E-01 9.81E-01 0.935 295.94 0.45 1.02E+OO 2.08E+Ol miss 344.28 2 6.60 -3.2 9E-0 3 1.97E-01 0.957 367.79 0.86 2.87E-01 8.lOE+OO 0.884 411.12 2.24 1.71E-01 2.51E+OO 0.908 443.96 2.83 2.08E-01 2.2 7E+OO 0.934 488.68 0.4 2 1. 27E+OO 9.36E+OO miss 563.99 0.49 7.24E+OO 1.93E+Ol 0.934 586.2 6 0. 46 5.59E-01 1.68E+Ol 0.94 2 61 8.62 0.47 4.1 8E+OO 1. 72E+Ol 0.88 7 688.67 0.86 O.O OE+OO 2.17E+OO 0.980 7 1 9.35 0.2 8 1.25E+OO 2.69E+Ol miss 773. 90 12.96 -2.00E-02 4.41E-01 0.945 8 10.45 0.3 2 -2.24E+OO 2.08E+Ol 1. 050 8 67. 37 4.26 -2.00E-01 2.15E+OO 0.928 919.33 0.43 8.82E+OO 2.57E+Ol 0.981 964.08 14.65 2.42E-01 7.43E-01 1. 022 1085.87 J O. 2 4 2.1 8E-Ol 9. 49E--01 1.018 1089.74 1. 7 3 1.20E+OO 6.02E+OO 0.952 1112.07 13.69 9.82E-03 6.38E-01 0.992 1212.95 1. 43 -2 .13E-01 5.49E+OO 0. 929 1249.94 0.19 O.OOE+OO l.32E+Ol 1. 097 1299.1 4 1. 63 O.OOE+OO 1.83E+OO 0.944 1408.0 1 2 1.07 O.OOE+OO l.43E-01 0.983 1457.64 0.50 -3.75E+Ol 4.06E+Ol 1. 076 1528.10 0.2 8 O.OOE+OO 1.11E+Ol 1.007 + Eu-154 123.07 40.40 -4.75E-02 l.44E-0 1 1.44E-01 0.934 247.93 6.89 1.65E-01 9.2 6E-01 0.928 591.76 4.95 -2.69E-02 1.62E+OO 0.915 692.4 2 1. 78 4.08E-01 3.79E+OO 0.936 72 3. 30 2 0.0 6 5.59E-0 2 4.47E-01 0.935 756.80 4.52 3.48E-01 l.62E+OO 0.915 873.18 12.08 4.70E-02 5.18E-01 0.932 996.29 10.48 O.OOE+OO 2.31E-01 0.971 1004.76 18.01 5.79E-02 5.3 4E-01 0.978 1274.4 3 34.80 -1.37E-01 2.78E-01 0.981 1596.48 1. 80 O.OOE+OO 1.55E+OO 1.175 + Eu-155 45.30 1. 31 -9.43E+OO 4.14E-01 4.44E+Ol 0.999 60.01 1. 22 -4.43E+OO 4.15E+Ol 1.000 86.55 3 0.70 1.15E-01 4.14E-01 free 105.31 2 1.10 2.77E-0 1 4.74E-01 1. 000 + Tl-208 583.19 85.00 5.27E-02 1.67E-01 1.67E-01 0.932 + Bi-211 351.07

13.02 1.11E+OO 5.49E-01 5.49E-O l miss + Pb-211 404.85 3.78 -2.97E-01 1.15E+OO l.15E+OO miss 10/10/2016 3:06:11PM Page 6 of7 Ar;ialysis Report for 10-0ct-16-10016 L3-10219A-FRGS-008SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCVgrams) (pCilgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 -1.66E-01 1.15E+OO 2.97E+OO miss 832.01 3.5 2 -5.81E-01 1.60E+OO miss + Bi-212 39.86 1. 06 -2.69E+OO 1.40E+OO 4.26E+Ol 0.998 727. 33 6.67 4.53E-01 1.40E+OO 0.98 2 785.37 1.10 2.36E-01 8.52E+OO 0.944 1620.50 1. 47 O.OOE+OO 2.24E+OO 1. 006 + Pb-21 2 115.18 0.60 3.51E-01 1.65E-01 1.25E+Ol miss 238.63

43.60 3.99E-01 1.65E-01 free 300.09 3.30 3.92E-01 1.64E+OO free + Pb'.212-XR 74.82 10.28 1.97E+OO 1. 37E+OO 2.84E+OO miss 77.11 17.10 3.38E-01 1.37E+OO miss 87.35 3.97 8.48E-01 3.23E+OO miss 89.78 1. 46 8.45E-01 8.45E+OO mis s + Bi-214 609.32

45.49 4.62E-01 2.28E-01 2.28E-01 0.948 768.36 4.89 -1.31E-02 1.46E+OO 0.94 2 806.18 1. 2 6 -6.97E-01 5.97E+OO 0.923 934.06 3.11 4.25E-01 2.63E+OO 0.944 11 2 0.2 9 14. 9 2 1.79E-01 9.99E-01 0.944 1155.2 1 1. 63 -2.39E+OO 5.76E+OO 0.94 3 1238.12 5.83 9.17E-0 1 2.56E+OO 0.944 1 2 80.98 1. 43 1.08E-01 7.02E+OO 0.944 1377. 67 3.99 2.62E-01 1.93E+OO 1. 030 1385. 31 0.79 1.45E+OO 1.06E+Ol 0.945 1401. 52 1. 33 8.69E-01 6.40E+OO 0.945 1407.99 2.39 O.OOE+OO 1. 31E+OO 0.945 1509.2 1 2.13 O.OOE+OO 1. 55E+OO 0.950 1 661.27 1. 0 5 1.19E+OO 8.75E+OO 1. 001 1 729.59 2.88 O.OOE+OO 1.08E+OO 1.119 1764.49 15.30 4.2 6E-01 l.12E+OO 1.001 1 847.43 2.03 O.OOE+OO 1.69E+OO 1. 063 > 2 118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-21 4 241. 99 7.25 4.95E-01 2.0lE-01 l.13E+OO 1. 000 2 95.22

18.42 2.70E-01 3.72E-01 1. 000 351.93

35.60 4.07E-01 2.0lE-01 free 7 85.96 1. 06 9.86E-01 8.36E+OO 1. 000 + Pb214-XR 74.82 5.80 3.49E+OO 2.42E+OO 5.03E+OO miss 77 .11 9.70 5.95E-01 2.42E+OO miss 87.35 2.2 4 1. 50E+OO 5.73E+00 miss 89.78 0.82 1. 51E+OO 1.51E+Ol miss + Ra-226 186.2 1 3.64 9.53E-01 1.91E+OO 1.91E+OO free + Ac-228 129.0 7 2.42 7.37E-01 5.33E-01 3.35E+OO 0.944 209.25 3.89 -8.95E-02 1. 30E+OO 0.978 270.24 3.46 -4.47E-01 2.18E+OO 0.955 328.00 2.95 1.44E-02 2.03E+OO .o. 955 338.32 11. 2 7 2.04E-01 5.87E-01 0.992 409.46 1. 92 l.40E-01 2.83E+OO 0.937 463.00 4.40 -3.13E-01 l.16E+OO 0.933 7 94. 95 4.25 5.34E-01 2.23E+OO 0.942 911. 20 25.80 1.85E-01 5.33E-Ol 0.990 964.77 4.99 2.lOE-0 1 2.08E+OO 0.981 968.97 1 5.80 1.2 7E-01 7.67E-01 0.990 10/10/2016 3:06:11PM Page 7 of7 Analysis Report for 10-0ct-16-10016 L3-10219A-FRGS-008SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pC//grams) (pCilgrams)

Corr Ac-228 1588.2 0 3.22 l.12E+OO 5.33E-01 4.0lE+OO 1. 002 + Pa-231 27.36 10.30 2.85E+OO 2.19E+OO 6.06E+OO 0.998 2 83.69 1.70 -l.05E+OO 2.61E+OO 1. 000 300.07 2.47 5.23E-01 2.19E+OO 1.000 302.65 2.2 0 6.57E-01 2.47E+OO 1. 000 330.06 1. 40 3.16E-01 4.36E+OO 1. 000 + Th-234 92.38 2.13 3.04E+OO 7.69E+OO 7.69E+OO free 92.80 2.10 5.04E+OO 7.88E+OO free 112. 81 0.21 7.98E+OO 4.24E+Ol free + U-235 143.76 10. 96 l.84E-0 2 l.16E-01 5.73E-01 free 163.33 5.08 -3.63E-02 l.09E+OO free 185. 71 57.20 3.43E-02 l.16E-01 free 202 .11 1. 08 -2.15E+OO 4.2GE+OO miss 205.31 5.01 3.34E-01 l.16E+OO free + Am-241 59.54 35.90 -8.87E-02 l.41E+OO l.41E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Vl C: ::::, 60 55 50 45 40 35 8 30 25 20 15 .... i, 1000 2000 3000 0000016072.CNF 4000 channel Live Time :300.000 sec Real Time : 300.480 sec start: 1: -0 .1 (kev) stop : 8192 :2047 .O(kev) Acq. Start :Mon Oct 10 14:42:27 2016 6000 7000 8000 10/11/2016 7:01:52AM

~pex-Gamma Analysis Report for 11-0ct-16-10002 L 3-10219A-FRGS-009SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 11-0ct-16-10002

L3-10219A-FRGS-009SS

1 L 130G Soil Sample 1.198E+03 grams : Default : 10/3/2016 10:00: 00AM : 10/11/2016 6:38:33AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.15 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM : 1/27/2016

1/5/2015 : 16080 PEAK WITH NID REPORT Peak Analysis Performed on 10/11/2016 6:43:37AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of7 10/11/2016 7:01: 52AM Page 2 of7 Analysis Report for 11-0ct-16-10002 L3-10219A-FRGS-009SS Peak Energy ROI No. (keV) start 1 238.63 950 -2 295.23 1176 -3 351.69 1401 -4 609.02 2430 -5 1460.58 5835 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma ROI end 960 1185 1416 2443 5853 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 955.02 l.79E+Ol 20.53 7.23E+Ol 1181.24 1.80E+Ol 12.76 1. 99E+Ol 1406.96 7.26E+Ol 18.93 1.28E+Ol 2435.81 4.42E+01 14.2 7 5.60E+OO 5843.30 8.08E+Ol 18.2 7 2.36E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION UB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.8 2

10.66 8.28E+OO 2.0lE+OO Bi-211 0.97 351.07

13. 02 2.29E+O O 7.02E-01 Pb-21 2 1. 00 11 5 .18 0.60 238.63

43.60 l.31E-01 1. 53E-01 300.09 3.30 Bi-214 0.99 609.32

45.49 6.31E-01 2.17E-01 768.36 4.89 806.1 8 1. 2 6 934.0 6 3.11 1120.2 9 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 Tentative Nuclide Pb-212 Pb-214 Eu-152 Pb-2 14 Bi-2 11 Bi-214 K-40 Coinc Corr miss miss free 0.948 Analysis Report for 11-0ct-16-10002 L 3-10219A-FRGS-009SS Nuclide Id Energy Name Confidence (keV) Bi-2 1 4 0.99 1847.43 2118.51 Pb-2 1 4 0.99 241. 99 295.22 351.93 785. 96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required. Yield(%) 2.03 1.16 7.25 1 8.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/11/2016 7:01:52AM Page 3 of7 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 3.60E-01 2.61E-01 1. 000 8.37E-01 2.56E-01 free INTERFERENCE CORRECTED REPORT ? = X = Nuclide Name K-40 Bi-211 Pb-21 2 Bi-214 Pb-214 Nuclide Id Confidence 0.997 0.976 1. 000 0.998 0.998 nuclide is part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCUgrams) 8.28E+OO 1. 31E+OO 1.31E-01 6.31E-01 3.60E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 2.0lE+OO 1. OOE+OO 1.53E-01 2 .17E-01 2.61E-01 10/11/2016 7:01 :52AM Page 4 of7 Analysis Report for 11-0ct-16-10002

+ + + + + + + + + L 3-10219A-FRGS-009SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/11/2016 6:43: 37AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCl/grams) (pCilgrams)

Corr K-40 1460.8 2

10.6 6 8.28E+OO 8.20E-01 8.20E-01 miss Cr-51 320.08 9. 91 -1.04E-01 7.92E-01 7.92E-01 free Mn-54 834.85 99.98 -2.53E-03 7.04E-02 7.04E-02 miss Co-58 81 0.76 99.45 -1. 32E-02 7.36E-02 7.36E""'."02

1. 000 1674.73 0.5 2 O.OOE+OO 6.69E+OO 1. 024 Co-60 1173.23 99.85 -2 .13E-02 7.30E-02 7.30E-02 0.947 1332.49 99.98 6.17E-03 1.00E-01 0.94 7 Nb-94 702.65 99.81 -9.78E-03 7.54E-02 7.58E-02 0.944 871.09 99.89 -1.49E-0 2 7.54E-02 0.944 Ag-108m 79.13 6.60 8.60E-01 5.51E-02 2.54E+OO miss 433.94 90.50 -3.74E-02 5.51E-02 0.887 614.28 89.80 1.52E-02 7.07E-02 0.88 6 722. 94 90.80 -5.60E-03 6.18E-02 0.887 Sn-113 2 55 .13 2.11 -1.SOE+OO

7. 71E-02 2.77E+OO free 391.7 0 64.97 -3.lSE-0 2 7.71E-02 free Cs-134 475.36 1. 48 -2.15E+OO 6.17E-02 2.55E+OO miss 563.25 8.34 2.68E-0 1 1.0lE+OO 0.896 569.33 15.37 1.75E-01 5.56E-01 0.888 604. 72 97.62 -1.33E-03 6.17E-0 2 0.931 10/11/2016 7:01:52AM Page 5 of7 Analysis Report for 11-0ct-16-10002 L3-10219A-FRGS-009SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCl/grams) (pCilgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 5.04E-02 6.17E-02 1.2 8E-01 0.933 801.95 8.69 1.56E-0 2 6.88E-01 0.898 1038.61 0.99 1.63E+OO 8.66E+OO 0.94 3 1167. 97 1. 79 6.2 4E-01 5.83E+OO 1.081 1365.19 3.0 2 O.OOE+OO 8.31E-01 1.128 + Cs-137 661.66 85.10 1. 37E-02 9.82E-02 9.82E-02 miss + Eu-152 121.78 28.67 -6.08E-02 1.48E-01 2.39E-01 0.936 244.70 7.61 -1.87E-01 6.47E-01 0.935 295. 94 0.45 -2.67E+OO 2.25E+Ol miss 344.2 8 2 6.60 -6.85E-02 1.48E-01 0.957 367.79 0.86 7.05E-01 7.85E+OO 0.884 411.12 2.2 4 -7.69E-01 2.lOE+OO 0.908 443. 96 2.83 8.07E-02 2.40E+OO 0.934 488.68 0.42 -7.40E-01 l.33E+Ol miss 563.99 0.49 1.12E+OO 1.50E+Ol 0.934 586.26 0.46 7.59E+OO 2.04E+Ol 0.94 2 678.62 0.47 2.58E-01 1.44E+Ol 0.887 688.67 0.86 1. 43E+OO 8.38E+OO 0.980 719.35 0.28 8.54E+OO 3.17E+Ol miss 778.90 12. 96 O.OOE+OO 4.27E-01 0.945 810.45 0.32 -8.67E+OO 1.60E+Ol 1.050 867.37 4.26 3.23E-02 1.80E+OO 0.928 919.33 0.43 3.17E-01 1.40E+Ol 0.981 964.08 14.65 -8.24E-0 2 5.lO E-01 1.02 2 1085.87 10.24 -1.22E-0 2 7.94E-01 1. 018 1089.74 1. 73 9.30E-0 1 5.04E+00 0.95 2 11 12.07 13.69 4.76E-02 4.90E-01 0.99 2 1 212.95 1. 43 -6.20E-01 5.32E+OO 0.929 1 2 49.94 0.19 -1.55E+Ol 4.38E+Ol 1. 097 1299.14 1. 63 4.67E-02 6.07E+OO 0.944 1408.01 21. 07 5 .13E-02 5.53E-01 0.983 1457.64 0.50 -3.03E+Ol 3.03E+Ol 1. 076 1528.10 0.28 3.99E+OO 2.94E+Ol 1.007 + Eu-154 1 2 3.07 40.40 -8.68E-03 7.85E-02 l.69E-01 0.934 2 47.93 6.89 -1.2 7E-01 7.74E-01 0.928 591. 7 6 4.95 O.OOE+OO 3.53E-0 1 0.915 692.42 1. 78 7.25E-01 4.75E+OO 0.936 723. 30 20.06 O.OOE+OO 2.66E-01 0.935 756.80 4.52 -5.06E-01 1.57E+OO 0.915 873.18 12.08 2.84E-Ol 9.63E-01 0.932 996.2 9 10.48 7.35E-0 2 8.91E-01 0.971 1 004.76 18.01 O.OOE+OO 1.30E-01 0.978 1 274.43 34.80 O.OOE+OO 7.85E-02 0.981 1 596.48 1. 80 O.OOE+OO 1. 50E+OO 1.175 + Eu-155 45.30 1. 31 -5.94E+OO 4.42E-01 5.06E+Ol 0.999 60.01 1. 22 -6.44E-01 5.00E+Ol 1. 000 86.55 30.70 6.43E-0 2 4.42E-01 free 105.31 21.10 8.92E-0 3 4.50E-01 1. 000 + Tl-208 583.19 85.00 9.02E-02 1.44E-01 1.44E-01 0.932 + Bi-211 351.07

1 3.02 2.29E+OO 5 .13E-01 5 .13E-01 mis s + Pb-211 404.85 3.78 4.08E-01 5.71E-01 1.91E+OO miss 10/11/2016 7:01:52AM Page 6 of7 Analysis Report for 11-0ct-16-10002 L3-10219A-FRGS-009SS Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCi/grams) (pCilgrams)

Corr Pb-211 427.09 1. 76 8.03E-01 5. 71E-01 3.51E+OO miss 832.01 3.52 O.OOE+OO 5.71E-01 miss + Bi-21 2 39.86 1. 06 -4.18E+OO 1.12 E+OO 4.40E+Ol 0.998 727. 33 6.67 3.46E-02 1.12E+OO 0.98 2 785.37 1.10 1.15E-01 6.38E+OO 0.944 1 620.50 1. 47 1.60E+OO 7.43E+OO 1. 006 + Pb-212 115 .18 0.60 1.59E+OO 2.47E-0 1 1. 2 4E+Ol miss 238.63

43.60 1.31E-01 2.47E-01 free 300.0 9 3.30 7.31E-01 2.04E+OO free + Pb212-XR 74.8 2 10.28 -1.51E-02 l.46E+OO 2.29E+OO miss 77 .11 17.10 7.0lE-01 1.46E+OO miss 87.3 5 3.97 2.41E+OO 3.63E+OO miss 89.78 1. 46 5.65E+OO 9.90E+OO miss + Bi-2 1 4 609.32

45.49 6.31E-01 1. 57E-01 1.57E-01 0.948 768.36 4.89 3.74E-01 2.15E+OO 0.94 2 806.18 1. 26 O.OOE+OO 1.69E+OO 0.923 934.06 3.11 1.46E+OO 3.87E+OO 0.944 11 20.2 9 14.9 2 8.47E-01 1.34E+OO 0.944 11 55.2 1 1. 63 5.16E-01 5.59E+OO 0.943 1 2 38.12 5.83 1.14E+OO 2.93E+OO 0.944 1280.98 1. 43 7.33E-0 1 5.39E+OO 0.944 1377. 67 3.99 6.05E-02 2.74E+OO 1. 030 1385.31 0.79 1.40E+OO 1.03E+01 0.945 1401.52 1. 33 1.2 0E-01 7.82E+OO 0.945 1407.99 2.39 4.70E-0 1 5.06E+00 0.945 1509.2 1 2.13 7.SlE-01 5.14E+OO 0.950 1661. 27 1. 05 O.OOE+OO 3.12E+OO 1.001 1 729.59 2.88 O.OOE+OO 1. O S E+OO 1.119 1764.49 15.30 6.66E-01 1.38E+OO 1. 001 1847.43 2.03 1.0lE+OO 6.SlE+OO 1.063 > 2118.51 1.16 O.OOE+OO O.OOE+OO 1.041 + Pb-2 14 2 4 1.99 7.25 9.37E-01 l.88E-01 1.33E+OO 1. 000 295.22

1 8.42 3.60E-01 3.66E-01 1. 000 351.93

35.60 8.37E-01 1.88E-01 free 785.96 1. 06 2.70E+OO 8.lOE+OO 1. 000 + Pb214-XR 74.82 5.80 -2.68E-02 2.57E+OO 4.07E+OO miss 77 .11 9.70 1.24E+OO 2.57E+OO miss 87.35 2.24 4.28E+OO 6.43E+OO miss 89.78 0.82 1. OlE+Ol 1.76E+01 miss + Ra-226 186.2 1 3.64 8.64E-01 2.04E+OO 2.04E+OO free + Ac-228 129.07 2.42 -5.87E-01 3.33E-01 2.72E+OO 0.944 209.25 3.89 -1.44E-02 1.44E+OO 0.978 270.24 3.46 3.94E-01 2.18E+OO 0.955 328.00 2.95 6.51E-02 1.50E+00 0.955 338.32 11. 2 7 1.85E-01 6.98E-01 0.992 409.46 1. 92 6.51E-01 3.34E+OO 0.937 463.00 4.40 4.07E-01 1.93E+OO 0.933 794.95 4.25 8.91E-0 1 2.70E+OO 0.942 911.2 0 2 5.80 3.61E-02 3.33E-01 0.990 964. 77 4.99 5.2 5E-01 2.02E+OO 0.981 968.97 15.80 4.3 1E-01 9.19E-01 0.990 10/11/2016 7:01:52AM Page 7 of7 Analysis Report for 11-0ct-16-10002 L3-10219A-FRGS-009SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCl/grams) (pCilgrams) (pCilgrams)

Corr Ac-228 1588.20 3.22 O.OOE+OO 3.33E-01 9.77E-01 1.002 + Pa-2::;i 27. 36 10.30 -1.00E+OO l.83E+OO 3.95E+OO 0.998 283.69 1. 70 -l.50E+OO 2.53E+OO 1. 000 300.07 2.47 9.77E-01 2.73E+OO 1.000 302.65 2.2 0 -1.3 1E+OO l.83E+OO 1. 000 330.06 1. 40 O.OOE+OO 3.97E+OO 1.000 + Th-234 92.38 2 .13 2.34E+OO 7.32E+OO 7.32E+OO free 92.80 2.10 3.59E+00 7.78E+OO free 112. 81 0.2 1 4.00E+OO 4.94E+Ol free + U-235 143.76 1 0. 96 3.79E-02 l.41E-01 5.55E-01 free 163.33 5.08 2.86E-01 1.3 5E+OO free 185.71 57.2 0 l.lOE-01 l.41E-01 free 202.11 1. 08 -7.15E-01 4.79E+OO miss 205.31 5.01 6.40E-02 l.20E+OO free + Am-241 59.54 35.90 4.23E-01 l.83E+OO l.83E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed. free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

