ML19178A102

Restoration Project - Final Status Survey Release Record, Adjacent of South Restricted Area - Lakeshore Survey Unit 10220C - Final Report - Phase 1, Revision 1

ML19178A102
Person / Time
Site:	Zion  File:ZionSolutions icon.png
Issue date:	06/20/2019
From:	Yetter R ZionSolutions
To:	Office of Nuclear Material Safety and Safeguards
Shared Package
MML19178A106	List: ML19178A098 ML19178A100 ML19178A101 ML19178A102 ML19178A103 ML19178A104 ML19178A105 ML19178A107 ML19178A108 ZS-2019-0043, Transmittal of Revised Final Status Survey Report - Phase 1
References
ZS-2019-0043
Download: ML19178A102 (237)

Text

=ZION SOLUTIONS LLC-An EnergySo/utions Company

=1+++ ()=1.()+..()=3.622 / ()=1.()+..()=0.898 /

()=1..()+..+..()=3.494 /

5/5/2016 ~:46:03AM

• ~pex-Gamma Analysis Report for 05-May-16-10004 L3-10220C-FRGS-001 SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 05-May-16-10004

L3-10220C-FRGS-001SS (DRIED)

1L 130G Soil Sample 1.437E+03 grams : Default : 5/2/2016 9:45:00AM

5/5/2016 9:15:18AM

130G 1 L Sand Sam pie : JWelch : P11314X2 : 130G Sand : 1800.0 seconds : 1801.4 seconds : 0.07% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

11/26/2012

14849 PEAK WITH NID REPORT Peak Analysis Performed on : 5/5/2016 9:45:26AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BN L. N LB : 1.00 0FWHM Page l of8 5/5/2016 ~:46:03AM Analysis Report for 05-May-16-10004 M m M m L3-10220C-FRGS-001 SS (DRIED) Peak Energy RO! No. (keV) start 1 7 4.78 295 -2 77.06 295 -3 238.64 94 7 -4 241.85 947 -5 270.10 1076 -6 295.08 1174 -7 3 38.44 1346 -8 3 51.84 1400 -9 583.04 2325-10 609.09 2428 -11 661.69 26 37 -12 727.17 2902 -13 768 .13 3066 -14 911.20 3636 -15 969 .17 3868 -16 1120.31 4473 -17 1460.76 58 3 1 -18 150 9.50 60 3 2 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma RO! Peak end Centroid 315 300.37 315 3 0 9.48 975 954.87 9 75 967. 71 1085 1080.58 1189 1180.36 1359 13 5 3.62 1414 14 0 7.1: 2338 2331.18 2443 2435.29 2651 2645.56 2915 2907.38 3076 3071.14 3651 3643.30 3883 3875.18 4486 4479.80 5855 5842.38 6043 6037.51 NetPeak Net A r e a Area Uncertainty 8.08 E+O l 25.79 l.25E+02 2 8.19 2.95E+02 36.42 7.76E+O l 21.01 2.69E+Ol 21.66 9.14E+Ol 33. 64 6.25E+O l 27.90 1.81E+02 34.43 9.03E+O l 24.06 1. 48E+02 29.00 5.88E+D1 20.46 3.27E+Ol 16.53 1.34E+Ol 11. 99 7.18E+Ol 20. 73 5.82E+Ol 19.74 2.lOE+Ol 16.63 5.55E+02 48.19 8.17E+OO 6.95 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LJB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield(%) Activity Page 2 of8 r,...,.4;

...........

_,., ..........

~*** Tentative Counts Nuclide 2.72E+02 Pb214-XR Pb212-X R 2.62E+02 Pb214-XR Pb212-XR 1.66E+02 Pb-212 1.36E+02 Pb-2 1 4 8.0lE+Ol Ac-228 l.27E+02 Pb-214 Eu-152 l.09E+02 Ac-228 9.25E+Ol Pb-214 Bi-211 4.53E+Ol Tl-208 4. 77E+O l Bi-21 4 4.03E+Ol Cs-137 3.27E+D1 Bi-212 2.32 E+Ol Bi-214 3.05E+Ol Ac-228 3.36E+Ol Ac-228 4.80E+Ol Bi-214 1.81E+Ol K-40 3.66E+OO Bi-21 4 Activity Coinc Name Confidence (keV) (pCl/grams)

Uncertainty Corr K-40 1. 00 1460.82

• 10.66 7.18E+OO 8.BlE-01 miss Cs-137 1. 00 661.66

• 85.10 5.59E-02 2.06E-02 miss Tl-208 0.99 583.19

• 85.00 7.BBE-02 2.30E-02 miss Bi-212 0.99 39.86 1. 06 727. 33

• 6.67 4.22E-01 2.19E-01 miss 785.37 1.10 5/5/2016 !:f:46:03AM Page 3 of8 Analysis Report for 05-May-16-10004 L3-10220C-FRGS-001 SS (DRIED} Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr Bi-212 0.99 1620.50 1. 47 Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 2. 72E-01 5.54E-02 miss 300.09 3.30 Pb212-XR 1. 00 74.82

• 10.28 5.90E-01 2.24E-01 miss 77 .11

• 17.10 5.06E-01 1.54E-01 miss 87.35 3.97 89.78 1. 46 Bi-214 0.99 609.32

• 45.49 2.49E-01 5.72E-02 miss 768.36

• 4.89 2.45E-01 2.20E-01 miss 806.18 1. 26 934.06 3.11 1120.29

• 14.92 l.62E-01 1.29E-Ol miss 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 ,I,-2.13 5.42E-01 4.63E-01 miss 1661.27 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118. 51 1.16 Pb-214 0.99 241.99

• 7.25 4.35E-01 1. 37E-01 miss 295.22

• 18.42 2.30E-01 9.23E-02 miss 351.93

• 35.60 2.65E-01 6.58E-02 miss 785. 96 1. 06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24

• 3.46 3.40E-01 2.79E-01 miss 328.00 2.95 338.32

• 11. 27 2.82E-01 1.34E-01 mis~ 409.46 1. 9'.2 463.00 4.40 794.95 4.25 911. 20

• 25.80 2.79E-01 8.4 1E-02 miss 964. 77 4.99 968.97

• 15.80 3.85E-01 1.35E-Ol miss 1588.20 3.22 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWH M Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma A, 1alysis Report for 05-May-16-10004 L3-10220C-FRGS-001 SS (DRIED) Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was no t found in the coincidence library. 5/5/2016 lM6:03AM INTERFERENCE CORRECTED REPORT X X Nuclide Name K-40 Cs-137 Tl-208 Bi-211 Bi-212 Pb-212 Pb212-XR Bi-214 Pb-214 Pb214-XR Ac-228 Nuclide Id Confidence

1. 000 1.000 0.999 0.964 0.999 1.000 1.000 0.998 0.999 1. 000 0.999 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 7.18E+OO 5.59E-02 7.88E-02 4.22E-01 2. 72E-01 5.33E-01 2.39E-01 2. r:'E-01 3.04E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 8.81E-01 2.06E-02 2.30E-02 2.19E-01 5.54E-02 1. 27E-01 5.0SE-02 4.99E-02 f1.14E-02 Page4 of8 Comments 5/5/2016 9:46:03AM Analysis Report for 05-May-16-10004

+ + + + + + + + + L3-10220C-FRGS-001SS (DRIED) Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = Ffrst peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 5/5/2016 9:45:26AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Can berra\Apex\Root\Defa ult\Li brary\ZION LI B-BNL. N LB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCVgrams) (pCilgrams)

K-40 1460.82 ~l: 10.66 7.lBE+OO 2.50 E-01 2.SOE-01 Cr-51 320.08 9.91 -4.99E-02 1.38 E-01 l.38E-Ol Mn-54 834.85 99.98 -5.15E-04 2.03E-02 2.03E-02 Co-58 810.76 99.45 -7.29E-03 l.60E-02 1.60E-02 1674.73 0.52 -1.90E-01 2.24E+OO Co-60 1173.23 99.85 -3.29E-03 1.82E-02 2.39E-02 1332.49 99.98 3.68E-04 l.82E-02 Nb-94 702.65 99.81 4.40E-03 1.46E-02 1. 85E-02 871.09 99.89 -2.73E-03 1.46E-02 Ag-108m 79.13 6.60 l.76E-Ol l.33E-02 4.08E-01 433.94 90.50 -1.28E-03 1.67E-02 614.28 89.80 3.0BE-03 2.14E-02 722.94 90.80 -5.69E-03 l.33E-02 Sn-113 255 .13 2 .11 -7.28E-02 2.03E-02 6.29E-01 391.70 64.97 -5.70E-03 2.03E-02 Cs-134 475.36 1. 48 1. 2 6E-02 l.62E-02 9.32E-01 563.25 8.34 5.23E-02 l.91E-01 569.33 15.37 -3.33E-02 8.63E-02 604.72 97. 62 -5.83E-03 1.62E-02 Page 5 of8 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 5/5/2016 9:46:03AM Page 6 of8 Ai1alysis Report for 05-May-16-1 0004 L3-10220C-FRGS-001SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCUgrams) (pCilgrams)

Co" Cs-134 795.86 85.46 -2.72E-03 1.62E-02 2.09E-02 miss 801.95 8.69 4.90E-03 2.07E-01 miss 1038.61 0.99 3.24E-01 2. OlE+OO miss llfi7. 97 1. 79 2.04E-01 1.52E+OO miss 1365.19 3.02 -2.99E-01 4.04E-01 miss + Cs-137 661.66

• 85.10 5.59E-02 2.3'7E-02 2.37E-02 miss + Eu-152 121.78 28.67 8.25E-04 5.0lE-02 5.0lE-02 miss 244.70 7.61 -6.60E-02 l.73E-01 miss 295.94 0.45 5.98E+OO 5.25E+OO miss 344.28 26.60 l.70E-03 5.02E-02 miss 367.79 0.86 4.29E-01 1.65E+OO miss 411.12 2.24 -~.41E-01 5.99E-01 miss 443. 96 2.83 1.91E-01 5.33E-01 miss 488.68 0.42 3.58E-01 3.SlE+OO miss 563.99 0.49 5.02E-01 3.15E+OO miss 586.26 0.46 -2.27E+OO 2.94E+OO miss 67 8. 62 0.47 -3.19E-01 2.76E+OO miss 688.67 0.86 -3.72E-01 1.61E+OO miss 719.35 0.28 1.33E+OO 6.53E+OO miss 778.90 12.96 -4.83E-03 1.31E-01 miss 810.45 0.32 -8.17E-01 5.02E+OO miss 867.37 4.26 2.87E-02 4.57E-01 miss 919.33 0.43 5.89E-01 3,74E+OO miss 964. 08 14.65 4.91E-02 1.47E-01 miss 1085.87 10.24 4.47E-02 2.21E-01 miss 1089.74 1. 73 -1.17E-01

1. 27E+OO miss 1112. 07 13.69 1.38E-02 1.45E-01 miss 1212.95 1. 43 4.24E-01 1.90E+OO miss 1249.94 0.19 -2.92E-Ol l.35E+Ol miss 1299.14 1. 63 2.06E-01 l.41E+OO miss 1408.01 21. 07 5.09E-02 l.32E-01 miss 1457.64 0.50 -3.70E+OO 6.98E+OO miss 1528.10 0.28 -6.51E-01 3.73E+OO miss + Eu-154 123.07 40.40 5.27E-03 3.49E-02 3.49E-02 miss 247.93 6.89 -l.20E-01 l.99E-01 miss 591.76 4.95 -1. 35E-01 2.64E-01 miss 692.42 1. 78 -2.14E-01 8.83E-01 miss 723.30 20.06 -9.SBE-03 6.43E-02 miss 756.80 4.52 -5.BOE-03 4.39E-01 miss 873.18 12.08 -1.75E-02 9.68E-02 miss 996.29 10.48 -3.67E-02 1.43E-Ol miss 1004.76 18.01 -l.91E-02 8.93E-02 miss 1274.43 34.80 -3.33E-02 4.31E-02 miss 1596.48 1. 80 -9. 7 6E-02 9.87E-01 miss Eu-155 45.30 1. 31 -1.54E+OO 7.SlE-02 3.76E+OO miss 60.01 1. 22 6.34E-04 4.75E+OO miss 86.55 30.70 2.20E-03 7.90E-02 miss 105.31 21.10 9.78E-03 7.51E-02 miss + Tl-208 583.19

• 85.00 7.88E-02 2.35E-02 2.35E-02 miss + Bi-211 351.07

• 13.02 7.23E-01 1.52E-01 1.52E-01 miss + Pb-211 404.85 3.78 -1.46E-01 3.74E-Ol 3.74E-01 miss 5/5/2016 9:46:03AM Page 7 of8 A'nalysis Report for 05-May-16-10004 L3-1 0220C-F RGS-001 SS (ORIE D) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Goinc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 l. llE-01 3.74E-01 7. 63E-01 miss 83~.01 3.52 8.03E-02 5.38E-01 miss + Bi-212 39.86 1. 06 4.83E-01 ~.88E-01 4.53E+OO miss 727. 33 ... 6.67 4.22E-01 2.88E-01 miss 785.37 1.10 -2.38E-01 l.43E+OO miss 1620.50 1. 47 4.32E-01 l.43E+OO miss + Pb-212 115.18 0.60 -4.20E-01 4 .17E-02 2.43E+DO miss 238.63

• 43.60 2.72E-01 4 . 1 7E-02 miss 300.09 3.30 4.91E-01 5.75E-01 miss + Pb212-XR 74.32

• 10.28 5.90E-01 2.27E-01 4 .16E-01 miss 77 .11

• 17.10 5.06E-01 2.27E-01 miss 87.35 3.97 9.59E-02 6.04E-01 miss 89.78 1. 46 1. lOE+OO 1. 63E+OO miss + Bi-21 4 609.32

• 45.49 2.49E-01 4.81E-02 4. 81E-02 miss 768.36 , ,, 4.89 2.45E-01 3.34E-01 miss 806.18 1. 26 -l.90E-01 1.27E+OO miss 934.06 3 .11 3.82E-01 8.05E-01 miss 1120.29

• 14.92 l.62E-01 l.97E-01 miss 1155.21 1. 63 l.84E-01 1.72E+OO miss 1238.12 5.83 3.58E-01 6. OlE-01 miss 1280.98 1. 43 -7.80E-02 l.39E+OO miss 1377. 67 3.99 1. 21E-01 6.00E-01 miss 1385. 31 0.79 l.OOE+OO 2.36E+OO miss 1401.52 1. 33 1.44E-02 1.42E+OO miss 1407.99 2.39 4.48E-01 l.16E+DO miss 1509.21

• 2.13 5.42E-01 6.lOE-01 miss 1661. 27 1. 05 5.74E-01 1.91E+OO miss 1729.59 2.88 6.00E-01 9.89E-01 miss 1764.49 15.30 2.75E-01 2.89E-01 miss 1847.43 2.03 4.53E-01 1.29E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99

• 7.25 4.35E-01 5.57E-02 2.30E-01 miss 295.22

• 18.42 2.30E-01 1.21E-01 miss 351.93 "T 35.60 2.65E-01 5.57E-02 miss 785.96 1. 06 1.64E-01 1. 61E+OO miss + Pb214-XR 74.82

• 5.80 1.0SE+OO 4.00E-01 7.37E-01 miss 77 .11

• 9.70 8.91E-01 4.00E-01 miss 87.35 2.24 1.70E-01 1.07E+OO miss 89.78 0.82 1.97E+OO 2.89E+OO miss + Ra-226 186.21 3.64 3.81E-01 4.92E-01 4.92E-01 miss + Ac-228 129.07 2.42 1. 22E-01 8.69E-02 6.14E-Ol miss 209.25 3.89 2.36E-01 4.04E-01 miss 270.24

• 3.46 3.40E-01 4.29E-01 miss 328.00 2.95 2.50E-01 5.83E-01 miss 338.32

• 11. 27 2.82E-01 l.83E-01 miss 409.46 1. 92 2.14E-01 8.00E-01 miss 463.00 4.40 1.95E-Ol 4.23E-01 miss 794.95 4.25 1.28E-01 4.94E-01 miss 911.20

• 25.80 2.79E-01 8.69E-02 miss 964. 77 4.99 -5.81E-02 4.07E-Ol miss 968.97

• 15.80 3.85E-01 l.54E-01 miss 5/5/2016 9:46:03AM Page 8 of8 Analysis Report for 05-May-16-10004 L3-10220C-FRGS-001 SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

Corr Ac-228 1588.20 3.22 3.25E-01 8.69E-02 7.95E-01 miss + Pa-231 27.36 10.30 O.OOE+OO 3.9'7E-02

3. 97E-02 miss 283.69 1. 70 -2.BlE-01 7.82E-01 miss 300.07 2.47 6.56E-Ol 7.68E-01 miss 302.65 2.20 -2.00E-01 6.64E-01 miss 330.06 1. 40 -6.14E-01 1.05E+OO miss + Th-234 92.38 2 .13 1.20E+OO l.26E+OO l.26E+OO miss 92.80 2.10 1.21E+OO l.28E+OO miss 112.81 0.21 1. 53E-01 8.08E+OO miss + U-235 143.76 10. 96 -5.00E-02

3. lOE-02 l.19E-01 miss 163.33 5.08 3,04E-02 2.61E-01 miss 185.71 57.20 2.45E-02 3.lOE-02 miss 202 .11 1. 08 -4.87E-Ol l.13E+OO miss 205.31 5.01 l.75E-02 2.78E-01 miss + Am-241 59. 54 35.90 -2.24E-02 l.55E-01 l.55E-01 miss + -Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

120 110 100 90 80 70 V) +-' C: :::::s 0 60 u so 40 30 20 10 0. 1000 2000 0000014849.CNF ";-' *;.; 3000 4000 5000 channel Live Time :1800.000 sec Real Time :1801.350 sec start: 1: -0 .2(kev) stop : 8192: 2047. 4(kev) Acq. Start :Thu May OS 09: 15: 18 2016 6000 7000 8000 6/2/2016 8:27:15AM

~§:~pex-Gamma Analysis Report for 02-Jun-16-10001 L3-10220C-FRGS-002SS

{DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real lime Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range {in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number ; 02-Jun-16-10001

L3-10220C-FRGS-002SS

{DRIED) : Off Site Sample 1.311 E+03 grams : Default : 5/23/2016 2:30:00PM

6/2/2016 8:16:32AM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 600.0 seconds : 600.5 seconds : 0.08% : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

6/28/2012

15049 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 8:26:40AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of8 Analysis Report for 02-J un-16-1 0001 L3-10220C-FRGS-002SS (DRIED) Peak Energy ROI No. (keV) start 1 185.84 740 -2 238.58 948 -3 352.00 1400 -4 609.19 2428 -5 661.65 2637 -6 727.1 8 2903 -7 968. 98 3869 -8 1119.95 4473 -9 1460.71 5832 -M :a First peak in a multiplet region m :a other peak in a multiplet region F :a Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 750 743.94 961 954.65 1415 1407.81 2443 2435.68 2652 2645.41 2912 2907.41 3880 3874.39 4484 4478.39 5852 5842.19 6/2/2016 8:27:15AM Net Peak Net Area Area Uncertainty 2.15E+Ol 19.46 1. 04E+02 27.90 1.11E+02 25.16 1. 06E+02 22 .11 1.14E+02 23.05 8.13E+OO 9.22 1. 50E+Ol 9.59 1. 4 7E+Ol 9.97 1.53E+02 25.32 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLID ES Nuclide Id Energy Yield(%) Activity Page 2 of8 Continuum Tentative Counts Nuclide 6.09E+Ol U-235 Ra-226 6.59E+Ol Pb-212 3.68E+Ol Pb-214 Bi-211 1.28E+Ol Bi-214 1. 61E+Ol Cs-137 1.37E+Ol Bi-212 8.00E+OO Ac-228 1.05E+Ol Bi-214 5.81E+OO K-40 Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

• 10.66 6.45E+OO l.21E+OO miss Cs-137 1. 00 661.66

• 85.10 3.52E-01 8.27E-02 miss Bi-211 0.94 351.07

• 13. 02 1.43Et00 4.00E-01 miss Bi-212 0.99 39.86 1. 0 6 727.33

• 6.67 3.41E-Ol 3.89E-01 miss 785.37 1.10 16:20.50 1. 4 7 Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 3.llE-01 9. 72E-02 miss 300.09 3.30 Bi-214 0.99 609.32

• 45.49 5.76E-Ol 1. 39E-01 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29

• 14.92 3.69E-01 2.51E-Ol miss 1155.21 1. 63 1238.12 5.83 Analysis Report for 02-Jun-16-10001 L3-10220C-FRGS-002SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1280.98 1377. 67 1385. 31 1401.52 1407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118. 51 Pb-214 0 , 51 241. 99 295.22 351.93 785. 96 Ra-226 0.99 186.21 Ac-228 0.57 129.07 209.25 270.24 328.00 338.32 409.46 463.00 7 94. 95 911. 20 964. 77 968. 97 1588.20 U-235 0.99 143.76 163.33 185. 71 202.11 205.31 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. j,-* * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold=

0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1. 43 3.99 0.79 1. 33 2.39 2 .13 1. 05 .2. 8 8 15.30 2.03 1.16 7.25 18.4 2 35.60 1. 06 3.64 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 10. 96 5.08 57.20 1. 08 5.01 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 8:27:15AM Page3 of8 Activity Activity Caine (pCUgrams)

Uncertainty Corr 5.24E-O: 1.46E-Ol miss 6.74E-01 6.19E-01 mis s 3.23 E-0 1 2.0 8E-Ol mi s s 4.29E-02 3.94E-02 miss 6/2/2016 8:27:1 SAM Page 4 of8 Analysis Report for 02-Jun-16-10001 L3-10220C-FRGS-002SS (DRIED) llVTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.999 6.45E+OO 1.21E+OO Cs-137 1.000 3.52E-01 8.27E-02 ? Bi-211 0.948 1. 43E+OO 4.00E-01 Bi-212 0.999 3.41E-Ol 3.89E-01 Pb-212 1.000 3.llE-01 9. 72E-02 Bi-214 0.999 5.27E-Ol 1.22E-01 ? Pb-214 0.513 5.24E-01 1.46E-01 ? Ra-226 0.991 6.74E-01 6.19E-01 Ac-228 0.575 3.23E-01 2.0BE-01 ? U-235 0.999 4.29E-02 3.94E-02 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ -nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 6/2/2016 8:27:15AM Analysis Report for 02-Jun-16-10001

+ + +

+ + + + + + L3-10220C-FRGS-002SS (DRIED} Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 8:26:40AM

120 : 8192 Peak CPS (",{,) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canb erra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCUgrams) (pCi/grams) (pCilgrams)

K-40 1460.82

• 10.66 6.45E+OO 4.86E-01 4.86E-01 Cr-51 320.08 9.91 -3.57E-02 3.06E-01 3.06E-01 Mn-54 834.85 99.98 2. 72E-03 4. llE-02 4.llE-02 Co-58 810.76 99.45 -6.93 E-03 4.00E-02 4.00E-02 1674.73 0.52 O.OOE+OO 2.8 7E+O O Co-60 1173. 23 99.85 3.32E-03 3.90E-02 4.65E-02 1332.49 99.98 6.0lE-04 3.9 0 E-02 Nb-94 702.65 99.81 -l.67E-0 3 2.95E-02 2.95E-02 871.09 99.89 2.00E-02 5.27E-02 Ag-108m 79.13 6.60 2.53E-01 3.25E-02 8.42E-01 433.94 90.50 -4.33E-04 3.25E-02 614.28 89.80 -4.08E-03 3.92E-02 722. 94 90.80 -4.26E-03 3.30E-02 Sn-113 255.13 2 .11 -3. llE-01 5.80E-02 l.57E+OO 391.70 64.97 l.13E-02 5.80E-02 Cs-134 475.36 1. 48 -6.09E-01 3.34E-02 2.0lE+OO 563.25 8.34 l.33E-01 5.16E-Ol 569.33 15.37 -5.BOE-02 l.67E-01 604.72 97.62 2.04E-04 3.34E-02 Page 5 of8 Tolerance Nuclide Coinc Corr miss free m iss miss miss miss miss miss miss mi s s miss miss miss free free miss miss miss miss 6/2/2016 8:27:15AM Page 6 of8 Analysis Report for 02-Jun-16-10001 L3-10220C-FRGS-002SS (DRIED) Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 l.18E-02 3.34E-02 4.95E-02 miss 801.95 8.69 -6.36E-02 3.73E-01 miss 1038.61 0.99 -6.65E-01 3.37E+OO miss 1167.97 1. 79 l.98E-01 2.84E+OO miss 1365.19 3.02 4.76E-02 l.54E+OO miss + Cs-137 661.66

• 85.10 3.52E-Ol 5.25E-02 5.25E-02 miss + Eu-152 121. 78 28.67 1.29E-02 8.21E-02 9.49E-02 miss 244.70 7.61 4.88E-02 4.lOE-01 miss 295.9 4 0.45 9.82E+OO 1 .13E+Ol miss 344.28 26.60 3.00E-03 8.21E-02 miss 367.79 0.86 -l.16E+OO 3.37E+OO miss -Hl.12 2.24 -l.86E-Ol l.19E+OO miss 443. 96 2.83 5.32E-02 l.17E+OO miss 488.68 0.42 1.86E+OO 8.46E+OO miss 563.99 0.49 -3.84E-01 8.36E+OO miss 586.26 0.46 -4.0SE+OO 6.90E+OO miss 678.62 0.47 9.31E-01 8.51E+OO miss 688.67 0.86 2.52E+OO 5.70E+OO miss 719.35 0.28 3.18E+OO l.41E+Ol miss 778.90 12.96 -5.66E-02 2.lOE-01 miss 810.45 0.32 -5.00E+OO 1.0lE+Ol miss 867.37 4.26 0.00E+OO 2.00E-01 miss 919.33 0.43 8.95E-Ol 9.22E+OO miss 964.08 14.65 1. 23E-Ol 3.67E-01 miss 1085.87 10.24 l.()7E-01 3.86E-01 miss 1089.74 1. 73 -l.52E-01 l.56E+OO miss 1112.07 13. 69 -1.57E-01 2.53E-01 miss 1212.95 1. 43 3.95E-01 3.62E+OO miss 1249.94 0.19 2.74E+OO 2.79E+Ol miss 1299.14 1. 63 l.03E+OO 3.58E+OO miss 1408.01 21.07 1.04E-01 2. 72E-01 miss 1457.64 0.50 -8.42E+OO

1. 2 6E+Ol miss 1528.10 0.28 4.95E+OO 1.78E+Ol miss + Eu-154 123.07 40.40 -2.07E-02 5.74E-02 5.74E-02 miss 247.93 6.89 -3.51E-02 3.78E-01 miss 591.76 4.95 3.45E-02 5.91E-01 miss 692.42 1. 78 -7.63E-02 2.00E+OO miss 723. 30 20.06 -4.41E-02 1.29E-01 miss 756.80 4.52 8.36E-02 1.0lE+OO miss 873.18 12.08 -6.12E-02 2.82E-01 miss 996.29 10.48 1. 4 7E-02 3.56E-01 miss 1004.76 18.01 -1.29E-02 2.33E-Ol miss 1274.43 34.80 5.35E-02 1.65E-01 miss 1596.48 1. 80 O.OOE+OO 7.26E-01 miss + Eu-155 45.30 1. 31 -l.62E+OO 1.63E-01 8.48E+OO miss 60.01 1. 22 -4.87E-01 l.04E+Ol miss 86.55 30.70 4.72E-02 1.86E-Ol miss 105.31 21.10 5.59E-02 1.63E-01 miss + Tl-208 583.19 85.00 1.12E-01 9.41E-02 9.41E-02 miss + Bi-211 351.07

• 13. 02 l.43E+OO 3.29E-01 3.29E-01 miss + Pb-211 404.85 3.78 6.32E-01 8.0BE-01 l.14E+OO miss 6/2/2016 8:27:15AM Page 7 of8 Analysis Report for 02-Jun-16-10001 L3-10220C-FRGS-002SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) {pCi/grams) (pCi/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 6.44E-01 8.08E-01 2.15E+OO miss 832.01 3.52 -3.04E-01 8.08E-01 miss + Bi-212 39.86 1. 06 -1.14E+OO 6 .13E-01 9.81E+OO miss 727.33 ... 6.67 3.41E-01 6 .13E-01 miss 785.37 1.10 -1.78E-01 3.21E+OO miss 1620.50 1. 47 -2.28E-01 3.07E+OO miss + Pb-212 115 .18 0.60 9.88E-01 1. 02E-01 4.94E+OO miss 238.63

• 43.60 3. llE-01 1.02E-01 miss 300.09 3.30 1.64E-01 1.0lE+DO miss + Pb212-XR 74.82 10.28 7.04E-01 5.18E-01 8.91E-01 miss 77 .11 17.10 4.06E-01 5.18E-01 miss 87.35 3.97 1.46E+OO l.53E+OO miss 89.78 1. 46 3.62E-02 3.06E+OO miss + Bi-214 609.32

• 45.49 5.76E-01 8.BOE-02 8.80E-02 miss 768.36 4.89 7.21E-01 l.30E+OO miss 806.18 1. 26 5.45E-01 3. llE+OO miss 934.06 3.11 4.62E-01 l.69E+OO miss 1120.29

• 14. 92 3.69E-Ol 3.30E-01 miss 1155.21 1. 63 -1.40E-01 3.06E+OO miss 1238.12 5.83 3.97E-01 1.33E+OO miss 1280.98 1. 43 6.lOE-01 3.42E+OO miss 1377. 67 3.99 l.40E+OO 2.23E+OO miss 1385.31 0.79 -6.22E-01 5.05E+OO miss 1401.52 1. 33 2.40E+OO 5.19E+OO miss 1407.99 2.39 9.12E-01 2.39E+OO miss 1509.21 2.13 -2.94E-Ol 2.0lE+OO miss 1661.27 1. 05 -5.92E-02 3.49E+OO miss 1729.59 2.88 1.78E-01 1.31E+OO miss 1764.49 15.30 6.56E-01 7.99E-01 miss 1847.43 2.03 4.84E-01 2.84E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 5.98E-01 l.20E-01 6.33E-01 miss 295.22 18.42 3.65E-01 3.06E-01 miss 351.93 ... 35.60 5.24E-01 1. 20E-01 miss 785. 96 1. 06 8.80E-01 3.64E+OO miss + Pb214-XR 74.82 5.80 1.25E+OO 9.14E-01 l.58E+OO miss 77 .11 9.70 7.16E-01 9.14E-01 miss 87.35 2.24 2.59E+OO 2.72E+OO miss 89.78 0.82 6.44E-02 5.44E+OO miss + Ra-226 186.21 3.64 6.74E-01 9.65E-01 9.65E-Ol miss + Ac-228 129.07 2.42 3.49E-01 2.58E-Ol 1.31E+OO miss 209.25 3.89 l.94E-01 7.81E-Ol miss 270.24 3.46 3.16E-01 1.13E+OO miss 328.00 2.95 3.38E-01 l.28E+OO miss 338.32 11. 27 2.22E-01 3.79E-01 miss 409.46 1. 92 -1.24E-01 1.91E+OO miss 463.00 4.40 3.15E-01 1.12E+OO miss 794.95 4.25 3.06E-01 1.05E+OO miss 911.20 25.80 2.34E-Ol 3.22E-01 miss 964. 77 4.99 9.96E-02 8.90E-01 miss 968. 97

• 15.80 3.23E-Ol 2.58E-01 miss 6/2/2016 8:27:15AM Page 8 of8 Analysls Report for 02-Jun-16-10001 L3-10220C-FRGS-002SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr Ac-228 1588.20 3.22 4.36E-01 2.58E-01 1.79E+OO miss + Pa-231 27.36 10.30 O.OOE+OO l.40E-01 1.40E-01 miss 283.69 1. 70 1.89E-Ol 1.93E+OO miss 300.07 2.47 2.19E-01 l.34E+OO miss 302.65 2.20 -1.20E-01 l.35E+OO miss 330.06 1. 40 -1. 84E-01 2.46E+OO miss + Th-234 92.38 2.13 1.42E+OO 3.00E+OO 3.00E+OO miss 92.80 2.10 1.95E+OO 3.13E+OO miss 112. 8 1 0.21 4.12E+OO 2.08E+Ol miss + U-235 143.76 10.96 1. 33E-02 6.14E-02 2.69E-01 miss 163.33 5.08 2.00E-01 5.91E-01 miss 185. 71

• 57.20 4.29E-02 6.14E-02 miss 202 .11 1. 08 5.lOE-01 2.81E+OO miss 205.31 5.01 2.00E-01 6.23E-01 miss + Am-241 59.54 35.90 -1.67E-01 3.33E-01 3.33E-01 miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 "' ;:;! ' 35 Vl ,1...1 C: ::::s 8 30 25 20 :,e "' .!,, a: 15 "' I :::, 10 5 0 1000 ..... .... "' ' ..c, Cl. .... 9 a, ._ ..... .... ,l, V 2000 3000 0000015049.CNF 4000 5000 channel Live rime :600. 000 sec Rea1 Time :600.490 sec Start: 1: -0 .2 (kev) Stop : 8192: 2047.4(kev)

Acq. start : Thu Jun 02 08: 16: 32 2016 6000 7000 8000 6/2/201b 8:2 7:b3AM ~pe x-Gam 1 m a Analysis Report for 02-Jun-16-10002 L3-10220C-FRGS-003SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real Time Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number . 02-Jun-16-10002

L3-10220C-FRGS-003SS (DRIED) : Off Site Sample 1.397E+03 grams . Default : 5/23/2016 2:40:00PM

6/2/2016 8:16:39AM

130G 1L Soil Sample : JWelch : P40818B : 130G Soil : 600.0 seconds : 601.0 seconds : 0.17% : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15050 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 8:27:21AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

• C:\Ca nberra\Apex\Root\Default\Library\Zion Lib-BN L.NLB

• 1.000FWHM Page 1 of8 6/2/2016 8:27:53AM Page2 of8 Analysis Report for 02-Jun-16-10002 L3-10220C-FRGS-003SS (DRIED) M m Peak Energy ROI No. (keV) start 1 74.86 296 -2 76.93 296 -3 87.05 346 -4 238.57 948 -5 295.15 1174 -6 338.62 1351-7 351.85 1402 -8 583.40 2328 -9 609.24 2-Bl -10 661.52 2640 -11 1460.57 5833 -M = First peak in a multiplet region m = Other peak in a multiplet reg ion F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 312 300.53 312 308.77 352 349.24 960 954.79 1186 1180. 92 1358 1354. 69 1414 1407.59 2338 2333.36 2443 2436.70 2653 2645.79 5853 5843.25 Net Peak Net Area Continuum Area Uncertainty Counts 2.97E+Ol '.:..4 .00 5.52E+Ol 3.39E+Ol 14. 33 4.64E+Ol 1.43E+Ol 14.81 3.73E+01 1.02E+02 28.85 8.09E+01 4.57E+Ol 21.0 1 4.86E+Ol 1. llE+Ol 12. 62 3.17E+Ol 7.62E+Ol 21. 26 3.16E+Ol 3.07E+Ol ll.97 4.61E+OO 5.27E+Ol 18.26 2.66E+Ol 3.21E+Ol 13. 72 1.37E+Ol 1. 56E+02 25.23 2.90E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

• 10.66 6.83E+OO 1.26E+OO Cs-137 0.99 661.66

• 85.10 1.03E-01 4.58E-02 Tl-208 0.99 583.19

• 85.00 9.05E-02 3.70E-02 Pb-212 1. 00 115.18 0.60 238.63

• 43.60 3.21E-01 l.05E-01 300.09 3.30 Pb212-XR 0.99 74.82

• 10.28 1.30E+OO 6.68E-01 77 .11

• 17.10 7.95E-01 3.74E-01 87.35

• 3.97 8.70E-01 9.17E-01 89.78 1. 46 Bi-214 1. 00 609.32

• 45.49 2.99E-Ol 1.lOE-01 Tentative Nuclide Pb214-XR Pb212-XR Pb214-XR Pb212-XR Pb214-XR Pb212-XR Eu-155 Pb-212 Pb-214 Eu-152 Ac-228 Pb-21~ Bi-211 Tl-208 Bi-214 Cs-137 K-40 Caine Co" miss miss miss miss miss miss miss miss Analysis Report for 02-Jun-16-10002 L3-10220C-FRGS-003SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 768.36 806.18 934.06 1120.29 1155. 21 1238.12 1280.98 1377.67 1385.31 1401.52 1407.99 1509.21 1661.27 1729.59 1764.43 1847.43 2118. 51 Pb-214 1. 00 241.99 295.22 351.93 785.96 Ac-228 0.99 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964. 77 968.97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.DDDFWH M Nuclide confidence index threshold

= 0.30 Errors quoted at 2.0DOsigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 4.89 1.26 3.11 14.92 1. 63 5.83 1. 43 3.99 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11.27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 8:27:53AM Page 3 of8 Activity Activity Coinc (pCl/grams)

Uncertainty Co" 3 , 91E-01 l.90E-01 miss 3.77E-01 1.2iE-01 miss 1. 7 OE-01 1.94E-01 miss 6/2/2016 8:27:53AM Analysis Report for 02-Jun-16-10002 L3-10220C-FRGS-003SS (DRIED) INTERFERENCE CORRECTED REPORT X X X ? = X = @ = Nuclide Name K-40 Cs-137 E u-155 Tl-208 Bi-211 Pb-212 Pb212-XR Bi-214 Pb-214 Pb214-XR Ac-228 Nuclide Id Confidence

0. 996 0.999 0.991 0.997 0.963 1.000 0.998 1.000 1.000 0.998 0.999 nuclide is part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 6.83E+OO 1.03E-01 9.0SE-02 3.21E-Ol 9.lOE-01 2.99E-01 3.81E-01 l.70E-01 nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 1.26E+OO 4.58E-02 3.70E-02 1. OSE-01 3.07E-01 1.lOE-01 1.02E-01 1.94E-01 Page 4 of8 Comments 6/2/2016 8:27:53AM Analysis Report for 02-Jun-16-10002

+ +

+ + +

+ + + + L3-10220C-FRGS-003SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAK S : 6/2/2016 8:27:21AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCi!grams) (pCi/grams)

K-40 1460.82

• 10.66 6.83E+OO 3.92E-01 3.92E-01 Cr-51 320.08 9. 91 5.87E-02 4.29E-01 4.29E-01 Mn-54 834.85 99.98 4.35E-03 4.28E-02 4.28E-02 Co-58 810.76 99.45 5.42E-03 4.54E-02 4.54E-02 1674.73 0.52 O.OOE+OO 2.99E+OO Co-60 1173.23 99.85 8.89E-03 5.26E-02 6.06E-02 1332.49 99.98 -4.54E-03 5.26E-02 Nb-94 702.65 99.81 1.78E-02 4.31E-02 5.17E-02 871.09 99.89 -3.29E-03 4.31E-02 Ag-108m 79.13 6.60 7.67E-01 3.39E-02 1. 59E+OO 433.9 4 90.50 5.16E-04 3.39E-02 614.28 89.80 4.05E-03 4.59E-02 722. 9 4 90.80 l.97E-02 5.32E-02 Sn-113 255 .13 2.11 1.07E+OO 5.85E-02 2.15E+OO 391.70 64.97 1.60E-03 5.85E-02 Cs-134 475.36 1. 48 -6.84E-01 3.19E-02 2.36E+OO 563.25 8.34 -6.22E-02 4.70E-Ol 569.33 15.37 -l.56E-02 2.93E-Ol 604. 72 97.62 -l.78E-02 3.19E-02 Page S of8 Tolerance Nuclide Caine Co" miss free miss miss miss miss miss miss miss miss miss m iss miss free free miss miss miss miss 6/2/2016 8:27:53AM Page 6 of8 A,nalysis Report for 02-Jun-16-10002 L3-10220C-FRGS-003SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr Cs-134 795.86 85.46 1.47E-02 3.19E-02 5.48E-02 miss 801.95 8.69 5.61E-02 5.09E-01 miss 1038.61 0.99 -2.08E+OO 2.78E+OO miss 1167.97 1. 79 -3.22E-01