45 40 35 (I) .j..,I C: ::::J 8 30 25 ..... .... ..... I ..c, "-, W} 0 1000 ,...., ;:j I "' ;::: I ;::: I 2000 3000 0000016080.CNF 4000 channel 5000 Live Time : 300.000 sec Real Time : 300.460 sec start: 1: -0.l(kev) stop : 8192: 2047. O(kev) Acq. Start : Tue Oct 11 06: 38: 33 2016 6000 7000 8000 10/11/2016 8:02:18AM

~~~pex-Gamma Analysis Report for 11-0ct-16-10003 L3-10219A-FRGS-01 OSS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 11-0ct-16-10003

L3-10219A-FRGS-010SS

1L 130G Soil Sample 1.284E+03 grams : Default : 10/3/2016 10:10:00AM

10/11/2016 7:38:50AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.3 seconds : 0.12 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16081 PEAK WITH NID REPORT Peak Analysis Performed on 10/11/2016 7:43:58AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance \[c.\~~~.a

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB 1.000FWHM \Oft'-f (J.,-Page I of8 Analysis Report for 11-0ct-16-10003 L3-10219A-FRGS-01 OSS Peak Energy ROI No. (keV) start 1 238.50 949 -2 351.90 1 402 -3 609.0 6 2 430 -4 968.91 3870 -5 1460.70 5835 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 959 1413 2444 3881 5851 10/11/2016 8:02:18AM Peak Net Peak Net Area Centroid Area Uncertainty 954.48 4.43E+Ol 19.35 1407.80 3.22E+Ol 13.08 2435.97 4.45E+Ol 15.24 3875.39 1.81E+Ol 8.92 5843.75 7.08E+Ol 1 7.15 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of8 Continuum Tentative Counts Nuclide 4.14E+Ol Pb-212 9.60E+OO Pb-214 Bi-2 11 l. lOE+Ol Bi-2 14 1.82E+OO Ac-228 2.47E+OO K-40 Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.8 2

10.66 6.77E+OO 1. 7 4E+OO miss Bi-211 0.95 351.0 7

1 3.02 9.48E-01 4.14E-01 miss Pb-212 0.99 1 15.1 8 0.60 2 38.63

43.60 3.04E-0 1 1.42E-01 free 300.09 3.3 0 Bi-214 0.99 609.32

45.49 5.92E-01 2.lSE-01 0.948 768.36 4.89 806.18 1.2 6 934.06 3.11 11 2 0.2 9 14.92 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385. 31 0.79 140 1.52 1. 33 1407.99 2.39 1509.21 2.13 1661. 27 1. 05 1729.59 2.88 1764.49 15.30 1 847.43 2.03 Analysis Report for 11-0ct-16-10003 L3-10219A-FRGS-010SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 2118. 51 Pb-214 1. 00 241.99 295.22 351.93 785.96 Ac-22 8 0.3 1 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911.20 964. 77 968. 97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1.16 7.25 18.42 35.60 1. 06 2.4 2 3.89 3.46 2.95 11. 27 1. 92 4.40 4.2 5 2 5.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 10/11/2016 8:02:18AM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 3.47E-01 1.51E-01 free 8.95E-01 4.48E-01 0.990 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi/grams)

Uncertainty K-40 0.999 6. T7E+OO 1.74E+OO ? Bi-211 0.958 9.48E-01 4.14E-01 Pb-21 2 0.999 3.04E-01 l.42E-01 Bi-214 0.998 5.92 E-01 2.15E-01 ? Pb-214 1. 000 3.47E-01 1.51E-01 Ac-22 8 0. 311 8.95E-01 4.48E-01 Analysis Report for 11-0ct-16-10003

? :;: X :;: @ :;: L3-10219A-FRGS-01 OSS nuclide is part of an undetermined solution nuclide rejected by the interference analysis nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/11/2016 8:02:18AM Page 4 of8 10/11/2016 8:02:18AM Page 5 of8 Analysis Report for 11-0ct-16-10003

+ + + + + + + + + L3-10219A-FRGS-010SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/11/2016 7:43:SBAM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

Corr K-40 1460.82

10.66 6.77E+OO 7.84E-01 7.84E-01 miss Cr-51 32 0.08 9.91 -9.98E-0 2 6.26E-01 6.2 6E-01 free Mn-54 834.85 99.98 2.95E-0 2 9.97E-02 9.97E-02 miss Co-58 810.76 99.45 -1. llE-02 6.87E-0 2 6.87E-02 1.000 1674.73 0.52 O.OOE+OO 6.25E+OO 1. 024 Co-60 1173.23 99.85 2.81E-02 7.41E-02 1. llE-01 0.947 1332.49 99.98 4.31E-03 7.41E-02 0.947 Nb-94 702.65 99.81 -7.94E-03 7.89E-02 7.89E-02 0.944 871.09 99.89 1.61E-02 9.lOE-02 0.944 Ag-108m 79.13 6.60 -2.97E-01

5. 96E-02 2.77E+OO miss 433.94 90.50 3.69E-03 5. 96E-02 0. 887 614.28 89.80 -1.42E-03 6.60E-02 0.88 6 722. 94 90.80 7.84E-03 7.28E-02 0.887 Sn-113 255 .13 2 .11 3.20E-01 7.19E-02 2.46E+OO free 391.70 64.97 -l.60E-02 7.19E-02 free Cs-134 475.36 1. 48 -1.lOE+OO 7.44E-02 3.00E+OO miss 563.25 8.34 -1.94E-Ol 8.63E-01 0.896 569.33 15.37 -1.43E-01 4.26E-01 0.888 604. 72 97.62 -8.06E-0 3 7.44E-02 0.931 10/11/2016 8:02:18AM Page 6 of8 Analysis Report for 11-0ct-16-10003 L3-10219A-FRGS-O 1 OSS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 1.84E-02 7.44E-02 1.02E-01 0.933 801.95 8.69 8.73E-02 6.42E-01 0.898 1038.61 0.99 2.03E+OO 9.36E+OO 0.943 1167.97 1. 79 1.20E+OO 5.94E+OO 1. 081 1365.19 3.02 -2.46E-01 2. llE+OO 1.128 + Cs-13 7 661.66 85.10 -6.99E-03 9.16E-02 9.16E-0 2 miss + Eu-15 2 121.78 28.67 -1.66E-02 2.0lE-01 2.0lE-01 0.936 244.70 7.61 -2.68E-01 5.61E-01 0.935 295.94 0.45 6.18E+OO 1.72E+01 miss 344.28 2 6.60 O.OOE+OO 2.23E-01 0.957 367.79 0.86 9.48E-01 8.24E+OO 0.884 411.12 2.24 1.18E-01 2.77E+OO 0.908 443.96 2.83 8.90E-0 2 2.24E+OO 0.934 488.68 0.4 2 -1.38E+OO 1.2 4E+01 miss 563.99 0.49 -1.51E+OO l.40E+Ol 0.934 586.2 6 0.46 O.OOE+OO 3.42E+OO 0.94 2 678.62 0.47 -3.62E+OO l.34E+Ol 0.887 688.67 0.86 4.84E-01 7.82E+OO 0.98 0 719.35 0.28 2.26E+OO 1.66E+01 miss 778.90 1 2.96 -1.81E-02 5.83E-01 0.945 810.45 0.32 1.0lE+OO 2.18E+O l 1. 050 867.37 4.2 6 -1.14E+OO

1. 33E+OO 0.928 919.33 0.43 1.77E+OO 1.65E+01 0.981 964.08 14.65 4.91E-02 6.16E-01 1. 02 2 1085.87 10.24 2.39E-01 8.58E-01 1. 018 1089.74 1. 73 -1.81E-01 4.70E+OO 0.952 1112.07 13.69 7.99E-02 6.69E-01 0.992 1212.95 1. 43 1.2 3E+OO 8.85E+OO 0. 929 1249.94 0.19 -6.2 8E-01 3.24E+01 1. 097 1299.14 1. 63 1.31E+OO 7.33E+OO 0.944 1408.01 21. 07 1.92E-01 5.75E-01 0.983 1457.64 0.50 O.OOE+OO 2.66E+Ol 1. 076 1528.10 0.28 O.OOE+OO 1.0lE+Ol 1.007 + Eu-154 123.07 40.40 2.83E-02 1.47E-0 1 1.47E-01 0.934 247.93 6.89 -7.66E-02 7.63E-0 1 0.928 591.76 4.95 3.65E-01 1.31E+OO 0.915 692.42 1. 78 -1.84E-01 2.72E+OO 0.936 72 3.30 2 0.06 3.37E-02 3.63E-01 0.935 756.80 4.52 2.62E-02 1.46E+OO 0.915 873.18 12.08 -7.43E-02 4.69E-01 0.93 2 996.2 9 10.48 5.79E-02 7.1 7E-01 0.971 1004.76 18.01 8.98E-02 4.83E-01 0.978 1274.43 34.80 1.35E-0~ 2.51E-01 0.981 1596.48 1. 80 O.OOE+OO 1. 40E+OO 1.175 + Eu-155 45.30 1. 31 3.77E+Ol 3.30E-01 5.65E+Ol 0.999 60.01 1. 22 2.85E+01 5.18E+Ol 1. 000 86.55 30.70 -8.58E-02 3.30E-01 free 105.31 21.10 -2.48E-02 3.3 6E-01 1.000 + Tl-208 583.19 85.00 8.95E-02 1.43E-01 1.43E-01 0.932 + Bi-211 351.07

13. 02 9.48E-01 3.95E-01 3.95E-01 miss + Pb-211 404.85 3.78 4.93E-01 1.78E+OO 1.78E+OO miss 10/11/2016 8:02:18AM Page 7 of8 Analysis Report for 11-0ct-16-10003 L 3-10219A-FRGS-010SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Colnc Name (keV) (pCl/grams) (pCi/grams) (pCl!grams)

Corr Pb-211 427.09 1. 76 -1.83E-01 1.78E+OO 2.69E+OO miss 832.01 3.52 -2.52E-01 2.12E+OO miss + Bi-21 2 39.86 1. 06 -2.73E+OO 1.61E+OO 4.76E+Ol 0.998 727. 33 6.67 6.93E-01 1.61E+OO 0.982 785.37 1.10 2.14E-01 5.95E+00 0.944 1 620.50 1. 47 -3.73E-01 5.50E+00 1.006 + Pb-212 115 .18 0.60 -9.86E-01 1.77 E-0 1 l.19E+01 miss 238.63

43.60 3.04E-01 1.77E-01 free 300.09 3.30 -3.lOE-01 1.3 8E+OO free + Pb212-XR 74.8 2 10.28 2.17E-01 1.53E+OO 2.3 9E+OO miss 77 .11 1 7.10 8.2 7E-01 1.53E+OO miss 87.35 3.97 1.54E+OO 2.70E+OO miss 89.78 1. 46 2.79E+OO 6.2GE+OO mi ss + Bi-214 609.32

45.49 5.92E-01 l.93E-01 1.93E-01 0.948 7 68. 3 6 4.89 2.26E-01 1. 71E+OO 0.94 2 806.1 8 1. 26 -1.49E+OO 6.2 6E+OO 0.923 934.06 3 .11 2.99E-01 2.76E+OO 0.944 1120.29 14.9 2 6.2 6E-01 1.17E+OO 0.944 1155.21 1. 63 -9.62E-01 6.74E+00 0.94 3 1238.12 5.83 8.45E-01 2.47E+00 0.944 1280.98 1. 43 -1.86E+OO 6.35E+OO 0.944 1377. 67 3.99 2.54E-01 2.20E+OO 1. 030 1385.31 0.79 4.2 9E+OO 1.57E+Ol 0.945 1401. 52 1. 33 -4.49E-01

5. 78E+OO 0.945 1407.99 2.39 1.75E+OO 5.26E+OO 0.945 1509.21 2.13 5.1 7E-01 3.80E+00 0.950 1661. 27 1. 05 O.OOE+OO 2.91E+OO 1. 001 1729.59 2.88 3.61E-01 2.65E+OO 1.119 1764.49 15.30 5.39E-01 l.16E+OO 1. 001 1847.43 2.03 5.64E-01 4.15E+OO 1. 06 3 > 2 118.5 1 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 2 41. 99 7.25 3.18E-01 1.44E-01 9.35E-01 1.000 295.22 1 8.42 3.58E-01 4.92E-01 1. 000 351.93

35.60 3.47E-01 1.44E-01 free 785.96 1. 06 -1.15E+OO 4.63E+00 1. 000 + Pb214-XR 74.8 2 5.80 3.85E-01 2.70E+OO 4.23E+00 miss 77 .11 9.70 1.46E+OO 2.70E+OO miss 87.35 2.24 2.73E+OO 4.79E+OO miss 89.78 0.82 4.97E+OO 1. llE+Ol miss + Ra-226 186.21 3.64 -2.02E-01 1. 52E+00 1.52E+OO free + Ac-228 129.07 2.42 9.83E-01 3.51E-01 3.22E+00 0.944 2 09.25 3.89 7.0lE-01 1.82E+OO 0.978 27 0.2 4 3.46 4.llE-01 1.91E+OO 0.955 32 8.00 2.95 1.45E+OO 2.92E+OO 0.955 338.32 11. 27 5.04E-01 7.69E-01 0.992 409.46 1. 92 -1.42E-01 2.56E+00 0.937 463.00 4.40 4.76E-01 1.60E+OO 0.933 794.95 4.2 5 -2.52E-01 1.81E+00 0.94 2 911. 2 0 25.80 4.64E-01 6.33E-01 0.990 964. 77 4.99 3.76E-01 2.06E+OO 0.981 968.97

15.80 8.95E-01 3.51E-01 0.990 Analysis Report for 11-0ct-16-10003

+ + + + + * > L3-10219A-FRGS-010SS Nuclide Energy Yield(%) Activity Name (keV) (pCilgrams)

A.c-22 8 1588.2 0 3.22 3.79E-01 Pa-23 1 27.36 10.30 -1.29E+OO 283.69 1. 70 1.62E-01 300.07 2.47 -4.14E-01 30 2.65 2.20 -2.77E-01 330.06 1. 40 -9.99E-01 Th-23 4 92.38 2.13 1.87E+00 92.80 2.10 1. 2 0E-02 112. 81 0.2 1 -l.1 7E+Ol U-23 5 143.76 10.96 3.08E-01 163.33 5.08 -3.02E-01 185.71 57.20 6.58E-0 3 202.1 1 1. 08 5.39E-01 205.31 5.01 -1.25E-01 Am-24 1 59.54 35.90 2.37E-01 = Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/11/2016 NuclideMDA (pCl/grams) 3.51E-01 1.84E+OO 6.84E+OO 1. 02E-01 1. 71E+OO ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was noi. found in the coincidence iibrary. 8:02:18AM Page 8 of8 LineMDA Coinc (pCilgrams)

Corr 3.13E+OO 1.002 5.lOE+OO 0.998 2.95E+OO 1. 000 1.84E+OO 1. 000 2.08E+OO 1.000 4.17E+OO 1. 000 6.84E+OO free 6.88E+OO fre e 3.91E+Ol free 6 .13E-01 free 9.15E-01 free 1.02E-01 free 4.47E+OO miss 9.71E-Ol free 1. 71E+OO free 60 55 50 45 40 35 VI +-' C: ::J 8 30 25 20 15 0 ::;i ..c a. .... .... .... .... ';' m i~i~ 1000 2000 3000 0000016081.CNF 4000 channel 5000 Live Time :300.000 sec Rea 1 Tfae : 300. 350 sec start: 1: -0.l(kev) stop : 8192: 2047 .O(kev) Acq. Start : T ue Oct 11 07:38:50 2016 6000 7000 8000 10/11/2016 8:02:58AM

~§~p ex-Gamma Analysis Report for 11-0ct-16-10004 L3-10219A-FRGS-011SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels} Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 11-0ct-16-10004

L3-10219A-FRGS-011SS

1 L 130G Soil Sample 1.212E+03 grams : Default : 10/3/2016 12:25:00PM

10/11/2016 7:39:11AM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 300.0 seconds : 300.3 seconds : 0.08% : 2.80 : 120-8192 : 120 -8192 : 1.000FWHM : 1/27/2016

6/28/2012

16082 PEAK WITH NID REPORT Peak Analysis Performed on 10/11/2016 8:02:24AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleranc e V'~\-~r&:O

C:\Canberra\Apex\Root\Defaul t\Library\Zion Lib-BNL.NLB

1.000FWHM la{,~fl~ Page 1 of8 10/11/2016 8:02:58AM Page 2 of8 Analysis Report for 11-0ct-16-10004 L3-10219A-FRGS-011 SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide 1 76.99 305 -314 309.17 2.88E+Ol 19.66 5.03E+Ol Pb214-XR Pb212-XR 2 87.39 345 -353 350.70 1.45E+Ol 15.92 3.90E+Ol Pb214-XR Pb212-XR M 3 238.61 949 -97 2 954.75 5.70E+Ol 1 6.09 2.63E+Ol Pb-212 m 4 241.85 949 -97 2 967. 71 2.2 3E+Ol 12.08 3.73E+Ol Pb-214 5 295.2 1 1176 -1187 11 80.89 5.33E+Ol 16.2 0 9.42E+OO Pb-214 Eu-152 6 351.99 1401 -1414 1407.76 1.02E+02 22.07 1.68E+Ol Pb-214 Bi-211 7 609.29 2429 -2 442 2436.09 7.82E+Ol 18.43 5.60E+OO Bi-214 8 1120.11 4474 -4485 4479.01 1. 78E+O l 9.41 4.46E+OO Bi-214 9 1460.77 58 33 -5851 5842.41 8.90E+Ol 18.87 O.OOE+OO K-40 -:::1"7) ,_.. M = First peak in a multiplet region lo-lf"{g m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 1. 00 1460.82

10.66 8.1 2E+OO 1.86E+OO miss Pb-21 2 1. 00 115 .18 0.60 2 38.63

43.60 3.69E-01 1.20E-01 miss 3 00.09 3.30 Pb212-X R 1. 00 74.82 1 0.2 8 77 .11

1 7.10 8.5 9E-01 6. llE-01 miss 87.35

3.97 1. 30E+OO 1.46E+OO miss 89.78 1. 46 Bi-214 1. 00 609.32

45.49 9.23E-01 2.44E-01 miss 768.36 4.89 806.18 1. 2 6 934.06 3 .11 1120.2 9

14.92 9.63E-0 1 5.16E-Ol mis s 1155. 21 1. 63 Analysis Report for 11-0ct-16-10004 L3-10219A-FRGS-011SS Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1238.12 1280.98 1377. 67 1385.31 1401.52 1407.99 1509.2 1 1661. 2 7 1729.59 1764.49 1847.43 2 118.51 Pb-214 1. 00 241. 99 295.22 351.93 785.96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 5.83 1. 43 3.99 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/11/2016 8:02:58AM Page 3 of8 Activity Activity Caine (pCilgrams)

Uncertainty Corr 8.76E-01 4.94E-01 miss 9.39E-01 3.2 3E-01 miss 1. 04E+OO 2. 81E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1.000 8.12E+OO 1.86E+00 X f8 .2,.* s../-~t 0.974 X Bi-211 0.949 Pb-212 1. 000 3.69E-0 1 1.2 0E-01 Pb212-XR 1. 000 9.25E-01 5.64E-01 Bi-214 1.000 9.30E-01 2.21E-01 Pb-214 1. 000 9.79E-01 1.95E-01 X Pb214-XR 1.000 ..,?.,,/ /Q...ft*...f.J, Analysis Report for 11-0ct-16-10004 L3-10219A-FRGS-011 SS ? = nuclide is part of an undetem,ined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/11/2016 8:02:58AM Page 4 of8 10/11/2016 8:02:58AM Analysis Report for 11-0ct-16-10004

+ + + + + + + + + L 3-10219A-FRGS-O 11 SS Peak Locate Performed on Peak Loca te From Channel Peak Loca te To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/11/2016 8:02: 24AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCl/grams) (pCl/grams) (pCilgrams)

K-40 1460.8 2

10.6 6 8 .. 12E+OO 2.47E-01 2.47E-01 Cr-51 320.08 9.91 -1.2 6E-01 5.93E-01 5.93E-01 Mn-54 834.85 99.98 9.0 lE-03 8.86E-02 8.8GE-02 Co-58 810.76 99.45 8.2 4E-03 6.56E-02 6.56E-02 1674.73 0.52 O.OOE+OO 6.09E+00 Co-60 1173.23 99.85 O.OOE+OO 2.2 7 E-02 2.27E-0 2 1332.49 99.98 1.27E-02 1.09E-01 Nb-94 702.65 99.81 -2.15E-02 5.0 3E-02 7.12E-02 8 71. 09 99.89 -5.70E-03 5.03E-02 Ag-108m 79 .13 6.60 -1.44E-01 4.89E-02 1. 48E+OO 433.94 90.5 0 1.03E-02 5.63E-02 614.28 89.80 -1.80E-03 8.48E-02 722. 94 90.80 -5.53E-03 4.89E-02 Sn-113 255 .13 2 .11 -1.0lE+OO 9.5 7 E-02 2.44E+OO 391.70 64.97 2.17E-02 9.57E-02 Cs-134 475.36 1. 48 1.85E-01 5.12E-02 4.35E+OO 563.25 8.34 -2.58E-01 4.52E-01 569.33 15.37 6.7 1E-0 3 4.40E-01 604. 72 97.62 -1.lOE-03 5.12E-02 Page 5 of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss m i ss miss mis s miss miss free free miss miss miss miss 10/11/2016 8:02:58AM Page 6 of8 Analysis Report for 11-0ct-16-10004 L3-10219A-FRGS-O 11 SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

Corr Cs-134 795.86 85.46 4.06E-02 5.12E-02 1.07E-01 miss 801.95 8.69 -1.25E-02 6. 96E-01 mis s 1038.61 0.99 1.17E+OO 7.27E+OO miss 1167.97 1. 79 -5.34E-01 3.44E+OO miss 1365.19 3.02 2.64E-01 2.27E+OO miss + Cs-137 661.66 85.10 6.12E-02 1. 21E-01 1.21E-01 miss + Eu-15 2 1 21.78 2 8.67 4.98E-02 l.2 6E-01 2.05E-01 m:i_ss 2 44.70 7.61 -1.97E-01 5.66E-01 miss 2 95.94 0.45 2. 61E+Ol 2.47E+Ol miss 344.28 26.60 2.71E-03 l.2 6E-01 miss 367.79 0.86 1.49E+OO 6.58E+OO miss 411.12 2.24 6.2 8E-01 2.58E+OO miss 443.96 2.83 -3.43E-01 1.83E+OO miss 488.68 0.42 O.OOE+OO 1.32E+Ol miss 563.99 0.49 -3. llE-01 9.64E+OO miss 586.2 6 0. 4 6 -1.37E+OO 1.61E+Ol miss 678.62 0.47 -2.45E+OO l.14E+Ol miss 688.67 0.86 7.93E-01 8.17E+OO miss 719.35 0.28 1.02E+Ol 3.04E+Ol miss 778.90 12. 96 1.06E-01 5.2 7E-01 miss 810.45 0.32 l.35E+OO l.88E+Ol miss 867.37 4.26 -9.34E-02 l.92E+OO miss 919.33 0.43 l.94E+OO l.79E+Ol miss 964. 08 14.65 1. 09E-01 5.39E-01 miss 1085.87 10.2 4 O_OOE+OO 2_10E-01 miss 1089_74 1. 73 -5.91E-Ol 4.27E+OO miss 1112.07 13.69 O.OOE+OO 1. 59E-01 miss 1212.95 1. 43 9.23E-01 7.84E+OO miss 1 2 49.94 0.19 -2.lOE+Ol 3.39E+Ol miss 1 2 99.14 1. 63 -7.06E-01 5.lOE+OO miss 1408.01 2 1. 07 -6.74E-02 5.39E-01 miss 1457.64 0.50 O.OOE+OO 2.32E+01 miss 1528.10 0.28 O.OOE+OO 9.67E+OO miss + Eu-154 123.07 40.40 1.37E-02 6.86E-02 l.39E-01 miss 2 47.93 6.89 1.05E-02 5.93E-01 miss 591.76 4.95 -l.49E+OO 7.84E-01 miss 6 9 2.42 1. 78 -9.08E-01 3.07E+OO miss 723.30 2 0.06 5.02E-0 3 2.80E-01 miss 756.80 4.52 O.OOE+OO 3.73E-01 miss 873.18 12.08 -2.84E-02 4.18E-01 miss 996.29 10.48 4.30E-01 1. OlE+OO miss 1004.76 18.01 8.38E-02 3.89E-01 miss 1 2 74.43 34.80 O.OOE+OO 6.86E-0 2 miss 1 596.48 1. 80 6.53E-01 5.39E+OO miss + Eu-155 45.30 1. 31 9.17E-01 2.82E-01 l.47E+Ol miss 60.01 1. 22 5.98E+OO l.78E+01 miss 86.55 30.70 -1.03E-01 2.82E-01 miss 105.31 21.10 4.55E-02 3.lOE-01 miss + Tl-208 583.19 85.00 1.13E-01 1.53E-01 1.53E-01 miss + Bi-211 351.07

13.02 2.85E+OO 4.91E-01 4.91E-0 1 mis s + Pb-211 404.85 3.78 7.84E-02 1. 51E+OO l.51E+OO miss 10/11/2016 8:02:58AM Page 7 of8 Analysis Report for 11-0ct-16-10004 L3-10219A-FRGS-011 SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 7.63E-01 1. 51E+OO 3.12E+OO miss 832.01 3.52 3.70E-01 2.47E+OO miss + Bi-2 12 39.86 1. 06 3.71E+OO 1. 51E+OO 1.90E+Ol mis s 727. 33 6.67 6.50E-01 1.51E+OO miss 785.37 1.10 1.25E+OO 6.23E+OO mi ss 1620.50 1. 47 9.40E-01 6.65E+OO miss + Pb-21 2 115.18 0.60 -3.41E+OO l.2 6E-01 8.37E+OO miss 2 38.63 ;t; 43.60 3.69E-01 l.2 6E-01 miss 300.09 3.3 0 1.04E+OO 2.12E+OO miss + Pb212-XR 74.82 10.28 1.70E+OO 8.8'7 E-0 1 1.78E+OO miss 77 .11

17.10 8.59E-01 8.87E-01 miss 87.35

3.97 1.30E+OO 2.31E+OO miss 89.78 1. 46 4.68E+OO 6.62E+OO miss + Bi-214 609.32

45.49 9.23E-01 1.33E-01 1.33E-01 miss 768.36 4.89 8.32E-01 2.33E+OO miss 806.18 1. 2 6 5.42E-01 5.52E+OO miss 934.06 3 .11 4.36E-01 2.49E+OO miss ll.'.20.29

14.9 2 9.63E-01 5.20E-01 miss 1155.2 1 1. 63 7.22E-02 4.69E+OO miss 1238.1 2 5.83 1. 25E+OO 2.79E+OO miss 12 80.98 1.43 -1.58E+OO 5.72E+OO miss 1377. 67 3.99 1.46E+OO 3.50E+OO miss 1385.31 0.79 2.52E+OO 1.41E+Ol miss 1401. 52 1. 33 2.12E+OO 9.29E+OO miss 1407.99 2.39 -5.92E-01 4.74E+OO miss 1509.2 1 2.13 2.34E+OO 6.14E+OO miss 1661.2 7 1. 05 O.OOE+OO 7.55E+OO mis s 1729.59 2.88 8.56E-01 5.04E+OO miss 1764.49 15.30 8.09E-01 1. 33E+OO miss 1847.43 2.03 1.14E+OO 5.31E+OO miss > 2 118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99

7.2 5 8.76E-01 1.79E-01 8.94E-01 miss 295.2 2

18.42 9.39E-01 2.51E-01 miss 351.93

35.60 1.04E+OO 1.79E-01 miss 785.96 1. 06 1. lOE+OO 6.48E+OO miss + Pb214-XR 74.82 5.80 3.02E+OO 1.5 6E+OO 3.16E+OO miss 77 .11

9.70 1.51E+OO 1.56E+OO miss 87.35

2.24 2 , 3 1E+OO 4.09E+OO miss 89.78 0.82 8.33E+OO l.18E+Ol miss + Ra-226 186.2} 3.64 5.58E-01 1.66E+OO 1. 66E+OO miss + Ac-2 2 8 1 2 9.07 2.42 -2.48E-01 3.86E-01 1.92E+OO miss 209.25 3.89 -1.77E-01 l.44E+OO miss 270.24 3.46 4.42E-02 l.16E+OO miss 328.00 2.95 2.95E-01 1.77E+OO miss 338.32 11. 27 3.2 9E-01 6.54E-01 miss 409.46 1. 92 -1.78E-01 2.78E+OO miss 463.00 4.40 -2.02E-02 1.51E+OO miss 794.95 4.2 5 7.85E-01 2 .13E+OO miss 911.2 0 25.80 8.2 0E-02 3.86E-01 miss 964. 77 4.99 1.96E-01 l.36E+OO miss 968.97 15.80 1.49E-01 7.39E-01 miss 10/11/2016 8:02:58AM Page 8 of8 Analysis Report for 11-0ct-16-10004 L3-10219A-FRGS-O 11 SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Colnc Name (keV) (pCilgrams) (pCUgrams) (pCi/grams)

Corr Ac-228 1588.2 0 3.2 2 4.60E-0 2 3.86E-01 2.99E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 3.03E-0 1 3.03E-01 miss 2 83.69 1. 70 4.77E-01 2.95E+OO miss 300.07 2.47 1. 38E+OO 2.83E+OO miss 302.65 2.20 -4.03E-01 2.38E+OO miss 330.06 1. 40 1. 41E-01 3.00E+OO miss + Th-234 92.38 2.13 2.22E+OO 4.89E+OO 4.89E+OO miss 92.80 2.10 2.93E+00 5.22E+OO miss 112.8 1 0.2 1 -5.92E+OO 3.34E+Ol miss + U-235 143.76 10.96 7.47E-03 1. 06E-01 4.43E-01 miss 163.33 5.08 8.69E-02 9.2 6E-01 miss 185. 71 57.20 2.42E-02 l.06E-01 miss 202 .11 1. 08 2.3 9E-01 4.95E+OO miss 205.31 5.01 -1.3 3E-01 8.23E-Ol miss + Arn-241 59.54 35.90 2.9 7E-01 6.65E-01 6.65E-Ol miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 VI +-' C ::s 8 30 25 20 "' 9 I 15 {e 1000 .... 9 ..c a.. 2000 .... 9 "" 3000 0000016082.CNF 4000 channel Live Time 300.000 sec Real Ti~e 300.250 sec start: 1 -0.2(kev) stop : 8192 2047 .4(kev) Acq. start Tue oct 11 07: 39: 11 2016 5000 6000 7000 8000 10/11/2016 8: 34:56AM Analysis Report for 11-0ct-16-10005 L3-10219A-FRGS-012SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 11-0ct-16-10005

L3-10219A-FRGS-012SS

1L 130G Soil Sample 1.267E+03 grams : Default : 10/3/2016 12: 50:00PM : 10/11/2016 8:11:38AM

130G 1 L Soil Sample : JWelch : P408188 : 130G S oil : 300.0 seconds : 300.6 seconds : 0.19% : 2.80 : 120-8192 : 120-8192 : 1.000FWHM : 1/27/2016

1/5/2015 : 16083 PEAK WITH NID REPORT Peak Analysis Performed on 10/11/2016 8:16:41AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB 1.000FWHM Page I of7 10/11/2016 8:34:56AM Page 2 of7 Analysis Report for 11-0ct-16-10005 L3-10219A-FRGS-012SS Peak Energy ROI No. (keV) start 1 2 38.62 949 -2 2 95.11 1174 -3 351.64 1401 -4 609.06 2 431 -5 1 460.62 5835 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1186 1415 2441 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.99 4.16E+Ol 21. 2 1 5.27E+Ol 1180.79 4.06E+O l 15.2 8 l.2 9E+Ol 1406.74 3.81E+Ol 16.78 2.58E+Ol 2436.00 2.33E+Ol 11. 99 l.14E+Ol 5843.44 9.95E+Ol 20. 72 7.02E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

10.66 9.64E+OO 2.17E+OO Pb-2 12 1. 00 115 .18 0.60 238.63

43.60 2.90E-01 1.5 5E-Ol 300.09 3.30 Bi-214 0.99 609.32

45.49 3.15E-01 l.66E-Ol 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155. 21 1. 63 1238.1 2 5.83 1 2 80.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.2 1 2 .13 1661.2 7 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 Tentative Nuclide Pb-212 Pb-214 Eu-152 Pb-214 Bi-2 11 Bi-214 K-40 Coinc Corr miss free 0.948 Analysis Report for 11-0ct-16-10005 L3-10219A-FRGS-012SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 2118.51 Pb-214 0.99 2 41.99 2 95.22 351.93 785. 96 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1.16 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/11/2016 8:34:56AM Page 3 of7 Activity Activity Coinc (pCUgrams)