2. 96E+OO miss 1365.19 3.02 -1.28E-Ol 1.09E+OO miss + Cs-137 661.66 ,.. 85.10 l.03E-01 4.95E-02 4.95E-02 miss + Eu-152 121.78 28.67 -1.22E-02 1.36E-01 l.44E-01 miss 244.7 0 7.61 2.04E-01 5.03E-01 miss 295.9 4 0.45 -2.20E-01 l.30E+Ol miss 344.28 26.60 3.92E-03 l.36E-01 miss 367.79 0.86 -l.95E+OO 3.83E+OO miss 411.12 2.24 7. llE-01 1.83E+OO miss 443. 96 2.83 -2.20E-01 9.63E-01 miss 488.68 0.42 -3.13E+OO 7.94E+OO miss 563.99 0.49 2.80E+OO 8.70E+OO miss 586.26 0.46 -4.16E+OO 8.69E+OO miss 678.62 0.47 -3.17E+OO 8.85E+OO miss 688.67 0.86 8.18E-01 5.19E+OO miss 719.35 0.28 1.67E+OO l.46E+Ol miss 778. 90 12. 96 -8.0lE-02 3.09E-01 miss 810.45 0.32 -6.lOE-01 l.17E+Ol miss 867.37 4.26 1.74E-01 l.16E+OO miss 919.33 0.43 1.07E+OO 7.42E+OO miss 964.08 14.65 5.49E-02 3.40E-01 miss 1085.87 10.24 1. 20E-01 5.26E-01 miss 1089.74 1. 73 -9.80E-01 2.06E+OO miss 1112. 07 13. 69 -5.67E-02 3.0SE-01 miss 1212.95 1. 43 6.59E-01 4.06E+OO miss 1249.94 0.19 -1.27E+OO

2. 66E+01 miss 1299.14 1. 63 3.47E-01 3.73E+OO miss 1408.01 21.07 2.78E-02 2.84E-01 miss 1457.64 0.50 -5.99E+OO 2.04E+Ol miss 1528.10 0.28 9.84E-Ol 1.27E+Ol miss + Eu-154 123.07 40.40 -1.38E-02 9.74E-02 9.74E-02 miss 247.93 6.89 6.79E-02 4.82E-01 miss 591.76 4.95 2.0SE-01 7.70E-Ol miss 692.42 1. 78 l.99E-01 1.91E+OO miss 723.30 20.06 9.50E-02 2.41E-01 miss 756.80 4.52 l.84E-02 9.35E-01 miss 873.18 12.08 6.37E-02 3.85E-01 miss 996.29 10.48 1.78E-01 5.18E-01 miss 1004.76 18.01 2.02E-02 1.48E-01 miss 1274.43 34.80 2.04E-02 l.31E-01 miss 1596.48 1. 80 O.OOE+OO 7.57E-01 miss + Eu-155 45.30 1. 31 -4.74E+OO 1.86E-01 2.64E+Ol miss 60.01 1. 22 4.22E+OO 2.79E+Ol miss 86.55

• 30.70 1.13E-01 1.86E-01 miss 105.31 21.10 4.06E-02 2.38E-01 miss + Tl-208 583.19

• 85.00 9.0SE-02 3.00E-02 3.00E-02 miss + Bi-211 351. 07

• 13.02 1.03E+OO 3.07E-01 3.07E-01 miss + Pb-211 404.85 3.78 1.46E-01 9.74E-01 1.04E+OO miss 6/2/2016 8:27:53AM Page 7 of8 Analysis Report for 02-Jun-16-10002 L3-10220C-FRGS-003SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 2.25E-01 9.74E-01 2.08E+OO miss 832.01 3.52 -3.92E-01 9.74E-01 miss + Bi-212 39.86 1. 06 9.67E+OO 9.30E-01 3.14E+Ol miss 727. 33 6.67 4.25E-01 9.30E-01 miss 785. 37 1.10 -5.79E-02 3.34E+OO miss 1620.50 1. 47 1.07E+00 4.15E+OO miss + Pb-212 115 .18 0.60 -1.46E+00 1.16E-01 6.SOE+OO miss 238.63

• 43.60 3.21E-01 1.16E-01 miss 300.09 3.30 1.lSE-02 1. 21E+OO miss + Pb212-XR 74.82

• 10.28 l,30E+OO 5.90E-01 1.19E+OO miss 77 .11

• 17.10 7.95E-01 5.90E-01 miss 87.35

• 3. 97 8.70E-01 1.44E+OO miss 89.78 1. 46 3.83E+OO 5.18E+OO miss + Bi-21 4 609.32

• 45.49 2.99E-01 1.19E-01 1.19E-01 miss 768.36 4.89 2.95E-01 1.03E+00 miss 806.18 1. 26 -3.70E-01 2.96E+OO miss 934.06 3.11 6. llE-01 1. 85E+OO miss 1120.29 14. 92 2.74E-01 5.41E-01 miss 1155.21 1. 63 -1.74E-02 2.92E+00 miss 1238.12 5.83 8.16E-01 1.52E+OO miss 1280.98 1. 43 -4.24E-01 4.18E+OO miss 1377. 67 3.99 5.75E-01 l.58E+OO miss 1385. 31 0.79 1. 03E+00 6.llE+OO miss 1401.52 1. 33 1.02E+OO 3.67E+OO miss 1407.99 2.39 2.45E-01 2.49E+OO miss 1509.21 2.13 6. 77E-01 2.43E+OO miss 1661.27 1. 05 9.27E-01 4.59E+OO miss 1729.59 2.88 5.28E-01 2.23E+OO miss 1764.49 15.30 3.17E-01 6.17E-01 miss 1847.43 2.03 O.OOE+OO 7.46E-01 miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 3.50E-01 1.12E-01 6.15E-01 miss 295.22

• 18.42 3.91E-01 2.49E-01 miss 351.93

• 35.60 3. 77E-01 1.12E-01 miss 785.96 1. 06 6. llE-01 4.08E+OO miss + Pb214-XR 74.82

• 5.80 2.30E+OO 1.04E+OO 2.lOE+OO miss 77 .11

• 9.70 1.40E+00 1.04E+OO miss 87.35

• 2.24 1. 54E+OO 2.54E+OO miss 89.78 0.82 6.82E+OO 9.23E+OO miss + Ra-226 186.21 3.64 1.37E-01 9.92E-01 9.92E-01 miss + Ac-228 129.07 2.42 2.96E-01 3.lOE-01 1.61E+OO miss 209.25 3.89 -4.28E-01 7.47E-01 miss 270.24 3.46 5.25E-01 1.16E+OO miss 328.00 2.95 8.56E-01 1.53E+OO miss 338.32

• 11. 27 1.70E-01 3.lOE-01 miss 409.46 1. 92 3.23E-01 2.12E+OO miss 463.00 4.40 2. llE-01 9.46E-01 miss 794.95 4.25 6. 96E-01 1. 32E+OO miss 911.20 25.80 3.33E-01 3.65E-01 miss 964. 77 4.99 9.43E-02 9.27E-01 miss 968. 97 15.80 3.66E-01 5.27E-01 miss 6/2/2016 8:27:53AM Page 8 of8 Analysis Report for 02-Jun-16-10002 L3-10220C-FRGS-003SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCi!grams) (pCi!grams)

Corr Ac-228 1588.2 0 3.22 2.13E-01 3.lOE-01 1.67E+OO miss + Pa-231 27.36 10.30 5.02E-01 1.51E+OO 3.16E+OO miss 283.69 1. 70 7.88E-01 2.51E+OO miss 300.07 2.47 1.54E-02 l.61E+OO miss 302.65 2.20 -4.18E-01

_. 51E+OO miss 330.06 1. 40 -4.49E-01 2.50E+OO miss + Th-234 92.38 2 .13 1.74E+OO 4.30E+OO 4.30E+OO miss 92.80 2.10 2.09E+OO 4.38E+OO miss 112. 81 0.21 2.lOE+OO 2.78E+Ol miss + U-235 143.76 10. 96 6.95E-03 7. llE-02 3.60E-01 miss 163.33 5.08 1.21E-01 7.21E-01 miss 185.7 1 57.20 3.83E-02 7. llE-02 miss 202 .11 1. 08 -1.lOE+OO

2. 71E+OO miss 205.31 5.01 -5.55E-02 5.75E-01 miss + Am-241 59.54 35.90 -6.14E-02 9.40E-01 9.40E-01 miss + :a; Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > :a; MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss "'Nuclide energy was not found in the coincidence library.

II) ..... C: ::::J 60 55 50 40 35 8 30 25 20 15 10 5 1000 2000 3000 0000015050.CNF 4000 channel 5000 Live Time :600.000 sec Rea 1 Ti me : 601. 010 sec start: 1: -0. l(kev) stop : 8192: 2047 .O(kev) Acq. start :Thu Jun 02 08:16:39 2016 0 ! 6000 7000 8000 Analysis Report for 02-Ju n-16-1 0003 L3-10220C-FRGS-004SS (DRIED) 6/2/2016 8:50:12AM GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead T1me Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 02-Jun-16-10003

• L3-10220C-FRGS-004SS (DRIED)

• Off Site Sample 1 .176E+03 grams : Default : 5/23/2016 3:10:00PM

6/2/2016 8:39:33AM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 600.0 seconds : 600.5 seconds : 0.08 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

6/28/2012

15051 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 8:49:39AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C: \Ca n berra\Apex\Root\Default\Li brary\Zion Lib-BN L. NLB : 1.000FWHM Page 1 of8 Analysis Report for 02-Jun-16-10003 L3-10220C-FRGS-004SS (DRIED) Peak Energy ROI No. (keV) start 1 77.15 305 -2 238.61 949 -3 295.22 1174 -4 351.84 1401 -5 583.23 2326 -6 609.20 2430 -7 661.61 2639 -8 1460.56 5832 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 315 309.82 961 954.77 1186 1180.92 1412 1407.16 2337 2331.94 2444 2435.73 2653 2645.27 5851 5841.55 6/2/2016 8:50:12AM Net Peak Net Area Area Uncertainty 4.43E+Ol 25. 34 7.80E+Ol 28.57 3.78E+Ol 1 9.40 7.28E+Ol 20.18 3. 96E+Ol 1 3.40 7.54E+Ol 19.91 7.96E+Ol 1 8.23 1.27E+02 22.54 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of8 Continuum Tentative Counts Nuclide 8.15E+Ol Pb214-XR Pb212-XR 9.00E+Ol Pb-212 4.24E+Ol Pb-.214 Eu-152 2.64E+Ol Pb-214 Bi-211 4.80E+OO Tl-208 1.93E+Ol Bi-214 2.86E+OO Cs-137 O.OOE+OO K-40 Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

• 10.66 5.97E+OO 1.lBE+OO miss Cs-137 1. 00 661.66

• 85.10 2.74E-01 7.09E-02 miss Tl-208 1. 00 583.19

• 85.00 1.25E-01 4.49E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 2.60E-D1 l.D4E-01 miss 300.09 3.30 Pb212-XR 1. 00 74.82 10.28 77 .11

• 17.10 6.75E-01 4. llE-01 miss 87.35 3.97 89.78 1. 46 Bi-214 1. 00 609.32

• 45.49 4.58E-01 l.33E-01 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155. 21 1. 63 1238.12 5.83 Analysis Report for 02-Jun-16-10003 L3-10220C-FRGS-004SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1280.98 1377.67 1385. 31 1401.52 1407.99 1509.21 1661. 27 1729.59 1764.49 1847.43 2118.51 Pb-214 1. 00 241.99 295.22 351.93 785. 96 Pb214-XR 1. 00 74.82 77 .11 87.35 89.78 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWH M Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1. 43 3.99 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 5.80 9.70 2.24 0.82 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 8:50:12AM Page 3 of8 Activity Activity Caine (pCilgrams)

Uncertainty Corr 3.43E-0 1 1.85E-01 miss 3. 85E-O::..

1. 23E-01 miss 1.19E+OO 7.32E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.996 5.97E+OO 1.18E+OO Cs-137 1. 000 2.74E-Ol 7.09E-02 Tl-208 1. 000 1.25E-01 4.49E-02 X Bi-211 0.964 Pb-212 1. 000 2.60E-01 1.04E-Ol Analysis Report for 02-Jun-16-10003 L3-10220C-FRGS-004SS (DRIED) Nuclide Name ? Pb212-XR Bi-214 Pb-214 ? Pb214-XR Nuclide Id Confidence

1. 000 1. 000 1. 000 1. 000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis 6/2/2016 8:50:12AM Wt mean Wt mean Activity Activity (pCilgrams)

Uncertainty 6.75E-01 4. llE-01 4.58E-01 l.33E-01 3. 72E-Ol 1.02E-01 1.19E+OO 7.32E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Page 4 of& Comments 6/2/2016 8:50:12AM Analysis Report for 02-Jun-16-10003

+ + + + +

+

+ + + L3-10220C-FRGS-004SS (DRIED) Peak Locate Performed on Peak Locate From Chan nel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 8:49:39AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C :\Ca nberra\Apex\Root\Defau lt\Library\Z ION LI B-BNL.N LB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

K-40 1460.82

• 10.66 5.97E+OO 1.27E-01 1.27E-01 Cr-51 320.08 9.91 -1.89E-02 3.79E-01 3.79E-01 Mn-54 834.85 99.98 -1.84E-02 4.20E-02 4.20E-02 Co-58 810.76 99.45 -6.19E-03 3.45E-02 3.45E-02 1674.73 0.52 O.OOE+OO 3.20E+OO Co-60 1173.23 99.85 1.23E-02 5.19E-02 5.19E-02 1332. 49 99.98 2.0lE-02 6.15E-02 Nb-94 702.65 99.81 -6.62E-03 4.00E-02 4.00E-02 871.09 99.89 -2.79E-03 4.23E-02 Ag-108m 79.13 6.60 5.54E-01 3.63E-02 1. 04E+OO 433.94 90.50 3.87E-03 3.63E-02 614.28 89.80 -7.44E-04 4.06E-02 722.94 90.80 4. 71E-03 4. llE-02 Sn-113 255.13 2 .11 -1.91E-01 4.99E-02 1.63E+OO 391.7 0 64.97 -l.52E-02 4.99E-02 Cs-134 475.36 1. 48 6.19E-01 3.42E-02 2.65E+OO 563.25 8.34 9.83E-02 4.47E-Ol 569.33 15.37 -3.99E-02 l.61E-01 Page 5 of 8 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss 604.72 97.62 -7.40E-03 3.42E-02 miss 6/2/2016 8:50:12AM Page 6 of8 Analysis Report for 02-Jun-16-10003 L3-10220C-FRGS-004SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCVgrams) (pCUgrams) (pCi/grams)

Corr Cs-134 7 95. 8 6 85.46 -5.48E-03 3.42E-02 5.13E-02 miss 801.95 8.69 2.12E-01 5.46E-01 miss 1038.61 0.99 -3.37E-01 2.98E+OO miss 1167.97 1. 79 6.69E-01 3.17E+OO miss 1365.19 3.02 2.05E-01 1.48E+OO miss + Cs-137 661. 66

• 85.10 2.74E-01 3.05E-02 3.05E-02 miss + Eu-152 121. 78 28.67 2;60E-02 1.06E-01 1.06E-01 miss 244.70 7.61 -1. 78E-01 3.24E-01 miss 295.94 0.45 9.37E-02 1.22E+01 miss 344.28 26.60 -2 .13E-02 l.16E-01 miss 367.79 0.86 -2.26E+OO 3.18E+OO miss 411.12 2.24 -9.42E-02 1.57E+OO miss 443. 96 2.83 1.54E-01 1.37E+OO miss 488.68 0.42 -4.42E+OO 6.80E+OO miss 563.99 0.49 1.93E-01 7.02E+OO miss 586.26 0.46 -4.34E+OO 7.05E+OO miss 678.62 0.47 2. llE+OO 9.49E+OO miss 688.67 0.86 O.OOE+OO 2.58E+OO miss 719. 35 0.28 1.81E+OO 1.34E+Ol miss 778.90 12. 96 -6.73E-02 l.86E-01 miss 810.45 0.32 8.14E-01 1.13E+Ol miss 867.37 4.26 -1.68E-01 9.91E-01 miss 919.33 0.43 1. 76E+OO 9.22E+OO miss 964. 08 14. 65 1. 85E-01 4.30E-01 miss 1085.87 10.24 3.99E-02 4.80E-01 miss 1089.74 1. 73 -3. 72E-01 1.74E+OO miss 1112. 07 13.69 -2.38E-02 2.82E-01 miss 1212.95 1. 43 1. 76E-01 3.32E+OO miss 1249.94 0.19 1.37E+01 3.56E+01 miss 1299.14 1. 63 2.43E-01 2.08E+OO miss 1408.01 21. 07 6.68E-02 3.04E-01 miss 1457.64 0.50 O.OOE+OO 1.50E+D1 miss 1528.10 0.28 -5.26E-01

1. 36E+Ol miss + Eu-154 123.07 40.40 -l.16E-02 6.60E-02 6.60E-02 miss 247.93 6.89 -l.12E-02 4.74E-01 miss 591.76 4. 95 2.12E-01 9.15E-01 miss 692.42 1. 78 -1. 31E+OO 1.25E+OO miss 723. 30 20.06 4.53E-03 1.87E-01 miss 756.80 4.52 1. 30E-01 1.00E+OO miss 873.18 12.08 -4.39E-02 3.51E-D1 miss 996.29 10.48 4.31E-02 3.98E-01 miss 1004.76 18.01 -4.BOE-03 2.33E-01 miss 1274.43 34.80 3.73E-03 1.57E-01 miss 1596.48 1. 80 2.49E-01 3.22E+OO miss + Eu-155 45.30 1. 31 -3.BOE+OO 1.78E-01 7.95E+D0 miss 60.01 1. 22 -4.84E+OO l.06E+D1 miss 86.55 30.70 6.93E-02 1.79E-01 miss 105.31 21.10 1.57E-02 1.78E-01 miss + Tl-208 583.19

• 85.00 1. 25E-01 3.25E-02 3.25E-D2 miss + Bi-211 351.07

• 13 .02 1.05E+OO 2.95E-01 2.95E-01 miss + Pb-211 404.85 3.78 -1.79E-01 7.22E-01 7.22E-Ol miss 6/2/2016 8:50:12AM Page 7 of8 Analysis Report for 02-Jun-16-10003 L3-10220C-FRGS-004SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCl!grams) (pCi!grams)

Corr Pb-211 427.09 1. 76 -5.94E-01 7.22E-01 l.61E+OO miss 832.01 3.52 5.38E-01 l.54E+OO miss + Bi-212 39.86 1. 06 l.12E+OO 7.79E-01 l .13E+Ol miss 727.33 6.67 l.68E-01 7.79E-01 miss 785.37 1.10 l.49E-01 4.20E+OO miss 1620.50 1. 47 7.39E-Ol 3.43E+OO miss + Pb-212 115 .18 0.60 2.65E+OO l.32E-Ol 6.16E+OO miss 238.63

• 43.60 2.60E-01 l.32E-01 miss 300.09 3.30 7.78E-01 l.23E+OO miss + Pb212-XR 74.82 10.28 4.66E-01 5.82E-01 8.89E-01 miss 77 .11

• 17 .10 6.75E-01 5.82E-01 miss 87.35 3. 97 3.02E-01 l.42E+OO miss 89.78 1. 46 1. 69E+OO 3.66E+OO miss + Bi-214 609.32

• 45.49 4.58E-Ol 1.14E-01 l.14E-Ol miss 768.36 4.89 2.0lE-01 l.05E+OO miss 806.18 1. 26 2.17E+OO 4.61E+OO miss 934.06 3 .11 1.74E-01 l. 43E+OO miss 1120.29 14.92 2.78E-01 5.96E-01 miss 1155. 21 1. 63 1.69E+OO 4. 72E+OO miss 1238.12 5.83 4.65E-01 l.27E+OO miss 1280.98 1. 43 9.98E-01 4.16E+OO miss 1377. 67 3.99 5.47E-Ol l.80E+OO miss 1385.31 0.79 5.20E-Ol 5.64E+OO miss 1401. 52 1. 33 l.46E+OO 4.38E+OO miss 1407.99 2.39 5.87E-Ol 2.67E+OO miss 1509.21 2 .13 7.58E-01 3.16E+OO miss 1661. 27 1. 05 O.OOE+OO l.43E+OO miss 1729.59 2.88 l.98E-01 l.46E+OO miss 1764.49 15.30 3.46E-01 6.87E-01 miss J..847.43 2.03 5.40E-01 3.17E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 3.56E-Ol 1.08E-01 6.19E-01 miss 295.22

• 18.42 3.43E-01 2.49E-01 miss 351.93

• 35.60 3.85E-01 l.08E-01 miss 785.96 1. 06 1.24E+OO 4.66E+OO miss + Pb214-XR 74.82 5.80 8.25E-01 l.03E+OO l.58E+OO miss 77 .11

• 9.70 l.19E+OO l.03E+OO miss 87.35 2.24 5.35E-01 2.52E+D0 miss 89.78 0.82 3.02E+OO 6.51E+OO miss + Ra-226 186.21 3. 64 3.23E-01 9.55E-01 9.55E-01 miss + Ac-228 129.07 2.42 -2.39E-02 4.15E-01 l.29E+OO miss 209.25 3.89 2.45E-01 9.04E-Ol miss 270.24 3.46 3.30E-01 l.14E+OO miss 328.00 2.95 5.71E-02 l.15E+OO miss 338.32 11.27 3.75E-01 4.85E-01 miss 409.46 1. 92 3.03E-01 2.20E+OO miss 463.00 4.40 -1.17E-01 1.05E+OO miss 794.95 4.25 -l.17E-Ol

1. 02E+OO miss 911.20 25.80 3.81E-Ol 4.lSE-01 miss 964. 77 4.99 3.94E-01 1. 2 6E+OO miss 968. 97 15.80 3.15E-01 4.97E-01 miss 6/2/2016 8:50:12AM Page 8 of8 An;ilysis Report for 02-J un-16-1 0003 L3-10220C-FRGS-004SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCl/grams) (pCl/grams)

Corr Ac-228 1588.20 3.22 4.98E-01 4.lSE-01 l.79E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 1. 56E-01 1.56E-01 miss 283.69 1. 70 -1. llE-01 2.04E+OO miss 300.07 2, 47 1.04E+OO l.65E+OO miss 302.65 2.20 1.50E-02 l.29E+OO miss 330.06 1. 40 -2.93E-01 2.15E+OO miss + Th-234 92.38 2.13 2.32E+OO 3.58E+OO 3.SBE+OO miss 92.80 2 .10 2.77E+OO 3.65E+OO miss 112.81 0.21 7.95E+OO 2.16E+Ol miss + U-235 143.76 10. 96 8.87E-02 5.66E-02 2.78E-01 miss 163.33 5.08 1.57E-01 5.22E-Ol miss 185.7 1 57.20 -4.21E-03 5.66E-02 miss 202 .11 1. 08 -6.19E-01 2.55E+OO miss 205.31 5.01 -9.84E-02 5.38E-01 miss + Am-241 59.54 35.90 2.76E-02 4.14E-01 4.14E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ "" Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie ~.1DA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was no t found in the coincidence library.

60 55 so 45 40 35 II) .j.-1 C ::::J 8 30 "" 25 ":' ;'!; "" .0 "" "' ...... 1 ';' 20 15 10 s 0 1000 2000 ..,. ...... "" ..... ' ...., *,.. 7 I'.) 00 ,:::: 3000 0000015051.CNF 4000 channel 5000 Live Time :600.000 sec Real Time :600.480 sec start: 1: -0. 2(kev) stop : 8192: 2047. 4(kev) Acq. Start :Thu Jun 02 08: 39: 33 2016 6000 7000 8000 6/2/2016 8:50:52AM

Atpe.x-G amma Analysis Report for 02-Jun-16-10004 L3-10220C-FRGS-005SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 02-Jun-16-10004

L3-10220C-FRGS-005SS (DRIED) : Off Site Sample 1.320E+03 grams : Default : 5/16/2016 3:25:00PM

6/2/2016 8:39:39AM

130G 1 L Soil Sample : JWeJch ; P40818B : 130G Soil : 600.0 seconds 601.0 seconds

• 0.16 %

• 2.80 .120-8192 120 -8192

• 1.000FWHM 1/27/2016

1/5/2015 15052 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 8:50:18AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of 8 ~{1, Anfllysis Re'port for 02-Jun-16-10004 L3-10220C-FRGS-005SS (DRIED) Peak Energy ROI No. (keV) start 1 238.63 948 -2 295.08 117 6 -3 351. 71 1400 -4 609.31 2430 -5 661.52 2 640 -6 968. 97 3 870 -7 1460.77 5835 -M"' First peak in a multiplet region m "' Other peak in a multiplet region F "' Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 960 955.00 1185 1180. 65 1413 1407.01 2442 2436.98 2652 2645.77 3881 3875.65 5853 5844.03 6/2/2016 8:50:52AM Net Peak Net Area Area Uncertainty 5.79E+Ol 26. 95 2.97E+Ol 16. 34 3.98E+Ol 1 8.30 5.0lE+Ol 1 5.39 4.15E+Ol 15.38 9.38E+OO 7.8 5 1. 34E+02 23.69 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page2 of& Continuum Tentative Counts Nuclide 9.42E+Ol Pb-212 3.27E+Ol Pb-21 4 Eu-152 3.63E+Ol Pb-214 Bi-2 11 7.86 E+OO Bi-214 1.69E+Ol Cs-137 5.25E+O O Ac-228 5.12E+OO K-40 Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 1. 00 1460.82

• 10.66 6.25E+OO 1. 23E+OO miss Cs-137 0.99 661.66

• 85.10 1.41E-01 5.50E-02 miss Pb-212 1. 00 115.18 0.60 238.63

• 43.60 1.93E-01 9.53E-02 miss 300.09 3.30 Bi-214 1. 00 609.32

• 45.49 3.0lE-01 9.93E-02 miss 76 8.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1661. 27 1. 05 Analysis Report for 02-Jun-16-10004 L3-10220C-FRGS-005SS (DRIED) Nuclide Id Energy Name Confidence (keV) B i-214 1. 00 1729.59 1764.49 1847.43 2118.51 Pb-214 0.99 241.99 295.22 351.93 785.96 Ac-228 1. 00 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964. 77 968. 97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold=

0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield{%) 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11.27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 8:50:52AM Page3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 2.68E-01 1.54E-01 miss 2.0 9E-Ol 1.0lE-01 miss 2.22E-01 1.87E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name

• Id Activity Activity Confidence (pCi/grams)

Uncertainty K-40 1. 000 6.25E+OO l.23E+OO Cs-137 0.999 l.41E-Ol 5.50E-02 X Bi-211 0.976 Pb-212 1.000 1.93E-01 9.53E-02 Analysis Report for 02-Jun-16-10004 L3-10220C-FRGS-005SS (DRIED) Nuclide Nuclide Name Id Confidence Bi-214 1. 000 Pb-214 0.998 Ac-228 1.000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis 6/2/2016 wt mean Activity (pCilgrams) 3.0lE-01 2.2 7E-01 2.22E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 8:50:52AM Page 4 of8 Wt mean Comments Activity Uncertainty 9.93E-02 8.47E-02 l.87E-01 6/2/2016 8:50:52AM Ana 1¥sis Report for 02-J u n-16-1 0004 L3-10220C-FRGS-005SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 8:50:18AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canb erra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

+ K-40 1460.82

• 10.66 6.25E+OO 4.98E-01 4.98E-01 + Cr-51 320.08 9.91 -8.67E-02 4.49E-Ol 4.49E-01 + Mn-54 834.85 99.98 -7.02E-03 3.26E-02 3.26E-02 + Co-58 810.76 99.45 -1.05E-02 2.89E-02 2.89E-02 1674.73 0.52 O.OOE+OO 3.39E+OO + Co-60 1173.23 99.85 2.00E-02 5.0lE-02 6.43E-02 1332.49 99.98 O.OOE+OO 5.0lE-02 + Nb-94 7 02.65 99.81 -1.68E-02 2.80E-02 2.80E-02 871.09 99.89 1.44E-02 5.23E-02 + Ag-108m 79.13 6.6 0 -1.68E-01 3 .13E-02 l.49E+O O 433.94 90.50 1. 24E-03 3 .13E-02 614.28 89.80 8.57E-03 4.0lE-02 722. 94 90.80 -2.82E-03 3.64E-02 + Sn-113 255 .13 2 .11 -5.13E-0 1 5.15E-02 l.55E+OO 391.70 64.97 -l.12E-02 5.15E-02 + Cs-134 475.36 1. 48 6.28E-Ol 4. 72E-02 2.98E+OO 563.25 8.34 2.93E-01 5.50E-01 569.33 15.37 4.14E-03 2.26E-01 Pag e 5 of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss m i ss miss mis s miss miss miss free free miss miss mise 604.72 97. 62 1.62E-02 4. 72E-02 miss 6/2/2016 8:50:52AM Page 6 of8 Analysis Report for 02-Jun-16-10004 L3-10220C-FRGS-005SS (DRIED) Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCVgrams) (pCl/grams)

Corr Cs-134 795.86 85.46 -6.35E-03

4. 72E-02 5.lOE-02 miss 801. 95 8.69 -l.07E-02 5.42E-01 miss 1038.61 0.99 4.47E-02 4.33E+OO miss 1167.97 1. 79 7.38E-01 2.89E+OO miss 1365 .19 3.02 3.17E-01 l.47E+OO miss + Cs-137 661.66

• 85.10 1. 41E-01 5.62E-02 5.62E-02 miss + Eu-152 121.78 28.67 -2.03E-02 l.31E-01 l.31E-01 miss 244.70 7.6 1 -l.45E-01 3.67E-01 miss 295.94 0.45 -1.64E+OO l.19E+Ol miss 344.28 26.60 3.52E-03 l.35E-01 miss 367.79 0.86 -1. 02E+OO 3.90 E+OO miss 411.12 2.24 5.79E-01 1.93E+OO miss 443.96 2.83 -2.15E-Ol l.02E+OO miss 488.68 0.42 -1.lOE+OO 7.35E+OO miss 563.99 0.49 -1.74E+OO 6.94E+OO miss 586.26 0.46 -1.48E+OO 9.67E+OO miss 678. 62 0.47 7.46E-01 8.81E+OO miss 688.67 0.86 -6.36E-01 3.73E+OO miss 719. 35 0.28 1. 22E+OO l.18E+Ol miss 778.90 1 2. 96 3.08E-02 3.27E-01 miss 810.45 0.32 -1.38E+OO 9.61E+OO miss 867.37 4.26 2.93E-Ol l.23E+OO miss 919.33 0.43 8.46E-01 1.02E+Ol miss 964.08 14.65 -2.55E-02 3.07E-01 miss 1085.87 10.24 -5.37E-02 3.67E-01 miss 1 089.7 4 1. 73 -8. 71E-01 1.73E+OO miss ll12. 07 13.69 1.00E-02 3.23E-01 miss 1212.95 1. 43 4.98E-02 4.58E+OO miss 1 249.94 0.19 3.19E+OO 2.82E+01 miss 1299.1 4 1. 63 -5.34E-0 2 3.02E+OO miss 1408.01 21. 07 -1. 97E-02 l.69E-Ol miss 1457.64 0.50 -1. 21E+Ol 1. 48E+Ol miss 1528.10 0.2 8 O.OOE+OO 4.94E+OO miss + Eu-154 123.07 40.40 -8.13E-03 9.73E-02 9.73E-02 miss 247.93 6.89 -6.21E-02 4.37E-01 miss 591.76 4.95 -3.55 E-01 5.85E-01 miss 692.42 1. 78 9.36E-03 2.38E+OO miss 723. 30 20.06 2.18E-02 1.85 E-01 miss 756.80 4.52 -2.58E-Ol 7.57E-Ol miss 873.18 12.08 -1. 45E-02 3.48E-01 miss 996.29 10.48 1.16E-01 4.79E-01 miss 1004.7 6 18.01 -6.42E-02 1. 99E-01 miss 1274.43 34.80 -8.32E-03 l.20E-01 miss 1596.48 1. 80 -1.85E-01 2.76E+OO miss + E u-155 45.30 1. 31 -2.15E+OO 2.30E-01 2.70E+Ol miss 60.0 1 1. 22 9.82 E+OO 2.80E+Ol miss 86.55 30.70 -5.6 4E-02 2.30E-01 miss 105.31 21.10 8.81E-02 2.60E-01 miss + Tl-208 583.19 85.00 6.26E-02 8.39E-0 2 8.39E-02 m i ss + Bi-211 351.07 13.02 5.70E-01 3.51E-01 3.SlE-01 miss + Pb-211 404.85 3.78 -3. 72E-Ol 9.09E-01 9.09E-01 m iss 6/2/2016 8: 50:52AM Page 7 of8 Ancilysis Report for 02-Jun-16-10004 L3-10220C-FRGS-005SS (DRIED) Nuclide Energy Yield{%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCi/grams) (pCilgrams)

Corr Pb-211 427.09 1. 76 -4.86E-01 9.09E-01 1. 71E+OO miss 832.01 3.52 O.OOE+OO 1.1 5E+OO miss + Bi-21 2 39.86 1. 06 -8.85E-01 8.05E-01 2.41E+Ol miss 727. 33 6.67 3.39E-01 8.05E-01 miss 785.37 1.10 2.9 4E-02 3.86E+OO miss 1620.50 1. 47 O.OOE+OO 9.89E-01 miss + Pb-212 115.18 0.60 -6.19 E-02 1. 31E-01 7.47E+OO miss 238.63

• 43.60 1.93E-01 1.31E-01 miss 300.09 3.3 0 -1.92E-01 9.61E-01 miss + Pb212-XR 74.82 10.28 5.99E-01 8.00E-0 1 l.49E+OO miss 77 .11 17.10 3.44E-01 8.00E-01 miss 87.35 3.97 l.17E+OO 2. 06E+OO miss 89.78 1. 46 l.18E+OO 4.63E+OO miss + Bi-214 609.32

• 45.49 3.0lE-01 7.60E-02 7.60E-02 miss 768.36 4.89 2.90E-01 l.14E+OO miss 806.18 1.26 1.35E+OO 4.35E+OO miss 934.06 3.11 -1. 96E-01 l.09E+OO miss 1120.29 14.92 2.00E-01 5.20E-01 miss 1155. 21 1. 63 5.96E-01 3.38E+OO miss 1 238.1 2 5.83 -l.67E-01 l.06E+OO miss 1280.98 1. 43 -3.59 E-01 2.31E+OO miss 1377. 67 3.99 .3.44E-01 1. 43E+OO miss 1385.31 0.7 9 9.22E-01 7.21E+OO miss 1401.52 1. 33 2.45E-01 4.34E+OO miss 1407.99 2.39 -1. 73E-01 1.48 E+OO miss 1509.2 1 2 .13 2.39E-01 2.22E+OO miss 1661.27 1. 05 5.23E-01 3.85E+OO miss 1729.59 2.88 1. 96E-01 1. 45E+OO miss 1764.49 15.30 3.38E-01 6.25E-01 miss 1847.43 2.03 -7.30E-0 2 2.15E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 5.0SE-01 1.28E-01 6.73E-01 miss 295.22

• 18.42 2.68E-0 1 2.06E-01 miss 351.93

• 35.60 2.09E-01 1. 28E-01 miss 785.96 1. 06 1. 74E-01 4.0lE+OO miss + Pb214-XR 74.82 5.80 1.06E+OO 1. 41E+OO 2.64E+OO miss 77.11 9.70 6.06E-01 1.41E+OO miss 87.35 2.24 2.07E+OO 3.65 E+OO miss 89.78 0.82 2. llE+OO 8.24E+OO miss + Ra-226 186.21 3.64 7.89E-01 1. 23E+OO 1. 23E+OO miss + Ac-228 129.07 2.42 -4.17E-01 2.55E-01 l.4 2E+OO miss 209.25 3.89 -2.14E-01 8.47E-01 miss 270.24 3.46 6.09E-01 1. 25E+OO miss 328.00 2.95 6.84E-01 1. 48E+OO miss 338.32 11. 27 3.58E-01 4.75E-01 miss 409.46 1. 92 3.84E-01 2.04E+OO miss 463.00 4.40 6.30E-02 8.16E-01 miss 794.9 5 4.25 3.52E-01 1. 28E+OO miss 911. 20 25.80 1. 04E-01 2.71E-01 miss 964.77 4.99 2.37E-01 l.06E+0D miss 968.97

• 15.80 2.22E-0 1 2.55E-0 1 miss 6/2/2016 8:50:52AM Page 8 of& Analysis Report for 02-Jun-16-10004 L3-10220C-FRGS-005SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

Corr Ac-228 1588.20 3.22 4.18E-01 2.55E-01 1.77E+OO miss + Pa-231 27.36 10.30 9.lOE-01 1.28E+OO 3.42E+OO miss 283.69 1. 70 1.91E-01 l.80E+OO miss 300.07 2.47 -2.56E-01 l.28E+OO miss 302.65 2.20 7.96E-01 1.77E+OO miss 330.06 1. 40 1.1 7E-01 2.80E+OO miss + Th-234 92.38 2.13 3.23E+OO 5.75E+OO 5.75E+OO miss 92.80 2.10 5.55E+OO 6.25E+OO miss 112. 81 0.21 1.77E+OO 3.44E+Ol miss + U-235 143.76 10. 96 4.55E-02 7.37E-02 3.27E-01 miss 163.33 5.08 1.19E-01 6.87E-01 miss 185.71 57.20 2.16E-02 7.37E-02 miss 202 .11 1. 08 -7.SlE-01 2.87E+OO miss 205.31 5.01 1.29E-01 7.04E-01 miss + Am-241 59.54 35.90 8.55E-02 9.37E-01 9.37E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 Ill ,i-1 C: :::I 8 30 25 20 ..... i 15 10 5 ~f . I I 0 I 1000 ;:'!j 1 ;!; ;'!; 2000 3000 0000015052.CNF 4000 Channel 5000 Live Time :600.000 sec Real Time : 600. 980 sec start: 1: -0.l(kev) stop : 8192; 2047.0(kev)

Acq. Start :Thu Jun 02 08: 39: 39 2016 6000 7000 8000 6/2/2016 9:21:44AM Apex-Gamma Analysis Report for O?.-Jun-16-10005 L3-10220C-FRGS-006SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 02-Jun-16-10005

L3-10220C-FRGS-006SS (DRIED) : Off Site Sample 1.111 E+03 grams : Default : 5/16/2016 3:45:00PM

6/2/2016 9:11:04AM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 600.0 seconds : 600.4 seconds : 0.07 % : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

6/28/2012

15053 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 9:21:10AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Can berra\Apex\Root\Default\Library\Zion Li b-BN L. N LB : 1.000FWHM Page l of8 Analysis Report for 02-Jun-16-10005 L3-10220C-FRGS-006SS (DRIED) Peak Energy ROI No. (keV) start 1 74.73 297 -2 238.61 948 -3 295.23 1176 -4 351.83 1401-5 583.16 2326 -6 60 9. 2 9 2427 -7 661.50 2638 -8 1460.64 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 303 300.17 961 954.78 1187 1180.96 1413 1407.12 2337 2331.66 2443 2436.08 2651 2644.82 5850 5841. 87 6/2/2016 9:21:44AM Net Peak Net Area Area Uncertainty 2.59E+Ol 17.45 9.36E+Ol 24.30 3.43E+Ol 17.22 5.55E+Ol 18. 92 4.75E+Ol 14.85 5.31E+Ol 18.52 6.27E+Ol 18.00 1.10E+02 21. 24 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLID ES Nuclide Id Energy Yield(%) Activity Page 2 of8 Continuum Tentative Counts Nuclide 4.62E+Ol Pb214-)~R Pb212-XR 3.88E+Ol Pb-212 3.14E+Ol Pb-214 Eu-152 2.91E+Ol Pb-214 Bi-211 6.96E+OO Tl-208 2.39E+Ol Bi-214 1.66E+Ol Cs-137 2.68E+OO K-40 Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

• 10.66 5.45E+OO 1.16E+OO miss Cs-137 0.99 661.66

• 85.10 2.28E-01 7. llE-02 miss Tl-208 1. 00 583.19

• 85.00 1.59E-01 5.32E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 3.30E-01 1. OlE-01 miss 300.09 3.30 Bi-214 1. 00 609.32