Uncertainty Corr 7.65E-0 1 3 .13E-01 1. 000 4.lSE-0 1 l.95E-01 free INTERFERENCE CORRECTED REPORT Nuclide Name K-40 X Bi-211 Pb-21 2 Bi-214 Pb-214 Nuclide Id Confidence 0.997 0.980 1.000 0.998 0.997 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 9.64E+OO 2.90E-01 3.15E-01 5 .13E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 2.17E+OO 1.55E-01 1.66E-01 1.65E-01 10/11/2016 8:34:56AM Page 4 of7 Analysis Report for 11-0ct-16-10005

+ + + + + + + + + L3-10219A-FRGS-O 12SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/11/2016 8:16:41AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCi/grams) (pCilgrams)

Corr K-40 1460.82

1 0.66 9.64E+OO l.15E+OO l.15E+OO miss Cr-51 320.08 9.9 1 2.06E-02 6.33E-01 6.33E-01 free Mn-54 834.85 99.98 -8.36E-03 6.65E-02 6.65E-0 2 miss Co-58 81 0.76 99.45 -6.25E-04 6.96E-02 6. 96E-02 1. 000 1674.73 0.52 O.OOE+OO 6.33E+OO 1. 024 Co-6 0 1173.23 99.85 -4.02E-03 7.51E-02 8. 71E-02 0.947 1332.49 99.98 -8.74E-03 7.51E-02 0.947 Nb-94 702.65 99.81 -2.27E-02 6.1 8E-0 2 6.18E-0 2 0.944 871. 09 99.89 l.66E-02 9.2 2E-0 2 0.944 Ag-108m 79.13 6.60 l.19E-01 l.95E-02 2.48E+OO miss 433.94 90.50 -2.36E-02 6.04E-02 0.887 614.28 89.80 O.OOE+OO l.95E-02 0.88 6 722.94 90.80 -l.85E-02 7.38E-02 0.887 Sn-113 255.1 3 2 .11 -l.42E+OO 7.2 9E-02 2.06E+OO free 391.70 64.97 -9.93E-03 7.2 9E-02 free Cs-134 475.36 1.48 -l.24E+OO 5.83E-02 2.41E+OO miss 563.25 8.34 l.75E-01 l.03E+OO 0.896 569.33 15.37 -1. 36E-01 3.73E-01 0.888 604. 72 97.62 l.88E-03 5.83E-02 0.931 10/11/2016 8:34:56AM Page 5 of7 Analysis Report for 11-0ct-16-10005 L3-10219A-FRGS-012SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Corr Cs-13 4 795.86 85.46 -4.79E-04 5.83E-02 9.27E-02 0.933 801.95 8.69 -7.37E-02 6.51E-01 0.898 1 038.61 0.99 l.47E-01 8.18E+OO 0.94 3 1167.97 1. 79 -l.12E+OO 4.2 6E+OO 1.081 1365.1 9 3.02 2.90E-01 2.14E+OO 1.1 2 8 + Cs-137 661.66 85.10 3.60E-02 9.99E-0 2 9.99E-02 miss + Eu-152 121.78 28.67 -7.62E-03 2.2 6E-01 2.26E-Ol 0.936 244.70 7.6 1 -2.71E-02 8.73E-01 0.935 295.94 0.45 -l.94E+OO 2.41E+Ol miss 344.28 26.60 3.8 5E-0 2 2.62E-01 0.957 367.79 0.86 3.22E+OO 8.77E+OO 0.884 411.12 2.2 4 -4.92E-01 2.57E+00 0.908 443. 96 2.83 7 .13E-01 2.60E+OO 0.934 488.68 0.42 3.26E+OO l.64E+Ol miss 563.99 0.49 4.0lE+OO l.66E+Ol 0.934 586.2 6 0.46 -7.05E+OO l.19E+Ol 0.94 2 678.62 0.47 2.02E+OO 1.76E+Ol 0.887 688.67 0.86 -9.81E-01 7.92E+OO 0.980 719.35 0.2 8 -4.76E+OO 2.12E+Ol miss 778. 90 12.96 -l.46E-01 4.04E-01 0.945 8 10.45 0.32 5.13E-01 1.90E+Ol 1. 050 867.37 4.26 3.05E-02 1.70E+OO 0.92 8 919.33 0.43 2.99E+OO 1.67E+Ol 0.981 964.08 14.65 1. lOE-01 5.59E-01 1. 022 1.085.87 10.24 3.08E-0 2 8.70E-01 1. 018 1089.74 1. 73 5.13E-01 3.77E+OO 0.952 1112.07 1 3.69 2.25E-02 5.85E-01 0.99 2 121 2.95 1. 43 -l.86E+OO 6.35E+OO 0.929 1249.94 0.19 5.31E+OO 4.80E+Ol 1. 097 1299.14 1. 63 -7.07E-01 4.55E+OO 0.944 1408.01 21.07 9.71E-0 2 4.51E-01 0.983 1457.64 0.50 -8.3 6E+OO 2.87E+Ol 1. 076 1528.10 0.28 2.16E+OO 2.78E+Ol 1. 007 + Eu-154 123.07 40.4 0 -7.56E-03 1.44E-0 1 l.44E-01 0.934 247.93 6.89 -3.12E-01 6.39E-0 1 0.928 591.76 4.95 l.97E-01 1.48E+OO 0.915 692.42 1. 78 -1.87E-01 4.90E+OO 0.936 723.30 2 0.06 -l.22E-0 1 3.17E-01 0.935 756.80 4.52 7.09E-02 1.72E+OO 0.915 873.18 12.08 -5.38E-02 5.99E-01 0.932 996.29 10.48 7.82E-02 5.76E-01 0. 971 100 4.76 18.01 7.58E-03 3.35E-01 0.978 1274.43 34.80 1.37E-01 3.60E-01 0.981 1 596.48 1. 80 O.OOE+OO 1. 42E+OO 1.175 + Eu-155 45.30 1. 31 l.50E+OO 3.85E-01 3.91E+Ol 0.999 60.01 1. 22 6.75E+OO 4.87E+Ol 1.000 86.55 30.70 8.66E-02 4.18E-01 free 105.31 2 1.10 7.84E-02 3.85E-01 1. 000 + Tl-2 08 583.1 9 85.00 1.27E-Ol 1. 71E-01 l.71E-01 0.93 2 + Bi-2 11 351.0 7

13.02 l.14E+OO 6.38E-01 6.38E-01 miss + Pb-2 11 404.85 3.78 6.2 5E-0 2 1. 36E+OO 1.36E+OO miss 10/11/2016 8:34:56AM Page 6 of7 Analysis Report for 11-0ct-16-10005 L3-10219A-FRGS-012SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi/grams) (pCVgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 -6.41E-01 l.36E+OO 2. 72E+OO miss 832.01 3.52 -1.13E+OO l.47E+OO miss + Bi-212 39.86 1. 06 l.73E+OO l.2 9E+OO 4.39E+Ol 0.998 727. 33 6.67 3.59E-02 1.29E+OO 0.982 785.37 1.10 l.12E+OO 6.99E+OO 0.944 1620.50 1. 47 l.51E+OO 7.03E+OO 1. 006 + Pb-2 12 115.18 0.60 -2.03E+OO 2.12E-01 1. llE+Ol miss 238.63

43.60 2.90E-01 2.12E-01 free 300.09 3.30 6.04E-02 1.93E+OO free + Pb212-XR 74.82 10.28 4.62E-01 1.15E+OO 2.17E+OO miss 77 .11 17.10 4.27E-02 1.15E+OO miss 87.35 3.97 l.59E+OO 3.lOE+OO miss 89.78 1. 46 l.97E+O O 6.57E+OO miss + Bi-2 1 4 609.32

45.49 3.15E-Ol 1.90E-01 l.90E-01 0.948 768.36 4.89 7.46E-0 1 2.17E+OO 0.942 806.18 1. 2 6 -l.18E+OO 5.48E+OO 0.923 934.06 3 .11 3.03E-01 2.41E+OO 0.944 1120.2 9 14.92 4.09E-01 1. 23E+OO 0.944 1155.2 1 1. 63 1. 22E+OO 6.83E+OO 0.943 1238.1 2 5.83 -1.59E-02 1.79E+OO 0.944 1280.98 1. 43 -5.94E-01 5.lOE+OO 0.944 1 377.67 3.99 7.47E-01 2.89E+OO 1. 030 1385. 3 1 0.79 -7.57E-Ol 9.75E+OO 0.945 1401. 52 1. 33 O.OOE+OO 2.16E+OO 0.945 1407.99 2.39 8.88E-01 4.12E+OO 0.945 1509.21 2.13 O.OOE+OO 1.42E+OO 0.950 166 1.27 1. 05 1.09E+OO 8.02E+OO 1. 001 1 729.59 2.88 7.31E-01 3.39E+OO 1.119 1764.49 15.30 6.51E-01 1. 30E+OO 1. 001 1 847.43 2.03 O.OOE+OO l.55E+OO 1. 063 > 2118. 51 1.1 6 O.OOE+OO O.OOE+OO 1. 041 + Pb-21 4 241.99 7.2 5 1.2 4E-01 2.33E-01 9. 71E-01 1. 000 2 95.22

18.42 7.65E-01 3.12E-01 1. 000 351.93

35.60 4.15E-01 2.33E-01 free 785.96 1. 06 1. 24E+OO 6.87E+OO 1. 000 + Pb214-XR 74.82 5.80 8.18E-O l 2.03E+OO 3.85E+OO mis s 77.11 9.70 7.54E-02 2.03E+OO miss 87.35 2.24 2.82E+OO 5.50E+OO miss 89.78 0.8 2 3.51E+OO l.17E+Ol miss + Ra-226 186.2 1 3.64 1.25E-01 l.63E+OO l.63E+OO free + Ac-228 1 2 9.0 7 2.42 -8.71E-Ol 5.51E-01 2.41E+OO 0.944 209.25 3.89 1. 43E+OO 1.84E+OO 0.978 2 70.2 4 3.46 -3.llE-0 2 1.87E+OO 0.95 5 328.00 2.95 8.79E-02 1. 8 6E+OO 0.955 338.32 11. 27 2.00E-01 6.82E-01 0.992 409.46 1. 92 1. 25E+OO 3.61E+OO 0.937 463.00 4.40 -2.29E-02 l.62E+OO 0.933 794.95 4.25 3.69E-01 2.04E+00 0.942 911. 2 0 2 5.80 2.55E-01 5.51E-01 0.990 964.77 4.99 2.47E-01 1.71E+OO 0.981 968.97 15.80 2.98E-01 8.31E-01 0.990 10/11/2016 8:34:56AM Page 7 of7 Analysis Report for 11-0ct-16-10005 L3-10219A-FRGS-012SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr Ac-22 8 1588.20 3.22 3.42E-01 5.51E-01 2.51E+OO 1.002 + Pa-231 2 7. 36* 10.30 2.09E+OO 2.58E+OO 5.73E+OO 0.998 283.69 1. 70 2.44E-Ol 3.32E+OO 1. 000 300.07 2.47 8.07E-02 2.58E+OO 1. 000 302.65 2.2 0 2.81E-01 3.13E+OO 1.000 330.06 1. 40 -5.54E-01 3.49E+OO 1.000 + Th-234 92. 38 2 .13 -1.23E+OO 5.89E+OO 5.89E+OO free 92. 80 2.10 -9.27E-01 5.93E+OO free 112. 81 0.21 -3.93E+OO 3.68E+O l free + U-235 143.76 10. 96 -4.88E-0 2 1.13E-01 5.09E-01 free 163.33 5.08 4.34E-01 1.28E+OO free 185.71 57.2 0 4.36E-02 1.13E-01 free 2 02 .11 1. 08 2.76E+OO 5.39E+OO miss 2 05.31 5.01 8.47E-02 9.41E-01 free + Am-241 59.54 35.90 2.71E-01 l.68E+OO 1.68E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required. miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 VI +-' C ::::, 8 30 25 20 15 1000 ..c 0.. 2000 3000 0000016083.CNF 4000 channel 5000 Live Tire 300.000 sec Real Time 300.560 sec Start: 1 -0. l(kev) stop : 8192 2047. O(kev) Acq. start Tue Oct 11 08:11:38 2016 6000 7000 8000 6/5/2018 7:43:17AM

~pex-Gamma Analysis Report for 05-Jun-18-10004 L3-10219A-FRGS-013SS GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Fill Height Certificate Name Certificate Date : 05-Jun-18-10004

L3-10219A-FRGS-013SS

Soil 1.205E+03 grams : Default : 10/3/2016 1:10:00PM

6/5/2018 7:28:08AM

130G_S0IL_1

jwelch : P11314 : 130G_SOIL_

1 : 900.0 seconds : 900.2 seconds ! 0.03% : 3.00 : 120-8192 : 120-8192 : 1.000 keV : 12/15/2017

6/5/2018

26529 . 1205.00 gram . Eu155-Na22

12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/5/2018 7:43:11AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Page 1 of7 M m Analysis Report for 05-Jun-18-10004 L3-10219A-FRGS-O 13SS Peak Energy ROI No. (keV) start 1 74.91 2 94 -2 77.27 294 -3 209.03 831 -4 238.78 948 -5 295.23 1173 -6 338.50 1347 -7 352.00 1402 -8 583.16 2322 -9 609.21 2427 -10 1460.55 5829 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma ROI end 316 316 840 961 1186 1358 1416 2337 2442 5851 6/5/2018 7:43:17AM Peak NetPeak Net Area Centroid Area Uncertainty 300.19 5.39E+Ol 9.71 309.60 1. 05E+02 12.15 835.86 1.97E+Ol 9.43 954.71 1. 53E+02 18.40 1180 .19 8.99E+Ol 12.71 1353.07 1.99E+Ol 9.23 1407.00 1.17E+02 14.85 2330.75 5.30E+Ol 10. 06 2434.87 9.50E+Ol 11. 48 5840.16 3.14E+02 18.01 No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of7 Continuum FWHM Counts (keV) 7.86E+Ol 0.87 7.99E+Ol 0.87 3.03E+Ol 0.48 6.69E+Ol 1.20 2.61E+Ol 1.:'..3 2.51E+Ol 0.95 3.58E+Ol 0.44 1.60E+Ol 1. 09 1. 20E+Ol 1.57 2.70E+OO 1. 99 Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.98 1460.82

10.66 7.67E+OD 5.52E-01 Tl-208 1. 00 583.19

85.00 8.58E-02 1. 71E-02 Pb-212 0.99 115.18 0.60 238.63

43.60 2.58E-01 3.74E-02 300.09 3.30 Bi-214 0.99 609.32

45.49 2.96E-01 4.00E-02 768.36 4.89 Analysis Report for 05-Jun-18-10004 L3-10219A-FRG S-O 13SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 806.18 934.06 1120.29 1155. 21 1238.12 1280.98 1377.67 1385. 31 1401.52 1407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118. 51 Pb-214 1. 00 241. 99 295.22 351.93 785. 96 Pb214-XR 0.99 74.82 77 .11 87.35 89.78 Ac-228 0.57 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964. 77 968. 97 1588.20 * = Energy line found in the spectrum.

+ = Manually added nuclide. ? = Manually edited nuclide. * * * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1,000 keV Nuclide confidence index threshold

= 0.30 Errors quoted at 1.000sigma 6/5/2018 7:43:17AM Page 3 of7 Yield(%) Activity Activity (pCilgrams)

Uncertainty 1.26 3.11 14.92 1. 63 5.83 1. 43 3.99 0.79 1. 33 2.39 2 .13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 4. lOE-01 6.65E-02 35.60 3.lSE-01 4.73E-02 1. 06 5.80 1.26E+OO 2.69E-01 9.70 1.35E+OO 2.lBE-01 2.24 0.82 2.42 3.89 3.46E-01 1.68E-01 3.46 2.95 11. 27 1.64E-01 7.73E-02 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 Analysis Report for 05-Jun-18-10004 L3-10219A-FRGS-013SS Nuclide Name K-40 Tl-208 X Bi-211 Pb-212 X Pb2 1 2-XR Bi-214 Pb-214 Pb214-XR Ac-228 Nuclide Id Confidence 0.989 1. 000 0. 872 0.997 0.997 0.999 1. 000 0.997 0.576 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis 6/5/2018 7:43:17AM Wt mean Wt mean Activity Activity (pCilgrams)

Uncertainty 7.67E+OO 5.52E-01 8.58E-02 1. 71E-02 2.58E-01 3.74E-02 2. 96E-01 4.00E-02 3.47E-01 3.BSE-02 1. 32E+OO l.69E-01 l.96E-01 7.02E-02 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma Page 4 of7 Comments 6/5/2018 7:43:17AM Analysis Report for 05-Jun-18-10004

+ L3-10219A-F RGS-013SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma UNIDENTIFIED PEAKS : 6/5/2018 7:43:11AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION UB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCUgrams) (pCilgrams) (pCl/grams)

An Pk 511. 00 100. 00 6.18E+Ol 1.39E+02 1.39E+02 BE-7 477.60 10.44 -1.61E+Ol 1.06E+03 1.06E+03 K-40 1460.82

10.66 7.67E+OO 3.32E-Ol 3.32E-01 Co-60 1173.23 99.85 -1.56E-03 6.12E-02 6.12E-02 1332.49 99.98 6.34E-02 7.SlE-02 Nb-94 702.65 99.81 2.78E-02 4.71E-02 4.71E-02 871. 09 99.89 1. 69E-03 4.97E-02 Ag-108rn 79.13 6.60 1.1 7E-Ol 3.99E-02 1.41E+OO 433.94 90.50 -1. 99E-02 3.99E-02 614.28 89.80 -2.37E-02 7.25E-02 722. 94 90.80 -1.55E-02 5.62E-02 Sb-125 176.31 6.84 2.12E-02 1.86E-Ol 7.30E-01 380.45 1. 52 2.13E+OO 3.74E+OO 427.87 29.60 -5.12E-02 1.86E-01 463.36 10.49 1. 28E-01 5.82E-01 600.60 17.65 1.88E-01 3.47E-Ol 606. 71 4.98 3.30E+OO 2.39E+OO 635.95 11.22 4.41E-01 5.95E-01 671.44 1. 79 -l.80E+OO 3.46E+OO Page 5 of7 Tolerance Nuclide 6/5/2018 7:43:17AM Page 6 of7 Analysis Report for 05-Jun-18-10004 L3-1021 SA-FRGS-O 13$$ Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCUgrams) (pCilgrams) (pCi/grams)

Ba-133 79.61 2.65 8.52E-Ol 8.66E-02 3.80E+OO 81. 00 32.90 -1.08E-01 2.20E-Ol 276.40 7.16 -2.31E-01 5.lOE-01 302.85 18.34 1. 80E-01 2.22E-Ol 356.01 62.05 8.68E-03 8.66E-02 383.85 8.94 -1.57E-01 4.78E-Ol Cs-134 475.36 1. 48 2.52E+OO 9.05 E-02 4.68E+OO 563.25 8.34 -3.92E-01 8.34E-01 569.33 15.37 -2.19E-02 4.21E-01 604. 72 97. 62 2.90E-03 1.15E-01 795.86 85.46 -6.13E-02 9.05E-02 801.95 8.69 2.13E-02 9.45E-01 1038.61 0.99 -2.54E+OO

1. OlE+Ol 1167.97 1. 79 7.90E-Ol 5.83E+OO 1365.19 3.02 6.99E-01 2.59E+OO Cs-137 661.66 85.10 4.43E-02 6.02E-02 6.02E-02 Eu-152 121.78 28.67 -1. 36E-02 1.22E-01 1.27E-01 244.7 0 7.61 2.87E-01 5.83E-01 295.9 4 0.45 7.66E+OO 1.24E+Ol 344.28 26.60 5.09E-03 1.22E-01 367.79 0.86 1.41E+OO 4.60E+OO 411.12 2.24 8.lBE-01 1.99E+OO 443.96 2.83 -9.77E-Ol 1.50E+OO 488.68 0.42 3.83E+OO 9.83E+OO 563.99 0.49 2.81E+OO 8.82E+OO 586.26 0.46 -4.89E+OO l.57E+Ol 678.62 0.47 -2.lOE+OO 9.31E+OO 688.67 0.86 -5.73E-01 5.53E+OO 719.35 0.28 6. llE+OO 1.81E+Ol 778.9 0 12. 96 -5.63E-01 3.66E-Ol 810.45 0.32 9.06E+OO 1.71E+Ol 867.37 4.26 -2.66E-01 1.24E+OO 919.33 0.43 -7.79E+OO 1.14E+Ol 964. 08 14.65 4.58E-01 5.29E-01 1085.87 10.24 1. 63E-Ol 5.35E-01 1089.74 1. 73 1. 37E+OO 3.38E+OO 1112. 07 13. 69 -2.61E-Ol 4.67E-01 1212.95 1. 43 -9.99E-01 5.14E+OO 1249.94 0.19 -l.53E+Ol 3.66E+Ol 1299.14 1. 63 4.99E-01 4.05E+OO 1408.01 21. 07 -9.05E-03 2.64E-Ol 1457.64 0.50 1.82E+02 5.0lE+Ol 1528.10 0.28 -4.27E+OO

1. 42E+Ol Eu-154 123.07 40.40 -2.SlE-02 9.22E-02 9.22E-02 247.93 6.89 1.58E-01 5.41E-01 591.76 4.95 -3.21E-01 8.93E-Ol 692.42 1. 78 5.49E-01 2.68E+OO 723. 30 20.06 l.26E-02 2.96E-01 756.80 4.52 2.76E-D1 1. 25E+OO 873.18 12.08 l.09E-Ol 4.86E-01 996.29 10.48 4.57E-Ol 5.41E-01 6/5/2018 7:43:17AM Page 7 of7 Analysis Report for 05-Jun-18-10004 L3-10219A-FRGS-013SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV} (pCUgrams) (pCl/grams) (pCi/grams)

Eu-154 1004.76 18.01 -3.lOE-01 9.22E-02 3.03E-01 1274.43 34.80 1.16E-02 2.lSE-01 1596.48 1. 80 2.31E+OO 3.58E+OO Eu-155 45.30 1. 31 2.0lE+OO 2.43E-01 1.46E+Ol 60.01 1. 22 2.27E+OO l.73E+Ol 86.55 30.70 2.62E-02 2.43E-Ol 105.31 21.10 4.SlE-02 2.61E-01 Ra-226 186.21 3.64 8.98E-01 1. llE+OO 1. llE+OO Pa-231 27.36 10.30 l.25E+OO l.46E+OO l.46E+OO 283.69 1. 70 -6.lSE-01 2.22E+OO 300.07 2.47 5.86E-02 1.52E+OO 302.65 2.20 1.27E+OO 1.67E+OO 330.06 1. 40 l.OlE+OO 2.61E+OO U-235 143.76 10. 96 1.06E-01 7. llE-02 3.30E-01 163.33 5.08 -6.14E-02 6.54E-Ol 185. 71 57.20 6.97E-02 7. llE-02 202 .11 1. 08 1.49E+OO 3.19E+OO 205.31 5.01 -3.17E-01 6.14E-01 Am-241 59.54 35.90 -4.56E-02 4.76E-01 4.76E-01 + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level 60 I 55 ' so-= -45 40 7 m ... 35 VI ..... C: ::::, B 30 25 .... ..... ' m ... 20 15 a:> ::::l ' u "" 10 5 0 1000 .... 7 m ... I 2000 co ...J .... ;;!j z "' ROI Type: 1 05-JUN-18-1000445E5.CNF 3000 4000 channel 5000 live Tiae :900.000 sec Real Time :900.240 sec start: 1: -0.0(kev) stop : 8192 :2047. 8(kev) Acq. start :Tue Jun 05 07:28:08 2018 6000 ROI Type: 2 7000 8000 10/10/2016 1 :36:55PM ~~-~pex-Gamma Analysis Report for 10-0ct-16-10013 L3-10219A-FRGS-014SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold

10-0ct-16-10013

L3-10219A-FRGS-014SS

1 L 130G Soil Sample 1.245E+03 grams : Default : 10/3/2016 1 :20:00PM : 10/10/2016 1:31:18PM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 300.0 seconds : 300.3 seconds : 0.09% : 2.80 : 120 -8192 : 120 -8192 Page I of8 Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description

1.000FWHM

1/27/2016

6/28/2012 I c;(ro{c' Sample Number Peak Analysis Performed on Peak Analysi s From Channel Peak Analysi s To Channel : 16069 PEAK WITH NID REPORT 10/10/2016 1 :36:20PM : 120 : 8192 Tentative NID Library Peak Match Toleranc e : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Analysis Report for 10-0ct-16-1001 3 L3-10219A-FRGS-014SS Peak Energy ROI No. (keV) start 1 77.00 305 -2 238.65 948 -3 351.91 1400 -4 609.41 2429 -5 1460.87 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 314 960 1414 2442 5853 10/10/2016 1:36:55PM Peak NetPeak Net Area Centroid Area Uncertainty 309.24 2.87E+Ol 16.18 954.91 5.76E+Ol 18.72 1407.4 2 4.75E+01 17.20 2436.59 4 .13E+Ol 13.84 5842.81 8.40E+Ol 18.33 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page2 of8 Continuum Tentative Counts Nuclide 2.67E+Ol Pb214-XR Pb212-XR 2.28E+Ol Pb-21 2 2. llE+Ol Pb-214 Bi-211 5.42E+OO Bi-214 O.OOE+OO K-40 Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 1. 00 1460.82

10.66 7.46E+00 1. 7 5E+OO miss Bi-2 11 0.95 351.07 "k 13. 02 1. 30E+00 5.1 4E-01 miss Pb-212 1. 00 115 .18 0.60 238.63

43.60 3.62E-01 1. 32E-01 miss 300.09 3.30 Pb21 2-XR 1. 00 74.82 10.28 77 .11

17.10 8.3 0E-01 4.99E-01 miss 87.35 3.97 89.78 1. 46 Bi-'.214 1. 00 609.32

45.49 4.75E-01 1. 69E-01 mi ss 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120.2 9 14. 92 11 55. 2 1 1. 63 1 2 38.12 5.8 3 1 2 80.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 Analysis Report for 1 O-Oct-16-10013 L3-10219A-FRGS-O 14SS Nuclide Id Energy Name Confidence (keV) Bi-2 14 1. 00 1509.21 1661.27 1729.59 1764.49 1847.43 2 118.51 P b-214 1. 00 241.99 295.22 35 1.93 785. 96 Pb214-XR 1. 00 74.82 77 .11 87.35 89.78 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * ,i: @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) ~.13 1. 05 2.88 1 5.30 2.03 1.16 7.2 5 18.42 35.60 1. 06 5.80 9.70 2.24 0.82 miss = Nuclide energy was not found in the coincidence library. 10/10/2016 1:36:55PM Page 3 of8 Activity Activity Caine (pCl/grams)

Uncertainty Corr 4.74E-01 1.88E-01 mis s 1. 4 6E+OO 8.89E-01 mi ss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1.000 7.46E+OO l.75E+OO ? Bi-211 0.958 1.30E+OO 5.14E-01 Pb-21 2 1.000 3.62E-O l l.32E-01 ? Pb21 2-X R 1. 000 8.30E-01 4.99E-01 Bi-2 14 1. 000 4.75E-0 1 1.69E-01 ? Pb-2 14 1. 000 4.74E-01 1. 88E-01 ? Pb214-XR 1. 000 1. 46E+OO 8.89E-01 Analysis Report for 10-0ct-16-10013

? X @ = = = L3-10219A-FRGS-014SS nuclid e is part of an undetermined solution nuclid e rejected by the Interference analysis nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/10/2016 1 :36:55PM Page 4 of8 10/10/2016 1 :36:55PM Page 5 of8 Analysis Report for 10-0ct-16-10013

+ + + + + + + + + L3-10219A-FRGS-014SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 1 :36:20PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCl!grams) (pCilgrams)

Corr K-40 1460.82

10.66 7.46E+OO 2.40E-01 2.40E-01 miss Cr-51 320.08 9.91 -6.02E-02 4.32E-01 4.32E-01 free Mn-54 834.85 99.98 1.09E-03 6.lOE-02 6.lOE-02 miss Co-58 310.76 99.4 5 3.07E-02 8.95E-02 8.95E-02 miss 1674.73 0.5 2 O.OOE+OO 5.88E+OO miss Co-60 1173.2 3 99.8 5 1. 4 7E-02 6.51E-02 8.77E-02 miss 1332.49 99.98 -5.06E-03 6.51E-0 2 miss Nb-94 702.65 99.81 1. 03E-02 6.21E-02 6.2 1E-02 miss 871.09 99.89 1. 33E-02 7.17E-02 miss Ag-108m 79.13 6.60 -3.48E-01 6.43E-02 1. 21E+OO miss 433.94 90.50 1.57E-02 6.43E-02 miss 614.2 8 89.80 2.34E-02 8.2 6E-0 2 miss 722. 94 90.80 3.23E-03 7.76E-02 miss Sn-113 255.13 2 .11 -5.25E-01 9.79E-02 1.86E+OO free 391.70 64.97 2.04E-02 9.79E-02 free Cs-134 475.3 6 1. 48 1. 50E+OO 5.77E-02 3.93E+OO miss 563.25 8.34 l.05E-01 7.18E-01 miss 569.33 15.37 -6.53E-03 3.92E-0 1 miss 604.72 97.62 7.15E-03 5.77E-02 miss 10/10/2016 1:36:55PM Page 6 of8 Analysis Report for 10-0ct-16-10013 L3-10219A-FRGS-014SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCl!grams) (pCi/grams)

Corr Cs-1 34 795.86 85.46 9.83E-03 S.77E-02 6.85E-02 miss 801. 95 8.69 7.29E-02 6.77E-01 miss 1038.61 0.99 -7.62E-01 5.61E+OO miss 11 67.97 1. 79 9.53E-01 4.90E+OO miss 1365.19 3.02 1.71E-01 2.21E+OO miss + Cs-13.., 661.66 85.10 4.12E-02 l.13E-01 l.13E-01 miss + Eu-152 121. 78 28.67 1.24E-02 l.54E-01 1.54E-01 miss 244.70 7.61 4.93E-0 2 5.82E-01 miss 295.94 0.45 1.~lE+Ol l.84°E+Ol miss 344.28 2 6.60 2.64E-02 l.98E-01 miss 367.79 0.86 -5.97E-01 3.14E+OO miss 411.12 2.24 3.20E-01 1.92E+OO miss 44 3.96 2.83 2.97E-01 1.38E+OO miss 488.68 0.4 2 4.99E+OO 1.51E+Ol miss 563.99 0.49 6.06E+OO l.42E+O l miss 586.2 6 0.46 -2.66E+OO l.03E+Ol miss 678. 62 0.47 -1.99E+OO 8.78E+OO miss 688.67 0.86 7.72E-01 7.13E+OO miss 719.35 0.28 2.97E+00 2.52E+Ol miss 778.90 1 2.96 4.77E-02 3.51E-0 1 miss 810.45 0.32 8.23E+00 2.59E+Ol miss 867.37 4.2 6 O.OOE+OO 4.22E-01 miss 919.33 0.43 3.23E+OO 1.94E+Ol miss 964. 08 14.65 4.57E-01 8.49E-01 miss 1085.87 10 .24 -6 , 73E-02 9.06E-01 miss 1089.74 1. 73 -1.60E+OO 4.1 6E+OO miss 111 2.07 13. 69 2.95E-01 8.60E-Ol miss 1 212.95 1. 43 2.77E-0 2 6.27E+OO miss 1 249.94 0.19 -1.18E+Ol 4.16E+Ol miss 1299.14 1. 63 1.07E+OO 4.96E+OO miss 1408.01 21.07 9.37E-02 5.25E-01 miss 1457.64 0.50 -3.44E+Ol 2.26E+Ol miss 1528.10 0.28 3.48E+00 2.56E+Ol miss + Eu-154 1 23.07 40.40 -4.0lE-0 2 8.48E-0 2 8.48E-02 miss 247.93 6.89 3.50E-01 7.70E-01 miss 591.76 4.95 8.29E-02 l.12E+OO miss 692.4 2 1. 78 -8.57E-01 2.36E+OO miss 723. 30 20.06 -8.47E-02 3.16E-01 miss 756.80 4.52 -1.62E-01 l.61E+OO *miss 873.1 8 1 2.08 -4.60E-0 2 4.06E-01 miss 996.29 10.48 2.09E-01 7.50E-01 miss 1004.76 18.01 O.OOE+OO l.lOE-01 miss 1274.43 34.80 1.06E-02 l.81E-0 1 miss 1596.48 1. 80 1.13E+OO 5.25E+OO miss + Eu-155 45.30 1. 31 -8. 61E-01 2.24E-01 9.27E+OO miss 6 0.0 1 1. 22 8.91E-01 1. 34E+Ol miss 86.55 30.70 7.15E-02 2.74E-01 miss 105.31 2 1.10 l.84E-02 2.24E-01 miss + Tl-208 583.19 85.00 1.00E-01 1.37E-0 1 1.37E-01 miss + Bi-211 351.07

13.02 1.30E+OO 5.36E-01 5.36E-Ol mi ss + Pb-211 404.85 3.78 2.46E-01 1.35E+OO 1.36E+00 miss 10/10/2016 1:36:55PM Page 7 of8 Analysis Report for 10-0ct-16-10013 L3-10219A-FRG$-014SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi!grams) (pC//grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 3.94E-01 1. 35E+OO 2.79E+OO miss 83 2.01 3.5 2 -2.1 4E-01 1.35E+OO miss + Bi-2 1 2 39.86 1. 06 -2. 53E-0 1 1.25E+OO 1.59E+Ol miss 727.33 6.67 4.07E-01 l.25E+OO miss 785.37 1.1 0 -8.13E-Ol 6.06E+OO miss 1 620.5 0 1. 47 O.OOE+OO l.89E+OO miss + Pb-212 115.18 0.60 8.94E-01 l.30E-01 7.54E+00 miss 238.63

43.60 3.62E-01 l.30E-01 miss 300.09 3.30 5.08E-01 l.82E+OO miss + Pb21 2-XR 74.82 10.2 8 8.89E-01 6.56E-01 l.56E+OO miss 77 .11