• 45.49 3.42E-01 1.26E-01 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 3 1 0.79 1401.52 1. 33 Analysis Report for 02-Jun-16-10005 L3-10220C-FRGS-006SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118.51 Pb-214 1. 00 241.99 295.22 351. 93 785.96 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 9:21:44AM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 3.30E-0 1 1. 7 4E-01 miss 3.lOE-0:.. l.17E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.998 5.45E+OO 1.16E+OO Cs-137 0.998 2.28E-01 7. llE-02 Tl-208 1. 000 1.59E-01 5.32E-02 X Bi-211 0. 965 Pb-212 1. 000 3.30E-01 l.OlE-01 Bi-214 1. 000 3.42E-01 1.26E-01 Pb-214 1. 000 3.16E-01 9.70E-02 Analysis Report for 02-Jun-16-10005

? X @ = =

= L3-10220C-FRGS-006SS (DRIED) nuclide is part of an undetermined solution nuclide rejected by the interference analysis nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 6/2/2016 9:21 :44AM Page4 of8 6/2/2016 9:21:44AM Analysis Report for 02-Jun-16-10005

+ + + + + + + + + L3-10220C-FRGS-006SS

{DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) l 74.:3 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 9:21:10AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 4.31519E-02 33.70 Peak Type Tol. NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

K-40 1460.82

• 10.66 5.45E+OO 4.25E-01 4.25E-Ol Cr-51 320.08 9.91 2.28E-01 5.39E-01 5.39E-01 Mn-54 834.85 99.98 -3.13E-03 3.49E-02 3.49E-02 Co-58 810.76 99.45 5.61E-03 5.SlE-02 5.51E-02 1674.73 0.52 -2.68E+OO 9.86E+OO Co-60 1173.23 99.85 1. 53E-02 1. 35E-02 6.00E-02 1332. 49 99.98 O.OOE+OO 1.35E-02 Nb-94 702.65 99.81 6.lOE-03 4.56E-02 4.56E-02 871.09 99.89 2.24E-02 5.26E-02 Ag-108m 79.13 6.60 -4.12E-01 3.36E-02 9.16E-01 433.94 90.50 -3.41E-04 3.60E-02 614.28 89.80 -2.19E-04 4.63E-02 722. 94 90.80 -6.04E-03 3.36E-02 Sn-113 255.13 2 .11 -8. 71E-01 6.90E-02 l.47E+OO 391.70 64.97 9.53E-03 6.90E-02 Cs-134 475.36 1. 48 -6.44E-01 3.64E-02 1.82E+OO Page 5 of8 Tolerance Nuclide Pb212-XR Pb214-XR Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free m iss 6/2/2016 9:21:44AM Page 6 of8 Analysis Report for 02-Jun-16-10005 L3-10220C-FRGS-006SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pCilgrams) (pCi/grams)

Corr Cs-134 563.25 8.34 8.03E-02 3.64E-02 5.63E-01 miss 569.33 15.37 -4.06E-02 l.99E-01 miss 604. 72 97.62 -6.97E-03 3.64E-02 miss 795.86 85.46 1. 30E-02 5.88E-02 miss 801.95 8.69 -1.17E-01 3.83E-01 miss 1038.61 0.99 -1.76E+OO 4.00E+OO miss 1167.9 7 1. 79 2. llE-01 3.09E+OO miss 1365.19 3.02 O.OOE+OO 4.59E-01 miss + Cs-137 661.66

• 85.10 2.28E-01 6.12E-02 6.12E-02 miss + Eu-152 121.78 28.67 4.57E-02 1.12E-01 l.12E-01 miss 244.70 7.61 -1.73E-01 3.73E-01 miss 2 95. 94 0.45 1.35E+01 1.30E+Ol miss 344.28 26.60 4.78E-02 1.39E-01 miss 36 7.79 0.86 8.20E-02 3.59E+OO miss 411.12 2.24 7.91E-01 1.94E+OO miss 443. 96 2.83 -1.61E-01 l.17E+OO miss 488.68 0.42 -l.42E+OO 8.46E+OO miss 563.99 0.49 2.63E+OO 9.44E+OO miss 586.26 0.46 -S.22E+OO 6.69E+OO miss 678.62 0.47 -5.80E-01 8.77E+OO miss 688.67 0.86 1.06E+OO 4.87E+OO miss 719.35 0.28 -3.92E-01 1.41E+Ol miss 778.9 0 12.96 -7.35E-02 3.21E-01 miss 810.45 0.32 -2. 96E+OO 1.19E+Ol miss 867.37 4.26 -2.04E-01 8.12E-01 miss 919.33 0.43 -9.07E-01 8.42E+OO miss 964.08 14.65 -5.0lE-02 2.54E-01 miss 1085.8 7 10.24 -8.16E-02 5.08E-01 miss 1089.74 1. 73 7.17E-02 3.0lE+OO miss 1112. 07 13.69 -1.70E-Ol 3.86E-01 miss 1212.95 1. 43 4.67E-02 3.03E+OO miss 1249.9 4 0.19 -4.67E+OO 2.71E+Ol miss 1299.1 4 1. 63 3.00E-01 2.21E+OO miss 1408.01 21. 07 4.90E-02 2.28E-01 miss 1457.64 0.50 O.OOE+OO l.67E+Ol miss 1528.10 0.28 O.OOE+OO 5.28E+OO miss + Eu-154 123.07 40.40 -1.72E-02 7.19E-02 7.19E-02 miss 247.93 6.89 2.24E-02 4.16E-01 miss 591.76 4.95 l.45E-01 8.21E-01 miss 692.42 1. 78 5.71E-01 2.36E+OO miss 723.3 0 20.06 l.78E-02 1.98E-01 miss 756.8 0 4.52 1. 25E-02 6.99E-01 miss 873.18 12.08 -1.40E-Ol 2.28E-Ol miss 996.29 10.48 4.89E-02 ll. 70E-01 miss 1004.76 18.01 2.67E-02 2.47E-01 miss 1274.43 34.80 4.65E-02 1.66E-01 miss 1596.48 1. 80 O.OOE+OO 8.58E-01 miss + Eu-155 45.30 1. 31 -2. 96E+OO 1.76E-01 8.07E+OO miss 60.01 1.22 1.79E+OO 1. 07E+Ol miss 86.55 30.70 -7.93E-03 1.76E-01 miss 105.31 21.10 3.89E-02 1.89E-01 miss 6/2/2016 9:21;44AM Page 7 of8 Analysis Report for 02-Jun-16-10005 L3-10220C-FRGS-006SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr + Tl-208 583.19

• 85.00 l.59E-01 3.94E-02 3.94E-02 miss + Bi-211 351.0'7

• 13.02 8.48E-01 3.35E-01 3.35E-Ol miss + Pb-211 404.85 3.78 -9.33E-02 7.55E-01 8.75E-01 miss 427.09 1. 76 6.28E-01 2.36E+OO miss 832.01 3.52 -1. 71E-Ol 7.55E-01 miss + Bi-212 39.86 1. 06 -3.44E+OO 9.32E-01 9.43E+OO miss 727. 33 6.67 3.34E-01 9.32E-01 miss 785.37 1.10 5.26E-01 4.74E+OO miss 1620.50 1. 47 3.91E-01 2.87E+OO miss + Pb-212 115.18 0.60 4.61E+OO 9.47E-02 7.13E+OO miss 238.63

• 43.60 3.30E-01 9.47E-02 miss 300.09 3.30 1.29E-01 1.06E+OO miss + Pb212-XR 74.82 10.28 7.58E-Ol 6.41E-01 1.03E+OO miss 77 .11 17.10 6.79E-01 6.41E-01 miss 87.35 3.97 5.81E-01 1.42E+D0 miss 89.78 1. 46 9. 71E-01 3.72E+OO miss + Bi-214 609.32

• 45.49 3.42E-01 l.39E-01 l.39E-01 miss 768.36 4.89 1.SOE-01 1.05E+OO miss 806.18 1. 26 1. 03E-01 3.67E+OO miss 934.06 3.11 5.25E-01 1.78E+OO miss 1120.29 14.92 4.57E-01 6.BOE-01 miss 1155.21 1. 63 7.95E-01 3.61E+OO miss 1238.12 5.83 1.80E-D1 1.06E+OO miss 1280.98 1. 43 -3.84E-01 3.12E+OO miss 1377.67 3.99 5.09E-01 1. 53E+OO miss 1385. 31 0.79 3.85E+OO 9.05E+OO miss 1401.52 1. 33 6.07E-01 4.16E+OO miss 1407.99 2.39 4.31E-01 2.00E+OO miss 1509.21 2.13 -7.29E-01 l.88E+OO miss 1661.27 1. 05 4.89E-01 4. llE+OO miss 1729.59 2.88 1.05E+OO 2.75E+OO miss 1764.49 15.30 2.38E-01 6.02E-01 miss 1847.43 2.03 6.23E-01 3.36E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 3.46E-01 1. 23E-01 6.03E-01 miss 295.22

• 18.42 3.30E-Ol 2.26E-Ol miss 351.93

• 35.60 3.lOE-01 1. 23E-01 miss 785.96 1. 06 3.46E-01 4.63E+OO miss + Pb214-XR 74.82 5.80 1.34E+OO 1.13E+OO l.83E+OO miss 77 .11 9.70 1.20E+OO 1.13E+OO miss 87.35 2.24 1.03E+OO 2.52E+OO miss 89.78 0.82 1.73E+OO 6.62E+OO miss + Ra-226 186.21 3.64 9.30E-01 1.19E+OO 1.19E+OO miss + Ac-228 129.07 2.42 6. llE-01 3.18E-01 l.57E+OO miss 209.25 3.89 2.91E-01 8.26E-Ol miss 270.24 3.46 4.56E-01 l.18E+OO miss 328.00 2. 95 4.35E-01 1. 45E+OO miss 338.32 11.27 3.40E-01 4.85E-01 miss 409.46 1. 92 2.43E-01 2.33E+OO miss 463.00 4.40 1.llE-01 9.58E-01 miss 6/2/2016 9:21:44AM Page 8 of 8 Analysis Report for 02-Ju n-16-1 0005 L3-10220C-FRGS-006SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCl/grams)

Corr Ac-228 794.95 4.25 3.81E-01 3.18E-01 l.31E+00 miss 911.20 25.80 1.29E-01 3.lSE-01 miss 964. 77 4.99 -2.BOE-01 8.63E-01 miss 968. g7 15.80 4. 71E-01 6.23E-01 miss 1588.20 3.22 5. 27E-Ol l.89E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 1.65E-Ol 1.65E-01 miss 283.69 1. 70 -2.60E-01 1.91E+OO miss 300.07 2.47 1. 73E-01 1.41E+OO miss 302.65 2.20 2.86E-01 1.48E+OO miss 330.06 1. 40 9.90E-01 2.82E+OO miss + Th-234 92.38 2.13 2.38E+OO 3.BOE+OO 3.94E+OO miss 92.8 0 2.10 2. llE+OO 3.80E+OO miss 112. 81 0.21 2.26E+OO 2.79E+Ol miss + U-235 143.76 10. 96 l.89E-02 6. 91E-02 3.00E-01 miss 163.33 5.08 5.19E-02 5.53E-01 miss 185.71 57.20 2.21E-02 6.91E-02 miss 202 .11 1. 08 -5.86E-01 2.07E+OO miss 205.31 5.01 -6.75E-02 5.13E-01 miss + Am-241 59.54 35.90 -4.55E-02 3.63E-01 3.63E-01 miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 40 35 V) ...... C: 8 30 25 20 15 co ,:::: 10 5 0 1000 2000 .._ 7 "' u 3000 0000015053.CNF 4000 channel 5000 Live Time :600.000 sec Real Time :600.440 sec start: 1: -0. 2(kev) stop : 8192: 2047 .4(kev) Acq. Start :Thu Jun 02 09:11:04 2016 C, .... 6000 7000 8000 6/2/2016 9:22:24AM

~pex-Gamma Analysis Report for 02-Jun-16-10006 L3-10220C-FRGS-007SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 02-Jun-16-10006

L3-10220C-FRGS-007SS (DRIED) : Off Site Sample 1.243E+03 grams : Default : 5/23/2016 4:00:00PM

6/2/2016 9:11:11AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 600.0 seconds : 600.9 seconds : 0.15% : 2.80 :120-8192

120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15054 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 9:21 :SOAM Peak Analysis From Channel Peak Analysis To Channe l : 120 : 8192 Tentative NID Library Peak Match Tolerance

C: \Ca n berra\Apex\Root\Default\Library\Zion Li b-BN L. NLB : 1.000FWHM Page 1 of8 Analysis Report for 02-Ju n-16-1 0006 L3-10220C-FRGS-007SS (DRIED) Peak Energy ROI No. (keV) start 1 186.03 740 -2 238.59 94 7 -3 338.48 1349 -4 351.78 1401 -5 609.21 2432 -6 661.69 2642 -7 968.94 3870 -8 1460.71 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 749 744.79 962 954.84 1360 1354.12 1414 1407.30 2443 2436.57 2652 2646.45 3881 3875.52 5853 5843.79 6/2/2016 9:22:24AM Net Peak Net Area Area Uncertainty 1.74E+Ol 21.08 6.84E+Ol 28. 45 2.22E+Ol 15.46 4.54E+Ol 20.81 2.92E+Ol 13.77 2.44E+Ol 13 .11 1.70E+Ol 9.17 1.20E+02 22. 96 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page?. of8 Continuum Tentative Counts Nuclide 8 .13E+Ol Ra-226 U-235 8.72E+Ol Pb-212 3.36E+Ol Ac-228 5 .13E+Ol Pb-21<; Bi-211 l.56E+Ol Bi-214 l.92E+Ol Cs-137 4.00E+OO Ac-228 9.02E+OO K-40 Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.99 1460.82

• 10.66 5.95E+OO 1. 25E+OO miss Cs-137 1. 00 661. 66

• 85.10 8.82E-02 4.85E-02 miss Bi-211 0.97 351.07

• 13. 02 6.90E-01 3.35E-01 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 2.43E-01 l.OBE-01 miss 300.09 3.30 Bi-214 1. 00 609.32

• 45.49 l.86E-01 9.07E-02 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 Analysis Report for 02-Jun-16-10006 L3-10220C-FRGS-007SS (DRIED) &1 ** ,.1;111'ti Id ~narnu .........

,,uv -**-*::11 Name Confidence (keV) Bi-214 1. 00 1509.21 1661.27 1729.59 1764.49 1847.43 2118.51 Pb-214 0.99 241.99 295.22 351.93 785. 96 Ra-226 0.99 186.21 Ac-228 0.57 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964.77 968.97 1588.20 U-235 0.99 143.76 163.33 185. 71 202 .11 205.31 .. = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FW HM Nuclide confidence index threshold=

0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 3.64 2.42 3.89 3.46 2.95 11. 27 1.92 4.40 4.25 25.80 4.99 15.80 3.22 10. 96 5.08 57.20 1. 08 5.01 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 9:22:24AM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 2.52E-Ol 1.23E-01 miss 6.57E-01 8.05E-01 miss 3.81E-0:i_ 2.72E-01 miss 4.28E-O::..

2.34E-01 miss 4.lBE-02 5.12E-02 miss INTERFERENCE CORRECTED REPORT Analysis Report for 02-Ju n-16-10006 L3-10220C-FRGS-007SS (DRIED) Nuclide Name K-40 Cs-137 ? Bi-211 Pb-212 Bi-214 ? Pb-214 ? Ra-226 Ac-228 ? U-235 Nuclide Id Confidence 0.999 1. 000 0.970 1. 000 1. 000 0.999 0.998 0.573 0. 996 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis 6/2/2016 9:L2:24AM Wt mean Wt mean Activity Activity (pCilgrams)

Uncertainty 5.95E+OO 1. 25E+OO 8.82E-02 4.BSE-02 6.90E-01 3.35E-01 2.43E-01 l.08E-01 l.86E-01 9.07E-02 2.52E-01 1.23E-01 6.57E-01 8.0SE-01 4.0BE-01 1.77E-01 4.lBE-02 5.12E-02 @ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Page4 of8 Comments 6/2/2016 9:22:24AM Analysis Report for 02-Jun-16-10006

+ + + + +

+ + + + L3-10220C-FRGS-007SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (ke V) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 9:21 :50AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA Name (keV) (pCilgrams) (pCilgrams)

K-40 1460.82

• 10.66 5.95E+OO 6.80E-01 Cr-51 320.08 9.91 l.64E-01 4.97E-01 Mn-54 834.85 99.98 -2.51E-02 3.41 E-02 Co-58 810.76 99.45 8.22E-03 4.19E-02 1674.73 0.52 3. llE-01 Co-60 1173.23 99.85 2.68E-02 6.81E-02 1332.49 99.98 2.93E-02 Nb-94 702.65 99.81 9.61E-03 1.00E-02 871.09 99.89 O.OOE+OO Ag-108m 79 .13 6.60 3.04E-01 2.73E-02 433.9 4 90.50 -2.49E-02 614.28 89.80 1.09E-02 722. 9 4 90.80 2.28E-02 Sn-113 255.13 2 .11 -6.76E-03 4.92E-02 391.70 64.97 -8. 61E-03 Cs-134 475.36 1. 48 -2.SlE-01 3.91E-02 ~63.25 8.34 3.27E-01 569.33 15.37 -2.91E-02 604.72 97.62 -8.36E-03 Peak Type LineMDA (pCi/grams) 6.80E-01 4.97E-01 3. 41E-02 4.19E-02 9.15E+OO 6.81E-02 8.21E-02 4.52E-02 1. OOE-02 1.61E+OO 2.73E-02 5.16E-02 6.SlE-02 1. 82E+OO 4.92E-0~ 2.65E+OO 6.27E-01 2.38E-01 3.91E-02 Page 5 of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 6/2/2016 9:22:24AM Page 6 of8 Analysis Report for 02-Jun-16-10006 L3-10220C-FRGS-007SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 5.47E-03 3. 91E-02 5.38E-02 miss 801.95 8.69 -8.12E-02 5.72E-01 miss 1038.61 0.99 9.55E-01 5.lOE+OO miss 1167.97 1. 79 7.25E-02 3.05E+OO miss 1365.19 3.02 5.38E-01 2.0lE+OO miss + Cs-137 661.66

• 85.10 8.82E-02 6.lOE-02 6.lOE-02 miss + Eu-152 121.78 28.67 9.13E-02 6.59E-02 :: . 64E-01 miss 244.70 7.61 -6.04E-02 4.76E-01 miss 295.94 0.45 5.37E+00 1.20E+Ol miss 344.28 26. 60 -3. llE-02 l.lOE-01 miss 367.79 0.86 -8.55E-01

3. 96E+OO miss 411.12 2.24 1. 05E+OO 2.llE+OO miss 443. 96 2.83 2.33E-01 l.50E+OO miss 488.68 0.42 -2.30E+OO 6.40E+OO miss 563.99 0.49 5.75E+OO l.06E+Ol miss 586.26 0.46 -2.53E+OO 9.25E+OO miss 678.62 0.47 2. 78E+OO 8.69E+OO miss 688.67 0.86 1. 20E+OO 5.19E+OO miss 719.35 0.28 -6.48E-02 l.26E+Ol miss 778. 90 12.96 2.lOE-02 3.18E-01 miss 810.45 0.32 1. 83E-01 l.02E+Ol miss 867.3 7 4.26 4.28E-01 1.22E+OO miss 919.33 0.43 -1.SOE+OO 8.34E+OO miss 964. 08 14.65 1.61E-01 4.07E-01 miss 1085.87 10.24 -7.39E-02 4.52E-01 miss 1089.74 1. 73 -l.14E+OO l.83E+OO miss 1112. 07 13.69 6.37E-02 5.06E-01 m i ss 1212.95 1. 43 -2.08E-01 3.89E+OO miss 1249.94 0.19 2.73E+OO 2.68E+Ol miss 1299.14 1. 63 8.29E-01 3.57E+OO miss 1408.01 21.07 O.OOE+OO 6.59E-02 miss 1457.64 0.50 -7.78E+OO 1.74E+01 miss 1528.1 0 0.28 3.87E+OO 1.80E+Ol miss + Eu-154 123.07 40.40 5.95E-02 1.0lE-01 l.18E-01 miss 247.93 6.89 2. llE-01 5.88E-01 miss 591.76 4.95 -4.61E-02 9.14E-01 miss 692.42 1. 78 1.98E-02 2.52E+OO miss 723. 30 20.06 7.28E-02 2.84E-01 miss 756.80 4.52 -5.28E-02 8.95E-01 miss 873.18 12.08 2.56E-02 2.85E-01 miss 996. 2 9 10.48 4.52E-02 4.17E-Ol miss 1004.76 18.01 -1.89E-02 1.67E-01 miss 1274.43 34.80 -5.lOE-02 l.OlE-01 miss 1596.48 1. 80 O.OOE+OO 8.51E-01 miss + Eu-155 45.30 1. 31 7.48E-01 2.27E-01 .2.97E+Ol miss 60.01 1. 22 -l.07E+Ol 2.61E+Ol miss 86.55 30.70 2.lOE-03 2.27E-01 miss 105.31 21.10 -5.02E-02 2.56E-01 miss + Tl-208 583.19 85.00 7.77E-02 8.91E-02 8.91E-02 miss + Bi-211 351. 07

• 13.02 6.90E-01 4.38E-01 4.38E-01 miss + Pb-211 404.85 3.78 -3.54E-01 8.69E-01 8.69E-01 miss 6/2/2016 9:22:24AM Page 7 of8 Analysis Report for 02-Jun-16-10006 L3-10220C-FRGS-007SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi!grams) (pCilgrams) (pCi/grams)

Co" Pb-211 427.09 1. 76 2.19E-01 8.69E-01 2.05E+OO miss 832.01 3.52 5.13E-01 1. 61E+OO miss + Bi-212 39.86 1. 06 2.78E+OO 8.18E-01 2.75E+Ol miss 727. 33 6.67 1.20E-01 8.18E-01 miss 785.37 1.10 3.57E-01 4.70E+OO miss 1620.50 1. 47 2.43E-Ol 2.86E+OO miss + Pb-212 115 .18 0.60 -4.69E-02 l.45E-01 7.57E+OO miss 238.63

• 43.60 2.43E-01 1.45E-01 miss 300.09 3.30 4.02E-01 1.36E+OO miss + Pb212-AR 74.82 10.28 3.91E-01 8.40E-01 l.28E+OO miss 77 .11 17.10 4.55E-01 8.40E-Ol miss 87.35 3. 97 9.80E-01 2.14E+OO miss 89.78 1. 46 1.87E-01 5.06E+OO miss + Bi-214 609.32

• 45.49 l.86E-01 l.07E-01 l.07E-01 miss 768.36 4.89 1.88E-01 1.04E+OO miss 806.18 1. 26 9.25E-01 3. 91E+OO miss 934.06 3.11 6.45E-01 l.88E+OO miss 1120.29 14.92 2.35E-01 5.90E-01 miss 1155.21 1. 63 -5.34E-01 2.94E+OO misc; 1238.12 5.83 7.33E-01 l.45E+OO miss 1280.98 1. 43 -1.76E+OO 2.45E+OO miss 1377. 67 3.99 6.46E-Ol 1.78E+OO miss 1385. 31 0.79 -8.20E-01 4.69E+OO miss 1401.52 1. 33 O.OOE+OO l.04E+OO miss 1407.99 2.39 O.OOE+OO 5.79E-01 miss 1509.21 2.13 5.07E-01 2.35E+OO miss 1661. 27 1. 05 1. llE+OO 5.16E+OO miss 1729.59 2.88 2.09E-01 1.53E+OO miss 1764.49 15.30 2.39E-01 5.62E-01 miss 1847.43 2.03 2.32E-01 2.88E+OO miss > 2118. 51 1.16 O.OOE+OO 0.00E+OO miss I* Pb-214 241.99 7.25 3.44E-01 l.60E-01 7.15E-01 miss 295.22 18.42 3.17E-01 3.23E-01 miss 351.93

• 35.60 2.52E-01 l.60E-01 miss 785. 96 1. 06 l.32E-01 4.88E+OO miss + Pb214-XR 74.82 5.80 6.93E-01 1.48E+OO 2.27E+OO miss 77 .11 9.70 8.02E-Ol l.48E+OO miss 87.35 2.24 1.74E+OO 3.79E+OO miss 89.78 0.82 3.34E-01 9.0lE+OO miss + Ra-226 186.21

• 3.64 6.57E-01 1. 31E+OO 1.31E+OO miss + Ac-228 129.07 2.42 -1.12E-01 2.34E-01 1. 71E+OO miss 209.25 3.89 4.79E-01 1.07E+OO miss 270.24 3.46 3.SOE-01 1.19E+OO miss 328.00 2.95 2.69E-01 l.37E+OO miss 338.3~ " 11. 27 3.BlE-01 3.92E-01 miss 409.46 1. 92 2.30E-02 2.08E+OO miss 463.00 4.40 3.02E-02 l.06E+OO miss 79-1.95 4.25 3.50E-Ol l.23E+OO miss 911. 20 25.80 l.90E-01 3.15E-01 miss 964. 77 4.99 4. llE-01 l.19E+OO miss 968. 97

• 15.80 4.28E-01 2.34E-01 miss 6/2/2016 9:22:24AM Page 8 of8 Analysis Report for 02-J un-16-10006 L3-10220C-FRGS-007SS (DRIED) Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr Ac-228 1589.20 3.22 1. OSE+OO 2.34E-01 2.46E+OO miss + Pa-231 27.36 10.30 -1.lSE+OO l.77E+(10 2. 92E+OO miss 283.69 1. 70 -2.64E-01 l.77E+OO miss 300.07 2.47 5.37E-01 1.81E+OO miss 302.65 2.20 -4.45E-02 l.79E+OO miss 330.06 1. 40 -6.60E-01 2.65E+OO miss + Th-234 92.38 2 .13 -l.24E+OO 4.13E+OO 4.13E+OO miss 92.8 0 2 .10 -7.95E-01 4.22E+OO miss 112.81 0.21 -2.79E+OO 2.63E+Ol miss + U-235 143.76 10. 96 -3.43E-02 8.32E-02 3.17E-01 miss 163.33 5.08 -1.13E-01 6.52E-01 miss 185.71

• 57.20 4.18E-02 8.32E-02 miss 202 .11 1. 08 3.54E-01 3.19E+OO miss 205.31 5.01 2.29E-01 7.21E-01 miss + Am-241 59.5 4 35.90 -2.21E-01 9.30E-01 9.30E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > MDA value not calculated

@ -Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

0000015054.CNF . *600.000 sec live r1me :500 890 sec Real rm 1: -0. l(kev) Start: 8192 i 2047. O(keOV2)09"11

• 11 2016 Stop .t rt *Thu Jun . . Acq. s a . 50 ' 1000 2000 3000 5000 5/5/2016 9:46:43AM

=Apex-G amm a Analysis Report for 05-May-16-10005 L3-10220C-FRGS-008SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy C~libration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 05-May-16-1 0005 : L3-10220C-FRGS-008SS (DRIED)

1 L 130G Soil Sample 1.514E+03 grams : Default : 5/2/2016 1 :40:00PM : 5/5/2016 9:15:31AM

130G 1 L Sand Sample : JWelch : P40818B : 130G Sand : 1800.0 seconds : 1802.9 seconds : 0.16 % : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 14850 PEAK WITH NID REPORT Peak Analysis Performed on : 5/5/2016 9:46:10AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

• C:\Canbenra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

• 1.000FWHM Page I of8 5/5/2016 9:46:43AM Page2 of8 Analysis Report for 05-May-16-10005 L3-10220C-FRGS-008SS (DRIED) Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide 1 77.02 306 -315 309.16 7.48E+Ol 37.99 2.12E+02 Pb214-XR Pb212-XR 2 87.34 344 -353 350.39 5.36E+Ol 38.20 2.29E+02 Pb214-X!\

Pb212-XR Cd-109 Eu-155 3 185.86 737 -750 744.12 4.09E+Ol 41.86 2.84E+02 U-235 Ra-226 4 238.56 94 6 -960 954.73 2.76E+02 54. 95 3.33E+02 Pb-212 5 295.19 1175 -1186 1181.11 9.20E+O l 31.19 l.20E+02 Pb-214 Eu-152 6 338.20 1347 -1358 1353.00 3.49E+O l 24.16 1.00E+02 Ac-228 7 351.84 1401 -1416 1407.56 2.05E+02 37.86 1.18E+02 Pb-214 Bi-211 8 583.04 2324 -2341 2331.92 1.16E+02 27.35 5.04E+Ol Tl-208 9 609.30 2430 -2443 2436.93 1.16E+02 25.65 4.05E+Ol Bi-214 10 661.51 2640 -2653 2645.75 4.lOE+Ol 18.82 4.0lE+Ol Cs-137 iv'4"f'I' 11 846.41 3381 -3390 3385.30 1.29E+01 12.04 2.42E+Ol bJn 56 12 911.18 3636 -3651 3644.42 5.99E+01 19.99 3.43E+01 Ac-228 13 969. 04 3869 -3883 3875.92 2.39E+O l 16.92 4.22E+Ol Ac-228 14 1460.48 5831 -5854 5842.89 4.37E+02 42.86 1.69E+Ol K-40 efl)w' M = First peak in a multiplet regio n .f-S-/1, m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield(%) Activity Activity Caine Name Confidence (keV) (pCi!grams)

Uncertainty Corr K-40 0.99 1460.82

• 10.66 5.95E+OO 7.80E-01 miss Cs-137 0.99 661.66 .. 85.10 4.lOE-02 l.95E-02 miss Tl-208 0.99 583.19

• 85.00 1.06E-01 2.82E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 2.73E-01 6.99E-02 miss 300.09 3.30 Pb212-XR 1. 00 74.82 10.28 5/5/2016 9:46:43AM Page 3 of8 Analysis Report for 05-May-16-10005 L3-10220C-FRGS-008SS (DRIED) Nuclide Id Energy Yield{%) Activity Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr Pb212-XR 1. 00 77 .11

• 17.10 5.22E-01 2.86E~Ol miss 87.35 *'* 3.97 9.77E-01 7.24E-01 miss 89.78 1. 46 Bi-214 1. 00 609.32

• 45.49 2.05E-01 5.16E-02 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155. 21 1. 63 123 8.12 5.83 1280.98 1. 43 13 77. 67 3.99 13 85. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 1 847.43 2.03 2118. 51 1.16 Pb-214 1. 00 241.99 7.25 295.22

• 18.4~ 2.46E-0 1 9.21E-0 2 mis s 351.93

• 35.60 3.17E-01 7.74E-0 2 miss 785. 96 1. 06 Ra-226 0.99 186.21

• 3.64 4.2 9 E-01 4.46E-01 m iss Ac-228 1. 00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32

• 11.27 1.66E-01 1.18E-01 miss 409.46 1. 92 463.00 4.40 794.95 4.25 911.20

• 25.80 2.45E-01 8.44E-02 miss 964. 77 4.99 968.97

• 15.80 1.66E-01 l.19E-0 1 miss 1588.20 3.22 U-235 0.99 1 43.76 10. 96 1 63.33 5.08 1 85. 71

• 57.20 2.73E-02 2.84E-02 miss 202 .11 1. 08 205.31 5.01 * = Energy line found in the spectrum.

-= Manually added nuclide. ? "' Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma Analysis Report for 05-May-16-1 0005 L3-10220C-FRGS-008SS (DRIED) Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 5/5/2016 9:46:43AM INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.993 5.95E+OO 7.BOE-01 X Cd-109 0.971 Cs-137 0.999 4.lOE-02 1.95E-02 Tl-208 0.999 1.06E-01 2.82E-02 X Bi-211 0. 964 Pb-212 1. 000 2.73E-01 6.99E-02 Pb212-XR 1. 000 5.84E-Ol 2.66E-01 Bi-214 1. 000 2.0SE-01 5.16E-02 Pb-214 1. 000 2.87E-01 5.93E-02 X Pb214-XR 1. 000 ? Ra-226 0.993 4.29E-01 4.46E-01 Ac-228 1. 000 2.05E-01 5.95E-02 ? U-235 0.999 2.73E-02 2.84E-02 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy fines not used in Weighted Mean Activity Errors quoted at 2.000sigma Page 4 of8 Comments 5/5/2016 9:46:43AM Analysis Report for 05-M ay-16-1 0005 L3-10220C-FRGS-008SS (DRIED) Peak Locate Performed on Peak Locate From Chann el Peak Locate To Channel Peak No. Energy (keV) 11 846.41 M = First peak in a multiplet region m = Other peak in a multiplet regio n F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 5/5/2016 9:46:10AM

120 : 8192 Peak CPS (%) Peak Size (CPS) Uncertainty 7.17037E-03

<:9 Peak Type S u m NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbe rra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield{%) Activity Nuc/ideMDA LineMDA Name (keV} (pCilgrams) (pCilgrams) (pCi/grams)

+ K-40 1460.82

• 10.66 5.95E+OO 2.51E-01 2.51E-01 + Cr-51 320.08 9.91 4.31E-02 1.86E-01 l.86E-Ol + Mn-54 334.85 9~.98 2.85E-03 2.13 E-02 2.13E-02 + Co-58 810.76 99.45 l.26E-04 l.90E-02 l.90E-02 1674.73 0.52 1. OOE+OO 4.20E+OO + Co-60 1173.23 99.85 4.12E-03 2.27E-02 2.27E-02 1332.49 99.98 3.49E-03 2.36E-02 + Nb-94 702.65 99.81 9.03E-03 1. 62E-02 2.04E-02 871.09 99.89 -9.55E-03 1.62E-02 + rtg-108m 79.13 6.60 -2.25E-Ol

1. 66E-02 6.BlE-01 433.94 90.50 -9.0lE-03 l.66E-02 614.28 89.80 1.30E-03 2.07E-02 722. 94 90.80 4.81E-03 2.58E-02 + Sn-113 255 .13 2 .11 -2.81E-02 2.23E-02 7.91E-01 391.70 64.97 -8.31E-03 2.23E-02 + Cs-134 475.36 1. 48 -3.68E-01 l.93E-02 1.06E+OO 563.25 8.34 2.57E-02 2.06E-Dl 569.33 15.37 l.57E-02 1.2DE-01 Page 5 of8 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss 5/5/2016 9:46:43AM Page 6 of8 Analysis Report for 05-May-16-10005 L3-10220C-FRGS-008SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCUgrams) (pCilgrams)

Corr Cs-134 604.72 97.62 -1.66E-03 1.93E-02 1. 93E-02 miss 795.86 85.46 -5.76E-03

1. 97E-02 miss 801.95 8.69 4.SOE-02 2.24E-01 miss 1038.61 0.99 l.58E-01 1.85E+OO miss 1167.97 1. 79 -2.49E-03 1.31E+OO miss 1365.19 3.02 l.lOE-01 7.28E-01 miss + Cs-137 661.66

• 85.10 4.lOE-02 2.54E-02 2.54E-02 miss + Eu-152 12 1. 78 28.67 2.33E-02 5.92E-02 7.loE-02 miss 244.70 7.61 3.48E-02 2.31E-01 miss 295. 94 0.45 -2.02E-01 6.00E+OO miss 344.28 26.60 -1.30E-02 5.92E-02 miss 367.79 0.86 -3.45E-01 l.71E+OO miss 411.12 2.24 -2.72E-01 6.0 l E-01 miss 443.96 2.83 2.13E-02 5.73E-01 miss 488.68 0.42 -l.05E+OO 2.99E+OO miss 563.99 0.49 -7.19E-Ol 3.57E+OO miss 586.26 0.46 8.97E-03 4.0lE+OO miss 678.62 0.47 -1. 96E+OO 2.75E+OO miss 688.67 0.86 -8.14E-01 1. 92E+OO miss 719.35 0.28 -9.26E-01 6.28E+OO miss 778.90 12. 96 4.25E-02 1.43E-01 miss 810.45 0.32 3.68E-01 5.50E+OO miss 867.37 4.26 3.99E-02 3.99E-01 miss 919.33 0.43 1. 48E-01 3.73E+OO miss 964.08 14.65 3.51E-02 1.87E-01 miss 1085.87 10.24 2.48E-02 2.18E-01 miss 1089.74 1. 73 -3.83E-02 1.20E+OO miss 1112.07 13.69 -2.32E-02 1.60E-01 miss 1212.95 1. 43 1.19E-Ol 1.96E+OO miss 1249.94 0.19 1. llE+OO 1.47E+Ol miss 1299.14 1. 63 2.15E-01 1.49E+OO miss 1408.01 21.07 2.85E-02 1.22E-01 miss 1457.64 0.50 -1.65E+OO 1.0lE+Ol miss 1528.10 0.28 2.03E-01 5.75E+OO miss + Eu-154 123.07 40.40 -3.43E-03 4.61E-02 4.61E-02 miss 247.93 6.89 7.73E-03 2.48E-01 miss 591.76 4.95 2.16E-02 3.58E-01 miss 692.42 1. 78 l.47E-01 1.16E+OO miss 723. 30 20.06 l.95E-03 1.17E-01 miss 756.80 4.52 -2.04E-01 4.0lE-01 miss 873.18 12.08 3.41E-02 1.65E-Ol miss 996.29 10.48 -7.88E-02 1.SlE-01 miss 1004.76 18.01 -l.37E-02 9.40E-02 miss 1274.43 34.80 7.79E-03 6.59E-02 miss 1596.48 1. 80 -2.17E-02 9.33E-01 miss + Eu-155 45.30 1. 31 -2.78E+OO l.l':E-01 l .13E+Ol miss 60.01 1. 22 6.80E-02 l.19 E+Ol miss 86.55 30.70 5.78E-02 1.29E-0 1 miss 105.31 21.10 l.90E-02 1.17E-01 miss + Tl-208 583.19

• 85.00 1.06E-Ol 2.80E-02 2.BOE-02 miss + Bi-211 351. 07

• 13.02 8.66E-01 l.83E-01 l.83E-01 miss 5/5/2016 9:46:43AM Page 7 of8 Analysis Report for Ofi..May-16-10005 L3-10220C-FRGS-008SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr + Pb-211 404.85 3.78 4.81E-02 4.39E-01 4. 39E-01 miss 427.09 1. 76 -2.73E-01 8.42E-01 miss 832.01 3.52 -2.35E-02 5.83E-01 miss + Bi-212 39.86 1. 06 -2.88E+OO 4.26E-01 1.24E+Ol miss 727.33 6.67 2.49E-01 4. 26E-01 miss 785.37 1.10 5.87E-01 1.94E+OO miss 1620.50 1. 47 2.23E-01 1.15E+OO miss + Pb-212 115.18 0.60 -5.llE-01 7.36E-02 3.53E+OO miss 238.63

• 43.60 2.73E-01 7.36E-02 miss 300.09 3.30 1.02E-Ol 5.41E-01 miss + Pb212-XR 74.82 10.28 2.05E-01 4.07E-01 6.42E-01 miss 77.11

• 17.10 5.22E-01 4.07E-01 miss 87.35

• 3.97 9. 77E-01 1. llE+OO miss 89.73 1. 46 4.83E-01 2.32E+OO miss + Bi-214 609.32 ~!-45.49 2.0SE-01 4.54E-02 4.54E-02 miss 768.36 4.89 l.35E-01 4.52E-01 miss 806.18 1. 26 3 .. 84E-01 1.64E+OO miss 934.06 3.11 1.16E-01 6.95E-01 miss 1120.29 14.92 2.18E-01 2.58E-01 miss 1155. 21 1. 63 4.68E-01 1.70E+OO miss 1238.12 5.83 3.05E-01 6.15E-01 miss 1280.98 1. 43 4.25E-01 1.91E+OO miss 1377.67 3.99 6.64E-02 5.81E-01 miss 1385.31 0.79 2.91E-01 2.64E+OO miss 1401.52 1. 33 -3.78E-01 l.14E+OO miss 1407.99 2.39 2.51E-01 l.07E+D0 miss 1509.21 2.13 1.82E-01 1. 11E+D0 miss 1661.27 1. 05 1.53E-01 l.13E+D0 miss 1729.59 2.88 3.04E-01 8.64E-D1 miss 1764.49 15.30 2.94E-01 3.14E-D1 miss 1847.43 2.03 3.63E-01 l.36E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 2.19E-01 6.71E-02 3.24E-01 miss 295.22

• 18.42 2.46E-01 1.lSE-01 miss 351.93

• 35.60 3.17E-01 6. 71E-02 miss 785.96 1. 06 3.19E-01 l.97E+OO miss + Pb214-XR 74.82 5.80 3.64E-01 7.18E-01 1.14E+D0 miss 77 .11

• 9.70 9.21E-01 7.18E-01 miss 87.35

• 2.24 1.73E+D0 1.96E+OO miss 89.78 0.82 8.60E-01 4.12E+OO miss + Ra-226 186.21

• 3.64 4.29E-01 7.18E-01 7.18E-01 miss + Ac-228 129.0 7 2.42 -8.87E-03 9.62E-02 8.00E-01 miss 209.25 3.89 6.31E-01 5.26E-01 miss 270.24 3.46 5.50E-01 6.49E-01 miss 328.00 2.95 2.85E-01 6.75E-01 miss 338.32

• 11.27 1.66E-01 1.78E-01 miss 409.46 1. 92 1.66E-01 8 .13E-01 miss 463.00 4.40 2.91E-01 4.98E-01 miss 794.95 4.25 -l.40E-02 4.55E-01 miss 911. 20

• 25.80 2.45E-01 9.62E-02 miss 964. 77 4.99 2.lOE-01 5. 71E-01 miss 5/5/2016 9:46:43AM Page 8 of 8 Analysis Report for 05-May-16-1 0005 L3-10220C-FRGS-008SS (ORI ED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCi!grams)

Corr Ac-228 968.97 .... *~ 15.80 1.66E-01 9.62E-02 1.77E-01 miss 1588.20 3.22 1.68E-01 6.79E-01 miss + Pa-231 27.36 10.30 1. 39E-01 7.23E-01 l.38E+OO miss 283.69 1. 70 2.47E-01 l.06E+OO miss 300.07 2.47 1. 36E-01 7.23E-01 miss 302.65 2.20 -6.89E-02 7.38E-01 miss 330.06 1. 40 -4.19E-02 l.28E+OO miss + Th-234 92.38 2.13 6. 96E-Ol 1. 72E+OO 1.72E+OO miss 92. 80 2.10 1. 4 7E+OO 1.BOE+OO miss 112. 31 0 .21 2.61E-01 l.07E+Ol miss + U-235 143.76 10. 96 -2.75E-03 4.57E-02 1. 67E-01 miss 163.33 5.08 2.00E-02 3.38E-01 miss 185.71

• 57.20 2.73E-02 4.57E-02 miss 202 .11 1. 08 -9.41E-01 1.22E+OO miss 205.31 5.01 4.22E-02 3.lOE-01 miss + Am-241 59.54 35.90 9.45E-02 4.28E-01 4.28E-Ol miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Vl +-' C :::I 120 110 100 90 80 70 8 60 50 40 30 20 10 1000 2000 3000 0000014850.CNF 4000 channel 5000 Live Time :1800.000 sec Real Time :1802. 870 sec start: 1: -0.l(kev) stop : 8192: 2047. O(kev) Acq. Start : Thu May OS 09: 1S: 31 2016 6000 7000 8000 5/5/2016 10:26:03AM Analysis Report for 05-May-16-10007 L3-10220C-FRGS-009SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification

• Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done O n Efficiency Calibration Description Sample Number : 05-May-16-10007

L3-10220C-FRGS-009SS (DRIED) : 1 L 130G Soil Sample 1.325E+03 grams : Default : 5/2/2016 2:00:00PM

5/5/2016 9:55:00AM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 1800.0 seconds : 1801.2 seconds : 0.07 % : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

6/28/2012

14852 PEAK WITH N/0 REPORT Peak Analysis Performed on : 5/5/2016 10:25:31AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 5/5/2016 10:26:03AM Page2 of8 Analysis Report for 05-May-16-10007 L3-10220C-FRGS-009SS (DRIED) Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide M 1 74.77 294 -315 300.33 5.54E+Ol 21.97 2.14E+02 Pb214-XR Pb212-XR m 2 77.04 294 -315 30~.40 9.76E+Ol 27.15 2.40E+02 Pb214-XR Pb212-XR 3 238.62 947 -960 954.79 2.77E+02 49.15 2.38E+02 Pb-212 4 295.10 1174 -1188 1180.45 8.67E+Ol 34. 92 1.51E+02 Pb-214 Eu-152 5 338.36 1346 -1361 1353.30 5.50E+Ol 26.88 9.60E+Ol Ac-228 6 351.95 1399 -1416 1407.59 2.02E+02 37.81 1.09E+02 Pb-214 Bi-2 11 7 510.56 2033 -2047 2041.45 3.24E+O l 24.45 8.73E+Ol ...... ,1µJ1-s-l

• 8 583.06 2325 -2337 2331.22 7.24E+O l 21::. 32 6.51E+Ol Tl-208 9 609.16 2428 -2444 2435.56 l.48E+02 28.34 3.92E+Ol Bi-'214 10 661.47 2638 -2655 2644.69 3.06E+02 39.44 6.15E+Ol Cs-137 11 727.18 2902 -2912 2907.42 2.36E+Ol 15.38 3.69E+Ol Bi-212 12 860.46 3435 -3445 3440.39 1.85E+O l 10.7 8 1.lOE+Ol ..... 17-.:.~¥ 13 911. 06 3634 -3650 3642.76 6.41E+Ol 18.79 1.98E+Ol Ac-228 14 968. 97 3867 -3882 3874.38 3.88E+Ol 17.57 3.24E+Ol Ac-228 15 1460.78 5832 -5853 5842.45 3.91E+02 41.36 2.85E+Ol K-40 16 1764.50 7052 -7066 7058.67 3.20E+O l 11.68 2.09E+OO Bi-214 ef"IJJ M = First peak in a multiplet region m = Other peak in a multiplet region $'-f-'1'4 F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield{°.!o)

Activity Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 1. 00 1 460.82

• 10.66 5.43E+OO 7.44E-01 miss Cs-137 0.99 661.66

• 85.10 3.12E-01 5.49E-02 miss Tl-208 0.99 583.19

• 85.00 6.77E-02 2.41E-02 miss Bi-212 0.99 39.86 1. 06 727.33

• 6.67 3.26E-01 2.16E-01 miss 785.37 1.10 1620.50 1. 47 Pb-212 1. 00 115 .18 0.60 5/5/2016 10:26:03AM Page 3 of8 Analysis Report for 05-May-16-10007 L3-10220C-FRGS-009SS (DRIED) Nuclide Id Energy Yield{%) Activity Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr Pb-212 1. 00 238.63

• 43.60 2.73E-01 6.55E-02 miss 300.09 3.30 Pb212-XR 1. 00 74.82

• 10.28 4.54E-01 2.03E-01 miss 77 .11

• 17.10 4.42E-01 1.53E-01 miss 87.35 3.97 89.78 1. 46 Bi-214 0.79 609.32

• 45.49 2.67E-01 6.03E-02 miss 768.36 4.89 806.18 1. 26 934.06 3 .11 1 120.29 14.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1661.27 1. 05 1 729.59 2.88 1 764.49

• 1 5.30 3.58E-01 1. 34E-01 m iss 1 847.43 2.03 2118. 51 1.16 Pb-214 1. 00 241.99 7.25 295.22

• 18.42 2.33E-01 1.0lE-01 miss 3 5 1.93

• 35.60 3.16E-01 7.79E-02 miss 785. 96 1. 06 Ac-228 1. 00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32

• 11. 27 2.65E-01 l.36E-01 mi ss 409.46 1. 92 463.00 4.40 794.95 4.25 911. 20

• 25.80 2.67E-01 8.17E-02 miss 964. 77 4.99 968.97

• 15.80 2.75E-01 l.27E-01 miss 1 588.20 3.22 * = Energy line found in the spectrum. = Manually added nuclide. ? = Manually edited nuclide. @ = Energy fine not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold=

0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

5/5/2016 10:26:03AM Page4 of8 Analysis Report for 05-May-16-10007 L3-10220C-FRGS-009SS (DRIED} INTERFERENCE CORRECTED REPORT Nuclide Name Nuclide Id Confidence Wt mean Activity (pCilgrams)

Wt mean Comments X X ? = X = K-40 Cs-13 7 Tl-208 Bi-211 Bi-212 Pb-212 Pb212-XR Bi-214 Pb-214 Pb214-XR Ac-228 1.000 0.998 0.999 0.954 0.999 1.000 1.000 0.798 1.000 1. 000 1.000 nuclide is part of an undetermined solution nuclide rejected by the interference analysis Activity Uncertainty

5. 43E+OO .. ,.---....t:ML

7. 44E-01 3.12E-Ol~'T 5.49E-02 6.77E-02 i/t3/lv,2.41E-02 3.26E-01 2.73E-01 4.46E-01 2.82E-01 2.85E-01 2.69E-01 2.16E-01 6.55E-02 1.22E-01 5.SOE-02 6.17E-02 6.14E-02 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 5/5/2016 10:26:03AM Analysis Report for 05-May-16-1 0007 L3-10220C-FRGS-009SS (DRIED) Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. 7 12 Energy (keV) 510.56 860.46 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 5/5/2016 10:25:31AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 1.79854E-02 1.02778E-02 37.76 29.13 Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Can berra\Apex\Root\Default\Li brary\Z I ON LI 8-BN L. NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

+ K-40 1460.82

• 10.66 5.43E+OO 3.15E-01 3.15E-Ol + Cr-51 320.08 9.91 2.03E-02 1.73E-01 l.73E-01 + Mn-54 834.85 99.98 6.45E-03 l.98E-02 1.98E-02 + Co-58 810.76 99.45 -1. 71E-04 1.71E-02 1.71E-02 1674.73 0.52 4.09E-02 2.41E+OO + Co-60 1173.23 99.85 -3.52E-04 2.08E-02 2.64E-02 1332.49 99.98 7.91E-04 2.0BE-02 + Nb-94 702.65 99.81 9.84E-04 1.8"7E-02 1. 87E-02 871.09 99.89 4.59E-03 2.lOE-02 + Ag-108m 79.13 6.60 2 .13E-01 l.44E-02 4.83E-01 433.94 90.50 -9.64E-03

1. 44E-02 614.28 89.80 -1.23E-03 1.79E-02 722. 94 90.80 -l.73E-03 1.97E-02 + Sn-113 255.13 2 .11 1.35E-01 2.45E-02 7.71E-01 391. 70 64.97 5.51E-03 2.45E-02 + Cs-134 475.36 1. 48 1. 96E-01 1.97E-02 1. 24E+OO Page 5 of8 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss 5/5/2016 10:26:03AM Page 6 of8 Analysis Report for 05-May-16-10007 L3-10220C-FRGS-009SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Cs-134 563.25 8.34 -3.29E-02

1. 97E-02 1.76E-01 miss 569.33 15.37 -2.26E-02 9.24E-02 miss 604. 72 97. 62 2.45E-03 1. 97E-02 miss 795.86 85.46 6.68E-03 2.~8E-02 miss 801.95 8.69 -6.16E-02

..1. 98E-01 miss 1038.61 0.99 2.26E-01 1.79E+OO miss 1167.97 1. 79 1.70E-Ol l.24E+OO miss 1365.19 3.02 1.00E-01 6.60E-01 miss + Cs-137 661.66

• 85.10 3.12E-01 3.32E-02 3.32E-02 miss + Eu-152 121.78 28.67 7.lOE-03 5.39E-02 5.39E-02 miss 244.70 7.61 -2.56E-02 l.84E-01 miss 295.94 0.45 4.85E+OO 5.65E+OO miss 344.28 26.60 -7.05E-04 5.90E-02 miss 367.79 0.86 4.78E-Ol l.70E+OO miss 4 1 1.12 2.24 -3.18E-01 6.40E-01 miss 443. 36 2.83 -7.68E-02 5.34E-Ol miss 488.68 0.42 9.89E-02 4.19E+OO miss 563.99 0.49 -5.84E-02 3.0BE+OO miss 586.26 0.46 -8.87E-01 4.34E+OO miss 678.62 0.47 5.89E-01 3.87E+OO miss 688.67 0.86 l. llE-01 l.80E+OO miss 719.35 0.28 l.6~E+OO 6.61E+OO miss 778.90 12.96 -2.44E-02 l.24E-Ol miss 810.45 0.32 -4.04E+OO 3.33E+OO miss 867.37 4.26 -9.35E-02 4.06E-01 miss 919.33 0.43 1.13E+OO 4.59E+OO miss 964.08 14.65 3.82E-02 1.67E-01 miss 1085.87 10.24 -2.89E-03

1. 77E-01 miss 1089.74 1. 73 5.27E-01 1.36E+OO miss 1112. 07 13.69 -3.17E-02 l.63E-01 miss 1212. 95 1. 43 -7.32E-01 l.45E+OO miss 1249.94 0.19 -2.22E+OO 1.17E+Ol miss 1299.14 1. 63 -4.90E-01 1.00E+OO miss 1408.01 21. 07 4.89E-02 l.14E-Ol miss 1457.64 0.50 -6.94E+OO

6. lOE+OO miss 1528.10 0.28 -9.33E-01 5.06E+OO miss + Eu-154 123.07 40.40 5.64E-04 3.64E-02 3.64E-02 miss 247.93 6.89 l.02E-01 2.48E-01 miss 591. 76 4.95 -8.92E-03 3.46E-Ol miss 692.42 1. 78 1.93E-01 9.12E-01 miss 723.30 20.06 9.60E-03 9.78E-02 miss 756.80 4.52 4.65E-02 4.22E-01 miss 873.18 12.08 -6.72E-03 1.63E-01 miss 996.29 10.48 -7.45E-02 1.43E-01 miss 1004.76 18.01 -1.46E-03 1.0lE-01 miss 1274.43 34.80 -1.45E-03 7.00E-02 miss 1596.48 1. 80 -5.52E-02 6.50E-01 miss + Eu-155 45.30 1. 31 -1.45E+OO 8.02E-02 4.17E+OO miss 60.01 1. 22 7.98E-01 5.56E+OO miss 86.55 30.70 1.26E-02 9.47E-02 miss 105.31 21.10 1. 05E-02 8.02E-02 miss 5/5/2016 10:26:03AM Page 7 of8 Analysis Report for 05-May-16-10007 L3-10220C-FRGS-009SS

{DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr + Tl-208 583.19

• 85.00 6. 77E-02 2.92E-02 2. 92E-02 miss + Bi-211 351. 07

• 13. 02 8.65E-01 1.87E-01 1.87E-01 miss + Pb-211 404.85 3.78 -2.51E-02 3.92E-01 3.92E-01 miss 427.09 1. 76 1.19E-01 8.73E-01 miss 832.01 3.52 -1.15E-01 4.31E-01 miss + Bi-212 39.86 1. 06 6. 96E-02 3.09E-01 5.28E+OO miss 727.33

• 6.67 3.26E-01 3.09 E-01 miss 785.37 1.10 4.54E-Ol 1.83E+OO miss 1620.50 1. 47 4.lOE-02 1.0lE+OO miss + Pb-212 115 .18 0.60 6.25 E-Ol 6.12E-02 2.65E+OO miss 238.63

• 43.60 2.73E-01 6.12E-02 miss 300.09 3.30 2. 96E-01 5.50E-01 miss + Pb212-XR 74.82

• 10.28 4.54E-01 2.43E-01 4.17E-01 miss 77 .11

• 17.10 4.42E-01 2.43E-01 miss 87.35 3.97 9.22E-Ol 7.90E-01 miss 89.78 1. 46 8.00E-01 1.81E+OO miss + Bi-214 609.32

• 45.49 2.67E-01 4.77E-02 4.77E-02 miss 768.36 4.89 3. 72E-01 5.51E-01 miss 806.18 1. 26 -8.74E-01 l.17E+OO miss 934.06 3.11 4.89E-02 4.97E-01 miss 1120.29 14.92 1.34E-01 2.22E-01 miss 1155. 21 1. 63 4.40E-01 1.60E+OO miss 1238.12 5.83 1.89E-01 5.31E-01 miss 1280.98 1. 43 5.72E-01 1.77E+OO miss 1377.67 3.99 3.0lE-01 7.37E-01 miss 1385.31 0.79 6.45E-01 2.53E+OO miss 1401.52 1. 33 4.63E-02 1. 52E+OO miss 1407.99 2.39 4.30E-01 1.00E+OO miss 1509.21 2.13 3.77E-01 1.19E+OO miss 1661.27 1. 05 -2.15E-01 1.45E+OO miss 1729.59 2.88 6.39E-01 1.14E+OO miss 1764.49

• 15.30 3.58E-01 8.47E-02 miss 1847.43 2.03 3.49E-01 1.05E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 1.83E-01 6.83E-02 2.73E-01 miss 295.22

• 18.42 2.33E-Ol 1.38E-01 miss 351.93

• 35.60 3.16E-01 6.83E-02 miss 785.96 1. 06 8.69E-01 1.95E+OO miss + Pb214-XR 74.82

• 5.80 8.04E-01 4.29E-01 7.39E-01 miss 77 .11

• 9.70 7.79E-01 4.29E-01 miss 87.35 2.24 1.63E+OO 1.40E+OO miss 89.78 0.82 1.42E+OO 3.22E+OO miss + Ra-226 186.21 3. 64 5.69E-01 5.44E-01 5.44E-01 miss + Ac-228 129.07 2.42 7.97E-02 7.88E-02 6.93E-01 miss 209.25 3.89 2.19E-01 4.29E-01 miss 270.24 3.46 3.18E-01 5.69E-01 miss 328.00 2.95 2.48E-01 5.98E-01 miss 338.32

• 11.27 2.65E-01 l.90E-01 miss 409.46 1. 92 1.94E-01 8.55E-01 miss 463.00 4.40 2.17E-01 4.53E-01 miss 5/5/2016 10:26:03AM Page 8 of8 Analysis Report for 05-May-16-10007 L3-10220C-FRGS-009SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

Corr Ac-228 ?94.95 4.25 1. 42E-01 7.88E-02 5.04E-01 miss 911. 20

• 25.80 2.67E-01 7. 88E-02 miss 964. 77 4.99 1.72E-01 5.03E-01 miss 968.97

• 15.80 2.75E-01 1. 64E-01 miss 1588.20 3 .22 3.44E-01 8.18E-01 miss + Pa-231 27.36 10.30 O.OOE+OO 4.63E-02 4. 63E-02 miss 283.69 1. 70 -2.53E-01 8.23E-01 miss 300.07 2.47 3.96E-01 7.35E-01 miss 302.65 2.20 -2.47E-01

5. 72E-01 miss 330.06 1. 40 -2.54E-02 1.02E+OO miss + Th-234 92.38 2.13 8.68E-01 1.32E+OO 1.32E+OO miss 92.80 2.10 1.31E+OO 1.35E+OO miss 112. 81 o.~1 -1.29E+OO 8.26E+OO miss + U-235 143.76 10. 96 3.78E-02 3.37E-02 1.32E-01 miss 163.33 5.08 1.94E-01 2. 94E-01 miss 185.71 57.20 2.99E-02 3.37E-02 miss 202 .11 1. 08 9.03E-02 l.21E+OO miss 205.31 5.01 l.07E-02 2. 66E-01 miss + Am-241 59.54 35.90 -3.75E-02 1.90E-01 1. 90E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

120 110 100 90 80 70 Ill ..... C: :::I 0 u so 40 -"" 1 30 -..,. ..... 20 -t\~V 1 10 \ 0 1000 ...... = ,' "' u ..... = co :;;: I 'i= *~f.1~, 2000 0000014852.CNF ";' co .J1i.~J,Ji~, '*V l~ 1~'1.\tJ\, l\ 3000 4000 channel 5000 Live Time :1800.000 sec Real Ti me : 1801.240 sec start: 1: -0.2(kev) stop : 8192: 2047. 4(kev) Acq. Start :Thu May 05 09: 55 :00 2016 6000 7000 8000 5/5/2016 11 :09:23AM Analysis Report for 05-May-16-10008 L3-10220C-FRGS-010SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done O n Efficiency Calibration Description Sample Number : 05-May-16-1 0008 : L3-10220C-FRGS-01 OSS (DRIED) : 1 L 130G Soil Sample 9.600E+02 grams : Default : 5/2/2016 1:20:00PM

5/5/2016 10:38:42AM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 1800.0 seconds : 1801.3 seconds : 0.07% : 2.80 : 120-8192 :120-8192

1.000FWHM

1/27/2016

6/28/2012

14853 .. PEAK WITH NID REPORT Peak Analysis Performed on : 5/5/2016 11 :08:50AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB 1.00 0FWHM IC) ~1;. f{___V \..,.LJ'{\J.l L-s-:-s-=-'t,o Page 1 of8 5/5/2016 11:09:23AM Page2 of8 Arialysis Report for 05-May-16-10008 L3-10220C-FRGS-010SS (DRIED) Peak Energy ROI ROI Peak NetPeak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide M 1 74.75 295 -315 300.25 5.48E+Ol 2 1.17 1.91E+02 Pb214-XR Pb212-XR m 2 77.08 295 -315 309.53 1.10E+02 26.34 1.77E+02 Pb214-XR Pb212-XR 3 186.08 737 -748 744.92 3.31E+O l 29.14 1.42E+02 Ra-226 U-235 M 4 238.66 951 -972 954.97 2.00E+02 31.10 1.01E+02 Pb-212 m 5 241.79 951 -972 967. 48 4.99E+Ol 18.79 l.29E+02 Pb-2 14 6 295.17 1177 -1187 1180. 72 6.45E+Ol 23.66 6.31E+Ol Pb-214 Eu-152 7 338.29 1346 -1357 1353.02 4.60E+01 2 1.38 6. 21E+Ol Ac-228 8 351.88 1399 -1414 1407.31 1. 4 9E+02 31.01 7.04E+Ol Pb-214 Bi-211 9 510.33 2034 -2045 2040.51 3.36E+O l 22.58 8.28E+Ol ..... l,/p-$1, 10 583.07 2324 -2338 2331.30 6.0lE+O l 20.80 3.77E+Ol Tl-208 11 609.19 2429 -2442 2435.68 1. 25E+02 26.29 3.94E+Ol Bi-214 12 6Sl.60 2640 -2653 2645.20 2.08E+02 31. 91 4.26E+Ol Cs-137 13 911. 34 3636 -3650 3643.87 4.65E+01 17.28 2.50E+Ol Ac-228 14 1460.89 5832 -5853 5842.90 3.02E+02 35.64 1.23E+Ol K-40 ~J M = First peak in a multiplet region f,S'lt, m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield{%) Activity Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 1. 00 1460.82

• 10.66 5.79E+OO 8.49E-01 miss Cs-137 1. 00 661.66 .... 85.10 2.92E-01 5.69E-02 miss Tl-208 0.99 583.19 *'* 85.00 7.76E-02 2.84E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 2.72E-01 6.lOE-02 miss 300.09 3.30 Bi-214 0.79 609.32

• 45.49 3. llE-01 7.52E-02 miss 768.36 4.89 806.18 1.26 5/5/2016 11:09:23AM Page 3 of8 Analysis Report for 05-May-16-10008 L3-10220C-FRGS-01 OSS (DRIED) Nuclide Id Energy Yield(%) Activity Activity Caine Name Confidence

{keV) (pCilgrams)

Uncertainty Corr Bi-214 0.79 934.06 3.11 1120.29 14.92 11 55.2! 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1 661.27 1. 05 1 729.59 2.88 1764.49 15.30 1847.43 2.03 2118. 51 1.16 Pb-214 1. 00 241.99

• 7.25 4.12E-01 1. 68E-01 miss 295.22

• 18.42 2.39E-01 9.57E-02 miss 351.93

• 35.60 3.21E-01 8.44E-02 miss 785. 96 1. 06 Pb214-XR 1. 00 74.82

• 5.80 1.lOE+OO 4.91E-01 miss 77 .11

• 9.70 l.21E+OO 3.98E-01 miss 87.35 2.24 89.78 0.82 Ra-226 0.99 186.21

• 3.64 4.73E-01 4.22E-01 miss Ac-228 0.74 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 .. 11.27 3.0SE-01 1. SOE-01 miss 409.46 1. 9~ 463.00 4.40 794.95 4.25 911. 20

• 25.80 2.68E-01 l.02E-01 miss 964. 77 4.99 968. 97 15.80 1 588.20 3.22 U-235 0.99 143.76 10.96 163.33 5.08 185.71

• 57.20 3.0lE-02 2.69E-02 miss 202 .11 1. 08 205.31 5.01 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold=

0.30 Errors quoted at 2.000sigma Analysis Report for 05-May-16-10008 L3-10220C-FRGS-010SS (DRIED) Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 5/5/2016 *11 :09:23AM INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1.000 5.79E+OO 8.49E-01 Cs-137 1.000 2.92E-01 5.69E-02 Tl-208 0.999 7.76E-02 2.84E-02 X Bi-211 0.960 Pb-212 1.000 2.72E-01 6.lOE-02 " Pb212-XR 1.000 ,~ Bi-214 0.798 3. llE-01 7.52E-02 Pb-214 1. 000 3.0lE-01 5.93E-02 Pb214-XR 1. 000 1.l?E+OO 3.09E-01 ? Ra-226 0.999 4.73E-Ol 4.22E-01 Ac-228 0.745 2.79E-01 8.45E-02 ? U-235 0.994 3.0lE-02 2.69E-02 ? ; nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Page 4 of8 Comments 5/5/2016 11 :09:23AM Page 5 of8 Analysis Re.port for 05-May-16-10008

+ + + + + + + + + L3-10220C-FRGS-010SS (DRIED) Peak Locate Performed on Peak Locate From Channe l Peak Locate To Channel Peak No. Energy (keV) 9 510.33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 5/5/2016 11 :08:50AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty l.86800E-02 33.58 NUCLIDE MDA REPORT Nuclide Library Used : C :\Can berra\Apex\Root\Default\Li brary\ZI ON LI B-BN L. NLB Nuclide Energy Yield(%) Activity NuclideMDA Name (keV} (pCilgrams) (pCilgrams)

K-40 1460.82

• 10.66 5.79E+OO 3.02E-01 Cr-51 320.08 9.91 -5.44E-03

1. 96E-01 Mn-54 834.85 99.98 -5.66E-03

2. llE-02 Co-58 810.76 99.45 6.06E-03 2.36E-02 1674.73 0.52 -2.82E-01 Co-60 1173.23 99.85 -1.17E-02

2. llE-02 1332.49 99.98 5.46E-04 Nb-94 702.65 99.81 3.32E-03 2.26E-02 871.09 99.89 6.48E-03 Ag-108m 79.13 6.60 -1.lBE-01 2.0lE-02 433.)4 90.50 -9.86E-04 614.28 89.80 -1.0lE-02 722. 94 90.80 -2.33E-04 Sn-113 255.13 2 .11 7.29E-02 3.26E-02 391.70 64.97 -7. 72E-03 Cs-134 475.36 1. 48 -1.03E+OO 2.65E-02 563.25 8.34 6.67E-02 569.33 15.37 -9.14E-03 Peak Type LineMDA (pCi/grams) 3.02E-01 1. 96E-01 2. llE-02 2.36E-02 3.32E+OO 2. llE-02 2.29E-02 2.26E-02 2.51E-0'.2 4.94E-01 2.04E-02 2.0lE-02 2.33E-02 9. 71E-01 3.26E-02 1.30E+OO 2.42E-01 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss 1.41E-01 miss 5/5/2016 11:09:23AM Page 6 of8 Analysis Report for 05-May-16-10008 L3-10220C-FRGS-O 1 OS S {DRIED) Nuclide r=narn11 Yield(%) A ... ,,.,;,.., Nuclide r,,fDA LineMDA r-:---**-*~:, .........

,, ""'""' Name (keV} (pCilgrams) (pCilgrams) (pCilgrams)

Corr Cs-134 604.72 97.62 3.12E-03 2.6~E-02 2. 65E-02 miss 795.36 85.46 1. 48E-02 3.38E-02 miss 801.95 8.69 -6.39E-02 2.36E-01 miss 1038.61 0.99 1. 24E+OO 3.09E+OO miss 1167. 97 1. 79 -2.80E-Ol

1. 63E+OO miss 1365.19 3.02 -3.23E-02 6.00E-01 miss + Cs-137 661.66

• 85 .10 2. 92E-01 3.54E-02 3.54E-02 miss + Eu-152 121.78 28.67 1.69E-02 6.23E-02 6.48E-02 miss 244.70 7.61 1.27E-01 2.82E-01 miss 295.94 0.45 8.27E+OO 6.97E+OO miss 344.23 26.60 -1.95E-02 6.23E-02 miss 367.79 0.86 -3.44E-01 2.21E+OO miss 411.12 2.24 5.48E-02 9.62E-01 miss 443. 96 2.83 -3.14E-01 5.58E-01 miss 488.68 0.42 9.64E-Ol 5.05E+OO miss 563.99 0.49 -6.82E-01 3.46E+OO miss 586.26 0.46 -2.64E+OO 3.80E+OO miss 678.62 0.47 -7.73E-01 4.09E+OO miss 688.67 0.86 -1. 96E-01 2.38E+OO miss 7 19.35 0.28 O.OOE+OO 8.22E+OO miss 778.90 12.96 3.65E-02 l.87E-01 miss 810.45 0.32 l.23E+OO 6.77E+OO miss 867.37 4.26 -l.12E-02 5.05E-01 miss 919.33 0.43 -l.57E+OO 4.92E+OO miss 964.08 14.65 6.SOE-02 2.31E-01 miss 1085.87 10.~4 2.33E-02 2.58E-01 miss 1089.74 1. 73 -3.04E-Ol l.53E+OO miss 1112. 07 13. 69 -4.60E-02 l.33E-Ol miss 1212.95 1. 43 -4.49E-01 l.77E+OO miss 1249.94 0.19 -2.lOE+OO l.27E+Ol miss 1299.14 1. 63 -8.25E-02 1.39E+OO miss 1408.01 21.07 1.33E-02 1.33E-01 miss 1457.64 0.50 -1.06E+Ol 8.66E+OO miss 1528.10 0.28 2.20E+OO 9.03E+OO miss + Eu-154 123.07 40.40 5.72E-03 4.45E-02 4.45E-02 miss 247.93 6.89 -l.38E-01 2.08E-01 miss 591.76 4.95 -l.69E-02 4.90E-01 miss 692.42 1. 78 l.85E-Ol 1.21E+OO miss 723.30 20.06 -1.34E-02 9.50E-02 miss 756.80 4.52 l.18E-01 5.82 E-01 miss 873.18 12.08 -5.52E-02 1.89E-01 miss 996.29 10.48 2.89E-02 2.12E-01 miss 1004.76 18.01 3.82E-02 1.32E-01 miss 1274.43 34.80 2.81E-02 8.87E-02 miss 1596.48 1. 80 -7.93E-02 1.60E+OO miss + Eu-155 45.30 1. 31 -2.17E+OO l.12E-01 4.65E+OO miss 60.01 1. 22 -5.26E-01 6.32E+OO miss 86.55 30.70 3.00E-03 l.14E-Ol miss 105.31 21.10 2.33E-02 l.12E-Ol miss + Tl-208 583.19

• 85.00 7.76E-02 3.29E-02 3.29E-02 miss + Bi-211 351.07

• 13.02 8.78E-01 2.02E-01 2.02E-01 miss 5/5/2016 11 :09:23AM Page 7 of8 Analysis Report for 05-May-16-10008 L3-10220C-FRGS-010SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCUgrams) (pC/lgrams) (pCi!grams)

Corr + Pb-211 404.85 3.78 9.00E-03 5.52E-01 5. 52E-01 miss 427.09 1. 76 2.00E-01 1.20E+OO miss 832.01 3.52 7.13E-02 6.90E-Ol miss + Bi-212 39.86 1. 06 3.54E+OO 4.68E-01 7.28E+OO miss 727.33 6.67 2.80E-01 4.68E-01 miss 785.37 1.10 6.90E-01 2.37E+OO miss 1620.50 1. 4 7 -3.02E-01 1.40E+OO miss + Pb-212 115 .18 0.60 l.52E+OO 4.86E-02 3.45E+O(l miss 238.63

• 43.60 2.72E-01 4.86E-02 miss 300.09 3.30 3.20E-01 6.95E-01 miss + Pb212-XR 74.82

• 10. 28 6.20E-01 2.90E-01 5.45E-01 miss 77.11

• 17.10 6.88E-01 2. 90E-01 miss 87.35 3.97 6.68E-01 8. 96E-01 miss 89. 78 1. 46 1.lSE+OO 2.03E+OO miss + Bi-214 609.32 .,, 45.49 3. llE-01 6.30E-02 6.30E-02 miss 768.36 4.89 -3.BOE-02 5.76E-01 miss 806.18 1. 26 -7.38E-01 1.42E+OO miss 934.06 3.11 1. 22E-01 8.lOE-01 miss 1120.29 14.92 1.68E-01 2.96E-Ol miss 1155. 21 1. 63 4.63E-01 2.07E+OO miss 1238.12 5.83 3.35E-01 7.79E-01 miss 1280.98 1. 43 -l.16E-01 1.56E+OO miss 1377. 67 3.99 4.91E-01 9.87E-01 miss 1385.31 0.79 -6.81E-01 2.98E+OO miss 1401.52 1. 33 1.70E-01 1.60E+OO miss 1407.99 2.39 1.17E-01 l.17E+OO miss 1509.21 2 .13 1.62E-01 1.18E+OO miss 16 6 1.27 1. 05 1.35E-01 2.32E+OO miss 1729.59 2.88 1.32E-Ol 1.06E+OO miss 1764.49 15.30 2.80E-01 3.64E-01 miss 1847.43 2.03 4.06E-01 1.70E+OO miss > 2118.51 1.16 O.OOE+OO 0.00E+OO miss + Pb-214 241.99

• 7.25 4.12E-01 7.38E-02 3.31E-Ol miss 295.22

• 18.42 2.39E-01 l.16E-01 miss 351.93

• 35.60 3.21E-01 7.38E-02 miss 785.96 1. 06 4.59E-01 2.38E+OO miss + Pb214-XR 74.82 *'* 5.80 1.lOE+OO 5.12E-01 9.66E-01 miss 77.11

• 9.70 1.21E+OO 5.12E-Ol miss 87.35 2.24 1.18E+OO 1.59E+OO miss 89. 78 0.82 2.05E+OO 3.61E+OO miss + Ra-226 186.21

• 3.64 -l.73E-01 6.66E-Ol 6.66E-01 miss + Ac-228 129.07 2.42 l.OSE-01 l.16E-01 8.llE-01 miss ~09.25 3.89 4.09E-01 5.79E-01 miss 270.24 3.46 4.64E-D1 7.16E-01 miss 328.00 2.95 4.78E-01 8.08E-01 miss 338.32

• 11. 27 3.0SE-01 1.99E-01 miss 409.46 1. 92 -9.52E-02 1.00E+OO miss 463.00 4.40 8.91E-02 5.80E-01 miss 794.95 4.25 2.00E-01 6.78E-01 miss 911. 20

• 25.80 2.68E-01 1.16E-01 miss 964. 77 4.99 2.0lE-01 7.27E-01 miss 5/5/2016 11:09:23AM Page 8 of 8 Analysis Report for 05-May-16-10008 L3-10220C-FRGS-010SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCi!grams)

Corr Ac-228 968. 97 15.80 2.74E-01 1.16E-01 2. 96E-01 miss 1588.20 3.22 2.lSE-01 B.14E-01 miss + Pa-231 27.36 10.30 O.OOE+OO 6.39E-02 6.39E-02 miss 283.69 1. 70 5.87E-02 l.15E+OO miss 300.07 2.47 4.28E-01 9.29E-01 miss 302.65 2.20 -2.78E-01 8.20E-01 miss 330.06 1. 40 -8.74E-01 1.02E+OO miss + Th-234 92.38 2 .13 l.41E+OO 1. 73E+OO 1.73E+OO miss 92.80 2 .10 1. 81E+OO l.78E+OO miss 112. 81 0 .21 -l.60E+OO 9.03E+OO miss + U-235 143.76 10. 96 4.61E-02 4.24E-D2 l.62E-01 miss 163.33 5.08 -3.59E-02

2. 99E-01 miss 185.71

• 57.20 3.0lE-02 4.24E-02 miss 202 .11 1. 08 -6.56E-01 1.SOE+OO miss 205.31 5.01 -8.84E-02 3.0BE-01 miss + Am-241 59.54 35.90 1. 06E-Ol 2.47E-01 2.47E-01 miss + Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? ;;; CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not f ound in the coincidence library.