17.10 8.30E-0 1 6.56E-01 miss 87.35 3.97 2.48E-01 l.87E+OO miss 89.78 1. 46 -6.79E-01 4.14E+OO miss + Bi-214 609.32

45.49 4.75E-01 l.28E-01 l.28E-01 miss 768.36 4.89 3.41E-01 l.64E+00 miss 806.18 1. 26 -4.16E-01 3.68E+OO miss 934.0 6 3.11 -l.12E-01 2.42E+OO miss 11 20.2 9 14.92 4.64E-01 9.57E-01 miss 1155.2 1 1. 63 6.32E-01 6.45E+OO miss 1238.12 5.8 3 6.38E-01 2.03E+OO miss 128 0.98 1. 43 1. 20E+OO 5.57E+OO miss 1377.67 3.99 1.2 1E+OO 3.2 0E+OO miss 1385.3 1 0.79 O.OOE+OO 3.lOE+OO miss 1401. 52 1. 33 1.58E+OO 7.42E+OO miss 1407.99 2.39 8.24E-01 4.62E+OO miss 1509.21 2 .13 -1. llE+OO 3.35E+00 miss 1661. 27 1. 05 O.OOE+OO 2.70E+OO miss 1729.59 2.88 1.64E-01 3.48E+OO miss 1764.49 15.30 7.87E-01 1.30E+OO miss 1 847.43 2.03 6. 96E-0 2 4.lOE+OO miss > 2 118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-2 14 241.99 7.25 8.42E-01 1. 96E-01 1.08E+OO miss 295.2 2 1 8.42 4.88E-01 4.98E-01 miss 351.93

35.60 4.74E-01 1. 96E-01 miss 785.96 1. 0 6 7.32E-01 7.03E+00 miss + Pb214-XR 74.8 2 5.80 1. 58E+OO 1.16E+OO 2.76E+00 miss 77 .11

9.70 1.46E+OO 1.16E+OO miss 87.35 2.24 4.40E-01 3.31E+OO miss 89.78 0.82 -1. 21E+OO 7.38E+OO miss + Ra-226 186.21 3.64 3.61E-01 1.41E+OO 1. 41E+00 miss + Ac-228 1 29.07 2.42 -7.44E-02 5.35E-01 2. llE+OO miss 2 09.2 5 3.89 2.42E-01 1.2 4E+OO miss 2 70.2 4 3.46 4.31E-02 l.2 9E+OO miss 328.00 2.95 3.2 7E-01 1.82E+OO miss 338.32 11. 27 2.25E-01 5.35E-01 miss 409.46 1. 92 9.15E-01 3.lOE+OO miss 463.00 4.40 2.23E-01 1.06E+00 miss 794.95 4.2 5 -1.47E-01

1. 08E+OO miss 911.2 0 25.80 3.02E-01 5.36E-01 miss 964.77 4.99 l.42E+00 2.59E+OO miss 968.97 15.80 3.14E-01 7.19E-01 miss 10/10/2016 1:36:55PM Page 8 of8 Analysis Report for 1O-Oct-16-10013 L3-10219A-FRGS-014SS Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Colnc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Ac-228 1588.2 0 3.22 3.14E-01 5.35E-01 2.31E+OO miss + Pa-231 27.3 6 10.30 O.OOE+OO 2.95E-01 2.95E-01 miss 283.69 1. 70 8.92E-01 2.72E+OO miss 300.07 2.47 6.79E-01 2.44E+OO miss 30 2.65 2.20 -2.63E-01 1.92E+OO miss 330.06 1. 40 -1.03E+OO l.79E+OO miss + Th-234 92.38 2.1 3 1. 07E+00 4.22E+OO 4.2 8E+OO miss 92. 80 2.10 1. 03E+00 4.22E+OO miss 11 2. 81 0.2 1 -l.27E+Ol 2.67E+Ol miss + U-235 143.76 10.96 2.38E-02 8.94E-02 3.57E-01 miss 163.33 5.08 l.14E-01 8.40E-01 mi ss 185.71 57.20 1. l 7E-02 8.94E-02 miss 202 .11 1. 08 l.lOE+OO 4.05E+OO miss 205.31 5.01 2.87E-01 9.84E-01 miss + Am-241 59.54 35.90 -7.81E-02 4.96E-01 4.96E-01 miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 U\ ..... C: :::, 8 30 25 20 0.. !;1 15 ;:!. i 1 .D Q. 1000 ...... -~ "' ;:!. 9 "' 2000 3000 0000016069 .CNF 4000 channel 5000 Live Time :300.000 sec Real Time :300.260 sec start: 1: -0.2(kev) stop : 8192:2047

.4(kev) Acq. Start :Mon Oct 10 13: 31: 18 2016 6000 7000 8000 10/6/2(.,. _ 7:22:27AM Analysis Report for 06-0ct-16-10002 L3-10219A-FJGS-015SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 06-0ct-16-10002

L3-10219A-F JGS-015SS

1 L 130G Soil Sample 1.066E+03 grams : Default : 9/27/2016 2:05:00PM

10/6/2016 6:59:12AM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.15 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16041 PEAK WITH NID REPORT Peak Analysis Performed on : 10/6/2016 7:04:15AM Peak Analysi s From Channel Peak Analysi s To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of7 Analysis Report for 06-0ct-16-10002 L 3-10219A-FJGS-015SS Peak Energy ROI No. (keV) start 1 238.56 950 -2 351.91 1403 -3 609.19 2431 -4 1460.63 5837 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1413 2444 5851 10/6/201 ... 7:22:27AM Peak Net Peak Net Area Centroid Area Uncertainty 954.73 4.76E+Ol 1 7.30 1407.84 3.24E+Ol 13. 62 2436.52 4.64E+Ol 15.50 5843.49 5.90E+Ol 15.62 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 2.09E+Ol Pb-212 1.32E+Ol Pb-214 Bi-211 l.12E+O l Bi-214 l.95E+OO K-40 Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.99 1460.82

10.66 6.80E+OO 1.89E+OO miss Bi-2 11 0.95 351.07

1 3.02 1.1 5E+OO 5 .17E-01 miss Pb-212 1. 00 11 5.18 0.60 238.63

4 3.60 3.93E-01 1.57E-O l free 300.09 3.30 Bi-214 1. 00 609.32

45.49 7.45E-01 2.64E-Ol 0.948 768.36 4.89 806.1 8 1. 26 934.06 3.11 1 12 0.2 9 1 4.92 1155. 2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385.31 0.79 1401.5 2 1. 33 1 407.99 2.39 1 509.21 2 .13 1661.27 1.0 5 1729.59 2.88 1764.49 15.30 1847.43 2.03 2 118.51 1.16 Analysis Report for 06-0ct-16-10002 L3-10219A-FJGS-015SS Nuclide Id Energy Name Confidence (keV) Pb-214 1. 00 241.99 295.22 351. 93

7 85. 96 * == Energy line found in the spectrum.

-== Manually added nuclide. ? == Manually edited nuclide. @ == Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0 .. 30 Errors quoted at 2.000sigma Coincidence correction performed. free = No coincidence correction required.

Yield(%) 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/6/201-...

7:22:27AM Page 3 o f7 Activity Activity Caine (pCilgrams)

Uncertainty Corr 4.20E-01 1. 89E-Ol free INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? Bi-211 Pb-212 Bi-214 ? Pb-214 Nuclide Id Confidence 0.998 0.957 1. 000 1. 000 1.000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 6.80E+00 1.15E+OO 3.93E-0 1 7.45E-01 4.20E-01 @ = nuclide conta i ns energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 1.89E+OO 5.17E-01 1. 57E-01 2.64E-01 1.89E-01 10/6/201..

7:22:27 AM Page 4 of7 Analysis Report for 06-0ct-16-10002

+ + + + + + + + + L 3-10219A-FJGS-015SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/2016 7:04: 15AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nu c lide Library Used : C:\Canbe r ra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pC/lgrams) (pCilgrams)

Corr K-40 1 460.82

10.66 6.80E+OO 8.41E-01 8.41E-01 miss Cr-51 320.08 9. 91 -1.50E-01 5.0 6E-01 5.06E-01 free Nn-54 834.85 99.98 3.98E-03 1.12E-01 l.12E-01 miss Co-58 810.76 99.45 O.OOE+OO 2.43E-02 2.43E-0 2 1. 000 1674.73 0.52 8.41E+OO 3.02E+01 1. 024 Co-6 0 1173.23 99.85 1.28E-02 l.13E-01 1.20E-0 1 0.947 1 332.49 99.98 l.73E-03 l.13E-01 0.947 Nb-94 702.65 99.81 9.89E-03 6. 72E-02 7.35E-02 0.944 871.09 99.89 -3.80E-02 6.72E-0 2 0.944 Ag-108m 79.13 6.60 -5.21E-01 4.91E-02 2.94E+OO miss 433.94 90.50 -2.93E-02 4.91E-02 0.887 614.28 89.80 -1.37E-02 6.30E-02 0.886 7 22.94 90.80 7.87E-03 8.77E-02 0.887 Sn-1 13 255 .13 2.11 2.95E-01 1.14E-Ol 3.41E+OO free 3 91. 70 64.97 3.67E-02 l.14E-01 free Cs-134 475.36 1. 48 4.36E-01 6.94E-02 5.lOE+OO miss 563.25 8.34 2.42E-01 l.13E+OO 0.896 569.33 15.3 7 5.2 5E-02 5.73E-01 0.888 604.72 97.62 -2.32E-02 6.94E-02 0.931 10/6/2011, 7:22:27AM Page S of7 Analysis Report for 06-0ct-16-10002 L3-10219A-F JGS-015SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Cain e Name (keV) (pCilgrams) (pCl/grams) (pCl!grams)

Corr Cs-134 795.86 85.46 1.15E-02 6.94 E-02 1.23E-01 0.933 801.95 8.69 O.OOE+OO 2.85E-01 0.898 1038.61 0.99 1.66E+OO 9.73E+OO 0.94 3 11 67. 97 1. 79 -3.90E-01 4.02E+OO 1. 081 1 3 65.1 9 3.0 2 O.OOE+OO 9.35E-01 1.128 + Cs-137 661.66 85.10 5.33E-02 1. 4 7E-01 1.47E-01 miss + Eu-152 121.78 2 8.67 -4.17E-04 1.56E-01 2.12E-01 0.936 244.70 7.6 1 2.2 6E-01 9.36E-01 0.935 295.94 0.4 5 6.0lE+OO 2.17E+01 miss 344.2 8 2 6.60 2.2 4E-02 2.84E-01 0.957 367.79 0.86 2.09E-02 8.83E+00 0.884 411.12 2.2 4 -9.66E-01 2.36E+OO 0.908 443.96 2.83 1.07E+OO 3.43E+OO 0.934 488.68 0.42 3.60E+OO 2.20E+01 miss 563.99 0.49 -1.68E+OO l.68E+Ol 0.93 4 586.2 6 0.4 6 3.2 3E+OO 2.00E+Ol 0.94 2 678. 62 0.47 4.55E+OO 1.88E+Ol 0.887 688.67 0.86 -4.86E-02 9.41E+OO 0.980 719.35 0.2 8 -6.34E+OO 2.00E+Ol miss 778.90 12. 96 -4. 72E-02 7.03E-01 0.945 810.45 0.3 2 -2.03E+OO 1.79E+Ol 1. 050 867.37 4.26 O.OOE+OO 5.89E-01 0.928 919.33 0.43 -5.69E+OO 1.57E+Ol 0.981 964. 08 14.65 2.53E-01 8.l OE-01 1. 022 1085.87 10.2 4 1.74E-01 1.03E+OO 1. 018 1089.74 1. 73 9.58E-01 5.66E+OO 0.952 11 12.07 13. 69 1.07E-0 2 6.95E-01 0.992 1 2 12.95 1. 43 9.29E-01 8.75E+OO 0.9 2 9 1 249.94 0.19 1.32E+Ol 6.36E+Ol 1. 097 1 2 99.14 1. 63 3.67E+OO 9.63E+OO 0.944 1408.01 2 1. 07 O.OOE+OO 1.56E-01 0.983 1457.64 0.50 -1.04E+Ol 2. llE+Ol 1. 076 1 528.10 0.28 O.OOE+OO 1.21E+Ol 1. 007 + Eu-1 54 1 23.0 7 40.40 -5.59E-0 2 1.49E-01 1.49E-01 0.93 4 2 47.9 3 6.89 -8.69E-02 7.59E-01 0.928 591. 7 6 4.95 5.2 8E-01 2.07E+OO 0.915 692.42 1. 78 2.22E-01 5.3 4E+OO 0.936 7 2 3.30 20.06 6.76E-03 3.77E-01 0.935 756.8 0 4.52 -1.26E-Ol 2.04E+OO 0.915 873.1 8 12.08 6.82E-0 2 8.26E-01 0.932 996.29 10.48 O.OOE+OO 2.52E-01 0. 971 1004.76 18.01 1. 05E-01 5.82E-01 0.978 1 274.43 34.80 3.26E-02 2.40E-01 0.981 1596.48 1. 80 O.OOE+OO 1. 69E+OO 1.175 + Eu-155 45.3 0 1. 31 -7.79E+OO 2.82E-0 1 4.24E+Ol 0.999 60.01 1. 22 -6.61E+00 5.29E+Ol 1. 000 86.55 30.70 2.29E-01 5.19E-01 free 105.31 2 1.10 -l.46E-01 2.82E-01 1.000 + Tl-208 583.19 85.00 6.65E-02 1.50E-01 1.50E-Ol 0.932 + Bi-2 11 35 1.07

1 3.02 1.15E+OO 5.32E-01 5.32E-0 1 miss + Pb-2 11 404.85 3.78 -2.07E-01 1.45E+OO l.45E+OO miss 10/6/201'..

7:22:27AM Page 6 of7 Analysis Report for 06-0ct-16-10002 L3-10219A-FJGS-015SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 3.0lE-01 1.45E+OO 3.61E+OO miss 832.01 3.52 -1.03E+OO 2.20E+OO miss + Bi-212 39.86 1. 06 -9.05E+OO 1.75E+OO 5.22E+Ol 0.998 727. 33 6.67 8.16E-01 1.75E+OO 0.98 2 785.37 1.10 -2.1 9E+OO 5.68E+OO 0.944 1620.50 1. 47 O.OOE+OO 2.43E+OO 1. 006 + Pb-212 115 .18 0.60 1.76E+OO 1.65E-01 l.36E+01 miss 238.63

43.60 3.93E-01 1.65E-01 free 300.09 3.30 3.00E-01 2.38E+OO free + Pb212-XR 74.82 1 0.28 1. llE+OO 1.74E+OO 3.04E+OO miss 77 .11 17.10 6.48E-01 1.74E+OO miss 87.35 3.97 1.56E+OO 3.93E+OO miss 89.78 1. 46 -1.2 6E+OO 7.54E+OO miss + Bi-214 609.32

45.49 7.45E-01 2.33E-01 2.3 3E-01 0.948 768.36 4.89 6.87E-01 2.06E+OO 0.94 2 806.18 1. 26 1. 05E+OO 7.54E+OO 0.923 934.06 3 .11 9.85E-01 4.35E+OO 0.944 1120.2 9 14.9 2 5.03E-01 1.26E+OO 0.944 1155. 21 1. 63 1. 06E+OO 6.28E+OO 0.943 1238.12 5.83 -1.98E-01

1. 84E+OO 0.944 128 0.98 1. 43 O.OOE+OO 6.06E+OO 0.944 1377.67 3.99 9.2 9E-01 3.43E+OO 1. 030 1385.31 0.79 2.2 5E-01 1.46E+01 0.945 1401.52 1. 33 9.47E-01 8.79E+OO 0.945 1407.99 2.39 O.OOE+OO 1. 43E+OO 0.945 1509.21 2 .13 O.OOE+OO 1.68E+OO 0.950 1661. 2 7 1. 05 O.OOE+OO 3.50E+OO 1. 001 1729.59 2.88 4.34E-01 3.20E+OO 1.119 1764.49 15.30 4.64E-01 1. 22E+OO 1. 001 1847.43 2.03 1.36E+OO 6.31E+OO 1. 063 > 2 118. 51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 1 4 241.99 7.25 7.16E-01 1.95E-01 1.26E+OO 1. 000 295.22 18.42 3.86E-01 5.92E-01 1. 000 351.93

35.60 4.20E-01 1. 95E-01 free 785.96 1. 06 -1.64E+OO 5.58E+OO 1. 000 + Pb214-XR 74.82 5.80 1.97E+OO 3.08E+OO 5.38E+OO miss 77 .11 9.70 l.14E+OO 3.08E+OO miss 87.35 2.24 2.77E+OO 6.96E+OO miss 89.78 0.82 -2.24E+OO 1.34E+Ol miss + Ra-226 186.2 1 3.64 1.66E+OO 2.33E+OO 2.33E+OO free + Ac-228 1 2 9.07 2.42 l.90E-01 6. 78E-01 3.33E+OO 0.944 2 09.25 3.89 1.06E+OO 2.lOE+OO 0.978 2 70.24 3.46 2.95E-02 2.06E+OO 0.955 328.00 2.95 6.90E-02 2.05E+OO 0.955 338.32 11. 27 2.74E-01 8.lOE-01 0.992 409.46 1. 92 6.29E-01 3.75E+OO 0.937 463.00 4.40 2.59E-01 1.64E+OO 0.933 794.95 4.2 5 l.57E-01 2.1 8E+OO 0.942 9 11.20 2 5.80 3.89E-0 1 6.78E-01 0.990 964. 77 4.99 1.2 6E-01 2.03E+OO 0.981 968.97 15.80 3.49E-01 8.90E-01 0.990 Analysis Report for 06-0ct-16-10002

+ + + + + > L3-10219A-FJGS-015SS Nuclide Energy Yield(%) Activity Name (keV) (pCi/grams)

Ac-228 15*88. 20 3.22 4.06E-01 Pa-231 27.36 10.30 2.26E-01 283.69 1. 70 2.20E-0 1 300.07 2.47 4.0lE-01 302.65 2.20 1.75E+OO 330.06 1. 40 -6.12E-01 Th-234 92.38 2.13 3.50E+OO 92.80 2.10 3.64E+OO 11 2. 81 0.2 1 6.32E+OO U-235 1 43.76 10. 96 2.84E-01 163.33 5.08 -4.67E-01 185.71 57.20 9.32E-02 2 02 .11 1. 08 1.35E+OO 205.31 5.0 1 5.71E-Ol Am-241 59.54 35.90 8.87E-Ol = Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/6/201'.

NuclideMDA (pCilgrams) 6.78E-01 3.18E+OO 7.97E+OO 1.SlE-01 2.17E+OO ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 7:22:27AM Page 7 of7 LineMDA Coinc (pCi/grams)

Corr 2.99E+OO 1. 00 2 5.65E+OO 0.998 3.56E+OO 1. 000 3.18E+OO 1. 000 3.71E+OO 1. 000 3.41E+OO 1. 000 8.26E+OO free 7.97E+OO free 5 .. ~5E+Ol free 6.92E-01 free 1. OOE+OO free 1.51E-01 free 6.02E+OO miss 1.35E+OO free 2.17E+OO free V'I +-' C: :::::, 60 55 50 40 35 8 30 25 1000 2000 3000 0000016041.CNF 4000 channel 5000 Live Time : 300.000 sec Real Time :300.450 sec start: 1: -0.l(kev) stop : 8192: 2047 .O(kev) Acq. Start :Thu Oct 06 06:59:12 2016 6000 7000 8000 10/6/20 , -8:05: 26AM Analysis Report for 06-0ct-16-10003 L3-10219A-FJGS-016SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real lime Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Peak Analysis Performed on . Peak Analysis From Channel Peak Analysis To Channel : 06-0ct-16-1 0003 : L3-10219A-FJGS-016SS

1 L 130G Soil Sample 1.130E+03 grams : Default : 9/27/2016 2:10:00PM

10/6/2016 7:42:11AM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.4 seconds : 0.14 % : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16042 PEAK WITH NID REPORT 10/6/2016 7:47:14AM

120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM

-~{J*,AiD '0/b(I~ Pagel of7 Analysis Report for 06-0ct-16-10003 L3-10219A-FJGS-016SS Peak Energy ROI No. (keV) start 1 201.35 803 -2 2 38.53 950 -3 351.79 1401 -4 609.09 243 2 -5 1460.64 5836 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 810 960 1414 2442 5852 10/6/20h.

8:05:26AM Peak Net Peak Net Area Centroid Area Uncertainty 806.00 7.25E+00 8.24 954.60 3.31E+Ol 18.32 1407.35 4.53E+Ol 14.71 2436.11 2.91E+Ol 11.10 5843.52 5.80E+Ol 15.50 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 9.50E+OO utfq}t= 4.17E+Ol Pb-212 7.44E+OO Pb-214 Bi-211 1.71E+OO Bi-214 2.0lE+OO K-40 #J~ /1)-f,-,/t, Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

10.66 6.3 0E+00 1.77E+OO miss Bi-211 0.96 351.07

13. 02 l.5 1E+OO 5.49E-01 miss Pb-212 0.99 115 .18 0.60 238.63

43.60 2.59E-01 1.49E-Ol f r ee 300.09 3.30 Bi-214 0.99 609.32

45.49 4.41E-Ol 1.76E-01 0.948 768.36 4.89 806.18 1. 26 934.06 3 .11 11 2 0.2 9 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385.3 1 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1661. 27 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 Analysis Report for 06-0ct-16-10003 L3-10219A-FJGS-016SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 2118. 51 Pb-214 0.99 241.99 295.22 351.93 785. 96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1.16 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/6/2011..

8:05:26AM Page 3 of7 Activity Activity Coinc (pCi/grams)

Uncertainty Corr 5.54E-01 2.0lE-01 free INTERFERENCE CORRECTED REPORT Nucllde Name K-40 ? Bi-211 Pb-212 Bi-214 ? Pb-214 Nuclide Id Confidence 0.998 0. 969 0.999 0.999 0.999 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 6.30E+OO l.51E+OO 2.59E-01 4.41E-01 5.54E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 1.77E+OO 5.49E-01 1. 4 9E-01 1. 7 6E-01 2.0lE-01 10/6/201\, 8:05:26AM Page 4 of7 Analysis Report for 06-0ct-16-10003

+ + + + + + + + + L3-10219A-F JGS-016SS Peak Locat e Performed on Peak Locat e From Channel Peak Locat e To Channel Peak No. Energy (keV) 1 201.35 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/2016 7:47:14AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 2.41667E-02 Peak Type Tol. Tolerance Nuclide tpu/ 10,6-/t NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Caine Name {keV) (pCilgrams) (pCl!grams) (pCilgrams)

Corr K-40 1460.8 2

10.66 6.30E+OO 8.0;E-01 8.07E-01 miss Cr-51 320.08 9.91 6.99E-0 2 7.73E-01 7.73E-01 free Mn-54 834.85 99.98 -2.0lE-0 2 8.67E-02 8.67E-02 miss Co-5B 810.76 99.45 -7.07E-0 3 6.2 4E-0 2 6. 24E-02 1. 000 1674.73 0.52 O.OOE+OO 7.16E+OO 1.02 4 Co-6 0 1173.23 99.85 l.15E-02 3.lOE-02 l .13E-01 0.947 1332.49 99.98 O.OOE+OO 3.lOE-0 2 0.947 Nb-94 70 2.65 99.8 1 2.14E-02 9.2 7E-02 9.79E-02 0.944 871.09 99.89 -3.35E-03 9.2 7E-02 0.944 Ag-1 08m 79.13 6.60 l.16E+OO 5.84E-02 3.0lE+OO miss 433.94 90.50 -5.66E-03 5.84E-02 0.887 614.28 89.80 l.61E-03 5.94E-02 0.886 722. 94 90.80 1.98E-03 9.59E-02 0.887 Sn-113 255.13 2 .11 -1.32E+OO 9.17E-02 2.33E+OO free 391. 70 64.97 -1.30E-02 9.17E-02 free Cs-134 475.36 1. 48 -5.87E-01 6.54E-02 2.70E+OO miss 563.2 5 8.34 2.25E-01 9.81E-01 0.896 569.33 15.37 -1.80E-0 2 4.18E-01 0.888 10/6/20h, 8:05:26AM Page 5 of7 Analysis Report for 06-0ct-16-10003 L3-1 0219A-F J GS-016SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCl/grams) (pCUgrams) (pC/lgrams)

Corr C s-134 604. 72 97.6 2 -l.69E-02 6.54 E-02 6.54E-02 0.931 7 95. 8 6 85.46 -7.25E-03 8.98E-02 0.93 3 801.95 8.69 l.65E-02 9.22E-0 1 0.898 1038.61 0.99 4.40E-01 l.06E+Ol 0.943 1167.97 1. 79 2.54E+OO :.27E+OO 1.081 1365.19 3.0 2 O.OOE+OO 8.82E-01 1.128 + Cs-137 661.66 85.10 4.50E-02 l.2 6E-01 l.26E-01 miss + Eu-152 121.78 28.67 6.84E-02 l.57E-01 2.61E-Ol 0.936 244.70 7.61 -l.77E-02 8.83E-01 0.935 295.94 0.45 1.2 1E+Ol 2.22E+Ol miss 344.28 2 6.60 -l.OlE-01

1. 57E-01 0.957 367.79 0.86 1. 2 5E+OO 7.74E+OO 0.884 411.12 2.24 -1.2 5E-01 3.14E+OO 0.908 443. 96 2.83 -l.1 7E-01 2.34E+OO 0.934 488.68 0.42 -3.49E-01

1. 41E+Ol miss 563.99 0.49 -1.85E+OO l.42E+Ol 0.934 586.26 0.46 -1.06E+Ol 1.55E+Ol 0.94 2 678.62 0.47 9.86E+OO 2.32E+Ol 0.887 688.67 0.86 2.48E+OO 8.88E+OO 0.980 719.35 0.28 9.97E+OO 3.62E+Ol miss 778.90 12.96 l.23E-01 5. 72E-01 0.94 5 810.45 0.32 -5.37E+OO l.69E+Ol 1.050 867.37 4.2 6 1.71E-01 1.51E+OO 0.928 919.33 0.4 3 6.04E+OO 2.17E+Ol 0.981 964.08 14.65 3. 88E-*02 4.2 9E-0 1 1. 022 1085.87 10.24 1.81E-01 8.41E-01 1. 018 1 089.74 1. 73 O.OOE+OO l.56E+OO 0.952 11 12. 07 1 3.69 7.06E-0 2 6.56E-01 0. 992 1 212.95 1. 43 6.03E-01 7.12E+OO 0. 929 1249.94 0.19 O.OOE+OO 1. 35E+Ol 1. 097 1299.14 1. 63 9.90E-02 7.46E+OO 0.944 1408.01 2 1. 07 2.72E-01 7.14E-Ol 0.983 1457.64 0.50 -3.91E+Ol 3.57E+Ol 1.076 1528.10 0.28 O.OOE+OO l.14E+Ol 1. 007 + Eu-154 1 23.07 40.40 -5.13E-0 2 8.32 E-0 2 l.48E-0 1 0.934 2 47.93 6.89 -7.81E-03 8.2 0E-01 0.928 591. 76 4.95 2.33E-01 1.81E+OO 0.915 692.42 1. 78 -6.99E-02 3.09E+OO 0.936 723. 30 2 0.06 4.47E-02 4.12E-01 0.935 756.80 4.52 -4.77E-01 1.32E+OO 0.915 87 3.1 8 12.08 2.90E-01 8.70E-Ol 0.932 996.2 9 10.48 -7.31E-02 6.46E-01 0. 971 1004.76 18.01 8.50E-03 3.75E-01 0.978 1274.43 34.80 O.OOE+OO 8.32E-02 0.981 1596.48 1. 80 5.89E-01 4.33E+OO 1.175 + Eu-155 45.30 1. 3 1 5.88E+OO 3.05E-01 5.07E+Ol 0.999 60.01 1. 22 -1.39E+Ol 3.61E+Ol 1. 000 86.55 3 0.70 1.3 8E-01 4.59E-Ol free 1 05.31 2 1.10 -1.2 6E-02 3.05E-01 1. 000 + Tl-208 583.19 85.00 1. 39E-01 l.84E-0 1 1.84E-01 0.932 + Bi-2 11 351.07

13.0 2 l.51E+OO 4.18E-0 1 4.18E-01 miss 10/6/2011, 8:05:26AM Page 6 of7 Analysis Report for 06-0ct-16-10003 L3-10219A-FJGS-016SS Nuclide Energy Yield{%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr + Pb-211 404.85 3.78 4.99E-01 1.67E+OO 1.67E+00 miss 427.09 1. 7 6 4.62E-01 4.2 6E+OO miss 832.01 3.5 2 -1.49E-01 2.41E+OO miss + Bi-2 12 39.86 1. 0 6 2.21E+Ol 1.18E+OO 6.05E+Ol 0.998 727.33 6.67 6. llE-03 l.18E+OO 0.98 2 785.37 1.10 2.87E+OO 9.55E+00 0.944 1620.50 1. 47 8.49E-01 6.2 5E+OO 1. 006 + Pb-212 115.18 0.60 1.50E+OO 2.04 E-01 l.17E+Ol miss 2 38.63

43.60 2.59E-01 2.04E-01 free 300.09 3.30 1.70E-01 1.79E+00 free + Pb212-XR 74.82 10.2 8 -1.3 6E-01 1. 57E+OO 2. llE+OO mis s 77 .11 17.10 1.15E+00 1.57E+OO mis s 87.35 3.97 5.89E-01 3.24E+OO miss 89.78 1. 46 4.96E+00 8.89E+OO miss + Bi-214 609.3 2

45.49 4.41E-01 1. 03E-01 1. 03E-01 0.948 768.36 4.89 5.40E-01 2.43E+00 0.94 2 806.18 1. 26 1. lOE-01 4.86E+OO 0.921 934.06 3 .11 9.70E-02 2.14E+00 0.944 1120.29 14.92 3.36E-01 1. 03E+OO 0.944 1155. 21 1. 63 O.OOE+OO 1.73E+OO 0.943 1 238.12 5.83 4.89E-01 2.63E+OO 0.944 1 280.98 1. 43 -1.66E+00

5. 72E+OO 0.944 1377. 67 3.99 1. 04E+OO 3.53E+OO 1.030 1385. 31 0.79 1.63E+OO 1.60E+Ol 0.945 1401.52 1. 33 O.OOE+OO 2.42E+00 0.945 1407.99 2.39 2.49E+OO 6.53E+00 0.945 1509.21 2 .13 4.19E-01 4.32E+OO 0.950 1661.27 1. 05 O.OOE+OO 3.30E+OO 1.00 1 17 2 9.59 2.88 8.20E-01 3.81E+OO 1.119 1764.49 15.30 3.59E-01 1.15E+OO 1.00 1 1847.43 2.03 O.OOE+OO 1.73E+00 1. 063 > 2 118.51 1.16 O.OOE+OO O.OOE+OO 1. 04 1 + Pb-214 241. 99 7.25 8.57E-01 1.53E-01 1.2 9E+OO 1. 000 2 95. 22 18.42 3.66E-01 5.68E-01 1. 000 3 51.93

35.60 5.54E-01 1.53E-01 free 785. 96 1. 06 O.OOE+OO 7.70E+00 1. 000 + Pb214-XR 74.8 2 5.80 -2.41E-01 2.77E+OO 3.74E+OO miss 77 .11 9.70 2.03E+OO 2.77E+OO miss 87.35 2.24 1.04E+00 5.74E+OO miss 89.78 0.82 8.84E+00 1.58E+Ol miss + Ra-2 2 6 186.21 3.64 9.70E-01 1.91E+OO 1. 91E+OO free + A.c-22 8 1 2 9.07 2.4 2 7.65E-01 5. 96E-01 3.14E+OO 0.944 209.25 3.89 -3.60E-02 1.26E+OO 0.978 2 70.2 4 3.46 -1.39E-01 1.94E+OO 0.955 328.00 2.95 2.92E-01 2.35E+OO 0.955 338.32 11. 27 3.89E-01 7.88E-01 0.992 409.46 1. 92 1.04E+OO 4.70E+00 0.937 463.00 4.40 3.2 9E-01 1. 69E+OO 0.933 794.95 4.25 5.09E-01 2.2 9E+OO 0.942 911.2 0 2 5.80 3.61E-01 5. 96E-01 0.990 964. 77 4.99 2.67E-01 1.65E+OO 0.981 10/6/201l.

8:05:26AM Page 7 of7 Analysis Report for 06-0ct-16-10003 L3-10219A-FJGS-016SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCilgrams) (pCi!grams)

Corr Ac-228 968.97 15.80 2.89E-01 5. 96E-01 8.40E-01 0.990 1588.2 0 3.22 4. 31E-01 3.56E+OO 1. 00 2 + Pa-231 2 7.36 10.30 -2.0lE-01 2.36E+OO 5.33E+OO 0.998 2 83.69 1. 70 -3.3 5E-01 3.54E+OO 1. 000 3 00.07 2.47 2.2 8E-01 2.39E+OO 1. 000 3 02.65 2.2 0 -l.47E+OO 2.36E+OO 1.000 330.06 1. 40 -2.19E+OO 3.92E+OO 1. 000 + Th-234 92. 38 2 .13 -9.89E-01 5.99E+OO 5.99E+OO free 92. 80 2.10 5.95E-01 6.44E+OO free 112.81 0.21 -8.65E-01 3.89E+Ol free + U-235 143.76 10. 96 1.40E-01 l.2 7E-01 5.88E-01 free 163.33 5.08 -2.69E-01 l.12E+OO free 185.71 5:.20 6.59E-02 l.2 7E-0 1 free 202 .11 1. 08 O.OOE+OO 4.86E+OO miss 205.31 5.0 1 2.llE-01 l.19E+OO free + Am-241 59.54 35.90 O.OOE+OO 1.3:'E+OO 1.37E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) ...... C: :::::, 60 55 50 45 40 35 8 30 25 1000 2000 3000 0000016042.CNF 4000 channel 5000 Live Time :300.000 sec Real Time :300.410 sec start: 1: -0.l(kev)