...... -...... ' ..c, 60 c.. 55 50 45--40 "" '>f' 35 V) ..... C: ::::J 8 30 = ...... 25 ' :::, "' "" 20 15 10 5 0 -1000 *..; .... 9 .s::, c.. co 00 ...... 'i= ...... ' !;£ 2000 ::;:; 3000 0000014853.CNF 4000 channel 5000 Live Time :1800.000 sec Real Time :1801.270 sec Start: 1: -0 .2 (kev) stop : 8192: 2047 .4(kev) Acq. Start : Thu May OS 10: 38: 42 2016 6000 7000 8000 5/5/2016 12:35:30PM Analysis Report for 05-May-16-10011 L3-10220C-FRGS-011 SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 05-May-16-10011

L3-10220C-FRGS-011SS (DRIED)

1 L 130G Soil Sample 1.303E+03 grams : Default : 5/2/2016 1 :05:00PM : 5/5/2016 12:04:43PM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 1800.0 seconds : 1801.3 seconds : 0.07% : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

6/28/2012

14856 PEAK WITH NJD REPORT Peak Analysis Performed on : 5/5/2016 12:34:53PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of 8 5/5/2016 12:35:30PM Page 2 of8 Analysis Report for 05-May-16-10011 L3-10220C-FRGS-O 11 SS (DRIED) Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide M 1 74.69 294 -315 300.00 7.70E+Ol 24. 91 2.62E+02 Pb214-XR Pb212-XP, m 2 76.89 294 -315 308. 77 l.01E+02 27.48 2.50E+02 Pb214-XR Pb212-XR 3 109.37 435 -442 438.52 2.03E+O l 22.30 8.75E+Ol ..... 1,t fF 4 185. 96 739 -752 744.44 7.58E+O l 37.04 1.92E+02 U-235 Ra-226 5 209.30 832 -844 837.68 3.88E+Ol 31.87 1.63E+02 Ac-228 M 6 238.66 948 -976 954.95 2.89E+02 36.72 1.70E+02 Pb-'212 m 7 241.93 948 -976 968. 04 5.93E+O l 18. 94 l.14E+02 Pb-214 8 295.20 1175 -1186 1180.86 5.94E+O l 29.23 1.23E+O~ Pb-2 1 4 Eu-152 9 338.26 1347 -1360 1352. 90 4.0lE+O l 25.71 l.04E+02 Ac-228 10 351.95 1400 -1414 1407.60 2.07E+02 36.99 l.08E+02 Pb-214 Bi-211 11 583.17 2323 -2340 2331.69 1. 22E+02 27.76 5.05E+Ol Tl-208 12 609.17 2429 -2443 2435.62 l.39E+02 27. 64 4.12E+Ol B i-214 13 661.60 2637 -2654 2645.22 1. 59E+02 29.92 5.12E+Ol Cs-13'7 14 911. 28 3635 -3650 3643.63 5.61E+Ol 17.56 1.78E+Ol Ac-228 15 968. 88 3868 -3882 3873.99 4.41E+Ol 16.07 l.78E+Ol Ac-228 16 1119.97 4472 -4484 4478.45 3.42E+Ol 16.11 3.16E+Ol Bi-214 17 1460.89 5832 -5853 5842.91 3.82E+02 39.87 1.22E+Ol K-40 18 1764.34 7052 -7065 7058.05 3.lOE+O l 12.58 8.03E+OO Bi-214 efl},J M = First peak in a multiplet region s,,,r~tt m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLID ES Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCi!grams)

Uncertainty Corr K-40 1. 00 1460.82

• 10.66 5.40E+OO 7.33E-01 miss Cs-137 1. 00 661.66

• 85.10 1.65E-01 3.68E-02 miss Tl-208 1. 00 583.19

• 85.00 1.16E-01 2.98E-02 miss Bi-211 0.95 351.07

• 13.02 9.00E-01 2.17E-01 mis s Pb-212 1. 00 115 .18 0.60 5/5/2016 12:35:30PM Page 3 of8 Analysis Report for 05-May-16-1 0011 L3-10220C-FRGS-011SS (DRIED) Nuclide Id Energy Yield{%) Activity Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr Pb-212 1. 00 238.63

• 43.60 2.90E-01 5.95E-02 miss 300.09 3.30 Pb212-XR 0.99 74.82

• 10.28 6.44E-01 2.47E-01 miss 77 .11

• 17.10 4.68E-01 1.60E-01 miss 87.35 3.97 89.78 1. 46 Bi-214 0.9 9 609.32

• 45.49 2.55E-01 5.91E-02 miss 768.36 4.89 806.18 1.26 934.06 3.11 11 20.29

• 14.92 2.87E-01 1.37E-01 miss 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1 4 07.99 2.39 1 5 09.21 2.13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 3.5 3 E-01 1.46E-01 m i ss 1847.43 2.0 3 211 8.51 1.16 Pb-214 1. 00 241.99

• 7.25 3.61E-01 1. 29E-01 miss 295.2 2

• 18.42 l.62E-01 8.40E-0 2 miss 351.93

• 35.60 3.29E-01 7.90E-02 mi s s 785.96 1. 06 Ra-226 0.99 186.21

• 3.64 7.96E-01 4.lOE-01 miss Ac-228 1. 00 129.07 2.42 209.25

• 3.89 4.06E-01 3.40E-01 miss 270.24 3.46 328.00 2.95 3 3 8.3 2

• 11.27 1. 96E-01 1.30E-01 miss 409.46 1. 92 463.00 4.40 7 9 4. 95 4.25 911.20

• 2 5.80 2.38E-0 1 7, 72E-02 miss 964. 77 4.99 968.97

• 15.80 3.lBE-01 1.19E-0 1 miss 1588.20 3.22 U-235 0.99 143.76 10. 96 163.33 5.08 185. 71

• 57.20 5.07E-02 2.61E-02 miss 202 .11 1. 08 205.31 5.01 Analysis Report for 05-May-16-10011 L3-10220C-FRGS-011SS (DRIED) * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 5/5/2016 12:35:30PM INTERFERENCE CORRECTED REPORT X ? ? Nuclide Name K-40 Cs-137 Tl-208 Bi-211 Pb-212 Pb212-XR Bi-214 Pb-214 Pb214-;~R Ra-226 Ac-228 U-235 Nuclide Id Confidence

1. 000 1. 000 1.000 0.953 1.000 0.998 0.998 1. 000 0.998 0.996 1. 000 0.997 ? "" nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wtmean Activity (pCi/grams) 5.40E+OO 1.65 E-01 l.16 E-01 2.94 E-01 2.90 E-Ol 5.20 E-Ol 2. 71 E-Ol 2.22 E-01 7.96E-01 2.53E-0 1 5.0':'E-02

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 7.33E-01 3.68E-02 2.98E-02 2.89E-0 1 5.95E-02 1.34 E-01 5.09E-02 7.04E-02 4.lOE-01 5. 72E-02 2.6 1E-02 Pag e 4 of8 Comments 5/5/2016 12:35:30PM Analysis Report for 05-May-16-10011

+ + +

+ + + + +

+ L3-10220C-FRGS-011SS (DRIED) Peak Locate Performed on Peak Locate From Channe l Peak Locate To Channel Peak No. Energy (keV) 3 109. 37 M "' First peak in a multiplet region m "' Other peak in a multiplet region F "' Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 5/5/2016 12:34:53PM

120 : 8192 Peak Size (CPS) 1.12587E-02 Peak CPS(%) Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

K-40 1460.82

• 10.66 5.40E+OO 2.21E-01 2.21E-Ol Cr-51 320.08 9.91 -8.36E-02 1.53E-Ol l.53E-01 Mn-54 834.85 99.98 3.32E-03 2.02E-02 2.02E-02 Co-58 810.76 99.45 8. 71E-05 2.lOE-02 2. lOE-02 1674.73 0.52 1.66E-01 2.45E+OO Co-60 1173.23 99.85 4 .13E-03 1.84E-02 2.68E-02 1332.49 99.98 1.SlE-03 1.84E-02 Nb-94 702.65 99.81 l.OlE-03 1.92E-02 1. 96E-02 871.09 99.89 1.94E-03 l.92E-02 A.g-108m 79.13 6.60 ~.74E-02 l.55E-D2 4.48E-01 433.94 90.50 -3.22E-03 1.55E-02 614.28 89.80 -4.95E-03 l.99E-02 722.94 90.80 -l.OBE-02

1. 72E-02 Sn-113 255.13 2 .11 -2.34E-01 2.30E-02 7.16E-Ol 391.70 64. 97 -6.12E-04 2.30E-02 Cs-134 475.36 1. 48 2.09E-01 l.54E-02 l.14E+OO 563.25 8.34 -3.00E-02 l.97E-01 569.33 15.37 3.32E-02 1.19E-01 Page 5 of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss 5/5/2016 12:35:30PM Page 6 o f8 Analysii; Report for 05-May-16-1 0011 L3-10220C-FRGS-O 11 SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCl!grams)

Corr Cs-134 604.72 97.62 -6. 51E-03 l.54E-02 l.54E-02 miss 7 95.86 85.46 6.88E-04 2.56E-02 miss 801.95 8.69 4.32E-02 2.33E-01 miss 1038.61 0.99 -5.06E-01 2.0lE+OO miss 1167.97 1. 79 2.39E-01 1.26E+OO miss 1365.19 3.02 -8.16E-02 t;. 42E-Ol miss + Cs-137 661.66 -.. 85.10 1.65E-Ol 3.0lE-02 3. OlE-02 miss + Eu-152 121.78 28.67 6.07E-04 5.12E-02 5.16E-02 miss 244.70 7.61 -6.13E-02

1. 90E-01 miss 295.94 0.45 8.87E-01 5.75E+OO miss 344.28 26.60 -3.00E-05 5.73E-02 miss 367.79 0.86 -4.00E-01 l.45E+OO miss 411.12 2.24 -3.0lE-01 5.87E-01 miss 443. 96 2.83 3.39E-Ol 6.85E-Ol miss 488.68 0.42 -3.08E-Ol 3.63E+OO miss 563.99 0.49 -3.54E-Ol 3.33E+OO miss 586.26 0.46 -4.42E-01 3.55E+OO miss 678.62 0.47 -9.65E-01 3.57E+OO miss 688.67 0.86 4.69E-01 2.18E+OO miss 719. 35 0.28 2.88 E-01 6.06E+OO miss 778.90 12. 96 l.26E-03 1.38E-01 miss 810.45 0.32 1.84E+D0 6.88Et00 miss 867.37 4.26 -1.33E-D1 3.93E-01 miss 919.33 0.43 1.38E+D0 4.48E+OO mis~ 964.08 14.65 8.4eE-02 1.82E-01 miss 1085.87 10.24 1. 20E-02 2.09E-D1 miss 1089.74 1. 73 -1.02E+OO 6.61E-01 miss 1112. 07 13. 69 -7.69E-02

1. 20E-01 miss 1 212.95 1. 43 -l.03E+OO l.54E+OO miss 1249.94 0.19 -1.49E+OO l.24E+Ol miss 1299.14 1. 63 -1.22E-02 1.28E+OO miss 1408.01 21. 07 -2.29E-02 5.12E-02 miss 1457.64 a.so -2.67E+OO 6.38E+OO miss 1528.10 0.28 1. 27E+OO 5. 96E+OO miss + Eu-154 123.07 40.40 -2.58E-02 3.34E-02 3.34E-02 miss 247.93 6.89 -8.03E-03 2.21E-Ol miss 591.76 4.95 2.08E-01 3.79E-Ol miss 692.42 1. 78 5.28E-02 8.91E-Ol miss 723.30 20.06 -1.37E-02 8.46E-02 miss 756.80 4.52 -4.27E-03 3.72E-01 miss 873.18 12.08 5.14E-02 l.59E-01 miss 996.29 10.48 2.36E-02 1.76E-01 miss 1004.76 18.01 -1.45E-02 l.OBE-01 miss 1274.43 34.80 7.81E-D3 7.89E-02 miss 1596.48 1. 80 -6.18E-D2 1.08E+D0 miss + Eu-155 45.30 1. 31 1.55E+D0 8.82E-02 4.69E+OO miss 60.01 1. 22 6.49E-D1 5.49E+OO miss 86.55 30.70 2.32E-02 8.82E-02 miss 105.31 21.10 5.12E-02 9.36E-02 miss + Tl-208 583.19

• 85.00 1.16E-01 2.89E-02 2.89E-02 miss + Bi-211 351.07

• 13.02 9.00E-01 1.78E-Ol 1.78E-01 miss 5/5/2016 12:35:30PM Page 7 of8 Analysis Report for 05-May-16-10011 L3-10220C-FRGS-011 SS (DRIED) Nuclide Energy Yield(%) Ar;tivity Nuc!ideMDA Line MD.4. Coinc Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

Corr + Pb-211 404.85 3.78 2.17E-02 4.6"7E-01

4. 67E-01 miss 427.09 1. 76 -1.75E-Ol 8.49E-Ol miss 832.01 3.52 -5.59E-02 5.08E-Ol miss + Bi-212 39.86 1. 06 2.24E+OO 4.36E-01 6.13E+OO miss 727. 33 6.67 2.97E-01 4.36E-01 miss 785.37 1.10 -5.08E-01 l.63E+OO miss 1620.50 1. 47 -3.82E-01 l.03E+OO miss + Pb-212 11 5 .1 8 0.60 -6 .13E-01 4.57E-02 2. 63E+OO miss 238.63

• 43.60 2.90E-01 4.57E-02 miss 300.09 3.30 3.88E-01 6.02E-01 miss + Pb212-XR 74.82

• 10.28 6.44E-01 2.53E-01 4. 68E-01 miss 77 .11

• 17.10 4.68E-01 2.53E-01 miss 87.35 3. 97 3.68E-01 6.BOE-01 miss 89.78 1. 46 7.28E-01 1.70E+OO miss + Bi-214 609.32 :,': 45.49 2.55E-01 4.82E-02 4.82E-02 miss 768.36 4.89 2. llE-01 5.07E-01 miss 806.18 1. 26 -3.SlE-01 l.44E+OO miss 934.U6 3.11 1. 96E-01 7.42E-01 miss 1120.29

• 14.92 2.87E-01 1.76E-01 miss 1155.21 1. 63 5.35E-01 1.84E+OO miss 1238.12 5.83 3.41E-Ol 6.07E-01 miss 1280.98 1. 43 ~.73E-01 1. 92E+OO miss 1377. 67 3.99 3.07E-01 6.56E-01 miss 1385.31 0.79 3.91E-01 2.19E+OO miss 1401.52 1. 33 2.22E-01 1.74E+OO miss 1407.99 2.39 -2.0lE-01 4.SOE-01 miss 1509.21 2 .13 -5. 96E-02 8.72E-01 miss 1661. 27 1. 05 2.19E-01 l.71E+OO miss 1729.59 2.88 4.26E-01 9.94E-01 miss 1764.49

• 15.30 3.53E-01 1.41E-01 miss 1847.43 2.03 2.77E-01 1.06E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99

• 7.25 3.61E-01 6.51E-02 2.30E-01 miss 295.22

• 18.42 1.62E-01 l.19E-01 miss 351.93

• 35.60 3.29E-01 6.51E-02 miss 785.96 1. 06 2. 96E-01 1.93E+OO miss + Pb214-XR 74.82

• 5.80 1.14E+OO 4,47E-01 8.29E-01 miss T: .11

• 9.70 8.25E-Ol 4.47E-01 miss 87.35 2.24 6.52E-Ol l.21E+OO miss 8!'.l.78 0.82 1.30E+OO 3.04E+OO miss + Ra-226 186.21

• 3.64 7.96E-01 5.93E-01 5.93E-01 miss + Ac-228 129.07 2.42 l.35E-01 7.54E-02 6.84E-01 miss 209.25

• 3.89 4.06E-01 5.34E-Ol miss 270.24 3.45 2.78E-01 5.40E-01 miss 328.00 2.95 4.84E-01 6.58E-01 miss 338.32

• 11. 27 1. 96E-01 l.93E-01 miss 409.46 1. 92 2.06E-01 8.69E-01 m i ss 463.00 4.40 1.29E-01 4.34E-01 m i ss 7 94. 95 4.25 3.34E-01 5.63E-01 miss 911. 20

• 25.80 2.38E-01 7.54E-02 miss 964.77 4.99 2.22E-01 5.36E-01 miss 5/5/2016 12:35:30PM Page 8 of8 Analysts Report for 05-May-16-10011 L3-10220C-FRGS-011SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCi!grams)

Corr Ac-228 968.97 }: 15.80 3.lBE-01 7.54E-02 l.27E-01 miss 1588.20 3.22 3.09E-01 7.SOE-01 miss + Pa-231 27.36 10.30 O.OOE+OO 4.71E-02 4.71E-02 miss 283.69 1. 70 2.80E-01 9.37E-01 miss 300.07 2.47 5.18E-01 8.0SE-01 miss 302.65 2.20 -1.46E-01 6.25E-01 miss 330.06 1. 40 -5.26E-01

1. llE+OO miss + Th-234 92.38 2.13 1.66E+OO 1.44E+OO l.44E+OO miss 92.80 2.10 2.0lE+OO 1.SOE+OO miss 112.81 0.21 -5.15E+OO 8.lOE+OO miss + U-235 143.76 10.96 -3.28E-02 3.77E-02 1.13E-01 miss 163.33 5.08 4.68E-02 2. 60E-01 miss 185.71

• 57.20 5.07E-02 3.77E-02 miss 202 .11 1. 08 -2.42E-01 1.28E+OO miss 205.31 5.01 -1. 4 8E-02 2.81E-01 miss + Am-241 59.54 35.90 -5.84E-02

1. 82E-01 1.82E-01 miss + -.. Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > ;; MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

VI ' C ::s 120 110 100 90 80 70 8 60 50 40 30 20 1000 2000 3000 0000014856.CNF 4000 channel 5000 Live Time :1800.000 sec Real Time :1801.260 sec Start: 1: -0. 2(kev) stop : 8192: 2047 .4(kev) Acq. Start :Thu May 05 12:04:43 2016 6000 7000 8000 Analysis Report for 05-May-16-1 0012 L3-10220C-FRGS-012SS (DRIED) 5/5/2016 12:36:09PM GAMMA SPECTRUM ANAL YSJS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done O n Efficiency Calibration Description Sample Number : 05-May-16-10012

L3-10220C-FRGS-012SS (DRIED) : 1L 130G Soil Sample 1.534E+03 grams : Default : 5/2/2016 12:45:00PM

5/5/2016 12:05:08PM

130G 1 L Soil Sample : JWelch : P408188 : 130G Soil : 1800.0 seconds : 1802.B seconds : 0.16 % : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 14857 PEAK WITH N/0 REPORT Peak Analysis Performed on : 5/5/2016 12:35:36PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C: \Can berra\Apex\Root\Default\Library\Zion Lib-BN L. NLB : 1.000FWHM Page 1 of8 5/5/2016 12:36:09PM Page 2 of8 Analysis Report for 05-May-16-10012 L3-10220C-FRGS-012SS (DRIED) Peak. Energy ROI ROI Peak. Net Peak. Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide 1 77.19 307 -314 309.82 3.84E+Ol 33.06 l.93E+02 Pb214-X~ Pb212-XR 2 185.83 740 -747 743.99 2.35E+Ol 29.81 l.93E+02 U-235 Ra-226 3 238.50 948 -972 954.52 2.49E+02 73.44 4.98E+02 Pb-212 4 295.17 1172 -1189 1181. 00 9.54E+O l 41.09 1.99E+02 Pb-2 14 Eu-152 5 351.74 1400 -1416 1407.14 1.61E+02 35.58 l.15E+02 Pb-214 Bi-211 6 510.51 2037 -2049 2041.92 4.66E+O l 24 .11 8.28E+Ol ..... h//./~5Jf 7 583.09 2325 -2338 2332.12 8. 52E+0.1 25.25 6.16E+Ol Tl-2 08 8 609.23 2427 -2445 2436.68 l.37E+02 28.52 4.56E+Ol Bi-2 14 9 661.59 2638 -2655 2646.07 2.30E+02 35.03 6.07E+Ol Cs-137 10 911.11 3638 -3651 3644.15 4.94E+Ol 17.15 2 .13E+Ol Ac-228 11 964. 20 385 1 -3862 3856.55 l.20E+Ol 12.01 2.40E+Ol Eu-152 A.c-228 12 1460.58 58 31 -5854 5843.30 4.79E+02 44.40 1.03E+Ol K-40 ~p,.J M = First peak in a multiplet region 5,S:-t l, m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Caine Name Confidence

{keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

• 10.66 6.39E+OO 8. llE-01 miss Cs-137 1. 00 661.66

• 85.10 2.24E-01 4.35E-02 miss Tl-208 0.99 5 83.19

• 85.00 7.63E-02 2.44E-02 miss Pb-212 0.99 115 .18 0.60 238.63

• 43.60 2.39E-Ol 8.02E-02 miss 300.09 3.30 Pb212-XR 1. 00 74.82 10. 28 77 .11

• 17.10 2.7 0 E-01 2.3 9E-0 1 m iss 87.35 3.97 89.78 1. 46 Bi-214 1. 00 609.32

• 45.49 2.36 E-0 1 5.68E-02 miss 5/5/2016 12:36:09PM P11ge 3 of8 Analysis Report for 05-May-16-10012 L3-10220C-FRGS-012SS (DRIED} Nuclide Id Energy Yield(%) Activity Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr Bi-214 1. 00 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1661.27 1. 05 1729.59 2.88 1764.49 15.30 18 47.43 2.03 2118. 51 1.16 Pb-214 0.99 241. 99 7.25 295.22

• 18.42 2.48E-01 1.14E-01 miss 351.93

• 35.60 2.41E-01 6.59E-02 miss 785. 96 1. 06 Pb214-XR 1. 00 74.82 5.80 77 .11

• 9.70 4.75E-01 4.24E-01 miss 87.35 2.24 89.78 0.82 Ra-226 0.99 186.21

• 3.64 2.40E-01 3.07E-Ol miss Ac-228 0.48 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11. 27 409.46 1. 92 463.00 4.40 794.95 4.25 911. 20

• 25.80 l.97E-01 7.05E-02 miss 964. 77

• 4.99 2.57E-01 2.59E-01 miss 968. 97 15.80 1588.20 3.22 U-235 0.99 143.76 10. 96 163.33 5.08 185.71

• 57.20 1.53E-02 1.95E-02 miss 202 .11 1. 08 205.31 5.01 = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Analysis Report for 05-May-16-1 001 2 L3-10220C-FRG S-012SS (DRIED) Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 5/5/2016 12:36:09PM INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.997 6.39E+OO 8. llE-01 Cs-137 1. 000 2.24E-01 4.35E-02 Tl-208 0.999 7.63E-02 2.44E-02 X Bi-211 0.973 Pb-212 0.999 2.39E-Ol 8.02E-02 ? Pb212-):R 1.000 2.70E-01 2.39E-01 Bi-214 1. 000 2.36E-Ol 5.68E-02 Pb-214 0.999 2.43E-Ol 5.70E-02 ? Pb214-XR 1. 000 4.75E-01 4.24E-01 ? Ra-226 0.991 2.40E-01 3.07E-Ol Ac-228 0.481 '.2.0lE-01 6.81E-02 ? U-235 0.999 1. 53E-02 1.~SE-02 ? .,,,_ nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma P a ge 4 of 8 Comments 5/5/2016 12:36:09PM Analysis Report for 05-May-16-10012

+. + + + + + + + + L3-10220C-FRGS-012SS (DRIED) Peak Locate Performed on Peak Locate From Channe l Peak Locate To Channel Peak No. Energy (keV) 6 510.51 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 5/5/2016 12:35:36PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 2.59003E-02 25.86 Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

K-40 1460.82

• 10.66 6.39E+OO 2.00E-01 2.00E-01 Cr-51 320.08 9.91 -7.63E-03 1.72E-01 1.72E-Ol Mn-54 834.85 99.98 1. 22E-02 2.34E-02 2.34E-02 Co-58 810.76 99.45 1.08E-02 1. 98E-02 1.98E-02 1674.73 0.52 6.68E-01 3.77E+OO Co-60 1173.23 99.85 6.22E-03 2. llE-02 2.60E-02 1332.49 99.98 4.22E-03 2. llE-02 Nb-94 702.65 99.81 -1.59E-03 1.57E-02 1.57E-02 871.09 99.89 -8.53E-03 1.58E-02 Ag-108m 79 .13 6.60 3.07E-Ol 1.99E-02 7.29E-01 433.94 90.50 9.43E-03 1.99E-02 614.28 89.80 7.90E-03 2.06E-02 722.94 90.80 6.67E-03 2.12E-02 Sn-113 255.13 2 .11 4.97E-01 2.63E-02 8.87E-01 391.70 64.97 -7.76E-03 2.63E-02 Cs-134 475.36 1. 48 1.97E-01 1.84E-02 1.19E+OO 563.25 8.34 -9.68E-03 2.05E-01 Page 5 of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss 569.33 15.37 -2.73E-02 1.22E-01 miss 5/5/2016 12:36:09PM Page 6 of8 Analysis Report for 05-May-16-10012 L3-10220C-FRGS-012SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

Corr Cs-134 604. 72 97.62 1. 33E-03 1. 84E-02 l.84E-02 miss 795.86 85.46 1.59E-02 3.lOE-02 miss 801.95 e.69 6.00E-02 2.05E-01 miss 1038.61 0.99 5.77E-01 2.36E+OO mis~ 1167.97 1. 79 -4.57E-01 l.19E+OO miss 1365.19 3.02 l.99E-01 7.12E-01 miss + Cs-137 661.66

• 85.10 2.24E-01 3.08E-02 3.08E-02 miss + Eu-152 121. 7 8 28.67 -1.36E-02 6.55E-02 6.55E-0~ miss 244.70 7.61 2.30E-02 2.40E-01 miss 295.94 0.45 6.19E+OO 5.83E+OO miss 344.28 26.60 3.94E-03 6.73E-02 miss 367.79 0.86 -3.93E-01 1.66E+OO miss 411.12 2.24 -6.41E-02 7.30E-01 miss 443. 96 2.83 -4.60E-02 5.68E-01 miss 488.68 0.42 2.41E-01 3.60E+OO miss 563.99 0.49 -4.54E-01 3.48E+OO miss 586.26 0.46 -9.96E-01 3.82E+OO miss 67 8. 62 0.47 1. 52E+OO 3.91E+OO miss 688.67 0.86 -2.53E-01 2.00E+OO miss 719.35 0.28 -9.74E-02 6.33E+OO miss 778.90 12.96 -4. llE-02 1.34E-01 miss 810.45 0.32 l.38E+OO 5.57E+OO miss 867.37 4.26 4.86E-02 4.70E-01 miss 919.33 0.43 -2.83E-01 3.42E+OO miss 964. 08 14.65 l.02E-01 1.86E-01 miss 1085.87 10.24 7.39E-02 2.28E-01 miss 1089.74 1. 73 7.03E-02 1.26E+OO miss 1112. 07 13.69 3.97E-02 1.73E-01 miss 1212.95 1. 43 6.24E-03 1.76E+OO miss 1249.94 0.19 -5.57E-01 l.39E+Ol miss 1299.14 1. 63 l.23E+OO l.84E+OO miss 1408.01 21.07 -7.62E-03 1.04E-Ol miss 1457.64 0.50 -3 .13E+OO 9.28E+OO miss 1528.10 0.28 -4.48E-01 3.84E+OO miss + Eu-154 123.07 40.40 -3.57E-03

4. 72E-02 4.72E-02 miss 247.93 6.89 -1.42E-01 2.19E-01 miss 591.76 4.95 8.64E-02 3.22E-01 miss 692.42 1. 78 -8.02E-02 9.38E-01 miss 723.30 20.06 1. 71E-03 9.lOE-02 miss 756.80 4.52 -6.86E-02 3.78E-Ol miss 873.18 12.08 l.26E-02 l.76E-01 miss 996.29 10.48 9.87E-03 1.97E-01 miss 1004.76 18.01 l.73E-02 1.15E-01 miss 1274.43 34.80 1. 22E-02 6.71E-02 miss 1596.48 1. 80 2.07E-01 1.02E+OO miss Eu-155 4~.30 1. 31 -4.83E+OO 1.14E-01 l.24E+Ol miss 60.01 1. 22 -2.97E-01 1.22E+Ol miss 86.55 30.70 1. 66E-02 1.22E-Ol miss 105.31 21.10 2.08E-02 1.14E-Ol miss + Tl-208 583.19

• 85.00 7.63E-02 2.78E-02 2.78E-02 miss + Bi-211 351. 07

• 13. 02 6.59E-D1 1. 80E-01 1.BOE-01 miss 5/5/2016 12:36:09PM Page 7 of8 Analysis RP.port for 05-May-16-10012 L3-10220C-FRGS-012SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr + Pb-211 404.85 3.78 6.40E-02 3.60E-01 4.47E-01 miss 427.09 1. 76 -9.67E-02 8.72E-01 miss 832.01 3.52 -2.38E-01 3.60E-01 miss + Bi-212 39.86 1. 06 O.OOE+OO 3.73E-01 :.29E+Ol miss 727. 33 6.67 2.26E-01 3.73E-01 miss 785.37 1.10 l.16E-01 l. 64E+OO miss 1620.50 1. 47 4.59E-01 l.57E+OO miss + Pb-212 115. 18 0.60 9.68E-01 1.0'7E-Ol 3.69E+OO miss 238.63 ..... , 43.60 2.39E-01 1.07E-01 miss 300.09 3.30 2.04E-01 5.63E-01 miss + Pb212-;~R 74.82 10.28 3.62E-01 3.74E-01 6.88E-Ol miss 77 .11

• 17.10 2.70E-01 3.74E-01 miss 87.35 3.97 8.73E-01 9. 72E-01 miss 89.78 1. 46 9.76E-01 2.29E+00 miss + Bi-214 609.32 *'* 45.49 2.36E-01 5.08E-02 5.08E-02 miss 768.36 4.89 1. 47E-01 4.40E-01 miss 806.18 1. 26 5.53E-02 l.12E+OO miss 934.06 3.11 2.94E-01 7.93E-01 miss 1120.29 14.92 l.71E-01 2.40E-01 miss 1155.21 1. 63 1.BlE-01 l.66E+OO miss 1238.12 5.83 2.67E-01 5.91E-Ol miss 1280.98 1. 43 2.14E-01 1.7DE+OO miss 1377. 67 3.99 4.58E-02 5.94E-01 miss 1385. 31 0.79 -1.97E-01 l.60E+OO miss 1401.52 1. 33 5.23E-01 1.64E+OO miss 1407.99 2.39 -6.70E-02 9.16E-01 miss 1509.21 2.13 5.56E-01 1.24E+OO miss 1661. 27 1. 05 -9.38E-02 1.lOE+OO miss 1729.59 2.88 2.34E-01 8.46E-01 miss 1764.49 15.30 2.32E-01 2.74E-01 miss 1847.43 2.03 -8.37E-02 l.OlE+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241. 99 7.25 4.82E-02 6.57E-02 2.83E-Ol miss 295.22

• 18.42 2.48E-01 1.61E-01 miss 351. 93

• 35.60 2.41E-01 6.57E-02 miss 785. 96 1. 06 1.94E-01 1.65E+OO miss + Pb214-XR 74.82 5.80 6.41E-01 6.58E-01 1.22E+OO miss 77 .11

• 9.70 4.75E-01 6.58E-Ol miss 87.35 2.24 1.55E+D0 1. 72E+OO miss 89.78 0.82 1.74E+OO 4.09E+OO miss + Ra-226 186.21

• 3.64 2.40E-Ol 5.0lE-01 5.0lE-01 miss + Ac-228 129.07 2.42 1.37E-01 7.53E-02 8.17E-01 miss 209.25 3.89 3.21E-01 4.63E-01 miss 270.24 3.46 1.78E-01 5.44E-01 miss 328.00 2.95 1.79E-01 6.28E-01 miss 338.32 11. 27 1.51E-Ol 1. 96E-01 miss 409.46 1. 92 -2.22E-01 8.48E-01 miss 463.00 4.40 2.38E-01 4.84E-01 miss 794.95 4.25 4.34E-01 6.58E-01 miss 911. 20

• 25.80 1.97E-01 7.53E-02 miss 964. 77

• 4.99 2.57E-01 4.04E-01 miss 5/5/2016 12:36:0SPM Page 8 of8 Analysis Report for 05-May-16-10012 L3-10220C-FRGS-012SS (DRIED) Nuclide Energy Yield{°/o)

Activity NuclideMDA LineMDA Coim: Name (keV) (pCilgrams) (pCi!grams) (pCi!grams)

Corr Ac-228 968. 97 15.80 1.30E-01 7.53E-02 l.94E-01 miss 1588.20 3.22 -1.35E-01 4.38E-01 miss + Pa-231 27.36 10.30 1.64E-01 7.52E-01 1.54E+OO miss 283.69 1. 70 5.91E-01 1.lOE+OO miss 300.07 2.47 2.73E-01 7.52E-01 miss 302.65 2.20 4.25E-01 8.0lE-01 miss 330.06 1. 40 -3.75E-01 l.18E+OO miss + Th-234 92.~8 2 .13 8.69E-01 1. 78E+OO 1.78E+OO miss 92.80 2.10 1.24E+OO 1.82E+OO miss 112. 81 0.21 1.54E+OO 1.02E+Ol miss + U-235 143.76 10. 96 -9.19E-03 3.19E-02 1. 61E-01 miss 163.33 5.08 2.SOE-02 3.31E-01 miss 185.71

• 57.20 l.53E-02 3.19E-02 miss 202 .11 1. 08 -1.69E-01 l.44E+OO miss 205.31 5.01 3.34E-02 3.19E-01 miss + Am-241 59.54 35.90 -8.44E-02 4.16E-01 4.16E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ ;;;; Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performe d. free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V> +-' C: 0 u 120 1000 :,, .lo, I I ' ,J I ***1 1 wJ~i; 2000 3000 QQQQQ14SS?.CNF

.. -----Li-ve-Ti.m_e_:i-:~-t 00 s-2~-!:-~ -Real Time 1: -0.l(kev) 4000 channel 5000 Start: 8192; 2047. O(k~t\2 *OS :08 2016 Stops 'tart :Thu May . Acq.

.~pex-Gamma Anaiysis Report for 05-May-"i6-i 0002 L3-10220C-FRGS-013SS (DRIED) 5/5/2016 8:57:02AM GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done O n Efficiency Calibration Description Sample Number : 05-May-16-10002

L3-10220C-FRGS-013SS (DRIED) : 1 L 130G Soil Sample 1.624E+03 grams : Default : 5/3/2016 7:50:00AM

5/5/2016 8:19:53AM

130G 1 L Sand Sample : JWelch : P11314X2 : 130G Sand : 1800.0 seconds : 1801.3 seconds : 0.07% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

11/26/2012

14847 PEAK WITH NID REPORT Peak Analysis Performed on : 5/5/2016 8:56:30AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of8 5/5/2016 8:57:02AM Page 2 of8 Analysis Report for 05-May-16-10002 L3-10220C-FRGS-013SS (DRIED) Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide M 1 74.82 296-315 300.53 8.74E+Ol 25.90 2.28E+02 Pb214-XR Pb212-XR m 2 77.01 296 -315 309.24 1. 24E+02 28.55 2.49E+02 Pb214-XR Pb212-XR 3 86.80 345 -354 348.35 4.30E+O l 35.39 2.00E+02 Eu-155 Pb212-XR Pb214-XR 4 92.76 367 -377 37':. .18 5.19E+Ol 40.50 2.50E+02 Th-'.234 Th-234 Ac228-XR U235-XR 5 209.4 0 835 -842 838.09 2.77E+Ol 23.49 l.09E+02 Ac-228 M 6 238.63 949 -973 954.83 2.84E+02 36.51 1. 4 9E+02 Pb-212 m 7 241.87 949 -973 967.79 6.00E+O l 21.03 1.78E+02 Pb-214 8 295.16 1176 -1188 1180. 68 1.28E+02 30.70 8.16E+Ol Pb-214 Eu-152 9 338.33 1347 -1360 1353.18 7.14E+O l 26.73 8.91E+Ol Ac-228 10 351.90 1400 -1414 1407.39 1.85E+02 35.32 1. 01E+02 Pb-214 Bi-2 11 11 510.74 2037 -2052 2042.17 4.84E+O l 23.79 7.llE+Ol ..... ,4,/H,rl( 12 583.05 2324 -2340 2331. 20 9.40E+Ol 27.07 6.60E+Ol Tl-208 13 609.30 2429 -2444 2436.12 l.54E+02 29.07 4.42E+Ol Bi-214 14 661. 69 2639 -2653 2645.57 5.37E+Ol 21.88 5.66E+Ol Cs-137 15 911.06 3636 -3652 3642.75 6.40E+O l 20.26 3.21E+Ol Ac-228 16 969.36 3869 -3883 3875.92 4.04E+O l 16.62 2.53E+Ol Ac-228 17 1120.16 4473 -4485 4479.21 2.92E+O l 15.76 3.37E+Ol Bi-214 18 1238.36 4947 -4958 4952.19 1. OlE+Ol 12.65 3.18E+Ol Bi-214 19 1460.90 5832 -5855 5842.94 5.71E+02 49.26 2.67E+Ol K-40 20 1764.64 7053 -7066 7059.25 2.47E+O l 10.79 4.56E+OO Bi-214 ~",J M = First peak in a multiplet regio n _s-.... s~t t, m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLID ES 5/5/2016 8:57:02AM Page 3 of8 Analysis Report for 05-May-16-10002 L3-10220C-FRGS-013SS (DRIED) Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 1. 00 1460.82

• 10.66 6.53E+OO 8.00E-01 miss Cs-137 1. 00 661.66

• 85.10 4. SlE-02 l.92E-02 miss Tl-208 0.9 9 583.19

• 85.00 7.26E-02 2.27E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 2.32E-01 4.79E-02 miss 300.09 3.30 Pb212-XR 0.99 74.82

• 10.28 5.64E-01 2.04E-01 miss 77 .11

• 17.10 4.47E-01 1. 38E-01 miss 87.35 "' 3.97 4.84E-Ol 4. llE-01 miss 89.78 1. 46 Bi-214 0.99 609.32

• 45.49 2.29E-01 5.12E-02 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29

• 14.92 1.99E-01 1.09E-01 miss 1155. 21 1. 63 1238.12

• 5.83 1.87E-01 2.36E-01 miss 1280.98 1. 43 1377. 67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2 .13 1661. 27 1. 05 1729.59 2.88 1 764.49

• 15.30 2.28E-01 1.0lE-01 miss 1 847.43 2.03 2118.51 1.16 Pb-L14 1. 00 241.99

• 7.25 2.97E-01 1.15E-01 miss 295.22

• 18.42 2.85E-01 8.22E-02 miss 351.93

• 35.60 2.40E-Ol 5.97E-02 miss 785.96 1. 06 Ac-228 0.99 129.07 2.42 209.25

• 3.89 2.36E-01 2.04E-Ol miss 270.24 3.46 328.00 2.95 338.32

• 11. 27 2.85E-01 l.16E-01 miss 409.46 1. 92 463.00 4.40 794.95 4.25 911. 20

• 25.80 2.20E-Ol 7.22E-02 miss 964. 77 4.99 968. 97

• 15.80 2.36E-01 9.95E-02 miss 1 588.20 3.22 Ac228-XR 0.98 89. 96 1. 90 93.35

• 3.10 6.85E-01 5.80E-01 miss Th-234 1. 00 92.38 2 .13 92.80

• 2.10 l.07E+OO 8.87E-01 mis s 112. 81 0.21 U235-XR 0.98 89. 96 3.47 93.35

• 5.60 3.79E-Ol 3.06E-01 miss 105.60 1. 32 Analysis Report for 05-May-16-10002 L3-10220C-FRGS-013SS (DRIED) * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWH M Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 5/5/2016 8:57:02AM INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1.000 6.53E+OO 8.00E-01 Cs-137 1.000 4.SlE-02 l.92E-02 X Eu-155 0.998 Tl-208 0.999 7.26E-02 2.27E-02 X Bi-211 0.958 Pb-212 1. 000 2.32E-01 4.79E-02 Pb212-XR 0.997 4.84E-01 l.lOE-01 Bi-214 0.999 2.23E-01 4.lSE-02 Pb-214 1. 000 2.62E-01 4.45E-02 X Pb214-XR 0.997 Ac-228 0.998 2.37E-01 5.06E-02 ? Ac228-XR 0. 987 6.85E-01 5.80E-01 ? Th-234 1.000 l.07E+OO 8.87E-01 ? U235-XR 0.989 3.79E-01 3.06E-01 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Page 4 of8 Comments 5/5/2016 8:57:02AM Analysis Report for 05-May-16-10002

+ + + + + + + + + L3-10220C-FRGS-013SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 11 510.74 M = First peak in a multiplet regio n m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAK S : 5/5/2016 8:56:30AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 2.69034E-02 24.56 Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NL B Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCUgrams) (pCi!grams)

K-40 1460.82

• 10.66 6.53E+OO 2.57E-01 2.57E-01 Cr-51 320.08 9.91 4.09E-02 1. 42E-01 1.42E-Ol Mn-54 834.85 99.98 1.93E-03 1.88E-02 l.88E-02 Co-58 810.76 99.45 -2.66E-03 l.lBE-02 1.18E-02 1674.73 0.52 -3.33E-02

1. 96E+OO Co-60 1173.23 99.85 5.50E-04 1. 06E-02 2.36E-02 1332.49 99.98 -6.18E-03 l.06E-02 Nb-94 702.65 99.81 -6.63E-04 1.24E-02 1.24E-02 871.09 99.89 -1.00E-03 1.36E-02 Ag-108m 79.13 6.60 2.40E-02 1. 4 8E-02 3.68E-01 433.94 90.50 -7.04E-04 l.48E-02 614.28 89.80 7.30E-03 1.97E-02 722.94 90.80 1.71E-03 1.68E-02 Sn-113 255 .13 2 .11 1.55E-01 1.79E-02 6.12E-01 391.70 64.97 -3.05E-03 1.79E-02 Cs-134 475.36 1. 48 -2.14E-01 1.25E-02 8.24E-01 563.25 8.34 1. 37E-02 l.34E-01 569.33 15.37 1.95E-02 8. 72E-02 Page 5 of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss 5/5/2016 8:57:02AM Page 6 of8 Analysis Report for 05-May-16-10002 L3-10220C-FRGS-013SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi/grams) (pCi/grams) (pCilgrams)

Corr Cs-134 604. 72 97.62 -5.27E-03

1. 25E-02 l.25E-D2 miss 795.86 85.46 O.OOE+OO 1. 91E-02 miss 801.95 8.69 3.SlE-02 2.00E-01 miss 1038.61 0.99 4.71E-01 1.91E+OO miss 1167.97 1. 79 6.30E-01 1. 49E+OO miss 1365.19 3.02 2.02E-02 4.14E-01 miss + Cs-137 661.66

• 85.10 4.51E-02 2.48E-02 2.48E-02 miss + Eu-152 121. 7 8 28.67 2.34E-03 4. llE-02 4.31E-02 miss 244.70 7.61 -2.25E-02

1. 68E-01 miss 295.94 0.45 8.86E+OO 5.13E+OO miss 344.28 26.60 -l.18E-02 4.llE-02 miss 367.79 0.86 -4.49E-01 1.30E+OO miss 411.12 2.24 -5.24E-02 6.69E-Ol miss 443. 96 2.83 5.44E-02 4.42E-01 miss 488.68 0.42 -4.lOE-01 2.87E+OO miss 563.99 0.49 3.79E-01 2.07E+OO miss 586.26 0.46 -4.41E-01 3.05E+D0 miss 678.62 0.47 1.62E+OO 3. 46E+OO miss 688.67 0.86 1.23E-01 l.77E+D0 miss 719.35 0.28 -5.54E-01 5.lOE+OO miss T: 7 8.90 12. 96 -5.27E-02 l.03E-01 miss 810.45 0.32 -2.43E-01 3.83E+OO miss 867.37 4.26 2.0lE-03 3.SOE-01 miss 919.33 0.43 -1.41E+OO 3.13E+OO miss 964. 08 14.65 5.59E-02 1.60E-01 miss 1085.87 10.24 -5.36E-03 l.96E-Ol miss 1089.74 1. 73 -4.78E-01 8.14E-Ol miss 1112. 07 13. 69 3.40E-03 1. 66E-Ol miss 1212.95 1. 43 -l.24E-01 l.60E+OO miss 1249.94 0.19 -8.25E-02 l.05E+Ol miss 1299.14 1. 63 4.92E-02 l.30E+OO miss 1408.01 21.07 6.26E-02 l.13E-01 miss 1457.64 0.50 -5.22E+OO 6.83E+OO miss 1528.10 0.28 3.63E-01 4.82E+OO miss + Eu-1 54 123.07 40.40 -1.23E-02 2.90E-02 2.90E-02 miss 247.93 6.89 3.69E-02 l.94E-Ol miss 591.76 4.95 8.13E-02 3.0lE-01 miss 692.42 1. 78 2.31E-01 l.04E+OO miss 723.30 20.06 -6.12E-03 7.38E-02 miss 756.80 4.52 1. 89E-02 3.37E-01 miss 873.18 12.08 2.49E-02 1. 24E-01 miss 996.29 10.48 -2.53E-02 l.43E-01 miss 1004.76 18.01 8.29E-03 9.54E-02 miss 1274.43 34.80 l.78E-02 6. 77E-02 miss 1596.48 1. 80 -2.73E-02 6.75E-01 miss + Eu-155 45.30 1. 31 -3.62E-01 7.64E-02 3.32E+OO miss 60.01 1. 22 -5.35E-01 4.07E+OO miss 86.55