Stop : 8192: 2047. O(kev) Acq. start : Thu oct 06 07: 42: 11 2016 6000 7000 8000 10/6/2!, . 8:56:00AM Analysis Report for 06-0ct-16-10004 L3-10219A-FJGS-017SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Peak Analysis Performed on Peak Analysi s From Channel Peak Analysi s To Channel : 06-0ct-16-10004

L3-10219A-FJGS-017SS

1 L 130G Soil Sample 8.590E+02 grams : Default : 9/27/2016 2:20:00PM

10/6/2016 8:32:39AM

130G 1 L Soil Sample : HTomlin : P408188 : 130G Soil : 300.0 seconds : 300.4 seconds : 0.14 % : 2.80 : 120-8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16043 PEAK WITH NID REPORT 10/6/2016 8:37:42AM

120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL. NLB 1.000FWHM J)~ vJ\*J.:&-D c;:122(....

,~ 1~ r, '° Page I of7 10/6/201~

8:56:00AM Page2 of7 Analysis Report for 06-0ct-16-10004 L3-10219A-FJGS-017SS Peak Energy ROI No. (keV) start 1 351.89 1403 -2 609.06 2432 -3 1460.11 5836 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 1414 2441 5847 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 1407.76 3.16E+Ol 12.84 8.80E+OO 2436.00 l.94E+Ol 9.52 3.2 8E+OO 5841. 39 2.86E+Ol 13. 40 1.69E+Ol NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0. 96 1460.82

10.66 4.08E+OO 1.95E+OO Bi-211 0.95 351.07

13.02 1.3 9E+OO 6.0SE-01 Bi-21 4 0.99 609.32 *k 4 5.49 3.85E-01 1. 95E-01 768.36 4.89 806.18 1.26 934.06 3 .11 1120.2 9 14.92 1155. 2 1 1. 63 1 2 38.12 5.83 1280.98 1. 4 3 1377.67 3.99 1385.31 0.79 1401. 52 1. 33 1407.99 2.39 1509.2 1 2.13 1661. 2 7 1. 0 5 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1. 00 2 41. 99 7.25 2 95.22 18.42 351.93

35.60 5.09E-01 2.22E-01 785. 96 1. 06 Tentative Nuclide Pb-214 Bi-211 Bi-214 K-40 Coinc Corr miss miss 0.948 free Analysis Report for 06-0ct-16-10004 L 3-10219A-FJGS-017SS

= Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 10/6/20*1 8:56:00AM INTERFERENCE CORRECTED REPORT ? ? ? = X = Nuclide Name K-40 Bi-211 Bi-214 Pb-214 Nuclide Id Confidence

0. 969 0.959 0.998 1. 000 nuclide is part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 4.08E+OO l.39E+OO 3.85E-01 5.09E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 1.95E+00 6.08E-01 1.95E-01 2.22E-01 Page3 of7 Comments 10/6/20'1" 8:56:00AM Page 4 of7 Analysis Report for 06-0ct-16-10004

+ + + + + + + + + L3-10219A-FJGS-017SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/2016 8:37:42AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi!grams) (pCilgrams) (pCi!grams)

Corr K-40 1 460.82

10.66 4.08E+OO 2.29E+OO 2.29E+OO miss Cr-51 320.08 9.91 4.08E-01 1.13E+00 l.13E+OO free Mn-54 834.85 99.98 5.30E-03 9.83E-02 9.83E-02 mis s Co-58 810.76 99.45 O.OOE+OO 3.02E-0 2 3. 02E-02 1. 000 1674.73 0.52 O.OOE+OO 9.42E+OO 1. 024 Co-60 1173.2 3 99.85 4.62E-03 1.40E-0 1 1. 4 9E-01 0.947 1332.49 99.98 3.0lE-02 1.40E-01 0.947 Nb-94 702.65 99.81 4. 91E-03 8.33E-02 9.12E-02 0.944 871.09 99.89 -9.44E-03 8.33E-02 0.944 Ag-108m 79.13 6.60 -5.87E-0 1 8.91E-02 2.48E+OO miss 433.94 90.50 1.16E-02 8.91E-02 0.887 614.28 89.80 8.49E-03 1.14E-01 0.886 7 2 2.94 90.80 1.95E-03 1.2 6E-01 0.887 Sn-113 2 55 .13 2 .11 1.1 7E-01 1.51E-0 1 3.06E+OO free 391. 70 64.97 4.27E-02 1.51E-01 free Cs-134 475.36 1. 48 5.80E-01 8.61E-02 5.2 0E+OO miss 563.25 8.34 -5.37E-0 1 7.90E-01 0.896 569.33 15.37 -2.84E-01 4.36E-01 0.888 604. 72 97.62 -1.30E-02 8.61E-02 0.931 10/6/201 .. 8:56:00AM Page 5 of7 Analysis Report for 06-0ct-16-10004 L3-10219A-FJGS-017SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 -3.82E-02 8.61E-02 l.37E-01 0.933 801.95 8.69 1.09E-01 1. 2 1E+OO 0.898 1038.61 0.99 9.76E-01 l.2 1E+Ol 0.943 1167. 97 1. 79 -4.84E-01 4.99E+OO 1.081 1365.19 3.02 4.2 9E-01 3.15E+00 1.1 2 8 + Cs-137 661.66 85.10 7.45E-02 1.82E-01 1.82E-01 miss + Eu-152 121.78 28.67 2.75E-02 2.0:E-01 3.00E-01 0.936 244.70 7.61 3.27E-01 l.16E+OO 0.935 295.94 0.4 5 5.69E+OO 2.31E+Ol miss 344.2 8 2 6.60 -5.33E-0 2 2.39E-01 0.957 367.79 0.86 3. llE-01 9.33E+OO 0.884 411.12 2.24 -1.34E+OO 3.79E+00 0.908 443.96 2.83 1.39E+OO 3.61E+OO 0.934 488.68 0.42 3.44E+OO l.60E+Ol miss 563.99 0.49 -2.78E+OO l.2 8E+Ol 0.934 586.26 0.46 2.90E+OO 2.04E+Ol 0.94 2 678. 62 0.47 6.49E+OO 2.33E+Ol 0.887 688.67 0.86 O.OOE+OO l.17E+Ol 0.980 719.35 0.2 8 7.3 1E+OO 3.63E+Ol miss 779. 90 12. 96 O.OOE+OO 2.19E-01 0.945 810.45 0.32 3.02E+OO 2.2 3E+Ol 1.050 867.37 4.26 5.40E-01 2.51E+OO 0.92 8 919.33 0.43 4.42E-01 l.95E+Ol 0.981 964. 08 14.65 O.OOE+OO 2.07E-01 1. 0 22 1085.87 10.24 4.77E-01 1.43E+00 J.. 018 1089.74 1. 73 O.OOE+OO 2.05E+OO 0.952 1112. 07 13.69 -1.99E-02 8.63E-01 0.992 1212.95 1. 43 O.OOE+OO 2.73E+OO 0.929 1249.94 0.19 -1.78E+Ol 4.84E+Ol 1. 097 1299.14 1. 63 O.OOE+OO 2.47E+OO 0.944 1408.01 2 1.07 4.60E-02 6.65E-01 0.983 1457.64 0.50 -3.66E+Ol 2.61E+Ol 1.076 1528.10 0.2 8 O.OOE+OO 1. 51E+Ol 1. 007 + Eu-154 123.07 40.40 -5.03E-02 l.82E-01 l.95E-01 0.934 247.93 6.89 4.67E-01 1. 35E+OO 0.928 591.76 4.95 -6.92E-01 l.34E+00 0.915 692.4 2 1. 78 -6.89E-Ol 5.12E+OO 0.936 723.30 2 0.06 2.52E-02 5.42E-01 0.935 756.80 4.52 -4.71E-01 2.19E+OO 0.915 873.18 12.08 -7.94E-02 7.0lE-01 0.932 996.2 9 10.48 -2.89E-01 8.49E-01 0. 971 1004.76 18.01 O.OOE+OO l.82E-01 0.978 1274.43 34.80 1.21E-01 4.36E-01 0.981 1596.48 1. 80 O.OOE+OO 2.lOE+OO 1.175 + Eu-155 45.30 1. 31 -8.28E+OO 4.16E-01 5.26E+Ol 0.999 60.01 1. 22 -8.05E+OO 4.75E+Ol 1.000 86.55 3 0.70 3.28E-03 4.16E-01 free 105.31 2 1.10 1. OlE-01 5.53E-01 1. 000 + Tl-208 583.19 85.00 8.23E-02 1. 63E-01 1.63E-01 0.93 2 + Bi-2 11 351.07

13. 02 1.39E+OO 5.68E-01 5.68E-01 miss + Pb-211 404.85 3.78 -2.35E-01 l.2 3E+OO l.2 3E+OO miss 10/6/2011., 8:56:00AM Page 6 of7 Analysis Report for 06-0ct-16-10004 L 3-10219A-FJGS-017SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCl!grams) (pCilgrams) (pCi!grams)

Corr Pb-211 427.09 1. 7 6 7.47E-02 1. 23E+OO 3.4 7E+OO miss 8 32.0 1 3.5 2 -3.92E-01 2.1 7E+OO miss + Bi-212 39.86 1. 06 3.1 8E+OO 2.17E+OO 5.76E+Ol 0.998 727. 33 6.67 9.05E-01 2.17E+OO 0.982 785. 37 1.1 0 1.12E+OO 1.03E+Ol 0.944 1 620.50 1. 47 O.OOE+OO 3.02E+OO 1. 006 + Pb-2 1 2 115 .18 0.60 2.02E+OO 2. 71E-0 1 l.42E+Ol miss 238.63 43.60 1.36E-01 2.71E-01 free 300.09 3.30 1.02E+OO 2.73E+OO free + Pb21 2-X R 74.82 10.28 -1.56E-01 l.66E+OO 2.87E+OO miss 77 .11 17.10 5.2 7E-01 1.66E+OO miss 87.35 3.97 -4.54E-01 2.92E+OO miss 89.78 1. 4 6 1.33E+OO 9.36E+OO miss + B i-2 1 4 609.32

45.49 3.85E-Ol 1.69E-01 l.69E-01 0.948 768.36 4.89 3.02E-01 2.56E+OO 0.94 2 806.18 1. 26 3.48E+OO 1.04E+Ol 0.92 3 934.0 6 3.11 3.83E-01 2.82E+OO 0.944 11 20.2 9 14.92 4.62E-01 1. 35E+OO 0.944 11 55.2 1 1. 63 2.16E+OO 1.0lE+Ol 0.94 3 1238.12 5.83 7.37E-01 2.95E+OO 0.944 128 0.98 1. 43 -1.17E+OO 9.49E+OO 0.944 1377. 67 3.99 1. 06E+OO 3.82E+OO 1. 030 1385. 3 1 0.79 O.OOE+OO 5.2 9E+OO 0.945 1401. 52 1. 33 O.OOE+OO 3.18E+OO 0.945 1 407.99 2.39 4.2 1E-01 6.08E+OO 0.945 1509.21 2 .13 7. 72E-01 5.68E+OO 0.950 1 661. 27 1. 05 O.OOE+OO 4.35E+OO 1. 001 1729.59 2.88 1.68£-01 5.0lE+OO 1.119 1764.49 15.30 5.76E-01 1.51E+OO 1. 001 1 8 4 7.4 3 2.03 8.43E-01 6.2 1E+0() 1.063 > 2 118.5 1 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 1 4 241.99 7.25 3.40E-01 2.08E-0 1 1. 46E+OO 1. 000 295.22 1 8.42 3.06E-01 6.09E-01 1. 000 351.93

35.60 5.09E-Ol 2.0BE-01 free 785.96 1. 06 1.57E-01 8.74E+OO 1.000 + Pb214-XR 74.8 2 5.80 -2.77E-01 2.92E+OO 5.08E+OO mi s s 77 .11 9.70 9.2 8E-01 2.92E+OO miss 87.35 2.24 -8.05E-01 5.18E+OO miss 89.78 0.82 ~.36E+OO 1.67E+Ol miss + Ra-226 1 86.2 1 3.64 8.49E-01 2.58E+OO 2.58E+OO f re e + Ac-228 129.07 2.42 l.36E+OO 6.09E-01 4.33E+OO 0.944 209.25 3.89 2.17E-01 2.08E+OO 0.978 270.24 3.46 5.25E-01 2.44E+OO 0.955 328.00 2.95 -5.39E-01 2.92E+OO 0.955 338.32 11.2 7 -5.60E-02 6.55E-01 0.992 409.46 1. 92 7.38E-01 4.65E+OO 0.937 463.00 4.40 4.16E-01 2.54E+OO 0.933 794.95 4.25 1.25E-01 3.0lE+OO 0.942 91 1.20 25.80 1. 51E-01 6.09E-01 0.990 964. 77 4.99 -1.95E-Ol 1. 73E+OO 0.981 968.97 15.8 0 3.2 6E-01 9.64E-01 0.990 10/6/201v 8:56:00AM Page 7 of7 Analysis Report for 06-0ct-16-10004 L 3-10219A-FJGS-017SS Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Coin c Name (keV) (pCilgrams) (pCUgrams) (pCi!grams)

Corr Ac-228 1588.2 0 3.2 2 5.04E-01 6.09E-01 3.71E+OO 1. 00 2 + Pa-2 31 2 7.36 10.30 6.41E-01 2.55E+OO 6.31E+OO 0.998 283.69 1. 70 1.03E+OO 4.66E+OO 1.000 300.07 2.47 1.36E+OO 3.65E+OO 1. 000 302.65 2.20 -9.46E-01 2.55E+OO 1. 000 330.06 1. 40 5.97E-01 5.15E+OO 1. 000 + Th-23 4 92.38 2.13 6.98E-01 7.2 9E+OO 7.29E+OO free 92. 80 2.10 7.73E-01 7.93E+OO free 112. 81 0.2 1 -4. 72E+OO 5.36E+Ol free + U-2 3 5 143.76 10. 96 1.65E-01 1.48E-01 8.17E-01 free 163.33 5.08 -l.03E-01 l.31E+OO free 185.71 57.20 4.35E-03 l.48E-01 free 2 02 .11 1. 08 -l.53E-0 1 6.68E+OO miss 2 05.3 1 5.01 -3.82E-01 8.97E-01 free + Am-241 59.54 35.90 4.59E-Ol l.90E+OO l.90E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) ' !C ::::, 60 55 50 45 40 35 8 30 25 1000 2000 3000 0000016043.CNF 4000 channel 5000 Live Time : 300.000 sec Real Time :300.420 sec start: 1: -0.l(kev)

Stop : 8192: 2047. O(kev) Acq. start :Thu Oct 06 08:32:39 2016 C) .... 6000 7000 8000 10/6/2l. J 9:23:41AM

~~.~pex-Gamma Analysis Report for 06-0ct-16-10006 L3-10219A-FJGS-018SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real lime Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Peak Analysis Performed on Peak Analysi s From Channel Peak Analysi s To Channel : 06-0ct-16-10006

L3-10219A-FJGS-018SS

1 L 130G Soil Sample 1.171 E+03 grams : Default : 9/27/2016 2:25:00PM

10/6/2016 9:00:19AM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.17 % : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16044 PEAK WITH NID REPORT 10/6/2016 9:05:21AM

120 : 8192 Tentative NID Library Peak Match Toleranc e : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM 10/fo{f~ v~r.Jl:.O Page I of8 10/6/201~

9:23:41AM Page 2 of8 Analysis Report for 06-0ct-16-10006 L3-10219A-FJGS-018SS Peak Energy ROI No. (keV) start 1 76.98 304 -2 238.76 947 -3 295.06 1177 -4 351.70 1402 -5 609.10 2431 -6 1460.67 5835 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 314 960 1185 1412 2441 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 308.99 2.17E+Ol 15.10 2.45E+Ol 955.54 3.65E+Ol 18.41 3.49E+Ol 1180.59 2.lOE+Ol 14.02 2.60E+Ol 1407.00 3.42E+Ol 14.2 7 1.56E+Ol 2 436.14 2.40E+Ol 9.80 O.OOE+OO 5843.64 6.66E+Ol 16.97 4.83E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.8 2

10.66 6.98E+OO 1.88E+OO Pb-212 0.99 115 .18 0.60 2 38.6 3

43.60 2.75E-01 1.46E-01 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77 .11

17.10 1.21E+00 8.80E-Ol 87.35 3.97 89.7 8 1. 46 Bi-214 0.99 609.32

45.49 3.51E-01 1.49E-01 768.36 4.89 806.18 1. 2 6 934.06 3.11 11 2 0.2 9 14.92 1155. 2 1 1. 63 1 2 38.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 Tentative Nuclide Pb214-XR Pb212-XR Pb-212 Pb-214 Eu-152 Pb-214 Bi-211 Bi-214 K-40 Caine Corr miss free miss 0.948 Analysis Report for 06-0ct-16-10006 L3-10219A-F J GS-018SS Nuclide Id Energy Name Confidence (keV) B i-214 0. 9'.) 1407.99 1509.2 1 1661.2 7 17 2 9.59 1764.49 1847.43 2 118.51 Pb-214 0.99 241.99 295.22 3 51.93 785. 96 Pb214-XR 0.99 74.82 77.11 87.35 89.78 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 5.80 9.70 2.24 0.82 miss = Nuciide energy was not found in the coincidence library. 10/6/201 ... 9:23:41AM Page 3 of8 Activity Activity Coinc (pCi/grams)

Uncertainty Corr 4.28E-01 2.94E-01 1. 000 4.03E-01 l.80E-Ol free 2.14E+OO l.56E+OO miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi/grams)

Uncertainty K-40 0.999 6.98E+OO l.88E+OO X Bi-211 0.976 Pb-212 0.999 2.75E-01 1.46E-Ol ? Pb212-XR 0.999 1. 21E+OO 8.80E-01 Bi-214 0.999 3.51E-01 1.49E-01 Pb-214 0.998 4.lOE-0 1 1.54E-01 ? Pb214-XR 0.999 2.14E+OO 1.56E+OO Analysis Report for 06-0ct-16-10006

? = X = @ = L3-10219A-F J GS-018SS nuclid e i s part of an undetermined solution nuclid e r ejected by the interference analysis nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/6/20h 9:23:41AM P age 4 of8 10/6/2011..

9:23:41AM P age 5 of8 Analysis Report for 06-0ct-16-10006

+ + + + + + + + + L3-10219A-FJGS-018SS Peak Locat e P erformed on Peak Locat e F rom Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/2016 9:05: 21AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuci i de Library Used : C:\Canbe rra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCl/grams) (pCilgrams)

Corr K-40 1 460.8 2 ~, , 10.66 6.98E+OO 1. 09E+OO l.09E+OO miss Cr-51 320.0 8 9.91 3.54E-01 7.89E-01 7.89E-01 free Mn-54 834.85 99.98 1.89E-0 2 1. 02E-01 1. 02E-01 miss Co-58 810.76 99.45 1.77E-0 2 8.81E-02 8. 81E-02 1. 000 1 674.73 0.52 2.55E+OO 1.88E+Ol 1. 0 2 4 Co-60 1173.23 99.85 -5.95E-02 7.47E-02 7.47E-02 0.947 13 32.49 99.98 1. 58E-03 1.03E-01 0.947 Nb-94 702.65 99.8 1 -7.20E-03 6.69E-0 2 6.69E-02 0.944 871. 09 99.89 -6.23E-03

7. 72E-02 0.944 Ag-108m 79.13 6.60 3.02E-01 6.32E-02 2.60E+OO miss 433.94 90.50 6.07E-03 7. 96E-02 0.887 614.28 89.8 0 -8.57E-03 7.23E-02 0.886 72 2.94 9 0.8 0 -1.00E-02 6.32E-02 0.887 Sn-11 3 2 55.13 2 .11 3.42E-01 8.85E-02 3.lOE+OO free 39 1. 70 64.97 -2.21E-03 8.85E-02 free Cs-134 475.36 1. 48 9.92E-01 2.52E-02 5.00E+OO miss 563.25 8.34 5.25E-03 8.48E-01 0.896 569.33 15.37 1. 24E-01 5.22E-01 0.888 604.72 97.62 4.08E-0 3 7.32E-02 0.931 10/6/2011..

9:23:41AM Page 6 of8 Analysis Report for 0 6-0ct-16-10006 L 3-1021 SA-FJGS-01855 Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Colnc Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 O.OOE+OO 2.52E-02 2.52E-02 0.933 801.95 8.69 1.81E-01 1. 0 3 E+OO 0.898 1 038.61 0.99 -2.07E+OO 8.86E+OO 0.943 1167.97 1. 79 -9.95E-01 3.66E+OO 1. 081 1365.19 3.0 2 O.OOE+OO 8.SlE-01 1.128 + Cs-137 661.66 85.10 6.90E-02 1. 2 8E-01 l.28E-01 miss + Eu-152 121.78 28.67 3.0lE-02 1. 52E-01 2.29E-01 0.936 244. '70 7.61 -1.lSE-01 7.83E-01 0.935 295.94 0.45 -6.31E-01 2.41E+Ol mi ss 344.2 8 26.60 -6.35E-0 2 1.96E-01 0.957 367.79 0.8 6 1. 52E-0 1 6.13E+OO 0.884 411.12 2.2 4 -9.26E-02 2.lSE+OO 0.908 4 4 3.96 2.83 -2.25E-01 2.02E+OO 0.934 488.68 0.42 -3.03E+OO l.36E+Ol miss 563.99 0.49 -4.59E+OO 9.39E+OO 0.934 586.26 0.46 -7.21E+OO l.2 9E+Ol 0.94 2 678.62 0.47 6.56E+OO 2.08E+Ol 0.887 688.67 0.86 1.3 3E-O l 7.39E+OO 0.980 7 1 9.35 0.28 1.65E+OO 2.66E+Ol miss 778. 90 12.96 O.OOE+OO 1. 61E-01 0.945 8 10.45 0.3 2 1. llE+OO 2.06E+Ol 1. 050 867.37 4.2 6 3.30E-02 1.84E+OO 0.92 8 919.33 0.43 1.62E+OO 1.43E+Ol 0.981 964.08 14.65 O.OOE+OO 1. 52E-01 1. 022 1085.87 10.24 O.OOE+OO 2.37E-01 1. 018 10 89.74 1. 73 1.64E+OO 6.66F.+00 0.952 1112.07 13. 69 9.74E-03 6.33E-01 0.99 2 1212.95 1.43 1.06E-01 6.87E+OO 0.929 1249.94 0.19 -4 .13E+OO 3.SSE+Ol 1. 097 1299.14 1. 63 6.69E-01 4.92E+OO 0.94 4 1408.01 21. 07 4.SOE-0 2 3.87E-01 0.98 3 1457.64 a.so -1.2 7E+Ol 2.71E+Ol 1. 076 1 52 8.10 0.28 4.08E+OO 3.00E+Ol 1.007 + Eu-154 123.07 40.40 -2.lOE-02 1.49E-01 1.49E-01 0.934 247.93 6.89 2.40E-02 9.56E-01 0.928 591. 76 4. 95 -2.67E-02 9.83E-01 0.915 692.4 2 1. 78 -6.07E-01 3.76E+OO 0.936 7 2 3.30 20.06 -1. 42E-01 2. 72E-01 0.935 756.80 4.52 5.18E-01 1. 86E+OO 0.915 873.1 8 12.08 -8.15E-0 2 7.52E-01 0.932 996.29 10.48 1.41E-02 7.86E-01 0.971 10 0 4.76 18.01 4.lOE-02 4.57E-Ol 0.978 1 274.43 34.8 0 2.97E-02 2.18E-01 0.98 1 1 596.48 1. 8 0 O.OOE+OO 1. 54E+OO 1.175 + Eu-155 45.30 1. 3 1 -2.03E+OO 3.87E-0 1 5.18E+Ol 0.999 6 0.0 1 1. 22 2.83E+Ol 5.27E+Ol 1. 000 86. 55 30.70 7.06E-0 2 3.87E-01 free 105.31 2 1.10 8.56E-0 2 4.28E-01 1.000 + Tl-208 583.19 85.00 1.17E-01 1.69E-01 1. 69E-01 0.932 + Bi-211 351.07

13. 02 1.lOE+OO 5.21E-01 5.21E-01 miss + Pb-2 11 404.85 3.78 1.97E-01 1.73E+00 1.73E+OO miss 10/6/201\, 9:23:41AM Page 7 of8 Analysis Report for 06-0ct-16-10006 L3-10219A-FJGS-018SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCilgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 -1.31E+OO 1.73E+OO 2.54E+OO mis s 832.01 3.52 -2.88E-01 2.32E+OO mis s + Bi-212 39.86 1. 06 -6.66E+OO 1.68E+OO 4.23E+Ol 0.998 727. 33 6.67 8.48E-01 1.68E+OO 0.982 785.37 1.10 1.52E+OO 7.57E+OO 0.944 1 620.50 1. 47 O.OOE+OO 2.22E+OO 1. 006 + Pb-212 115 .18 0.60 -2.84E+OO 1.92E-Ol 9.96E+OO miss 238.63

43.60 2.75E-01 l.92E-01 free 300.09 3.30 -3.17E-01 1.51E+OO free + Pb212-XR 74.8 2 10.28 6.05E-01 1. 2 4E+OO 2.46E+OO miss 77 .11

17.10 1.21E+OO 1.2 4E+OO miss 87.35 3.9 7 8.09E-01 2. 96E+OO miss 89.78 1. 46 -4.86E-01 6.86E+OO miss + Bi-214 609.32

45.49 3.51E-01 3.87E-02 3.87E-02 0.~48 768.36 4.89 3.07E-01 2.05E+OO 0.94 2 806.18 1. 2 6 7.80E-01 6.87E+OO 0.923 934.0 6 3.11 9.48E-01 3.37E+00 0.944 1120.2 9 14. 92 5.60E-01 1.28E+OO 0.944 1155.2 1 1. 63 9.67E-01 6.63E+OO 0.94 3 1238.12 5.83 9.26E-0 2 2.36E+OO 0.944 128 0.98 1. 43 1. 3 1E+OO 9.83E+OO 0.944 1377. 67 3.99 2.60E-01 1.91E+OO 1. 030 1385. 31 0.79 -3.48E+OO 1.05E+Ol 0.945 1401.52 1. 33 l.72E+OO 8.00E+OO 0.945 1407.99 2.39 4.12E-01 3.54E+OO 0.945 1509.2 1 2 .13 1.13E+OO 5.2 6E+OO 0.950 1661.27 1. 05 4.42E-01 8.67E+OO 1. 001 1 729.59 2.88 3.95E-01 2.91E+OO 1.119 1764.49 15.30 3.74E-0 1 l. llE+OO 1. 001 1847.43 2.03 6.19E-01 4.55E+OO 1.063 > 2118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 1 4 2 41.99 7.25 7.98E-01 l.91E-01 1.14E+OO 1. 000 2 95.22

18.42 4.28E-01 4. ll E-01 1. 000 351.93

35.60 4.03E-01 l.91E-01 free 785.96 1. 06 2.07E+OO 7.43E+OO 1.000 + Pb214-XR 74.82 5.80 l.07E+OO 2.19E+OO 4.36E+OO miss 77 .11

9.70 2.14E+OO 2.19E+OO miss 87.35 2.2 4 1.43E+OO 5.2 5E+OO miss 89.78 0.82 -8.66E-01 1.2 2E+Ol miss + Ra-22 6 186.2 1 3.64 5.43E-01 1.80E+OO l.80E+OO free + Ac-228 1 2 9.07 2.42 -l.58E-0 1 4.1 5E-01 2.95E+OO 0.944 2 0 9.25 3.89 4.46E-02 1.41E+OO 0.978 270.24 3.46 6.79E-01 2.23E+OO 0.955 328.00 2.95 -4.28E-02 2.0lE+OO 0.955 338.32 11. 2 7 1.22E-01 6.65E-01 0.992 409.46 1. 92 1.42E+OO 4.13E+OO 0.937 463.00 4.40 6.73E-01 2.16E+OO 0.933 794.95 4.25 5.52E-01 1. 98E+OO 0.942 911.20 2 5.80 1. 21E-Ol 4.15E-01 0.990 964. 77 4.99 1. 72E-Ol l.27E+OO 0.981 968. 97 15.80 3.70E-01 8.99E-01 0.990 Analysis Report for 06-0ct-16-10006

+ + + + + * > L3-10219A-FJGS-018SS Nuclide Energy Yield(%) Activity Name (keV) (pCl/grams)

Ac-2 2 8 1588.20 3.22 O.OOE+OO Pa-231 2 7.36 10.30 -4. llE-01 283.69 1. 70 -3.l OE-01 300.07 2.47 -4.2 3E-01 302. 65 2.2 0 -1. 2 8E+OO 330.06 1. 40 1.44E-01 Th-234 92.38 2 .13 -8. 92E-01 92.80 2.10 -1.84E+OO 112. 81 0.21 -3.76E+OO U-235 143.76 10. 96 2.06E-01 163.33 5.08 -1.68E-01 1 85. 71 57.2 0 7.3 4E-02 202 .11 1. 08 1.1 4E+OO 2 05.31 5.01 -8.21E-02 Am-241 59.54 35.90 -1.65E-01

= Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/6/201'.

NuclideMDA (pCilgrams) 4.15E-01 1.61E+OO 6.18E+OO 1.2 5E-01 1.59E+OO ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 9:23:41AM Page 8 of8 LineMDA Coinc (pCi!grams)

Corr 1.00E+OO 1. 00 2 6.20E+OO 0.998 3.42E+OO 1. 000 2.02E+00 1. 000 1.61E+OO 1.000 4.06E+OO 1. 000 6.18E+OO free 6.22E+OO free 4.68E+Ol free 6.30E-01 free 1.08E+OO free 1.2 5E-01 free 5.lOE+OO miss 9.70E-01 free 1.59E+OO free 60 55 50 45 40 35 V) .J-1 C ::::, 8 30 25 20 "' '1-..,. ;;j ..c "' 15 ;!; ;;j ..c '1. "' ..,. ...... '.b ... 1000 2000 3000 0000016044.CNF 4000 channel 5000 Live Tirie :300.000 sec Real Time :300.510 sec start: 1: -0.l(kev) stop : 8192: 2047. O(kev) ACq. Start :Thu Oct 06 09:00:19 2016 6000 7000 8000 10/6/21. . J 9:49:37 AM Analysis Report for 06-0ct-16-10007 L3-10219A-F J GS-019SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Peak Analysis Performed on Peak Analysi s From Channel Peak Analysis T o Channel : 06-0ct-16-10007

L3-10219A-F JGS-019SS

1 L 130G Soil Sample 1.082E+03 grams : Default : 9/27/2016 2: 30:00PM : 10/6/2016 9:26:29AM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.4 seconds : 0.14 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16045 PEAK WITH NID REPORT 10/6/2016 9:31:31AM

120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.N LB : 1.000FWHM Ditn"1' \IA f. rlTt--0. IC/t:,/f~

Page 1 of7 Analysis Report for 06-0ct-16-10007 L3-10219A-FJGS-019SS Peak Energy ROI No. (keV) start 1 3 51.83 1401 -2 1460.53 5836 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 1411 5851 10/6/201~

9:49:37AM Peak Net Peak Net Area Centroid Area Uncertainty 1407.51 2.50E+Ol 1 2.41 5843.07 5.50E+Ol 14.83 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 1.21E+Ol Pb-214 Bi-2 11 O.OOE+OO K-40 Activity Coinc Name Confidence (keV) (pCi/gramsj Uncertainty Corr K-40 0.99 1460.82 Bi-211 0.96 351.07 Pb-214 1. 00 241.99 295.22 351.93 785. 96 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

10.66 13. 02 7.2 5 1 8.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 6.2 4E+OO 1.77E+OO miss 8. 72E-01 4.56E-01 mis s 3.19E-01 1.67E-O l free 10/6/201..

9:49:37AM Analysis Report for 06-0ct-16-10007 L3-10219A-FJGS-019SS INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? Bi-211 ? Pb-214 Nuclide Id Confidence 0.995 0. 965 1. 000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 6.24E+OO 8. 72E-01 3.19E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 1.77E+00 4.56E-01 1.67E-01 Page 3 of7 Comments 10/6/201...

9:49:37 AM Page4 of7 Analysis Report for 06-0ct-16-10007

+ + + + + + + + + L3-10219A-FJGS-019SS Peak Locate Performed on Peak Locate From Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAK S : 10/6/2016 9:31:31AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCl!grams) (pCi!grams)

Corr K-40 1460.82

10.66 6 . .'.24E+OO 3.07E-01 3.07E-01 miss Cr-51 320.08 9.91 -8.08E-02 5.80E-01 5.80E-Ol free Mn-54 834.85 99.98 1.68E-02 7.81E-0 2 7.81E-0 2 miss Co-58 810.76 99.45 O.OOE+OO 2.40E-02 2. 40E-0 2 1. 000 1674.7 3 0.52 O.OOE+OO 7.48E+OO 1. 024 Co-60 11 73.23 99.85 6.2 8E-03 3.23E-02 1.02E-Ol 0.947 1332.49 99.98 O.OOE+OO 3.23E-02 0.947 Nb-94 702.65 99.81 4.76E-03 G.62E-02 8.39E-02 0.944 871. 09 99.89 -7.49E-03 6.62E-02 0.944 Ag-108m 79.13 6.60 -3.96E-01 6.lOE-02 2.44E+OO miss 433.94 90.50 -2.63E-03 6.lOE-02 0.887 614.2 8 89.80 -2.87E-0 2 6.2 0E-02 0.886 722. 94 90.80 9.30E-0 3 6.84E-02 0.887 Sn-113 255.13 2.11 5.60E-01 1. 05E-01 3.36E+OO free 391.70 64.97 -1. 28E-02 1. 05E-01 free Cs-134 475.36 1. 48 8.44E-01 9.65E-0 2 4.61E+OO miss 563.25 8.34 -2.22E-01 7.92E-01 0.896 569.33 15.37 -3.95E-01 4.37E-01 0.888 604.72 97.62 3.68E-0 2 9.65E-02 0.931 10/6/20h, 9:49:37AM Page 5 of7 Analysis Report for 06-0ct-16-10007 L3-10219A-FJGS-019SS Nuclide Energy Yield(%) Activity Nucl/deMDA LineMDA Caine Name (keV) (pCi/grams) (pCi!grams) (pCi/grams)

Corr Cs-134 795.86 85.46 4.04E-02 9.65E-02 1. 21E-01 o.~33 801.95 8.69 1.04E-01 9.63E-01 0.898 1038.61 0.99 -1.72E+OO 7.60E+00 0.94 3 1167.S7 1. 79 1.03E-01 5.79E+OO 1. 081 1365.19 3.02 1.46E-01 2.50E+OO 1.128 + Cs-137 661.66 85.10 6.57E-0 2 1.38E-01 1.38E-01 miss + Eu-152 121.78 28.67 -3.41E-0 2 1. 74E-01 2.56E-Ol 0.936 2 44.70 7.61 -2.57E-01 6.66E-01 0.935 2 95.94 0.45 9.94E+OO 2.19E+Ol miss 344.28 26.60 4.23E-02 2.49E-01 0.957 3 67.79 0.86 1.99E+OO 8.70E+OO 0.884 411.1 2 2.24 -2.25E-01 2.33E+OO 0.908 443.96 2.83 2.84E-01 1.89E+OO 0.934 488.68 0.42 -1.64E+OO 1.93E+Ol miss 563.99 0.49 3.17E+OO l.66E+Ol 0.934 586.2 6 0.46 3.00E+OO 1.97E+Ol 0.94 2 678.62 0.47 -1.57E+OO l.59E+Ol 0.887 688.67 0.86 -1.44E-01 1.03E+Ol 0.980 719.35 0.28 O.OOE+OO 7.2 5E+OO miss 778.90 12.96 O.OOE+OO 1.74E-01 0.945 810.45 0.32 O.OOE+OO 6.50E+OO 1. 050 867.37 4.26 O.OOE+()O 5.80E-01 0.928 919.33 0.43 -9. llE+OO 1.55E+Ol 0.981 964.08 1 4.65 3.72E-02 6.55E-01 1. 022 1085.87 10. 24 5.86E-02 1.02E+OO 1. 018 1089.74 1. 73 -8.58E-0 2 5.58E+OO 0.952 1 112.07 13. 69 4.74E-0 2 6.85E-01 0.992 1 2 12.95 1. 43 1.60E+OO 7.44E+OO 0.929 1249.94 0. 19 2.98E+OO 3.84E+Ol 1. 097 1299.14 1. 63 O.OOE+OO l.96E+OO 0.944 1408.01 21. 07 -9.75E-02 4.18E-01 0.98 3 1457.64 0.50 O.OOE+OO 2.41E+Ol 1. 076 1528.10 0.28 4.42E+OO 3.25E+Ol 1.007 + Eu-154 123.07 40.40 -8.84E-03 1.08E-01 1. 98E-01 0.934 247.93 6.89 -2.08E-01 9.51E-01 0.928 591. 76 4.95 2.70E-01 1.55E+OO 0.915 692.4 2 1. 78 -2.92E-01 4.07E+OO 0.936 723. 30 2 0.06 O.OOE+OO 1.08E-Ol 0.935 756.80 4.52 O.OOE+OO 5.06E-01 0.915 873.18 12.08 1. 26E-02 7.02E-01 0.932 996.29 10.48 1.22E-Ol 9.86E-01 0.971 1004.76 18.01 5.33E-02 3.92E-01 0.978 1274.43 34.80 3.21E-02 2.36E-01 0.981 1596.48 1. 80 O.OOE+OO 1.66E+OO 1.175 + Eu-155 45.30 1. 3 1 -7.89E+OO 3.53E-01 3.45E+Ol 0.999 60.01 1. 22 1.12E+Ol 4.66E+Ol 1. 000 86.55 30.70 1.2 1E-01 4.06E-01 free 105.31 2 1.10 4.2 4E-02 3.53E-01 1. 000 + Tl-208 583.19 85.00 1.55E-01 2.04E-01 2.04E-01 0.932 + Bi-211 351.07

13 .0 2 8.72E-Ol 5.17E-01 5.17E-01 miss + Pb-211 404.85 3.78 -4.20E-01 6.32E-01 1.74E+00 miss 10/6/20 *~ 9:49:37AM P age 6 of7 Analysis Report for 06-0ct-16-10007 L3-10219A-FJGS-019SS Nuclide Energy Yield(%) Activity Nucl/deMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams)

{pCl/grams)

Corr Pb-211 427.09 1. 76 -4.35E-01 6.32E-01 3.19E+OO miss 832.01 3.52 O.OOE+OO 6.32E-01 miss + Bi-212 39.86 1. 06 1.15E+Ol 1. 38E+OO 5.14E+Ol 0.998 727. 33 6.67 4.59E-01 1.38E+OO 0.98 2 785.37 1.10 3.04E+OO 9.14E+OO 0.944 1620.50 1. 47 O.OOE+OO 2.40E+OO 1. 006 + Pb-212 115 .18 0.60 2.04E+OO 2.82E-01 l.17E+Ol mis s 238.63 43.60 3.14E-01 2.82E-01 free 300.09 3.30 1.2 5E-01 2.17E+OO free + Pb212-XR 74.8 2 10.28 9.14E-01 1. 35E+OO 2.48E+OO miss 77 .11 1 7.10 2.47E-Ol 1.3 5E+OO miss 87.35 3.97 -2.2 0E-01 2.80E+OO miss 89.78 1. 4 6 1.60E+OO 8.1 8E+OO miss + Bi-2 14 609.32 45.49 3.43E-01 3.87E-Ol 3.87E-Ol 0.948 768.36 4.89 -2.54E-01 1.57E+OO 0.94 2 806.1 8 1. 2 6 1.73E-01 6.41E+OO 0.923 934.0 6 3.11 6.08E-01 3.2 7E+OO 0.944 1120.29 14.92 1. 91E-01 8.57E-01 0.944 1155.21 1. 63 5.71E-01 6.19E+00 0.943 1 2 38.12 5.83 8.43E-01 2.93E+OO 0.944 1280.98 1. 43 8. llE-01 5.97E+OO 0.944 1377. 67 3.99 -1.09E+OO 2.07E+OO 1. 030 1 385.31 0.79 1. 55E+OO l.14E+Ol 0.945 1 401.52 1. 33 O.OOE+OO 2.52E+OO 0.945 1407.99 2.39 -8.92E-01 3.83E+OO 0.945 1509.21 2 .13 6 .13E-01 4.51E+OO 0.950 1661.27 1. 05 1.28E+OO 9.39E+OO 1. 001 1 729.59 2.88 8.56E-01 3.97E+OO 1.119 1764.49 15.30 5.60E-01 1.37E+OO 1. 001 1847.43 2.03 O.OOE+OO l.81E+OO 1. 063 > 2 118.51 1.16 O.OOE+OO O.OOE+OO 1.041 + Pb-214 241.99 7.25 4. 91E-01 l.89E-01 l.14E+OO 1. 000 295.22 18.42 4.97E-01 5.94E-01 1. 000 3 51.93

35.60 3.19E-01 1.89E-01 free 785.96 1. 06 2.99E+OO 8.97E+OO 1.000 + Pb214-XR 74.82 5.80 l.62E+OO 2.38E+OO 4.39E+OO mis s 77 .11 9.70 4.35E-01 2.38E+OO miss 87.35 2.24 -3.90E-01 4.97E+OO miss 89.78 0.82 2.86E+OO 1.46E+Ol miss + Ra-226 186.21 3.64 1.90E-01 1.75E+OO 1.75E+OO free + Ac-228 129.0 7 2.42 -1.75E-01 4.84E-01 2.82E+OO 0.944 209.25 3.89 5.80E-01 1.77E+OO 0.978 270.24 3.46 1.1 9E+OO 2.19E+OO 0.955 328.00 2.95 7.41E-01 2.45E+OO 0.955 338.32 11. 27 6.3 5E-02 5. 96E-01 0.992 409.46 1. 92 3.lOE-01 3.38E+OO 0.937 463.00 4.40 2.35E-01 1. 61E+OO 0.933 794.95 4.25 7.97E-01 2.3 9E+OO 0.942 91 1. 2 0 25.80 1.43E-01 4.84E-01 0.990 964. 77 4.99 -8.07E-01 l.73E+OO 0.981 968.97 15.80 2.03E-01 8.23E-01 0.990 10/6/20 *~ 9:49:37AM Page 7 of7 Analysis Report for 06-0ct-16-10007 L3-10219A-FJGS-019SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCl/grams) (pCilgrams)

Corr Ac-22 8 1588.2 0 3.22 1.20E+OO 4.84E-01 4.31E+OO 1. 00 2 + Pa-23 1 27.36 10.30 -1.47E+OO 2.46E+OO 4.38E+OO 0.998 2 83.69 1. 70 8.94E-01 3.89E+OO 1. 000 300.07 2.47 1.66E-01 2.90E+OO 1. 000 302.65 2.20 -4.51E-01 2.46E+OO 1. 000 330.06 1. 40 -7.49E-01 3.36E+OO 1. 000 + Th-234 92.38 2.13 6.SlE-01 6.53E+OO 6.89E+OO free 92. 80 2.10 -3.12E+OO 6.53E+OO free 112. 81 0.2 1 3.49E-01 3.67E+Ol free + U-235 143.76 10.96 5.56E-0 1 1.2 1E-01 7.56E-01 free 163.33 5.08 -8.31E-02 1.17E+OO free 185.71 57.20 2.67E-02 1.2 1E-01 free 202 .11 1. 08 1.37E+OO 4.83E+OO miss 205.31 5.01 3.04E-01 l.15E+OO free + Am-241 59.54 35.90 -2.93E-01 1.59E+OO 1.59E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA vc1lue not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Vl .µ C: :::, 60 55 50 45 40 35 8 30 25 1000 2000 3000 0000016045 .CNF I 4000 channel 5000 Live Tille 300.000 sec Real Time 300.430 sec start: 1 -0.l(kev) stop : 8192 2047 .O(kev) Acq. Start Thu Oct 06 09: 26: 29 2 016 0 .... 6000 7000 8000 10/4/20 . _ 8:34:27 AM Page I of8 Analysis Report for 04-0ct-16-10001 L3-10219A-FJGS-020SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real lime Dead Time Peak Locate Threshold Peak Locate Range (in channels}

Peak Area Range (in channels}

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 04-0ct-16-10001

L3-10219A-FJGS-020SS

1 L 130G Soil Sample 1.045E+03 grams : Default : 9/28/2016 2:58:00PM

10/4/2016 8:10:51AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.17 % : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16012 PEAK WITH NID REPORT Peak Analysis Performed on 10/4/2016 8:15:53AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB 1.000FWHM t}.1~/1(

10/4/201\..

8:34:27AM Page 2 of8 Analysis Report for 04-0ct-16-10001 L3-10219A-FJGS-020SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide 1 185.80 738 -749 743.87 2.40E+Ol 1 5.69 3.00E+Ol Ra-226 2 238.68 949 -961 955.23 4.13E+Ol 16.36 1. 95E+Ol Pb-212 3 295.23 1177 -1185 1181.25 2.2 9E+Ol 13. 07 1.83E+Ol Pb-214 Eu-152 4 352.01 1402 -1414 1408.23 3.88E+Ol 14.65 l.2 5E+Ol Pb-214 Bi-211 5 609.2 6 2429 -2442 2436.80 3.16E+Ol 11. 84 2.80E+OO Bi-214 6 1460.66 5836 -5851 5843.61 5.70E+Ol 15.10 O.OOE+OO K-40 :J7)w' M = First peak in a multiplet region /o.,t{1r, m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION UB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{°./a)

Activity Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

10.66 6.70E+OO l.87E+OO miss Pb-212 1. 00 115.18 0.60 23 8.63

43.60 3.48E-01 l.49E-Ol free 300.09 3.30 Bi-214 1. 00 609.32

45.49 5.1 7E-01 2.04E-01 0.948 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120.2 9 14;92 1155. 2 1 1. 63 1238.12 5.83 1 2 80.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.2 1 2.13 1 661. 2 7 1. 05 1729.59 2.88 Analysis Report for 04-0ct-16-10001 L3-10219A-F J GS-020SS Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1764.49 1847.43 2 118.51 Pb-2 1 4 1. 00 2 41. 99 2 95.22 351.93 785.96 Ra-2 2 6 0.99 186.2 1 U-235 1. 00 143.76 163.33 185.71 202 .11 205.31 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 3. 64 10.96 5.08 57.2 0 1. 08 5.01 miss = Nuclide energy was not found in the coincidence library. 10/4/201\.

8:34:27AM Page 3 of8 Activity Activity Caine (pCi/grams)

Uncertainty Corr 5.23E-01 3.lOE-01 1.000 5 .13E-01 2. llE-01 free 2.16E+OO 1. 45E+OO f ree 1.37E-01 9.25E-02 free INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi/grams)

Uncertainty K-40 0.998 6.70E+OO 1.87E+OO X Bi-211 0.947 Pb-212 1. 000 3.48E-01 1. 49E-01 Bi-2 14 1. 000 5.17E-01 2.04E-01 Pb-214 1. 000 5.16E-01 1.74E-Ol ? Ra-2 2 6 0.990 2.1 6E+OO 1. 45E+OO ? fllf-,;.)..." 1.~ 9.~2 :fl'v' ,~-4,1t Analysis Report for 04-0ct-16-10001 L3-10219A-F JGS-020SS

? = nuclid e is part of an undetermined solution X = nuclid e rejected by the interference analysis @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/4/201..

8:34:27AM Page 4 of8 10/4/201t.

8:34:27AM Page S of8 Analysis Report for 04-0ct-16-10001

+ + + + + + + + + L 3-1 0219A-F J GS-020SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified. M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/4/2016 8:15:53AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nucl ide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield{%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCUgrams) (pCl/grams) (pCi/grams)

Corr K-40 1 460.82

10.66 6.70E+OO 3.1 8E-01 3.18E-01 miss Cr-51 320.08 9.91 -2.84E-01 7.75E-01 7.75E-01 free Mn-54 8 3 4.85 99.98 -2.02E-02 8.0 3E-02 8.03E-0 2 miss Co-58 810.76 99.45 2.82E-0 2 1.0 7E-01 1.07E-01 1.000 1674.7 3 0.52 O.OOE+OO 7.51E+OO 1. 024 Co-6 0 1173.23 99.85 1.14E-02 8.3':: E-02 8.37E-02 0.947 1332.49 99.98 2. 71E-02 1. 33E-01 0.947 Nb-94 70 2.65 99.81 -6.73E-03 5.94E-02 5.94E-0 2 0.944 871. 09 99.89 -3.26E-02 8.65E-02 0.944 Ag-108m 79.13 6.60 -5.97E-01 6.32E-02 2.30E+OO miss 433.94 90.50 -1.91E-02 6.32E-02 0.887 61 4.28 89.80 6.98E-03 8.lOE-02 0.886 72 2.94 90.80 3.21E-03 7.09E-02 0.887 Sn-113 2 55 .13 2 .11 5 .13E-01 1. 06E-01 3.28E+OO free 391.70 64.97 2.33E-02 1. 06E-Ol free Cs-134 475.36 1. 48 -2.57E-01 8.18E-02 4.76E+OO miss 563.25 8.34 -8.36E-0 2 l.06E+00 0.896 569.33 15.37 -1.15E-01 6.36E-01 0.888 604. 72 97.62 -7.60E-03 8.18E-0 2 0.931 10/4/2011..

8:34:27AM Page 6 of8 Analysis Report for 04-0ct-16-10001 L3-10219A-FJGS-020SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 -3.47E-02 8.18E-0 2 9.68E-02 0.933 801.95 8.69 8.03E-02 9.94E-01 0.898 1038.61 0.99 8.89E-01 7.85E+OO 0.943 1167. 97 1. 79 5.56E-01 4.09E+OO 1. 081 1365.19 3.02 2.2 6E-01 3.2 6E+OO 1.128 + Cs-137 6 61. 6 6 85.10 1.06E-01 1.83E-01 1.83E-01 miss + Eu-152 121. 7 8 2 8.67 -5.44E-02

1. 96E-Ol 2.37E-O l 0.936 2 44.70 7.61 2.63E-01 1. 0 6E+OO O. 935 2 95. 94 0.45 -1.18E+OO 2.77E+Ol miss 344.2 8 2 6.60 -8.64E-02 1.96E-01 0.957 367.79 0.86 -2.81E+OO 5.93E+OO 0.884 411.12 2.24 -4.15E-0 2 3.40E+OO 0.908 443.96 2.83 -1.2 6E-01 2.2 6E+OO 0.934 488.68 0.42 -1.41E+OO 1. 31E+Ol miss 563.99 0.49 -9.14E+OO 1.05E+Ol 0.934 586.26 0.46 -8.70E+OO 1.14E+Ol 0.94 2 678.62 0.47 2.22E+OO 1.65E+Ol 0.887 688.67 0.86 -l.49E+OO 8.2 8E+OO 0.980 719.35 0.28 3.93E+OO 2.57E+Ol miss 778. 90 12.96 3.70E-02 7.17E-01 0.945 810.45 0.32 9.94E+OO 2.99E+Ol 1.050 867.37 4.2 6 -3.70E-02 2.06E+OO 0.928 919.33 0.43 O.OOE+OO 5.89E+OO 0.981 964.08 14.65 1.31E-01 7. 57E-01 1. 022 1085.87 10.24 2.94E-01 1.05E+OO 1.018 1089.74 1.73 -6.21E-01 4.57E+OO 0.952 1112.07 13. 69 -7.64E-02 7.09E-01 0.992 1212.95 1. 43 -2.76E-01 8.93E+OO 0.929 1249.94 0.19 O.OOE+OO 1.46E+Ol 1.097 1 299.1 4 1. 63 7.49E-01 5.51E+OO 0.944 1 408.01 21. 07 1.18E-01 5.46E-01 0.983 1457.64 0.50 O.OOE+OO 3.2 6E+01 1.076 1528.10 0.28 O.OOE+OO 1.24E+Ol 1.007 + Eu-154 123.07 40.40 3.47E-02 1.99E-01 1.99E-01 0.934 247.93 6.89 -1.18E-01

8. 8.7E-01 0.928 591.76 4.95 -4.49E-01 1.lOE+OO 0.915 692.42 1. 78 O.OOE+OO 1. 23E+OO 0.936 723. 30 2 0.06 8.28E-02 3.84E-01 0.935 756.80 4.52 -3.55E-01 l.42E+OO 0.915 873.18 12.08 3 .13E-01 9.40E-Ol 0.932 996.2 9 10.48 -1.58E-01 6.98E-01 0. 971 1004.76 18.01 -4.59E-02 4.06E-01 0.978 1 2 74.43 34.80 -1.42E-02 3.09E-01 0.981 1596.48 1. 80 O.OOE+OO 1.72E+OO 1.175 + Eu-155 45.30 1. 31 1.27E+Ol 4.41E-01 5.47E+Ol 0.999 60.01 1. 22 7.87E+OO 5.39E+Ol 1. 000 86.55 3 0.70 6.02E-02 4.59E-01 free 105.31 2 1.10 -9.23E-02 4.41E-0 1 1. 000 + Tl-208 583.19 85.00 5.72E-02 1.53E-0 1 l.53E-01 0.932 + Bi-211 351.07

13.02 1.40E+OO 5.58E-01 5.58E-01 miss + Pb-2 11 404.85 3.78 6.06E-0 2 1.81E+OO 1.81E+OO mis s 10/4/201t-8:34:27AM Page 7 of8 Analysis Report for 04-0ct-16-10001 L3-10219A-FJGS-020SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCUgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 1.04E+OO 1. 81E+OO 4.61E+OO miss 832.0 1 3.5 2 6.86E-01 2.91E+OO miss + Bi-212 39.86 1. 06 -1.34E+OO 1.98E+OO 4.40E+Ol 0.998 727. 33 6.67 9.49E-01 l.98E+OO 0.98 2 785.37 1.10 4.56E+OO l.18E+Ol 0.944 1 620.50 1. 47 9.18E-01 6.75E+OO 1. 006 + Pb-2 12 115 .18 0.60 5.80E+OO 1.64E-01 1.50E+Ol miss 2 38.63

43.60 3.48E-0 1 1.64E-01 free 300.09 3.30 l.15E-0 1 1.94E+OO free + Pb212-XR 74.82 10.28 9.45E-01 1. 56E+OO 2.50E+OO miss 77 .11 17.10 3.31E-01 1.56E+OO miss 87.35 3.97 8.24E-01 3.41E+OO miss 89.78 1. 46 5.62E+OO 1.04E+Ol miss + Bi-2 1 4 609.32

45.49 5.17E-Ol l.41E-01 1.41E-01 0.948 768.36 4.89 7.12E-01 2.30E+OO 0.942 806.18 1. 26 -2.38E-01 5.26E+OO 0.923 934.0 6 3 .11 6.82E-01 3.78E+OO 0.944 1120.29 14.92 3.63E-01 l.llE+OO 0.944 1155. 2 1 1. 63 O.OOE+OO 1. 87E+OO 0.943 1238.12 5.83 4.33E-01 2.42E+OO 0.944 1 2 80.98 1. 43 7.2 0E-01 7.80E+OO 0.944 1377. 67 3.99 3.33E-01 3.14E+OO 1.030 1385. 31 0.79 6.42E+OO 1.93E+Ol 0.945 1401.5 2 1. 33 1.93E+OO 8.97E+OO 0.945 1407.99 2.39 l.08E+OO 5.00E+OO 0.945 1509.2 1 2 .13 O.OOE+OO 1. 72E+OO 0.950 1 66 1.27 1. 05 1. 32E+OO 9.72E+OO 1.001 1 729.59 2.88 4.43E-01 3.26E+OO 1.119 1 764.49 15.30 2.84E-01 l.02E+OO 1. 001 1 847.43 2.03 2.77E+OO 8.33E+OO 1.063 > 2118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 1 4 24 1.99 7.25 8.86E-01 2.04E-01 l.28E+OO 1.000 2 95.22

1 8.42 5.2 3E-01 3.97E-01 1. 000 351.93

35.60 5 .13E-01 2.04E-01 free 785.96 1. 06 3.27E+OO 1.09E+Ol 1. 000 + Pb214-XR 74.8 2 5.8 0 1.67E+OO 2.74E+OO 4.43E+OO miss 77 .11 9.7 0 5.83E-01 2.74E+OO miss 87.35 2.24 l.46E+OO 6.05E+OO miss 89.78 0.82 1.00E+Ol 1.86E+Ol miss + Ra-226 186.2 1

3.64 2.16E+OO 2.06E+OO 2.06E+OO free + Ac-228 129.07 2.4 2 -3.23E-01 6.19E-Ol 3.21E+OO 0.944 209.25 3.89 3.87E-01 1.77E+OO 0.978 270.24 3.46 l.18E+OO 2.35E+OO 0.955 3 2 8.00 2.95 -2.24E-01 l.72E+OO 0.955 338.32 11.27 3.38E-01 6.85E-01 0.992 409.46 1. 92 -l.1 7E-0 1 3.50E+OO 0.937 463.00 4.40 2.0 3E-01 2.09E+OO 0.933 794.95 4.25 6.88E-02 2.48E+OO 0.942 911. 20 25.80 2.40E-01 6.19E-01 0.990 964.77 4.99 1.16E+OO 2. 72E+OO 0.981 968. 97 15.80 9.74E-02 6.51E-01 0.990 10/4/20~ ... 8:34:27AM Page 8 of8 Analysis Report for 04-0ct-16-10001 L3-10219A-F J GS-020SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Colnc Name (keV) (pCi/grams) (pCl!grams) (pCilgrams)

Corr hc-22 8 1588.20 3.22 8.45E-01 6.1 9E-01 4.46E+00 1. 00 2 + Pa-231 27.36 10.30 2. 13E+OO 2.59E+OO 6.27E+00 0.998 2 83.69 1. 70 -1.03E+OO 3.63E+OO 1.000 300.07 2.47 1. 54E-01 2.5 9E+OO 1. 000 302.65 2.2 0 8.20E-01 2.92E+OO 1. 000 330.06 1. 40 -1.68E+OO 3.00E+OO 1. 000 + Th-234 92.38 2.13 3.55E+OO 6.77E+OO 6.90E+OO free 92.80 2.10 2.58E+OO 6.77E+OO free 112. 81 0.2 1 -2.3 6E+Ol 3.48E+Ol free + U-235 143.76 10.96 -4.49E-02 1.31E-01 6.17E-01 free 163.33 5.08 5.21E-02 1. 2 6E+00 free 185.71

57.20 1.37E-01 l.31E-01 free 202 .11 1. 0 8 7.28E-01 6.14E+OO miss 205.31 5.01 1. 88E-01 1.09E+OO free + Am-241 59.54 35.90 -6.87E-02 1. 79E+OO 1.79E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 V) ...... C: ::I 8 30 25 20 15 :§ I "' "" "' .... '"" I :::, '"" ...... J: a.. 1000 2000 3000 0000016012.CNF 4000 channel 5000 Live Ti m e :300.000 sec Real Time :300.510 sec start: 1: -0.l(kev) stop : 8192: 2047. O(kev) Acq. start :Tue Oct 04 08:10:51 2016 6000 7000 8000 10/4/20 . -8:52: 53AM ~~~ex-Gamma Analysis Report for 04-0ct-16-10002 L3-10219A-FJGS021 SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 04-0ct-16-10002

L3-10219A-FJGS021SS

1 L 130G Soil Sample 1.187E+03 grams : Defau lt : 9/28/2016 3: 07:00PM : 10/4/2016 8:21:03AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.18 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM : 1/27/2016

1/5/2015 : 16013 PEAK WITH NID REPORT Peak Analysis Performed on 10/4/2016 8:34:33AM Peak Analysi s From Channel : 120 Peak Analysi s To Channel : 8192 Tentative NID Library Peak Match Toleranc e : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of7 10/4/201'

.. 8:52:53AM Page 2 of7 Analysis Report for 04-0ct-16-10002 L3-10219A-F J GS021 SS Peak Energy ROI No. (keV) start 1 238.51 950 -2 295 .13 1176 -3 351. 72 1401 -4 1460.60 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1186 1414 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.55 3.12E+Ol 16.98 3.36E+Ol 1180.84 2.16E+Ol 14.22 2.28E+Ol 1407.08 5.15E+Ol 16.37 1.30E+Ol 5843.35 8.32E+Ol 18.98 5.59E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 0.99 1460.82 Pb-212 0.99 115 .18 238.63 300.09 Pb-214 0.99 241.99 295.22 351.93 785. 96 = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 10.66 0.60 43.60 3.30 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. Activity (pCi/grams) 8.60E+OO 2.32E-01 4.35E-01 6.00E-01 Activity Uncertainty 2.lOE+OO 1. 32E-01 2.95E-01 2 .13E-01 Tentative Nuclide Pb-212 Pb-214 Eu-152 Pb-214 Bi-211 K-40 Coinc Corr miss f ree 1. 000 free 10/4/2011, 8:52:53AM Analysis Report for 04-0ct-16-10002 L3-10219A-FJGS021 SS INTERFERENCE CORRECTED REPORT Nuclide Name K-40 X Bi-2 11 Pb-21 2 Pb-214 Nuclide Id Confidence 0.997 0.974 0.999 0.998 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 8.60E+OO 2.32E-01 5.43E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 2.lOE+OO 1. 32E-01 l.73E-01 Page 3 of7 Comments 10/4/201t.

8:52:53AM Page 4 of7 Analysis Report for 04-0ct-16-10002

+ + + + + + + + + L3-10219A-FJGS021SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/4/2016 8:34:33AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (kGV} (pCl/grams) (pCilgrams) (pCi!grams)

Corr K-40 1460.82

10.66 8.60E+OO 1.1 7E+OO 1.1 7E+OO miss C r-51 320.08 9.91 -2.50E-02 5. 96E-01 5. 96E-01 free Mn-54 834.85 99.98 -8.88E-03 7.07E-02 7.07E-02 miss Co-58 810.76 99.45 l.14E-02 9.42E-02 9.42E-02 1. 000 1674.73 0.52 2.44E+OO l.80E+Ol 1. 024 Co-60 1173.2 3 99.85 -1.14E-02 7.37E-02 7.37E-0 2 0.947 13 32.49 99.98 1.09E-02 8. OlE-0'.2 0.947 Nb-94 702.65 99.81 -2.0lE-02 2.22E-02 5.23E-02 0.944 871.09 99.89 O.OOE+OO 2.22E-02 0.944 Ag-108m 79 .13 6.60 l.33E-01 6.45E-02 2. 72E+OO mis s 433.94 90.50 1.36E-02 6.45E-02 0.887 614.2 8 89.80 2.92E-02 1.0lE-01 0.886 722. 94 90.80 9.18E-03 7.87E-02 0.887 Sn-113 255 .13 2 .11 8.70E-01 7.68E-02 3.12E+OO free 391.70 64.97 -8.56E-03 7.68E-02 free Cs-134 475.36 1. 48 -7.67E-01 8.04E-02 3.24E+OO miss 563.25 8.34 -1.55E-02 7.20E-01 0.896 569.33 15.37 8.98E-02 5 .13E-01 0.888 604.72 97.62 2.17E-02 8.04E-02 0.931 1Q/4/2Q1L 8: 52: 53AM Page 5 of7 Analysis Report for 04-0ct-16-10002 L3-10219A-FJGS021SS Nuclide Energy Yield{%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi!grams) (pCl!grams) (pC//grams)

Corr Cs-134 7 95.86 85.46 3.26E-02 8.04E-02 1.29E-01 0.933 801. 95 8.69 -6.28E-02 6.94E-01 0.898 1 038.6 1 0.99 -1.56E+OO 6.91E+OO 0.943 11 67. 97 1. 79 O.OOE+OO 1.32E+OO 1. 081 1365.19 3.02 6.19E-01 2.87E+00 1.128 + Cs-137 661. 66 85.10 6.93E-02 1.3 7E-0 1 1.37E-01 miss + Eu-152 121. 78 28.67 -8.83E-02 1.40E-0 1 2.55E-01 0.936 244.70 7.61 -2.61E-01 7.72E-01 0.935 2 95. 94 0.45 2.99E+OO 2.3 4E+01 miss 344.2 8 2 6.60 -1.99E-0 2 2. llE-01 0.957 367.79 0.86 1.09E+O O 8.44E+OO 0.884 411.12 2.2 4 -2.05E-01 2.12E+OO 0.908 443.96 2.83 4.93E-02 1.99E+00 0.934 488.68 0.42 2.74E+OO 1.75E+Ol miss 56 3.99 0.49 -5.03E+OO 9.26E+OO 0.934 586.2 6 0.46 2.74E+OO 1.64E+01 0.94 2 678.62 0.47 -7.82E-01

1. lSE+Ol O. 887 688.67 0.86 5.23E-01 7.29E+OO 0.980 719.35 0.28 1.63E+OO l.80E+01 miss 778. 90 12.96 -4.88E-03 7.04E-01 0.945 810.45 0.32 6.93E+OO 2.87E+01 1. 050 867.3 7 4.26 2.28E-01 2.lOE+OO 0.928 919.33 0.43 -1.60E+OO l.41E+Ol 0.981 964. 08 14.65 O.OOE+OO 1.50E-0 1 1. 02 2 1.0 85.87 10.2 4 2.59E-01 9.28E-01 1. 018 1089.74 1. 73 -1.1 7 E-01 5.08E+00 0.952 1112.0 7 13.69 -6. 72E-02 6.2 4E-01 0.992 1212.95 1. 43 -1.67E+OO 5.37E+OO 0.929 1 249.94 0.19 6.79E-01 4.42E+01 1.097 1299.14 1. 63 5.65E-01 4.85E+OO 0.944 1408.01 2 1. 07 O.OOE+OO 1.40E-01 0.983 1457.64 0.50 -1.66E+01 3.97E+01 1. 07 6 1528.10 0.2 8 2.30E+OO 3.74E+Ol 1. 007 + Eu-1 54 1 23.07 40.40 1.90E-02 1.99E-01 1. 99E-01 0.934 2 47.93 6.89 -1.09E-01 9.06E-01 0.928 591.76 4.95 6.58E-0 2 1.58E+OO 0.915 692.42 1. 78 -2.2 6E+O O 2.94E+OO 0.936 723. 30 2 0.06 1. 09E-0 1 3.92E-01 0.935 756.8 0 4.52 O.OOE+OO 4.61E-01 0.915 873.1 8 12.08 -2.30E-02 5.07E-01 0.932 996.29 10.48 1.04E-01 7.75E-0 1 0.971 1004.76 18.01 -l.86E-01 3.57E-01 0. 978 1274.43 34.80 2.93E-0 2 2.15E-01 0.981 1596.48 1. 80 O.OOE+OO 1.52E+OO 1.175 + Eu-155 45.30 1. 3 1 -1.37E+O l 3.5'7E-01 3.60E+Ol 0.999 60.0 1 1. 22 6.49E+OO 4.06E+Ol 1.000 , 86.55 30.70 -9.80E-02 3.57E-O l free 105.31 2 1.10 6.92E-02 3.76E-01 1. 000 + Tl-208 583.19 85.00 7.30E-0 2 1. 40E-01 1.40E-01 0.932 + Bi-211 351.07

1 3.02 1.64E+OO 4.98E-01 4.98E-01 miss + Pb-211 404.85 3.78 1.64E-01 5.76E-01 1.46E+OO miss 10/4/201'..