• 30.70 6.26E-02 8.27E-02 miss 105.31 21.10 3.03E-02 7.64E-02 miss + Tl-208 583.19

• 85.00 7.26E-02 2.olE-02 2.61E-02 miss + Bi-211 351.07

• 13.02 6.56E-01 l.41E-01 l.41E-Ol miss 5/5/2016 8:57:02AM Page 7 of8 Analysis Report for 05-May-16-10002 L3-10220C-FRGS-013SS (DRIED) Nuclide E;;e;gy Yield(%} Activity Nuclide ,.'1DA Lim;MDA Coinc Name (keV} (pCi/grams) (pCilgrams) (pCi/grams)

Corr + Pb-211 404.85 3.78 -4.66E-02 3.24E-01 3.24E-01 miss 427.09 1. 76 4.81E-01 8.48E-01 miss 832.01 3.52 2.52E-01 5.44E-01 miss + Bi-212 39.86 1. 06 -1.04E+OO 3.22E-01 3.96E+OO miss 727.33 6.67 1. 56E-01 3.22E-01 miss 785.37 1.10 1.08E+OO l.99E+OO miss 1620.50 1. 47 l.50E-01 9.67E-01 miss + Pb-212 115.18 0.60 -3.81E-01 3.50E-02 2.33E+OO miss 238.63

• 43.60 2.32E-01 3.SOE-02 miss 300.09 3.30 2.82E-01 4.91E-Ol miss + Pb212-XR 7 4.82

• 10.28 5.64E-01 1. 96E-01 3.38E-01 miss 77.11

• 17.10 4.47E-01 l.96E-01 miss 87.35

• 3.97 4.84E-01 6.39E-01 miss 89.78 1. 46 7.28E-01 1.43E+OO miss + Bi-214 609.32

• 45.49 2.29E-01 4. llE-02 4.llE-02 miss 768.36 4.89 8.07E-02 3.44E-01 miss 806.18 1. 26 -l.12E-01 1.22E+OO miss 934.06 3.11 l.98E-01 6.19E-01 miss 1120.29

• 14.92 1.99E-01 1.47E-01 miss 1155.21 1. 63 5.88E-01 1.56E+OO miss 1238.12

• 5.83 1.87E-01 3.BSE-01 miss 1280.98 1. 43 2.65E-01 l.35E+OO miss 1377. 67 3.99 2.93E-02 3.84E-01 miss 1385. 31 0.79 5. 91E-01 1.78E+OO miss 1401.52 1. 33 -6.77E-02 1.25E+OO miss 14 0 7.99 2.39 5. 51E-Ol 9.97E-01 miss 1509.21 2.13 2.lOE-01 8.28E-01 miss 1661. 27 1. 05 3.28E-01 1.69E+OO miss 1729.59 2.88 2.95E-01 7.25E-01 miss 1764.49

• 15.30 2.28E-01 8.84E-02 miss 1847.43 2.03 8.76E-01 1.40E+OO miss > 2118.51 1.16 O.OOE+OO 0.00E+OO miss + Pb-214 241.99

• 7.25 2.97E-01 5.14E-02 2.31E-Ol miss 295.22

• 18.42 2.85E-01 8.19E-02 miss 351.93

• 35.60 2.40E-Ol 5.14E-02 miss 785.96 1. 06 8.73E-01 1.97E+OO miss Pb214-XR 74.82

• 5.80 l.OOE+OO 3.46E-01 5.99E-01 miss 77 .11

• 9.70 7.88E-01 3. 46E-01 miss 87.35

• 2.24 8.58E-01 1.13E+OO miss 89.78 0.82 1.30E+OO 2.55E+OO miss + Ra-226 186.21 3.64 3.lSE-01 4.03E-01 4.03E-01 miss + Ac-228 129.07 2.42 2.76E-01 7.97E-02 5. 71E-01 miss 209.25

• 3.89 2.36E-01 3.18E-Dl miss 270. 24 3.46 4.49E-01 4.75E-Ol miss 328.00 2.95 3.32E-01 5.95E-01 miss 338.32

• 11. 27 2.85E-01 1.47E-01 miss 409.46 1. 92 2.68E-01 8.40E-01 miss 463.00 4.40 l.20E-01 3.48E-01 miss 794.95 4.25 l.OSE-01 4.27E-01 miss 911.20

• 25.80 2.20E-01 7.97E-02 miss 964. 77 4.99 1.09E-01 4.62E-01 miss 5/5/2016 8:57:02AM Page 8 of8 Analysis Report for 05-May-16-1 0002 L3-10220C-FRGS-013SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCi/grams) (pCi!grams)

Corr Ac-228 968. 97

• 15.80 2.36E-01 7.9,E-02 1.19E-01 miss 1588.20 3.22 2.64E-01 7.04E-01 miss + Pa-231 27.36 10.30 O.OOE+OO 3.52E-02 3.52E-02 miss 283.69 1. 70 -2. 89E-02 7.20E-01 miss 300.07 2.47 3. 77E-01 6.55E-01 miss 302.65 2.20 -9.48E-02 5.88E-01 miss 330.06 1. 40 -1.65E-01 9.90E-Ol miss + Th-234 92.38 2 .13 1.18E+OO 1.14E+OO .:.14E+OO miss 92.80

• 2.10 1. 07E+OO 1.34E+OO miss 112. 81 0.21 -2.36E+OO 7.06E+OO miss + 0-235 143.76 10.96 -3.63E-02 2.63E-02 l.03E-01 miss 163.33 5.08 3.44E-02 2.53E-01 miss 185.71 57.20 2.46E-02 2. 63E-02 miss 202 .11 1. 08 -2.41E-01 1.03E+OO miss 205.31 5.01 6.83E-03 2.lSE-01 miss + Am-241 59.54 35.90 -2.90E-03 1.48E-01 1.48E-Ol miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

120--110-100-90 80 70 tn ,1,-1 i:: ::::, 0 60 u 50 "" X 'c< "'x 40 X ' ::::, ;,; 30 ...... ' I-20 10 0 7 .D 1000 2000 3000 0000014847.CNF 4000 channel 5000 Live Time :1800.000 sec Real Time :1801.340 sec Start: 1: -0. 2(kev) stop : 8192: 2047 .4(kev) Acq. start :Thu May 05 08: 19: 53 2016 6000 7000 8000 5/5/2016 8:58:07AM

~~,~pex-Gamma Analysis Report for 05-May-16-10003 L3-10220C-FRGS-014SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 05-May-16-1 0003 : L3-10220C-FRGS-014SS (DRIED) : 1 L 130G Soil Sample 1.828E+03 grams : Default : 5/3/2016 8:16:00AM

5/5/2016 8:20:06AM

130G 1 L Sand Sam pie : JWelch : P40818B : 130G Sand : 1800.0 seconds : 1803.0 seconds : 0.17 % : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 14848 PEAK WITH NJD REPORT Peak Analysis Performed on : 5/5/2016 8:57:32AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.N LB : 1.000FWHM Page 1 of8 5/5/2016 8:58:07AM Page 3 of8 Analysis Report for 05-May-16-1 0003 L3-10220C-FRGS-014SS (DRIED) Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCi!grams)

Uncertainty Corr Bi-214 0.99 806.18 1. 26 934.06 3.11 1120.29

• 14.92 l.94E-0 1 l.06E-01 miss 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1 407.99 2.39 1 509.21 2 .13 1661.27 1. 05 1729.59 2.88 1764.49

• 15.30 l.75E-O l 8.77E-02 miss 1847.43 2.03 2118.51 1.16 Pb-214 1. 00 241.99 7.25 295.22

• 18.42 2.57E-0 l 9.25E-02 miss 351.93

• 35.60 2.68E-Ol 6.37E-02 miss 785. 96 1. 06 Pb214-XR 1. 00 74.82

• 5.80 5.16E-01 6.61E-01 miss 77 .11 9.70 87.35 2.24 89.78 0.82 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32

• 11. 27 2.88E-Ol 1.15E-01 miss 409.46 1. 92 463.00 4.40 794.95 4.25 911. 20

• 25.80 2.88E-01 8.12E-02 miss 964. 77 4.99 968. 97

• 15.80 1.98E-01 l.16E-01 miss 1 588.20 3.22 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

5/5/2016 8:58:07AM Page 4 of8 Analysis Report for 05-May-16-10003 L3-10220C-FRGS-014SS (DRIED) INTERFERENCE CORRECTED REPORT Nuclide Name Nuclide Id Confidence Wt mean Activity Wt mean Comments X ? ? ? = X = @ = K-40 Cs-137 Tl-208 Bi-211 Pb-212 Pb212-XR Bi-214 Pb-214 Pb214-XR Ac-228 0. 996 1. 000 1. 000 0.957 1. 000 1. 000 0.999 1.000 1.000 0.998 nuclide is part of an undetermined solution nuclide rejected by the interference analysis Activity (pCilgrams)

Uncertainty 5.47E+OO 6.92E-01 1. 90E-02 C..::: ~,ct\ 1. 37E-02 7.39E-02 \J.l,. 2.19E-02 2.18E-Ol 5.40E-02 2.91E-Ol 3.72E-01 2.00E-01 3.96E-02 2.64E-01 5.25E-02 5.16E-01 6.61E-01 2.66E-01 5.76E-02 nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 5/5/2016 8:58:07AM Analysis Report for 05-May-16-10003

+ + + + +

+ + + + L3-10220C-FR GS-014SS (DRIED) Peak Locate Performed on Peak Locate From Channe l Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 5/5/2016 8:57:32AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C: \Can berra\Apex\Root\Default\Li brary\ZI ON LIB-BN L. N LB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

K-40 1460.82

• 10.66 5.47E+OO l.61E-01 1.61E-01 Cr-51 320.08 9. 91 1.74E-02 1. 48E-Ol l.48E-01 Mn-54 834.85 99.98 4.71E-03 2.03E-02 2.03E-02 Co-58 810.76 99.45 -8.07E-03

1. 31E-02 1.31E-02 1674.73 0.52 5.60E-01 3.16E+OO Co-60 1173.23 99.85 3.37E-03 1.78E-02 2.14E-02 1332.49 99.98 3.53E-03 l.78E-02 Nb-94 702.65 99.81 4.59E-03 1. 54E-02 l.77E-02 871.09 99.89 1.04E-03 1.54E-02 Ag-108m 79.13 6.60 1.74E-02 l.62E-02 5.86E-01 433.94 90.50 2.22E-03 1.62E-02 614.28 89.80 1.lOE-02 2.04E-02 722. 94 90.80 -5.0SE-03

1. 71E-02 Sn-113 255.13 2. 11 2.57E-01 1.68E-02 7.57E-01 3 91. 70 64.97 -1.17E-02 1.68E-02 Cs-134 475.36 1. 48 1. llE-01 1.80E-02 9.90E-01 563.25 8.34 6.00E-02 2.17E-01 569.33 15.37 2.38E-02 1. llE-01 604.72 97. 62 6.41E-03 1.BOE-02 Page 5 of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 5/5/2016 8:58:07AM Page 6 of8 Analysis Report for 05-M ay-16-10003 L3-10220C-FRGS-014SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCi!grams)

Corr Cs-134 795.86 85.46 -7.78E-04 1.80E-02 2.20E-02 miss 801.95 8.69 -1.02E-02 l.97E-01 miss 1038.61 0.99 -3.06E-01 1.82E+OO miss 1167. 97 1. 79 -3.05E-01 1.0SE+OO miss 1365.19 3.02 2.59E-02 6.33E-01 miss + Cs-137 661.66

• 85.10 l.90E-02 2.03E-02 2.03E-02 miss + Eu-152 121.78 28.67 l.87E-02 4.69E-02 5. 67E-02 miss 244.70 7.61 -4.52E-03 2.06E-01 miss 295.94 0.45 6.43E+OO 5.lOE+OO miss 344.28 26.60 -2.82E-02 4.69E-02 miss 367.79 0.86 -1.97E-01 1.49E+OO miss 411.12 2.24 -4.91E-02 6.21E-01 miss 443. 96 2.83 -2.24E-01 4.15E-01 miss 488.68 0.42 -2.02E+OO 2.99E+OO miss 563.99 0.49 3.38E+OO 3.89E+OO miss 586.26 0.46 -5.28E-01 3.32E+OO miss 678.62 0.47 2.53E-02 2. 96E+OO miss 688.67 0.86 8.58E-02 l.89E+OO miss 719.35 0.28 -8.26E-01 6.00E+OO miss 778. 90 12. 96 3.54E-02 1.33E-01 miss 810.45 0.32 -8.55E-01 4.73E+OO miss 867.37 4.26 3.46E-02 4.llE-01 miss 919.33 0.43 2.12E+OO 4.13E+OO miss 964.08 14.65 2. llE-02 l.55E-01 miss 1085.87 10.24 4.47E-02 l.93E-01 miss 1089.74 1. 73 -l.17E-01

9. 91E-01 miss 1112.07 13. 69 1. 54E-02 1.42E-01 miss 1212.95 1. 43 2.12E-02 l.66E+OO miss 1249.94 0.19 -2.50E+OO 1.07E+Ol miss 1299.14 1. 63 2.19E-01 1.41E+OO miss 1408.01 21.07 5.65E-02 l.15E-01 miss 1457.64 0.50 -2.77E+OO 7.32E+OO miss 1528.10 0.28 -3.16E-01 4.76E+OO miss + Eu-154 123.07 40.40 7.64E-03 3.93E-02 3.93E-02 miss 247.93 6.89 -2.74E-02 2.18E-01 miss 591. 76 4.95 -4.84E-03

2. 96E-01 miss 692.42 1. 78 5.45E-01 1.14E+OO miss 723.30 20.06 -2.88E-02 7.73E-02 miss 756.80 4.52 1.62E-01 4.43E-01 miss 873.18 12.08 -4.09E-02 1.05E-01 miss 996.29 10.48 1. 03E-03 l.54E-Ol miss 1004.76 18.01 -1.21E-03 9.03E-02 miss 1274.43 34.80 -2.46E-02 5.46E-02 miss 1596.48 1. 80 -1.44E-01 7.73E-01 miss + Eu-155 45.30 1. 31 4.75E+OO 9 , 96E-02 1.07E+Ol miss 60.01 1. 22 -1.40E+OO 1.08E+Ol miss £'6.55 30.70 -1.66E-02 1.07E-01 miss 105.31 21.10 6.61E-03 9. 9oE-02 miss + Tl-208 583.19

• 85.00 7.39E-02 2.38E-02 2.38E-02 miss + Bi-211 351.07

• 13. 02 7.33E-01 1. 40E-01 1. 40E-01 miss + Pb-211 404.85 3.78 1.27E-01 4.28E-01 4.28E-01 miss 5/5/2016 8:58:0?AM Page 7 of8 Analysis Report for 05-May-16-1 0003 L3-10220C-FRGS-014SS (DRIED) Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 2.80E-01 4.28E-01 9.31E-01 miss 832.01 3.52 4.5 1 E-02 4. 97E-01 miss + Bi-212 39.86 1. 06 -7.95E+OO 2.53E-01 9.89E+OO miss 727.33 6.67 2.19E-02 2.53E-01 miss 785.37 1.10 1.21E-01 1. 69E+OO miss 1620.50 1. 47 5.70E-01 l.33E+OO miss + Pb-212 115 .18 0.60 8.56E-01 5.32E-02 3.19E+OO miss 238.63

• 43.60 2.18E-01 5.32E-02 miss 300.09 3.30 3.79E-01 5.09E-01 miss + Pb212-i~R 74.82

• 10.28 2.91E-01 3.43E-01 6.04E-01 miss 77 .11 17.10 4.02E-01 3.43E-01 miss 87.35 3.97 5.93E-01 8.53E-01 miss 89.78 1. 46 4.63E-01 1.86E+OO miss + Bi-21 4 609.32

• 45.49 2.09E-01 4.21E-02 4.21E-02 miss 768.36 4.89 -5.62E-02 3.74E-01 miss 806.18 1. 26 -2.03E-01 1.36E+OO miss 934.06 3 .11 -4.77E-02 5.57E-01 miss 1120.29

• 14.92 1.94E-01 1.42E-01 miss 1155.21 1. 63 2.74E-01 1.44E+OO miss 1238.12 5.83 2.08E-01 4. 93E-01 miss 1280.98 1. 43 3.03E-01 1.53E+OO miss 1377.67 3.99 2.33E-01 5.BlE-01 miss 1385. 31 0.79 1.21E+OO 2.75E+OO miss 1401.52 1. 33 -1.13E-01 1.39E+OO miss 1407.99 2.39 4.97E-01 1.0lE+OO miss 1509.21 2 .13 4.37E-01 1.0lE+OO miss 1661. 27 1. 05 1.06E-02 1.37E+OO miss 1729.59 2.88 4.76E-01 8.30E-01 miss 1764.49

• 15.30 1. 7 5E-01 7.95E-02 miss 1847.43 2.03 7.96E-02 9.98E-01 miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 2.09E-01 5.12E-02 2. 71E-01 miss 295.22

• 18.42 2.57E-01 1.18E-01 miss 351.93

• 35.60 2.68E-01 5.12E-02 miss 785.96 1. 06 1.82E-01 1. 71E+OO miss + Pb214-XR 74.82

• 5.80 5.16E-01 6.04E-01 1.07E+OO miss 77 .11 9.70 7.09E-01 6.04E-01 miss 87.35 2.24 1. 05E+OO 1.51E+OO miss 89.7(3 0.82 8.24E-01 3.32E+OO miss + Ra-226 186.21 3.64 5.23E-01 5.02E-01 5.02E-01 m i ss + Ac-228 129.07 2.42 1.41E-01 8.40E-02 7.40E-01 miss 209.25 3.89 2.17E-01 4.08E-01 miss 270.24 3.46 1.64E-01 5.16E-01 miss 328.00 2.95 4.95E-01 6.15E-01 miss 33 8.32

• 11. 27 2.88E-01 1.43E-01 miss 409.46 1. 92 7.36E-02 7.33E-01 miss 463.00 4.40 2.74E-01 4.34E-01 miss 794.95 4.25 2.28E-01 5.12E-01 miss 911. 20

• 25.80 2.88E-01 8.40E-02 miss 964.77 4.99 1.39E-Ol 4.64E-Ol miss 968.97

• 15.80 1.98E-01 1.68E-Ol miss 5/5/2016 8:58:07AM Page 8 of8 Analysis Report for 05-May-16-10003 L3-10220C-FRGS-014SS (DRIED) Nuclide Energy Yield(%) Activif1/

NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCi!grams) (pCilgrams)

Corr Ac-228 1588.20 3.22 2.SOE-01 8.40E-02 6.33E-01 miss + Pa-231 27.36 10.30 2.59E-03 5.31E-01 1.21E+OO miss 283.69 1. 70 -9.04E-02

8. 99E-01 miss 300.07 2.47 5.06E-01 6.80E-01 miss 302.65 2.20 -4.76E-01 5.31E-01 miss 330.06 1. 40 -7.38E-01 9.BlE-01 miss + Th-234 92.38 2 .13 9.33E-Ol 1.47E+OO l.47E+OO miss 92.80 2.10 l.08E+OO 1.48E+OO miss 112. 81 0 .21 5.56E+OO 1.03E+Ol miss + U-235 143.76 10. 96 5.69E-02 3.19E-02 1.49E-01 miss 163.33 5.08 3.32E-02 2.86E-Ol miss 185.71 57.20 2.65E-02 3.19E-02 miss 202 .11 1. 08 -7.44E-02 l.28E+OO miss 205.31 5.01 1.59E-01 2.85E-01 miss + Am-241 59. 54 35.90 l.SSE-01 3.88 E-01 3.88E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Vl .µ C: =i 120 110 100 90 80 70 8 60 50 40 30 20 10 1000 2000 3000 0000014848 .CNF 4000 channel 5000 Live Time :1800.000 sec Real Time :1803.010 sec Start: 1: -0. l(kev) Stop : 8192: 2047. O(kev) Acq. start :Thu May 05 08: 20: 06 2016 c:, ! 6000 7000 8000 6/2/2016 12:57:50PM

~§~pex-Gamma Analysis Report for 02-Jun-16-10007 L3-10220C-FJGS-015SS (DRIED) GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real Time Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 02-Jun-16-10007

' L3-10220C-FJGS-015SS (DRIED) Off Site Sample 1.151 E+03 grams Default : 5/23/2016 4:10:00PM

6/2/2016 12:47:11 PM : 130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 600.0 seconds : 600.5 seconds : 0.08% : 2.80 : 120

• 8192 : 120

• 8192 : 1.000FWHM

1/27/2016

6/28/2012

15055 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 12:57:17PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of8 6/2/2016 12:57:SOPM Page 2 of8 Analysis Report for 02-Jun-16-10007 L3-10220C-FJGS-015SS (DRIED) Peak Energy ROI No. (keV) start 1 76.84 305 -2 238.57 948 -3 338.36 1348 -4 352.00 1400 -5 582.90 2326 -6 609.32 2429 -7 661.55 2639 -8 911. 39 3640 -9 1460.70 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 314 308.57 961 954.58 1359 1353. 30 1412 1407.78 2335 2330.61 2441 2436.20 2652 2645.02 3650 3644.08 5851 5842.12 Net Peak NetArea Continuum Area Uncertainty Counts 3. 96E+Ol 22.80 6.68E+Ol 4.68E+Ol 25.63 8.23E+Ol 1.70E+Ol 1 4.29 2.80E+Ol 4.78E+Ol 1 7.74 2.64E+Ol 2.31E+Ol 1 2.16 1. 39E+Ol 3.91E+Ol 13.88 7.83E+OO 5.26E+Ol 1 6.70 1.48E+Ol l.63E+Ol 9.70 7.33E+OO l.14E+02 22.22 '.3. 03E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.82

• 10.66 5.47E+OO 1.17E+OO Cs-137 0.99 661.66

• 85.10 l.85E-01 6.28E-02 Tl-208 0.99 583.19

• 85.00 7.44E-02 4.02E-02 Bi-211 0.94 351.07

• 13.02 7.06E-01 2.86E-01 Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 1. 59E-01 9.09E-02 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77 .11

• 17.10 6.24E-01 3.81E-01 87.35 3.97 89.78 1. 46 Bi-214 1. 00 609.32

• 45.49 2.43E-01 S. llE-02 768.36 4.89 806.18 1.26 934.06 3 .11 1120.29 14.92 1155. 21 1. 63 Tentative Nuclide Pb214-XR Pb212-XR Pb-212 Ac-228 Pb-214 Bi-2 11 Tl-208 Bi-214 Cs-137 Ac-228 K-40 Coinc Corr miss miss miss miss mi3S miss miss Analysis Report for 02-Jun-16-10007 L3-10220C-FJGS-015SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1238.12 1280.98 1377.67 1385. 31 1401.52 1407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118. 51 Pb-214 1. 00 241.99 295.22 351.93 785.96 Pb214-XR 0.99 74.82 77 .11 87.35 89.78 Ac-228 0.99 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911.20 964. 77 968. 97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWH M Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 5.83 1. 43 3.99 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 5.80 9.70 2.24 0.82 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 12:57:50PM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 2.58E-0 1 1. 04E-01 miss l.lOE+OO 6.80E-01 mi ss 2.83E-0 1. 2.42E-Ol miss 2.35E-01 1. 41E-01 miss INTERFERENCE CORRECTED REPORT Analysis Report for 02-Jun-16-10007

? ? ? ? L3-10220C-FJGS-015SS (DRIED) Nuclide Name K-40 Cs-137 Tl-208 Bi-211 Pb-212 Pb212-XR Bi-214 Pb-214 Pb214-XR Ac-228 Nuclide Id Confidence 0.999 0.999 0.995 0.948 1. 000 0.998 1. 000 1.000 0.998 0.999 ? " nuclide is part of an undetermined solution X " nuclide rejected by the interference analysis 6/2/2016 12:57:50PM Wt mean Wt mean Activity Activity (pCi/grams)

Uncertainty 5.4':"E+OO 1.1 7E+OO 1.85E-Ol 6.28E-02 7.44E-02 4.02E-02 7.06E-01 2.86E-01 1. 59E-01 9.09E-02 6.24E-01 3.BlE-01 2.43E-01 9. llE-02 2.58E-01 1. 04E-01 l.lO E+OO 6.SOE-01 2.47E-01 1.22E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Page4 of8 Comments 6/2/2016 12:57:50PM Analysis Report for 02-Jun-16-10007

+ + + + + + + + + L3-10220C-FJGS-015SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy {ke VJ All peaks were identified.

M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 12:57:17PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canb erra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCUgrams) (pCi/grams)

K-40 1460.82

• 10.66 5.47E+OO 6.15E-01 6.15E-01 Cr-51 320.08 9.9 1 9.90E-02 4.06E-01 4.06E-01 Mn-54 834.85 99.98 2.78E-03 3.85E-02 3.85E-02 Co-53 810.76 99.45 O.OOE+OO 1.03E-02 1.03E-02 1674.73 0.52 O.OOE+OO 3.27E+OO Co-6 0 1173.23 99.85 l.78 E-02 1.30E-02 6.62E-02 1332.49 99.9 8 O.OOE+OO 1.30E-02 Nb-94 702.65 99.81 1.41E-02 2.65E-02 5.20E-0 2 871.09 99.89 -7.80 E-03 2.65E-02 Ag-108m 79 .13 6.60 2.32E-01 2.94E-02 9.94E-01 433.9 4 90.50 1.18 E-03 3.23E-0 2 614.28 89.80 -6.33E-03 2.9 4 E-0 2 722. 94 90.8 0 4.0 8E-0 3 3.76E-02 Sn-113 255 .13 2 .11 -3.27E-01 4.79E-0 2 1.24E+OO 391.7 0 64. 97 -6.79E-0 3 4.79E-02 Cs-134 475.36 1. 48 -1.77E+O O 3.49E-02 l.95E+OO 563.25 8.34 -2.16E-0 1 3.89E-01 569.33 15.37 9.99E-02 3.08E-01 6 04.7 2 97. 62 2.33E-03 3.49E-02 Page 5 of8 Tolerance Nuclide Caine Corr miss free miss miss mi ss miss miss m iss miss miss miss miss miss free free miss miss miss miss 6/2/2016 12:57:50PM Page 6 of8 Analysis Report for 02-Jun-16-10007 L3-10220C-FJGS-015SS (DRIED) Nuclide Energy Yield{°./o)

Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi!grams) (pCi/grams)

Corr Cs-134 795.86 85. 4 6 9.33E-03 3.49E-02 5.64E-02 miss 801.95 8.69 -9.55E-02 3.67E-01 miss 1038.6 1 0.99 -1.03E+OO 3.04E+OO miss 1167. 97 1. 79 -6.69E-01 1.82E+OO miss 1365.19 3.02 2.14E-Ol 2 .13E+OO miss + Cs-137 661.66

• 85.10 l.85E-Ol 5.74 E-02 5.74E-02 miss + Eu-152 121.78 28.67 3.19E-02 1.0l E-01 l.03E-01 miss 244.70 7.61 -1.43E-02 3.lSE-01 miss 295.94 0.45 5.18E+OO 9.94E+OO miss 344.28 26.60 -2.62E-03 l.OlE-01 miss 367.79 0.86 -2.15E-01 3.25E+OO miss 411.12 2.24 2.59E-01 1.45E+OO miss 443. 96 2.83 -l.18E-Ol 8.64E-01 miss 488.68 0.42 l.85E+OO 8.68E+OO miss 563.99 0.49 -l.24E+OO

7. 71E+OO miss 586.26 0.46 -3.48E+OO 7.20E+OO miss 678.62 0.47 -4.30E-01 6.95E+OO miss 689.67 0.86 -l.19E+OO 4.30E+OO miss 719.35 0.28 1.77E+OO l.22E+Ol miss 778. 9 0 12. 96 2.04E-02 3.lOE-01 miss 810.45 0.32 2.14E+OO 9.93E+OO miss 867.37 4.26 -1.26E-01 7.83E-01 miss 919.33 0.43 1.89E+OO l.05E+Ol miss 964.08 14.65 1. 41E-01 4.40E-01 miss 1085.8 7 10.24 l.55E-01 5.35E-01 miss 1089.74 1. 73 5.19E-Ol 2.91E+OO miss 1112.07 13. 69 8.86E-03 3. 72E-01 miss 1212.95 1. 43 -5.40E-01 2.92E+OO miss 1249.94 0.19 -1.62E+OO 2.61E+Ol miss 1 299.1 4 1. 63 O.OOE+OO 7.83E-01 miss 1408.01 21. 07 -5.74E-02 l.74E-01 miss 1457.64 0.50 -l.15E+Ol l.61E+Ol miss 1528.10 0.28 O.OOE+OO *s.09E+OO miss + Eu-154 123.07 40.40 -l.68E-02 7.12E-02 7.12E-02 miss 247.93 6.89 l.32E-01 4.17E-01 miss 591.76 4.95 4. llE-02 6.04E-01 miss 692.42 1. 78 -5.94E-01 l.61E+OO miss 723.30 20.06 1. 76E-02 1. 71E-01 miss 756.8 0 4.52 -2.12E-01

8. 72E-01 miss 873.18 12.08 2.99E-02 3.22E-01 miss 996.29 10.48 -4.40E-02 2.78E-Ol miss 1004.76 18.01 4.78E-02 2.65E-01 miss 1274.43 34.80 1.43E-02 l.24E-01 miss 1596. 48 1. 80 6.50E-01 3.29E+OO miss + Eu-155 45.30 1. 31 -8.74E-01

1. 51E-01 7.40E+OO miss 60.01 1. 22 6.76E+OO 1.23E+Ol miss 86.55 30.70 2.90E-02 l.75E-01 miss 105.31 21.10 -6.47E-03 l.51E-Ol miss + Tl-208 583.19

• 85.00 7.44E-02 4.83E-02 4.83E-02 miss + Bi-211 351.07

• 13.02 7.06E-01 3.lOE-01 3.lOE-01 miss + Pb-211 404.85 3.78 l.03E-01 8.93E-01 8.93E-01 miss 6/2/2016 12:57:50PM Page 7 of8 Analysis Report for 02-Jun-16-10007 L3-10220C-FJGS-015SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCi/grams) (pCilgrams)

Corr Pb-211 427.09 1. 76 1. 84E-01 8.93E-01 1.77E+OO miss 832.01 3.52 5.78E-02 l.19E+OO miss + Bi-212 39.86 1. 06 2. 96E+OO 5.74E-01 1. 08E+Ol miss 727. 33 6.67 4.78E-02 5.74E-01 miss 785.37 1.10 -4.06E-01 2.83E+OO miss 1620.50 1. 47 O.OOE+OO 1.02E+OO miss + Pb-212 115 .18 0.60 1.69E+OO 1. 30E-01 5.62E+OO miss 238.63

• 43.60 l.59E-01 1.30E-01 miss 300.09 3.30 -l.83E-01 9.12E-01 miss + Pb212-XR 74.82 10.28 7.15E-01 5.35E-01 9.28E-01 miss 77 .11

• 17.10 6.24E-01 5.35E-01 miss 87.35 3.97 l .13E-01 1.27E+OO miss 89.78 1. 46 5.22E-01 3.15E+OO miss + Bi-214 609.32

• 45.49 2.43E-01 7.84E-02 7.84E-02 miss 768.36 4.89 2.25E-02 8. llE-01 miss 806.18 1. 26 2.93E-01 3.24E+OO miss 934.06 3 .11 4.31E-01 l.93E+OO miss 1120.29 14.92 6.81E-02 4.97E-01 miss 1155.21 1. 63 -6.84E-01 2.86E+OO miss 1238.12 5.83 2.88E-Ol l.17E+OO miss 1280.98 1. 43 1.30E+OO 3.89E+OO miss 1377.67 3.99 3.86E-D1 l.61E+D0 miss 1385. 31 0.79 1.15E+D0 5.76E+D0 miss 1401. 52 1. 33 -2.13E-01 3.46E+OO miss 1407.99 2.39 -5.05E-01 1.53E+OO n1iss 1509.21 2.13 1. 06E-Ol 1. 81E+OO miss 1661.27 1. 05 O.OOE+OO 1.46E+OO miss 1729.59 2.88 O.OOE+OO 5.48E-01 miss 1764.49 15.30 2.71E-01 5.81E-01 miss 1847.43 2.03 O.OOE+OO 8.14E-01 miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 3.23E-01 l.13 E-D1 5.46E-01 miss 295.22 18.42 2.79E-01 2.84E-01 miss 351.93

• 35.60 2.58E-Ol 1.13E-01 miss 785.96 1. 06 8.18E-01 3.80E+OO miss + Pb214-XR 74.82 5.80 l.27E+OO 9.44E-D1 1.65E+OO miss 77.11

• 9.70 1.lOE+OO 9.44E-01 miss 87.35 2.24 2.0lE-01 2.26E+OO miss 89.78 0.82 9.29E-01 5.61E+OO miss + Ra-226 186.21 3.64 l.88E-01 9.43E-01 9.43E-D1 miss + Ac-228 129.07 2.42 3.42E-01 l.66E-01 1.26E+OO miss 209.25 3.89 l.06E-01 7.78E-01 miss 270.24 3.46 2.51E-01 1.lOE+OO miss 328.00 2.95 l.24E-01 1.13E+OO miss 338.32

• 11. 27 2.83E-01 3.64E-01 miss 409.46 1. 92 -2.14E-01 l.68E+OO miss 463.00 4.40 6.16E-01 1. 07E+OO miss 794.95 4.25 2.52E-01 1.12E+D0 miss 911. 20

• 25.80 2.35E-01 1.66E-01 miss 964.77 4.99 5.44E-01 l.35E+OO miss 968.97 15.80 3.28E-01 5.22E-01 miss 6/2/2016 12:57:50PM Page 8 of8 Analysis Report for 02-Jun-16-10007 L3-10220C-FJGS-015SS (DRIED) Nuclide Energy Yield{°/o)

Activity Nuc/ideMDA LineMDA Caine Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr Ac-228 1588.20 3.22 -7.27E-02 l.66E-01 l.57E+OO miss + Pa-231 27.36 10.30 O.OOE+OO l.60E-01 1.60E-01 miss 283.69 1. 70 4.90E-02 1.38E+OO miss 300.07 2.47 -2.45E-01 1.22E+OO miss 302.65 2.20 -l.19E-01 1.49E+OO miss 330.06 1. 40 3.18E-Ol 2.48E+OO miss + Th-234 92.38 2.13 5.65E-01 3. l7 E+OO 3.17E+OO miss 92.80 2.10 7.92E-01 3.25E+OO miss 112. 81 0.21 -2.20E-01 l.87E+Ol miss + U-235 143.76 10. 96 -2.67E-02 6.39E-02 2. 72E-01 miss 163.33 5.08 -2.02E-Ol 5.04E-01 miss 185.71 57.20 3.90E-02 6.39E-02 miss 202 .11 1. 08 6.74E-01 2. 9GE+OO miss 205.31 5.01 1. lOE-01 .5.SOE-01 miss + Am-241 59.54 35.90 5.63E-03 3.88E-01 3.88E-01 miss + = Nuclide identified during the nuclide identification

• ;, Energy line found in the spectrum > -MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 V1 ,I-' C: :::::s 8 30 25 "" >;< ... 20 "" >;< "' ;;j ..D 0.. 15 10 5 0 1000 2000 3000 0000015055.CNF 4000 channel 5000 Live Time :600.000 sec Real Time :600.500 sec start: 1: -0. 2 (kev) stop : 8192 :2047.4(kev)

Acq. Start :Thu Jun 02 12:47:11 2016 6000 7000 8000 6/2/2016 12:58:27PM Analysis Report for 02-Jun-16-10008 L3-10220C-FJGS-016SS (DRIED) GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 02-J un-16-1 0008 : L3-10220C-FJGS-016SS (DRIED) : Off Site Sample 1.362E+03 grams Default 5/23/2016 4:15:00PM 6/2/2016 12:47:18PM 130G 1 L Soil Sample JWelch ; P40818B

• 130G Soil

• 600.0 seconds ; 601.0 seconds ; 0.17% ; 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15056 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 12:57:56PM Peak Analysis From Channel Peak Analysis To Chann el : 120 : 8192 Tentative NID Library Peak Match Tolerance

C: \C a nberra\Apex\Root\Defau lt\Library\Zion Lib-B NL. N LB : 1.000FWHM Pager of8 6/2/2016 12:58:27PM Page 2 of8 Analysis Report fer 02-Ju n-16-1 0008 L3-10220C-FJGS-016SS (DRIED) Peak Energy ROI No. (keV) start 1 238.70 947 -2 295.06 1175 -3 351.92 1403 -4 511. 07 2039 -5 583.09 2325 -6 608.90 2430 -7 910.92 3638 -8 1460.81 5834 -9 1764.04 7052 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 960 955.28 1188 1180. 57 1416 1407.88 2049 2044.15 2339 2332.12 2444 2435.37 3649 3643.37 5854 5844.20 7065 7058.57 Net Peak NetArea Continuum Area Uncertainty Counts 9.47E+Ol 30. 53 1.01E+02 4.25E+Ol 21. 09 4.90E+Ol 6.67E+Ol 20.98 3.47E+Ol 2.27E+Ol 1 2.7 6 1.67E+Ol 4.15E+Ol :i.5.53 1.50E+Ol 5. 78E+Ol 1 8.72 2.24E+Ol 3.33E+Ol ::;_2. 47 5.50E+OO 1. 36E+02 23.93 5.75E+OO 1.80E+Ol 8.94 1.91E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 1. 00 1460.82

• 10.66 6 .13E+OO l.20E+OO Tl-208 0.99 583.19

• 85.00 l.25E-01 4.93E-02 Pb-212 1. 00 115.18 0.60 238.63

• 43.60 3.07E-01 1. llE-01 300.09 3.30 Bi-214 0.99 609.32

• 45.49 3.36E-01 1.16E-01 768.36 4.89 806.18 1. 26 934.06 3 .11 1120.29 14. 92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 Tentative Nuclide Pb-212 Pb-21 4 Eu-152 Pb-2U Bi-211 Tl-208 Bi-214 Ac-228 K-40 Bi-214 Coinc Corr miss miss miss miss Analysis Report fer 02-Jun-16-10008 L3-10220C-FJGS-016SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118.51 Pb-214 1. 00 241.99 295.22 351.93 785. 96 Ac-228 0.99 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911. 20 964. 77 968.97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2.13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 12:58:27PM P a ge 3 of8 Activity Activity Caine (pCilgrams)

Uncertainty Corr 6.56E-O l 3.29E-01 m iss 3.73E-0 1 1.94E-01 m iss 3.38E-01 1.1 9E-01 m iss 4.48E-01 l.73E-01 m iss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1. 000 6 .13E+OO 1.20E+OO Tl-208 0.999 1.25E-01 4.93E-02 Analysis Report for 02-Jun-16-1000A X L3-10220C-FJGS-016SS (DRIED) Nuclide Nuclide Name Id Confidence Bi-211 0.956 Pb-212 1.000 Bi-214 0.994 Pb-214 1.000 Ac-228 0.998 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis 6/2/2016 Wt mean Activity (pCilgrams) 3.0-:'E-01

3. 72E-Ol 3.48E-Ol 4.48E-01 @ "' nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 12:58:27PM Page4 of8 Wt mean Comments Activity Uncertainty l.llE-01 l.lOE-01 1. 02E-01 l.73E-Ol 6/2/2016 12:58:27PM Analysis Report for 02-Jun-16-10008

+ + + + + + + + + L3-10220C-FJGS-016SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 4 511. 07 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAK S : 6/2/2016 12:57:56PM

120 : 8192 Peak CPS {°/o) Peak Size (CPS) Uncertainty 3.77527E-02 28.15 Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LI B-BNL. NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)

K-40 1460.82

• 10.66 6.13E+OO 5.17E-01 5.17E-01 Cr-51 320.08 9.91 O.OOE+OO 4.81E-Ol 4.BlE-01 Nn-54 834.85 99.98 ~.07E-0~ 5.SBE-02 5.58E-02 Co-58 810.76 99.45 -1.48E-02 3.83E-02 3.83E-02 1674.73 0.52 1.84E+OO 1. 22E+Ol Co-60 1173.23 99.85 2.13E-02 5.40E-02 6.56E-02 1332.49 99.98 9.63E-03 5.40E-02 Nb-94 702.65 99.81 -1.78E-02 4.lZE-02 4.12E-02 871.09 99.89 1.35E-03 4.42E-02 Ag-108rn 79.13 6.60 -8.29E-01 3.89E-02 1.31E+OO 433.9 4 90.50 -2.22E-03 4.03E-02 614.28 89.80 -7.36E-03 3.89E-02 722.94 90.80 1.60E-02 5.46E-02 Sn-113 255.13 2.11 -1.30E-01 5.78E-02 1.62E+OO 391.70 64.97 3.0lE-03 5. 78E-02 Cs-134 475.36 1. 48 7.17E-01 3.27E-02 2.87E+OO 563.25 8.34 -7.18E-03 5.SlE-01 569.33 15.37 2.37E-02 2.49E-01 Page 5 of8 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss 6/2/2016 12:58:27PM Page 6 of8 Analysis Report for 02-Jun-16-10008 L3-10220C-FJGS-016SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

Corr Cs-134 604. 72 97.62 -2.59E-03 3.27E-02 3.27E-02 miss '795.86 85.46 5.20E-04 5.28E-02 miss 801.95 8.69 -2.47E-02 3.99E-01 miss 1038.61 0.99 3.16E+OO 6.75E+OO miss 1167.97 1. 79 1. lOE-01 2.49E+OO miss 1365.19 3.02 O.OOE+OO 4.13E-01 miss + Cs-137 661.66 85.10 2.48E-02 6.20E-02 6.20E-02 miss + Eu-152 121. 73 28.67 -6.78E-02 1.15E-01 l.15E-01 miss 244.70 '7. 61 5.86E-02 4.53E-01 miss 295.94 0.45 9.05E+OO l.25E+Ol miss 344.28 26.60 l.16E-02 1. 39E-01 miss 367.79 0.86 7.24E-01 4.36E+OO miss 411.12 2.24 3.48E-Ol l.64E+OO miss 443. 96 2.83 -8.37E-03 l.25E+OO miss 488.68 0.42 l.08E-01 6.51E+OO miss 563.99 0.49 -4.lOE-02 8.92E+OO miss 586.26 0.46 -l.54E+OO 8.91E+OO miss 678.62 0.47 -l.41E+OO 7.93E+OO miss 688.67 0.86 5.87E-01 4.03E+OO miss 719.35 0.28 3.55E-01 l.39E+Ol miss 778.90 12. 96 -l.61E-02 2.60E-01 miss 810.45 0.32 -5.12E+OO l.08E+Ol miss 867.37 4.26 8.77E-02 8.50E-01 miss 919.33 0.43 -1. 91E+OO 7.61E+OO miss 964. 08 14.65 l.09E-01 4.31E-01 miss 1085.87 10.24 2.40E-02 5.02E-01 miss 1089.74 1. 73 -1. 50 E+OO 2.98E+OO miss 1112. 07 13.69 l.38E-01 4. lOE-01 miss 1212.95 1. 43 6.33E-01 3.55E+OO miss 1249.94 0.19 3.90E+OO 2.98E+Ol miss 1299.14 1. 63 O.OOE+OO 2.52E+OO miss 1 408.01 21.07 -9.20E-02 2.06E-01 miss 1457.64 0.50 -1.23E+Ol 1.73E+Ol miss 1528.10 0.28 3.53E+OO l.64E+Ol miss Eu-154 123.07 40.40 -5.~6E-03 9.41E-02 9.41E-02 miss 247.93 6.89 5.BSE-02 4.60E-Ol miss 5 9 1.76 4.95 -1.63E-01 4.88E-01 miss 692.42 1. 78 l.09E-01 2.58E+OO miss 723.30 20.06 7.lBE-02 2.48E-01 miss 756.80 4.52 3.40E-02 9.59E-01 miss 873.18 12.08 -3.50E-03 3.36E-Ol miss 996.29 10.48 -8.84E-02 4.25E-01 miss 1004.76 18.01 -2.41E-02 l.92E-01 miss 1274.43 34.80 1.79E-03 l.16E-Ol miss 1596.48 1. 80 5.38E-01 2.67E+OO miss + Eu-155 45.30 1. 31 -1.99E+Ol 2.3'7E-01 2.29E+Ol miss 60.01 1. 22 -4.39E+OO 2.50E+Ol miss 86.55 30.70 -1. 24E-01 2.37E-01 miss 105.31 21.10 -2.22E-02 2.51E-Ol miss + Tl-208 583.19

• 85.00 1. 25E-01 5.14E-02 5.14E-02 miss + Bi-211 351. 0 7

• 13.02 9.25E-01 3.38E-01 3.38E-01 miss 6/2/2016 12:58:27PM Page 7 of 8 Analysis Report for 02-Jun-16-10008 L3-10220C-FJGS-016SS

{DRIED) Nuclide Energy Yield{°/o)

Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr + Pb-211 404.85 3.78 -l.09E-01 8.80E-01 8.80E-01 miss 427.09 1. 76 4.71E-02 l.87E+OO miss 832.01 3.52 -9.90E-02 1.22E+OO miss + Bi-212 39.86 1. 06 8. 72E+OO 8. 72E-01 3.22E+Ol miss 727. 33 6.67 2.26E-01 8. 72E-01 miss 785.37 1.10 -3.17E-02 3.07E+OO miss 1620.50 1. 47 1.06E+OO 3.81E+OO miss + Pb-212 115 .18 0.60 8.92E-01 1.34E-01 1.86E+OO miss 238.63

• 43.60 3.07E-01 l.34E-01 miss 300.09 3.30 7.14E-02 9.64E-Ol miss + Pb212-XR 74.82 10.28 3.87E-01 9.73E-01 1.48E+OO miss 77 .11 17 .10 9.97E-01 9.73E-01 miss 87.35 3.97 4.04E-Ol 2.04E+OO miss 89.78 1. 46 1.60E+OO 5.21E+OO miss Bi-214 609.32

• 45.49 3.36E-01 l.20E-01 l.20E-01 miss 768.36 4.89 -2.00E-01 8.93E-01 miss 206.18 1. 26 5.90E-01 3.57E+OO miss 934.06 3 .11 1.76E-01 1.37E+OO miss 1120.29 14.92 2.21E-01 4.85E-01 miss 1155.21 1. 63 -7.60E-01 3.52E+OO miss 1238.12 5.83 2.18E-01 l.03E+OO miss 1280.98 1. 43 -8.69E-02 3.28E+OO miss 1377. 67 3.99 7.03E-01 l.73E+OO miss 1385. 31 0.79 -1.58E+OO 4.28E+OO miss 1401. 52 1. 33 -3.25E-01 3.25E+OO miss 1407.99 2.39 -8.08E-01 1.81E+OO miss 1509.21 2 .13 5.18E-01 2.49E+OO miss 1661. 27 1. 05 -6.34E-01 3.73E+OO miss 1729.59 2.88 4.04E-01 2.29E+OO miss 1764.49

• 15.30 6.56E-01 2.64E-01 miss 1847.43 2.03 1.13E+OO 3.40E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-21-J 241.99 7.25 4.58E-01 1. 24E-01 6.73E-01 miss 295.22

• 18.42 3.73E-01 2.63E-01 miss 351.93

• 35.60 3.38E-01 l.24E-01 miss 785.96 1. 06 3.46E-01 3.19E+OO miss + Pb214-XR 74.82 5.80 6.85E-01 1. 72E+OO 2.62E+OO miss 77 .11 9.70 1.76E+OO 1. 72E+OO miss 87.35 2.24 7.16E-01 3. 61E+OO miss 89.78 0.82 2.85E+OO 9.27E+OO miss + Ra-226 186.21 3. 64 5.35E-01 1.14E+OO l.14E+0D miss + Ac-228 129.07 2.42 1.98E-01 1.42E-01 1.63E+D0 miss 209.25 3.89 7.71E-02 9.02E-01 miss 2'70.2 4 3.46 1.77E-01 1.17E+OO miss 328.00 2. 95 1.45E-01 1.28E+OO miss 338.32 1 1. 27 3.92E-01 4.85E-01 miss 409.46 1. 92 -2.78E-01 1.26E+OO miss 463.00 4.40 1.57E-01 7.48E-01 miss 794.95 4.25 5.49E-01 1.30E+OO miss 911. 20

• 25.80 4.48E-01 1.42E-01 miss 964. 77 4.99 3.50E-01 1.26E+OO miss 6/2/2016 12:58:27PM Page 8 of8 Analysis Report for 02-Jun-16-10008 L3-10220C-FJGS-016SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCJ/grams)

Corr Ac-228 968. 97 15.80 3. 96E-01 l.42E-01 5.40E-01 miss 1588.20 3.22 5.97E-02 1.17E+OO miss + Pa-231 27.36 10.30 2.25E-01 1.24E+OO 2. 97E+OO miss 283.69 1. 70 2.35E-01 1. 92E+OO miss 300.07 2.47 9.53E-02 l.29E+OO miss 302.65 2.20 O.OOE+OO l.24E+OO miss 330.06 1. 40 -9.91E-02 2.33E+OO miss + Th-234 92.38 2 .13 -3.50E-Ol 4 , 06E+OO 4.06E+OO miss 92.80 2.10 1.65E+OO 4.41E+OO miss 112. 81 0.21 8.15E+OO 3.06E+Ol miss + U-235 143.76 10. 96 -5.92E-02 7.45E-02 3.51E-01 miss 163.33 5.08 -4.32E-02 7.39E-01 miss 185.71 57.20 4.54E-02 7.45E-02 miss 202 .11 1. 08 1. 23E+OO 3.25E+OO miss 205.31 5.01 2.08E-02 5.90E-01 miss + Am-241 59.54 35.90 3.20E-01 9.46E-01 9.46E-01 miss + = Nuclide identified during the nuclide identification

• =-Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 V) -' !I;:: ::::J 8 30 ::;:: 25 20 15 ;:!; ...,. ...... '";' ""~ ~-* 10 'i= 5 0 1000 2000 3000 0000015056.CNF 1'.:l I !a! 4000 channel 5000 Live Time :600.000 sec Real Time :601.050 sec Start: 1: -0.l(kev) stop : 8192:2047 .O(kev) Acq. start :Thu Jun 02 12: 47: 18 2016 6000 7000 8000 6/2/2016 2:33:11PM

~~:Apex-Ga m ma Analysis Report for 02-Jun-16-10009 L3-10220C-FJGS-017SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number

• 02-Jun-16-10009

• L3-1 0220C-F JGS-017SS (DRIED)

• Off Site Sample 1.290E+03 grams Default 5/23/2016 4:33:00PM 6/2/2016 2:22:29PM

130G 1 L Soil Sample

JWelch ; P11314X2

• 130G Soil

• 600.0 seconds

• 600.4 seconds

• 0.07% : 2.80 : 120-8192 : 120-8192 ! 1.000FWHM

• 1/27/2016

6/28/2012 I 15057 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 2:32:39PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Libra ry\Zi on Li b-BN L. N LB : 1.000FWHM

&-J-/& Page I of7 Analysis Report for 02-Ju n-16-10009 L3-10220C-FJGS-017SS (DRIED) Peak Energy ROI No. {keV) start 1 238.69 949 -2 295.02 11 76 -3 351.92 1401-4 583.16 2327 -5 609.24 2431 -6 661.64 2638 -7 1460.73 5831 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 960 955.10 1187 1180

.14 1416 1407.47 2337 2331.63 2441 2435.90 2652 2645.36 5852 5842.26 6/2/2016 2:33:11PM Net Peak Net Area Area Uncertainty 8.35E+Ol 23. 67 2.69E+Ol 1 5.65 5.43E+Ol '.:..9. 78 2.61E+Ol 1 2. 93 3.19E+Ol 1 3.38 7.85E+Ol 19.53 l.36E+02 23.'70 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLI DES Nuclide Id Energy Yield(%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 4.51E+Ol Pb-212 2.63E+Ol Pb-214 Eu-152 3.34E+Ol Pb-214 Bi-211 1. 39E+Ol Tl-208 l.22E+Ol Bi-214 l.50E+Ol Cs-13: 3.08E+OO K-40 Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.99 1460.82

• 10.66 5.85E+OO l.14E+OO miss Cs-137 1. 00 661.66

• 85.10 2.46E-01 6.81E-02 miss Tl-208 1. 00 583.19

• 85.00 7.51E-02 3.83E-02 miss Pb-212 1. 00 115.18 0.60 238.63

• 43.60 2.53E-01 8.27E-02 miss 300.09 3.30 Bi-214 1. 00 609.32

• 45.49 1. 77E-01 7,72E-02 miss 768.36 4.89 806.18 1. 26 934.06 3.11 11~0.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 Analysis Report for 02-Jun-16-10009 L3-10220C-FJGS-017SS

{DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1661.27 1729.59 1764.49 1847.43 2118.51 Ph-214 0.99 241.99 295.22 351.93 785.96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold=

0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 2:33:11PM P age 3 of7 Activity Activity Caine (pCi/grams)

Uncertainty Corr 2.23E-O l 1.34E-Ol miss 2.62E-0 1 l.04E-01 miss INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Cs-137 Tl-208 X Bi-211 Pb-212 Bi-214 Pb-214 Nuclide Id Confidence 0.999 1. 000 1.000 0.956 1.000 1.000 0.999 ? = nuclide is part of an undetermined solution X ., nuclide rejected by the interference analysis wt mean Activity (pCilgrams) 5.85E+OO 2.46E-01 7.51E-02 2.53E-01 1.77E-01 2.47E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 1.14E+OO 6.81 E-02 3.83E-0 2 8.2 7 E-02 7.7 2 E-02 8.23E-02 6/2/2016 2:33:11 PM Analysis Report for 02-Jun-16-10009

+ + + + + + + + + L3-10220C-FJGS-017SS (DRIED) Peak LocatePerformed o n Peak Locate F ro m Chan nel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 2:32:38PM

120 : 8192 Peak CPS ("AJ) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C: \Canberra\Apex\Root\Default\Li brary\ZI ON LIB-BN L. N LB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCi/grams) (pCilgrams)

K-40 1460.82 *.~ 10.66 5.85E+OO 3. 96E-01 3. 96E-01 Cr-51 320.08 9.91 -7.57E-03 3.78E-01 3.78E-01 Mn-54 834.85 99.98 7.98E-04 3.83E-02 3.83E-02 Co-58 810.76 99.45 -3.67E-03 3.15E-02 3.lSE-02 1674.73 0.52 -1.35E-01 7.95E+OO Co-60 1173.23 99.85 5.76E-03 4.60E-02 4.73E-02 1332.49 99.98 8.76E-03 4.60E-02 Nb-94 702.65 99.81 l.67E-03 3.65E-02 3.65E-02 871.09 99.89 -2.14E-03 3.86E-02 Ag-108m 79.13 6.60 -3.60E-02 3.04E-02 9.17E-01 433.94 90.50 7.19E-03 4.15E-02 614.28 89.80 -5.65E-03 3.04E-02 722. 94 90.80 5.20E-03 4.40E-02 Sn-113 255 .13 2 .11 -3.15E-01 5.28E-02 1.21E+OO 391.70 64. 97 l.94E-02 5.28E-02 Cs-134 475.36 1. 48 -4.28E-01 4.32E-02 2.30E+OO 563.25 8.34 9.74E-02 4.0SE-01 569.33 15.37 1.90E-02 1.70E-01 604.72 97.62 5.19E-04 4.32E-02 Page 4 of7 Tolerance Nuclide Caine Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 6/2/2016 2:33:11PM Page 5 o f 7 Analysis Report for 02-Jun-16-10009 L3-10220C-FJGS-017SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi!grams) (pCl/grams)

Corr Cs-134 795.86 85.46 l.35E-02 4.32E-02 5.03E-02 miss 801.95 8.69 -2.94E-02 2.60E-01 miss 1038.61 0.99 4.43E-01 4.84E+OO miss 1167.S7 1. 79 -l.18E-01 2.64E+OO miss 1365.19 3.02 8.29E-02 l.07E+OO miss + Cs-137 661. 66 .. 85.10 2.46E-01 5.09E-02 5.09E-02 miss + Eu-152 121.78 28.67 -2.26E-02 7.73E-02 7.73E-02 miss 244.70 7.61 -2.56E-02 3.45E-01 miss 295.94 0.45 4.22E+OO 8. 71E+OO miss 344.28 26.60 -l.09E-02

1. llE-01 miss 367.79 0.86 -6.02E-01 4.0lE+OO miss 411.12 2.24 -3.93E-02 l.29E+OO miss 443.96 2.83 *L09E-03 l.08E+OO miss 488.68 0.42 2.6BE+OO 7.75E+OO miss 563.99 0.49 l.94E+OO 6.88E+OO miss 586.26 0.46 -6.42E+OO 7.0lE+OO miss 678. 62 0.47 2.55E+OO 8.65E+OO miss 688.67 0.86 -5.33E-Ol 2.97E+OO miss 719. 35 0.28 -l.35E+OO l.43E+Ol miss 778. 90 12. 96 7.67E-03 2.48E-01 miss 810.45 0.32 2.94E+OO l.15E+Ol miss 867.37 4.26 -2.07E-01 6.99E-01 miss 919.33 0.43 -7.81E-01 5.74E+OO miss 964. 08 14.65 6.28E-02 3.09E-01 miss 1085.87 10.24 -3.47E-03 5.14E-01 miss 1089.74 1. 73 6.79E-01 2.83E+OO miss 1112. 07 13. 69 3.56E-02 3.32E-01 miss 1212.95 1. 43 O.OOE+OO 7.61E-01 miss 1249.94 0.19 4.51E+OO 2.84E+Ol miss 1299.14 1. 63 1.29E+OO 3.38E+OO miss 1408.01 21.07 4.22E-02 1. 96E-01 miss 1457.64 0.50 -6.75E+OO l.71E+Dl miss 1528.10 0.28 -1.68E+OO l.56E+Ol miss + Eu-154 123.07 40.40 2.14E-02 6.67E-02 6.67E-02 miss 247.93 6.89 -1.50E-01 2.97E-Ol miss 591. 7 6 4.95 -1.50E-01 3.68E-01 miss 692.42 1. 78 l.94E-02 l.86E+OO miss '723.30 20.06 -2.89E-02 1.70E-01 miss 756.80 4.52 1. 84E-01 7.78E-01 miss 873.18 12.08 -5.22E-02 3.20E-01 miss 996.29 10.48 -2.81E-02 2.48E-01 miss 1004.76 18.01 l.31E-02 2.37E-01 miss 1274.43 34.80 -4.54E-02 1.28E-Ol miss 1596.48 1. 80 5.46E-01 2.53E+DO miss + Eu-155 45.30 1. 31 1.39E-01 l.46E-01 7.25E+OO miss 60.01 1. 22 -1.94E+OO 8.66E+OO miss 86.55 30.70 6.32E-02 1.46E-01 miss 105.31 21.10 2.93E-02 l.66E-Ol m i ss + Tl-208 583.19

• 85.00 7.51E-02 4.54E-02 4.54E-02 miss + Bi-211 351.07

• 13. 02 7.16E-01 3.22E-01 3.22E-01 miss + Pb-211 404.85 3. 78 -1.71E-01 7.08E-01 7.08E-01 miss 6/2/2016 2:33:11PM Page 6 of7 Analysis Report for 02-Jun-16-10009 L3-10220C-FJGS-017SS (DRIED) Nuclide Energy Yield{°/o)

Activity Nuclide MDA LineMDA Caine Name (keV) (pCUgrams) (pCUgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 3.36E-01 7.0BE-01 2. llE+OO miss 832.01 3.52 5.40E-02 9.52E-01 miss + Bi-212 39.86 1. 06 -7.60E-01 7.43E-01 9.29E+OO miss 727. 33 6.67 4.26E-01 7.43E-01 miss 785. 37 1.10 -6.34E-01 2.00E+OO miss 1620.50 1. 47 O.OOE+OO 9. llE-01 miss + Pb-212 115 .18 0.60 -8.82E-01 8.34E-02 4.69E+OO miss 238.63 \, 43.60 2.53E-01 8.34E-02 miss 300.09 3.30 4.0BE-01 l.12E+OO miss + Pb212-XR 74.82 10.28 1.28E-01 5.84E-01 8.0lE-01 miss 77 .11 17.10 6.28E--:01 5.84E-01 miss 87.35 3.97 2.31E-01 1.19E+OO miss 89.78 1. 4G 2.44E-01 2.86E+OO miss + Bi-214 609.32

• 45.49 1.77E-01 8.05E-02 8.05E-02 miss 768.36 4.89 -5.03E-03 7.24E-01 miss 806.18 1. 26 ~.38E-02 2.60E+OO miss 934.06 3 .11 -1.09E-01 1.0lE+OO miss 1120.29 14.92 1.68E-01 4.44E-01 miss 1155.21 1. 63 -5.68E-01 2.85E+OO mis:::: 1238.12 5.83 4.07E-01 1.lOE+OO miss 1280.98 1. 43 -7.72E-01 3.12 E+OO miss 1377. 67 3.99 2.09E-01 l.18E+OO miss 1385. 31 0.79 -4.35E-01 5.14E+OO miss 1401.52 1. 33 9.51E-02 3.09E+OO miss 1407.99 2.39 3. 71E-01 l.72E+OO miss 1509.21 2.13 7.07E-01 2.64E+OO miss 1661. 27 1. 05 O.OOE+OO 1. 30E+OO miss 1729.59 2.88 2.37E-01 l.68E+OO miss 1764.49 15.30 4.61E-02 3.72E-01 miss 1847.43 2.03 -2.35E-01 l.98E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241. 99 7.25 4.20E-01 l.18E-01 5.57E-01 miss 295.22

• 18.42 2.23E-01 l.82E-01 miss 351.93

• 35.60 2.62E-Ol l.18E-01 miss 785.96 1. 06 -l.27E+OO 2.08E+OO miss + Pb214-XR 74.82 5.80 2.27E-01 1. 03E+OO l.42E+OO miss 77 .11 9.70 l. llE+OO l.03E+OO miss 87.35 2.24 4.lOE-01 2. llE+OO miss 89.78 0.82 4.35E-01 5.lOE+OO miss + Ra-226 186.21 3.64 8.44E-01 9.88E-01 9.88E-01 miss + Ac-228 129.07 2.42 -1.45E-01 2.95E-01 l.07E+OO miss 209.25 3.89 1.00E-01 6.95E-01 miss 270.24 3.46 -4.37E-02 8.62E-01 miss 328.00 2.95 2.38E-Ol l.04E+OO miss 338.32 11. 27 2.48E-01 3.85E-01 m iss 409.46 1. 92 5.78E-01 l.94E+OO miss 463.00 4.40 2.75E-01 9.23E-01 miss 794.95 4.25 2.81E-01 l.07E+OO miss 911. 20 25.80 l.84E-01 2.95E-01 miss 964.77 4.99 2.88E-01 9.74E-Dl miss 968.97 15.80 1.58E-01 3.81E-01 miss 6/2/2016 2:33:11PM Page 7 of7 Analysis Report for 02-Jun-16-10009 L3-10220C-FJGS-017SS (DRIED) Nuclide Energy Yie/d{°/o)

Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Ac-228 1588.20 3.22 0.00E+OO 2.95E-01 4.lOE-01 miss + Pa-231 27.36 10.30 O.OOE+OO 1. 43E-01 l.43E-01 miss 283.69 1. 70 -5. llE-01 l.59E+OO miss 300.07 2.47 5.45E-01 l.50E+OO miss 302.65 2.20 3.70E-01 l.42E+OO miss 330.06 1. 40 5.87E-01 2.36E+OO miss + Th-234 92.38 2.13 2.66E+OO 3.38E+OO 3.38E+OO miss 92.80 2.10 2.72E+OO 3.44E+OO miss 112.81 0.21 -5.32E+OO 2..67E+Ol miss + U-235 143.76 10.96 -5.95E-02 6.12E-02 2.26E-01 miss 163.33 5.08 -4.30E-04 4.35E-01 miss 185.71 57.20 4.59E-02 6.12E-02 miss 202 .11 1. 08 4.86E-01 2.52E+OO miss 205.31 5.01 -7.86E-02 4.25E-01 miss + Am-241 59.54 35.90 -3.02E-02 2.84E-01 2.84E-01 miss + -Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) -I-' C: :::::s 60 55 50 40 35 8 30 25 20 15 10 5 1000 2000 3000 0000015057.CNF 4000 channel 5000 Live Time :600.000 sec Real Time :600.450 sec start: 1: -0.2(kev) stop : 8192 :2047.4(kev)

Acq. Start :Thu Jun 02 14:22 :29 2016 6000 7000 8000 6/2/2016 2:33:48PM Analysis Report for 02-Jun-16-10010 L3-10220C-FJGS-018SS (DRIED} GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels}

Peak Area Range (in channels}

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number ; 02-Jun-16-10010 L3-10220C-FJGS-018SS (DRIED} Off Site Sample 1.858E+03 grams

• Default

• 5/16/2016 4:44:00PM

• 6/2/2016 2:22:36PM

• 130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 600.0 seconds : 600.9 seconds : 0.16% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15058 PEAK WITH NID REPORT Peak Analysis Performed on : 6/2/2016 2:33:17PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of7 Analysis Report for 02-Jun-16-10010 L3-10220C-FJGS-018SS (DRIED) Peak Energy ROI No. (keV) start 1 209.06 832 -2 238.57 949 -3 295.3U 1174 -4 351.84 1401 -5 583.01 2325 -6 609.21 2428 -7 1460.63 5833 -M = First peak in a multiplet regio n m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 842 836.81 961 954.77 1190 1181. 55 1413 1407.56 2339 2331.80 2445 2436.58 5853 5843.48 6/2/2016 2:33:48PM Net Peak Net Area Area Uncertainty 1.87E+Ol 18.30 8.97E+Ol 31.10 6.52E+Ol 23.26 5.97E+Ol 19.25 4.08E+Ol 1 5.34 6.47E+Ol 17.82 1. 50E+02 25.10 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDE S Nuclide Id Energy Yield(%) Activity Page2 of7 Continuum Tentative Counts Nuclide 5.46E+Ol Ac-228 1.13E+02 Pb-212 4.35E+Ol Pb-214 Eu-152 2.86E+Ol Pb-214 Bi-2 11 1. 43E+Ol Tl-208 1. 0 6E+Ol Bi-214 5.92E+OO K-40 Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.99 1 460.82

• 10.66 4. 96E+OO 9.34E-01 miss Tl-208 0.99 583.19

• 85.00 9.06E-02 3.57E-02 miss Pb-212 1. 00 115.18 0.60 238.63

• 43.60 2 .13E-01 8.14E-02 miss 300.09 3.30 Bi-214 1. 00 609.32

• 45.49 2.76E-01 8.30E-02 miss 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155. 21 1. 63 1238.12 5.83 1 280.98 1. 43 1 377.67 3.99 1385.31 0.79 1 401. 52 1. 33 1 407.99 2.39 1 509.21 2.13 1 661.27 1. 05 Analysis Report for 02-Jun-16-10010 L3-10220C-FJGS-018SS (DRIED) IJuclide Name Bi-214 Pb-214 Id Confidence

1. 00 1. 00 Energy (keV) 1 729.59 1764.49 1 847.43 2118.51 241.99 295.22 351. 93 785.96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed. free = No coincidence correction required.

Yield(%) 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 6/2/2016 2:33:48PM Page 3 of7 Activity Activity Coinc (pCilgrams)

Uncertainty Co" 4.20E-01 1.64 E-01 miss 2.22E-01 7.99E-02 miss INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Tl-208 X Bi-211 Pb-212 Bi-214 Pb-214 Nuclide Id Confidence 0.998 0.99 8 0. 964 1. 000 1. 000 1. 000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCl/grams) 4.96E+OO 9.06E-02 2.1 3E-01 2.76E-01 2.oOE-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 9.34E-0 1 3.5 7 E-0 2 8. l4E-02 8.3 0 E-02 7.18E-02 6/2/2016 2:33:48PM Analysis Report for 02-Jun-16-10010

+ + + + + + + + + L3-10220C-FJGS-018SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 1 209.06 M = First peak in a multiplet region m = Other peak in a multiplet reg ion F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 2:33:17PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 3.11775E-02 48.90 Peak Type T ol. NUCLIDE MDA REPORT Nuclide Library Used : C:\Canb erra\Apex\Root\Default\Ubrary\ZION LIB-BNL.NLB Nuclide Energy Yield{°/o)

Activity Nuc/ideMDA LineMDA Name (keV) (pCi/grams) (pCi/grams) (pCi!grams)

K-40 1460.82

• 10.66 4. 96E+OO 3.85E-Ol 3.BSE-01 Cr-51 320.08 9.91 -6.60E-02 4.09E-01 4.09E-01 Mn-54 834.85 99.98 3.00E-03 4.15E-02 4.lSE-02 Co-58 810.76 99.45 -5.12E-03 3.35E-02 3.35E-02 1674.73 0.52 O.OOE+OO 2. 41E+OO Co-60 1173.23 99.85 l.87E-02 3.56E-02 4.82E-02 1332.49 99.98 3.30E-03 3.56E-02 Nb-94 702.65 99.81 1.0BE-02 3.02E-02 3.02E-02 871.09 99.89 2.34E-03 3.49E-02 Ag-108m 79.13 6.60 3.65E-01 2.SlE-02 1.26E+OO 433.94 90.50 9.68E-03 3.20E-02 614.28 89.80 3.92E-03 2.61E-02 722.94 90.80 -2.12E-02 2.BBE-02 Sn-113 255.13 2 .11 -6.99E-02 4.06E-02 1. 21E+OO 391.70 64. 9'7 -4.98E-03 4.06E-02 Cs-134 475.36 1. 48 -2.72E-01 2.63E-02 1.87E+OO 563.25 8.34 1.35E-01 3.90E-01 569.33 15.37 l.54E-lJ2 1.84E-01 Page4 of7 Tolerance Nuclide Ac-228 Colnc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss 6/2/2016 2:33:48PM Page 5 of7 Analysis Report for 02-Jun-16-10010 L3-10220C-FJGS-018SS (DRIED) Nuclide Energy Yield{°/o)

Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCi!grams)

Co" Cs-134 604.72 97.62 -5.95E-03 2.63E-02 2.63E-02 miss 795.86 85.46 -9.21E-03 3.32E-02 miss 801.95 8.69 9. llE-02 3.85E-01 miss 1038.61 0.99 O.OOE+OO 2.lOE+OO miss 1167.97 1. 79 1.43E+OO 2.84E+OO miss 1365.19 3.02 O.OOE+OO 3.05E-01 miss + Cs-137 661. 66 85.10 1. 62E-02 4.55E-02 4.55E-02 miss + Eu-152 121. 7 8 28.67 4.54E-02 8.20E-02 1.lOE-01 miss 244.70 7.61 6.02E-04 3.46E-01 miss 295.94 0.45 1.08E+Ol l.03E+Ol miss 34-L 28 26.60 3.94E-03 8.20E-02 miss 367.79 0.86 -l.07E-01 2.88E+OO miss 411.12 2.24 2.05E-01 l.33E+OO miss 443. 96 2.83 -2.32E-01 7.79E-01 miss 488.68 0.42 7.32E-01 5.22E+OO miss 563.99 0.49 -5.18E-01 6.2GE+OO miss 586.26 0.46 -4.70E+OO 4.44E+OO miss 678.62 0.47 -l.52E+OO 5.82E+OO miss 688.67 0.86 6.39E-01 3.70E+OO miss 719. 35 0.28 4.0lE+OO 1.36E+Ol miss 778.90 12. 96 6.63E-02 2.66E-Ol miss 810.45 0.32 -1.lOE+OO 8.83E+OO miss 867.37 4.26 7.73E-02 7.60E-01 miss 919.33 0.43 -5.34E-01 6.47E+OO miss 964.08 14.65 1. 34E-01 3.41E-01 miss 1085.87 10.24 6.55E-02 3. 96E-01 miss 1089.74 1. 73 -3.81E-01

1. 79E+OO miss 1112. 07 13.69 8.53E-03 2.BOE-01 miss 1212.95 1. 43 1. OlE+OO 3.06E+OO miss 1249.94 0.19 -2.62E+OO l.80E+Ul miss 1299.14 1. 63 O.OOE+OO 5.39E-01 miss 1408.01 21. 07 3.49E-0~ l.96E-01 miss 1457.64 0.50 -3.50E+OO 1.17E+Ol miss 1528.10 0.28 3.89E+OO l.40E+Ol miss + Eu-154 123.07 40.40 -2.46E-02 6.80E-02 6.80E-02 miss 247.93 6.89 -4.09E-02 3.63E-0 1 miss 5 91. 7 6 4.95 -2.65E-02 5.80E-01 miss 692.42 1. 78 -4.78E-01 8.80E-01 miss 723. 30 20.06 -l.12E-02 1.64E-01 miss 756.80 4.52 -3.62E-01 6.00E-01 miss 873.18 12.08 2.87E-02 3.26E-01 miss 996.29 10.48 1.04E-02 3.40E-01 miss 1004.76 18.01 3.29E-02 l.82E-01 miss 1274.43 34.80 2.87E-02 l.30E-01 miss 1596.48 1. 80 O.OOE+OO 5.70E-01 miss + Eu-155 45.30 1. 31 -4.61E+OO

1. Ti'E-0 1 1.99E+Ol miss 60.01 1. 22 2.16E+OO 2.20E+Ol miss 86.55 30.70 6.89E-02 2.02E-Ol miss 105.31 21.10 1.42E-02 1.77E-Ol miss + Tl-208 583.19

• 85.00 9.06E-02 3.69E-02 3.69E-O: miss + Bi-211 351.07

• 13.02 6.07E-Ol 2.19E-01 2.19E-01 miss 6/2/2016 2:33:48PM Page 6 of7 Ana l ysis RP.port for 02..Jun-16-10010 L3-10220C-FJGS-018SS (DRIED) Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCi/grams) (pCilgrams)

Corr + Pb-.211 40 4.85 3.78 -l.02E-01 6.45E-01 6.45E-01 miss 427.09 1. 76 3.37E-01 1. 62E+OO miss 832.01 3.52 -1. 93E-01 8.17E-01 miss + Ei-212 39.86 1. 06 -1.13E+OO 6.18E-01 2.3 G E+01 miss 727. 33 6.67 5.97E-02 6.18E-01 miss 785.37 1.10 4.23E-01 3.14E+OO miss 1620.5 0 1. 47 O.OOE+OO 7.03E-01 miss + Pb-212 11 5.1 8 0.60 3.68E+OO 1.03E-01 6.58E+OO miss 238.63

• 43.60 2.13E-Ol 1.03E-01 miss 300.09 3.30 3.22E-01 9.25E-01 miss + Pb212-XR 74.82 10.28 4.65E-01 6.45E-01 l.09E+OO miss 77 .11 17.10 4.54E-01 6.45E-01 miss 87.35 3.97 -2.30E-01 l.38E+OO miss 89.78 1. 46 4.93E-01 3.43E+OO miss + Bi-214 60S.32 .*. 45.49 2.76E-01 6.54E-02 6.54E-02 miss 768.36 4.89 3.48E-01 9.04E-01 miss 806.18 1.26 7.73E-01 3.09E+OO miss 934.06 3 .11 -6. 96E-03 1.00E+OO miss 1120.29 14.92 2.59E-01 4.51E-01 miss 1155. 21 1. 63 -2.35E-01 1.70E+OO miss 1238.12 5.83 2.91E-01 9.72E-01 miss 1280.98 1. 43 7.0lE-01 2.92E+OO miss 1377. 67 3.99 1.BlE-01 l.OlE+OO miss 1385. 31 0.79 -7.92E-01 3.14E+OO miss 1401. 52 1. 33 -3.67E-01 2.76E+OO miss 1407.99 2.39 3.07E-01 1.72E+OO miss 1509.21 2.13 1.45E-01 1.57E+OO miss 1661. 27 1. 05 O.OOE+OO 1.0lE+OO miss 1729.59 2.88 O.OOE+OO 3.77E-01 miss 1764.49 15.30 2.17E-01 4.44E-01 miss 1847.43 2.03 4.15E-01 1. 92E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 4.79E-Ol 8.03E-02 5.49E-01 miss 295.22

• 18.42 4.20E-01 l.94E-01 miss 351.93

• 35.60 2.22E-01 8.03E-02 miss 785. 96 1. 06 7.82E-01 3.27E+OO miss + Pb214-XR 74.82 5.80 8.25E-01 l.14E+OO 1.94E+OO miss 77 .11 9.70 8.0lE-01 l.14E+OO miss 87.35 2.24 -4.08E-01 2.44 E+OO m iss 89.78 0.82 8.79E-01 6.lOE+OO miss + Ra-226 186.21 3.64 2.13E-01 8.41E-01 8.41E-01 miss + Ac-228 129.07 2.42 -6.61E-03 2.4:E-01 1.35E+OO miss 209.25 3.89 4.60E-01 7.76E-01 miss 270.24 3.46 2.37E-01 8.70E-01 miss 328.00 2.95 5.68E-01 l.15E+OO miss 338.32 11.27 3.0lE-01 3.37E-01 miss 409.46 1. 92 -2.37E-01

1. 34E+OO miss 463.00 4.40 2.26E-Ol 7.57E-01 miss 794.95 4.25 3.64E-02 7.71E-01 miss 91 1.20 25.80 2.03E-01 2.47E-01 miss 964. 77 4.99 2.17E-02 8.86E-01 miss 6/2/2016 2:33:48PM Page 7 of7 Analysis Report for 02-Jun-16-10 01 O L3-10220C-FJGS-018SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCi!grams)

Corr Ac-228 968. 97 15.80 9 .13E-02 2.4 7 E-01 3.05E-01 miss 1588.20 3.22 7.29E-02 8. 59E-01 miss + Pa-231 27.36 10.30 5.85E-01 1.24E+OO 2. 65E+OO miss 283.69 1. 70 1. OlE+OO 1. 76E+OO miss 300.07 2.47 4.30E-01 1.24E+OO miss 302.65 2.20 1.15E-01 1.20E+OO miss 330.06 1. 40 -2.87E-01 1.88E+OO miss + Th-234 92.38 2.13 2.73E+OO 4.22E+OO 4.27E+OO miss 92.80 2.10 2.47E+OO 4.22E+DO miss 112. 81 0.21 -6.55E+OO 2.57E+01 miss + U-235 143.76 10.96 -9.15E-02 5.46E-02 2.43E-01 miss 163.33 5.08 -6.02E-02 5.19E-01 miss 185. 71 57.20 3.0lE-02 5.46E-02 miss 202 .11 1. 08 1.02E+D0 2.72E+OO miss 205.31 5.01 -7.27E-02

4. 72E-Ol miss + Am-241 59.54 35.90 9.24E-02 7.69E-01 7. 69E-01 miss + :: Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ :: Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Ill ..... C: :::I 35 8 30 25 20 1 5 10 5 ;!; ..... ..... "' J: n. I 1/~i 1000 ;'!; co";' *;;; *;::: -~M: 2000 3000 0000015058.CNF 4000 5000 channel Live Time :600.000 sec Real Time :600.950 sec start: 1: -0.l(kev)

Stop : 8192: 2047 .O(kev) Acq. Start :Thu Jun 02 14:22:36 2016 6000 7000 8000 6/2/2016 2:49:25PM Analysis Report for 02-Jun-16-10011 L3-10220C-FJGS-019SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels}

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 02-Jun-16-10011

L3-10220C-FJGS-019SS (DRIED) : Off Site Sample 5.972E+02 grams : Default : 5/23/2016 5:00:00PM

6/2/2016 2:38:48PM

130G 1 L Soil Sample : JWelch ; P11314X2 ; 130G Soil : 600.0 seconds

• 600.4 seconds 0.07% 2.80 120 -8192 120 -8192 1.000FWHM 1/27/2016

6/28/2012

15059 PEAK WITH NID REPORT Peak Analysis Performed on

6/2/2016 2:48:SOPM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C: \Can berra\Apex\Root\Defa ult\Library\Zion Lib-BN L. N LB : 1.000FWHM Page l of7 6/2/2016 2:49:25PM Page 2 of7 Analysis Report for 02-Jun-16-10011 L3-10220C-FJGS-019SS (DRIED) M m Peak Energy ROI No. {keV) start 1 74.74 2 97 -2 76. 96 297 -3 238.37 949 -4 351.83 1401 -5 661.66 2641 -6 1460.58 5834 -M = First peak in a multiplet regio n m = Other peak in a multiplet reg ion F = Fitted singlet Errors quoted at 2.000sigma ROI Peak end Centroid 315 300.19 315 309.05 960 953.81 1412 1407.10 2652 2645.46 5851 5841.64 Net Peak Net Area Continuum Area Uncertainty Counts 1.41E+Ol 8.17 1.45E+Ol 2.35E+01 10.26 1.07E+Ol 2.77E+O l 14.63 2.06E+Ol 3.57E+0 1 14.44 1.46E+Ol 2.65E+O l 13.93 2. llE+Ol 4.98E+Ol 14.48 2.31E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1 460.82

• 10.66 4.61E+OO 1.40E+OO Cs-137 1. 00 661.66 *'* 85.10 l.79E-01 9.68E-02 Bi-211 0. 96 351.07

• 13. 02 1.02E+OO 4.42E-01 Pb-212 0.99 115.18 0.60 238.63

• 43.60 1.BlE-01 1.00E-01 300.0 9 3.30 Pb212-XR 0.99 74.82

• 10.28 7.68E-01 4.73E-01 77 .11

• 17.10 7.lOE-01 3.43E-Ol 87.35 3.97 89.7 8 1. 46 P b-214 0.51 241. 99 7.25 295.22 18.42 3 51.9 3

• 35.60 3.71E-Ol l , 62E-01 785. 96 1. 06 Tentative Nuclide Pb214-XR Pb212-XR Pb214-X?..