8:52:53AM Page 6 of7 Analysis Report for 04-0ct-16-10002 L3-10219A-FJGS021 SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 -1.62E-01 5.76E-01 2.91E+OO miss 832.01 3.5 2 O.OOE+OO 5.76E-01 miss + Bi-212 39.86 1. 06 -6. llE+OO 7.70E-01 3.87E+Ol 0.998 727. 33 6.67 O.OOE+OO 7.70E-01 0.98 2 785.37 1.10 1.62E+OO 9.78E+OO 0.944 1620.50 1. 47 O.OOE+OO 2.19E+OO 1. 006 + Pb-212 115.18 0.60 1. 25E+OO 1.76E-01 l. llE+Ol miss 238.63 "" 43.60 2.32E-01 1.76E-01 free 300.09 3.30 2.16E-01 1.80E+OO free + Pb212-XR 74.82 10.2 8 4.13E-01 1. 4 7E+OO 2.08E+OO miss 77 .11 17.10 7. 77E-01 1.47E+OO miss 87.35 3.97 9.09E-01 3.08E+OO mi ss 89.78 1. 46 2.05E+OO 8.82E+OO miss + Bi-214 609.32 45.49 3.80E-01 3.98E-01 3.98E-01 0.948 768.36 4.89 7.2 0E-01 2.32E+OO 0.94 2 806.18 1. 2 6 -5.2 4E-01 4.63E+OO 0.92 3 934.06 3.11 8.43E-01 3.33E+OO 0.944 1120.2 9 14.92 2.87E-01 1.08E+OO 0.944 1155.21 1. 63 5.20E-01 7.2 9E+OO 0.94 3 1238.12 5.83 7.21E-01 2.3 3E+OO 0.944 1280.98 1. 43 7.92E-01 6.87E+OO 0.944 1377. 67 3.99 2.3 8E-01 2.3 8E+OO 1.0 3 0 1385.31 0.79 -4.04E-01 1.31E+Ol 0.945 1401.52 1. 33 -4.86E-01 6.2 6E+OO 0.945 1407.99 2.39 O.OOE+OO 1. 2 8E+OO 0.945 1509.2 1 2 .13 1.12E+OO 5.19E+OO 0.950 1661. 2 7 1. 05 2.33E+OO 1.08E+Ol 1.001 17 2 9.59 2.88 O.OOE+OO l.06E+OO 1.119 1764.49 15.30 5.2 1E-02 7.74E-01 1. 001 1847.43 2.03 O.OOE+OO 1.65E+OO 1. 063 > 21 18.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 241.99 7.25 3.81E-01 1.82E-0 1 1. 13E+OO 1.000 295.22

18.42 4.35E-01 4.llE-01 1. 000 351.93

35.60 6.00E-01 1.82E-01 free 785.96 1. 06 1.78E+OO 9.60E+OO 1. 000 + Pb214-XR 74.82 5.80 7.3 1E-01 2.59E+OO 3.68E+OO miss 77 .11 9.70 1.37E+OO 2.59E+OO mis s 87.35 2.2 4 1.61E+OO 5.47E+OO mi ss 89.78 0.82 3.65E+OO 1.57E+Ol miss + Ra-226 186.21 3.64 2.97E-01 1.69E+OO l.69E+OO free + Ac-228 129.07 2.42 2.39E-01 4.69E-01 2.74E+OO 0.944 209.25 3.89 -3.58E-01 1.27E+OO 0.978 270.24 3.46 9.87E-01 2.38E+OO 0.955 328.00 2.95 4.02E-01 2. llE+OO 0.955 338.32 11. 2 7 l.89E-01 7.2 8E-01 0.99 2 409.46 1. 92 3.85E-01 3.08E+OO 0.937 463.00 4.40 -2.45E-02 1. 32E+OO 0.933 "794.95 4.2 5 5.45E-02 2.38E+OO 0.942 911.2 0 2 5.80 1.79E-Ol 4.69E-01 0.990 964. 77 4.99 -1.13E-01 1. 25E+OO 0.981 968.97 15.80 3.73E-01 7.99E-01 0.990 10/4/201~

8:52:53AM Page 7 of7 Analysis Report for 04-0ct-16-10002 L3-10219A-FJGS021 SS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi!grams)

Corr A.c-22 8 1588.20 3.22 O.OOE+OO 4.69E-01 9.87E-01 1. 002 + Pa-23 1 27.36 10.30 3.04E-01 2.41E+OO 5.52E+OO 0.998 283.69 1. 70 9.62E-01 3.70E+OO 1. 000 30 0.0 7 2.47 2.89E-01 2.41E+OO 1.000 302.65 2.2 0 -l.71E-01 2.57E+OO 1. 000 330.06 1. 40 -3.41E-01 3.41E+OO 1. 000 + Th-234 92.38 2.1 3 1. 04E+OO 6.38E+OO 6.3 8E+OO free 92. 80 2.10 2.00E+OO 6.42E+OO free 11 2. 81 0.2 1 -4.08E+OO 3.84E+Ol free + U-235 143.76 10.96 -1. 29E-01 l.OlE-0 1 5.2 6E-01 free 163.33 5.08 -l.18E-01 1. 03E+OO free 1 85.7 1 57.2 0 3.60E-0 3 l.OlE-01 free 2 02 .11 1. 08 -l.85E-01 4.63E+OO miss 2 05.31 5.01 -2.86E-01 1. OOE+OO free + Arn-241 59.54 35.90 8.lOE-02 l.51E+OO 1. 51E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) ,1,-1 C: ::I 60 55 50 45 40 35 B 30 25 1000 2000 3000 0000016013.CNF 4000 channel 5000 Live Time :300.000 sec Real Time : 300. 530 sec start: 1: -0. l(kev) stop : 8192:2047.0(kev)

Acq. Start :Tue oct 04 08:21:03 2016 6000 7000 8000 10/4/21., ,., 9:11 : 20AM Analysis Report for 04-0ct-16-10003 L3-10219A-FJGS-022SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 04-0ct-16-10003

L3-10219A-FJGS-022SS

1 L 130G Soil Sample 1.137E+03 grams : Default : 9/28/2016 3: 11:00PM : 10/4/2016 8:35:22AM

130G 1 L Soil Sample : JWelc h : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.17 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16014 PEAK WITH NID REPORT Peak Analysis Performed on 10/4/2016 8:52:59AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB : 1.000FWHM Page 1 of7 Analysis Report for 04-0ct-16-10003 L3-10219A-FJGS-022SS Peak Energy ROI No. (keV) start 1 238.71 949 -2 609.37 2 433 -3 911.00 3639 -4 1460.63 5838 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 2 442 3649 5850 10/4/201 ... 9:11:20AM Peak Net Peak NetArea Centroid Area Uncertainty 955.33 2.43E+Ol 16.50 2437.21 1.77E+Ol 10.32 3643. 72 1. 96E+Ol 9.44 5843.50 4.95E+Ol 14.45 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Page 2 of 7 Continuum Tentative Counts Nuclide 3.34E+Ol Pb-212 8.64E+OO Bi-21-1 2.86E+OO Ac-228 2.95E+OO K-40 Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

10.66 5.35E+OO 1.63E+OO miss Pb-21 2 1. 00 115 .18 0.60 2 38.63

43.60 l.88E-01 1.32E-01 free 300.09 3.30 Bi-214 1. 00 609.32

45.49 2.66E-01 1.59E-01 0.948 768.36 4.89 806.18 1. 2 6 934.06 3 .11 11 2 0.2 9 14.92 1155.21 1. 63 123 8.12 5.83 1 2 80.98 1. 43 1 3 77.67 3.99 1 3 85.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1661.27 1. 05 17 2 9.59 2.88 1764.49 15.30 1847.4 3 2.03 2 118.51 1.16 Ac-2 2 8 0.91 129.07 2.4 2 209.25 3.89 Analysis Report for 04-0ct-16-10003 L3-10219A-F JGS-022SS Nuclide Id Energy Name Confidence (keV) Ac-228 0.91 270.24 328.00 338.32 409.46 463.00 794.95 911.20 964. 77 968.97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 3.46 2.95 11.27 1. 92 4.40 4.25 25.80 4.99 15.80 3.2 2 miss = Nuclide energy was not found in the coincidence library. 10/4/20*,. 9:11 :20AM Page 3 of7 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 6.42E-01 3.15E-01 0. 990 INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Pb-212 Bi-214 Ac-228 Nuclide Id Confidence 0.998 1. 000 1.000 0.918 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 5.35E+OO l.88E-01 2.66E-Ol 6.42E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty l.63E+00 1. 32E-01 l.59E-01 3.15E-01 10/4/20*,_ 9:11:20AM Page 4 of7 Analysis Report for 04-0ct-16-10003

+ + +

+ + + + + + L3-10219A-FJGS-022SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified. M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/4/2016 8:52:59AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCilgrams) (pCUgrams) (pCl!grams)

Corr K-40 1460.82

10.66 5.35E+OO 8.73E-01 8.73E-01 miss C r-5 1 320.08 9.91 O.OOE+OO 5.70E-01 5.70E-01 free Mn-54 834.85 99.98 9.27E-03 8.56E-02 8.5GE-02 miss Co-58 810.76 99.45 -6.82E-03 6.02E-02 6. 02E-02 1. 000 1 674.73 0.52 O.OOE+OO 6.91E+OO 1. 024 Co-60 1173.2 3 99.85 O.OOE+OO 2.83E-02 2.83E-02 0.947 1332.49 99.98 O.OOE+OO 3.07E-02 0.947 Nb-94 702.65 99.81 1.48E-0 2 6.30E-02 7.99E-02 0.944 871. 09 99.89 -3.57E-02 6.30E-0')

0.944 Ag-108m 79.13 6.60 6.86E-01 5.81E-02 2.59E+OO miss 433.94 90.50 -6.25E-03 5.81E-02 0.887 614.2 8 89.80 2.41E-02 8.63E-02 0.886 722.94 90.80 8.48E-03 1.06E-01 0.887 Sn-113 255 .13 2 .11 9 .13E-01 1.18E-01 3.02E+OO free 391.70 64. 97 2.33E-02 l.18E-01 free Cs-134 475.36 1. 48 -1.82E-01 8.39E-02 3.38E+OO miss 563.2 5 8.34 3.33E-01 1.06E+OO 0.896 569.33 15.37 O.OOE+OO 1. 21E-01 0. 888 604.72 97.62 -1.0lE-02 8.39E-02 0.931 10/4/20*,~ 9:11:20AM Page 5 of7 Analysis Report for 04-0ct-16-10003 L3-1 0219A-FJ GS-022SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi!grams) (pCilgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 2.83E-02 8.39E-0~ l.lSE-01 0.933 801.95 8.69 1. 64E-02 9.14E-01 0.898 1038.61 0.99 -6.53E-01

1. 06E+Ol 0.943 1167.97 1. 79 2.92E-01 4.74E+OO 1.081 1365.19 3.0 2 O.OOE+OO 8.74E-01 1.128 + Cs-137 661.66 85.10 7.23E-0 2 1.37E-01 1.3 7E-01 miss + Eu-15 2 121. 78 2 8.67 -2.97E-02 1.46E-01 2.35E-01 0.936 244.70 7.61 -2.02E-01 7.26E-0 1 0.935 295.94 0.45 9.06E+OO 2.08E+Ol mis s 344.2 8 2 6.60 1. 51E-02 2.0lE-01 0.957 367.79 0.86 3.99E+OO 9.31E+OO 0.884 411.12 2.2 4 -1.43E-01 2.56E+OO 0.908 443. 96 2.83 8.2 7E-01 2.53E+OO 0.934 488.68 0.42 1.56E+OO 1.40E+Ol miss 563.99 0.49 9.19E+OO 1.97E+Ol 0.934 586.26 0.46 l.14E+OO 1.54E+Ol 0.94 2 678.62 0.47 1.36E+OO 1. 2 0E+Ol 0.887 688.67 0.86 -1.82E-01 8.82E+OO 0.980 719.35 0.28 -1.02E+Ol l.87E+Ol miss 778.90 12.96 5.lOE-02 5.68E-01 0.945 810.45 0.3 2 -1.52E+OO

1. 68E+Ol 1. 050 867.37 4.2 6 O.OOE+OO 5.52E-01 0.928 919.33 0.43 6.67E-01 1.47E+Ol 0.981 964.0 8 14.65 3.86E-0 2 4.2 6E-01 1. 02 2 1085.87 10.2 4 1.3 5E-0 1 8.3 6E-01 1. 018 1089.74 1. 73 1.14E+OO 5.30E+OO 0.952 111 2.07 13.69 -1.00E-02 5.16E-01 0.992 1212.95 1. 43 -3.48E+OO 5.61E+OO 0.929 1 2 49.94 0.19 -3.19E+OO 4.61E+01 1. 097 1299.14 1. 63 -1.67E+OO 5.07E+OO 0.944 1408.01 2 1. 07 O.OOE+OO 1.46E-01 0.983 1457.64 0.50 -4.32E+Ol 2.55E+Ol 1. 07 6 1528.10 0.2 8 7.50E+OO 3.90E+Ol 1. 007 + Eu-154 123.07 40.40 3.13E-02 l.83E-01 1.83E-01 0.934 247.93 6.89 -1.36E-02 9.45E-01 0.9 28 5 91. 7 6 4.95 2.75E-01 1.2 8E+OO 0.915 692.42 1. 78 -9. 72E-01 3.87E+OO 0.936 72 3. 30 20.06 -4.0lE-02 4.09E-01 0.935 756.80 4.52 5.33E-01 1.91E+OO 0.91 5 873.18 12.08 l.36E-01 7.74E-01 0.932 996. 2 9 10.48 7.75E-02 9.38E-01 0. 971 1004.76 18.01 1. 75E-01 6.08E-01 0.978 1274.43 34.80 8.73E-0 3 3.2 9E-01 0.98 1 1 596.48 1. 80 O.OOE+OO 1.58E+OO 1.175 + Eu-155 45.30 1. 31 2.50E+OO 3.02E-01 3.97E+Ol 0.999 60.01 1. 22 8.90E+OO 4.78E+01 1. 000 86.55 30.70 1.2 6E-01 3.98E-01 free 105.31 21.10 -1.89E-01 3.02E-0 1 1. 000 + Tl-208 583.19 85.00 6.48E-02 1.3 0E-01 1.30E-01 0.932 + Bi-211 351.07 13.02 2.36E-01 7.08E-01 7.08E-01 mis s + Pb-211 404.85 3.78 5. llE-01 1.64E+OO 1.66E+OO miss 10/4/20*1~

9:11:20AM Page 6 of7 Analysis Report for 04~0ct-16-10003 L3-10219A-FJGS-022SS Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCl!grams)

Corr Pb-211 427.09 1. 76 -5.64E-01 1.64E+OO 3.04E+00 mis s 832.01 3.52 -2.2 2E-01 1.64E+OO miss + Bi-212 39.86 1. 06 9.2 6E+OO 1. 54E+OO 4.90E+Ol 0.998 727. 33 6.67 5.04E-01 1.54E+OO 0.982 785.37 1.10 -1.69E+OO 5.33E+00 0.944 1620.50 1. 47 O.OOE+OO 2.28E+OO 1. 006 + P b-2 1 2 115 .18 0.60 2.83E+OO 1. 90E-01 l.31E+Ol miss 238.63

43.60 l.88E-01 l.90E-01 free 300.09 3.30 2.19E-01 2.06E+OO free + Pb212-XR 74.82 10.2 8 -3.64E-01 1.46E+OO 1.71E+00 miss 77 .11 17.10 7.05E-Ol l.46E+00 miss 87.35 3.97 l.84E+OO 3.53E+00 mis s 89.78 1. 46 2.07E+OO 7.55E+OO mis s + Bi-214 609.3 2

45.49 2.66E-01 1.85E-01 1.85E-01 0.948 768.36 4.89 2.68E-0 2 1.50E+00 0.94 2 806.1 8 1. 2 6 7.67E-01 7.07E+00 0.923 934.06 3 .11 O.OOE+OO 7.83E-01 0.944 1120.2 9 14.9 2 3.71E-01 1.02E+OO 0.944 1155.2 1 1. 63 -9.06E-02 4.66E+00 0.943 1238.1 2 5.83 5.83E-01 2.43E+OO 0.944 1280.98 1. 43 -6.62E-01 5.68E+00 0.944 1377.67 3.99 5.3 6E-01 2.49E+00 1. 030 1385. 31 0.79 O.OOE+OO 3.99E+OO 0.945 1401.52 1. 33 O.OOE+OO 2.40E+OO 0.945 1407.99 2.39 0.00E+OO 1.34E+OO 0.945 1509.2 1 2 .13 5.83E-01 4.2 9E+OO 0.950 1661.2 7 1. 05 2.43E+OO 1.13E+Ol 1. 001 1 72 9.59 2.88 O.OOE+OO 1.lOE+OO 1.119 1764.49 15.30 6.09E-01 1. 31E+OO 1. 001 1847.43 2.03 6.37E-01 4.69E+00 1. 063 > 2 118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 2 41.99 7.25 2.68E-01 2.92E-01 1.00E+OO 1. 000 2 95.22 18.42 4.32E-01 5.65E-01 1. 000 3 51. 93 35.60 1.94E-01 2.92E-01 free 785.96 1. 06 -l.18E-01 5.23E+OO 1. 000 + Pb214-XR 74.82 5.80 -6.44E-01 2.57E+OO 3.03E+OO miss 77 .11 9.70 1. 24E+OO 2.57E+00 miss 87.35 2.24 3.27E+OO 6.2 6E+OO miss 89.78 0.82 3.69E+OO l.35E+Ol miss + Ra-226 186.21 3.64 1.07E+OO 1. 99E+OO 1.99E+OO free + Ac-228 129.07 2.42 6.64E-01 2.65E-01 2.86E+OO 0.944 209.25 3.89 3.97E-01 1. 83E+00 0.978 270.2 4 3.46 8.0SE-01 2.30E+OO 0.955 32 8.00 2.95 -1.65E-01 1.93E+OO 0.955 33 8.3 2 11. 27 3.26E-01 7.36E-01 0.992 409.46 1. 92 7.15E-0 2 2.89E+OO 0.937 463.00 4.40 8.98E-01 2.03E+OO 0.9 33 794.95 4.25 -3.16E-01 1. 76E+OO 0.942 911. 20

2 5.80 6.42E-01 2.65E-01 0.990 964. 77 4.99 O.OOE+OO 4.79E-01 0.981 968.97 15.80 1.78E-01 7.84E-01 0.990 10/4/20*,~ 9:11:20AM Page 7 of? Analysis Report for 04-0ct-16-10003 L3-10219A-FJGS-022SS Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Coinc Name (keV) (pCilgrams) (pCl/grams) (pCi/grams)

Corr Ac-228 1588.20 3.22 3.81E-01 2.65E-0 1 2.80E+OO 1.002 + Pa-231 27.36 10.30 -7.62E-01 2.52E+OO 4.16E+OO 0.998 283.69 1. 70 -1. llE-01 3.33E+OO 1. 000 300.07 2.47 2.93E-01 2.7GE+OO 1. 000 302.65 2.20 9.46E-0 1 2.52E+OO 1. 000 330.0 6 1. 40 -3.56E-0 1 4.46E+OO 1. 000 + Th-234 92.38 2 .13 -4.83E-02 5.0SE+OO 5.0SE+OO free 92.80 2.10 -8.76E-01 5.08E+OO free 112. 81 0.21 2.32E+OO 3.86E+Ol free + U-235 143.76 10.96 8.27E-02 1.2 6E-01 5.12E-01 free 163.33 5.08 -3.07E-01 8.37E-01 free 185. 71 57.2 0 4.83E-02 1.2 6E-01 free 2 02 .11 1. 08 2.42E+00 5.05E+OO miss 2 05.31 5.01 7.26E-01 1. 34E+OO free + Am-241 59.54 35.90 8.45E-01 1.88E+OO 1.88E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 V) .J.-1 C: ::::J 8 30 25 20 15 ft~' ...... ' ..Q D.. 1000 2000 3000 0000016014.CNF 4000 channel 5000 Live Tfae :300.000 sec Real Time :300.510 sec start: 1: -0. l(kev) stop : 8192: 2047 .O(kev) Acq. Start :Tue oct 04 08: 35: 22 2016 6000 7000 8000 10/10/2016 1:46:34PM Analysis Report for 10-0ct-16-10014 L3-10219A-FQGS-006SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance

10-0ct-16-10014

L3-10219A-FQGS-006SS

1 L 130G Soil Sample 1.250E+03 grams : Default : 10/3/2016 9:10:00PM

10/10/2016 1 :40:56PM : 130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 300.0 seconds : 300.2 seconds : 0.06% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016 Page I of7 /~ Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 6/28/2012

~(,,~ltt : 16070 PEAK WITH NID REPORT Peak Analysis Performed on 10/10/2016 1 :45:59PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce Vk.-A { c.J:.d-~.J) ,o/~,~ : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL. NLB : 1.000FWHM 10/10/2016 1 :46:34PM Page 2 of7 Analysis Report for 10-0ct-16-10014 L3-10219A-FQGS-006SS Peak Energy ROI No. (keV) start 1 163 .11 650 -2 238.61 949 -3 352.16 1401 -4 583.23 2327 -5 609.46 2430 -6 1461.03 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 656 960 1414 23 36 2443 5853 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 653.14 6.71E+OO 9.37 1.46E+01 954.76 2.95E+01 2 1.52 6.90E+01 1408. 45 3.74E+01 14.27 1. llE+Ol 2 331.91 2.lOE+Ol 1 0.93 8.06E+OO 2 436.79 4.45E+01 13.91 3.03E+OO 5843.45 8.47E+01 18.74 2.68E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams)

Uncertainty K-40 0.99 1460.82

10.66 7.49E+OO 1. 78E+OO Tl-208 1. 00 583.19

85.00 1.25E-01 6.67E-02 Bi-211 0. 92 351.07

13. 02 1.02E+OO 4.22E-01 Pb-2 1 2 1. 00 115.18 0.60 23 8.63

43.60 1. 85E-01 1.38E-01 300.09 3.30 Bi-214 0.99 609.32

45.49 5.09E-01 1.71E-01 768.36 4.89 806.18 1.2 6 934.06 3.11 11 2 0. 2 9 14.92 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401. 52 1. 33 1407.99 2.39 1509.2 1 2.13 1661. 2 7 1. 05 1729.59 2.88 Tentative Nuclide ~ft/~/,}~

Pb-212 Pb-214 Bi-211 Tl-208 Bi-214 K-40 .f'l"_., /tJAf-'1~

Caine Corr miss miss mis s miss miss Analysis Report for 10-0ct-16-10014 L 3-10219A-FQGS-006SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1764.49 1847.43 2118.51 Pb-214 0.99 241.99 295.22 351.93 785.96 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 15.30 2.03 1.16 7.25 1 8.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/10/2016 1 :46: 34PM Page 3 of7 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 3.73E-01 l.54E-01 mis s INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Tl-208 ? Bi-2 11 Pb-21 2 Bi-214 ? Pb-214 Nuclide Id Confidence 0.997 1. 000 0. 929 1.000 0.999 0.998 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 7.49E+OO l.25E-Ol 1. 02E+OO l.85E-01 5.09E-01 3.73E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty l.78E+OO 6.67E-02 4.2 2E-01 1. 3 8E-01 l.71E-01 l.54E-01 10/10/2016 1 :46:34PM Analysis Report for 10-0ct-16-10014

+ + + + + + + + + L3-10219A-FQGS-006SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 1 163.11 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 1 :45:58PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 2.23810E-02 Peak Type Tol. NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (keV) (pCl/grams) (pCi/grams) (pCi/grams)

K-40 1460.8 2

10.6 6 7.49E+O O 7.58E-01 7.58E-01 Cr-51 3 20.08 9.9 1 -1.98E-03 5.20E-01 5.20E-01 Nn-54 834.85 99.98 1.63E-03 6.07E-0 2 6.07E-02 Co-58 810.76 99.45 1.13E-03 6.2 9E-02 6.29E-0 2 1 674.73 0.52 O.OOE+OO 5.84E+OO Co-60 117 3.23 99.85 1. 31E-02 8.18E-02 8.73E-02 13 32.49 99.98 1.76E-02 8.18E-02 Nb-94 702.65 99.8 1 -6.38E-04 6.16E-02 8.lOE-02 871.09 99.89 -7.1 8E-03 6.1 6E-02 Ag-108m 79.13 6.60 -3.23E-01 1.74E-02 1.55E+OO 433.94 90.50 2.44E-02 6.41E-02 614.28 89.80 -7.00E-03 4.29E-02 722.94 90.80 O.OOE+OO 1.74E-02 Sn-113 2 55.1 3 2.11 -2.73E-01 9.21E-02 2.2 4E+OO 3 91.70 64.97 1.75E-03 9.21E-02 Cs-134 475.36 1. 48 6.57E-01 6.82E-02 3.21E+OO 563.25 8.34 2.78E-02 8.39E-Ol 569.33 1 5.37 3.90E-02 3.50E-01 Page4of7 Tolerance Nuclide Colnc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss 10/10/2016 1:46:34PM Page 5 of7 Analysis Report for 10-0ct-16-10014 L3-10219A-FQGS-006SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCl!grams) (pCi/grams)

Corr Cs-134 604.72 97. 62 1.64E-02 6.82E-02 7.00E-02 miss 795.86 85.46 1.22E-03 6.82E-02 miss 80 1.95 8.69 3.67E-01 1.02E+OO miss 1038.61 0.99 -3.79E-01 5.58E+OO miss 1167.97 1. 79 -1.1 6E+OO 3.33E+OO mis s 1365.19 3.0 2 1.71E-01 2.2 0E+OO miss + Cs-137 661.66 85.1 0 -3.2 4E-03 8.49E-0 2 8.49E-0 2 miss + Eu-152 121.78 28.67 7.76E-02 1.80E-01 1.80E-01 miss 244.70 7.61 -2.81E-01 5.49E-01 miss 295.94 0.45 1.17E+Ol l.83E+Ol miss 344.2 8 2 6.60 -4.50E-03 1.97E-01 miss 367.79 0.86 -8.49E-02 4.57E+OO miss 411.12 2.2 4 7.09E-02 2.13E+OO miss 443.96 2.8 3 1. 71E-01 1.94E+OO miss 488.68 0.42 2.34E+OO 1.28E+Ol miss 563.99 0.49 6.04E-01 l.42E+Ol miss 586.2 6 0. 4 6 -l.72E+OO 1.45E+Ol miss 678. 62 0.47 -9.90E-01 1.2 8E+Ol miss 688.6: 0.86 1.65E+00 7.92E+OO miss 71 9. 35 0.2 8 3.31E+OO 1.94E+Ol miss 778.90 12.96 9.49E-02 4.41E-01 miss 810.45 0.3 2 -3.44E+OO 1.83E+Ol miss 867.37 4.26 O.OOE+OO 4.2 0E-01 miss 919.33 0.43 3.22E+OO l.49E+Ol miss 964. 0 8 14.65 6.47E-02 5.2 3E-01 miss 10 85.87 10.24 6.98E-0 2 6.98E-0 1 mi ss 1 0 89.74 1. 73 O.OOE+OO 1.21E+OO miss 11 12. 07 13. 69 -1.55E-01 4.20E-01 miss 1212.95 1. 43 O.OOE+OO 1.57E+OO miss 1249.94 0.19 O.OOE+OO 1.21E+Ol miss 1299.14 1. 63 -l.45E+OO 3.92E+OO mis s 1408.0 1 21.07 8.50E-02 4.69E-01 mi ss 1457.64 0.50 -1.77E+Ol 1.74E+Ol miss 1528.10 0.2 8 O.OOE+OO 9.37E+OO miss + Eu-1 54 123.07 40.40 -4.2 1E-03 7.90E-02 9.97E-02 mis s 247.93 6.89 -5.70E-01 3.00E-01 mis s 591.7 6 4.95 -4 .13E-02 7.60E-01 miss 692.4 2 1. 78 -6.93E-01 3.45E+OO miss 723. 30 20.06 O.OOE+OO 7.90E-02 miss 756.80 4.52 -2.15E-01 1.44E+OO miss 873.18 1 2.08 9.17E-0 3 5. llE-01 miss 996.29 10.48 -l.27E-01

5. llE-01 miss 1004.76 18.01 -1.63E-01 2.99E-01 miss 1 274.43 34.80 3.51E-03 2.28E-01 miss 1 596.48 1. 80 O.OOE+OO 1.52E+OO miss + Eu-155 45.3 0 1. 31 4.2 9E-01 2.61E-01 l.61E+Ol miss 60.0 1 1. 22 1.59E+OO 1. 73E+Ol miss 86.55 30.70 5.25E-0 2 2.61E-01 miss 105.31 2 1.10 9.34E-0 2 2.61E-01 miss + Tl-208 583.19

85.00 1.2 5E-01 7.44E-02 7.44E-02 miss + Bi-211 351.07

13. 02 1.02E+OO 4.02E-01 4.02E-01 miss 10/10/2016 1:46:34PM Page 6 of7 Analysis Report for 10-0ct-16-10014 L3-10219A-FQGS-006SS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Corr + Pb-2 11 404.85 3.78 6.54E-01 1.69E+OO 1.73E+OO miss 427.0 9 1. 76 -5.08E-01 2.49E+OO miss 832.01 3.52 2.89E-01 1.69E+OO miss + Bi-2 12 39.86 1. 06 6.09E+OO 1.15E+OO 1.59E+Ol miss 727.33 6.67 3.0SE-01 l.15E+OO miss 785.37 1.10 6.78E-01 6.74E+OO miss 1620.50 1. 47 2.61E-01 5. llE+OO mis s + Pb-212 115 .1 8 0.60 3.02E+OO 2.08E-01 8.67E+OO miss 2 38.63

43.60 1.85E-01 2.08E-01 miss 300.09 3.30 5.31E-01 1.68E+OO miss + Pb212-X R 74.82 10.2 8 3.2 0E-01 7.85E-01 1.35E+OO miss 77 .11 17.10 3.04E-01 7.85E-Ol miss 87.35 3.97 8.14E-01 1. 96E+OO miss 89.78 1. 46 2.12E+OO 4.58E+OO miss + Bi-2 1 4 609.3 2

45.49 5.0 9E-01 1.05E-01 l.05E-01 miss 768.36 4.89 6.29E-0 1 1. 75E+OO miss 806.1 8 1. 26 -4.98E-0 1 4.62E+OO miss 934.0 6 3 .11 5.35E-0 1 2.41E+OO miss 112 0.2 9 14. 9 2 3.68E-01 7.89E-01 miss 1155.2 1 1. 63 1.66E+00 5.88E+OO miss 1238.1 2 5.83 -6.05E-01 1.72E+OO mi ss 1280.98 1. 43 2.39E+OO 7.17E+OO miss 1377.67 3.99 3.23E-02 2.lOE+OO miss 1385. 31 0.79 l.1 4E+OO 8.40E+OO miss 1401. 52 1. 33 6.87E-01 5.0SE+OO miss 1407.99 2.39 7.48E-01 4.12E+OO miss 1509.21 2.13 1.36E+OO 4.89E+OO miss 1661.27 1. 05 O.OOE+OO 2.69E+OO miss 1729.59 2.88 4.20E-01 3.46E+OO miss 1 764.49 15.30 4.28E-01 1.0lE+OO miss 1 847.43 2.03 6.93E-0 2 4.08E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 3.04E-01 1.47E-01 8.54E-01 miss 295.22 18.42 5.13E-01 5.lOE-01 miss 351.93

35.60 3.73E-0 1 1.47E-01 miss 785.96 1. 06 5.59E-01 7. OlE+OO miss + Pb214-XR 74.82 5.80 5.67E-01 1.38E+OO 2.40E+OO miss 77 .11 9.70 5.36E-01 l.38E+OO miss 87.35 2.24 1.44E+OO 3.47E+OO miss 89.78 0.82 3.78E+OO 8.15E+OO miss + Ra-226 186.2 1 3.64 9.53E-01 1.48E+OO 1.48E+OO miss + Ac-228 129.0 7 2.4 2 -1.73E-01 4.99E-01 1.65E+OO miss 209.25 3.89 -1.60E-01

1. 09E+OO miss 270.24 3.46 1. 23E-01 1. 36E+OO miss 328.00 2.95 1.43E-01 1. 82E+OO miss 338.32 11. 2 7 1.20E-0 1 5.76E-0 1 miss 409.46 1.92 8.23E-02 2.,0E+OO miss 463.00 4.40 2.SlE-01 1.47E+OO miss 794.95 4.25 3.09E-01 1. 58E+OO miss 9 1 1. 20 2 5.80 2.67E-01 4.99E-01 miss 964. 77 4.99 6.49E-01 2.0lE+OO miss 10/10/2016 1:46:34PM Page 7 of7 An a ly s is Rep o rt for 10-0ct-16-10014 L3-10219A-FQGS-006SS Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Colnc Name (keV) (pCi!grams) (pCl!grams) (pCilgrams)

Corr Ac-228 968.97 15.80 3.69E-01 4.99E-01 7.86E-01 mis s 1588.2 0 3.2 2 3.12E-01 2.30E+OO mis s + Pa-23 1 27.36 10.30 O.OOE+OO 2.94E-01 2.94E-01 mis s 283.69 1. 70 1.62E+OO 3.14E+OO mi ss 300.07 2.47 7.09E-01 2.24E+OO miss 30 2.65 2.2 0 -6.06E-0 2 1.57E+OO mis s 330.06 1. 40 8.96E-01 3.1 8E+OO miss + Th-234 92.38 2 .13 1.67E+00 4.36E+OO 4.41E+OO miss 92.80 2.10 1.05E+OO 4.36E+OO miss 112. 81 0.21 1.90E+OO 2.95E+Ol miss + U-235 143.76 10.96 -1.44E-0 2 8.40 E-02 4.lGE-01 miss 163.33 5.08 1.79E-01 9.2 7E-0 1 miss 185.71 57.20 2.78E-02 8.40E-02 mis s 202 .11 1. 08 -4.05E-01 3.48E+OO mis s 205.31 5.01 1.26E-01 8.76E-01 mis s + Am-241 59.54 35.90 1.54E-01 5.64E-O l 5.64E-Ol miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) ..... C ::s 60 55 50 45 40 35 8 30 25 co 2 I 'i= 1000 2000 3000 0000016070.CNF 4000 channel 5000 Live Time :300.000 sec Real Ti11e :300.180 sec start: 1: -0.Z(kev) stop : 8192:2047

.4(kev) Acq. Start :Mon Oct 10 13:40:56 2016 6000 7000 8000 10/10/2016 11:39:23AM

~~~pex-Gamma Analysis Report for 10-0ct-16-10012 L3-10219A-FQGS-O 14SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 10-0ct-16-10012

L3-10219A-FQGS-014SS

1 L 130G Soil Sample 1.295E+03 grams : Default : 10/3/2016 1 :20:00PM : 10/10/2016 11:15:57AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.16 % : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16068 PEAK WITH NID REPORT Peak Analysis Performed on : 10/10/2016 11:21:05AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of7 10/10/2016 11:39:23AM Page 2 of7 Analysis Report for 10-0ct-16-10012 L3-10219A-FQGS-014SS Peak Energy ROI No. (keV) start 1 2 38.49 947 -2 351.99 1401 -3 609.32 2431 -4 1 4 60.39 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 961 1415 2443 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.44 4.81E+Ol 19.68 3.38E+Ol 1408.13 5.33E+Ol 15.48 5.44E+OO 2437.03 3.05E+Ol 11. 69 2.90E+OO 5842.54 7.18E+Ol 17.26 2.40E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.98 1460.82

10.66 6.81E+OO l.74E+OO Bi-211 0.95 351.07

13.02 l.56E+OO 5.1 7E-01 Pb-21 2 0.99 115 .18 0.60 2 38.63

43.60 3.2 7E-01 l.44E-01 300.09 3.30 Bi-214 1. 00 609.32

45.49 4.04E-01 l.62E-Ol 768.36 4.89 806.18 1. 2 6 934.06 3 .11 11 2 0.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.2 1 2 .13 1661. 27 1. 05 1729.59 2.88 1 764.49 1 5.30 1 847.43 2.03 2118.5 1 1.16 Tentative Nuclide Pb-212 Pb-214 Bi-211 Bi-214 K-40 Coinc Corr miss miss free 0.948 Analysis Report for 10-0ct-16-10012 L3-10219A-FQGS-014SS Nuclide Id Energy Name Confidence (keV) Pb-21 4 0.51 241.99 295.22 351.93 785. 96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed. free = No coincidence correction required.

Yield(%) 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/10/2016 11:39:23AM Page 3 of7 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 5.69E-01 1.89E-01 free INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? Bi-211 Pb-212 Bi-214 ? Pb-2 14 Nuclide Id Confidence 0.989 0.950 0.999 1.000 0. 513 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 6.81E+OO 1.56E+OO 3.27E-01 4.04E-01 5.69E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 1.74E+OO 5.17E-01 1.44E-01 1.62E-01 1.89E-0 1 10/10/2016 11 :39:23AM Page 4 of7 Analysis Report for 10-0ct-16-10012

+ + + + + + + + + L3-1021 SA-FQGS-O 14SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 11:21:05AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCl!grams) (pCi!grams)

Corr K-40 1460.82

10.66 6. 81E+OO 7.66E-01 7.66E-01 miss Cr-51 320.08 9.91 l.39E-01 6.45E-01 6.45E-01 free Mn-54 834.85 99.98 2.04E-0 2 8.40E-02 8.40E-02 miss Co-58 810.76 99.45 -l.82E-02 5.35E-02 5.35E-02 1.000 1 674.73 0.52 O.OOE+OO 6.14E+OO 1.024 C o-60 1173.2 3 99.85 8.52E-03 9.2 6E-02 l.l OE-01 0.947 1332.49 99.98 5.70E-03 9.2 6E-02 0.947 Nb-94 702.65 99.81 -l.09E-0 2 7.0lE-02 7.0lE-02 0.944 8 71. 09 99.89 4.51E-0 2 l.06E-01 0.944 Ag-108m 79.13 6.60 l.87E-0 1 6.54E-02 2.04E+OO miss 433.94 90.50 3.29E-02 7.74E-0 2 0.88 7 614.28 89.80 l.20E-02 6.54E-02 0.886 722.94 90.80 3. llE-02 9.33E-02 0.887 Sn-113 255.13 2 .11 -6.34E-01 7.91E-02 2.55E+OO free 391. 70 64.97 6.59E-04 7.91E-02 free Cs-134 475.36 1. 48 -l.2 8E+O O 7.37E-02 2.97E+OO miss 563.25 8.34 -3.1 3E-01 9.33E-01 0.896 569.33 15.37 l.06E-01 4.71E-01 0.888 604. 72 97.62 2.76E-03 7.37E-02 0.931 10/10/2016 11: 39: 23AM Page 5 of7 Analysis Report for 1 0-0ct-16-10012 L 3-10219A-FQGS-014SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCilgrams) (pCl!grams) (pCilgrams)

Corr Cs-134 795.86 85.46 -1.40E-03 7.37E-02 9.07E-02 0.933 8 01.95 8.69 1.87E-01 9.31E-01 0.898 1038.61 0.99 -7.18E-01 6.34E+00 0.943 1167.97 1. 7 9 4.49E-01 4.83E+00 1. 08 1 1 365.1 9 3.0 2 3.65E-01 2.64E+00 1.1 2 8 + Cs-137 661.66 85.10 3.05E-02 l.04E-01 1.04E-01 miss + Eu-1 52 1 2 1.78 28.67 -5.63E-02 1.28E-01 1.74E-01 0.936 2 44.70 7.61 -4.19E-01 5.lOE-01 0.935 2 95.94 0.45 1.08E+Ol 1.87E+Ol miss 344.28 26.60 -1.47E-03 2.08E-01 0.957 367.79 0.86 -2.58E-01 4.78E+OO 0.884 4 11.12 2.24 9.20E-01 3.32E+00 0.908 443.96 2.83 6.45E-01 2.22E+OO 0.934 488.68 0.4 2 O.OOE+OO 3.09E+OO m i ss 563.99 0. 49 6.15E-01 1.63E+Ol 0.934 586.26 0.46 -l.OOE-01 1.64E+Ol 0.94 2 678.62 0.47 O.OOE+OO 3.88E+OO 0.887 688.67 0.86 O.OOE+OO l.95E+OO 0.980 71 9.35 0.28 2.2 4E+OO 2.08E+Ol miss 778.90 12. 96 -1.07E-01 3.95E-01 0.945 810.45 0.32 O.OOE+OO 5.43E+OO 1.050 867.37 4.26 3.58E-01 1.66E+OO 0.9 2 8 919.33 0.43 -5.71E+OO 1.63E+Ol 0.981 964. 0 8 14.65 -3.39E-02 4.72E-01 1. 022 10 85.87 10.24 -2.26E-02 8.51E-01 1.018 10 89.74 1. 73 4.78E-0 1 5.40E+00 0.952 11 12.07 13.69 -3.52E-02 5.72E-01 0.99 2 1212.95 1. 43 -l.21E+OO 7.2 0E+OO 0.929 1249.94 0.19 3.43E+OO 4.05E+Ol 1. 097 1299.14 1. 63 -1.64E+OO 4.45E+OO 0.944 1 408.0 1 21. 07 O.OOE+OO 1.28E-01 0.983 1 457.64 0.50 -1. 2 5E+Ol 3.25E+Ol 1. 076 1528.10 0.28 O.OOE+OO 9.99E+OO 1. 007 + Eu-154 123.07 40.40 -1.58E-0 2 l.20E-01 1.41E-01 0.934 247.93 6.89 -1.64E-01 8.30E-01 0.9 2 8 591. 7 6 4.95 -2.90E-01 l.12E+OO 0.9 1 5 692.4 2 1. 78 1. 81E+OO 5.16E+OO 0.936 723.30 20.06 l.34E-01 4. OlE-01 0.935 756.80 4.52 1.30E-01 1.15E+OO 0.915 873.18 12.08 -6.00E-01 4.65E-Ol 0.932 996.29 10.48 1. 72E-01 9.19E-01 0.971 1004.76 18.01 O.OOE+OO 1.20E-01 0.978 1274.43 34.80 3.83E-02 ~.49E-01 0.981 1 596.48 1. 80 O.OOE+OO 1.39E+OO 1.175 + Eu-155 45.30 1. 31 7.0lE+OO 3.33E-01 3.30E+Ol 0.999 60.01 1. 22 -1.2 3E+O l 3.35E+Ol 1. 000 86. 55 30.70 1.35E-02 3.91E-01 free 105.31 2 1.10 -3.05E-02 3.33E-01 1. 000 + Tl-208 583.19 85.00 8.8 7 E-02 1. 53E-01 1.53E-01 0.932 + Bi-211 351.07

13.02 1.56E+OO 3.26E-01 3.26E-01 miss + Pb-2 11 404.85 3.78 1.33E-01 1.2 0E+OO 1.20E+OO miss 10/10/2016 11:39:23AM Page 6 of7 Analysis Report for 10-0ct-16-10012 L3-10219A-FQGS-O 14SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCUgrams) (pCi!grams)

Corr Ph-2 11 427.09 1. 76 -2.35E-01 1.20E+OO 2.97E+OO miss 832.01 3.5 2 1.30E-01 2.lOE+OO miss + Bi-21 2 39.86 1. 06 3.81E+OO 1.1 5E+OO 4.51E+Ol 0.998 727. 33 6.6, 3.84E-01 l.15E+OO 0.982 785.37 1.10 -1.06E+OO 4.68E+OO 0.944 1620.50 1. 47 O.OOE+OO 2.00E+OO 1.006 + Pb-212 115 .18 0.60 4.05E-01 1.75E-01 7.62E+OO miss 2 38.63

43.60 3. 27E-01 1.75E-01 free 300.09 3.30 3.90E-01 1. 4 7E+OO free + Pb212-XR 74.82 10.28 3.57E-01 1.33E+OO 2.17E+OO miss 77 .11 17.10 6. llE-01 1.33E+OO miss 87.35 3.97 1.68E+OO 3.17E+OO miss 89.78 1. 46 -5.50E-02 5.23E+OO miss + Bi-2 1 4 609.32

45.49 4.04E-01 1.16E-01 1.16E-Ol 0.948 768.36 4.89 7.54E-01 2.12E+OO 0.94 2 806.18 1. 26 -1.06E+OO 4.24E+OO 0.923 934.06 3.11 7.62E-01 2.73E+OO 0.944 1120.2 9 14.92 3.77E-01 8.95E-01 0.944 1155.2 1 1. 63 1. 25E+OO 5.99E+OO 0.943 1238.1 2 5.83 8.38E-01 2.45E+OO 0.944 1 280.98 1. 43 1.60E+OO 8.14E+OO 0.944 1377.67 3.99 3.36E-02 2.53E+OO 1. 030 1385. 31 0.79 1. 30E+OO 9.53E+OO 0.94 5 1401.52 1. 33 1.63E+OO 8.39E+OO 0.94 5 1407.99 2.39 O.OOE+OO 1.18E+OO 0.945 1509.21 2.13 O.OOE+OO l.39E+OO 0.950 166 1.27 1. 05 2.13E+OO 9.90E+OO 1. 00 1 1729.59 2.88 7.15E-01 3.32E+OO 1.119 1764.49 15.30 7.64E-02 5.62E-01 1. 001 1847.43 2.03 l.12E+OO 5.19E+OO 1.063 > 2118. 51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 14 2 4 1.99 7.25 5.54E-01 1.1 9E-01 9.93E-01 1. 000 295.22 18.42 3.44E-01 4.79E-01 1. 000 351.93

35.60 5.69E-01 l.19E-01 free 785.96 1. 06 7.28E-01 5.80E+OO 1.000 + Pb214-XR 74.82 5.80 6.32E-01 2.34E+OO 3.85E+OO miss 77 .11 9.70 1.08E+OO 2.34E+OO miss 87.35 2.2 4 2.98E+OO 5.62E+OO miss 89.78 0.82 -9.79E-02 9.32E+OO miss + Ra-226 186.2 1 3.64 7.0lE-01 1.67E+OO 1.67E+OO free + Ac-228 129.0 7 2.42 1. 51E-01 5.58E-01 2.81E+OO 0.944 209.25 3.89 8.71E-01 1.73E+OO 0.978 270.24 3.46 8.02E-01 2.18E+OO 0.955 328.00 2.95 4.21E-0 1 1.82E+OO 0.955 338. 3:2 11. 27 3.98E-01 7.26E-01 0.992 409.46 1. 92 -6.73E-02 3.53E+OO 0.937 463.00 4.40 1.07E-01 1.35E+OO 0.933 794.95 4.25 5.27E-01 2.18E+OO 0.942 911.2 0 2 5.80 3.28E-0 1 5.58E-01 0.990 964.77 4.99 -2.59E-01 l.44E+OO 0.981 968.97 15.80 1.69E-01 6.88E-01 0.990 10/10/2016 11:39:23AM Page 7 of7 Analysis Report for 10-0ct-16-10012 L3-10219A-FQGS-014SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCl/grams) (pCi!grams)

Corr Ac-228 1588.20 3.22 4.80E-01 5.58E-01 3.lOE+OO 1. 002 + Pa-231 27.36 10.30 7.17E-01 1. 96E+OO 4.19E+OO 0.998 283.69 1. 70 -l.44E+OO 2.75E+OO 1. 000 30 0.0 7 2.47 5.2 1E-0 1 l.96E+OO 1.000 302.65 2.2 0 1.37E-01 2.49E+OO 1. 000 330.06 1. 40 4.43E-01 3.13E+OO 1. 000 + Th-234 92.38 2.13 2.05E+00 6.lOE+OO 6.19E+OO free 92.80 2.10 1.72E+OO 6.lOE+OO free 112. 81 0.21 5.06E+OO 3.77E+Ol free + U-235 143.7 6 1 0.96 -1. l 7E-01 l.04E-01 4.49E-01 free 163.33 5.08 3.54E-02 l.05E+OO f ree 1 85.71 57.2 0 3.15E-02 l.04E-01 f ree 202 .11 1. 08 -6.79E-01 4.24E+OO miss 205.31 5.01 -3.73E-Ol 9.21E-01 free + Am-241 59.54 35.90 -l.33E-01 1.38E+OO l.38E+OO free + = Nuclide identified during the nuclide identification " = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) ' C ::::J 60 55 50 40 35 8 30 25 20 15 1000 2000 3000 0000016068.CNF 4000 channel 5000 Live Time 300.000 sec Real Time 300.490 sec start: 1 -0. l(kev) stop : 8192 2047. O(kev) Acq. start Mon Oct 10 11:15:57 2016 6000 7000 8000

Printed: 6/13/2018 9:07 AMPage 1 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a mpleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnits17-03011-01LCSKNOWN03/03/17 00:003/3/20173/14/201717-03 011Nickel-63ASTM 3500-Ni Modified1.51E+034.52E+01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.52E+039.33E+009.01E+012.11E+00pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.58E+001.27E+001.27E+002.11E+00UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.19E+001.39E+001.39E+002.29E+00UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.71E+001.37E+001.37E+002.28E+00UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified3.46E+001.39E+001.40E+002.25E+00pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.88E-011.36E+001.36E+002.31E+00UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified-1.69E+001.65E+001.65E+002.90E+00UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified6.89E-011.40E+001.40E+002.37E+00UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified8.22E-011.30E+001.30E+002.20E+00UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.06E+001.27E+001.27E+002.13E+00UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified3.84E+001.40E+001.42E+002.25E+00pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.34E+001.48E+001.49E+002.44E+00UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.97E+001.36E+001.37E+002.26E+00UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.09E+001.42E+001.42E+002.39E+00UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified9.12E-011.44E+001.44E+002.44E+00UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.02E+011.52E+001.64E+002.24E+00pCi/g17-03011-01LCSKNOWN03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.43E+013.04E-01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.16E+011.65E+002.15E+018.24E-01pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified-2.14E-024.23E-014.23E-019.04E-01UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified7.78E-013.45E-014.39E-016.48E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.42E-013.48E-013.96E-016.83E-01UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.59E-013.59E-013.81E-017.29E-01UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.97E-013.66E-013.91E-017.40E-01UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.85E-014.17E-014.64E-018.27E-01UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.39E-023.97E-013.98E-018.41E-01UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified9.84E-013.37E-014.80E-016.09E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified4.59E-013.45E-013.80E-016.86E-01UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.36E-013.86E-014.45E-017.54E-01UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified8.09E-014.19E-015.05E-018.12E-01UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified7.29E-013.98E-014.72E-017.75E-01UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.09E-013.90E-014.04E-018.00E-01UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified1.03E-013.61E-013.62E-017.59E-01UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.03E-013.78E-014.17E-017.53E-01UpCi/gZion, IL 60099Work Order Details:67149817-03011SOENV IRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh BlvdCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/13/2018 9:07 AMPage 2 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a mpleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-01LCSKNOWN03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified6.21E+012.48E+00pCi/g17-03011-01LCSKNOWN03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified3.94E+011.58E+00pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified7.58E+015.03E+006.36E+006.59E-01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.44E+014.02E+004.62E+006.97E-01pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.74E-024.81E-024.82E-028.85E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified1.72E-022.56E-022.57E-024.39E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.29E-021.46E-021.46E-022.73E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-1.28E-041.27E-021.27E-021.91E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.40E-031.48E-021.48E-022.34E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.37E-011.68E-011.69E-013.28E-01UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Lead-212LANL ER-130 Modified6.28E-031.70E-021.70E-022.64E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Lead-214LANL ER-130 Modified-3.01E-032.42E-022.42E-023.65E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified-5.23E-034.16E-024.16E-026.34E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.11E-011.33E-011.34E-012.02E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.84E-011.17E-011.19E-011.04E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-2.54E-033.32E-023.32E-024.18E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified2.64E-041.18E-021.18E-024.72E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified5.75E-024.30E-024.31E-027.05E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.01E+011.11E+001.23E+004.65E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified4.00E-015.25E-025.64E-028.50E-02pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.90E-011.31E-011.33E-019.32E-02pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.46E-016.92E-027.04E-025.39E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.23E-011.04E-011.06E-012.03E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.66E-011.11E-011.13E-018.49E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified4.50E-043.33E-023.33E-023.46E-02UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-5.96E-031.09E-021.09E-024.15E-02UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.04E-023.06E-023.08E-024.76E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.02E+011.13E+001.24E+005.53E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.75E-015.11E-025.46E-028.70E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified4.00E-011.33E-011.35E-011.11E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified1.86E-016.47E-026.54E-026.95E-02pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/13/2018 9:07 AMPage 3 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a mpleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.95E-016.68E-026.98E-022.26E-01pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.88E-016.28E-026.59E-028.04E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.89E-022.04E-022.04E-022.86E-02UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-3.06E-031.04E-021.04E-022.78E-02UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.11E-016.15E-026.50E-023.88E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified6.85E+008.02E-018.76E-012.60E-01pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.45E-015.27E-025.56E-024.16E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.73E-016.08E-026.37E-027.27E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.93E-017.55E-027.82E-026.80E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.14E-011.00E-011.02E-011.05E-01pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.82E-017.07E-027.34E-027.96E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified2.05E-031.95E-021.95E-022.33E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified4.00E-036.34E-036.34E-032.49E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified2.25E-022.00E-022.01E-023.30E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified8.06E+001.03E+001.11E+004.94E-01pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.61E-011.24E-011.26E-016.77E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.73E-011.30E-011.31E-016.84E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.87E-017.16E-027.31E-025.18E-02pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.85E-011.06E-011.07E-012.08E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.30E-019.29E-029.55E-021.27E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.61E-039.25E-039.25E-035.27E-02UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified8.33E-031.55E-021.55E-024.39E-02UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.93E-011.06E-011.12E-016.05E-02pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified4.65E+007.78E-018.14E-015.30E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.59E-025.32E-025.33E-021.04E-01UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.45E-018.88E-029.05E-021.15E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.39E-018.59E-028.67E-021.47E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/13/2018 9:07 AMPage 4 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a mpleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.93E-011.05E-011.06E-012.39E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.41E-016.34E-026.57E-021.35E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-3.32E-024.28E-024.28E-025.98E-02UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified6.49E-032.04E-022.04E-024.57E-02UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.03E-017.19E-027.49E-028.51E-02pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified8.03E+001.20E+001.27E+006.92E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.68E-015.53E-025.84E-021.09E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified2.92E-016.40E-026.57E-021.03E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified4.27E-011.02E-011.04E-011.72E-01pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.67E-011.03E-011.03E-017.51E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.06E-016.14E-026.33E-026.49E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.29E-021.47E-021.47E-021.62E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified1.85E-035.88E-035.88E-032.29E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified5.77E-031.18E-021.18E-021.84E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified4.97E+006.50E-016.98E-013.09E-01pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Lead-212LANL ER-130 Modified2.92E-019.35E-029.47E-025.97E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.26E-011.09E-011.11E-015.08E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.49E-016.26E-026.39E-026.96E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.56E-018.81E-029.11E-021.90E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.52E-011.14E-011.16E-017.67E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-1.95E-032.38E-022.38E-022.96E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-2.43E-031.04E-021.04E-023.39E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified1.68E-021.97E-021.97E-023.18E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified5.89E+007.05E-017.67E-014.46E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.13E-015.35E-025.96E-028.50E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Lead-214LANL ER-130 Modified4.53E-011.30E-011.32E-016.76E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.20E-016.85E-027.04E-023.88E-02pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/13/2018 9:07 AMPage 5 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a mpleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.10E-011.38E-011.39E-012.87E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified2.90E-018.05E-028.19E-021.08E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-1.08E-024.50E-024.50E-025.74E-02UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified7.65E-031.58E-021.58E-024.69E-02UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified3.28E-016.71E-026.92E-028.42E-02pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified9.77E+001.40E+001.49E+006.37E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.17E-015.43E-025.66E-029.23E-02pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.38E-017.09E-027.30E-021.13E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.08E-011.13E-011.14E-011.65E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.28E-018.53E-028.80E-021.50E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.40E-017.01E-027.22E-029.44E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.84E-022.40E-022.40E-023.33E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-2.32E-022.89E-022.89E-023.14E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified2.81E-022.43E-022.43E-023.95E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified7.18E+008.97E-019.70E-015.24E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.13E-017.92E-028.35E-026.71E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.46E-015.95E-026.21E-027.38E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.96E-018.55E-028.78E-021.12E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.89E-011.08E-011.09E-011.71E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.18E-018.65E-028.91E-027.83E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified6.19E-032.06E-022.06E-022.63E-02UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified6.73E-031.17E-021.17E-022.91E-02UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.84E-022.08E-022.11E-023.89E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified7.14E+009.28E-019.97E-014.26E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.24E-011.13E-011.15E-019.05E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.61E-011.29E-011.30E-015.38E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.52E-017.63E-027.74E-021.17E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/13/2018 9:07 AMPage 6 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a mpleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified2.73E-019.62E-029.72E-021.03E-01pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.99E-016.02E-026.21E-026.14E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified2.51E-021.55E-021.56E-022.24E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified-5.07E-039.42E-039.43E-032.76E-02UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified3.38E-014.02E-024.38E-023.33E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.77E+008.72E-019.39E-013.88E-01pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Lead-212LANL ER-130 Modified3.17E-011.10E-011.11E-016.70E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Lead-214LANL ER-130 Modified2.31E-018.83E-028.91E-025.75E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified3.12E-017.53E-027.70E-025.09E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified3.28E-015.75E-025.99E-021.19E-01pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.77E-015.55E-025.72E-027.49E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified2.22E-031.65E-021.65E-022.20E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified2.87E-036.84E-036.84E-031.89E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified2.03E-021.30E-021.30E-022.04E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.22E+006.92E-017.62E-012.36E-01pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Lead-212LANL ER-130 Modified2.87E-014.16E-024.42E-024.20E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Lead-214LANL ER-130 Modified2.66E-014.22E-024.44E-024.27E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified2.87E-015.58E-025.77E-024.54E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified3.84E-011.09E-011.11E-012.05E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.85E-019.70E-029.81E-021.05E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified8.55E-033.20E-023.20E-025.09E-02UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified1.76E-031.48E-021.48E-024.53E-02UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified3.37E-016.23E-026.46E-027.54E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.05E+008.31E-018.87E-015.71E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Lead-212LANL ER-130 Modified4.33E-015.83E-026.23E-028.32E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Lead-214LANL ER-130 Modified3.29E-011.49E-011.50E-011.23E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified2.56E-018.59E-028.69E-021.05E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

ML19178A100

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