Pb212-XR Pb-212 Pb-2 14 Bi-211 Cs-137 K-40 Coinc Corr miss miss miss miss miss miss m i s s Analysis Report for 02-Jun-16-10011 L3-10220C-FJGS-019SS (DRIED) * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 6/2/2016 2:49: 25PM INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Cs-137 ? Bi-211 Pb-212 Pb212-XR ? Pb-214 X Pb214-XR Nuclide Id Confidence

0. 996 1. 000 0. 965 0.996 0.999 0.512 0.999 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 4.61E+OO 1. 7 9E-01 1.02E+OO 1. BlE-01 7.30E-01 3.71E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 1.40E+OO 9.68E-02 4.42E-01 1.00E-01 2.78E-01 1.62E-01 P age 3 of7 Comments 6/2/2016 2:49:25PM Analysis Report for 02-Jun-16-10011

+ + + + + + + + + L3-10220C-FJGS-019SS (DRIED) Peak Locate Performed o n Peak Locate From Channel Peak Locate To Channel Peak No. Energy (ke V) All peaks were identified.

M"' First peak in a multiplet regio n m "' other peak in a multiplet region F "' Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 6/2/2016 2:48:SOPM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

K-40 1460.82

• 10.66 4.61E+OO 7.35E-01 7.35E-01 Cr-51 320.08 9.91 -5.62E-02 3.31E-01 3.31E-01 Mn-54 834.85 99.98 8.04E-03 7.42E-02 7.42E-02 Co-58 810.76 99.45 -9.76E-03 5.39E-02 5.39E-02 1674.73 0.52 O.OOE+OO 6.31E+OO Co-60 1173.23 99.85 1.70E-02 2.50E-02 7.89E-02 1332.49 99.98 O.OOE+OO 2.50E-02 Nb-94 702.65 99.81 2.33E-02 6.44E-02 7.88E-02 871.09 99.89 -l.56E-02 6.44E-02 Ag-108m 79.13 6.60 -1.61E-02 5.12E-02 1.02E+OO 433.94 90.50 1.59E-03 5.12E-02 614.28 89.80 -7.32E-03 6.57E-02 722. 94 90.80 2.52E-02 8.83E-02 Sn-113 255 .13 2 .11 5.48E-01 7.05E-02 2.26E+OO 391. 70 64.97 -l.75E-03 7.05E-02 Cs-134 475.36 1. 48 -2.63E+OO 4.12E-02 3.37E+OO 563.25 8.34 -1.62E-01 4.60E-01 569.33 15.37 -2.73E-02 2.51E-01 604.72 97. 62 -l.57E-02 4.12E-02 Pagc4 of7 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 6/2/2016 2:49:25PM Page 5 of7 Analysis Report for 02-Jun-16-10011 L3-10220C-FJGS-019SS (DRIED) Nuclide Energy Yield{°/,,)

Activity Nuclide MDA LineMDA Coim: Name (keV) (pCi!grams) (pCVgrams) (pCi!grams)

Corr Cs-134 795.86 85.46 1.BOE-02 4.12E-02 9.26E-02 miss 801.95 8.69 1.65E-01 9.15E-01 miss 1038.61 0.99 -9.29E-01 7.40E+OO miss 1167.97 1. 79 3.40E-01 3.50E+OO miss 1365.19 3.02 4.48E-02 2.31E+OO miss + Cs-13: 661.66

• 85.10 l.79E-01 l.23E-01 l.23E-01 miss + Eu-152 121.78 28.67 -2.07E-03 l.34E-01 l.54E-01 miss 244.70 7.61 9.88E-02 7.20E-01 miss 295.94 0.45 l.84E+OO l.29E+Ol miss 344.28 26.60 -3.02E-02 l.80E-01 miss 367.7 9 0.86 -2.13E-01 5.83E+OO miss 411.12 2.24 l.19E-01 2.43E+OO miss 443. 96 2.83 -3.40E-Ol

1. 67E+OO miss 488.68 0.42 2.12E+OO l.34E+Ol miss 563.99 0.49 1.26E+OO 1. 13E+Ol miss 586.26 0.46 9.24E-01 l.39E+Ol miss 678.62 0.47 2.07E-01 l.34E+Ol miss 688.67 0.86 6.90E-01 5.08E+OO miss 719.35 0.28 3.lOE+OO 2.63E+Ol miss 778.90 12. 96 O.OOE+OO l.34E-01 miss 810.45 0.32 -2.06E+OO l.52E+Ol miss 867.37 4.26 -1.22E-01 l.51E+OO miss 919.33 0.43 4.27E+OO 2.21E+Ol miss 964. 08 14.65 1.02E-01 4.72E-01 mi~s 1085.87 10.24 1.87E-Ol 8.47E-01 miss 1089.74 1. 73 -1. 93E+OO 3.43E+OO miss 1112. 07 13.6S 1.71E-02 4.40E-01 miss 1212.)5 1. 43 -1.39E+OO 5.64E+OO miss 1249.94 0.19 O.OOE+OO 1.26E+Ol miss 1299.14 1. 63 7. 96E-02 5.18E+OO miss 1408.01 21.07 4.23E-02 4.23E-01 miss 1457.64 0.50 -3.64E+OO 2.30E+Ol miss 1528.10 0.28 O.OOE+OO 9.82E+OO miss + Eu-154 123.07 40.40 -2.09E-03

6. 96E-02 l.04E-01 miss 247.93 6.89 -2.67E-02 6.77E-01 miss 591.76 4.95 -6.06E-01 7.96E-Ol miss 692.42 1. 78 3.35E-01 3. llE+OO miss 723. 30 20.06 -8.92E-03 3.67E-01 miss 756.80 4.52 -3.50E-01 l.03E+OO miss 873.18 12.08 -8.64E-02 5.35E-01 miss 996.29 10.48 1.21E-02 6.75E-01 miss 1004.76 18.01 -3.55E-02 3 .13E-01 miss 1274.43 34.80 O.OOE+OO 6. 96E-02 miss 1596.48 1. 80 O.OOE+OO 1.59E+OO miss + Eu-155 45.30 1. 31 -4.91E+OO 2.03E-01 l.18E+Ol miss 60.01 1. 22 -1.70E+OO l.47E+Ol miss 86.55 30.70 -8.38E-02 2.03E-01 miss 105.31 21.10 5.61E-02 2.55E-01 miss + Tl-208 583.19 85.00 2.69E-02 1.13E-01 1.13E-01 miss + Bi-211 351.07 7< 13.02 1. 02E+OO 4.56E-01 4.56E-01 miss + Pb-211 4 0 4.85 3.78 4.34E-02 l.30E+OO 1.30E+OO miss 6/2/2016 2:49:25PM Page 6 of7 Analysis Report for 02-Jun-16-1001 1 L3-10220C-FJGS-019SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCilgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 -3.22E-01

1. 30E+OO 2. 60E+OO miss 832.01 3.52 -l.27E-01 l.41E+OO miss + Bi-212 39.86 1. 06 -1. llE+OO 1.21E+OO 1.45E+Ol miss 727. 33 6.67 2.46E-02 1.21E+OO miss 785.37 1.10 9.78E-02 5.45E+OO miss 1620.50 1. 47 O.OOE+OO l.97E+OO miss + Pb-212 115 .18 0.60 2.26E-01 l.27E-01 7.16E+OO miss 238.63

• 43.60 1.81E-01 l.27E-01 miss 300.09 3.30 -3.94E-01

!.

• 32E+OO miss + Pb212-XR 74.82

• 10.28 7.68E-01 4.07E-01 8.33E-01 miss 77 .11

• 17.10 7.lOE-01 4.07E-01 miss 87.35 3.97 1.34E+OO 2.0SE+OO miss 89.78 1. 46 -6.35E-01 1.75E+OO miss + Bi-214 609.32 45.49 2.31E-01 2.94E-Ol 2.94E-01 miss 768.36 4.89 2.17E-02 1.21E+OO miss 806.18 1.26 1.13E+OO 6.25E+DO miss 934.06 3 .11 3.22E-01 2.82E+OO miss 1120.29 14.92 3.85E-01 8.26E-Ol miss 1155.21 1. 63 -3.66E-01 3.77E+OO miss 1238.12 5. 83 -2. 58K-01 l.39E+OO miss 1280.98 1. 43 1.70E+OO 7.51E+OO miss 1377. 67 3.99 2.70E-01 2.55E+OO miss 1385. 31 0.79 1.45E+OO 1. llE+Ol miss 1401. 52 1. 33 8.73E-01 6.67E+OO miss 1407.99 2.39 3.72E-01 3.72E+OO miss 1509.21 2 .13 -2.04E-01 3.SOE+OO miss 1661. 27 1. 05 1.04E+OO 7.66E+OO miss 1729.59 2.88 7.81E-01 3.63E+OO miss 1764.49 15.30 7.93E-02 6.93E-01 miss 1847.43 2.03 7.25E-02 4.27E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 2.59E-01 1.6?E-01 7.75E-Ol miss 295.22 18.42 1.53E-01 3.60E-01 miss 351.93

• 35.60 3. 71E-01 1.67E-01 miss 785.96 1. 06 -5.09E-01 5.67E+OO miss + Pb214-XR 74.32

• 5.80 1.36E+OO 7.18E-01 1.48E+OO miss 77 .11

• 9.70 1.25E+OO 7.lBE-01 miss 87.35 2.24 2.38E+OO 3.63E+OO miss 89.78 0.82 -1.13E+OO 3.12E+OO miss + Ra-226 186.21 3.64 2.32E-01 1.47E+OO 1.47E+OO miss + Ac-228 129.07 2.42 7.16E-01 4.63E-01 2.26E+OO miss 209.25 3.89 6.98E-01 1.33E+OO miss 270.24 3.46 -1.05E-Ol l.SOE+OO miss 328.00 2.95 1.58E-01 1.80E+OO miss 338. 3'.2 11.27 2.39E-01 6.03E-01 miss 409 . .J.6 1. 92 1.lSE-01 2.32E+OO miss 463.00 4.40 3.48E-01 1. 62E+OO miss 794.95 4.25 7.67E-02 1.42E+OO miss 911.20 25.80 2.13E-01 4.63E-01 miss 964. 77 4.99 2.98E-01 1. 38E+OO miss 968. 97 15.80 2.36E-01 6.19E-01 miss 6/2/2016 2:49:25PM Page 7 of7 Analysis Report for 02-J un-16-100 11 L3-10220C-FJGS-019SS (DRIED) Nuclide Energy Yield{°/o)

Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCUgrams) (pCilgrams)

Corr Ac-228 1588.20 3.22 -2.80E-01 4.63E-01 3. 03E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 3.08E-01 3. 08E-01 miss 283.69 1. 70 -l.48E-Ol

2. 83E+OO miss 300.07 2.47 -5.26E-Ol 1.77E+OO miss 302.65 2.20 O.OOE+OO 2. 54E+OO miss 330.06 1. 40 -2.17E-Ol

3. 81E+OO miss + Th-234 92.38 2.13 6.67E-01 4.49E+OO 4. 49E+OO miss 92.80 2.10 2.27E+OO 5.00E+OO miss 112. 81 0.21 7.54E+OO 2. 90E+Ol miss + U-235 143.76 10.96 -4.37E-02 9.5-:'E-02 3.15E-01 miss 163.33 5.08 -2.61E-01 6.33E-01 miss 185. 71 57.20 1.93E-02 9.57E-02 miss 202 .11 1. 08 -3.15E-01 3.18E+OO miss 205.31 5.01 5.45E-02 7.91E-01 miss + Am-241 59.54 35.90 -1.81E-Ol 4.89E-01 4.89E-01 miss + Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 40 35 VI µ C: ::::, 8 30 25 20 "' 1 15 10 5 0 1000 2000 3000 000001 5059.CNF 4000 channel 5000 Live Time 600.000 sec Real Ti me 600 .420 sec start: 1 -0.2(kev) stop : 8192 2047. 4(kev) Acq. start Thu Jun 02 14: 38:48 2016 6000 7000 8000

...............

~Apex-Gamma 5/5/2016 11:10:08AM Analysis Report for 05-May-16-10009 L3-10220C-FQGS-011SS (DRIED) GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 05-May-16-1 0009 : L3-10220C-FQGS-011SS (DRIED) : 1 L 130G Soil Sample 1.091 E+03 grams : Default : 5/2/2016 1 :05:00PM : 5/5/2016 10:39:24AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 1800.0 seconds : 1803.1 seconds : 0.17 % : 2.80 : 120-8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 14854 PEAK WITH NID REPORT Peak Analysis Performed on : 5/5/2016 11 :09:33AM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Defau lt\Libra ry\Zio n Lib-BN L. N LB : 1.000FWHM Page 1 of8 5/5/2016 11:10:0SAM Page 2 of8 Analysis Report for 05-M ay-16-10009 L3-10220C-FQGS-011SS (DRIED) Peak Energy ROI ROI Peak Alaf Pa:s,,I, "'""'* A ..... ... _ ... ,.., ...... ,..,. ........ '"" "'""******a.-w***

Tentative No. {keV) start end Centroid Area Uncertainty Counts Nuclide M 1 238.59 948 -974 954.86 2.47E+02 33.40 1.46E+02 Pb-212 m 2 241.45 948 -974 966. 30 5.17E+Ol 17. 95 1.19E+02 Pb-214 3 295.24 1175 -1186 1181.31 5.08E+Ol 28.04 1.16E+02 Pb-214 Eu-152 4 338.24 1346 -1359 1353. 20 4.18E+Ol 24.08 8.44E+Ol Ac-228 5 351.83 1403 -1414 1407.49 1. 01E+02 29.23 1.01E+02 Pb-214 Bi-211 6 462.55 1846 -1855 1850 .13 1.59E+Ol 17.28 5.82E+Ol Cs-138 Ac-228 Sb-125 7 510.63 2036 -2047 2042.38 3.31E+Ol 22.23 8.18E+Ol ..... tffl/11-51( 3 583.14 2325 -2337 2332.35 5.84E+Ol 21.69 5.12E+D1 Tl-208 9 609.27 2430 -2442 2436.81 8.64E+Ol 23.91 4.92E+Ol Bi-214 10 661.43 2638 -2654 2645.44 l.43E+02 28.20 4,67E+Ol Cs-137 11 768.54 3068 -30B 3073.83 2.03E+Ol 12.58 1.74E+Ol Bi-214 12 911.15 3637 -3652 3644.30 5.52E+Ol 18.19 2.35E+Ol Ac-228 13 968.77 3869 -3881 3874.85 3.15E+Ol 14.41 1.90E+Ol Ac-228 14 1460.32 583 1 -5854 5842.26 2.83E+02 34.14 6.54E+OO K-40 ,rpv/ M = First peak in a multiplet region 5,5-((., m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.98 1460.82

• 10.66 5.3DE+OO 7.89E-01 miss Cs-137 0.99 661. 66

• 85.10 l.95E-Ol 4.52E-02 miss Tl-208 1. 00 583.19

• 85.00 7. 35E-02 2.87E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

• 43.60 3.32E-01 7. OlE-02 miss 300.09 3.30 Bi-214 1. 00 609.32

• 45.49 2.09E-01 6.32E-02 miss 768.36

• 4.89 5.34E-01 3.37E-01 miss 806.18 1. 26 934.06 3.11 Analysis Report for 05-May-16-1 0009 L3-10220C-FQGS-011SS (DRIED) Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1120.29 1155.21 1238.12 1280.98 1377. 67 1385.31 1401.52 1407.99 1509.21 1661.27 1 729.59 1 764.49 1 847.43 2118. 51 Pb-214 0 , 99 241.99 295.22 351.93 785. 96 Ac-228 0.99 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911.20 964. 77 968.97 15 88.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. .... * * * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold=

0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 14.92 1. 63 5.83 1. 43 3.99 0.79 1. 33 2.39 2 .13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.25 25.80 4.39 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 5/5/2016 11 :10:0BAM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 4.22E-01 1.61E-01 miss 1.86E-01 1. 07E-01 miss 2.14E-Ol 7.06E-02 miss 2.:2E-01 l.63E-01 miss 3.29E-01 3.61E-01 miss 3.lOE-01 1. 0 6E-01 miss 3.0lE-01 l.40E-01 miss INTERFERENCE CORRECTED REPORT Analysis Report for 05-May-16-10009 L3-10220C-FQGS-011SS (DRIED) Nuclide Name K-40 Cs-137 Tl-208 Nuclide Id Confidence 0.985 0.997 1. 000 X Bi-211 0. 966 ? = X = Pb-212 Bi-214 Pb-214 Ac-228 1. 000 1. 000 0.998 0.999 nuclide is part of an undetermined solution nuclide rejected by the interference analysis 5/5/2016 11:10:08AM Wt mean Wt mean Activity Activity (pCilgrams)

Uncertainty 5.30E+OO 7.89E-01 1.95E-Ol 4.52E-02 7.35E-02 2.87E-02 3.32E-01 7.0lE-02 2.20E-01 6.21E-02 2.31E-01 5.53E-02 3.0lE-01 7.33E-02 @ ;;;: nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Page4 of 8 Comments 5/5/2016 11: 10:08AM Analysis Report for 05-May-16-10009

+ + + + + + + + + L3-10220C-FQGS-011SS (DRIED) Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 7 510.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 5/5/2016 11 :09:33AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 1.84024E-02 33.55 Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbe rra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

K-40 1460.82

• 10.66 5.30E+OO 2.32E-Ol 2.32E-01 Cr-51 320.08 9.91 5.76E-03 2.16E-01 2.16E-Ol Mn-54 834.85 99.98 5.85E-03 2.76E-02 2.76E-02 Co-58 810.76 99.45 -1.84E-03

1. 66E-02 1.66E-02 1674.73 0.52 -6.62E-Ol 3.25E+OO Co-60 1173.23 99.85 -2.39E-03

3. llE-02 3.23E-02 1332.49 99.98 8.09E-03 3. llE-02 Nb-94 702.65 99.81 5.81E-04 1.98E-02 2.52E-02 871.09 99.89 -7.49E-03 1.98E-02 Ag-108rn 79 .13 6.60 5.17E-01 2.3:E-02 l.OOE+OO 433.94 90.50 7.06E-04 2.46E-02 614.28 89.80 6.76E-03 3.03E-02 722.94 90.80 -1.14E-04 2.37E-02 Sn-113 255 .13 2 .11 1.02E-01 3.48E-02 l.07E+OO 391. 70 64.97 3.56E-03 3.48E-02 Cs-134 475.36 1. 48 -9.17E-01 2.47E-02 l. lOE+OO 563.25 8.34 5.38E-03 3.02E-01 569.33 15.37 -2.34E-02 l.29E-01 Page 5 uf8 Tolerance Nuclide If µ/./-5' ( Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss 5/5/2016 11:10:08AM Page 6 of8 Analysis Report for 05-May-16-10009 L3-10220C-FQGS-011 SS (DRIED) Nuclide Energy Yield(%) Activity Nuclid e MDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi!grams)

Corr Cs-134 604. 72 97. 62 -6.76E-04 2.47E-02 2. 47E-02 miss 795.86 85.46 6.82E-03 3. llE-02 miss 801. 95 8.69 8.82E-02 3.08E-01 miss 1038.61 0.99 8.52E-01 3. OlE+OO miss 1167. 97 1. 79 -3.67E-01 1.74E+OO miss 1365.19 3.02 -7.66E-02 5.86E-Ol miss + Cs-137 661. 66

• 85.10 1.95E-01 3.75E-02 3. 75E-02 miss + Eu-152 121. 78 28.67 -'.2.62E-03 6.98E-02 8.84E-02 miss 244.70 7.61 -l.06E-01 2. 61E-01 miss 295.94 0.45 -4.14E-01 6.90E+OO miss 344.28 26.60 -4.0lE-02

6. 98E-02 miss 367.79 0.86 9.80E-01 2.76E+OO miss 411.12 2.24 l.lOE-01 l.03E+OO miss 443. 96 2.83 5.64E-02 7.36E-01 miss 488.68 0.42 6.0lE-02 5.06E+OO miss 563.99 0.49 l.77E+OO 5.43E+OO miss 586.26 0.46 -4.07E+OO 5.61E+OO miss 678.62 0.47 -3.35E-02 4.38E+OO miss 688.67 0.86 7.29E-01 3.0SE+OO miss 719.35 0.28 2.61E+OO 8. 62E+OO miss 778.90 12. 96 -3.13E-02 l.51E-01 miss 810. 45 0.32 -1. llE+OO 5.00E+OO miss 867.37 4.26 -1.75E-01 6.18E-01 miss 919.33 0.43 1.22E+OO 5.93E+OO miss 964.08 14.65 6.03E-02 2.36E-01 miss 1085.87 10.24 3.91E-02 2.09E-01 miss 1089.74 1. 73 -2.25E-02 l.33E+OO miss 1112. 07 13.69 -4.00E-02 l.81E-01 miss 1212.95 1. 43 8.42E-01 2.55E+OO miss 1249.94 0.19 9.0SE+OO 2.07E+Ol miss 1299.14 1. 63 -4.39E-01 l.79E+OO miss 1408.01 21.07 4.14E-02 1.39E-01 miss 1457.64 0.50 -2.33E+OO 1.26E+Ol miss 1528.10 0.28 l.15E+OO 6.82E+OO miss + Eu-154 123.07 40.40 l.70E-02 6.15E-02 6.15E-02 miss 247.93 6.89 -1.27E-01 2.84E-Ol miss 591.76 4.95 1.61E-01 5.57E-Ol miss 692.42 1. 78 -2.09E-01 9.55E-01 miss 723. 30 20.06 -1.38E-02 9.80E-02 miss 756.80 4.52 3 .17E-02 5.12E-01 miss 873.18 12.08 -2.24E-02 l.75E-01 miss 996.29 10.48 -3.18E-02 2.21E-01 miss 1004.76 18.01 l.20E-02 1.SOE-01 miss 1274.43 34.80 -l.OlE-02 7.81E-02 miss 1596.48 1. 80 1.34E-01 1.68E+OO miss + Eu-155 45.30 1. 31 4.75E+OO 1.43E-0 1 l.71E+Ol miss 60.01 1. 22 7.04E+OO 1.75E+Ol miss 86.55 30.70 -3.82E-02 1.49E-01 miss 105.31 21.10 6.23E-03 1.43E-01 miss + Tl-208 583.19

• 85.00 7.35E-02 3.53E-02 3.53E-02 miss + Bi-211 351.07

• 13.02 5.86E-01 2.1.,E-01 2.17E-01 miss 5/5/2016 11 :10:08AM Page 7 of8 Analysis Report for 05-May-16-10009 L3-10220C-FQGS-011SS (DRIED) Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin*: Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Corr + Pb-211 404.85 3.78 -2.48E-01 5.28E-01 5.28E-01 miss 427. 09 1. 76 -1.09E-01

1. 13E+OO miss 832.01 3.52 -1.88E-01 6.13E-01 miss + Bi-212 39.86 1. 06 -1.36E+OO 4.75E-01 l.70E+Ol miss 727.33 6.67 2.19E-01 4. 75E-01 miss 785.37 1.10 2.52E-01 2. 39E+OO miss 1620.50 1. 47 4.05E-01 l.77E+OO miss + Pb-212 115 .18 0.60 1.66E+OO 5. 72E-02 4.48E+OO miss 238.63

• 43.60 3.32E-01 5.72E-02 miss 300.09 3.30 3.82E-01 7. 33E-01 miss + Pb212-XR 74.82 10.28 5.44E-01 4. 96E-01 8.72E-01 miss 77 .11 17.10 4.70E-01 4. 96E-01 miss 87.35 3.97 7.25E-01 1.21E+OO miss 89.78 1. 46 5.59E-01 2. 97E+OO miss + Bi-214 609.32

• 45.49 2.09E-01 6.65E-02 6.65E-02 miss 768.36

• 4.89 5.34E-01 4.52E-01 miss 806.18 1. 26 8.43E-01 2.42E+OO miss 934.06 3.11 -1.31E-01

8. 60E-01 miss 1120.29 14.92 1.48E-01 2. 94E-01 miss 1155. 21 1. 63 4.45E-02 l.56E+OO miss 1238.12 5.83 2.68E-01 7.46E-01 miss 1280.98 1. 43 8.81E-01 2.21E+OO miss 1377. 67 3.99 3.15E-01 7. 61E-01 miss 1385. 31 0.79 5.67E-01 3.17E+OO miss 1401.52 1. 33 1.87E-01 1.91E+OO miss 1407.99 2.39 3.65E-01 1.22E+OO miss 1509.21 2.13 3.03E-01 1.26E+0D miss 1661.27 1. 05 2.46E-01 2.27E+OO miss 1729.59 2.88 3. 96E-01 1.04E+D0 miss 1764.49 15.30 2.28E-01 3.31E-Ol miss 1847.43 2.03 6.93E-01 1. 96E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241. 9 9

• 7.25 4.22E-Ol 7.93E-02 3.15E-01 miss 295.22

• 18.42 1.86E-01 l.55E-01 miss 351.93

• 35.60 2.14E-01 7. 93E-02 miss 785.96 1. 06 -2.95E-01 2.32E+OO miss + Pb214-XR 74.82 5.80 9.65E-01 8.74E-01 1.55E+OO miss 77 .11 9.70 8.28E-01 8.74E-01 miss 87.35 2.24 J.,.29E+OO 2.14E+OO miss 89.78 0.82 9.95E-01 5.30E+OO miss + Ra-226 186.21 3.64 6.71E-Ol 7.28E-01 7.28E-01 miss + Ac-228 129.07 2.42 1.39E-01 1.12E-01 1.09E+OO miss 209.25 3.89 2.93E-01 6.44E-01 miss 270.24 3.46 2.53E-Ol 7.17E-01 miss 328.00 2.95 -9.93E-02 8.18E-01 miss 338.32

• 11. 27 2.72E-01 2.35E-01 miss 409.46 1. 92 3.85E-01 1.27E+OO miss 463.00

• 4.40 3.29E-01 5.78E-01 miss 794.95 4.25 5.43E-01 7.76E-01 miss 911. 20

• 25.80 3.lOE-01 l.12E-D1 miss 964. 77 4.99 1.41E-01 6.77E-01 miss 5/5/2016 11:10:0SAM Page 8 of8 Analysis Report for 05-May-16-1 0009 L3-10220C-FQGS-011SS (DRIED) Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr Ac-228 968. 97

• 15.80 3.0lE-01 l.12E-01 1. 68E-01 miss 1588.20 3.22 3.08E-01 9.95E-01 miss + Pa-231 27.36 10.30 -2.21E-01 9.51E-01 1.85E+OO miss 283.69 1. 70 4.25E-01 l.32E+OO miss 300.07 2.47 5.llE-01 9.79E-01 miss 302.65 2.20 -2.95E-01 9.51E-01 miss 330.06 1. 40 6.lOE-01 l.BOE+OO miss + Th-234 92.38 2.13 8.82E-01 2.24E+OO 2.24E+OO miss 92.80 2.10 l.31E+OO 2.29E+OO miss 112. 81 0.21 -4.55E+OO l.33E+Ol miss + U-235 143.76 10. 96 1. 52E-02 4.35E-02 l.87E-01 miss 163.33 5.08 l.97E-01 4. 65E-01 miss 185.71 57.20 2.82E-02 4.35E-02 miss 202 .11 1. 08 l.26E-01 1.83E+OO miss 205.31 5.01 l.lBE-01 4.17E-01 miss + Am-241 59.54 35.90 l.90E-01 6.14E-01 6.14E-01 miss + = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum > ; MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

II) ...... C: ::::s 60 55 50 40 35 8 30 25 20 15 10 5 ;:!; .... t?. 1::l ' !;! 1000 2000 ._ :::'.l .l, u .... ..... ' 3000 0000014854.CNF 4000 channel 5000 Live Time :1800.000 sec Real Time :1803.100 sec start: 1: -0. l(kev) stop : 8192: 2047. O(kev) Acq. start :Thu May 05 10: 39: 24 2016 6000 7000 8000

Printed: 6/12/2018 3:20 PMPage 1 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnits17-03011-01LCSKNOWN03/03/17 00:003/3/20173/14/201717-0 3011Nickel-63ASTM 3500-Ni Modified1.51E+034.52E+01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.52E+039.33E+009.01E+012.11E+00pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.58E+001.27E+001.27E+002.11E+00UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.19E+001.39E+001.39E+002.29E+00UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.71E+001.37E+001.37E+002.28E+00UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified3.46E+001.39E+001.40E+002.25E+00pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.88E-011.36E+001.36E+002.31E+00UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified-1.69E+001.65E+001.65E+002.90E+00UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified6.89E-011.40E+001.40E+002.37E+00UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified8.22E-011.30E+001.30E+002.20E+00UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.06E+001.27E+001.27E+002.13E+00UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified3.84E+001.40E+001.42E+002.25E+00pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.34E+001.48E+001.49E+002.44E+00UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.97E+001.36E+001.37E+002.26E+00UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.09E+001.42E+001.42E+002.39E+00UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified9.12E-011.44E+001.44E+002.44E+00UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.02E+011.52E+001.64E+002.24E+00pCi/g17-03011-01LCSKNOWN03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.43E+013.04E-01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.16E+011.65E+002.15E+018.24E-01pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified-2.14E-024.23E-014.23E-019.04E-01UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified7.78E-013.45E-014.39E-016.48E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.42E-013.48E-013.96E-016.83E-01UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.59E-013.59E-013.81E-017.29E-01UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.97E-013.66E-013.91E-017.40E-01UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.85E-014.17E-014.64E-018.27E-01UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.39E-023.97E-013.98E-018.41E-01UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified9.84E-013.37E-014.80E-016.09E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified4.59E-013.45E-013.80E-016.86E-01UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.36E-013.86E-014.45E-017.54E-01UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified8.09E-014.19E-015.05E-018.12E-01UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified7.29E-013.98E-014.72E-017.75E-01UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.09E-013.90E-014.04E-018.00E-01UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified1.03E-013.61E-013.62E-017.59E-01UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.03E-013.78E-014.17E-017.53E-01UpCi/gZion, IL 60099Work Order Details:67149817-03011SOEN VIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh BlvdCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:20 PMPage 2 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-01LCSKNOWN03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified6.21E+012.48E+00pCi/g17-03011-01LCSKNOWN03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified3.94E+011.58E+00pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified7.58E+015.03E+006.36E+006.59E-01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.44E+014.02E+004.62E+006.97E-01pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.74E-024.81E-024.82E-028.85E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified1.72E-022.56E-022.57E-024.39E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.29E-021.46E-021.46E-022.73E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-1.28E-041.27E-021.27E-021.91E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.40E-031.48E-021.48E-022.34E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.37E-011.68E-011.69E-013.28E-01UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Lead-212LANL ER-130 Modified6.28E-031.70E-021.70E-022.64E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Lead-214LANL ER-130 Modified-3.01E-032.42E-022.42E-023.65E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified-5.23E-034.16E-024.16E-026.34E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.11E-011.33E-011.34E-012.02E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.84E-011.17E-011.19E-011.04E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-2.54E-033.32E-023.32E-024.18E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified2.64E-041.18E-021.18E-024.72E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified5.75E-024.30E-024.31E-027.05E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.01E+011.11E+001.23E+004.65E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified4.00E-015.25E-025.64E-028.50E-02pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.90E-011.31E-011.33E-019.32E-02pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.46E-016.92E-027.04E-025.39E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.23E-011.04E-011.06E-012.03E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.66E-011.11E-011.13E-018.49E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified4.50E-043.33E-023.33E-023.46E-02UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-5.96E-031.09E-021.09E-024.15E-02UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.04E-023.06E-023.08E-024.76E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.02E+011.13E+001.24E+005.53E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.75E-015.11E-025.46E-028.70E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified4.00E-011.33E-011.35E-011.11E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified1.86E-016.47E-026.54E-026.95E-02pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:20 PMPage 3 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.95E-016.68E-026.98E-022.26E-01pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.88E-016.28E-026.59E-028.04E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.89E-022.04E-022.04E-022.86E-02UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-3.06E-031.04E-021.04E-022.78E-02UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.11E-016.15E-026.50E-023.88E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified6.85E+008.02E-018.76E-012.60E-01pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.45E-015.27E-025.56E-024.16E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.73E-016.08E-026.37E-027.27E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.93E-017.55E-027.82E-026.80E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.14E-011.00E-011.02E-011.05E-01pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.82E-017.07E-027.34E-027.96E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified2.05E-031.95E-021.95E-022.33E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified4.00E-036.34E-036.34E-032.49E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified2.25E-022.00E-022.01E-023.30E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified8.06E+001.03E+001.11E+004.94E-01pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.61E-011.24E-011.26E-016.77E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.73E-011.30E-011.31E-016.84E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.87E-017.16E-027.31E-025.18E-02pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.85E-011.06E-011.07E-012.08E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.30E-019.29E-029.55E-021.27E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.61E-039.25E-039.25E-035.27E-02UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified8.33E-031.55E-021.55E-024.39E-02UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.93E-011.06E-011.12E-016.05E-02pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified4.65E+007.78E-018.14E-015.30E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.59E-025.32E-025.33E-021.04E-01UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.45E-018.88E-029.05E-021.15E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.39E-018.59E-028.67E-021.47E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:20 PMPage 4 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.93E-011.05E-011.06E-012.39E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.41E-016.34E-026.57E-021.35E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-3.32E-024.28E-024.28E-025.98E-02UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified6.49E-032.04E-022.04E-024.57E-02UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.03E-017.19E-027.49E-028.51E-02pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified8.03E+001.20E+001.27E+006.92E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.68E-015.53E-025.84E-021.09E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified2.92E-016.40E-026.57E-021.03E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified4.27E-011.02E-011.04E-011.72E-01pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.67E-011.03E-011.03E-017.51E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.06E-016.14E-026.33E-026.49E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.29E-021.47E-021.47E-021.62E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified1.85E-035.88E-035.88E-032.29E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified5.77E-031.18E-021.18E-021.84E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified4.97E+006.50E-016.98E-013.09E-01pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Lead-212LANL ER-130 Modified2.92E-019.35E-029.47E-025.97E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.26E-011.09E-011.11E-015.08E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.49E-016.26E-026.39E-026.96E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.56E-018.81E-029.11E-021.90E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.52E-011.14E-011.16E-017.67E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-1.95E-032.38E-022.38E-022.96E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-2.43E-031.04E-021.04E-023.39E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified1.68E-021.97E-021.97E-023.18E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified5.89E+007.05E-017.67E-014.46E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.13E-015.35E-025.96E-028.50E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Lead-214LANL ER-130 Modified4.53E-011.30E-011.32E-016.76E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.20E-016.85E-027.04E-023.88E-02pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:20 PMPage 5 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.10E-011.38E-011.39E-012.87E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified2.90E-018.05E-028.19E-021.08E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-1.08E-024.50E-024.50E-025.74E-02UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified7.65E-031.58E-021.58E-024.69E-02UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified3.28E-016.71E-026.92E-028.42E-02pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified9.77E+001.40E+001.49E+006.37E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.17E-015.43E-025.66E-029.23E-02pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.38E-017.09E-027.30E-021.13E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.08E-011.13E-011.14E-011.65E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.28E-018.53E-028.80E-021.50E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.40E-017.01E-027.22E-029.44E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.84E-022.40E-022.40E-023.33E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-2.32E-022.89E-022.89E-023.14E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified2.81E-022.43E-022.43E-023.95E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified7.18E+008.97E-019.70E-015.24E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.13E-017.92E-028.35E-026.71E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.46E-015.95E-026.21E-027.38E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.96E-018.55E-028.78E-021.12E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.89E-011.08E-011.09E-011.71E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.18E-018.65E-028.91E-027.83E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified6.19E-032.06E-022.06E-022.63E-02UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified6.73E-031.17E-021.17E-022.91E-02UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.84E-022.08E-022.11E-023.89E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified7.14E+009.28E-019.97E-014.26E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.24E-011.13E-011.15E-019.05E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.61E-011.29E-011.30E-015.38E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.52E-017.63E-027.74E-021.17E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:20 PMPage 6 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S ampleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i on Solutions101 Shiloh Blvd17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified2.73E-019.62E-029.72E-021.03E-01pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.99E-016.02E-026.21E-026.14E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified2.51E-021.55E-021.56E-022.24E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified-5.07E-039.42E-039.43E-032.76E-02UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified3.38E-014.02E-024.38E-023.33E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.77E+008.72E-019.39E-013.88E-01pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Lead-212LANL ER-130 Modified3.17E-011.10E-011.11E-016.70E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Lead-214LANL ER-130 Modified2.31E-018.83E-028.91E-025.75E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified3.12E-017.53E-027.70E-025.09E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified3.28E-015.75E-025.99E-021.19E-01pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.77E-015.55E-025.72E-027.49E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified2.22E-031.65E-021.65E-022.20E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified2.87E-036.84E-036.84E-031.89E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified2.03E-021.30E-021.30E-022.04E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.22E+006.92E-017.62E-012.36E-01pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Lead-212LANL ER-130 Modified2.87E-014.16E-024.42E-024.20E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Lead-214LANL ER-130 Modified2.66E-014.22E-024.44E-024.27E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified2.87E-015.58E-025.77E-024.54E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified3.84E-011.09E-011.11E-012.05E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.85E-019.70E-029.81E-021.05E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified8.55E-033.20E-023.20E-025.09E-02UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified1.76E-031.48E-021.48E-024.53E-02UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified3.37E-016.23E-026.46E-027.54E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.05E+008.31E-018.87E-015.71E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Lead-212LANL ER-130 Modified4.33E-015.83E-026.23E-028.32E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Lead-214LANL ER-130 Modified3.29E-011.49E-011.50E-011.23E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified2.56E-018.59E-028.69E-021.05E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect