Text

Restoration Project - Final Status Survey Release Record, Area Far South of Switchyard Survey Unit 10219B - Final Report - Phase 1, Revision 1
	ML19178A101
Person / Time
Site:	Zion File:ZionSolutions icon.png
Issue date:	06/20/2019
From:	Yetter R; ZionSolutions
To:	; Office of Nuclear Material Safety and Safeguards
Shared Package
MML19178A106	List: ML19178A098; ML19178A100; ML19178A101; ML19178A102; ML19178A103; ML19178A104; ML19178A105; ML19178A107; ML19178A108; ZS-2019-0043, Transmittal of Revised Final Status Survey Report - Phase 1;
References
	ZS-2019-0043
	Download: ML19178A101 (183)
	v • d • e

=ZION SOLUTIONS LLC-An EnergySo/utions Company

=11+++ ()=1 1 3.630 ()+ 0.002 3.095 ()=3.622 / ()=1 1 1.091 ()+180.45914.458 ()=0.898 /

()=1 0.012 0.898 ()+0.00001 1.733+ 0.988 3.622 ()=3.494 /

10/3/~ 8:1 7:07AM .~~~pex-Gamma Analysis Report tor 03-0ct-16-10001 L3-102198-FRGS-001 SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real lime Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 03-0ct-16-10001

L3-102198-FRGS-001SS

1L 130G Soil Sample 1.500E+03 grams : Default : 9/27/2016 8:15:00AM

10/3/2016 7:48:39AM

130G 1 L Soil Sample : JWelch : P408188 : 130G Soil : 600.0 seconds : 600.9 seconds : 0.16 % : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15996 PEAK WITH NID REPORT Peak Analysis Performed on 10/3/2016 7:58:42AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM f..l*'\.~ c.F to/-S /z.o '"" P age I of8 10/3/21..

8:17:07AM Page 2 of8 Analysis Report for 03-0ct-16-10001 L3-102198-FRGS-001 SS Peak Energy ROI No. (keV) start 1 238.56 949 -2 351. 7 6 14 00 -3 583.47 2329 -4 609.1 7 2430 -5 911.15 3640 -6 1460.48 5835 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1413 2338 2443 3649 5853 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.74 6.99E+Ol 23.04 5.03E+Ol 1 407.22 7.04E+Ol 20.14 2.53E+Ol 2333.67 1.71E+Ol 11. 82 1.77E+Ol 2436.43 4.74E+Ol 1 6.55 1.71E+Ol 3644.30 2.79E+Ol 1 1. 29 4.27E+OO 5842.89 1.06E+02 22.39 1.63E+Ol NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield("/o)

Activity Activity Name Confidence (keV) (pCilgrams)

Uncertainty K-40 0.99 1460.8 2

10.66 4.3 3E+OO 9.90E-Ol Tl-208 0.99 583.19

85.00 5.1 9E-02 3.64E-02 B i-211 0.97 351.07

13. 02 8.86E-Ol 2. 91E-Ol Pb-212 1. 00 115.18 0.60 238.63

43.60 2.05E-01 7.54E-02 300.09 3.30 Bi-2 14 0.99 609.32

45.49 2.70E-01 9.98E-02 768.36 4.89 806.18 1. 2 6 934.06 3 .11 1120.29 14.92 1155. 21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1 407.99 2.39 1509.21 2 .13 1661.27 1. 05 17 2 9.59 2.88 Tentative Nuclide Pb-212 Pb-214 Bi-2 11 Tl-208 Bi-2 14 Ac-228 K-40 Coinc Corr miss 0.932 miss free 0.948 Analysis Report for 03-0ct-16-10001 L3-10219B-FRGS-001 SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1764.49 1847.43 2118.51 Pb-214 0.51 24 1.99 295.22 35 1. 93 785. 96 Ac-22 8 1. 00 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911.20 964. 77 968. 97 1588.20 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed. free = No coincidence correction required.

Yield{°A) 15.30 2.0 3 1.1 6 7.25 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4 .25 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 10/3/2l, -8:17:0?AM Page 3 of8 Activity Activity Caine (pCilgrams)

Uncertainty Corr 3.2 4E-01 1.0 6E-0 1 free 3.46E-01 1.43E-01 0.990 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.993 4.33E+OO 9.90E-01 Tl-208 0.995 5.19E-02 3.64E-02 ? Bi-211 0. 971 8.86E-01 2.91E-01 Pb-21 2 1.000 2.05E-01 7.54E-02 Bi-214 0.999 2.70E-01 9.98E-02 Analysis Report for 03-0ct-16-10001

? L3-10219B-FRGS-001 SS Nuclide Nuclide Name Id Confidence Pb-214 0.512 Ac-228 1. 000 ? = nuclid e is part of an undetermined solution X = nuclid e rejected by the interference analysis 10/3/21., Wt mean Activity (pCi/grams) 3.24E-01 3.46E-01 @ = nuclid e contains energy l i nes not used in Weighted Mean Activity Errors quoted at 2.000sigma 8: 17: 0?AM Page 4 of8 Wt mean Comments Activity Uncertainty

1. 06E-01 1.43E-01 10/3/21., Analysis Report for 03-0ct-16-10001 L3-10219B-FRGS-001 SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/3/2016 7:58:42AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 8:17:07AM Peak Type Page 5 of8 Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCUgrams) (pCilgrams)

Corr + K-40 1460.82

10.6 6 4.33E+OO 7.04E-01 7.04E-01 miss + Cr-51 320.08 9.9 1 -8.47E-02

2. 72E-01 2. 72E-Ol free + Mn-54 834.85 99.98 -9.04E-04 3.95E-02 3.95E-02 miss + Co-58 810.76 99.45 -l.30E-03 2.89E-02 2.89E-02 1.000 1674.73 0.52 O.OOE+OO '.2.62E+OO 1. 024 + Co-60 1173.2 3 99.85 l.37E-02 3.17E-02 5.19E-02 0.947 1332.49 99.98 4.31E-03 3 .17E-02 0.947 + Nb-94 702. 65 99.81 6.56E-04 2.39E-02 3.69E-02 0.944 871.09 99.89 3.24E-03 2.39E-02 0.944 + Ag-108 m 79 .13 6.60 1.76E-01 2.85E-02 1.33E+OO miss 433.94 90.50 -1.02E-02 2.85E-02 0.887 614.28 89.80 3.53E-03 3.99E-02 0.886 722. 94 90.80 4.33E-03 4.03E-0 2 0.887 + Sn-113 255 .13 2 .11 5.05E-03 3.04E-02 1.28E+OO free 3 91. 70 64.97 -2.71E-02 3.04E-02 free + Cs-134 475.36 1.48 -1.38E-02 3.98E-02 2.60E+OO miss 563.25 8.34 4.37E-02 4.87E-01 0.896 569.33 15.37 1. 4 9E-01 3.18E-01 0.888 604. 72 97.62 6.88E-03 3.98E-0 2 0.931 10/3/2l, . 8:17:0?AM Page 6 of8 Analysis Report for 03-0ct-16-10001 L3-10219B-FRGS-001 SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)

Corr Cs-134 795.86 85.46 2.54E-02 3.98E-02 5.45E-02 0.933 80 1. 95 8.69 7.46E-0 2 3.46E-01 0.898 1038.61 0.99 -3.lOE-0 2 3.45E+OO 0.943 11 67.97 1. 79 2.49E-01 2.08E+OO 1. 081 1 365.19 3.0 2 O.OOE+OO 3.31E-01 1.128 + Cs-137 661.66 85.10 2.84E-02 6.02E-02 6.02E-02 miss + Eu-152 12 1.78 28.67 -3.80E-02 1.llE-01 1.30E-01 0.936 244.70 7.61 -3.51E-02 3.45E-01 0.935 295.94 0.45 2.05E+OO 9.39E+OO miss 344.2 8 2 6.6 0 -2.75E-02 1.llE-01 0.957 367.79 0.86 -1.50E+OO 3.34E+OO 0.884 4 11.12 2.2 4 -1. 2 1E-01 1. 3 6E+00 0.908 443. 96 2.83 3.90E-02 1.03E+OO 0.934 488.68 0.42 2.17E+OO 7.81E+OO miss 563.99 0.49 -1. 2 1E+OO 6.52E+OO 0.934 586.2 6 0.46 -2. 71E+OO 9.02E+OO 0.94 2 678. 62 0.47 1.13E+OO 7.43E+OO 0.887 688.67 0.86 2.59E+OO 5.41E+OO 0.980 719.35 0.28 5.36E-01 1.04E+Ol miss 778.90 12. 96 -5.80E-02 2.50E-01 0.945 810.45 0.3 2 -1.44E+OO 8.04E+OO 1. 050 867.37 4.26 -1.42E-01 7.17E-01 0.928 919.33 0.43 1. 52E+OO 8.16E+OO 0.981 964. 0 8 14.65 1.68E-01 3.82E-01 1.02 2 10 85.87 10.2 4 -6.34E-02 3.67E-01 1. 018 1 0 89.74 1. 73 1.07E+OO 3.05E+OO 0.952 1112. 07 13.69 9.50E-03 3.19E-01 0.992 1212.95 1. 43 -2.27E-01 2.68E+OO 0.929 1249.94 0.19 -1.2 5E+Ol 1.75E+Ol 1.097 1 299.1 4 1. 63 -6.34E-01 1.92E+OO 0.944 1408.0 1 2 1. 07 3.42E-02 2.2 1E-01 0.983 1457.64 0.50 -7.75E+OO 1.34E+Ol 1. 076 1 528.10 0.28 l.59E+OO 1.17E+Ol 1. 007 + Eu-154 123.07 40.40 5.31E-02 8.94E-02 l.09E-01 0.9 3 4 247.93 6.89 -1.32E-02 4.38E-01 0.928 591.76 4.95 3.02E-01 8.27E-01 0.915 692.42 1. 78 -1.0SE+OO l.1 6E+OO 0.936 723.30 20.06 -1.04E-02

1. 55E-01 0.935 756.80 4.52 -2.81E-01 8.09E-01 0.915 873.18 12.08 O.OOE+OO 2.0lE-01 0.932 996.29 10.48 O.OOE+OO 8.94E-02 0.971 100 4.76 18.01 6.08E-02 2.52E-01 0.978 1274.43 34.80 -2.15E-02 1.08E-01 0.981 1 596.48 1. 80 8.31E-02 2.06E+OO 1.175 + E u-1 55 45.30 1. 31 1. 42E+Ol 1.91E-01 2.67E+Ol 0.999 60.01 1. 22 8.45E+OO 2.59E+Ol 1.000 86.55 3 0.70 1. 71E-02 1.98E-01 free 105.31 21.10 -2.54E-03 l.91E-01 1. 000 + Tl-208 583.19

85.00 5.19E-02 4.89E-02 4.89E-02 0.932 + Bi-211 351.07

13.02 8.86E-01 2.05E-01 2.65E-01 miss + Pb-211 404.85 3.78 8.4"7E-02 9.03E-01 9.03E-01 miss 10/3/21, 8:17:0?AM Page 7 of8 Analysis Report for 03-0ct-16-10001 L3-102198-FRGS-001 SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCl/grams) (pC//grams)

Corr Pb-211 427.09 1. 76 -3.38E-0 1 9.03E-01 1.40E+OO mis s 832.01 3.5 2 1. 60E-01 l.lOE+OO mis s + Bi-2 1 2 39.86 1. 06 9.90E+OO 9.06E-01 2.75E+Ol 0.998 727. 33 6.67 5.99E-01 9.06E-01 0.982 785.37 1.10 5.49E-02 3. 60E+OO O. 944 1 620.50 1. 47 -2.00E-01 2. 35E+OO 1. 006 + Pb-212 115.18 0.60 -1.30E+00 8.46E-02 5.48E+OO miss 238.63

43.60 2.05E-01 8.46E-02 free 300.09 3.30 -5.46E-0 2 9.04E-01 free + Pb21 2-XR 74.8 2 10.2 8 2.15E-01 7.35E-01 l.2 2E+OO miss 77 .11 17.10 2.70E-01 7.3 5E-01 miss 87.35 3.97 4.69E-01 1.47E+OO miss 89.78 1. 46 -4.74E-01 3.56E+OO miss + Bi-214 609.32

45.49 2.70E-01 9.93E-02 9.93E-02 0.948 768.36 4.89 5.86E-01 l.19E+OO 0.94 2 806.18 1. 26 9.55E-0 1 3.51E+OO 0.923 934.06 3.11 5.48E-02 1.55E+OO 0.944 1120.2 9 14.9 2 2.75E-01 5.1 8E-01 0.944 1155.2 1 1. 63 -6.18E-01 2.59E+OO 0.94 3 1238.12 5.83 4.2 7E-02 l.12E+OO 0.944 1280.98 1. 43 -2.09E-01 2.15E+OO 0.944 1377. 67 3.99 3.71E-01 1.33E+OO 1. 030 1385. 31 0.79 3.99E-01 4.12E+OO 0.945 1401.52 1. 33 -l.44E-01 3.12E+OO 0.945 1 407.99 2.39 3 .13E-01 2.02E+OO 0.945 1 509.2 1 2.13 -1.90E-01 l.63E+OO 0.950 1661.27 1. 05 O.OOE+OO l.24E+OO 1. 001 1729.59 2.88 -1.93E-01 1.43E+OO 1.119 1764.49 15.30 4.35E-01 6.63E-01 1. 001 1847.43 2.03 -2. llE-01 1.78E+OO 1.063 > 211 8. 51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 2 41.99 7.25 5.2 2E-01 9.69E-02 5.60E-01 1. 000 2 95.22 18.42 1.03E-01 2.3 1E-01 1.000 351.93

3 5.60 3.2 4E-01 9.69E-02 free 785.96 1. 06 -5.09E-01 2.90E+OO 1. 000 + Pb214-XR 74.82 5.80 3.82E-01 1.3 0E+OO 2.16E+OO miss 77 .11 9.70 4.76E-01 l.30E+OO miss 87.35 2.24 8.31E-01 2.61E+OO miss 89.78 0.82 -8.45E-01 6.34E+OO miss + Ra-22 6 186.21 3.64 3.88E-01 9.73E-01 9.73E-01 free + Ac-228 129.07 2.42 1. 42E-01 1. lSE-01 1.57E+OO 0.944 209.25 3.89 7 .13E-02 7.llE-01 0.978 270.24 3.46 8.40E-02 9.87E-01 0.955 328.00 2.95 -9.75E-02 1. 05E+OO 0.955 338.32 11. 27 2.62E-01 3.65E-01 0.99 2 409.46 1. 92 9.69E-01 1. 98E+OO 0.937 463.00 4.40 3.38E-01 9.44E-01 0.933 794.95 4.2 5 1.70E-0 1 9.42E-01 0.942 911.20

2 5.80 3.46E-Ol 1.15E-01 0.990 964.77 4.99 -6.71E-02 8.80E-01 0.981 968. 97 15.80 1.53E-01 3. 96E-01 0.990 Analysis Report for 03-0ct-16-10001

+ + + + + * > L3-102198-FRGS-OO 1 SS Nuclide Energy Yield(%) Activity Name (keV) (pCi/grams)

Ac-228 1588.2 0 3.2 2 O.OOE+OO Pa-231 27.36 10.30 -4.41E-01 283.69 1. 70 8.99E-01 300.07 2.47 -7.2 9E-02 302.65 2.20 1.57E-01 330.06 1. 40 9.87E-01 Th-234 92.38 2.1 3 1.67E+OO 92.80 2.10 l.02E+OO 112. 81 0.2 1 -1.20E+Ol U-235 143.76 10. 96 -6.59E-0 2 163.33 5.08 -4. 72E-01 185. 71 57.20 4.07E-0 2 202.11 1. 08 -3.71E-01 205.31 5.01 1. 06E-01 Am-241 59.54 35.90 2.33E-02 = Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/3/2(, NuclideMDA (pCilgrams) 1.15E-01 1.2 1E+OO 3.32E+OO 6.62E-02 8.91E-Ol ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 8:17:0?AM Page 8 of8 LineMDA Coinc (pCilgrams)

Corr 1.55E+OO 1. 002 2.SOE+OO 0.998 2.llE+OO 1. 000 l.2 1E+OO 1. 000 1.2 8E+OO 1. 000 2.46E+OO 1. 000 3.52E+OO free 3.3 2E+OO free l.95E+Ol free 2.97E-01 free 4.92E-01 free 6.62E-0 2 free 2.69E+OO miss 6.08E-01 free 8.91E-01 free 60 55 50 45 40 35 VI +-' C: :::::, 8 30 25 1000 ..Q 0.. ..... a, 2000 3000 0000015996.CNF 4000 channel 5000 Live Time :600.000 sec Real Time : 600.940 sec start: 1: -0.l(kev) stop : 8192:2047 .O(kev) Acq. Start : Mon Oct 03 07:48:39 2016 6000 7000 8000 10/3/:.C ., 9:32:04AM

~~~pex Gamma Analysis Report for 03-0ct-16-10002 L3-102198-FRGS-002SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range {in channels)

Peak Area Range {in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 03-0ct-16-10002

L3-102198-FRGS-002SS

1 L 130G Soil Sample 1.057E+03 grams : Default : 9/27/2016 9:52:00AM

10/3/2016 9:03:40AM

130G 1 L Soil Sample : JWelch : P408188 : 130G Soil : 600.0 seconds : 601.0 seconds : 0.16 % : 2.80 : 120-8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15997 PEAK WITH NID REPORT Peak Analysis Performed on 10/3/2016 9:13:43AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce ~K"A v-,~'c-.&--D cS:3lo--\013/J Jo : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 10/3/2(,. 9:32: 04AM Page 2 of8 Analysis Report for 03-0ct-16-10002 L3-102198-FRGS-002SS Peak Energy ROI No. (keV) start 1 77.01 305 -2 238.47 949 -3 351.66 140 3 -4 609.44 2 432 -5 661.39 2 637 -6 910.87 3639 -7 1460.60 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 314 961 1414 2 442 2 653 3649 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 309 .11 1.60E+Ol 17.70 4.60E+Ol 954.37 5.17E+Ol 23.82 6.66E+Ol 1406.8 2 4.30E+Ol 16.76 2.40E+Ol 2437.51 3.13E+Ol 12. 99 9.38E+OO 2645.2 5 6.61E+Ol 17.1 2 5.75E+OO 3643.19 1.68E+Ol 9.33 4.46E+00 5843.37 9.36E+Ol 19.69 2.78E+00 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0.99 1460.82

10.66 5.44E+OO 1.2 4E+00 Cs-137 0.99 661.66

85.10 2.81E-01 8.0lE-02 Bi-21 1 0.97 351.07

13. 02 7.68E-01 3.24E-01 Pb-212 0.99 115.18 0.60 238.63

43.60 2.1 6E-01 1.05E-01 300.09 3.30 Pb212-XR 1. 00 74.8 2 10.28 77 .11

17.10 4.95E-01 5.56E-01 87.3 5 3.97 89.78 1. 46 Bi-2 14 1. 00 609.32

45.49 2.53E-01 1.09E-01 768.36 4.89 806.18 1.2 6 934.06 3.11 1120.29 14.92 1155. 2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 Tentative Nuclide Pb214-XR Pb212-XR Pb-212 Pb-214 Bi-211 Bi-214 Cs-137 Ac-228 K-40 Caine Corr miss miss miss free miss 0.948 Analysis Report for 03-0ct-16-10002 L3-10219B-FRGS-002SS Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1385. 31 1401.52 1407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2 118.51 Pb-214 0.99 2 41.99 2 95.22 351.93 785. 96 Pb214-XR 1. 00 74.82 77.11 87.35 89.78 Ac-228 0.99 129.07 209.25 270.24 328.00 338.32 409.46 463.00 794.95 911.2 0 964. 77 968. 97 1588.20 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance:

1.000FWHM Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 0.79 1. 33 2.39 2.13 1. 05 2.88 15.30 2.03 1.1 6 7.25 18.42 35.60 1. 06 5.80 9.70 2.24 0.8 2 2.4 2 3.89 3.46 2.95 11.27 1. 92 4.40 4.2 5 2 5.80 4.99 15.80 3.2 2 miss = Nuclide energy was not found in the coincidence library. 10/3/2(, 9:32:04AM Page 3 of8 Activity Activity Coinc (pCi/grams)

Uncertainty Corr 2.81E-01 l.1 8E-01 free 8.72E-01 9.84E-01 miss 2. 96E-0 1 l.67E-Ol 0.990 INTERFERENCE CORRECTED REPORT Analysis Report for 03-0ct-16-10002

? ? ? ? ? = X = L3-102198-FRGS-002SS Nuclide Nuclide Name Id Confidence K-40 0.997 Cs-137 0.996 Bi-211 0.979 Pb-212 0.999 Pb212-XR 1. 000 Bi-214 1. 000 Pb-214 0.997 Pb214-XR 1. 000 Ac-228 0.998 nuclide is part of ali undetermined solution nuclide rejected by the interference analysis 10/3/21..

Wt mean Activity (pCi/grams) 5.44E+OO 2.81E-Ol' 7.68E-01 2.16 E-01 4.95 E-01 2.53E-01 2.81E-01 8. 72E-01 2.96E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 9:32:04AM Page4 of8 Wt mean Comments Activity Uncertainty 1.24E+OO 8.0lE-02 3.24E-01 1.0SE-01 5.56E-01 1.09E-01 1.18E-01 9.84E-01 1.67E-01 10/3/2l, Analysis Report for 03-0ct-16-10002 L3-10219B-FRGS-002SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/3/2016 9: 13:43AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 9:32:04AM Peak Type Page 5 of~ Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCi/grams) (pCi!grams)

Corr + K-40 1460.82

1 0.6 6 5.44E+OO 5.06E-01 5.06E-01 miss + Cr-5 1 320.08 9.9 1 1.17E-01 4.47E-0 1 4.47E-01 free + Mn-54 834.85 99.98 7.13E-04 4.60E-02 4.60E-02 miss + Co-58 810.76 99.45 l.47E-03 5.30E-02 5.30E-0 2 1. 000 1674.73 0.52 O.OOE+OO 3. 72E+OO 1. 024 + Co-60 117 3.23 99.85 1.77E-02 5.67E-02 7.37E-02 0.947 1332.49 99.98 6.98E-0 3 5.67E-0 2 0.947 + Nb-94 702.65 99.81 -1.33E-03 3.71E-02 3.71E-02 0.944 871.0 9 99.89 5.75E-03 5.53E-02 0.944 + h.g-108m 79.13 6.60 -3.31E-0 1 4.64E-02 1.44E+OO miss 433.94 90.50 9.42E-03 5.86E-0 2 0.887 614.28 89.80 5.75E-04 4.64E-02 0.886 722.94 90.80 -1.80E-0 2 5.12E-02 0.887 + Sn-113 255.1 3 2 .11 -1.86E-01 7.2 8E-02 2.14E+OO free 3 91. 70 64.97 2. llE-0 2 7.28E-02 free + Cs-134 475.36 1. 48 -3.52E-01 5.30E-02 2.94E+OO miss 563.25 8.34 -4.0lE-02 5.71E-01 0.896 569.33 15.37 1.16E-01 3.81E-01 0.888 60 4. 72 97.62 1.77E-02 5.30E-0 2 0.931 10/3/21.. , 9:32:04AM Page 6 of8 Analysis Report for 03-0ct-16-10002 L3-10219B-FRGS-002SS Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 7.30E-03 5.30E-02 7.27E-02 0.933 80 1.95 8.69 l.2 5E-01 6.94E-01 0.898 1038.61 0.99 -8.79E-01 4.90E+OO 0.943 11 67.97 1. 79 O.OOE+OO 7.43E-01 1.081 1365.19 3.02 O.OOE+OO 4.70E-01 1.128 + Cs-137 661.66

85.10 2.81E-01 ~.88E-02 4.88E-02 miss + Eu-152 121.78 28.67 1.56E-02 1.65 E-01 1. 65E-01 0. 936 244.70 7.61 9.98E-02 5.23E-01 0.935 295.94 0.45 6.44E+OO l.25E+Ol miss 344.2 8 26.60 1.58E-0 2 l.70E-01 0.957 367.79 0.86 -8.65E-01 4.74E+OO 0.884 411.12 2.24 2.31E-01 2.14E+OO 0.908 443. 96 2.83 3.74E-Ol l.47E+OO 0.934 488.68 0.42 1.68E+OO 9.85E+OO miss 563.99 0.49 -2.86E+OO 8.48E+OO 0.934 586.26 0.46 1. 23E+OO 1.08E+Ol 0.942 678.62 0.47 2.61E+OO l.24E+Ol 0.887 688.67 0.86 -l.03E+OO 3.24E+OO 0.980 719.35 0.28 l.83E+OO l.80E+O l miss 778.90 1 2.96 5.81E-02 4.31E-01 0.945 810.45 0.32 -3.07E+OO 1.32E+Ol 1. 050 867.37 4.26 4.75E-02 l.44E+OO 0.928 919.33 0.43 2.58E+OO l.41E+Ol 0.981 964.08 14.65 l.99E-01 5.1 9E-01 1. 022 1085.87 10.24 -6.92E-03 4.50E-01 1. 018 1.08 9.74 1. 73 3.73E-01 3.69E+OO 0.952 11 12.07 13.69 1.44E-0 2 4.06E-Ol 0. 992 1 212.95 1. 43 -9.3 7E-01 3.02E+OO 0.929 1249.94 0.19 -8.0lE+OO l.97E+Ol 1.097 1299.14 1. 63 O.OOE+OO l.OOE+OO 0.944 1408.01 2 1. 07 2.91E-02 2.14E-01 0.98 3 1457.64 0.50 O.OOE+OO l.91E+Ol 1. 076 1528.10 0.28 O.OOE+OO 6.12E+OO 1.007 + Eu-154 1 23.07 40.40 -4.03E-0 2 l.OlE-01 l.OlE-01 0.934 2 47.93 6.89 2. llE-01 7.0lE-01 0.928 591.76 4.95 -2.91E-01 7.96E-01 0.915 692.42 1. 78 1.64E-01 2.94E+OO 0.936 723. 30 2 0.06 -7.1 6E-02 l.90E-01 0.935 756.80 4.52 -1.43E-01 7.04E-01 0.915 873.18 12.08 -1.42E-01 3.59E-Ol 0.93 2 996. 2 9 10.48 5.47E-02 5.05E-01 0.971 100 4.76 18.0 1 -l.36E-02 2.0lE-01 0.978 1 2 74.4 3 34.80 2. llE-02 l.53E-01 0.981 1596.48 1. 80 O.OOE+OO 8.51E-01 1.175 + Eu-155 45.30 1. 31 -1.03E+Ol 2.37E-01 3.02E+Ol 0.999 60.01 1. 22 -5.62E+OO 2.57E+Ol 1. 000 86.55 3 0.70 8.41E-02 2.96E-01 free 105.31 2 1.10 -6.37E-04 2.37E-01 1. 000 + Tl-2 0 8 583.19 85.00 3.90E-02 8.67E-02 8.67E-02 0.932 + Bi-2 11 351.07

13.02 7.68E-01 3.55E-01 3.55E-01 miss + Pb-2 11 404.85 3.78 4.08E-0 2 9.60E-01 9.60E-01 mi ss 10/3/21., 9:32:04AM Page 7 of8 Analysis Report for 03-0ct-16-10002 L3-10219B-FRGS-002SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCl/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 -2.12E-01 9.60E-0 1 1.82E+OO mis s 8 32.0 1 3.52 1.8 7E-01 1.57E+OO mis s + Bi-212 39.86 1. 06 -3.71E+OO 8 . .2 8E-01 2.49E+Ol 0.998 727. 33 6.67 1.37E-01 8.28E-01 0.98 2 785.37 1.10 2.60E-01 3.62E+OO 0.9 4 4 1 620.50 1.47 O.OOE+OO 1. 2 3E+OO 1. 006 + Pb-212 115 .18 0.60 2.46E+OO 1. 42E-01 9.04E+OO miss 2 38.63

43.60 2.16E-01 1.42E-01 free 300.09 3.30 4.57E-02 1.32E+OO free + Pb212-XR 74.8 2 10.28 8.61E-01 8.86E-0 1 1.58E+OO miss 77.11

17.10 4.95E-01 8.86E-01 miss 87.35 3.97 -4.40E-01 2.02E+OO miss 89.78 1. 46 4.04E-01 5.43E+OO miss + Bi-214 609.32

45.49 2.53E-01 1.0 7 E-01 l.07E-01 0.948 768.36 4.89 6.90E-01 1.51E+OO 0.94 2 806.1 8 1. 2 6 -2.36E-01 4.2 4E+OO 0.923 934.0 6 3 .11 l.04E-01 1.1 4E+OO 0.944 1120.29 1 4.9 2 1.71E-01 5.80E-01 0.944 1155.21 1. 63 1.75E+OO 5.12E+OO 0.943 1238.1 2 5.83 3.46E-01 1. 50E+OO 0.944 1280.98 1. 43 O.OOE+OO 1.12E+OO 0.944 1377.67 3.99 -4.12E-02 1.34E+OO 1.030 1385. 31 0.79 1.59E+OO 7.37E+OO 0.945 1401.52 1. 33 O.OOE+OO l.29E+OO 0.945 1 407.99 2.39 2.66E-01 1. 96E+OO 0.945 1 509.2 1 2.13 2.2 4E-01 2.31E+OO 0.9 50 1661. 27 1. 05 O.OOE+OO 1.77E+00 1.001 1729.59 2.88 1. 2 3E-01 2.03E+OO 1.119 1764.49 15.30 1.40E-01 6 .13E-01 1. 001 1847.43 2.03 1.03E+OO 3.69E+OO 1. 06 3 > 2118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 14 2 41.99 7.25 1. 2 7E-01 1.3 0E-01 6.2 1E-01 1. 000 2 95.22 18.42 2.2 3E-01 3.2 3E-01 1. 000 351.93

35.60 2.81E-01 1.3 0E-01 free 785.96 1. 06 l.2 7E-01 2.81E+OO 1. 000 + Pb214-XR 74.8 2 5.80 1. 53E+OO 1.56E+OO 2.81E+OO miss 77 .11

9.70 8. 72E-01 1.56E+OO miss 87.35 2.2 4 -7.79E-01 3.58E+OO miss 89.78 0.82 7.19E-01 9.67E+OO miss + Ra-226 1 86.2 1 3.64 3.97E-0 1 1.22E+OO 1.22E+00 free + Ac-228 129.0 7 2.42 -1.53E-0 1 1.77E-01 1. 76E+OO 0.944 209.2 5 3.89 -1.22E-01 9.04E-0 1 0.97 8 27 0.2 4 3.46 -2.94E-01 l.16E+OO 0.95 5 328.00 2.95 l.83E-01 1.38E+OO 0.95 5 33 8.32 11. 27 2.58E-01 5.18E-01 0.99 2 409.46 1. 92 9.89E-02 2.17E+OO 0.937 4 63.00 4.40 4.31E-01 1.3 4E+OO 0.933 794.95 4.25 -9.52E-0 2 l.34E+OO 0.9 42 911. 2 0

25.80 2. 96E-0 1 1.77E-01 0.990 964. 77 4.99 6.14E-0 1 1. 59E+OO 0.981 968.97 15.80 3.2 3E-0 1 5.63E-01 0.990 Analysis Report for 03-0ct-16-10002

+ + + + + > L3-10219B-FRGS-002SS Nuclide Energy Yield(%) Activity Name (keV) (pCJ/grams)

Ac-228 1588.2 0 3.22 O.OOE+OO Pa-231 27.36 10.30 3.42E-01 283.69 1.70 -1.49E-01 300.07 2.47 6.lOE-0 2 302.65 2.20 4.SlE-01 330.06 1. 40 -1.30E+OO Th-234 92.38 2.13 1.26E+00 92. 80 2.10 1.62E+OO 112. 81 0.21 2. llE+Ol U-23 5 143.76 10.96 1. llE-01 163.33 5.08 6. 96E-02 185.71 57.2 0 3.48E-02 20 2 .11 1. 08 5.40E-01 205.31 5.01 1.0lE-01 Am-241 59.54 35.90 -8.44E-02

= Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/3/21..

NuclideMDA (pCUgrams) 1.77E-01 1.77E+OO 4.36E+OO 8.33E-02 1.0lE+OO ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required. miss = i'<iuclide energy was not found in the coincidence iibrary. , 9:32:04AM Page 8 of8 LineMDA Coinc (pCi!grams)

Corr 1.51E+OO 1.002 3.lOE+OO 0.998 1.99E+OO 1. 000 1.77E+OO 1. 000 1.87E+OO 1. 000 2.25E+OO 1. 000 4.36E+OO free 4.46E+OO free 3.39E+01 free 4.2 1E-01 free 7.83E-01 free 8.33E-02 free 3.67E+OO miss 7.41E-01 free 1.0lE+OO free 60 55 50 45 40 35 1000 2000 3000 0000015997.Cl~~

4000 channel 5000 Live Time :600.000 sec Real Time :600.980 sec Start: 1: -0.l(kev) stop : 8192:2047 .O(kev) Acq. start :Mon Oct 03 09:03:40 2016 = ! 6000 7000 8000 10/31£-., 10:05:56AM

~pex-Gamma Analysis Report for 03-0ct-16-10003 L3-10219B-FRGS-003SS GAMMA SPECTRUM ANAL YS/S Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 03-0ct-16-10003

L3-10219B-FRGS-003SS

1 L 130G Soil Sample 1.468E+03 grams : Default : 9/27/2016 8:07:00AM

10/3/2016 9:37:25AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 600.0 seconds : 601.1 seconds : 0.19% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 15998 PEAK WITH NID REPORT Peak Analysis Performed on 10/3/2016 9:47:28AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Oefault\Library\Zion Lib-BNL.NLB

1.000FWHM c:S:O Page I of8 10/3/2(,. 10:05:56AM Page 2 of8 Analysis Report for 03-0ct-16-10003 L3-10219B-FRGS-003SS Peak Energy ROI No. (keV) start 1 238.63 950 -2 338.38 1347 -3 351.86 1401 -4 582.87 2325 -5 609.37 2431 -6 661. 62 2639 -7 968. 49 3868 -8 1460.75 5833 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1358 1414 2 338 2 442 2 653 3879 5853 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 955.00 1. 05E+02 30 .13 1.01E+02 1353.73 3.44E+Ol 14.99 1.92E+Ol 1407.61 6.33E+Ol 22.15 4.94E+Ol 2331. 26 3.64E+Ol 14.46 1.32E+Ol 2437.23 3.77E+Ol 14. 97 1.67E+Ol 2646.17 5.83E+Ol 17. 64 1.73E+Ol 3873.73 1.90E+Ol 10.43 7.97E+OO 5843.98 1.40E+02 23.93 2.94E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 1. 00 1460.82

10.66 5.83E+OO l.12E+OO Cs-137 1. 00 661.66

85.10 1.78E-01 5.80E-02 Tl-208 0.99 583.19

85.00 l.13E-01 4.68E-02 Bi-211 0. 96 351.07

13. 02 8.15E-01 3.14E-01 Pb-212 1. 00 115 .18 0.60 238.63

43.60 3.15E-01 1.04E-01 300.09 3.30 Bi-2 14 1. 00 609.3 2

45.49 2.19E-01 9. llE-02 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385. 31 0.79 1401.52 1. 33 1407.99 2.39 Tentative Nuclide Pb-21 2 Ac-22 8 Pb-214 Bi-2 11 Tl-208 Bi-214 Cs-137 Ac-228 K-40 Caine Corr miss miss 0.932 miss free 0.948 Analysis Report for 03-0ct-16-10003 L3-10219B-FRGS-003SS Nuclide Id Energy Name Confidence (keV) Bi-214 1. 00 1509.21 1661. 27 1729.59 1764.49 1847.43 2118.51 Pb-214 1. 00 241. 99 2 95.2 2 351.93 785.96 Ac-228 0.57 129.07 209.25 270.2 4 32 8.00 338.3 2 409.46 463.00 794.95 9 11. 20 964.77 968. 97 1588.20 * = Energy line found in the spectrum.

-"' Manually added nuclide. ? = Manually edited nuclide. * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2 .13 1. 05 2.88 15.30 2.03 1.16 7.2 5 18.42 35.60 1. 06 2.42 3.89 3.46 2.95 11.27 1. 92 4.40 4.2 5 25.80 4.99 15.80 3.22 miss = Nuclide energy was not found in the coincidence library. 10/3/21.,., 10:05:56AM Page 3 of8 Activity Activity Coinc (pCilgrams)

Uncertainty Corr 2.98E-01 1.15E-01 free 5.06E-0 1 2.35E-01 0.992 4. llE-01 2.2 3E-01 0.990 INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1. 000 5.83E+OO 1.12E+OO Cs-137 1. 000 1.78E-01 5.80E-02 /

Analysis Report for 03-0ct-16-10003

? ? L3-10219B-FRGS-003SS Nuclide Nuclide Name Id Confidence Tl-208 0.994 Bi-211 0. 963 Pb-2 12 1. 000 Bi-214 1. 000 Pb-214 1.000 Ac-228 0.571 ? = nuclid e is part of an undetermined solution X = nuclid e rejected by the interference analysis 10/3/21,. Wt mean Activity (pCilgrams) 1.13E-01 8.lSE-01 3.15E-01 2.19 E-01 2.98E-01 4.57E-01 @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10:05:56AM Page 4 of8 Wt mean Comments Activity Uncertainty 4.68E-02 3.14E-01 1.04E-01 9. llE-02 1.lSE-01 1. 64E-01 10/3/21., . 10:05:56AM Page 5 of8 Analysis Report for 03-0ct-16-10003

+ + + + + + + + + L3-10219B-FRGS-003SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/3/2016 9:47:28AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCl/grams) loCilgrams)

Ct>rr K-40 1460.8 2

10.66 5.83E+OO 3.76E-01 3.76E-01 miss Cr-51 320.08 9.9 1 -4.93E-0 2 3.73E-01 3.73E-01 free Mn-54 834.85 99.98 -l.54E-03 3.32E-02 3.32E-02 miss Co-58 810.76 99.45 1. 2 7E-02 3.82E-0 2 3.82E-02 1.000 1 674.73 0.52 O.OOE+OO 2.68E+OO 1. 024 Co-60 1173.2 3 99.85 1.24E-02 4.74E-02 5.3 1E-0 2 0.947 1332.49 99.98 5.03E-03 4.74E-02 0.947 Nb-94 702.65 99.81 7.06E-03 3.5'7E-02 4.56E-02 0.944 871.09 99.89 -9.2 1E-04 3.57E-02 0.944 Ag-108m 79.13 6.60 1.80E-01 2.88E-02 l.66E+OO miss 433.94 90.50 5.87E-03 4.04E-02 0.887 614.28 89.80 -7.46E-03 2.88E-02 0.886 722. 94 90.80 -1.03E-02 3.69E-02 0.887 Sn-113 255.13 2 .11 -3.56E-01 5.44E-02 1.58E+OO free 391.70 64.97 7.71E-04 5.44E-02 free Cs-134 475.36 1. 48 3.95E-01 3.25E-02 2.46E+OO miss 563.25 8.34 -6.2 7E-03 5.46E-01 0.896 569.33 15.37 5.88E-02 3.0lE-01 0.888 604. 72 97.62 -1.08E-03 3.2 5E-02 0.931 10/3/2\, . 10:05: 56AM Page 6 of8 Analysis Report for 03-0ct-16-10003 L3-102198-FRGS-003SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 2.90E-02 3.25E-02 6.73E-02 0.933 801.95 8.69 -1.65E-01 4.lOE-01 0.898 1038.61 0.99 1.53E+OO 4. 98E+OO 0.943 11 67. 97 1. 79 -l.41E-01 2.1 3E+OO 1. 081 1365.19 3.02 O.OOE+OO 3.39E-01 1.128 + Cs-137 661.66

85.10 1. 78E-0 1 5.2 7 E-02 5.2 7E-02 miss + Eu-152 121.78 28.67 4.22E-03 1.2 7E-01 1.SOE-01 0.936 244.70 7.61 -7.82E-02 4.lOE-01 0.935 295.94 0.45 8.07E+OO l.13E+Ol mis s 344.2 8 26.60 -9.09E-03 l.27E-01 0.957 367.79 0.86 -7. 72E-01 4.12E+OO 0.884 411.12 2.2 4 -6.03E-01 1.54E+OO 0.908 443. 96 2.83 1.87E-02 1.41E+OO 0.934 488.68 0.42 5.03E-01 8.76E+OO miss 563.99 0.49 -1.90E+OO 7.64E+OO 0.934 586.26 0.46 -2.31E+OO 8.77E+OO 0.942 678.62 0.47 -1.54E+00 8.2 9E+OO 0.887 688.6 7 0.86 -l.06E+OO 3.81E+OO 0.980 719.35 0.28 -3.95E+OO 7.2 6E+OO miss 778.90 12. 96 5.45E-02 3.llE-01 0.945 810.45 0. 32' 1. 03E+OO 9. 52E+OO 1. 050 867.37 4.26 2.63E-02 7.33E-01 0.928 919.33 0.43 -9.04E-01 5.70E+OO 0.981 964.08 14.65 7.lOE-02 2.94E-01 1.022 10 85.87 10.24 -1.84E-01 3.24E-01 1.01 8 10 89.74 1. 73 -4.42E-01 2.05E+OO 0.952 1112.07 13. 69 3. llE-02 2.93E-01 0.99 2 1212.95 1. 43 -5.06E-01 2.74E+OO 0.929 1249.94 0.19 6.51E+OO 2.89E+Ol 1.097 1299.14 1. 63 -5. 72E-01 2.48E+OO 0.944 1408.01 21.07 5.98E-03 2.52E-01 0.983 1457.64 0.50 -3.65E+OO 1.66E+Ol 1.076 1 528.10 0.28 O.OOE+OO 4.40E+OO 1.007 + Eu-154 123.07 40.40 -1.78E-02 1.0 3E-01 1. 03E-01 0. 934 247.93 6.89 1.30E-01 4.60E-01 0.928 591.76 4.95 3.62E-01 8.87E-01 0.915 692.42 1. 78 -4.64E-01 2.56E+OO 0.936 723. 3 0 20.06 9.82E-04 1. 93E-01 0. 935 756.8 0 4.52 9.87E-02 9.03E-01 0.91.') 873.18 12.08 -3.25E-02 3.00E-01 0.93 2 996.2 9 10.48 -5.0 6E-0 2 2.48E-01 0.971 1004.76 1 8.01 -l.14E-0 2 2.36E-01 0.978 1274.43 34.8 0 2.77E-02 l.55E-01 0.98 1 1596.48 1. 8 0 O.OOE+OO 6.13E-01 1.175 + Eu-155 45.30 1. 3 1 -4.40E+OO 2.36E-0 1 2.51E+Ol 0.999 60.0 1 1.22 -1. 23E+Ol l.98E+Ol 1. 000 86.55 30.70 1.84E-01 2.63E-01 free 105.31 21.10 3.56E-0 2 2.36E-01 1. 000 + Tl-208 583.19

85.00 1.13E-01 4.76E-02 4.7 6E-02 0.932 + Bi-211 351.07

1 3.02 8.15E-01 3.61E-01 3.61E-01 miss + Pb-211 404.85 3. 78 -4.57E-0 2 9.23E-01 9. 23E-01 miss 10/3/21., ., 10:05:56AM Page 7 of8 Analysis Report for 03-0ct-16-10003 L3-10219B-FRGS-003SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCi/grams) (pCilgrams)

Corr Pb-211 427.09 1. 76 -2.95E-01 9.23E-01 1.73E+OO miss 832.0 1 3.5 2 2.73E-01 1.13E+OO miss + Bi-2 1 2 39.86 1. 06 -3.56E+OO 1.02E+OO 2.62E+Ol 0.998 727. 33 6.67 7.48E-01 l.02E+OO 0.982 785. 37 1.10 l.67E-01 4.2 1E+OO 0.944 1620.50 1. 47 l.63E-01 2.40E+OO 1.006 + Pb-212 115 .18 0.60 -3.17E+OO 1.17E-01 6.19E+OO miss 2 38.63 ....... 43.60 3.15E-01 1.17E-01 free 300.09 3.3 0 3.40E-01 1.17E+OO free + Pb212-XR 74.82 10.2 8 9.73E-01 8.2 4E-01 1.44E+OO miss 77 .11 17.10 6.71E-01 8.24E-01 miss 87.35 3.97 3.98E-01 l.97E+OO miss 89.78 1. 46 5. llE-01 4.51E+OO miss + Bi-2 1 4 609.32 :i~ 45.49 2.19E-01 9.58E-02 9.58E-0 2 0.948 768.36 4.89 2.62E-01 1.04E+OO 0.94 2 806.18 1. 2 6 3.39E-01 3.59E+OO 0.923 934.06 3.11 -4.67E-02 l.35E+OO 0.944 1120.29 14.92 3.0lE-01 5.76E-01 0.944 1 155.21 1. 63 1. 72E+00 3.69E+00 0.94 3 1238.12 5.83 9.07E-0 2 l.OlE+OO 0.944 1280.98 1. 43 2.39E-01 3.92E+OO 0.944 1377.67 3.99 6.lOE-01 1.56E+OO 1. 030 1 3 85.31 0.79 l.71E+OO 6.15E+OO 0.945 1401.52 1. 33 O.OOE+OO 9.30E-01 0.945 1407.99 2.39 5.48E-02 2.30E+OO 0.945 1509.21 2 .13 4.52E-01 2.lOE+OO 0.950 1661.27 1. 05 O.OOE+OO 1. 27E+OO 1. 001 1729.59 2.88 7.89E-01 2.07E+OO 1.119 1764.49 15.30 4.18E-01 6.56E-0 1 1. 001 1847.43 2.03 -4.32E-01 2.2 9E+OO 1.063 > 2 118.51 1.1 6 O.OOE+OO O.OOE+OO 1.041 + Pb-2 14 241.99 7.2 5 5.18E-01 1.32E-01 6.67E-01 1. 000 295.22 18.42 3.83E-01 3.lOE-01 1. 000 351.93

35.60 2.98E-Ol l.32E-01 free 785.96 1. 06 -6.27E-01 3.88E+OO 1. 000 + Pb214-XR 74.8 2 5.80 1. 72E+OO 1.45E+OO 2.56E+OO miss 77 .11 9.70 1.1 8E+OO 1.45E+OO miss 87.35 2.24 7.06E-01 3.49E+OO mi ss 89.78 0.82 9.lOE-01 8.03E+OO miss + Ra-226 186.21 3.64 1. 37E-01 1.02E+OO l.02E+OO free + Ac-228 129.07 2.42 -3.34E-02 2.60E-01 l.58E+OO 0.944 209.25 3.89 2.14E-01 8.70E-01 0.978 270.24 3.46 2.74E-01 1. 07E+OO 0.955 328.00 2. 95 3.19E-01 1.21E+OO 0.955 338.32

11. 27 5.06E-01 2.64E-01 0.992 409.46 1. 92 2.49E-01 2.02E+OO 0.937 463.00 4.40 l.49E-02 8.63E-01 0.933 794.95 4.25 l.99E-01 1.22E+OO 0.942 911.20 25.80 2.65E-01 3.40E-01 0.990 964.77 4.99 3.43E-01 9.67E-01 0.981 968.97

15.80 4. llE-01 2.60E-01 0.990 Analysis Report for 03-0ct-16-10003

+ + + + + > L3-10219B-FRGS-003SS Nuclide Energy Yield(%) Activity Name (keV) (pCilgrams)

Ac-22 8 1588.20 3.22 2.03E-01 Pa-23 1 27.36 10.30 3.34E-01 283.69 1. 70 -1.63E-01 300.07 2.47 4.54E-01 302.65 2.20 -9.35E-01 330.06 1. 40 -3.76E-0 2 T h-234 92.38 2.13 1. 43E+00 92.80 2.10 6.79E-01 112. 81 0.21 -3.64E+OO U-235 143.76 10. 96 1.60E-01 1 63.33 5.08 8.15E-02 185.71 57.2 0 3.47E-02 202 .11 1. 08 1.40E-02 205.31 5.01 -l.52E-01 Arn-241 59.54 35.90 -4.16E-02

= Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/3/2L NuclideMDA (pCl/grams) 2.?0E-01 1.15E+OO 3.36E+OO 6.77E-02 7.48E-01 ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 10:05:56AM Page 8 of8 LineMDA Coinc (pCi/grams)

Corr 1.59E+OO 1. 002 2. 96E+OO 0.998 l.62E+OO 1. 000 l.56E+OO 1. 000 l.15E+OO 1. 000 2.08E+OO 1. 000 3.47E+OO free 3.36E+OO free 2.42E+Ol free 3.55E-01 free 6.07E-01 free 6.77E-02 free 2.75E+OO miss 5.20E-01 free 7.48E-Ol free 60 55 50 45 40 "' ;:j I f?. 35 VI ...... C: :::J 8 30 I ,, 1000 ,_ "" oO 7 ,:: -1~\W m i 2000 3000 0000015998.CNF 4000 5000 channel Live Time : 600.000 sec Real Time : 601.130 sec Start: 1: -0.l(kev) stop : 8192: 2047 .O(kev) Acq. start :Mon Oct 03 09:3i:25 2016 6000 7000 8000 10/3/._ ., 11 :19:24AM ~~~p ex-Gam m a Analysis Report for 03-0ct-16-10004 L 3-10219B-FRGS-004SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real lime Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration U sed Done On Efficiency Calibration Description Sample Number : 03-0ct-16-10004

L3-10219B-FRGS-004SS

1 L 130G Soil Sample 5.430E+02 grams : Default : 9/27/2016 8:25:00AM

10/3/2016 10:44:10AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 1000.0 seconds : 1001.6 seconds : 0.16 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM : 1/27/2016

1/5/2015 : 15999 PEAK WITH NID REPORT Peak Analysis Performed on 10/3/2016 11 :00:55AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM ~iv\-;.~~-D \<0\~ll\... Page I of7 10/3/2l. 11:19:24AM Page 2 of7 Analysis Report for 03-0ct-16-10004 L3-10219B-FRGS-004SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV} start end Centroid Area Uncertainty Counts Nuclide 1 238.49 948 -961 954.45 6.14E+Ol 27.86 9.53E+Ol Pb-212 2 2~4.93 1174 -1185 1180. 0 3 4.15E+Ol 20.53 5.lOE+Ol Pb-214 Eu-152 3 351.67 1401 -1414 1406.85 5.57E+Ol 2 0.05 3.66E+Ol Pb-214 Bi-211 4 510. 72 2038 -2 048 2 042.73 2.03E+Ol 14.06 2.73E+Ol . . ,t-.v.Jf-5'"/f 5 582.98 2327 -2337 2 331.69 1.81E+Ol 12.2 0 1. 78E+Ol Tl-208 6 608.98 2429 -2442 2 435.67 4.74E+Ol 15.60 1.12E+Ol Bi-214 7 661.39 2637 -2653 2 645.26 1.18E+02 23.01 1.15E+Ol Cs-137 8 1460.44 5835 -5850 5842.71 6.67E+Ol 16.93 4.57E+OO K-40 :r'P,./ M = First peak in a multiplet region /(/'J-16 m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Caine Name Confidence (keV} (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

10.66 4.52E+OO l.21E+OO miss Cs-137 0.99 661.66

85.1 0 5.86E-0.1

1. 34E-01 miss Tl-208 0.99 583.19

85.00 9.09E-02 6.22E-02 0.932 Pb-212 0.99 115.18 0.60 238.63

43.60 2.99E-01 1.44E-01 free 300.09 3.30 Bi-214 0.99 609.32

45.49 4.48E-01 l.57E-01 0.948 768.36 4.89 806.18 1. 2 6 934.06 3.1 1 1120.2 9 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.79 1 401.52 1. 33 1407.99 2.39 Analysis Report for 03-0ct-16-10004 L3-10219B-FRGS-004SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1509.21 1661. 27 1729.59 1764.49 1847.43 2 11 8.51 Pb-214 0.99 2 41.9S 295.22 351.93 785. 96 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) ~.13 1. 05 2.88 15.30 2.03 1.16 7.2 5 1 8.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 10/3/21. 11:19:24AM Page 3 of7 Activity Activity Coinc (pCi/grams)

Uncertainty Corr 5.47E-0 1 2.85E-01 1. 000 4.25E-01 1.68E-01 free INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Cs-137 Tl-208 X Bi-211 Pb-212 Bi-214 Pb-214 Nuclide Id Confidence

0. 991 0. 996 0.997 0.979 0.999 0.997 0. 996 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 4.52E+OO 5.86E-01' 9.09E-02 2.99E-01 4.48E-01 4.57E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Comments Activity Uncertainty 1.21E+OO 1. 34E-01 6.22E-02 1.44E-01 1.57E-01 1.44E-01 10/3/21.. 11: 19:24AM Page 4 of7 Analysis Report for 03-0ct-16-10004

+ + + + + + + + + L3-10219B-FRGS-004SS Peak Locate Performed on Peak Locate From Channel Peak Loca te To Channel Peak No. Energy (keV) 4 510. 72 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/3/2016 11:00:55AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 2.03353E-02 Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Coinc Name (keV) (pCl!grams) (pCilgrams) (pCi!grams)

Corr K-40 1460.82

1 0.66 4.52E+OO 6.78E-01 6.78E-01 miss Cr-5 1 320.08 9.9 1 -2.41E-01 5.0 lE-01 5.0lE-01 free Mn-54 834.85 99.98 2.08E-03 6.0 0E-0 2 6.00E-02 miss Co-58 810.76 99.45 3.87E-03 6.2 0E-02 6. 2 0E-0 2 1. 000 1674.73 0.52 O.OOE+OO 4.35E+OO 1. 024 Co-60 1173.23 99.85 -l.13E-02 5.25E-02 6.lOE-02 0.947 1332.49 99.98 -9.18E-03 5.25E-02 0.947 Nb-94 702.65 99.81 l.09E-02 4.99E-02 6.57E-02 0.944 871.09 99.89 -4.03E-03 4.99E-02 0.944 Ag-1 0 8m 79 .13 6.60 5.86E-01 7.39E-02 2. 21E+OO miss 433.94 90.50 6.02E-03 7.39E-02 0.88: 614.28 89.80 4.08E-02 9.14E-02 0.886 722. 94 90.80 -l.32E-03 8.35E-02 0.887 Sn-1 1 3 255 .13 2 .11 -7.74E-02 8.17E-02 2.51E+OO free 3 91. 70 64.97 -8.63E-03 8.17E-02 free Cs-134 475.36 1. 48 1. 45E+OO 7.65E-02 5.49E+OO miss 563.25 8.34 l.73E-01 8.86E-01 0.896 569.33 15.37 6.25E-02 4.2 1E-01 0.888 10/3/21. 11:19:24AM Page 5 of7 Analysis Report for 03-0ct-16-10004 L3-10219B-FRGS-004SS Nucllde Energy Yield(%) Activity Nuclid e MDA LineMDA Coinc Name (keV) (pCilgrams) (pCl/grams) (pCi/grams)

Corr C s-13 4 604. 72 9'7.62 2.95E-0 2 7.65E-02 7. 65E-02 0.931 795.86 85.46 4.97E-0 2 1.00E-01 0.933 801.95 8.69 -2.78E-01 6.66E-01 0.898 1038.61 0.99 -9.24E-01 5.72E+OO 0.943 1167.97 1. 79 -5.04E-O l 3.85E+OO 1.081 1365.19 3.0 2 O.OOE+OO 5.49E-01 1.1 2 8 + Cs-13 7 661.66

85.10 5.86E-01 7.48E-0 2 7.48E-02 mis s + Eu-15 2 121. 78 2 8.67 4.0lE-0 2 1.98E-01 2.04E-01 0.936 244.70 7.61 -6.22E-0 2 6.47E-01 0.935 2 95. 94 0.45 1.36E-01 1.90E+Ol miss 344.2 8 2 6.60 -3.90E-02 1.98E-01 0.957 367.79 0.86 4.76E-01 6.68E+OO 0.884 411.12 2.24 -1.03E+OO 2.61E+OO 0.908 443.96 2.83 O.OOE+OO 2.02E+OO 0.93 4 488.68 0.4 2 3.63E+OO 1.29E+Ol mis s 563.99 0.49 2.1 4E-01 1.44E+Ol 0.934 586.2 6 0.46 4.74E+00 1.56E+Ol 0.94 2 678. 62 0.47 1.62E+OO 1.45E+Ol 0.887 688.67 0.86 -2.15E+OO 6.18E+OO 0.980 719.35 0.2 8 -2.13E+OO 2.40E+Ol miss 778.90 12. 96 6.54E-02 5.04E-01 0.945 810.45 0.32 2.33E+OO 1.72E+Ol 1.050 867.37 4.26 2.77E-01 1.54E+OO 0.928 919.33 0.43 -3.35E+OO 9.25E+OO 0.981 964. 08 14.65 -5.30E-0 2 4.37E-01 1.022 1 085.87 1 0.24 -5.0lE-0 2 7.41E-01 1. 018 1089.74 1. 73 -3.84E-01 4.31E+OO 0.952 1112. 07 13.69 -5.04E-02 3.24E-01 0.992 1212.95 1. 43 -3.42E-02 5.75E+OO 0.929 1249.94 0.19 7.80E+OO 3.75E+Ol 1. 097 1299.14 1. 63 -3.71E-01 3.18E+OO 0.944 1408.01 21. 07 8.74E-02 3.66E-01 0.983 1457.64 0.50 -3.07E+Ol 2.12E+Ol 1.076 1528.1 0 0.28 3.65E+OO 2.84E+Ol 1. 007 + Eu-154 123.07 40.40 -7.78E-02 1.33E-01 1.33E-01 0.934 247.93 6.89 -1.55E-01 7.84E-01 0.92 8 591.76 4. 95 1.38E-01 1.22E+OO 0.915 692.42 1. 78 8.63E-01 3.43E+OO 0.936 723. 30 20.06 -6.77E-02 3.37E-01 0.935 756.80 4.52 -3.91E-01 1.04E+OO 0.91 5 873.18 12.08 -2.51E-03 4.86E-01 0.93 2 996.2 9 10.48 -7.30E-0 2 5.08E-01 0.971 1004.76 18.0 1 -4.77E-02

2. 96 E-01 0.978 1274.43 3 4.80 -5.2 1E-02 l.41E-01 0.981 1596.48 1. 80 -2.91E-01 3.95E+OO 1.175 + Eu-155 45.30 1. 3 1 3.77E+OO 3.62E-01 4.08E+Ol 0.999 60.01 1. 22 -2.50E+Ol 3.31E+Ol 1.000 86.55 30.70 8.50E-02 4.00E-01 free 105.31 21.10 7.47E-02 3.62E-01 1. 000 + Tl-208 583.19

85.00 9.09E-0 2 8.34E-02 8.34E-02 0.932 + Bi-2 11 351.07

13. 02 1.16E+OO 5.16E-01 5.16E-01 miss 10/3/2.. , 11 :19:24AM Pa ge 6 of7 Analysis Report for 03-0ct-16-1 0004 L3-102198-FRGS-004SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCi/grams) (pCilgrams)

Corr + Pb-211 404.85 3.78 -4.23E-01

1. 38E+OO l.38E+OO miss 427.09 1. 76 -l.60E+OO

2. 66E+OO mis s 832.01 3.52 4.42E-Ol l.83E+OO mis s + Bi-2 12 39.86 1. 06 -l.12E+Ol

1. 03E+OO 4.13E+Ol 0.998 727. 33 6.67 3.69E-01 l.03E+OO 0.982 785.37 1.10 -l.24E+OO 6.41E+OO 0.944 1 620.50 1. 47 l.32E-01 3.90E+OO 1. 006 + Pb-21 2 115 .18 0.60 2.56E+OO l.98 E-01 l.12E+Ol mis s 2 38.63

43.60 2.99E-0 1 l.98E-01 fre e 300.09 3.30 6.52E-0 2 l.50E+OO free + Pb212-XR 74.8 2 10.2 8 7.64E-0 1 l.07E+OO 2.25E+OO miss 77.1 1 17.10 2.64E-01 l.07E+OO miss 87.35 3.97 l.53E+OO 3.13E+OO miss 89.78 1. 46 3.33E+OO 7.32E+OO miss + B i-21 4 609.32

45.49 4.48E-01 l.3 7 E-0 1 l.37E-01 0.948 768.36 4.89 -l.35E-01 l.52E+OO 0.942 806.1 8 1. 26 l.44E+OO 5.82E+OO 0.923 934.0 6 3.11 8.17E-01 3.03E+OO 0.944 1 120.2 9 14.9 2 4.71E-01 8.58E-Ol 0.944 11 55.2 1 1. 63 1.65E+OO 5.62E+OO 0.943 1238.12 5.83 1. 08E+OO 2.2 7E+OO 0.944 128 0.98 1. 43 -2.77E-01 4.50E+OO 0.944 1377. 67 3.99 l.68E-01 l.24E+OO 1. 030 1385. 31 0.79 -7.95E-01 6.82E+OO 0.945 1401.52 1. 33 1.12E+OO 5.18E+OO 0.945 1 407.99 2.39 7.99E-01 3.35E+OO 0.945 1 509.2 1 2.13 1.42E+OO 4.80E+OO 0.950 1 661. 27 1. 05 O.OOE+OO 2.06E+OO 1. 00 1 1 729.59 2.88 4.48E-01 2.75E+OO 1.119 1 764.49 15.30 2.41E-0 1 7.70E-01 1. 001 1 847.43 2.03 4.00E-01 3.72E+OO 1.063 > 2118.51 1.16 O.OOE+OO 0.00E+OO 1.041 + Pb-214 2 41.99 7.25 3.07E-01 1.89E-0 1 8.82E-01 1. 000 2 95.22

18.42 5.47E-Ol 3.83E-01 1. 000 351.93

35.60 4.2 5E-01 l.89E-01 free 785.96 1. 0 6 -l.41E+OO 6.30E+OO 1. 000 + Pb214-XR 74.82 5.80 l.35E+OO l.89E+OO 3.98E+OO miss 77 .11 9.70 4.65E-01 l.89E+OO mis s 87.35 2.24 2. 72E+OO 5.56E+OO miss 89.78 0.82 5.93E+OO 1.30E+Ol miss + Ra-22 6 186.2 1 3.64 5.99E-01 1. 71E+OO 1. 71E+OO free + Ac-22 8 129.07 2.42 8.36E-01 3.86E-0 1 2.74E+OO 0.944 '.209 .2 5 3.89 6.00E-0 1 1.48E+OO 0.978 270.2 4 3.46 5.58E-01 1.90E+OO 0.955 328.00 2.95 5.98E-01 2.22E+OO 0.955 338.32 11. 27 1.54E-01 5.7 0E-01 0.99 2 409.46 1. 92 1.64E+OO 3.87E+OO 0.937 463.00 4.40 -3.34E-01 l.40E+OO 0.933 79 4.95 4.25 1. 89E-01 l.68E+OO 0.942 911.20 25.8 0 l.69E-01 3.86E-01 0.990 964. 77 4.99 1. lSE-01 1.46E+OO 0.981 10/3/2.. _ 11:19:24AM Page 7 of7 Analysis Report for 03-0ct-16-10004 L3-10219B-FRGS-004SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCilgrams)

Corr Ac-228 968.97 15.80 2.lOE-01 3.86E-01 5.82E-01 0.990 1588.20 3.22 8.52E-01 2.87E+OO 1. 002 + Pa-231 2 7.36 10.30 -8.31E-0 2 2.00E+OO 4.2 5E+OO 0.998 2 83.69 1. 70 -5.58E-01 2.81E+OO 1. 000 300.07 2.47 8.70E-02 2.00E+OO 1. 000 302.65 2.2 0 -5.61E-02 2.33E+OO 1.000 330.06 1. 40 -5.lSE-01 3.97E+OO 1. 000 + Th-234 92. 38 2 .13 7.53E-01 5.42E+OO 5.42E+OO free 92.80 2.10 2.52E+00 5.67E+OO free 112. 81 0.2 1 -1.2 7E+OO 2.88E+Ol free + U-235 143.76 10. 96 6.73E-02 l.17E-01 5.00E-01 free 163.33 5.08 4.3 7E-01 l.17E+OO free 185. 71 57.20 8.23E-02 l.17E-01 free 20~ .11 1. 08 1. 4 7E+OO 5.0SE+OO miss 205.31 5.01 6.03E-Ol l.13E+OO free + Am-24 1 59.54 35.90 -3.79E-01 l.31E+OO l.3 1E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Vl +-' C: :::s 60 55 50 40 35 8 30 25 20 15 £1 I 1000 2000 3000 0000015999.CNF 4000 channel 5000 Live Time 1000.000 sec Real Time 1001.620 sec Start: 1 -0. l(kev) stop : 8192 2047 .O(kev) Acq. Start Mon Oct 03 10: 44: 10 2016 = ! 6000 7000 8000 10/3/:,. J 10:57:23AM Analysis Report for 03-0ct-16-10005 L3-102198-FRGS-OOSSS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 03-0ct-16-10005

L3-10219B-FRGS-005SS

1 L 130G Soil Sample 1.117E+03 grams : Default : 9/27/2016 10:00:00AM

10/3/2016 10:46:42AM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 600.0 seconds : 600.4 seconds : 0.07% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

6/28/2012

16000 PEAK WITH NID REPORT Peak Analysis Performed on 10/3/2016 10:56:48AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance VkCA \[ c:-\,~~ \.-\.31,~

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM

\\) Page I of7 10/3/21..

10:57:23AM Page 2 of7 Analysis Report for 03-0ct-16-10005 L3-10219B-FRGS-005SS Peak Energy ROI No. (keV) start 1 2 38.77 948 -2 2 95.30 1177 -3 351.94 1400 -4 661.64 2637 -5 1460.79 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 961 1186 1413 2653 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 955.38 6. 91E+Ol 25.73 6.98E+Ol 1181.26 l.05E+Ol 13.95 3.30E+Ol 1407.56 4.3~E+Ol 18.42 3.36E+Ol 2 645.36 5.93E+Ol 17.09 l .13E+Ol 5842.51 l.19E+02 21.82 O.OOE+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 1. 00 1460.82 Cs-137 1. 00 661.66 Bi-211 0.95 351.07 Pb-212 0.99 115 .18 238.63 300.09 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 10.66 85.10 13. 02 0.60 43.60 3.30 miss = Nuclide energy was not found in the coincidence library. Activity (pCilgrams) 5.89E+OO 2.15E-01 6.58E-0 1 2.42E-01 Activity Uncertainty l.19E+OO 6. 71E-02 3.00E-01 9.84E-02 Tentative Nuclide Pb-212 Pb-214 Eu-152 Pb-214 Bi-211 Cs-137 K-40 Coinc Corr miss miss miss miss 10/3/21_ 10:57:23AM Analysis Report for 03-0ct-16-10005 L3-10219B-FRGS-005SS INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Cs-137 Bi-211 Pb-21 2 Nuclide Id Confidence

1. 000 1. 000 0.954 0.999 X Pb-214 1. 000 ? X = = nuclid e is part of an undetermined solution nuclid e rejected by the interference analysis Wt mean Activity (pCilgrams) 5.89E+OO 2. lSE-01'~ 6.58E-01 2.42E-01 @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty l.19E+OO 6.71E-02 3.00E-01 9.84E-02 Page3 of7 Comments 10/3/2._ Analysis Report for 03-0ct-16-10005 L3-102198-FRGS-005SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 2 295.30 M = First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/3/2016 10:56:48AM

120 : 8192 Peak Size (CPS) 1.75309E-02 10:57:23AM Peak Type Tol. NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yie/d(°/o)

Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCi!grams) (pCi!grams)

+ K-40 1460.82

10.66 5.89E+OO 1.34E-01 1.34E-01 + Cr-51 32 0.08 9.91 -1.25E-01 2.86E-0 1 2.86E-01 + Mn-54 834.85 99.98 -3.85E-03 3.93E-02 3.93E-02 + Co-58 810.76 99.45 4.87E-03 4.53E-02 4.53E-02 1674.73 0.52 O.OOE+OO 3.25E+OO + Co-6 0 1173.23 99.85 -9.73E-03 3.34E-02 3.34E-02 1332.49 99.98 9.86E-03 4.58E-02 + Nb-94 702.65 99.81 8.04E-04 3.45E-02 3.86E-02 871. 09 99.89 -1.21E-02 3.45E-02 + Ag-108m 79.1 3 6.60 1.97E-02 3.88E-02 8.91E-01 433.94 90.50 8.76E-03 4.24E-02 614.28 89.80 5.22E-03 4.60E-02 722. 94 90.80 -4.80E-03 3.88E-02 + Sn-113 255.13 2 .11 -2.79E-01 5.43E-02 1. 31E+00 391.70 64.97 1.20E-0 3 5.43E-02 + Cs-134 475.36 1. 48 -4.17E-03 4.93E-0 2 2.65E+OO Page 4 of7 Tolerance Nuclide Eu-152 Pb-214 Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss 10/3/2 ... 10:57:23AM Page 5 of7 Analysis Report for 03-0ct-16-10005 L3-10219B-FRGS-005SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCi!grams)

Corr Cs-134 563.25 8.34 4.66E-02 4.93E-02 4. 36E-01 mis s 569.33 15.37 3.64E-03 1.69E-01 mis s 604. 72 97.6 2 1.67E-02 5.20E-02 miss 7 95.86 85.46 7.53E-03 4.93E-02 miss 801.95 8.69 -2. 71E-02 3.77E-01 miss 1038.61 0.99 5.66E-01 5.56E+OO miss 1167.97 1. 79 -5.25E-01 2.35E+OO miss 1365.19 3.0 2 5.0lE-01 1.80E+OO miss + Cs-137 661. 66

85.10 2.15E-01 5.39E-02 5.39E-02 miss + Eu-15 2 1 2 1.78 2 8.67 8.50E-04 9.23E-02 9.23E-02 miss 24-1.70 7.61 -1. 2 6E-02 3.98E-01 miss 2 95.94 0.45 3.94E-01 1.02E+Ol miss 3 44.2 8 26.60 4.65E-02 l.38E-01 miss 3 67.79 0.86 -3.33E-01 2.85E+OO miss 411.12 2.24 3.73E-01 1.40E+OO miss 443. 96 2.83 1.32E-01 1.24E+OO miss 488.68 0.4 2 -1.59E+OO 6.41E+OO miss 563.99 0.49 1. 99E+OO 7.94E+OO miss 586.2 6 0.46 -3.09E+OO 8.71E+OO miss 678.62 0.47 2.81E+OO 8.71E+OO miss 688.67 0.86 -1.84E-01 3.43E+OO miss 719.35 0.28 9.09E-01 1. 26E+Ol miss 778.90 12. 96 -1.62E-02 2.86E-01 miss 810.45 0.32 -7.34E-01 l.19E+Ol miss 867.37 4.26 3.76E-01 l.38E+OO miss 919.33 0.43 -l.95E+OO 9.69E+OO miss 964. 08 14.65 3.28E-02 3.2 6E-01 miss 1085.87 10.2 4 -1.17E-01 5.0SE-01 miss 1089.74 1. 73 4.35E-01 3.27E+OO miss 1112.07 13.69 -7.30E-02 3.44E-01 miss 1212.95 1. 43 -1.70E-01 4.58E+00 miss 1 2 49.94 0.19 2.50E+OO 2.32E+Ol miss 1 2 99.14 1. 63 1.31E+OO 3.91E+OO miss 1408.01 2 1. 07 2.44E-02 1.79E-01 miss 145,.64 0.50 O.OOE+OO l.13E+Ol miss 1528.10 0.28 O.OOE+OO 5.24E+OO miss + Eu-154 123.07 40.40 3.69E-02 7.70E-02 7.70E-0 2 miss 2 47.93 6.89 -3.02E-01 3.62E-01 miss 591.76 4.95 -8.09E-02 6.22E-01 miss 692.42 1. 78 -2.69E-01 2.35E+OO miss 723.30 20.06 -4.63E-02 1.76E-01 miss 756.80 4 .. 52 -8.72E-02 8.04E-01 miss 873.18 1 2.08 6.67E-02 3.70E-01 miss 996.29 10.48 1.94E-01 5.09E-01 miss 1 004.76 18.01 2.65E-02 2.45E-01 miss 1 2 74.43 34.80 7.20E-03 1.48E-01 miss 1 596.48 1. 80 -3.93E-01 2.32E+OO miss + Eu-155 45.30 1. 31 -1. 28E+OO 1.68E-01 7.99E+OO miss 60.01 1. 2 2 -2.83E+OO 1.06E+Ol miss 86.55 30.70 7.79E-0 2 1.91E-01 miss 105.31 21.10 -3. 77E-02 l.68E-01 miss 10/3/2. 10:57:23AM Page 6 of7 Analysis Report for 03-0ct-16-10005 L3-102198-FRGS-005SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)

Corr + Tl-208 583.19 85.00 8.39E-02 9.52E-0 2 9.52E-02 miss + Bi-2 1 1 351.07

13.0 2 6.58E-01 3.64E-01 3.64E-01 miss + Pb-211 404.85 3. 78 4.16E-01 9.2 0E-0 1 9.2 0E-01 miss 427.09 1. 76 5.47E-01 l.94E+OO miss 832.01 3.52 4.54E-0 2 l.lOE+OO miss + Bi-212 39.86 1. 06 -l.2 5E+OO 7.39E-01 9.85E+OO miss 727. 33 6.67 1. 32E-0 1 7.39E-01 miss 785.37 1.10 -3.66E-01 3.38E+OO miss 1620.50 1. 47 7.77E-01 3.61E+OO miss + Pb-212 115 .18 0.60 1. 51E+OO l.2 3E-0 1 5.92E+OO miss 238.63

43.60 2.42E-01 l.23E-01 miss 300.09 3.30 1.08E-0 2 7.08E-01 miss + Pb212-XR 74.8 2 10.2 8 3.76E-01 5.40E-01 8.45E-01 miss 77 .11 17.10 3. llE-01 5.40E-01 miss 87.3 5 3.97 4.39E-01 l.3 8E+OO miss 89. 78 1. 46 O.OOE+OO 3.06E+OO m i ss + Bi-214 609.32 45.49 2.06E-01 2.08E-0 1 2.08E-01 miss 768.36 4.89 1. 81E-01 1.05E+OO miss 806.18 1. 26 2.17E-01 3.00E+OO miss 934.06 3.11 -8.87E-0 2 l.SOE+OO miss 1120.29 14.92 2.14E-01 5.33E-01 miss 11 55.21 1. 63 6.50E-01 3.59E+00 miss 1 2 38.12 5.83 4.59E-02 l.27E+OO miss 1 2 80.98 1. 43 l.37E+OO 4.38E+OO miss 1377.67 3.99 3.79E-01 l.36E+OO miss 1385.31 0.79 6.16E-01 7.67E+OO miss 1401.52 1. 33 O.OOE+OO l.04E+OO miss 1407.99 2.39 2.14E-01 l.58E+OO miss 1 509.2 1 2 .13 O.OOE+OO 6.87E-Ol miss 1661.27 1. 0 5 1. llE+OO 5.17E+OO miss 1 729.59 2.88 4.1 8E-01 l.94E+OO miss 1 764.49 15.30 3.59E-01 6.65E-01 miss 1 847.43 2.03 7.75E-02 2.2 8E+OO miss > 2118.51 1.16 O.OOE+OO O.OOE+OO miss + Pb-214 241.99 7.25 l.12E-01 l.33E-01 5.22E-01 miss 2 95.22

18.42 1.0lE-01 2.20E-01 miss 351. 93

35.60 2.41E-01 1. 33E-01 miss 785. 96 1. 06 -l.63E-01 3.51E+OO miss + Pb2 1 4-XR 74.82 5.80 6.67E-01 9.52E-01 1.50E+OO miss 77 .11 9.70 5.47E-Ol 9.52E-01 miss 87.35 2.24 7.79E-01 2.44E+OO mi ss 89.78 0.82 O.OOE+OO 5.45E+OO miss + Ra-226 186.2 1 3.64 5.97E-01 1. lOE+OO 1.lOE+OO miss + Ac-228 129.07 2.42 1. 32E-01 3.49E-01 l.33E+OO miss 209.25 3.89 l.99E-01 9.16E-01 miss 270.24 3.46 4.02E-01 1. 02E+OO miss 328.00 2.95 -l.48E-01 l.07E+OO mi ss 333.32 1 1.27 3.35E-01 4.llE-0 1 miss 409.46 1. 92 -1.57E-01 l.51E+OO miss 463.0 0 4.40 5.13E-01 1.13E+OO miss 10/3/2, 10:57:23AM Page 7 of7 Analysis Report for 03-0ct-16-10005 L3-10219B-FRGS-005SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCi/grams) (pCi!grams)

Corr Ac-22 8 794.95 4.25 4.03E-01 3.49E-01 l.16E+OO miss 911.2 0 2 5.80 2.67E-01 3.49E-01 miss 964. 77 4.99 2.52E-01 1.05E+OO miss 968.97 15.80 2.31E-01 4.58E-01 miss 1 588.2 0 3.22 1. 7 5E-01 1. 29E+OO m i ss + Pa-2 31 27.36 10.30 O.OOE+OO 1.65E-0 1 1.65E-01 miss 283.69 1. 70 6.05E-01 2.09E+OO miss 300.07 2.47 1.44E-02 9.45E-01 miss 302.65 2.20 -4.52E-01 1. 36E+OO miss 330.0 6 1. 40 6.07E-01 2.46E+OO miss + Th-234 92.38 2.13 1.lOE+OO 2.93E+O O 2.93E+OO miss 92.80 2.10 1.73E+OO 3.04E+OO miss 112.81 0.2 1 8.26E+OO l.87E+O l miss + U-235 143.76 10.96 7.87E-02 6.59E-02 2.93E-01 miss 163.33 5.08 -1.lOE-01 4.68E-01 mis s 1 85.71 57.20 3.38E-02 6.59E-0 2 miss 2 02 .11 1. 08 1.31E+OO 3.05E+OO miss 2 05.3 1 5.0 1 8.49E-02 6.00E-01 miss + Am-241 59.54 35.90 -5.12E-03 3.81E-01 3.81E-01 miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) -I-' C: :::::ll 60 55 50 45 40 35 8 30 25 1000 2000 3000 0000016000 .CNF 4000 channel 5000 Live Time 600.000 sec Real Time 600.430 sec start: 1 -0.2(kev) stop : 8192 2047 .4(kev) Acq. Start Mon Oct 03 10:46:42 2016 6000 7000 8000 10/31~ d 12:12:20PM Analysis Report for 03-0ct-16-10006 L3-10219B-FRGS-006SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live lime Real lime Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 03-0ct-16-10006

L3-10219B-FRGS-006SS

1 L 130G Soil Sample 1.305E+03 grams : Default : 9/27/2016 10:25:00AM

10/3/2016 12:01:41PM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 600.0 seconds : 600.4 seconds : 0.07% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM : 1/27/2016

6/28/2012

16001 PEAK WITH NID REPORT Peak Analysis Performed on : 10/3/2016 12:11:46PM Peak Analysis From Channel Peak Analysis To Channel : 120 : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM

'l)A-.'A.

J '-'\--~ ;:k-_Q c:::s::;,0, IC> r { \ L. Page I of8 10/3/21..

_ 12:12:20PM Page 2 of8 Analysis Report for 03-0ct-16-10006 L3-10219B-FRGS-006SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide 1 186.11 739 -749 745.03 2.0lE+Ol 19.84 6.58E+Ol Ra-226 jl-235 M 2 238.69 948 -973 955.09 7.70E+Ol 19.59 6.29E+Ol Pb-212 m 3 24 2.08 948 -973 968. 64 2.38E+Ol 12.71 4.58E+O l Pb-214 4 295.17 1175 -1188 1180.74 4.65E+Ol 17. 03 l.90E+Ol Pb-214 Eu-152 5 351.93 1402 -1414 1407.50 6.64E+Ol 19.53 2.52E+Ol Pb-214 Bi-211 6 510.71 2038 -2047 2 042.07 8.84E+00 11. 09 2.03E+Ol . . /rtY. lf--5 I I 7 583.40 2326 -2339 2332.59 3.77E+Ol 12. '7 5 2.52E+OO Tl-208 8 609.09 2430 -2441 2435.31 3.94E+Ol 15.36 1. 72E+Ol Bi-214 9 661.65 2 639 -2651 2 645.41 4.66E+Ol 14.97 8.88E+OO Cs-137 10 911.13 3639 -3648 3643.02 1. 93E+Ol 10. 92 l.13E+Ol Ac-228 11 1460.81 5833 -5852 5842.55 1. 49E+02 24.41 O.OOE+OO K'-40 pw M = First peak in a multiplet region 1v1,J,l(,, m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCi!grams)

Uncertainty Corr K-40 1. 00 1460.82

10.66 6.31E+00 l. l 7E+OO miss Cs-137 1. 00 661.66

85.10 l.44E-01 4. 96E-02 miss Tl-208 0.99 583.19

85.00 l.07E-01 3.85E-02 miss Pb-212 1. 00 115 .18 0.60 238.63

43.60 2.3 1E-01 6.97E-02 miss 300.09 3.30 Bi-214 0.99 609.32

45.49 2.16E-01 8.81E-02 miss 768.36 4.89 806.18 1. 26 934.06 3 .11 1 120.29 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 Analysis Report for 03-0ct-16-10006 L3-10219B-FRGS-006SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1377.67 1385. 31 1401.52 1407.99 1509.21 1661.27 1729.59 1764.49 1847.43 2 118. 51 Pb-21 4 1. 00 241.99 ~,i. 295.22

351.93

785.96 Ra-226 0.99 186.2 1

Ac-228 1. 00 129.07 209.25 270.24 328.00 338.3 2 409.46 463.00 794.95 911.20

964. 77 968. 97 1588.20 U-235 0.99 143.76 163.33 185.71

202 .11 205.31 * == Energy line found in the spectrum.

-== Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

== 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 3.99 0.79 1. 33 2.39 2 .13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 3.64 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.2 5 25.80 4.99 15.80 3.2 2 10. 96 5.08 57.2 0 1. 08 5.01 miss = Nuclide energy was not found in the coincidence library. 10/3/2-. 12:12:20PM Page 3 of8 Activity Activity Caine (pCilgrams)

Uncertainty Corr 4.33E-01 2.42E-01 miss 3.81E-01 l.52E-01 miss 3.16E-01 1. 06E-01 miss 6.3 2E-0 1 6.33E-01 miss 2.46E-0 1 l.40E-01 miss 4.02E-02 4.03E-02 miss INTERFERENCE CORRECTED REPORT 10/3/L.. 12:12:20PM Page 4 of8 Analysis Report for 03-0ct-16-10006 L3-1 02198-FRGS-006SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 1.000 6.31E+OO 1.17E+OO Cs-137 1. 000 1.44E-01, 4.96E-02 Tl-208 0.997 1. 07E-0 1 3.BSE-02 X Bi-211 0.956 Pb-212 1. 000 2.31E-01 6.97E-02 Bi-214 0.999 2.16E-01 8.BlE-02 Pb-214 1.000 3.48E-01 8.lBE-02 ? Ra-226 0.999 6.32E-01 6.33E-01 Ac-228 1. 000 2.46E-01 1. 40E-01 ? fi. ,S--J. lt ~3 4.~2 4.0~ ? = nuclid e i s part of an undetermined solution ::r/a/ X = nuclid e rejected by the interference analysis J(),]A f? @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/3/:.. . ..:i 12:12:20PM Page 5 of8 Analysis Report for 03-0ct-16-10006

+ + + + + + + + + L3-10219B-FRGS-006SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) 6 510. 71 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/3/2016 12:11:46PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty 1.47368E-02 62.:0 Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Colnc Name (keV) (pCUgrams) (pCilgrams) (pCi/grams)

Corr K-40 1460.82

10.66 6.31E+OO l.15E-01 1.15E-01 miss Cr-5 1 320.08 9.9 1 1.40E-01 3.52E-01 3.52E-01 free Mn-54 834.85 99.98 -6.90E-03 3.75E-02 3.75E-02 miss Co-58 810.76 99.45 -1.61E-03 3.00E-02 3.00E-02 miss 1674.73 0.52 O.OOE+OO 2.78E+OO miss Co-60 1173.2 3 99.85 -2.58E-02 3.lOE-02 3.61E-02 miss 1 332.49 99.98 4.22E-03 3.l OE-02 miss NL-94 702.65 99.81 -8.94E-03 2.56E-02 2.56E-02 miss 871. 09 99.89 -3.84E-03 3.81E-02 miss Ag-108m 79.13 6. EiO 7.95E-02 2.34E-02 7.97E-01 miss 433.94 90.50 -1.31E-02 2.34E-02 miss 614.28 89.80 -6.70E-03 2.59E-02 miss 722.94 90.80 -3.0BE-03 2.86E-02 miss Sn-11 3 255.13 2 .11 3 .13E-01 4.88E-02 1. 43E+OO free 391.70 64.97 -2.47E-03 4.88E-02 free Cs-134 475.36 1. 48 5.llE-01 3.84E-02 2.27E+OO mi ss 563.25 8.34 2.28E-0 2 3.42E-01 mi ss 569.33 1 5.37 6.54E-0 2 2.20E-0 1 miss 10/3/2,. , 12:12:20PM Page 6 of8 Analysis Report for 03-0ct-16-10006 L3-10219B-FRGS-006SS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCi/grams) (pCl/grams) (pCilgrams)

Corr Cs-134 604. 72 97.6 2 5.69E-03 3.84E-02 3.84E-02 miss 795.86 85.46 4.35E-03 5.28E-02 miss 801.95 8.69 -6.18E-02 3.74E-01 miss 1038. 61 0.99 O.OOE+OO 9.83E-01 miss 1167. 97 1. 79 -1.86E-01 l.60E+OO miss 1365.19 3.0 2 O.OOE+OO 3.87E-0 1 miss + Cs-137 661.66

85.10 1. 44E-01 3.98E-02 3.98E-02 miss + Eu-152 121. 7 8 28.67 6.95E-0 3 7.55E-02 9.74E-02 miss 2 44.70 7.61 l.62E-02 3.52E-01 miss 2 95.94 0.45 1.2 4E+Ol l.13E+Ol miss 3 44.2 8 2 6.60 -1.26E-03 7.55E-02 miss 3 67.79 0.86 -8.95E-01 2.19E+OO miss 411.12 2.2 4 -2.89E-01 1.35E+OO miss 443.96 2.83 -5.66E-02 7.62E-01 miss 488.68 0.4 2 -8.16E-01 7.19E+OO miss 563.99 0.49 -7.39E-01 5.19E+OO miss 586.2 6 0.46 -4.12E+OO 3.89E+OO miss 678.62 0.47 -9.48E-01 5.2 8E+OO miss 688.67 0.86 3.68E-01 3.40E+OO miss 719.35 0.2 8 2.00E+OO 9.2 9E+OO miss 778.90 12. 96 5.99E-02 2.98E-01 miss 810.45 0.3 2 O.OOE+OO 8.75E+OO mis s 867.37 4.26 2.35E-01 8.93E-01 miss 919.33 0.43 -4.37E+OO 7.16E+OO miss 964. 08 14.6 5 4.00E-02 3.28E-01 mi ss 1085.87 10.2 4 l.44E-02 4.72E-01 miss 1089.74 1. 73 4.51E-01 2.80E+OO miss 1112. 07 13.69 -6.05E-02 2.54E-01 miss 1212.95 1. 43 4.56E-01 3. 92E+OO miss 1249.94 0.19 4.38E+OO 2.30E+Ol miss 1 2 99.14 1. 63 7.2 8E-01 3.06E+OO miss 1408.01 2 1.07 3 .13E-0 2 2.50E-Ol miss 1457.64 0.50 O.OOE+OO 1.49E+Ol miss 1528.10 0.28 4.98E+00 l.79E+Ol miss + Eu-154 123.07 40.40 2.29E-02 7.71E-02 7.71E-02 mis s 2 47.93 6.89 -1.17E-01 3.67E-01 miss 591.76 4.95 -1.19E-02 6.48E-01 miss 6 92.4 2 1. 78 4.90E-01 2.16E+OO miss 723. 30 2 0.06 -1.63E-0 2 l.50E-01 miss 756.80 4.52 1.49E-01 9.02E-01 miss 873.18 1 2.08 -l.61E-02 2.84E-01 miss 996.2 9 10.48 O.OOE+OO 9.00E-02 miss 1004.76 18.01 3.89E-02 2.34E-01 miss 1 274.43 34.80 -3.28E-02 l.09E-01 mis.::3 1 596.48 1. 80 -l.68E-Ol l.98E+OO miss + Eu-155 45.3 0 1. 31 -7.53E-01 1.39E-01 8.2 6E+OO miss 60.01 1. 22 5.42E+OO l.06E+Ol miss 86.55 3 0.70 3.46E-0 3 l.39E-01 miss 105.31 2 1.10 8.14E-02 1. 75E-Ol miss + Tl-208 583.19

85.00 l.07E-01 2.37E-0 2 2.37E-0 2 miss + Bi-211 351.07

13.02 8.65E-0 1 2.66E-01 2.66E-01 miss 10/3/,.._ . .i 12:12:20PM Page 7 of8 Analysis Report for 03-0ct-16-10006 L3-10219B-FRGS-006SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr + Pb-2 11 404.85 3. 78 -3.97E-02 7.45E-01 7.45E-01 miss 427.09 1. 76 -1. llE-01 1.66E+OO miss 832.01 3.5 2 4.81E-01 1.39E+OO miss + Bi-212 39.86 1. 06 -2.70E-01 8.21E-01 8.82E+OO miss 727. 33 6.67 3.2 0E-01 8.21E-01 miss 785.37 1.10 6.12E-01 3.79E+OO miss 1 620.50 1. 47 O.OOE+OO 9.00E-01 mi ss + Pb-212 115.18 0.60 -9.05E-02 8.64 E-02 4.75E+OO miss 238.63

43.60 2.31E-01 8.64E-02 miss 300.09 3.30 5.61E-01 1.09E+OO miss + Pb21 2-XR 74.8 2 10.28 9.53E-01 4.81E-01 9.43E-01 miss 77 .11 17.10 3.60E-01 4.81E-Ol mi ss 87.35 3. 97 5.2 9E-01 l.16E+O O mi ss 89.78 1. 46 9.30E-01 2.83E+OO miss + Bi-21 4 609.32

45.49 2.16E-01 9.46E-02 9.46E-02 miss 768. 3 6 4.89 4.90E-01 1.16E+OO miss 806.18 1. 2 6 1.35E-01 3.12E+OO miss 934.06 3 .11 2.07E-0 1 1.41E+OO miss 11 2 0.29 14. 9 2 3.83E-01 5.3 7E-Ol miss 11 55. 21 1. 63 5.70E-01 3.08E+OO miss 1 238.12 5.83 5.19E-02 1.03E+OO miss 1280.98 1. 43 8.74E-01 3.75E+OO miss 1377. 67 3.99 3.56E-01 l.63E+OO miss 1385.31 0.79 3.U7E+OO 8.21E+OO miss 140 1.52 1. 33 -4.2 3E-01 2.42E+OO miss 1407.99 2.39 2.75E-01 2.20E+OO miss 1 509.21 2.13 -1.86E-01 l.60E+OO miss 1 661. 27 1. 05 2.98E-01 4.42E+OO miss 1729.59 2.88 O.OOE+OO 4.84E-01 miss 1 764.49 15.30 3.07E-01 5.69E-01 miss 1 847.43 2.03 5.31E-01 2.47E+OO miss > 2118. 51 1.1 6 O.OOE+OO O.OOE+OO miss + Pb-2 1 4 2 41.99

7.25 4.33E-01 9. 72E-02 4.55E-01 miss 2 95.2 2

18.42 3.81E-01 1.59E-01 miss 3 51.93

35.60 3.16E-0 1 9.72E-02 miss 785. 96 1. 06 -3.82E-0 1 3.66E+OO miss + Pb214-XR 74.82 5.80 1.69E+OO 8.48E-01 1.67E+OO miss 77 .11 9.70 6.35E-01 8.48E-01 miss 87.35 2.2 4 9.38E-01 2.0 6 E+OO miss 89.78 0.8 2 1.66E+OO 5.04E+OO miss + Ra-226 1 86.2 1

3.64 6.32E-01 1. OOE+OO 1.00E+OO miss + Ac-228 129.07 2.42 -1.58E-0 2 1.70E-01 1.2 1E+OO miss 209.25 3.89 5.79E-0 1 8.14E-01 miss 27 0.24 3.46 5.12E-01 9.66E-01 miss 32 8.00 2.9 5 5.78E-01 1.23E+OO miss 338.32 11. 2 7 1.64E-01 3.59E-01 miss 409.46 1. 92 4.0lE-01 1.79E+OO miss 463.00 4.40 3.0lE-01 8.81E-01 miss 7 94. 95 4.25 1.99E-01 1. llE+OO miss 911. 20

2 5.80 2.46E-01 1.70E-01 miss 964. 77 4.99 3.41E-02 9.62E-01 miss 10/3/ ... _ .d 12:12:20PM Page 8 of8 Analysis Report for 03-0ct-16-10006 L3-10219B-FRGS-006SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCilgrams) (pCl!grams) (pCi!grams)

Corr Ac-228 968.97 15.80 2.41E-01 1.70E-01 4.21E-01 miss 1588.2 0 3.22 2.99E-01 l.39E+OO miss + Pa-231 27.36 10.30 O.OOE+OO 1.41E-01 l.41E-01 miss 283.69 1. 70 2.38E-01 l.57E+OO miss 300.07 2.47 7.49E-01 l.45E+OO miss 302.65 2.20 -4.36E-0 2 l.2 1E+OO miss 330.06 1. 40 -2.03E+00 l.52E+OO miss + Th-234 92.38 2 .13 3.68E-01 2.68E+O O 2.68E+OO miss 92. 80 2.10 1.20E+OO 2.87E+OO miss 112. 81 0.2 1 -1.03E+OO l.60E+Ol miss + U-235 143.76 10.96 -1.34E-02 6.3'7 E-02 l.99E-01 miss 163.33 5.08 -3.07E-0 3 4. 96E-01 miss 185.71

57.20 4.02E-02 6.37E-02 miss 2 02.1 1 1. 08 -l.94E-01 l.76E+OO miss 205.31 5.01 9.64E-02 5.41E-01 miss + Am-241 59.54 35.90 1.50E-01 3.73E-0 1 3.7 3E-01 miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

VI .j-1 s:::: :::s 60 55 50 45 40 35 8 30 1000 2000 3000 000001600 I . CNF 4000 channel 5000 Live Time : 600. 000 sec Real Time : 600. 430 sec Start: 1: -0.Z(keV) stop : 8192:2047.4(kev)

Acq. start :Mon Oct 03 12:01:41 2016 6000 7000 8000 10/31~ J 12:30:54PM

~~~pex-Gamma Analysis Report for 03-0ct-16-10007 L3-102198-FRGS-OO?SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real lime Dead lime Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 03-0ct-16-10007

L3-10219B-FRGS-007SS

1 L 130G Soil Sample 1.055E+03 grams : Default : 9/27/2016 10:05:00AM

10/3/2016 12:01:50PM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 600.0 seconds : 600.9 seconds : 0.15% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16002 PEAK WITH NID REPORT Peak Analysis Performed on 10/3/2016 12: 12:26PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 10/3/21. 12:30:54PM Page 2 of8 Analysis Report for 03-0ct-16-10007 L3-10219B-FRGS-007SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum Tentative No. (keV) start end Centroid Area Uncertainty Counts Nuclide 1 186.02 740 -748 744.73 1.66E+Ol 18.52 6.28E+Ol Ra-226 2 238.48 947 -960 954.41 6.26E+Ol 26.18 7.68E+Ol Pb-212 3 351.74 1 401 -1415 1407.15 6.51E+Ol 19.72 2.58E+Ol Pb-214 Bi-211 4 609.17 2429 -2442 2 436.43 4.67E+Ol 16.34 1.67E+O l Bi-21 4 5 661.49 2639 -2652 2 645.68 9.56E+Ol 20.51 8.87E+OO Cs-13 7 6 910.94 3639 -3649 3643.49 2.2 1E+O l 10.56 5.79E+OO Ac-~28 7 968.76 3869 -3880 3874.80 1. 40E+Ol 8.54 3.96E+OO Ac-228 8 1460.65 5834 -5852 5843.57 1.14E+02 21.97 5.43E+OO K-40 ~v M = First peak in a multiplet region /0')-//, m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.99 1460.82

10.66 6.65E+OO 1.40E+OO miss Cs-137 0.99 661.66

85.10 4.06E-01 9.99E-02 mis s Bi-211 0.97 351. 07

13.02 1.17E+OO 4.00E-01 miss Pb-212 0.99 115 .18 0.60 238.63

43.60 2.62E-01 l.17E-01 free 300.09 3.30 Bi-214 0.99 609.32

45.49 3.78E-01 1. 40E-01-0. 948 768.36 4.89 806.18 1. 2 6 934.06 3 .11 1120.2 9 14.92 1155.2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401.52 1. 33 1 407.99 2.39 Analysis Report for 03-0ct-16-10007 L3-10219B-FRGS-007SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1509.21 1661.27 1729.59 1764.49 1847.43 2118.51 Pb-214 0.51 2 41.99 2 95.22 351.93 785.96 Ra-22 6 0.99 186.21 Ac-22 8 0.99 129.07 209.25 270.2 4 328.00 338.3 2 409.46 463.00 794.95 911.20 964. 77 968.97 1588.2 0 U-235 0.99 143.76 163.33 185. 71 2 02 .11 205.31 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2 .13 1. 05 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 3.64 2.42 3.89 3.46 2.95 11. 27 1. 92 4.40 4.2 5 25.80 4.99 15.80 3.22 10. 96 5.08 57.2 0 1. 08 5.01 miss = Nuclide energy was not found in the coincidence library. 10/3/2\. . 12:30:54PM Page3 of8 Activity Activity Caine (pCi/grams)

Uncertainty Corr 4.2 6E-01 1. 4 6E-01 free 7.40E-01 8.34E-Ol free 3.91E-01 1.90E-01 0.990 4.22E-01 2.60E-0 1 0.990 4. 71E-02 5.31E-02 free INTERFERENCE CORRECTED REPORT 10/3/2L -12:30: 54PM Page 4 of8 Analysis Report for 03-0ct-16-10007 L3-10219B-FRGS-007SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCi!grams)

Uncertainty K-40 0.998 6.65E+OO 1.40E+OO Cs-137 0.998 4. 0 6E-Ol" 9.99E-02 ? Bi-211 0.973 1.17E+OO 4.00E-01 Pb-21 2 0.999 2.62 E-01 1.17E-01 Bi-214 0.999 3.78 E-01 1.40E-01 ? Pb-214 0.512 4.26E-01 1.46E-01 ? Ra-226 0.9St8 7.40E-01 8.34E-01 Ac-228 0.998 4.02E-01 1. 53E-01 ? u~ (lA--J.'-" 0~ 4.~2 5.~ ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis /p,-3-1? @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/3/'R/'L..,, 12:30:54PM Page 5 of8 Analys i s Report for 03-0ct-16-10007

+ + + + + + + + + L3-102198-FRGS-007SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified. M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/3/2016 12:12:26PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nucl i de Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCilgrams) (pCl/grams) (pCi/grams)

Corr K-40 1460.82 1: 1 0.66 6.65E+OO 6.42E-01 6.42E-01 miss Cr-51 320.08 9.9 1 -1.07E-01 4.86E-01 4.86E-01 free Mn-54 834.85 99.98 1.88E-0 2 6.44E-0 2 6.44E-02 miss Co-58 810.76 99.45 4.92E-04 4.76E-02 4.76E-02 1.000 1674.73 0.52 O.OOE+OO 3.73E+OO 1. 024 Co-60 1173.2 3 99.85 2.82E-03 5.2 3E-02 5.2 3E-02 0.947 1332.49 99.98 7.00E-03 6.59E-0 2 0.947 Nb-94 702.65 99.8 1 l.33E-03 2.94E-02 2.94E-0 2 0.944 871.09 99.89 -3.84E-03 3.39E-02 0.944 Ag-1 08m 79.13 6.60 2.78E-0 1 4.0lE-0 2 1.65E+OO miss 43 3.94 90.50 -1.04E-02 5.35E-02 0.887 614.2 8 89.80 -6.0SE-03 4.0lE-02 0.886 722. 94 90.80 1.15E-02 5.73E-0 2 0.887 Sn-113 255 .13 2 .11 6.61E-01 6.04E-02 1.94E+OO free 391.70 64.97 -2.25E-0 2 6.04E-02 free Cs-134 475.36 1. 48 -5.20E-01 4.0SE-02 3. llE+OO miss 563.25 8.34 -1.54E-01 4.70E-01 0.896 569.3 3 15.37 5.23E-02 3.82E-01 0.888 604. 72 97.62 -2.2 6E-02 4.0SE-0 2 0.931 10/3/2.._ , 12:30:54PM Page 7 of8 Analysis Report for 03-0ct-16-10007 L3-10219B-FRGS-007SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCi!grams)

Corr Pb-211 427.09 1. 76 -6.99E-01

1. 37E+00 2. 28E+OO mi.s s 832.01 3.5 2 5.99E-02 1. 69E+OO mis s + Bi-212 39.86 1. 06 5.54E+00 1.18E+OO 3.45E+O l 0.998 727. 33 6.67 7.16E-01 1.18E+OO 0.982 785.37 1.10 -2.44E-01

4. 69E+OO 0.944 1620.50 1. 47 O.OOE+OO 1.23E+OO 1. 006 + Pb-212 115 .18 0.60 2.29E+OO 1.55E-01 8. 61E+OO miss 238.63

43.60 2.62E-0 1 1. 55E-01 fre e 300.09 3.30 1.78E-02 l.40E+OO free + Pb212-XR 74.82 10.28 7.77E-01 1.04E+OO 1.78E+OO miss 77 .11 17.10 1.0lE+OO 1.04E+OO miss 87.35 3.97 7. 96E-01 2.23E+OO miss 89.78 1. 46 1.32E+OO 5.26E+OO miss + Bi-2 14 609.3 2

45.49 3.78E-01 l.38E-01 l.38E-01 0.948 768.36 4.89 3.61E-01 l.2 2E+OO 0.94 2 806.18 1. 2 6 1.77E-01 4.99E+OO 0.92 3 934.06 3 .11 8.31E-01 2.60E+OO 0.944 1120.2 9 14.92 3.35E-01 6.64E-01 0.944 1155.2 1 1. 63 4.88E-01 5. 13E+OO 0.943 1238.1 2 5.83 3.40E-01 1.3 1E+OO 0.944 1 2 80.98 1. 43 -3.2 7E-01 3.86E+OO 0.944 1 377.67 3.99 2.82E-01 1.55E+OO 1.030 1385.31 0.79 O.OOE+OO 2.15E+OO 0.945 1401.52 1. 33 4.78E-01 4.44E+OO 0.945 1407.99 2.39 5.97E-01 2.87E+OO 0.945 1509.21 2.13 7.78E-01 3.38E+OO 0.950 1661.2 7 1. 05 1.31E+OO 6.07E+OO 1.00 1 1729.59 2.88 4.39E-01 2.04E+OO 1.119 1764.49 15.30 1.52E-01 7.04E-01 1.001 1847.43 2.03 O.OOE+OO 9.2 9E-01 1.063 > 2 118.51 1.16 O.OOE+OO 0.00E+OO 1.041 + P b-214 241.99 7.25 7.17E-02 1.40E-01 7.46E-01 1.000 295.22 18.42 2.53E-01 3.60E-01 1. 000 351.93

35.60 4.26E-01 1.40E-01 free 785.96 1. 06 5. llE-01 5.02E+OO 1. 000 + Pb214-XR 74.82 5.80 1.3 8E+OO 1. 84E+OO 3.15E+OO miss 77 .11 9.70 1.78E+OO l.84E+OO miss 87.35 2.24 1.41E+OO 3. 96E+OO miss 89.78 0.82 2.34E+OO 9.36E+OO miss + Ra-226 186.2 1

3.64 7.40E-01 1.34E+OO l.34E+OO free + Ac-2 2 8 1 2 9.07 2.42 1.16E-01 1.87E-01 1. 88E+OO 0.944 2 09.25 3.89 5.74E-01 1. 3 1E+OO 0.978 2 70.2 4 3.46 4.72E-01 1.46E+OO 0.955 328.00 2.95 2.74E-0 1 l.82E+OO 0.955 338.32 11. 27 1.85E-01 4.68E-01 0.99 2 409.46 1. 92 2.28E+OO 3.24E+OO 0.937 463.00 4.40 5.82E-01 1. 43E+OO 0.933 794.95 4.2 5 -3.41E-02

1. 44E+OO 0.942 911. 2 0

2 5.80 3.91E-01 1.87E-01 0.990 964.77 4.99 3.98E-01 1. 25E+OO 0.981 968. 97

15.80 4.22E-01 2.83E-01 0.990 1013/L.~ J 12:30:54PM Page 8 of8 Analysis Report for O~-Oct-16-10007 L 3-102198-FRGS-OO?SS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Ac-228 1588.20 3.22 4.61E-01 l.87E-01 2.21E+OO 1.002 + Pa-231 27.36 10.30 -2.65E-01 1.8'7E+OO 3.4 4E+OO 0.998 283.69 1. 70 -3.84E-01 2.25E+OO 1.000 300.07 2.47 2.3 8E-02 l.87E+OO 1. 000 302.65 2.2 0 2.2 9E-01 2.llE+OO 1.000 330.06 1. 40 -3.2 0E-01 3.41E+OO 1. 000 + Th-234 92.38 2.13 1.60E+OO 4.71E+OO 4.71E+OO free 92.80 2.10 1. 96E+OO 4.87E+OO free 112. 81 0.21 5.07E+OO 3.12E+Ol free + U-235 143.76 10. 96 -3.79E-0 2 8.53E-02 4.29E-01 free 1 63.33 5.08 -1.87E-02 7.68E-01 free 185.71

57.2 0 4. 71E-02 8.53E-02 free 2 02 .11 1. 08 2.03E+OO 4.40E+OO miss 2 05.31 5.01 1.18E-01 7.97E-01 free + Am-241 59.54 35.90 1.28E-01 l.12E+OO l.12E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? :;; CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45 -40 35 V) """' C :::::, 8 30 25 20 15 ..... "' ' :::, ' "' ...... "' ' ..C> c.. ..C> c.. *;.; 1000 2000 3000 0000016002.CNF I 4000 channel 5000 Live Time 600.000 sec Real Ti me 600. 920 sec start: 1 -0.l(kev) stop : 8192 2047 .O(kev) Acq. start Mon act 03 12:01:50 2016 6000 7000 8000 10/6/2016 12:02:31PM

~~~pex-Gamma Analysis Report for 06-0ct-16-10008 L3-10219B-FRGS-008SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 06-0ct-16-10008

L3-10219B-FRGS-008SS

1 L 130G Soil Sample 1.153E+03 grams : Default : 10/3/2016 2:40:00PM

10/6/2016 11:39:21AM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 se conds : 300.5 seconds : 0.15% : 2.80 : 120-8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16046 PEAK WITH NID REPORT Peak Analysis Performed on 10/6/2016 11 :44:23AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM l)~ {f'u~~!) <<;:sDA-,~Jb(t~ Page I of7 10/6/2016 12:02:31PM Page 2 of7 Analysis Report for 06-0ct-16-10008 L3-102198-FRGS-OOBSS Peak Energy ROI No. (keV) start 1 2 38.54 950 -2 351.86 1401 -3 1460.78 5836 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1413 5852 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.66 3.88E+Ol 16.48 2.45E+Ol 1407.60 2.93E+Ol 11. 97 5.35E+OO 5844.09 5.49E+Ol 15.42 4.28E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 1. 00 1460.82 Bi-211 0. 96 351.07 Pb-212 1. 00 11 5.18 238.63 300.09 Pb-2 14 1. 00 241.99 295.22 351.93 785. 96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 10.66 13. 02 0.60 43.60 3.30 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. Activity (pCilgrams) 5.84E+00 9.61E-01 2.96E-01 3.52E-01 Activity Uncertainty

1. 72E+OO 4. 22E-*01 l.35E-01 l.54E-01 Tentative Nuclide Pb-212 Pb-214 Bi-211 K-40 Caine Corr miss miss free free 10/6/2016 12:02:31 PM Analysis Report for 06-0ct-16-10008 L3-102198-FRGS-OOBSS INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? B i-211 P b-2 12 ? Pb-214 Nuclide Id Confidence

1. 000 0.963 1. 000 1.000 ? X = = nuclide is part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 5.84E+00 9.61E-01 2. 96E-01 3.52E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 1.72E+OO 4.22E-01 1.35E-01 1.54E-01 Page 3 of7 Comments 10/6/2016 12:02:31PM Page 4 of7 Analysis Report for 06-0ct-16-10008

+ + + + + + + + + L3-10219B-FRGS-008SS Peak Locat e Performed on Peak Locat e From Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/201 6 11:44:23AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr K-40 1460.8 2

10.66 5.84E+OO 1.04E+OO 1.04E+OO miss Cr-51 320.08 9.91 -1.74E-02 5.71E-Ol 5.71E-01 free Mn-54 834.85 99.98 -1.17E-02 7.23E-02 7.2 3E-02 miss Co-58 810.76 99.45 -3.92E-03 5.78E-02 5.78E-02 1. 000 1674.73 0.52 O.OOE+OO 6.62E+OO 1. 024 Co-60 117 3.23 99.85 -2.06E-02 7.57E-02 7.57E-02 0.947 133 2.49 99.98 1. 3 6E-02 1.04E-01 0.947 Nb-94 702.65 99.81 -6.lOE-03 6.79E-02 6.79E-02 0.944 871.09 99.89 1.69E-02 9.0BE-02 0,944 Ag-108m 79.13 6.60 -9.87E-01 6.42E-02 1.97E+OO miss 433.94 90.50 -2.47E-0 3 8.08E-0 2 0.887 614.28 89.80 2.37E-02 8.51E-0 2 0.886 7 22.94 90.80 -6.55E-02 6.42E-02 0.887 Sn-11 3 2 55.13 2 .11 -1.80E-01

6. 71E-02 2.52E+OO free 391.70 64. 97 -3.03E-02 6.71E-02 free Cs-134 475.36 1. 48 -1.36E+OO 2.55E-02 4.3 0E+OO miss 563.25 8.34 2.55E-01 1.04E+OO 0.896 569.33 15.37 -2.46E-01 3.23E-01 0.888 604. 72 97.62 -2.20E-02 7.40E-02 0.931 10/6/2016 12:02:31PM P age 5 of7 Analysis Report for 06-0ct-16-10008 L3-10219B-FRGS-008SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 O.OOE+OO 2.55E-02 2.55E-0 2 0.933 8 01.95 8.69 O.OOE+OO 2.62E-01 0.898 1 038.61 0.99 -8.03E-01 7.09E+OO 0.943 1167.97 1. 79 2.18E+OO 6.58E+OO 1.08 1 1365.19 3.0 2 2. 72E-01 2.34E+OO 1.128 + Cs-137 661.66 85.10 1.88E-0 2 9.35E-02 9.35E-02 miss + Eu-1 52 121. 78 2 8.67 -5.2 0E-02 1.44E-01 2.05E-0 1 0.936 2 44.70 7.6 1 9.98E-02 7.56E-01 0.935 2 95.94 0.45 7.42E+OO 1.82E+Ol miss 344.28 26.60 -9.09E-03 1.99E-01 0.957 367.79 0.86 -3.47E-01 5.37E+OO 0.884 411.1 2 2.24 2.82E-01 2.53E+OO 0.908 443. 96 2.83 -3.62E-01 1.77E+OO 0.934 488.68 0.42 -3.84E+OO l.1 9E+Ol miss 563.99 0.49 2.33E+OO l.3 9E+Ol 0.934 586.2 6 0.46 -2.81E-01

1. 31E+Ol 0.94 2 678.62 0.47 -2.41E+OO 1.49E+Ol 0.887 688.67 0.86 O.OOE+OO 2.19E+OO 0.980 719.35 0.28 8.37E-Ol 2.70E+Ol miss 778.90 12. 96 -4.02E-02 7.25E-01 0.94 5 810.45 0.32 1.50E+OO 1.66E+Ol 1.050 867.37 4.26 2.34E-01 1.87E+OO 0.928 919.33 0.43 O.OOE+OO 5.34E+OO 0.98 1 964.08 14.65 9.51E-0 3 6.1 4E-01 1. 022 1085.87 10.24 -1.52E-01 8" 2 4E-01 1. 018 1.0 89. 74 1. 73 6.43E-01 6.06E+OO 0.952 1112.07 13. 69 -1.78E-01 5.09E-01 0.992 12 12.95 1. 43 -4.19E+OO 5.53E+OO 0. 9 2 9 1249.94 0.19 -6.99E-01 4.54E+Ol 1. 097 1299.14 1. 63 O.OOE+OO 1.84E+OO 0.944 1408.01 21.07 O.OOE+OO 1.44E-01 0.983 1457.64 0.50 -1.17E+Ol 2.96E+Ol 1. 076 1528.10 0.2 8 O.OOE+OO l.12E+Ol 1. 007 + Eu-154 123.07 40.40 4.39E-02 1.80E-01 1.80E-01 0.934 247.93 6.89 -4.0lE-02 7.54E-01 0.928 591.76 4.95 9.48E-01 2.03E+OO 0.915 692.4 2 1. 78 -1.09E+OO 3.02E+OO 0.936 723. 30 2 0.06 -1. 87E-01 3.48E-01 0.935 756.80 4.52 2.34E-01 1. 89E+OO 0.915 873.1 8 12.08 -8.86E-02 6.58E-01 0.932 996.29 10.48 3.49E-01 l.13E+OO 0.971 1004.76 18.01 7.49E-02 6.00E-01 0.978 1274.43 34.80 9.03E-02 3.24E-01 0.981 1 596.48 1. 80 O.OOE+OO 1.56E+OO 1.175 + Eu-1 55 45.3 0 1. 31 4.29E+OO 3.5 4E-01 4.lOE+Ol 0.999 60.01 1. 22 2.09E+Ol 4.88E+Ol 1. 000 86.55 3 0.70 3.43E-02 3.54E-01 free 105.31 2 1.10 2.33E-03 4.34E-01 1. 000 + Tl-208 58 3.19 85.00 1.15E-Ol 1. 59E-Ol 1.59E-01 0.932 + Bi-211 351.07

13.02 9.61E-01 3.64E-01 3.64E-01 miss + Pb-2 11 404.85 3.78 -9.98E-0 2 1.1 6E+OO l.16E+OO miss 10/6/2016 12:02:31PM Page 6 of7 Analysis Report for 06-0ct-16-10008 L3-102198-FRGS-OOBSS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCi!grams) (pCi/grams)

Corr Pb-2 11 427.09 1. 76 -5.84E-01 1.16E+OO 3.3 4E+OO miss 8 32.01 3.5 2 -7.31E-02 l.6 1E+OO miss + Bi-212 39.86 1. 06 -8.llE+OO l.62E+OO 4.2 9E+Ol 0.998 727.33 6.67 2.62E-01 l.62E+OO 0.98 2 785.37 1.10 8.33E-01 7.69E+OO 0.944 1620.50 1. 47 O.OOE+OO 2.25E+OO 1. 006 + Pb-212 11 5.1 8 0.60 2.79E+OO 1.56E-01 l.18E+Ol miss 2 38.63

43.60 2.96E-01 l.56E-01 free 300.09 3.30 6.95E-01 1.95E+OO free + Pb212-XR 74.82 10.2 8 7.08E-01 1. 2 3E+OO 2.50E+OO miss 77.11 17.10 2.58E-01 1.23E+OO miss 87.35 3.97 2.15E-02 2.42E+OO miss 89.78 1. 46 1.62E+OO 5.88E+OO miss + Bi-2 1 4 609.32 45.49 l.76E-01 3.18E-01 3.18E-01 0.948 763.36 4.89 2.47E-01 1.71E+OO 0.94 2 806.18 1. 26 O.OOE+OO 4.77E+OO 0.923 934.06 3.11 -3.80E-01 3.07E+OO 0.944 1120.2 9 14.92 2. llE-01 8.78E-01 0.944 11 55. 2 1 1. 63 6.70E-01 5.80E+OO 0.94 3 1238.12 5.83 -2.87E-01 2.40E+OO 0.944 1 2 8 0.98 1. 43 7.61E-0 1 5.60E+OO 0.944 1377. 67 3.99 7.93E-01 2.84E+OO 1. 030 1385.31 0.79 O.OOE+OO 3.94E+OO 0.94 5 1401.52 1.33 8.75E-01 6.44E+OO 0.94 5 1407.99 2.39 O.OOE+OO 1. 32E+OO 0.945 1509.21 2 .13 5.75E-01 4.2 3E+OO 0.950 1 661.27 1. 05 1.50E-01 8.81E+OO 1.001 1729.59 2.88 4.02E-01 2.96E+OO 1.119 1764.49 15.30 -1.07E-0 2 6.31E-01 1.001 1847.43 2.03 O.OOE+OO 1. 70E+OO 1.063 > 2 118. 51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 241.99 7.25 7.08E-01 1.33E-01 1.14E+OO 1. 000 2 95.22 18.42 1.66E-01 4.54E-01 1.000 351.93

35.60 3.52E-01 1.33E-Ol free 785. 96 1. 06 -1.75E-01 6.51E+OO 1. 000 + Pb214-XR 74.82 5.80 l.25E+OO 2.18E+OO 4.43E+OO miss 77 .11 9.70 4.54E-01 2.18E+OO miss 87.35 2.24 3.81E-02 4.2 8E+OO miss 89.78 0.82 2.88E+OO l.05E+Ol miss + Ra-226 1 86.2 1 3.64 3.77E-01 l.59E+OO 1.59E+OO free + Ac-228 129.07 2.42 4.80E-01 5.06E-0 1 2.64E+OO 0.944 209.25 3.89 -l.32E-01 l.44E+OO 0.978 270.24 3.46 -l.46E-01 1.82E+OO 0.955 328.00 2.95 l .13E+OO 2.63E+OO 0.955 338.32 11. 27 6.70E-02 7.0lE-01 0.992 409.46 1. 92 -3.17E-01 2.46E+OO 0.937 463.00 4.40 5.04E-02 1. 51E+OO 0.933 794.95 4.25 O.OOE+OO 5.06E-Ol 0.942 911. 20 2 5.80 2.95E-Ol 5.84E-01 0.990 964. 77 4.99 l.09E-01 2.lOE+OO 0.981 968. 97 1 5.80 l.3 0E-01 6.58E-01 0.990 10/6/2016 12:02:31PM Page 7 of7 Analysis Report for 06-0ct-16-10008 L3-102198-FRGS-OOBSS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCilgrams) (pCUgrams) (pCi/grams)

Corr Ac-228 1588.20 3.22 O.OOE+OO 5.06E-01 1.02E+OO 1. 00 2 + Pa-2 31 27.36 10.30 -9.40E-01 2.12E+OO 4.70E+OO 0.998 283.69 1. 70 -2.3 7E-01 3.09E+OO 1. 000 300.07 2.47 9.2 8E-01 2.60E+OO 1. 000 302.65 2.20 -2.9 7E-01 2.12E+OO 1. 000 330.06 1. 40 -2.2 8E+OO 2.72E+OO 1. 000 + Th-234 92.38 2.1 3 1.30E+OO 4.99E+OO 5.13E+OO free 92.80 2.10 3.61E-01 4.99E+OO free 112. 81 0.2 1 3.55E+OO 3.07E+Ol free + U-235 143.76 10.9 6 -1.41E-01 1.0lE-01 4.64E-01 free 163.33 5.08 1.94E-01 l.18E+OO free 185.71 57.20 1.30E-02 1.0lE-01 free 2 02.11 1. 08 1.74E-01 4.2 9E+OO miss 2 05.31 5.01 7.76E-03 9.85E-01 free + Am-241 59.54 35.90 -5.06E-01 1.42E+OO l.42E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) +-' C ::::I 60 55 50 45 40 35 8 30 25 20 1000 2000 3000 0000016046.CNF 4000 channel 5000 Live Time :300.000 sec Real Time : 300.460 sec Start: 1: -0.l(kev)

Stop : 8192: 2047 .O(kev) Acq. Start :Thu oct 06 11:39:21 2016 6000 7000 8000 10/6hv ,6 12:38:31PM

~5'~pex-Gamma Analysis Report for 06-0ct-16-10009 L3-10219B-FRGS-009SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels}

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 06-0ct-16-10009

L3-10219B-FRGS-009SS

1 L 130G Soil Sample 1.261 E+03 grams : Default : 10/3/2016 2:30:00PM

10/6/2016 12:15:01PM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.4 seconds : 0.15% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16047 PEAK WITH NID REPORT Peak Analysis Performed on : 10/6/2016 12:20:04PM Peak Analysi s From Channel Peak Analysi s To Channel : 120 : 8192 Tentative NID Library Peak Match Toleranc e -I.)~,./\ J~\ :~;x .. S) '0 (b(t~ : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page I of8 10/6/2C, *~ 12:38:31PM Page2 of8 Analysis Report for 06-0ct-16-10009 L3-102198-FRGS-OOSSS Peak Energy ROI No. (keV) start 1 186.15 742 -2 238.47 949 -3 351.88 1403 -4 609.15 2431 -5 661.37 2640 -6 1460.26 5835 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 749 959 1413 2441 2650 5850 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 745.28 1.66E+Ol 14.07 3.07E+Ol 954.37 2.93E+Ol 16.66 3.33E+Ol 1407. 71 2.07E+Ol 11. 30 1.07E+Ol 2 436.36 1.39E+Ol 8.60 4.lOE+OO 2 645.18 2.74E+Ol 11. 73 7.22E+OO 5841.99 5.58E+Ol 15.83 6.41E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCi/grams)

Uncertainty K-40 0. 98 1460.82

10.66 5.43E+OO 1.61E+OO Cs-137 0.99 661.66

85.10 1.95E-01 8.66E-02 Bi-2 11 0.96 351.07

13. 02 6.19E-01 3.53E-01 Pb-212 0.99 115.18 0.60 2 38.63

43.60 2.05E-O l 1.21E-01 300.09 3.30 Bi-2 1 4 0.99 609.32

45.49 l.89E-01 l.19E-01 768.36 4.89 806.18 1. 2 6 934.06 3 .11 11 2 0.29 14.92 1155. 2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377. 67 3.99 1385.31 0.79 1401.52 1. 33 1407.99 2.39 1509.21 2.13 1 661.27 1. 05 Tentative Nuclide Ra-226 Pb-212 Pb-214 Bi-211 Bi-214 Cs-137 K-40 fl'u./ /(J--lrl~

Coinc Corr miss miss miss free 0.948 Analysis Report for 06-0ct-16-10009 L3-10219B-FRGS-009SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1729.59 1 764.49 1847.43 21 18.51 P b-2 14 1. 00 241. 99 295.22 351.93 785. 96 Ra-226 1. 00 1 86.2 1 U-235 0.99 143.76 163.33 185.71 202 .11 205.31 * ;;; Energy line found in the spectrum.

-;;; Manually added nuclide. ? = Manually edited nuclide. * * -.t: @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 3.64 10. 96 5.08 57.2 0 1. 0 8 5.01 miss = Nuclide energy was not found in the coincidence library. 10/6/2u .... 12:38:31PM Page3 of 8 Activity Activity Caine (pCi/grams)

Uncertainty Corr 2.26E-01 l.2 9E-0 1 free 1. 2 4E+O O 1. 07E+OO free 7.90E-02 6.80E-02 free INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.981 5.43E+OO 1. 61E+OO Cs-137 0.995 l.95E-Ol / 8.66E-0 2 ? Bi-211 0. 960 6.19E-01 3.53E-01 Pb-212 0.999 2.05E-01 l.2 1E-01 Bi-214 0.999 l.89E-01 l.19E-01 ? Pb-214 1. 000 2.26E-01 1. 2 9E-01 ? Ra-226 1.000 1. 24E+OO l.07E+OO ? u~ a .,J,'.W ~2 7.~2 6.~2 {f)b1b /tvdf' Analysis Report for 06-0ct-16-10009 L3-10219B-FRGS-009SS

? = nuclid e is part of an undetermined solution X = nuclid e rejected by the interference analysis @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/6/2u,.., 12:38:31 PM Page4 of8 10/6/20h..

12:38:31 PM Page 5 of8 Analysis Report for 06-0ct-16-10009

+ + + + + + + + + L3-10219B-FRGS-009SS Peak Locate Performed on Peak Locat e From Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/2016 12:20:04PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LiB-BNL. NLB Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi!grams)

Corr K-40 1460.82

10.66 5.43E+OO 1.lOE+OO 1.lOE+OO miss Cr-51 320.08 9.91 -1.06E-01 4.2 9E-01 4.2 9E-01 free Mn-54 834.85 99.98 1.19E-03 6.GlE-02 6.61E-02 miss Co-58 810.76 99.45 1. 44E-0 2 7.73E-02 7.73E-02 1.000 1674.73 0.52 O.OOE+OO 6.06E+OO 1.024 Co-6 0 1173.23 99.85 5.65E-02 2.77E-02 l.33E-01 0.947 1332.49 99.98 O.OOE+OO 2.77E-02 0.947 Nb-94 702.65 99.81 2.23E-03 5.68E-02 8.03E-02 0.944 871.09 99.89 -1.29E-02 5.68E-02 0.944 Ag-108m 79 .13 6.60 2.16E-01 6.07E-02 2.09E+OO miss 433.94 90.50 -1.09E-02 6.07E-0 2 0.887 614.28 89.80 1. 45E-02 6. 72E-02 0.886 722.94 90.80 1.60E-02 7.41E-02 0.887 Sn-11 3 255 .13 2.11 -5.70E-01 1.05E-01 2.30E+OO free 391. 70 64.97 4.36E-02 l.05E-Ol free Cs-134 475.36 1. 48 -2.62E-01 1.70E-02 3.93E+OO miss 563.25 8.34 -1. 4 6E-0 2 7.83E-01 0.896 569.33 15.37 -5.62E-02 3.73E-01 0.888 604.72 97.62 O.OOE+OO 1. 70E-0 2 0. 931 10/6/2Q*1v 12:38:31PM Page 6 of8 Analysis Report for 06-0ct-16-10009 L3-10219B-FRGS-009SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCUgrams) (pCilgrams) (pCi/grams)

Corr Cs-134 795.86 85.46 1.05E-0 2 1.70E-02 9.28E-0 2 0.933 8 01.95 8.69 1. llE-0 1 8.22E-01 0.898 1038.6 1 0.99 -5.88E-01 9.49E+OO 0.94 3 11 67.97 1. 79 2.30E+OO 6.02E+OO 1. 081 1365.19 3.02 -2.49E-01 2.14E+OO 1.128 + Cs-13 7 661.66

85.10 1.95E-01 8.12E-02 8.12E-02 miss + Eu-152 1 2 1.78 2 8.67 3.90E-0 2 1.49 E-01 2.2 0E-01 0.936 2 44.70 7.61 3.07E-02 7.90E-0 1 0.935 2 95.94 0.45 9.4'.2E+OO l.66E+O l miss 344.2 8 2 6.60 1.12E-01 2.74E-01 0.957 367.79 0.86 -1.llE+OO 4.91E+OO 0.884 4 11.12 :2. 2 4 -8.59E-02 2.81E+OO 0.908 443. 96 2.83 1.2 2E-01 2.76E+OO 0.934 488.68 0.42 1.17E+OO 8.61E+OO m i ss 563.99 0.49 -7.46E+OO 1.lOE+Ol 0.934 586.26 0.46 2.32E+OO 1. 55E+Ol 0.9 42 678. 62 0.47 -1. 52E+OO 1. 93E+Ol 0.887 688.67 0.86 6.16E-01 6.86E+OO 0.980 719.35 0.28 -7.65E-01 2.13E+01 miss 778.9 0 1 2. 96 O.OOE+OO 1.49E-01 0.945 810.45 0.32 3.43E+OO 2.22E+Ol 1. 050 867.37 4.2 6 -1.22E-01 1.98E+OO 0.92 8 919.33 0.43 -2.70E+OO 1.33E+Ol 0.981 964.0 8 14.65 2.61E-02 5.62E-01 1. 022 1085.87 10.24 -1.85E-01 7.53E-01 1. 018 1089.74 1. 73 2.51E+OO 7.2 6E+OO 0.95 2 111 2.07 13. 69 1.36E-01 7.60E-01 0.992 1212.95 1. 43 1. 03E+OO 8.25E+OO 0.929 1249.94 0.19 O.OOE+OO l.21E+Ol 1. 097 1299.14 1. 63 1. 02E+OO 7.40E+OO 0.944 1408.01 21. 07 -9.75E-02 3.59E-Ol 0.983 1 457.64 0.50 -2. 51E+Ol 2.88E+O l 1. 07 6 1 528.10 0.28 O.OOE+OO 1.02E+Ol 1.007 + E u-154 123.07 40.40 -9.94E-03 1.50E-01 1. 50E-01 0.934 247.93 6.89 4.06E-01 9.84E-01 0.928 591.76 4.95 6.19E-02 1.15E+OO 0.915 692.42 1. 78 -3 .13E-01 2.76E+OO 0.936 7 2 3.30 20.06 4.28E-02 3.18E-Ol 0.935 756.8 0 4.52 -1.33E-01

1. 4 9E+OO 0.915 873.18 12.08 1.44E-01 6.97E-01 0.93 2 996.29 1 0.48 4.80E-0 2 8.45E-01 0.971 1004.76 1 8.01 9.13E-02 4.24E-01 0.978 1274.43 34.80 1.57E-02 2.03E-01 0.981 1596.4 8 1. 80 O.OOE+OO 1. 43E+OO 1.175 + Eu-155 45.3 0 1. 31 5.57E+OO 3.16E-0 1 4.53E+Ol 0.999 6 0.01 1. 22 2.29E+OO 4.75E+Ol 1. 000 86.55 30.70 5.95E-02 3.70E-0 1 free 105.31 2 1.10 1.06E-0 1 3.16E-01 1. 000 + Tl-208 583.19 85.00 5.84E-02 l.32E-01 l.32E-01 0.932 + Bi-211 351.07

13.0 2 6.19E-01 4.12E-01 4.12E-01 miss + Pb-211 404.85 3.78 2.42E-01 1.50E+OO 1.50E+OO miss 10/6/20*1

~* 12:38:31PM Page 7 of8 Analysis Report for 06-0ct-16-10009 L3-102198-FRGS-009SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCUgrams) (pCl/grams) (pCi/grams)

Corr Pb-211 427.09 1. 76 -1.40E-01

1. 50E+OO 3.05E+OO miss 832.01 3.52 6.02E-01 2.16E+OO miss + Bi-21 2 39.86 1. 06 9.2 7E-01 1.39E+OO 4.41E+Ol 0.998 727. 33 6.67 3.15E-01 1.3 9E+OO 0.98 2 785.37 1.10 2.75E+OO 9.80E+OO 0.944 1 620.50 1. 47 7.61E-01 5.60E+OO 1. 006 + Pb-212 115 .18 0.60 1.32E+OO 1.64E-0 1 9.66E+OO miss 238.63

43.60 2.05E-01 1.64E-01 free 30 0.0 9 3.30 -1.79E-01 1.60E+OO free + Pb21 2-XR 74.82 10.28 9.08E-01 1.16E+OO 2.2 8E+OO miss 77 .11 17.10 6.3 0E-01 1.16E+OO miss 87.35 3.97 3.73E-01 2.67E+OO miss 89.78 1. 4 6 1. 89E+OO 6.14E+OO miss + Bi-21 4 609.32

45.49 1.89E-01 1.2 9E-01 1.29E-01 0.948 768.36 4.89 2.00E-01 1.74E+OO 0.94 2 806.18 1. 2 6 9.87E-0 2 5.50E+OO 0.923 934.06 3.11 -4.35E-02 2.81E+OO 0.944 1120.2 9 14.92 3.82E-01 9.72E-0 1 0.944 1155.21 1. 63 1.52E+OO 7.49E+OO 0.943 1238.12 5.83 1.31E-01 2.0lE+OO 0.944 1280.98 1. 43 1. 49E+OO 8.36E+OO 0.944 1377. 67 3.99 4.83E-01 2.2 4E+OO 1. 030 1385.3 1 0.79 1.33E+OO 9.79E+OO 0.945 1401.52 1. 33 1.14E-01 5.89E+OO 0.945 1407.99 2.39 -8.92E-01 3.28E+OO 0.945 1509.21 2 .13 -7.51E-02 3.87E+OO 0.950 1661.27 1. 05 O.OOE+OO 2.96E+OO 1.001 1729.59 2.88 1.84E-01 3.41E+OO 1.119 1764.49 15.30 7.84E-02 5.77E-01 1.001 1847.43 2.03 O.OOE+OO 1. 55E+OO 1.063 > 2 11 8.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 1 4 241.99 7.25 4.95E-01 1.51E-01 9.98E-01 1. 000 2 95.22 18.42 4.00E-0 1 4.74E-01 1. 000 351.93

35.60 2.2 6E-01 l.SlE-01 free 785.96 1. 06 3.60E+OO 9.63E+OO 1. 000 + Pb214-XR 74.8 2 5.80 l.61E+OO 2.04E+OO 4.05E+OO miss 7 7 .11 9. 70 l. llE+OO 2.04E+OO miss 87.35 2.24 6.60E-01 4.73E+OO miss 89.78 0.82 3.36E+OO l.09E+O l miss + Ra-22 6 1 86.21

3.64 1.2 4E+OO 1.61E+OO 1.61E+OO free + Ac-228 129.07 2.4 2 5.2 6E-0 1 4.lSE-01 2.50E+OO 0.944 209.2 5 3.89 1.88E-01 1. 47E+OO 0.978 270.2 4 3.46 3.94E-01 2.0lE+OO 0.955 328.0 0 2.95 4.59E-01 2.2 1E+OO 0.955 338.32 11. 2 7 2.93E-01 7.06E-01 0.992 409.46 1. 92 1.50E+OO 3.84E+OO 0.937 463.00 4.40 -2.08E-0 1 1. 24E+OO 0.933 7 94. 95 4.25 1.99E-01 1. 84E+OO 0.942 911.20 2 5.80 1.66E-01 4.15E-01 0.990 964.77 4.99 -7.99E-02 1.92E+OO 0.981 968.97 15.80 4. llE-01 9.09E-01 0.990 10/6/201 ... 12:38:31PM Page 8 of8 Analysis Report for 06-0ct-16-10009 L3-1 0219B-FRGS-009SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Corr Ac-2 2 8 1588.20 3.22 8.58E-02 4.1 5E-01 2.53E+OO 1. 00 2 + Pa-231 27.36 10.30 6.78E-01 2.14E+OO 4.99E+OO 0.998 2 83.69 1:70 5.0lE-02 2.16E+OO 1. 000 300.07 2.47 -2.40E-01 2.14E+OO 1.000 30.'.2. 65 2.20 3.88E-01 2.92E+OO 1. 000 330.06 1. 40 9.37E-01 3.77E+OO 1. 000 + Th-234 92.38 2 .13 1. 03E+OO 5.00E+OO 5.00E+OO free 92.80 2.10 8.70E-01 5.17E+OO free 112. 81 0.21 -1.12E+Ol 2.81E+Ol free + U-235 143.76 10. 96 -1.07E-01 1.02E-01 4.43E-01 free 163.33 5.08 -3.52E-01 8.92E-01 free 185.71

57.20 7.90E-0 2 1.02E-01 free 202 .11 1. 08 1.57E-01 4.55E+OO miss 205.31 5.01 -l.OlE-01 8.52E-01 free + Am-241 59.54 35.90 2.32E-01 1.69E+OO l.69E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) ..... C: :::s 60 55 50 40 35 8 30 25 1000 2000 3000 0000016047.CNF 4000 channel 5000 Live Time :300.000 sec Real Time :300.440 sec start: 1: -0.l(kev) stop : 8192:2047.0(kev)

Acq. start :Thu Oct 06 12:15:01 2016 6000 7000 8000 10/6/2016 1: 10:35PM Page 1 of7 ~pex Gamma Analysis Report for 06-0ct-16-10010 L 3-10219B-FRGS-01 OSS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold GAMMA SPECTRUM ANALYSIS : 06-0ct-16-10010

L3-10219B-FRGS-010SS

1L 130G Soil Sample 9.990E+02 grams : Default : 10/3/2016 1: 35:00PM : 10/6/2016 12:47:25PM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.4 seconds : 0.13 % : 2.80 1;::: Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description

120-8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 ,~._ )> v--J2id It Sample Number Peak Analysis Performed on Peak Analysis From Channel Peak Analysis To Channel : 16048 PEAK WITH NID REPORT 10/6/2016 12:52:27PM

120 : 8192 Tentative NID Library Peak Match Tolerance

C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM "'"'~ J ./1,, c..." , -,...,.-e-t:) \0/10 (7.oll.,o 10/6/2016 1:10:35PM Page 2 of7 Analysis Report for 06-0ct-16-10010 L3-102198-FRGS-01 OSS Peak Energy ROI No. (keV) start 1 238.50 948 -2 352.02 1403 -3 1460.57 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 1412 5851 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.51 3.09E+Ol 16.33 2.62E+Ol 1408.26 2.81E+Ol 10.93 1. 78E+00 5843.25 5.70E+Ol 15.10 O.OOE+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 0.99 1460.8 2 Bi-211 0.94 351.07 Pb-21 2 0.99 115.18 238.63 300.09 Pb-214 1. 00 241.99 295.22 351.93 785. 96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 10.66 13.02 0.60 43.60 3.30 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. Activity (pCi/grams) 7.00E+OO 1.06E+OO 2.73E-01 3.89E-01 Activity Uncertainty 1.95E+00 4.48E-01 1.51E-01 1.64E-01 Tentative Nuclide Pb-212 Pb-214 Bi-211 K-40 Caine Corr miss miss free free 10/6/2016 1:10:35PM Analysis Report for 06-0ct-16-10010 L3-10219B-FRGS-O 10SS INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? Bi-211 Pb-21 2 ? Pb-214 Nuclide Id Confidence 0.996 0.946 0.999 1. 000 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 7.00E+OO 1.06E+OO 2 ,73E-01 3.89E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 1.95E+OO 4.48E-01 1.SlE-01 1.64E-01 Page 3 of? Comments 10/6/2016 1:10:35PM Page4 of7 Analysis Report for 06-0ct-16-10010

+ + + + + + + + + L3-102198-FRGS-010SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/2016 12:52:27PM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCl/grams) (pCilgrams)

Corr K-40 1 460.8 2

1 0.66 7.00E+OO 3.33E-01 3.33E-01 miss Cr-51 320.08 9.91 8.82E-0 2 6.05E-01 6.05E-Ol free Mn-54 834.85 99.98 -1.80E-02 6.62E-02 6.62E-02 miss Co-58 81 0.76 99.45 -3.02E-03 6.G7E-0 2 6.67E-0 2 1. 000 1674.73 0.52 O.OOE+OO 7.65E+OO 1. 02 4 Co-60 1173.2 3 99.85 7.35E-03 9.50E-02 1.2 8E-01 0.947 1332.49 99.98 -1. llE-0 2 9.50E-02 0.947 Nb-94 702.65 99.81 2.04E-0 2 7.17E-02 1.0lE-01 0.944 871.09 99.89 9.74E-0 3 7 .17E-0 2 0.944 Ag-108m 79.13 6.60 -1.2 3E-0 1 7.41E-02 2.2 7E+OO miss 433.9 4 9 0.5 0 5.02E-02 1.1 3E-01 0.887 614.2 8 89.80 1.28E-02 9.83E-02 0.886 722. 94 90.8 0 6. 72E-03 7.41E-02 0.887 Sn-11 3 255.1 3 2 .11 1.02E+OO 1. 09E-01 3.07E+OO free 391.70 64.97 1. 83E-02 1.09E-01 free Cs-134 475.36 1. 48 -3.03E-0 1 9.53E-02 4.45E+OO miss 563.25 8.34 1.84E-01 8.53E-01 0.896 569.33 1 5.37 1. OlE-01 4.70E-01 0.888 604. 72 97.62 1.59E-02 9.53E-02 0.931 10/6/2016 1:10:35PM Page 5 of7 Analysis Report for 06-0ct-16-10010 L3-102198-FRGS-01 OSS Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCilgrams) (pCi/grams) (pCi!grams)

Corr Cs-134 7 95. 8 6 85.46 2.05E-02 9.53E-02 1.17E-01 0.933 801.95 8.69 O.OOE+OO 3.02E-01 0.898 1038.61 0.99 1.85E-01 1.03E+Ol 0.943 1167.97 1. 79 2.79E+OO 8.18E+OO 1.081 1365.19 3.0 2 3.67E-01 2.70E+OO 1.128 + C s-13 7 661.66 85.10 2.36E-01 2.41E-01 2.41E-01 miss + Eu-1 52 121.78 28.67 -3.02E-02 l.66E-01 2.26E-01 0.936 244.70 7.6 1 1.37E-02 8.26E-01 0.935 295.94 0.45 7.47E+OO 2.21E+Ol miss 344.2 8 26.60 l.13E-01 2.87E-01 0.957 367.79 0.86 -2.57E+OO 8.02E+OO 0.384 411.1 2 2.24 3.79E-01 3.82E+OO 0.908 443. 96 2.83 -9.08E-01 2.37E+OO 0.934 488.68 0.4 2 4.97E+OO 2.08E+Ol miss 563.99 0.49 2.99E+OO l.39E+Ol 0.934 586.2 6 0.46 -l.95E+OO l.2 0E+Ol 0.94 2 678.62 0.47 -4.64E+OO l.37E+Ol 0.887 688.67 0.86 -l.55E+OO 6.86E+OO 0.980 719.35 0.2 8 7.24E+OO 3.12E+Ol miss 778.90 12. 96 -5.80E-02 6.46E-01 0.945 8 10.45 0.32 O.OOE+OO 1.91E+Ol 1.050 867.37 4.26 -7.73E-02 1.71E+OO 0.928 919.33 0.43 O.OOE+OO 6.1 6E+OO 0.981 964.08 14.65 3.95E-01 9.29E-01 1.02 2 1085.87 10.24 -2.78E-01 7. 54E-01 1. 018 1089.74 1. 73 -7.43E-01 4.78E+OO 0.952 11 12. 07 13.69 3.42E-02 7.41E-Ol 0.992 1 212.95 1. 43 8.2 6E-02 9.33E+OO 0.929 1 2 49.94 0.19 -4.84E+OO 4.16E+Ol 1.097 1 2 99.14 1. 63 O.OOE+OO 2.12E+OO 0.944 1408.01 2 1. 07 O.OOE+OO l.66E-01 0.983 1457.64 0.50 O.OOE+OO 3.17E+Ol 1.076 1 528.10 0.2 8 4.78E+OO 3. 52E+Ol 1. 007 + Eu-154 123.07 40.40 -2.44E-02 9.40E-0 2 1. 51E-01 0. 934 247.93 6.89 -l.57E-01 9.27E-01 0.928 591.76 4.95 O.OOE+OO 4.23E-01 0.915 692.4 2 1. 78 -1.66E+OO 3.49E+OO 0.936 723.30 2 0.06 O.OOE+OO 1.17E-Ol 0.935 756.80 4.52 -1.68E-01 l.49E+OO 0.915 873.18 12.08 -1.64E-01 6.02E-01 0.932 996.29 10.48 O.OOE+OO 2.68E-01 0.971 1 004.76 18.01 O.OOE+OO 4.24E-01 0.978 1274.43 34.80 O.OOE+OO 9.40E-02 0.981 1596.48 1. 80 O.OOE+OO l.80E+OO 1.175 + Eu-155 45.30 1. 31 3.21E+Ol 3.75E-01 5.54E+Ol 0.999 60.01 1. 22 1.83E+Ol 5.24E+Ol 1. 000 86.55 3 0.70 -1.43E-0 1 3.75E-01 free 105.31 2 1.10 -9.66E-02 3.81E-01 1. 000 + Tl-208 583.19 85.00 1.15E-01 1. 72E-01 1. 72E-01 0.932 + Bi-211 351.07

13.0 2 1.06E+OO 2.66E-01 2.66E-01 miss + Pb-211 404.85 3.78 2.02E-01 1.89E+OO 1.89E+OO miss 10/6/2016 1:10:35PM Page 6 of? Analysis Report for 06-0ct-16-10010 L 3-102198-FRGS-01 OSS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr Pb-211 427.0 9 1. 76 -1.93E+OO 1. 89E+OO 2.36E+OO miss 8 32.0 1 3.5 2 1.12E+OO 3.57E+00 miss + Bi-.212 39.36 1. 06 1.76E+Ol 1.34E+OO 6.12E+O l 0.998 727. 33 6.67 2.21E-01 1. 34E+OO 0.982 785.37 1.10 1. 27E+OO 9.90E+OO 0.944 1 620.50 1. 47 O.OOE+OO 2.60E+OO 1. 006 + Pb-212 115 .18 0.60 l.17E+00 l.98E-01 1.17E+01 miss 238.63

43.60 2.73E-01 1.98E-01 free 30 0.0 9 3.30 l. llE+OO 2.54E+OO free + Pb212-XR 74.82 10.28 1.08E+OO 1.31E+OO 2.68E+OO miss 77.11 17.10 7.59E-01 1.31E+OO miss 87.35 3.97 7.97E-01 3.37E+00 miss 89.78 1. 4 6 5.70E-01 7.12E+00 miss + Bi-214 609.32 45.49 2.68E-01 3.57E-01 3.57E-01 0.948 768.36 4.89 3.66E-01 1.70E+OO 0.942 8 0 6.1 8 1. 26 2.99E+OO 8.98E+OO 0.923 934.0 6 3.11 3.2 9E-0 1 2.42E+OO 0.944 1120.2 9 14.92 -5.52E-02 5.69E-01 0.944 1155.21 1. 63 3.61E+OO 9.46E+OO 0.943 1238.12 5.83 -4.37E-01 1.96E+00 0.944 1280.98 1. 43 O.OOE+OO 2.38E+OO 0.944 1377. 67 3.99 6.lOE-01 2.83E+00 1. 030 1385. 3 1 0.79 3.12E+00 l.81E+O l 0.94 5 1401.52 1. 33 -1.44E-01 7.43E+OO 0.945 1407.99 2.39 O.OOE+OO l.52E+OO 0.945 1509.21 2 .13 O.OOE+OO 1.80E+00 0.950 1 661.27 1. 05 O.OOE+OO 3.74E+OO 1. 00 1 1729.59 2.88 O.OOE+OO 1.25E+OO 1.119 1764.49 15.30 3.96E-01 1.19E+00 1. 001 1847.43 2.03 O.OOE+OO 1.96E+OO 1. 063 > 2 118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 1 4 241.99 7.25 3. 72E-01 9.74E-02 1.0lE+OO 1. 000 295.22 18.42 9.37E-02 5.37E-01 1. 000 351. 93

35.60 3.89E-01 9.74E-02 free 785. 96 1. 06 2.70E-01 8.71E+OO 1. 000 + Pb214-XR 74.8 2 5.80 1. 91E+OO 2.3 1E+OO 4.76E+OO miss 77.1 1 9.70 1. 34E+OO 2.31E+OO miss 87.35 2.24 1.41E+OO 5.97E+00 miss 89.78 0.82 1.0lE+OO 1.27E+Ol mis s + Ra-226 186.21 3.64 5. 71E-01 2.0lE+OO 2.0lE+OO free + Ac-228 12 9.07 2.42 -5.98E-01 4.00E-01 3.05E+OO 0.944 2 0 9.2 5 3.89 -1.29E-01

1. 43E+OO 0.978 2 70.2 4 3.46 1. OOE+OO 2.29E+00 0.955 32 8.00 2.95 -1.09E-01 2.0lE+OO 0.955 338.32 11. 27 1.58E-01 7.16E-01 0.992 409.46 1. 92 -l.40E+OO 3.28E+OO 0.937 463.00 4.40 4.2 7E-01 2.0SE+OO 0.933 794.95 4.2 5 6.02E-01 2.59E+OO 0.942 911.2 0 2 5.80 9.08E-02 4.00E-01 0.990 964. 77 4.99 3.36E-02 2.1 7E+00 0.981 968. 97 15.80 5.14E-01 1. 05E+OO 0.990 10/6/2016 1:10:35PM P age 7 of7 Analysis Report for 06-0ct-16-10010 L3-102198-FRGS-01 OSS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coln c Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)

Corr Ac-22 8 1588.2 0 3.22 1.30E+OO 4.00E-01 4.66E+OO 1. 002 + P a-23 1 27.36 10.3 0 1.69E-01 2.6 7E+OO 4.74E+OO 0.998 283.69 1. 70 -1.78E+OO 3.31E+OO 1. 000 300.0 7 2.47 1.49E+OO 3.39E+OO 1.000 302.65 2.20 -1.40E+OO 2.67E+OO 1. 000 330.0 6 1. 40 6.49E-01 4.43E+OO 1. 000 + Th-234 92.38 2.1 3 9.14E-0 1 5.31E+OO 5.31E+OO free 92. 80 2.10 9.2 1E-01 5.34E+OO free 112. 81 0.2 1 2.0 9E+Ol 4.2 1E+Ol free + U-2 35 143.76 10. 96 4.67E-02 1.17E-01 5.82E-01 free 163.33 5.08 1.lBE-01 l.13E+OO free 185. 71 57.20 -1.30E-02 1.1 7E-01 free 202 .11 1. 0 8 -7.70E-01 5.SOE+OO miss 205.31 5.01 -2.69E-02 1.14E+OO free + Arn-241 59.54 35.90 -3.95E-01 1.64E+OO 1.64E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

Vl .,_, C: :::I 60 55 50 40 35 8 30 25 1000 2000 3000 0000016048.CNF 4000 channel 5000 L i ve Ti 11 e :300.000 sec Real Time :300.380 sec start: 1: -0. l(kev) stop : 8192:2047 .O(kev) Acq. start :Thu Oct 06 12:47:25 2016 6000 7000 8000 10/6/2016 2:20:18PM

~~~pex-Gamma Analysis Report for 06-0ct-16-10011 L3-10219B-FRGS-011 SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 06-0ct-16-10011

L3-10219B-FRGS-011SS

1 L 130G Soil Sample 1.269E+03 grams : Default : 10/3/2016 1:45:00PM

10/6/2016 1:56:54PM

130G 1 L Soil Sample : HTomlin : P40818B : 130G Soil : 300.0 seconds : 300.4 seconds : 0.15% : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16049 PEAK WITH NID REPORT Peak Analysis Performed on 10/6/2016 2:01 :57PM Peak Analysi s From Channel : 120 Peak Analysi s To Channel : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM Page 1 of8 Analysis Report for 06-0ct-16-10011 L3-102198-FRGS-011 SS Peak Energy ROI No. (keV) start 1 77.08 306 -2 2 38.58 949 -3 351. 73 1402 -4 608.79 2 429 -5 661.61 2 641 -6 1460.52 5836 -* M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 315 959 1412 2441 2651 5851 10/6/2016 2:20:18PM Peak NetPeak Net Area Centroid Area Uncertainty 309.39 2.43E+Ol 13 .09 954.80 3.49E+Ol 17.91 1407 .11 2.64E+Ol 12.69 2434.90 2.46E+Ol 12.54 2646.14 3.05E+Ol 12.82 5843.04 5.09E+Ol 15.17 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of8 Continuum Tentative Counts Nuclide 1. 33E+Ol Pb214-XR Pb212-XR 3.61E+Ol Pb-212 1. 32E+Ol Pb-214 Bi-211 1.2 8E+Ol Bi-214 l.lOE+Ol Cs-137 6.24E+OO K-40 Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.99 1460.82

10.66 4.92E+OO l.53E+OO miss Cs-137 1. 00 661.66

85.10 2.1 6E-0 1 9.43E-02 miss Bi-211 0.97 351.07

13. 0 2 7.86E-01 3.99E-01 miss Pb-21 2 1. 00 115.18 0.60 238.63

43.60 2.43E-01 1. 3 1E-01 free 300.09 3.30 Pb212-XR 1. 00 74.82 10.28 77.11

1 7.10 1.25E+OO 7.18E-0 1 miss 87.35 3.97 89.78 1. 46 Bi-214 0.99 609.32

45.49 3.3 2E-01 1.74E-0 1 0.948 768.36 4.89 806.18 1. 2 6 934.06 3.11 1120.29 14.92 1155. 2 1 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385.31 0.7 9 Analysis Report for 06-0ct-16-10011 L3-10219B-FRGS-011SS Nuclide Id Energy Name Confidence (keV) Bi-214 0.99 1401.52 1407.99 1509.21 1661. 27 1729.59 1764.49 1847.43 2118.51 Pb-214 0.99 241.99 295.22 351.93 785.96 Pb214-XR 1. 00 74.82 77 .11 87.35 89.78 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 1. 33 2.39 2.13 1. 0 5 2.88 15.30 2.03 1.16 7.25 18.42 35.60 1. 06 5.80 9.70 2.24 0.82 miss = Nuclide energy was not found in the coincidence library. 10/6/2016 2:20:18PM Page 3 of8 Activity Activity Colnc (pCilgrams)

Uncertainty Corr 2.87E-01 1.46E-01 free 2.20E+OO 1.28E+OO mi ss INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence (pCilgrams)

Uncertainty K-40 0.994 4.92E+OO l.53E+OO Cs-137 1.000 2.16E-01 9.43E-0 2 ? Bi-211 0.974 7.86E-01 3.99E-01 Pb-21 2 1.000 2.43E-01 1.31E-01 ? Pb212-XR 1. 000 1. 25E+OO 7.1 8E-01 Bi-214 0.993 3.32E-01 1.74E-01 ? Pb-214 0.999 2.87E-01 1.46E-01 ? Pb214-XR 1.000 2.2 0E+OO 1. 28E+OO Analysis Report for 06-0ct-16-10011 L3-102198-FRGS-011 SS ? = nuclid e i s part of an undetermined solution X = nuclid e r ejected by the interference analysis @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma 10/6/2016 2:20:18PM Page 4 of8 10/6/2016 2:20:18PM Page 5 of8 Analysis Report for 06-0ct-16-10011

+ + + + + + + + + L3-10219B-FRGS-011 SS Peak Locate Performed on Peak Locat e From Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/6/2016 2:01 :57PM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Caine Name (keV) (pCilgrams) (pCilgrams) (pCl!grams)

Corr K-40 1460.82

10.66 4.92E+OO 1.08E+OO l.08E+OO miss Cr-51 320.08 9.91 3.37E-01 7.48E-01 7.48E-01 f r ee Mn-54 834.85 99.98 1.61E-02 7.6 2E-02 7.62E-02 miss Co-58 810.76 99.45 -1.55E-02 5.25E-02 5.25E-02 1.000 1674.73 0.52 2.23E+OO 1.64E+Ol 1. 024 Co-6 0 11 73.23 99.85 4.45E-04 7.48E-02 1.0lE-01 0.947 1332.49 99.98 1.02E-0 2 7.48E-02 0.947 Nb-94 702.65 99.81 -1.70E-0 2 7.12E-02 7.16E-02 0.944 871.09 99.89 1.2 8E-0 3 7.12E-02 0.944 Ag-108m 79.13 6.60 2.3 1E-01 1.52E-02 1.56E+OO miss 433.94 90.50 O.OOE+OO 1.52E-02 0.887 614.2 8 89.80 1. 72E-02 1.08E-01 0.886 7 22.94 90.80 -1. 32E-02 7.36E-02 0.887 Sn-113 2 55 .13 2 .11 -3.51E-01 9.2 6E-02 2.66E+00 free 3 91. 70 64.97 -7.88E-03 9.2 6E-02 free Cs-134 475.36 1. 48 9. llE-01 7.50E-02 4.59E+OO miss 563.2 5 8.34 4.70E-02 8.69E-01 0.896 569.33 15.37 1.12E-01 5.23E-01 0.888 604. 72 97.62 3.12E-03 7.50E-0 2 0.931 10/6/2016 2:20: 18PM Page 6 of8 Analysis Report for 06-0ct-16-10011 L3-102198-FRGS-011 SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)

Corr Cs-134 795.86 85.46 1.07E-0 2 7.50E-02 7.95E-02 0.933 801.95 8.69 2.15E-01 9.47E-01 0.898 10 3 8.61 0.99 1.75E+OO 8. 13E+00 0.943 1167.97 1. 79 8.48E-01 4.91E+OO 1. 081 1 365.19 3.0 2 O.OOE+OO 7.81E-01 1.128 + Cs-137 661.66

85.10 2.16E-01 9.48E-02 9.48E-02 miss + Eu-152 121.78 28.67 3.36E-02 1.31E-01 2.45E-01 0.936 244.70 7.61 -1.64E-01 7.22E-01 0.935 295.94 0.45 6.08E+OO l.61E+Ol miss 344.2 8 2 6.60 -6.91E-0 2 1.39E-01 0.957 3 67.79 0.86 -9.98E-01 4.88E+OO 0.884 411.12 2.2 4 1.95E-01 3.2 0E+OO 0.908 443. 96 2.83 -2.42E-01 2.08E+OO 0.934 488.68 0.42 -2.33E-01 l.40E+Ol miss 563.99 0.49 -7.06E-01 l.41E+01 0.934 586.26 0.46 1.79E+OO 1.38E+01 0.94 2 678. 62 0.47 4.63E+OO l.92E+01 0.887 688.67 0.86 O.OOE+OO 1.99E+00 0.980 719.35 0.28 -l.90E+00 1.68E+Ol miss 778.90 12. 96 O.OOE+OO 5.90E-01 0.945 810.45 0.32 1.19E+OO 1.90E+01 1. 050 867.37 4.26 -1. 52E-01 1.34E+OO 0.928 919.33 0.43 -l.49E+OO 1.32E+Ol 0.981 964. 08 14.65 1. 27E-01 5.58E-01 1. 02 2 1085.87 10.24 1.15E-02 7.49E-01 1. 018 1089.74 1. 73 1.13E+OO 6.14E+OO 0.95 2 1112. 07 13.69 6.29E-0 2 4.63E-01 0. 9 92 1212.95 1. 43 l.46E+OO 8.2 0E+00 0.929 1 2 49.94 0.19 7.84E+OO 4.79E+01 1. 097 1299.14 1. 63 6.17E-01 4.54E+OO 0.944 1408.01 2 1. 07 O.OOE+OO 1.31E-01 0.983 1457.64 0.50 -l.82E+Ol 2.69E+Ol 1.07 6 1528.10 0.2 8 7.53E+OO 3.50E+Ol 1. 007 + Eu-154 123.07 40.40 -3.24E-02 1.54E-01 l.54E-01 0.934 247.93 6.89 -9. 72E-02 7.30E-01 0.92 8 591.76 4.95 5.94E-01 1.85E+OO 0.91 5 692.42 1. 78 9.32E-0 2 3.4oE+OO 0.93 6 723. 30 2 0.06 9.46E-03 3.67E-01 0.93 5 756.80 4.52 1.59E-01 l.17E+OO 0.915 873.18 12.08 1.02E-01 5.98E-01 0.93 2 996.29 10.48 -7.80E-02 7.2 5E-01 0.971 1004.76 18.01 1.36E-01 4.88E-01 0.978 1274.43 34.80 2.74E-02 2.0lE-01 0.981 1596.48 1. 80 5.24E-01 3.85E+OO 1.175 + Eu-155 45.30 1. 31 1. 03E+Ol 3.51E-01 4.36E+Ol 0.999 60.01 1. 22 1.14E+Ol 4.28E+01 1.000 86.55 30.70 7.55E-02 3.98E-01 free 1 05.31 2 1.10 -6. OlE-02 3.51E-01 1. 000 + Tl-208 583.19 85.00 1.38E-01 1.81E-01 l.81E-01 0.932 + Bi-211 351.07

13. 02 7.86E-01 4.45E-01 4.45E-0 1 miss + Pb-211 404.85 3.78 4.83E-01 5.39E-01 1.70E+00 miss 10/6/2016 2:20:18PM Page 7 of8 Analysis Report for 06-0ct-16-10011 L3-10219B-FRGS-011 SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCUgrams) (pCilgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 O.OOE+OO 5.39E-01 2.72E+OO miss 832.01 3.52 O.OOE+OO 5.39E-01 miss + Bi-21 2 39.86 1. 06 1.84E+OO 1. 38E+OO 4.15E+Ol 0.998 727. 33 6.67 3.34E-01 l.3 8E+OO 0.98 2 785.37 1.10 O.OOE+OO 4.77E+OO 0.944 1 620.50 1. 47 O.OOE+OO 2.05E+OO 1. 006 + Pb-2 12 115 .18 0.60 2.31E+OO 1.73E-01 l.21E+Ol miss 238.63

43.60 2.43E-01 l.73E-01 free 300.09 3.30 4.49E-01 l.85E+OO free + Pb212-XR 74.8 2 10.28 1.53E+OO 8.64E-01 2.51E+OO miss 77.11

17.10 1. 25E+OO 8.64E-01 miss 87.35 3.97 7.36E-01 2.81E+OO mis s 89.78 1. 46 -6.95E-01 5.86E+OO mis s + Bi-2 14 609.32

45.49 3.32E-01 2.02E-01 2.02E-01 0.948 768.36 4.89 -3.85E-01 l.06E+OO 0.942 806.18 1. 26 5.89E-01 4.33E+OO 0.923 934.06 3.11 5.18E-01 2.41E+OO 0.944 1120.2 9 14.92 6.2 6E-0 2 7.98E-01 0.944 1155.2 1 1. 63 4.06E-01 4.18E+OO 0.94 3 1238.12 5.83 2.14E-0 1 2.18E+OO 0.944 1280.98 1. 43 -2.96E-01 5.09E+OO 0.944 1377.67 3.99 2.40E-01 1.77E+OO 1. 030 1385. 31 0.79 O.OOE+OO 3.58E+OO 0.945 1401. 52 1. 33 7.95E-01 7.39E+OO 0.945 1407.99 2.39 O.OOE+OO 1.2 0E+OO 0.945 1509.2 1 2.13 O.OOE+OO 1. 41E+OO 0.950 1661. 2 7 1. 05 O.OOE+OO 2.94E+OO 1. 00 1 1729.59 2.88 O.OOE+OO 9.87E-01 1.119 1 764.49 15.30 8.77E-02 7.24E-01 1. 001 1847.43 2.03 O.OOE+OO 1.54E+OO 1.063 > 2 118.51 1.1 6 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 241.99 7.25 1.3 8E-01 1.63E-01 l.06E+OO 1. 000 2 95.2 2 18.42 1.95E-01 4.12E-01 1. 000 351.93

35.60 2.87E-01 l.63E-01 free 785.96 1. 06 -2.23E+OO 4.69E+OO 1. 000 + Pb214-XR 74.82 5.80 2. 71E+OO 1.52E+OO 4.44E+OO miss 77 .11

9.70 2.20E+OO 1.52E+OO mis s 87.35 2.24 1. 30E+00 4.98E+OO miss 89.78 0.82 -1.2 4E+OO 1. 04E+Ol miss + Ra-22 6 186.2 1 3.64 5.2 6E-01 1. 4 9E+OO 1. 49E+OO free + Ac-2 28 129.07 2.42 -1.74E-02 6.56E-01 2.31E+OO 0.944 2 09.2 5 3.89 2.94E-01 l.60E+OO 0.978 2 70.2 4 3.46 3.93E-01 1.49E+OO 0.955 328.00 2.95 4.12E-01 2.39E+OO 0.955 338.32 11. ~7 3.12E-01 8.13E-01 0.9 92 409.46 1. 92 4.14E-01 3.81E+OO 0.937 463.00 4.40 4.47E-01 2.16E+OO 0.93 3 794.95 4.2 5 -1.42E-01 1.25E+OO 0.942 911. 2 0 25.80 4.19E-01 6.56E-01 0.990 964.77 4.99 2.64E-02 1.47E+OO 0.981 968. 97 15.80 4.07E-01 8.30E-01 0.990 Analysis Report for 06-0ct-16-10011

+ + + + + * > L3-10219B-FRGS-011SS Nuclide Energy Yield(%) Activity Name (keV) (pCilgrams)

Ac-22 8 1588.2 0 3.22 O.OOE+OO Pa-23 1 27.36 10.30 -4.46E-01 2 83.69 1. 70 1.51E+OO 300.07 2.47 5.99E-01 302.65 2.2 0 -1.llE+OO 330.06 1. 40 2.13E-01 Th-234 92.38 2.13 3.36E+OO 92.80 2.10 4.68E+OO 112. 81 0.21 6.62E-0 1 U-2 35 143.76 10.96 1.87E-01 163.33 5.08 -2.14E-01 1 85.71 57.2 0 6.25E-02 202 .11 1. 08 3.20E-01 205.31 5.01 9.87E-02 Am-2 4 1 59.54 35.90 3.lOE-01 = Nuclide identified during the nuclide identification

= Energy line found in the spectrum = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction 10/6/2016 Nuc/ideMDA (pCi/grams) 6.56E-01 1.72E+OO 6.67E+OO 1.06E-01 1. 4 7E+OO ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 2:20:18PM Page 8 of8 LineMDA Coin c (pCi/grams)

Corr 9.23E-01 1.002 4.9 6E+OO 0.998 3.61E+OO 1. 000 2.47E+OO 1. 000 1. 72E+OO 1. 000 4.43E+OO 1.000 6.67E+OO free 6.92E+OO free 3.76E+O l free 5.67E-01 free 8.8 6E-01 free 1.06E-01 free 5.06E+OO miss 9.82E-01 free 1. 4 7E+OO free 60 55 50 45 40 1000 2000 3000 0000016049.CNF 4000 channel 5000 Live Time : 300.000 sec Real Time : 300.440 sec start: 1: -0.l(kev) stop : 8192: 2047 .O(kev) Acq. Start : Thu Oct 06 13:56:54 2016 6000 7000 8000 10/10/2016 6:59:10AM Page 1 of7 ~~~pex-Gamma Analysis Report for 10-0ct-16-10002 L3-10219B-FRGS-012SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 10-0ct-16-10002

L3-10219B-FRGS-012SS

1 L 130G Soil Sample 9.11 OE+02 grams : Default : 10/3/2016 1:50:00PM

10/10/2016 6:35:31AM

130G 1 L Soil Sample : JWelch : P11314X2 : 130G Soil : 300.0 seconds : 300.2 seconds : 0.07% : 2.80 : 120 -8192 : 120-8192 : 1.000FWHM

1/27/2016

6/28/2012

16057 PEAK WITH NID REPORT Peak Analysis Performed on 10/10/2016 6:58:36AM Peak Analysi s From Channel : 120 Peak Analysi s To Channel : 8192 Tentative NID Library Peak Match Toleranc e UA~ J~-;t9 : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM \O{fof ((,.. tq)~ I 0-1()-/tp Analysis Report for 1O-Oct-16-10002 L3-10219B-FRGS-O 12SS Peak Energy ROI No. (keV) start 1 238.55 949 -2 352.03 1403 -3 661.57 2 641 -4 1460.80 5837 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 959 1413 2650 5849 10/10/2016 6:59:10AM Peak Net Peak Net Area Centroid Area Uncertainty 954.54 3.86E+01 14.42 1407.92 2.30E+Ol 10.87 2645.10 1.76E+Ol 9.38 5842.52 3.15E+Ol 11. 71 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuciide Id Energy Yield(%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 1. 07E+Ol Pb-212 5.95E+OO Pb-214 Bi-211 4.82E+OO Cs-137 2.94E+OO K-40 Activity Caine Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 1. 00 1460.82 Cs-137 1. 00 661.66 Bi-211 0. 94 351.07 Pb-21 2 1. 00 115 .18 2 38.63 300.09 Pb-214 1. 00 241.99 295.22 351.93 785.96 * = Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. * * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

10.66 85.10 13. 02 0.60 43.60 3.30 7.2 5 1 8.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. 3.83E+00 l.46E+OO miss 1.56E-01 8.54E-02 miss 8.59E-01 4.2 9E-01 mis s 3.32E-01 1.35E-01 miss 3.1 4E-01 l.57E-01 miss 10/10/2016 6:59:10AM Analysis Report for 10-0ct-16-10002 L3-102198-FRGS-012SS INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Cs-137 ? Bi-211 Pb-212 ? Pb-214 Nuclide Id Confidence

1. 000 1. 000 0.945 1. 000 1.000 ? X = = nuclide i s part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCilgrams) 3.83E+OO l.56E-01 8.59E-0 1 3.32E-01 3.14E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty l.46E+OO 8.54E-02 4.29E-01 1. 35E-01 1.57E-01 Page 3 of7 Comments 10/10/2016 6:59:10AM Analysis Report for 1O-Oct-16-10002

+ + + + + + + + + L3-102198-FRGS-O 12SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 6:58:36AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCUgrams) (pCUgrams) (pCi/grams)

K-40 1 460.8 2 10.66 3.83E+OO 9.88E-01 9.88E-01 Cr-51 32 0.08 9.91 2.27E-01 7.67E-01 7.67E-01 Mn-54 834.85 99.98 O.OOE+OO 2.43E-02 2.43E-02 Co-58 810.76 99.45 -4.65E-0 3 6.84E-02 6.84E-02 1674.73 0.52 O.OOE+OO 8.02E+OO Co-60 1173.23 99.85 3.34E-02 3.2 7E-02 1.20E-01 1332.49 99.98 O.OOE+OO 3.27E-02 Nb-94 702.65 99.81 1. 31E-03 7.32E-02 7.32E-02 871. 09 99.89 4.55E-03 8.45E-02 Ag-108m 79.13 6.60 -2.53E-01 6.71E-0 2 1. 34E+OO 433.94 90.50 7.48E-03 6. 71E-02 614.2 8 89.80 2.64E-02 9.61E-02 722.94 90.80 2.65E-02 9.51E-02 Sn-113 255.13 2.11 -5.61E-01 9.06E-02 2.54E+OO 391. 70 64.97 -1.52E-02 9.06E-02 Cs-134 475.36 1. 48 -6.55E-01 5.39E-02 3.0lE+OO 563.25 8.34 -1.14E-01 6.0lE-01 569.33 15.37 4.46E-02 3.2 8E-01 604. 72 97.62 -1.90E-02 5.39E-02 Page 4 of7 Tolerance Nuclide Coinc Corr miss free miss miss miss miss miss miss miss miss miss miss miss free free miss miss miss miss 10/10/2016 6:59:10AM P ag e 5 of7 Analysis Report for 10-0ct-16-10002 L 3-102198-FRGS-012SS Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Coin c Name (keV) (pCUgrams) (pCl/grams) (pCi/grams)

Corr Cs-134 795.86 85.46 5.88E-03 5.3 9E-02 9.35E-02 miss 801.95 8.69 7.4:E-02 9.25E-01 miss 1038.61 0.99 5.2 1E-01 7.66E+OO miss 1167. 97 1. 79 6.21E-01 4.57E+OO miss 1365 .19 3.02 4.lOE-01 3.0lE+OO miss + Cs-137 661.66

85.10 1. 56E-01 8.55E-02 8.55E-02 miss + Eu-152 1 2 1. 78 2 8.67 -2.90E-02 1.64E-01 1.64E-01 miss 2 44.70 7.61 -5.51E-02 8.73E-01 miss 2 95. 94 0.45 9.50E+00 l.94E+Ol miss 344.28 2 6.60 3.60E-03 l.67E-01 miss 367.79 0.86 7.28E-01 7.00E+OO miss 411.12 2.2 4 -1.22E-0 2 2.92E+OO miss 443.96 2.83 5.88E-01 2.44E+OO miss 488.68 0.4 2 8.76E-Ol 1.3 6E+Ol miss 563.99 0.49 -2.76E-01 l.02E+Ol miss 586.26 0.46 O.OOE+OO 4.lOE+OO miss 678.62 0.47 2.04E+OO 1. 51E+Ol miss 688.67 0.86 -5.28E-01 8.40E+OO miss 719.3 5 0.28 O.OOE+OO 7.76E+OO miss 778.90 12. 96 6.51E-02 6.05E-01 miss 810.45 0.32 2.70E+OO l.99E+Ol miss 867.37 4.26 2 .13E-01 1. 57E+OO miss 919.33 0.43 -6.07E+OO 2.05E+Ol miss 964.08 14.65 4.33E-01 l.OOE+OO miss 1085.87 10.24 -5.89E-0 2 7 . .58E-Ol miss 1089.74 1. 73 -8.74E-02 4.50£+00 miss 1112. 07 13. 69 3.22E-01 1. 03E+OO miss 1212.95 1. 43 1.78E+OO 8.56E+OO miss 1249.34 0.1 9 O.OOE+OO 1.66E+Ol miss 1299.14 1. 63 O.OOE+OO 1. 98E+OO miss 1408.01 21.07 6.83E-02 5.55E-01 miss 1457.64 0.50 -2.31E+Ol 2.77E+Ol miss 1 528.10 0.2 8 O.OOE+OO l.29E+Ol miss + Eu-154 123.07 40.40 4.00E-02 9.1 2E-0 2 l.30E-01 miss 247.93 6.89 -3.49E-02 6.71E-01 miss 591.76 4.95 O.OOE+OO 3.83E-01 miss 692.4 2 1. 78 l.46E-01 3.23E+OO miss 723. 30 20.06 1.2 0E-01 4.31E-01 mis s 756.80 4.52 O.OOE+OO 4. 96E-01 mis s 873.18 12.08 7.55E-02 9.07E-01 miss 996.29 10.48 -1.59E-01 7.0lE-01 mi ss 1004.76 18.01 O.OOE+OO l.51E-01 miss 1 274.43 34.80 O.OOE+OO 9.12E-02 miss 1596.48 1. 80 -4.82E-01 5.68E+OO miss + Eu-155 45.3 0 1. 31 4.02E+OO 3.33E-01 l.87E+Ol miss 60.01 1. 22 -3.55E-01 1.93E+O l miss 86.55 30.70 l.36E-01 3.49E-01 mi ss 105.31 2 1.10 6.79E-02 3.33E-01 mi ss + Tl-208 583.19 85.00 6.67E-02 1.3 6E-01 l.36E-01 miss + Bi-211 351.07

13.02 8.59E-01 4.15E-01 4.15E-01 miss + Pb-211 404.85 3.78 4.49E-01 6.78E-0 1 1.86E+OO miss 10/1012016 6:59:10AM Page 6 of7 Analysis Report for 1O-Oct-16-10002 L3-102198-FRGS-012SS Nuclide Energy Yield(%) Activity NuclldeMDA LlneMDA Coinc Name (keV) (pCi!grams) (pCl!grams) (pCl!grams)

Corr Pb-211 427.09 1. 76 -2.54E-01 6.78E-01 2. 33E+OO miss 832.0 1 3.52 O.OOE+OO 6.78E-01 miss + Bi-212 39.86 1. 06 -3.71E+OO 1. 81E+OO 2. 04E+Ol miss 727. 33 6.67 5.58E-01 1.81E+OO m i ss 785. 37 1.10 O.OOE+OO 2. 08E+OO miss 1 62 0.50 1. 47 O.OOE+OO 2. 58E+OO miss + Pb-212 115.18 0.60 3. llE+OO l.27E-01 9.86E+OO miss 2 38.63

43.60 3.32E-01 1.2 7E-01 miss 3 00.0 9 3.30 2.78E-01 1.74E+00 miss + Pb21 2-XR 74.82 10.2 8 1.19E+OO 9.48E-01 1. 68E+OO miss 77.11 17.10 6.21E-01 9.48E-01 miss 87.35 3.97 4.65E-01 2.41E+OO miss 89.78 1. 46 1.19E+OO 4.69E+OO miss + Bi-2 1 4 609.32 45.49 1. 96E-01 3.52E-01 3.52E-01 miss 768.36 4.89 O.OOE+OO 4. 62E-01 miss 8 0 6.18 1. 2 6 3.60E+OO 9.63E+OO miss 934.0 6 3 .11 9.22E-01 3.31E+OO miss 1 120.29 14.92 5.87E-01 1.26E+OO miss 11 55.2 1 1. 63 7.68E-01 7.24E+OO miss 1238.12 5.83 6.47E-01 2.37E+OO miss 1 280.98 1. 43 7.02E-Ol 7.61E+OO miss 1377. 67 3.99 3.99E-01 2.88E+OO miss 1 3 85.3 1 0.79 1.57E+OO 1.15E+Ol m i ss 1401. 52 1. 33 O.OOE+OO 2.55E+OO miss 1407.99 2.39 6.00E-01 4.88E+OO miss 1509.2 1 2.13 1. 25E+OO 5.'78E+OO miss 1661.2 7 1. 05 O.OOE+OO 3.69E+OO miss 1 729.59 2.88 5.12E-01 3. 77E+OO miss 1764.49 15.30 3.91E-01 l.17E+OO miss 1847.43 2.03 7.61E-01 5.60E+OO miss > 2118. 51 1.16 O.OOE+OO O.OOE+OO miss + Pb-2 14 24 1.99 7.2 5 2.17E-01 l.52E-01 9.09E-01 miss 295.22 18.42 2.94E-01 5.00E-01 miss 351.93

35.60 3.14E-01 1. 52E-01 miss 785.96 1. 06 O.OOE+OO 2.17E+OO miss + Pb214-XR 74.82 5.80 2.lOE+OO l.67E+OO 2.98E+OO miss 77 .11 9.70 1.09E+OO 1.67E+OO miss 87.35 2.24 8.23E-01 4.2 7E+OO miss 89.78 0.82 2.12E+OO 8.35E+OO miss + Ra-226 186.2 1 3.64 1.2 1E+O O 1.81E+OO 1. 81E+OO miss + Ac-228 129.07 2.42 6.18E-01 6.67E-01 2.26E+OO miss 209.25 3.89 2.76E-01 1.35E+OO miss 270.24 3.46 4.41E-01 2.1 3E+OO miss 328.00 2.95 5.llE-01 1.89E+OO miss 338.3 2 11. 27 2.44E-01 8.18E-01 miss 409.46 1. 92 -l.83E-01 3.39E+OO miss 463.00 4.40 -8.05E-02 9.87E-01 miss 794.95 4.25 2.51E-01 l.87E+OO mi ss 911. 20 2 5.80 4.48E-01 7.54E-01 miss 964. 77 4.99 1.2 1E+OO 3.lOE+OO miss 968.97 15.80 1.lOE-01 6.67E-01 miss 10/10/2016 6:59:10AM Page 7 of7 Analysis Report for 1O-Oct-16-10002 L3-10219B-FRGS-012SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Corr Ac-228 1588.2 0 3.22 O.OOE+OO 6.6 7 E-01 l .16E+OO miss + Pa-231 27.3 6 10.30 O.OOE+OO 4.04E-01 4.04E-01 miss 283.69 1. 70 4.33E-01 3.2 4E+OO miss 300.07 2.47 3. 71E-Ol ~.32E+OO miss 302.65 2.2 0 -6.74E-01 1. 85E+OO miss 330.06 1. 40 -8.31E-01 2.45E+OO miss + Th-234 92.38 2.13 1.60E+OO 4.57E+OO 4.57E+OO miss 92.80 2.1 0 3.25E+OO 5.12E+OO miss 11 2. 81 0.21 1.25E+Ol 3.47E+Ol miss + U-235 143.76 10. 96 6.59E-0 2 1.08E-01 3.52E-01 miss 163.33 5.0 8 3.2 2E-01 1.05E+OO miss 185.71 57.2 0 4.30E-02 l.08E-Ol miss 2 02 .11 1. 08 -6.75E-01 4.48E+OO miss 2 05.31 5.0 1 -1.73E-02 9.05E-01 miss + Am-241 59.54 35.90 1.26E-01 7. llE-0 1 7. llE-01 miss + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

V) s:::: :::::, 60 55 50 45 40 35 8 30 25 I 1000 2000 3000 0000016057.CNF 4000 channel 5000 Live Time :300.000 sec Real Time :300.200 sec start: 1: -0.2(kev)

Stop : 8192: 2047. 4(kev) Acq. Start : Mon Oct 10 06: 35: 31 2016 6000. 7000 8000 Analysis Report for 1 O-Oct-16-10004 L3-10219B-FRGS-013SS 10/10/2016 7:41:04AM GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number Peak Analysis Performed on Peak Analysis From Channel Peak Analysis To Channel : 10-0ct-16-10004

L3-10219B-FRGS-013SS

1 L 130G Soil Sample 1.161E+03 grams : Default : 10/3/2016 2:05:00PM

10/10/2016 7:17:49AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.17 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16059 PEAK WITH NID REPORT 10/10/2016 7:22:52AM

120 : 8192 Tentative NID Library : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB Peak Match Toler~ : 1.000FWHM .t~~ 'l .v--,c:,po l \" ~()/' Page 1 of7 Analysis Report for 1O-Oct-16-10004 L3-10219B-FRGS-013SS Peak Energy ROI No. (keV) start 1 238.37 950 -2 609.2 7 2 432 -3 1460.57 5834 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end* 961 2441 5851 10/10/2016 7:41:04AM Peak Net Peak Net Area Centroid Area Uncertainty 953.99 2.84E+Ol 16.71 2436.83 1.59E+Ol 9.42 5843.26 5.92E+Ol 16.51 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page 2 of7 Continuum Tentative Counts Nuclide 3 .13E+Ol Pb-212 6. llE+OO Bi-214 7.63E+OO K-40 Activity Coinc Name Confidence (keV) (pCi/grams)

Uncertainty Corr K-40 0.99 1460.82

10.66 6.2 6E+OO 1.83E+OO miss Pb-212 0.99 115 .18 0.60 23 8.63

43.60 2.15E-01 1. 32E-01 free 300.09 3.30 Bi-214 1. 00 609.32

45.49 2.35E-01 1.42E-01 0.948 768.36 4.89 806.18 1. 26 934.06 3.11 1120.29 14.92 1155.21 1. 63 1 23 8.12 5.83 1280.98 1. 43 1377. 67 3.39 1385.31 0.79 1401..52 1. 33 1407.99 2.39 1509.2 1 2.13 1661. 2 7 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.1 6 Analysis Report for 10-0ct-16-10004 L3-10219B-FRGS-013SS

= Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 10/10/2016 7:41:04AM INTERFERENCE CORRECTED REPORT ? = X = Nuclide Name K-40 Pb-212 Bi-214 Nuclide Id Confidence

0. 996 0. 996 1. 000 nuclide is part of an undetermined solution nuclide rejected by the interference analysis Wt mean Activity (pCl/grams) 6.26E+OO 2.15E-01 2.35E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty l.83E+OO 1.32E-01 1. 42E-01 Page 3 of7 Comments 10/10/2016 7:41:04AM Page 4 of7 Analysis Report for 1 O-Oct-16-10004

+ + + + + + + + + L3-10219B-FRGS-013SS Peak Locate Performed on Peak Locate From Channel Peak Locat e To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 7:22:52AM

120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (ke\lJ (pCi/grams) (pCilgrams) (pCl!grsms)

Corr K-40 1460.82 1* 10.6 6 6.26E+OO 1.33E+OO l.33E+00 miss Cr-51 320.08 9.91 -8.34E-02 6.2 5E-01 6.2 5E-01 free Mn-54 834.85 99.98 O.OOE+OO 2. llE-02 2. llE-02 miss Co-58 810.76 99.45 8.09E-0 3 5. 96E-02 5. 96E-02 1. 000 1674.73 0.52 O.OOE+OO 6.83E+OO 1. 024 Co-60 1173.2 3 99.85 -2.92E-0 3 7.53E-0 2 7.53E-02 0.947 13 32.49 99.98 l. llE-02 8.19E-02 0.947 Nb-94 702.65 99.81 6.05E-03 2.2 7E-02 5.35E-0 2 0.944 871. 09 99.89 O.OOE+OO 2.27E-02 0.944 Ag-108m 79.13 6.60 -7.20E-01 7.2 9E-02 1. 96E+OO miss 433.94 90.50 2.45E-03 7.36E-02 0.887 614.28 89.80 -l.lOE-0 2 7.2 9E-02 0.88 6 7 22.94 90.80 5.78E-0 3 1. 04E-01 0.887 Sn-113 2 55.13 2.11 l.2 8E+OO l.43E-01 3.21E+OO free 391.70 64. 97 4.2 6E-02 l.43E-01 free C s-13 4 475.36 1. 48 -1. 36E+OO 7.37E-02 2.62E+OO miss 563.25 8.34 -6.82E-01 5.84E-01 0.896 569.33 15.37 5.83E-02 4. 71E-01 0.88 8 604. 72 97.62 -4.56E-03 7.3 7E-02 0.931 10/10/2016 7:41:04AM Page 5 of7 Analysis Report for 1O-Oct-16-10004 L 3-10219B-FRGS-013SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV} (pCilgrams) (pCi/grams) (pCl/grams)

Corr Cs-134 795.86 85.46 -1.57E-03 7.37E-02 8. 72E-02 0.93 3 80 1.95 8.69 1.93E-01 8.96E-01 0.898 1 038.61 0.99 4.80E+OO l.26E+Ol 0.943 1167.97 1. 79 l.43E-0 1 5.39E+OO 1.081 1 365.19 3.0 2 O.OOE+OO 8.57E-01 1.128 + Cs-137 661.66 85.10 1.53E-01 1.93E-01 l.93E-01 miss + Eu-15 2 12 1. 78 2 8.67 -9.00E-0 2 1.62E-O l 1.94E-01 0.936 2 44.70 7.61 8.42E-02 7.89E-01 0.935 295.94 0.45 7.57E+OO l.81E+Ol miss 344.2 8 2 6.60 1.60E-02 2.47E-01 0.957 367.79 0.86 -9.58E-01 6.19E+OO 0.884 411.12 2.24 5.60E-01 3.29E+OO 0.908 443. 96 2.83 -l.51E-01 2.2 7E+00 0.934 488.68 0.4 2 -1.44E+OO l.3 7E+O l miss 563.99 0.49 -8.2 3E+OO 1.1 9E+Ol 0.934 586.2 6 0.46 O.OOE+OO 3. 78E+OO 0.94 2 6 7 8.62 0.47 8.00E-01 l.18E+Ol 0.887 688.67 0.86 l.38E+00 8.64E+OO 0.980 719.35 0.2 8 4.16E-01 2.32E+Ol miss 778.90 12.96 O.OOE+OO l.62E-01 0.945 810.45 0.32 2.24E+OO l.65E+Ol 1.050 867.37 4.26 4.33E-01 2.40E+OO 0.928 919.33 0.43 O.OOE+OO 5.30E+00 0.981 964. 0 8 14.65 -1.64E-01 6.lOE-01 1.022 1 0 85.87 10.24 l.7 6E-01 8.19E-01 1.018 10 89.74 1. 73 2.35E+OO 7.33E+OO 0.952 ll 12.07 13. 69 -1.96E-02 5.06E-0 1 0.992 1212.95 1. 43 -6.40E-01 5.49E+OO 0.929 1249.94 0.19 6.95E+OO 5.84E+Ol 1.097 1299.14 1. 63 O.OOE+OO 1.83E+00 0.944 1 408.01 21. 07 1. llE-01 5.70E-01 0.983 1 457.64 0.50 -2.65E+Ol 3.30E+Ol 1. 076 1 528.10 0.2 8 O.OOE+OO l. llE+Ol 1. 007 + Eu-154 123.07 40.40 -l.45E-02 l.SlE-01 1.51E-01 0.934 247.93 6.89 5.42E-01 l .13E+OO 0.928 591.76 4.95 -2.69E-02 1.25E+OO 0.915 692.4 2 1. 78 -4.76E-01 3.00E+OO 0.936 723.30 2 0.06 -l.61E-02 4.88E-01 0.935 756.80 4.52 O.OOE+OO 4.71E-01 0.915 873.18 12.08 2.02E-01 9.23E-01 0.932 996.29 10.48 -7.llE-02 7.93E-01 0.971 1004.76 18.01 -8.27E-02 3.65E-01 0.978 1274.43 34.80 -2.14E-0 2 2.20E-01 0.981 1 596.48 1. 80 O.OOE+OO l.55E+OO 1.175 + Eu-155 45.3 0 1. 31 2.32E+Ol 4.20E-01 4.77E+Ol 0.999 60.01 1.2 2 l.57E+Ol 4.34E+Ol 1. 000 86.55 30.70 2.18E-01 4.2 5E-01 free 105.31 21.10 1.60E-01 4.20E-01 1. 000 + Tl-208 583.19 85.00 1. llE-01 1.62E-01 1. 62E-01 0.93 2 + Bi-211 351.07 13.02 5.17E-01 8.59E-01 8.59E*-Ol miss + Pb-2 11 404.85 3.78 -6.82E-0 2 l.49E+OO 1.49E+00 miss 10/10/2016 7:41:04AM Page 6 of7 Analysis Report for 10-0ct-16-10004 L3-102198-FRGS-013SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 1.66E-01 1.49E+OO 2. 97E+OO mis s 83 2.01 3.5 2 3.63E-0 2 l.60E+OO miss + Bi-212 39.86 1. 06 2.07E+Ol 1. 28E+OO 5.26E+Ol 0.998 727. 33 6.67 -2.3 6E-01 l.28E+OO 0.9 82 785. 37 1.10 6.50E-01 6.58E+OO 0.944 1620.50 1. 47 8.2 6E-01 6.08E+OO 1.006 + Pb-2 12 115 .18 0.60 2.2 6E-01 1.81E-01 l.13E+Ol miss 238.63 *.1; 43.60 2.15E-01 l.81E-01 free 300.09 3.30 8.27E-01 l.84E+OO free + Pb21 2-XR 74.8 2 10.28 6.29E-01 1.35E+OO 2.31E+OO miss 77 .11 17.10 8.99E-0 1 1.35E+OO mi ss 87.35 3.97 4.80E-01 2.99E+OO miss 89.78 1. 46 -1.94E+OO 6.41E+OO miss + Bi-214 609.32

45.49 2.35E-01 1.57E-0 1 1.57E-Ol 0.948 768.36 4.89 4.86E-01 l.89E+OO 0.94 2 806.18 1. 26 6.43E-01 4.73E+OO 0.92 3 934.06 3.11 3.54E-01 3.40E+OO 0.944 1120.29 14. 92 1.43E-01 7.99E-01 0.944 1155.21 1. 63 -1.68E+00 4.57E+OO 0.94 3 1238.12 5.83 -3. llE-01 l.6 9E+OO 0.944 128 0.98 1. 43 -6.48E-01 5.56E+OO 0.944 1377.67 3.99 O.OOE+OO 7.lOE-01 1.030 1385. 31 0.79 O.OOE+OO 3.91E+OO 0.945 1401.52 1. 33 1. 49E+O O 8.07E+OO 0.945 1407.99 2.39 1.02E+O O 5.22E+OO 0.945 1509.21 2.13 -4.90E-01 4.20E+OO 0.950 1 661.27 1. 0 5 4.46E-01 8.75E+OO 1. 001 1729.59 2.88 3.99E-0 1 2.93E+OO 1.119 1764.49 15.30 5.llE-01 l.20E+OO 1.001 1847.43 2.03 6.24E-01 4.59E+OO 1. 063 > 2118. 5 1 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 1 4 2 4 1. 99 7.25 8.30E-01 3.46E-01 l.18E+OO 1. 000 295.22 18.42 2.99E-01 4.84E-01 1. 000 351. 93 35.60 3.45E-0 1 3.46E-01 free 785.96 1. 06 -5.80E-01 5.12E+OO 1. 000 + Pb214-XR 74.8 2 5.80 1. llE+OO 2.3 7E+OO 4.09E+OO miss 77 .11 9.70 1.59E+OO 2.37E+OO miss 87.35 2.2 4 8.51E-01 5.2 9E+OO miss 89.78 0.82 -3.45E+OO l.14E+Ol miss + Ra-226 1 86.2 1 3.64 7.51E-0 1 1.95E+OO l.95E+OO free + Ac-228 129.07 2.42 1. 2 4E+OO 3.84E-01 3.21E+OO 0.944 209.25 3.89 -6.82E-03 1.36E+OO 0.97 8 27 0.2 4 3.46 1.05E+OO 2.25E+OO 0.95 5 32 8.00 2.95 1.98E-01 2.40E+OO 0.95 5 33 8.32 11. 2 7 3.08E-01 6.96E-01 0.99 2 409.46 1. 92 -5.25E-02 3.15E+OO 0.937 463.00 4.40 O.OOE+OO l.64E+OO 0.933 794.95 4.25 1. 39E-01 2.23E+OO 0.94 2 911. 20 2 5.80 9.46E-02 3.84E-01 0.990 964. 77 4.99 -6.17E-01 l.87E+OO 0.981 968. 97 15.80 4.53E-02 6.54E-01 0.990 10/10/2016 7:41:04AM Page 7 of7 Analysis Report for 1 0-0ct-16-10004 L3-102198-FRGS-013SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCilgrams)

Corr Ac-228 1588.20 3.22 O.OOE+OO 3.84E-01 1.0lE+OO 1.002 + Pa-231 27.36 10.30 -1.58E+OO 2.lOE+OO 4.94E+OO 0.998 283.69 1. 70 -1.39E+OO 2.6 1E+OO 1. 000 300.07 2.47 1. llE+OO 2.46E+OO 1. 000 302.65 2.20 1.2 0E-01 2.lOE+OO 1. 000 330.06 1. 40 -5.33E-01 4.lOE+OO 1. 000 + Th-234 92.38 2.13 2.07E+OO 5.92E+OO 6.23E+OO free 92. 80 2.10 1. 40E-01 5.92E+OO free 112.81 0.2 1 -1.14E+Ol 3.74E+Ol free + U-235 143.76 10.96 -1.66E-01

1. 21E-01 3.62E-01 free 163.33 5.08 -2.32E-01 1.0lE+OO free 185.71 57.20 6.22E-0 2 1.21E-01 free 202 .11 1. 08 -1.77E-01 4.94E+OO miss 205.31 5.01 2.07E-01 1.24E+OO free + Am-241 59.54 35.90 2.88E-Ol 1.41E+OO l.41E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library.

60 55 50 45--40 35 VI ...... C: 8 30 25 20 ,...., ' ..c a.. 1000 2000 3000 0000016059.CNF 4000 channel 5000 Live Time :300.000 sec Real Ti~e :300.510 sec start: 1: -0. l(kev) Stop : 8192: 2047 .O(kev) Acq. start :Mon oct 10 07: 17:49 2016 6000 7000 8000 10/10/2016 8:05:37AM Analysis Report for 10-0ct-16-10006 L3-10219B-FRGS-014SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels}

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency Calibration Description Sample Number : 1 O-Oct-16-10006

L3-10219B-FRGS-014SS

1 L 130G Soil Sample 1.086E+03 grams : Default : 10/3/2016 2:15:00PM

10/10/2016 7:42:15AM

130G 1 L Soil Sample : JWelch : P40818B : 130G S oil : 300.0 s econds : 300.5 seconds : 0.15 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM : 1/27/2016

1/5/2015 : 16061 PEAK WITH NID REPORT Peak Analysis Performed on 10/10/2016 7:47:22AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM l'Ca, ... ,, \. Page 1 of7 10/10/2016 8:05:37AM Page 2 of7 Analysis Report for 10-0ct-16-10006 L3-10219B-FRGS-O 14SS Peak Energy ROI No. (keV) start 1 238.57 949 -2 351. 96 1 404 -3 1460.58 5836 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 961 1413 5851 Peak Net Peak Net Area Continuum Centroid Area Uncertainty Counts 954.77 2.82E+Ol 16.47 2. 96E+Ol 1408.0 2 1.62E+Ol 10.18 9.54E+OO 5843.27 5.lOE+Ol 14.86 4.04E+OO NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) K-40 0.99 1460.82 Bi-211 0.95 351.07 Pb-212 1. 00 115 .18 238.63 300.09 Pb-214 1. 00 241. 99 295.22 351.93 785. 96 * = Energy line found in the spectrum. -= Manually added nuclide. ? = Manually edited nuclide. * * * * @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

Yield(%) 10.66 13. 02 0.60 43.60 3.30 7.25 18.42 35.60 1. 06 miss = Nuclide energy was not found in the coincidence library. Activity (pCi/grams) 5.76E+OO 5.65E-01 2.2 9E-01 2.07E-01 Activity Uncertainty 1.75E+OO 3.66E-01 l.39E-01 1.34E-01 Tentative Nuclide Pb-2 12 Pb-214 Bi-211 K-40 Coinc Corr miss miss free free 10/10/2016 8:05:37AM Analysis Report for 1O-Oct-16-10006 L3-102198-FRGS-014SS INTERFERENCE CORRECTED REPORT Nuclide Name K-40 ? Bi-211 Pb-21 2 ? Pb-214 Nuclide Id Confidence

0. 996 0.953 1. 000 1. 000 ? = nuclid e is part of an undetermined solution X = nuclid e rejected by the interference analysis Wt mean Activity (pCilgrams) 5.76E+OO 5.65E-01 2.29E-01 2.07E-01 @ = nuclid e contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty 1.75E+OO 3.66E-01 1.39E-01 1.34E-01 Page 3 of7 Comments 10/10/2016 8:05:37AM Analysis Report for 1 O-Oct-16-10006 L3-10219B-FRGS-014SS Peak Locate Performed on Peak Locate From Channel Peak Loca te To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 7:47: 22AM : 120 : 8192 Peak CPS {°A,) Peak Size (CPS) Uncertainty Peak Type NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (keV) (pCilgrams) (pCUgrams) (pCilgrams)

+ K-40 1460.8 2

10.6 6 5.76E+OO 1.0"7E+OO l.07E+OO + Cr-51 320.08 9.91 -3.82E-0 2 7.18E-01 7.18E-01 + Mn-54 834.85 99.98 O.OOE+OO 2.2 6E-02 2.2 6E-02 Page 4 of7 Tolerance Nuclide Colnc Corr miss f r ee miss + Co-58 810.76 99.45 -7.2 1E-0 3 6.37E-02 6.3 7E-02 1.000 1 674.73 0.52 O.OOE+OO 7.30E+OO 1. 024 + Co-60 1173.23 99.85 O.OOE+OO 2.96E-02 2. 96E-02 0.947 1332.49 99.98 2.38E-02 l.lOE-01 0.947 + Nb-94 702.65 99.81 -2.07E-02 5. 72E-02 5.72E-02 0.944 8 71. 09 99.89 1.49E-03 8.32E-02 0.944 + Ag-108m 79.1 3 6.60 -9.69E-0 1 4.82E-02 2.09E+OO miss 433.94 90.50 -3.93E-03 4.82E-02 0.887 614.28 89.80 -1.0lE-02 7.80E-02 0.88 6 72 2. 94 90.80 1. OOE-02 8.61E-02 0.887 + Sn-113 2 55 .13 2 .11 -5.93E-01 7.29E-02 2.89E+OO free 391. 70 64.97 -1.33E-02 7.29E-02 free + Cs-134 475.36 1. 48 1.33E+OO 5.39E-02 4.58E+OO miss 563.25 8.34 2.12E-01 1. 02E+OO 0.896 569.33 15.37 -1. 31E-01 3.44E-01 0.888 604. 72 97.62 -7.32E-03 5.39E-02 0.931 10/10/2016 8:05:37AM Page 5 of7 Analysis Report for 1 O-Oct-16-10006 L3-102198-FRGS-O 14SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCilgrams) (pCi!grams)

Corr Cs-134 795.86 85.46 3.90E-03 5.3 9E-02 l.08E-01 0.933 801.95 8.69 1.80E-01 9.57E-01 0.898 1 038.61 0.99 O.OOE+OO 2.78E+OO 0.943 1167.97 1. 79 7.65E-0 2 4.97E+OO 1.081 1365.1 9 3.0 2 O.OOE+OO 9.16E-01 1.128 + Cs-137 661.66 85.10 1.93E-01 2. llE-01 2.llE-01 miss + Eu-152 121. 78 2 8.67 l.02E-01 1.2 9E-01 2.63E-01 0.936 244.70 7.6 1 1. 27E-01 8.03E-01 0.935 295.94 0.45 -1.53E+O O l.64E+Ol miss 344.2 8 2 6.60 -1.40E-0'2 l.29E-01 0.957 367.79 0.86 1.47E+OO 7.38E+OO 0.884 411.12 2.24 -3.99E-0 1 2.3 2E+OO 0.908 443. 96 2.83 6.88E-01 2.65E+OO 0.934 488.68 0.42 -1.36E-01 l.2 6E+Ol miss 563.99 0.49 l.19E+OO 1.48E+Ol 0.934 586.26 0.46 -7.77E+OO l.61E+Ol 0.94 2 678.62 0.47 O.OOE+OO 4.63E+OO 0.88 7 688.67 0.86 1.00E+OO 7.97E+OO 0.980 719.35 0.2 8 5.33E+OO 2.48E+Ol miss 778.90 12. 96 7.48E-02 5.95E-01 0.945 8 10.45 0.32 -1.20E+OO 1.76E+Ol 1.050 867.37 4.26 -1.78E-01 l.57E+OO 0.92 8 919.33 0.43 4.19E+OO l.95E+Ol 0.981 964.08 14.65 8.76E-02 6.52E-01 1. 022 1085.87 10.24 1.35E-02 8.75E-01 1. 018 10 89.74 1. 73 -2.48E+OO 4.4 0E+OO 0.952 11 12.07 1 3.69 7.3 5E-0 2 7.91E-01 0.992 1 2 12.95 1. 43 -4.56E-01 5.87E+00 0.929 1249.94 0.19 8.54E+00 4.83E+Ol 1.097 1299.14 1. 63 O.OOE+OO l.95E+OO 0.944 1408.01 21. 07 O.OOE+OO 1. 53E-01 0.98 3 1457.64 0.50 -2.35E+Ol 2.92E+Ol 1. 076 1528.10 0.28 4.40E+OO 3.24E+O l 1. 007 + E u-1 54 123.07 40.40 -6.0lE-0 2 1.44E-01 l.47E-01 0.934 247.93 6.89 1.85E-0 1 9.90E-01 0.928 591. 7 6 4.95 -3.2 6E-0 1 1.55E+OO 0.915 692.4 2 1. 78 O.OOE+OO l.18E+OO 0.936 723. 3 0 20.06 -1.99E-02 3.70E-01 0.93 5 756.8 0 4.52 1.55E-01 1.73E+OO 0.915 873.1 8 12.08 1.25E-02 6.99E-01 0.93 2 996.2 9 10.48 O.OOE+OO 2.47E-01 0.971 1004.7 6 18.01 O.OOE+OO 1.44E-01 0.978 1274.43 34.8 0 1.83E-02 2.35E-01 0.981 1596.48 1. 8 0 O.OOE+OO l.66E+OO 1.175 + Eu-15 5 45.30 1. 3 1 6.5 1E+OO 3.51E-01 4.75E+Ol 0.999 6 0.01 1. 2 2 -6.88E+OO 4.22E+Ol 1. 000 86.55 30.70 5.26E-02 4.30E-01 free 105.31 21.10 -2.32E-01 3.51E-01 1. 000 + Tl-208 583.19 85.00 l.12E-01 1.83E-01 l.83E-01 0.932 + Bi-211 351.07

13.02 5.65E-01 4.50E-01 4.50E-01 mi ss + Pb-2 11 404.85 3. 78 -5.74E-02 1.87E+OO 1. 87E+OO miss 10/10/2016 8:05:37AM Page 6 of7 Analysis Report for 10-0ct-16-10006 L3-10219B-FRGS-014SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Pb-211 427.09 1. 76 1.53E+OO 1.87E+OO 4.16E+OO mis s 832.01 3.52 9.31E-01 2.80E+OO mis s + Bi-2 12 39.86 1. 06 2.2 6E+Ol 1. 23E+OO 6.08E+Ol 0.998 727. 33 6.67 -3.05E-01 1.23E+OO 0.982 785.37 1.10 7.58E-01 5.58E+OO 0.944 1620.50 1. 47 O.OOE+OO 2. 39E+OO 1. 006 + Pb-21 2 115 .18 0.60 1.13E+OO 1. 90E-0 1 1.30E+Ol miss 238.63

43.60 2.29E-01 l.90E-01 free 300.09 3.30 3.52E-01 2.34E+OO free + Pb212-XR 74.B2 10.28 9.2 0E-01 1.20E+OO 2.34E+OO miss 77 .11 17.10 1.40E-01 l.20E+OO miss 87.35 3.97 8.56E-03 3.46E+OO miss 89.78 1. 46 1. llE+OO 7. 91E+OO miss + Bi-21 4 609.32 45.49 2.00E-01 3.00E-0 1 3.00E-01 0.948 768.36 4.89 1. 05E+OO 2. 81E+OO 0.942 806.18 1. 2 6 1.89E+OO 8.2 6E+OO 0.923 93 4.06 3.11 6.06E-01 2.81E+OO 0.944 11 2 0.2 9 14. 9 2 1.52E-0 1 8.54E-01 0.944 1155.2 1 1. 63 -5.69E-01 4.88E+OO 0.94 3 12 3 8.12 5.83 9.71E-01 2.55E+OO 0.944 1280.98 1. 43 1.15E-01 5.95E+OO 0.944 1377.67 3.99 4.0lE-02 2.60E+OO 1.030 1385.31 0.79 O.OOE+OO 4.1 8E+OO 0.94 5 1401.52 1. 33 1.13E+00 8.63E+OO 0.94 5 1407.99 2.39 O.OOE+OO 1.40E+OO 0.945 1509.2 1 2 .13 6. llE-01 4.49E+OO 0.950 1 66 1.27 1. 05 2.54E+OO 1.18E+Ol 1.001 1729.59 2.88 O.OOE+OO l.15E+OO 1.119 1764.49 15.30 2.67E-01 l.09E+OO 1.001 1847.43 2.03 O.OOE+OO l.81E+OO 1.0 63 > 2118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-2 14 2 41.99 7.2 5 6.36E-01 l.65E-01 l.05E+OO 1.000 2 95. 22 18.42 1. 7 6E-01 4.82E-01 1.000 351.93

35.60 2.07E-01 l.65E-01 free 785.96 1. 06 7.44E-01 5.48E+OO 1. 000 + Pb214-XR 74.82 5.80 1.63E+OO 2.12E+OO 4.14E+OO mis s 77 .11 9.70 2.46E-0 1 2.12E+OO mis s 87.35 2.24 1. 52E-02 6.13E+OO mis s 89.78 0.82 1.98E+00 1.41E+Ol miss + Ra-226 186.2 1 3. 64 6.0lE-01 1.85E+OO 1.85E+OO free + Ac-228 129.0 7 2.42 9.63E-02 5.95E-01 2.81E+OO 0.944 209.2 5 3.89 -3.28E-02 1.52E+OO 0.978 270.24 3.46 6.15E-01 2.02E+OO 0.955 328.00 2.9 5 4. 31E-02 2.02E+OO 0.955 338.32 11. 27 2.85E-01 7.70E-01 0.992 409.46 1. 92 1.12E-01 3.37E+OO 0.937 463.00 4.40 3.86E-01 2.0lE+OO 0.933 794.95 4.25 6.62E-02 2.14E+OO 0.942 911.2 0 2 5.80 3.02E-01 5.95E-01 0.990 964.77 4.99 2.16E-01 2.00E+OO 0.981 968.97 15.80 3.63E-01 8.74E-01 0.990 10/10/2016 8:05:37AM Page 7 of7 Analysis Report for 10-0ct-16-1 0006 L3-102198-FRGS-014SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCilgrams)

Corr Ac-22 8 1588.20 3.22 1.99E-01 5.95E-01 2. 93E+OO 1.00 2 + Pa-231 27.36 10.30 -9.98E-01 2.25E+OO 4. 99E+OO 0.998 2 83.69 1. 70 1. 57E+OO 3.87E+OO 1.000 300.07 2.47 4.70E-01 3.12E+OO 1. 000 30~.65 2.2 0 -3.2 8E-01 2.25E+OO 1. 000 330.06 1. 40 -2.61E-01 4.07E+OO 1. 000 + Th-234 92.38 2 .13 -1.46E+OO 5.44E+OO 5.44E+OO fre e 92.80 2.10 7.34E-01 6.13E+OO fre e 112. 8 1 0.21 -3.13E+OO 4.16E+Ol fre e + U-235 143.76 10. 96 l.48E-02 l.14E-01 5.3 6E-01 fre e 163.33 5.08 5.97E-03 l.21E+OO fre e 185.71 57.2 0 2.95E-02 1.14E-01 free 202 .11 1. 08 1.14E+OO 4.56E+OO miss 205.31 5.01 8.24E-02 l.15E+OO free + .Am-24 1 59.54 35.90 -1. 2 6E-01 l.50E+OO 1.50E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required. miss = Nuclide energy was not found in the coincidence library.

V) c:: ::::s 60 55 50 40 35 8 30 25 20 15 ...... ' ..c ,w~~h lL 1000 2000 3000 0000016061.

CNF 4000 channel 5000 Live Time 300.000 sec Real Time 300.450 sec start: 1 -0.l(kev) Stop : 8192 2047 .O(kev) Acq. start Mon act 10 07: 42: 15 2016 6000 7000 8000 10/10/2016 6:58:30AM Page 1 of7 ~~~pex-Gamma Analysis Report for 10-0ct-16-10001 L3-10219B-FQGS-O 12SS GAMMA SPECTRUM ANALYSIS Sample Identification Sample Description Sample Type Unit Sample Point Sample Size Facility Sample Taken On Acquisition Started Procedure Operator Detector Name Geometry Live Time Real Time Dead Time Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels)

Identification Energy Tolerance Energy Calibration Used Done On Efficiency Calibration U sed Done On Efficiency Calibration Description Sample Number Peak Analysis Performed on Peak Analys is From Channel Peak Analys is To Channel : 10-0ct-16-10001

L3-10219B-FQGS-012SS

1 L 130G Soil Sample 8. 790E+02 grams : Default : 10/3/2016 1: 50:00PM : 10/10/2016 6:35:08AM

130G 1 L Soil Sample : JWelch : P40818B : 130G Soil : 300.0 seconds : 300.5 seconds : 0.18 % : 2.80 : 120 -8192 : 120 -8192 : 1.000FWHM

1/27/2016

1/5/2015 : 16056 PEAK WITH NID REPORT 10/10/2016 6:40:15AM

120 : 8192 Tentative NID Library Peak Match Toleran ce : C:\Canberra\Apex\Root\Default\Library\Zion Lib-BNL.NLB

1.000FWHM

,...""\ . I . -f,~ '.Jlrrl" V{!fr, 101,0/1(.

lt)~ /0-/0-/(fJ Analysis Report for 10-0ct-16-10001 L3-102198-FQGS-01255 Peak Energy ROI No. (keV) start 1 238.63 950 -2 609.11 2 432 -3 661. 54 2 641 -4 1460.39 5836 -M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma ROI end 960 2441 2651 5848 10/10/2016 6:58:30AM Peak Net Peak NetArea Centroid Area Uncertainty 955.00 3.24E+Ol 16.72 2 436.19 2.lOE+Ol 10.01 2 645.87 2.62E+Ol 10.90 5842.5 3 3.50E+Ol 11. 8 3 NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Page2 of7 Continuum Tentative Counts Nuclide 3 .13E+Ol Pb-212 4.00E+OO Bi-214 3.67E+OO Cs-137 O.OOE+OO K-40 Activity Coinc Name Confidence (keV) (pCilgrams)

Uncertainty Corr K-40 0.98 1460.82

10.66 4.89E+00 1.71E+OO miss C s-1 37 0.99 661.66

85.10 2.67E-01 l.16E-01 miss Pb-212 1. 00 115 .18 0.60 238.63

43.60 3.25E-01 1.76E-01 free 300.09 3.30 Bi-2 14 0.99 609.32

45.49 4.09E-01 2.0lE-01 0.948 768.36 4.89 806.18 1. 2 6 934.06 3 .11 1120.2 9 14.92 1155.21 1. 63 1238.12 5.83 1280.98 1. 43 1377.67 3.99 1385. 31 0.79 1401. 52 1. 33 1407.99 2.39 1509.21 2 .13 1661. 27 1. 05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2 118.51 1.16 Analysis Report for 10-0ct-16-10001 L3-10219B-FQGS-012SS

= Energy line found in the spectrum.

-= Manually added nuclide. ? = Manually edited nuclide. @ = Energy line not used for Weighted Mean Activity Energy Tolerance

1.000FWHM Nuclide confidence index threshold

= 0.30 Errors quoted at 2.000sigma Coincidence correction performed.

free = No coincidence correction required.

miss = Nuclide energy was not found in the coincidence library. 10/10/2016 6:58:30AM INTERFERENCE CORRECTED REPORT Nuclide Name K-40 Cs-137 Pb-21 2 Bi-214 Nuclide Id Confidence 0.989 0.999 1.000 0.999 ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis Wt mean Activity (pCi/grams) 4.89E+OO 2. 67E-01" 3.25E-01 4.09E-01 @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma Wt mean Activity Uncertainty l.71E+OO l.16E-01 l.76E-01 2. OlE-01 Page 3 of7 Comments 10/10/2016 6:58:30AM Page4 of7 Analysis Report for 10-0ct-16-10001

+ + + + + + + + + L3-10219B-FQGS-012SS Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak No. Energy (keV) All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma UNIDENTIFIED PEAKS : 10/10/2016 6:40: 15AM : 120 : 8192 Peak CPS(%) Peak Size (CPS) Uncertainty Peak Type Tolerance Nuclide NUCLIDE*MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCl/grams) (pCilgrams) (pCi!grams)

Corr K-40 1460.82

10.66 4.89E+OO 3.78E-01 3.78E-01 miss Cr-51 320.08 9.9 1 -1.2 6E-01 8.87E-01 8.87E-01 free Mn-54 834.85 99.98 1.72E-02 9.57E-0 2 9.57E-02 miss Co-58 810.76 99.45 2.56E-02 1.40E-01 l.40E-01 1.000 1674.73 0.5 2 O.OOE+OO 9.02E+OO 1. 024 Co-60 1173.2 3 99.85 1.93E-03 3.98E-02 1.2 6E-01 0.947 13 32.49 99.98 O.OOE+OO 3.98E-02 0.947 Nb-94 702.65 99.81 O.OOE+OO 2.60E-02 2.60E-02 0.944 871.09 99.89 2. 2 1E-02 1.03E-01 0.944 Ag-108m 79.13 6.60 -4.88E-01 7.51E-02 2.73E+OO miss 433.94 90.50 -7.2 8E-03 7.51E-02 0.887 614.28 89.80 1.14E-02 9.64E-02 0.88 6 722.94 90.80 -7.63E-03 1.2 3E-01 0.887 Sn-113 255 .13 2.11 3.00E-01 1.37E-01 3.75E+OO free 3 91. 70 64.97 2.33E-02 1.37E-01 free Cs-1 34 475.36 1. 48 1.24E+OO 9.13E-02 7.07E+OO miss 563.25 8.34 1.47E-01 9.73E-01 0.896 569.33 15.37 6.93E-02 5.36E-01 0.888 604. 72 97.62 1.41E-02 1.19E-01 0.931 10/10/2016 6:58:30AM Page 5 of7 Analysis Report for 10-0ct-16-10001 L 3-102198-FQGS-012SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coinc Name (keV) (pCi!grams) (pCUgrams) (pCilgrams)

Corr Cs-134 795.86 85.46 l.24E-02 9 .13E-02 9.13E-02 0.933 801.95 8.69 2.76E-01 1.37E+OO 0.898 1038.61 0.99 4.23E-01 l.18E+Ol 0.943 1167.97 1. 79 -6.61E-01 4.87E+OO 1. 081 1365.19 3.0 2 O.OOE+OO l.13E+OO 1.128 + Cs-137 661.66

85.10 2.67E-01 9. 07E.,-02 9.07E-02 mis s + Eu-152 121.78 28.67 -8.19E-02 1.89 E-01 2.57E-01 0.936 244.70 7.61 -1.99E-02 l.13E+OO 0.935 295.94 0.45 4.2 0E+OO 2.32E+Ol miss 344.2 8 2 6.60 -4.56E-0 2 2.61E-01 0.957 367.79 0.86 O.OOE+OO 2.05E+OO 0.884 411.12 2.2 4 2.22E-01 4.04E+OO 0.908 443.96 2.83 6.00E-01 3.52E+OO 0.934 488.68 0.4 2 -l.34E+OO l.2 4E+O l miss 563.99 0.49 1. 02E+OO 1.2 5E+Ol 0.934 586.26 0.46 -4.43E+00

1. 72E+Ol 0.9 42 678.62 0.47 O.OOE+OO 5.72E+OO 0.887 688.67 0.86 7.07E-01 7.80E+OO 0.980 719.35 0.28 9.2 0E+OO 3.96E+Ol miss 778. 90 12.96 O.OOE+OO 2.1 4E-01 0.945 810.45 0.3 2 -6.90E+OO 3.1 8E+Ol 1.050 867.37 4.26 7.91E-01 2.84E+OO 0.92 8 919.33 0.43 -1. 29E+OO l.90E+Ol 0.98 1 964.08 14.65 3.74E-02 6.95E-01 1. 02 2 1085.87 10.24 -8.32E-02 8.57E-01 1.018 1089.74 1. 73 -5.28E-01 9.69E+OO 0.952 1112.07 1 3.69 7.78E-0 2 6.68E-01 0.992 1212.95 1. 43 2. 96E+OO l.06E+Ol 0. 929 1249.94 0.19 O.OOE+OO 1.74E+Ol 1. 097 1299.14 1. 63 O.OOE+OO 2.41E+OO 0.944 1408.01 21. 07 O.OOE+OO l.89E-01 0.983 1457.64 0.50 O.OOE+OO 2.55E+Ol 1. 076 1528.1 0 0.28 O.OOE+OO 1.47E+Ol 1. 00 7 + Eu-154 123.0 7 40.40 2.57E-02 2.07E-01 2.07E-01 0.934 247.93 6.89 2.63E-02 9.90E-01 0.928 591. 7 6 4.95 4.03E-01 1.91E+OO 0.915 692.42 1. 78 O.OOE+OO 1.46E+OO 0.936 7 2 3.30 20.0 6 6.56E-0 2 5.91E-01 0.935 756.8 0 4.5 2 O.OOE+OO 2.14E+OO 0.915 873.1 8 12.08 O.OOE+OO 2.52E-01 0.93 2 996.29 10.48 O.OOE+OO 3.05E-01 0. 971 1004.76 18.0 1 7.65E-02 7.06E-01 0.978 1274.43 34.80 7.06E-02 3.67E-01 0.981 1596.48 1. 80 O.OOE+OO 2.05E+OO 1.175 + Eu-155 45.30 1. 31 l.65E+Ol 4.13E-0 1 6.30E+Ol 0.999 60.01 1. 22 1.77E+Ol 5.97E+Ol 1. 000 86.55 30.70 2.04E-01 5.16E-01 free 105.31 21.10 -2.38E-0 1 4 .13E-01 1. 000 + Tl-208 583.19 85.00 6.94E-02 1.60E-01 1.60E-01 0.932 + Bi-211 351.07 13.02 4.2 6E-01 9.8"'E-01 9.87E-01 mi ss + Pb-211 404.85 3.78 3.2 7E-01 2.12E+OO 2.15E+OO mi ss 10/10/2016 6:58:30AM Page 6 of7 Analysis Report for 10-0ct-16-10001 L3-10219B-FQGS-012SS Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Coinc Name (keV) (pCi/grams) (pCUgrams) (pCi/grams)

Corr Pb-211 427.09 1. 76 -2.55E-01 2.1 2E+OO 3.39E+OO miss 832.01 3.5 2 -l.44E-01 2.12E+OO miss + Bi-212 39.86 1. 06 -4.32E+OO 1.70E+OO 6.33E+Ol 0.998 727. 33 6.67 4.71E-02 l.70E+OO 0.982 785. 37 1.10 1.09E+OO 1.0lE+Ol 0.944 1620.50 1. 47 1.09E+00 8.03E+OO 1. 006 + Pb-212 115 .18 0.60 l.49E-01 2.29E-01 l.26E+Ol miss 238.63

43.60 3.25E-01 2.2 9E-01 free 300.09 3.30 2.85E-01 2.30E+OO free + Pb212-XR 74.82 10.28 8.64E-01 l.53E+OO 2.43E+OO miss 77 .11 17.10 4.1 9E-01. 1.53E+OO miss 87.3 5 3.97 2.54E-01 3. 71E+OO miss 89.78 1. 46 1.77E+OO 9.46E+OO miss + Bi-2 14 609.32

45.49 4.09E-01 1.77E-01 1.77E-01 0.948 768.36 4.89 5.78E-02 2.24E+OO 0.94 2 806.18 1. 26 2.55E+OO 9.15E+OO 0.923 934.06 3.11 -3.1.2E-01 2.75E+OO 0.944 1120.29 14.9 2 4.39E-01 l.15E+OO 0.944 1155.21 1. 63 -1.17E-01 6.03E+OO 0.943 1238.12 5.83 7.46E-01 2.88E+OO 0.944 1280.98 1. 43 -9.2 7E-01 9.27E+OO 0.944 1377. 67 3.99 6.93E-01 3.73E+OO 1. 030 1385.31 0.79 O.OOE+OO 5.17E+OO 0.945 1401.52 1. 33 O.OOE+OO 3.llE+OO 0.945 1407.99 2.39 O.OOE+OO 1.73E+OO 0.945 1509.2 1 2.13 7.55E-01 5.55E+OO 0.950 1661.27 1. 05 O.OOE+OO 4.25E+OO 1. 001 1729.59 2.88 O.OOE+OO 1.43E+OO 1.119 1764.49 15.30 1.78E-01 l.2 1E+OO 1. 001 1847.43 2.03 O.OOE+OO 2.2 3E+OO 1.063 > 2118.51 1.16 O.OOE+OO O.OOE+OO 1. 041 + Pb-214 2 41. 99 7.25 5.29E-01 4.37E-01 1. 40E+OO 1. 000 2 95.22 18.42 1. 96E-01 5.63E-01 1. 000 351.93 35.60 4.05E-01 4.37E-01 free 785.96 1. 06 1.79E+OO 9.90E+OO 1. 000 + Pb214-XR 74.82 5.80 1. 53E+OO 2.70E+OO 4.30E+OO miss 77.11 9.70 7.39E-01 2.70E+OO miss 87.35 2.24 4.50E-01 6.57E+OO miss 89.78 0.82 3.15E+OO 1.69E+Ol miss + Ra-226 186.2 1 3.64 1.65E+OO 2.57E+OO 2.57E+OO free + Ac-228 129.07 2.42 -7.70E-01 6.64E-01 2.77E+OO 0.944 209.25 3.89 5.2 6E-01 1. 96E+OO 0.978 270.24 3.46 -4.30E-01 2.39E+OO 0.955 328.00 2.95 -3.61E-01 2.28E+OO 0.955 338.3 2 11. 27 3.52E-01 8.14E-01 0.992 409.46 1. 92 -5.55E-01 3.2.2E+OO 0.937 463.00 4.40 8.2 7E-01 2.17E+OO 0.933 794.95 4.25 O.OOE+OO 6.64E-01 0.942 911. 20 2 5.80 3.71E-O l 7.35E-01 0.990 964.77 4.99 -1. 91.E-Ol l.69E+OO 0.981 968.97 15.80 1.56E-01 8.63E-01 0.990 10/10/2016 6:58:30AM Page 7 of7 Analysis Report for 10-0ct-16-10001 L3-10219B-FQGS-012SS Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Coin c Name (keV) (pCl/grams) (pCilgrams) (pCi/grams)

Corr Ac-228 1588.20 3.22 4.92E-01 6.64 E-01 3.62E+OO 1. 002 + Pa-231 27.36 10.30 3.84E-01 2.15E+OO 7.16E+OO 0.998 283.69 1. 70 -1.lOE+OO 3.45E+OO 1. 000 300.07 2.47 3.BOE-01 3.08E+OO 1. 000 302.65 2.2 0 -6.94E-01 2.15E+OO 1. 000 330.06 1.40 -2.69E+OO 4.61E+OO 1. 000 + Th-234 92.3 8 2 .13 2.60E+OO 7.99E+OO 7.99E+OO free 92.80 2.10 3.97E+OO 8.2 8E+OO free 11 2. 81 0.2 1 5.38E+OO 4.93E+Ol free + U-235 143.76 10.96 -1.48E-01 1.41E-01 6.87E-01 f r ee 163.33 5.08 2.97E-01 1.39E+OO free 185. 71 57.2 0 3.85E-02 1.41E-01 free 202 .11 1. 08 1.81E+OO 6.25E+OO miss 205.31 5.01 2.62E-01 1.22E+OO free + Am-241 59.54 35.90 1. llE+OO 2.28E+OO 2.28E+OO free + = Nuclide identified during the nuclide identification

= Energy line found in the spectrum > = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level Coincidence correction performed.

free = No coincidence correction required. miss = Nuclide energy was not found in the coincidence library.

V) .µ C 60 55 50 45 40 35 8 30 25 "' ...... "' ' ..c CL 1000 2000 3000 0000016056.CNF 4000 channel 5000 Live Time : 300.000 sec Real Time : 300. 540 sec start: 1: -0.l(kev) stop : 8192:2047.0(kev)

Acq. start :Mon oct 10 06:35:08 2016 6000 7000 8000

Printed: 6/12/2018 3:23 PMPage 1 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a m pleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnits17-03011-01LCSKNOWN03/03/17 00:003/3/20173/14/201717-030 11Nickel-63ASTM 3500-Ni Modified1.51E+034.52E+01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.52E+039.33E+009.01E+012.11E+00pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.58E+001.27E+001.27E+002.11E+00UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.19E+001.39E+001.39E+002.29E+00UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.71E+001.37E+001.37E+002.28E+00UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified3.46E+001.39E+001.40E+002.25E+00pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.88E-011.36E+001.36E+002.31E+00UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified-1.69E+001.65E+001.65E+002.90E+00UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified6.89E-011.40E+001.40E+002.37E+00UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified8.22E-011.30E+001.30E+002.20E+00UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified1.06E+001.27E+001.27E+002.13E+00UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified3.84E+001.40E+001.42E+002.25E+00pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/14/201717-03011Nickel-63ASTM 3500-Ni Modified2.34E+001.48E+001.49E+002.44E+00UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.97E+001.36E+001.37E+002.26E+00UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.09E+001.42E+001.42E+002.39E+00UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified9.12E-011.44E+001.44E+002.44E+00UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/15/201717-03011Nickel-63ASTM 3500-Ni Modified1.02E+011.52E+001.64E+002.24E+00pCi/g17-03011-01LCSKNOWN03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.43E+013.04E-01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.16E+011.65E+002.15E+018.24E-01pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified-2.14E-024.23E-014.23E-019.04E-01UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified7.78E-013.45E-014.39E-016.48E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.42E-013.48E-013.96E-016.83E-01UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.59E-013.59E-013.81E-017.29E-01UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.97E-013.66E-013.91E-017.40E-01UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.85E-014.17E-014.64E-018.27E-01UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.39E-023.97E-013.98E-018.41E-01UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified9.84E-013.37E-014.80E-016.09E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified4.59E-013.45E-013.80E-016.86E-01UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified6.36E-013.86E-014.45E-017.54E-01UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified8.09E-014.19E-015.05E-018.12E-01UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified7.29E-013.98E-014.72E-017.75E-01UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified3.09E-013.90E-014.04E-018.00E-01UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified1.03E-013.61E-013.62E-017.59E-01UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/27/201717-03011Strontium-90EIChroM SRW01 Modified5.03E-013.78E-014.17E-017.53E-01UpCi/gZion, IL 60099Work Order Details:67149817-03011SOENVI RONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh BlvdCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:23 PMPage 2 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a m pleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-01LCSKNOWN03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified6.21E+012.48E+00pCi/g17-03011-01LCSKNOWN03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified3.94E+011.58E+00pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified7.58E+015.03E+006.36E+006.59E-01pCi/g17-03011-01LCSSPIKE03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.44E+014.02E+004.62E+006.97E-01pCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.74E-024.81E-024.82E-028.85E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified1.72E-022.56E-022.57E-024.39E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.29E-021.46E-021.46E-022.73E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-1.28E-041.27E-021.27E-021.91E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.40E-031.48E-021.48E-022.34E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.37E-011.68E-011.69E-013.28E-01UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Lead-212LANL ER-130 Modified6.28E-031.70E-021.70E-022.64E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Lead-214LANL ER-130 Modified-3.01E-032.42E-022.42E-023.65E-02UpCi/g17-03011-02MBLBLANK03/03/17 00:003/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified-5.23E-034.16E-024.16E-026.34E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.11E-011.33E-011.34E-012.02E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.84E-011.17E-011.19E-011.04E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-2.54E-033.32E-023.32E-024.18E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified2.64E-041.18E-021.18E-024.72E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified5.75E-024.30E-024.31E-027.05E-02UpCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.01E+011.11E+001.23E+004.65E-01pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified4.00E-015.25E-025.64E-028.50E-02pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.90E-011.31E-011.33E-019.32E-02pCi/g17-03011-03DUPL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.46E-016.92E-027.04E-025.39E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.23E-011.04E-011.06E-012.03E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.66E-011.11E-011.13E-018.49E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified4.50E-043.33E-023.33E-023.46E-02UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-5.96E-031.09E-021.09E-024.15E-02UpCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.04E-023.06E-023.08E-024.76E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified1.02E+011.13E+001.24E+005.53E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.75E-015.11E-025.46E-028.70E-02pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified4.00E-011.33E-011.35E-011.11E-01pCi/g17-03011-04DOL310212AFRGS002SS-A05/11/16 10:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified1.86E-016.47E-026.54E-026.95E-02pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:23 PMPage 3 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a m pleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.95E-016.68E-026.98E-022.26E-01pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.88E-016.28E-026.59E-028.04E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.89E-022.04E-022.04E-022.86E-02UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-3.06E-031.04E-021.04E-022.78E-02UpCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.11E-016.15E-026.50E-023.88E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified6.85E+008.02E-018.76E-012.60E-01pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.45E-015.27E-025.56E-024.16E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.73E-016.08E-026.37E-027.27E-02pCi/g17-03011-05TRGL310213AFRGS008SS-A04/14/16 08:003/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.93E-017.55E-027.82E-026.80E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.14E-011.00E-011.02E-011.05E-01pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.82E-017.07E-027.34E-027.96E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified2.05E-031.95E-021.95E-022.33E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified4.00E-036.34E-036.34E-032.49E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified2.25E-022.00E-022.01E-023.30E-02UpCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified8.06E+001.03E+001.11E+004.94E-01pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.61E-011.24E-011.26E-016.77E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.73E-011.30E-011.31E-016.84E-02pCi/g17-03011-06TRGL310219AFRGS006SS-A10/03/16 09:103/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.87E-017.16E-027.31E-025.18E-02pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.85E-011.06E-011.07E-012.08E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.30E-019.29E-029.55E-021.27E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.61E-039.25E-039.25E-035.27E-02UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified8.33E-031.55E-021.55E-024.39E-02UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.93E-011.06E-011.12E-016.05E-02pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified4.65E+007.78E-018.14E-015.30E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.59E-025.32E-025.33E-021.04E-01UpCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.45E-018.88E-029.05E-021.15E-01pCi/g17-03011-07TRGL310219BFRGS004SS-A09/27/16 08:253/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.39E-018.59E-028.67E-021.47E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:23 PMPage 4 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a m pleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.93E-011.05E-011.06E-012.39E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.41E-016.34E-026.57E-021.35E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-3.32E-024.28E-024.28E-025.98E-02UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified6.49E-032.04E-022.04E-024.57E-02UpCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified4.03E-017.19E-027.49E-028.51E-02pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified8.03E+001.20E+001.27E+006.92E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.68E-015.53E-025.84E-021.09E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified2.92E-016.40E-026.57E-021.03E-01pCi/g17-03011-08TRGL310220CRFGS002SS-A05/23/16 14:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified4.27E-011.02E-011.04E-011.72E-01pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.67E-011.03E-011.03E-017.51E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.06E-016.14E-026.33E-026.49E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.29E-021.47E-021.47E-021.62E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified1.85E-035.88E-035.88E-032.29E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified5.77E-031.18E-021.18E-021.84E-02UpCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified4.97E+006.50E-016.98E-013.09E-01pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Lead-212LANL ER-130 Modified2.92E-019.35E-029.47E-025.97E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.26E-011.09E-011.11E-015.08E-02pCi/g17-03011-09TRGL310223AFRGS004SS-A04/25/16 13:153/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.49E-016.26E-026.39E-026.96E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.56E-018.81E-029.11E-021.90E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.52E-011.14E-011.16E-017.67E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-1.95E-032.38E-022.38E-022.96E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-2.43E-031.04E-021.04E-023.39E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified1.68E-021.97E-021.97E-023.18E-02UpCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified5.89E+007.05E-017.67E-014.46E-01pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.13E-015.35E-025.96E-028.50E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Lead-214LANL ER-130 Modified4.53E-011.30E-011.32E-016.76E-02pCi/g17-03011-10TRGL310224AFRGS004SS-A06/02/16 12:403/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.20E-016.85E-027.04E-023.88E-02pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:23 PMPage 5 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a m pleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified3.10E-011.38E-011.39E-012.87E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified2.90E-018.05E-028.19E-021.08E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified-1.08E-024.50E-024.50E-025.74E-02UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified7.65E-031.58E-021.58E-024.69E-02UpCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified3.28E-016.71E-026.92E-028.42E-02pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified9.77E+001.40E+001.49E+006.37E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.17E-015.43E-025.66E-029.23E-02pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.38E-017.09E-027.30E-021.13E-01pCi/g17-03011-11TRGL310301AFRGS003SS-A06/14/16 13:273/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.08E-011.13E-011.14E-011.65E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified4.28E-018.53E-028.80E-021.50E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified3.40E-017.01E-027.22E-029.44E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified1.84E-022.40E-022.40E-023.33E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified-2.32E-022.89E-022.89E-023.14E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified2.81E-022.43E-022.43E-023.95E-02UpCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified7.18E+008.97E-019.70E-015.24E-01pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Lead-212LANL ER-130 Modified5.13E-017.92E-028.35E-026.71E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.46E-015.95E-026.21E-027.38E-02pCi/g17-03011-12TRGL310212AFJGS019SS-A05/16/16 10:453/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified3.96E-018.55E-028.78E-021.12E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Actinium-228LANL ER-130 Modified2.89E-011.08E-011.09E-011.71E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Bismuth-214LANL ER-130 Modified4.18E-018.65E-028.91E-027.83E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cobalt-60LANL ER-130 Modified6.19E-032.06E-022.06E-022.63E-02UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cesium-134LANL ER-130 Modified6.73E-031.17E-021.17E-022.91E-02UpCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Cesium-137LANL ER-130 Modified6.84E-022.08E-022.11E-023.89E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Potassium-40LANL ER-130 Modified7.14E+009.28E-019.97E-014.26E-01pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Lead-212LANL ER-130 Modified3.24E-011.13E-011.15E-019.05E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Lead-214LANL ER-130 Modified3.61E-011.29E-011.30E-015.38E-02pCi/g17-03011-13TRGL310219AFRJS019SS-A09/27/16 12:303/3/20173/6/201717-03011Thallium-208LANL ER-130 Modified2.52E-017.63E-027.74E-021.17E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:23 PMPage 6 of 6SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a m pleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-03011SOENVIRONMENTALFinal Report of AnalysisReport To:Patricia Giza Z i o n Solutions101 Shiloh Blvd17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified2.73E-019.62E-029.72E-021.03E-01pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.99E-016.02E-026.21E-026.14E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified2.51E-021.55E-021.56E-022.24E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified-5.07E-039.42E-039.43E-032.76E-02UpCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified3.38E-014.02E-024.38E-023.33E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.77E+008.72E-019.39E-013.88E-01pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Lead-212LANL ER-130 Modified3.17E-011.10E-011.11E-016.70E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Lead-214LANL ER-130 Modified2.31E-018.83E-028.91E-025.75E-02pCi/g17-03011-14TRGL310220CFRGS009SS-A05/02/16 14:003/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified3.12E-017.53E-027.70E-025.09E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified3.28E-015.75E-025.99E-021.19E-01pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.77E-015.55E-025.72E-027.49E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified2.22E-031.65E-021.65E-022.20E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified2.87E-036.84E-036.84E-031.89E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified2.03E-021.30E-021.30E-022.04E-02UpCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.22E+006.92E-017.62E-012.36E-01pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Lead-212LANL ER-130 Modified2.87E-014.16E-024.42E-024.20E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Lead-214LANL ER-130 Modified2.66E-014.22E-024.44E-024.27E-02pCi/g17-03011-15TRGL310224AFRGS012SS-A06/02/16 14:163/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified2.87E-015.58E-025.77E-024.54E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Actinium-228LANL ER-130 Modified3.84E-011.09E-011.11E-012.05E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Bismuth-214LANL ER-130 Modified2.85E-019.70E-029.81E-021.05E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cobalt-60LANL ER-130 Modified8.55E-033.20E-023.20E-025.09E-02UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cesium-134LANL ER-130 Modified1.76E-031.48E-021.48E-024.53E-02UpCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Cesium-137LANL ER-130 Modified3.37E-016.23E-026.46E-027.54E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Potassium-40LANL ER-130 Modified6.05E+008.31E-018.87E-015.71E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Lead-212LANL ER-130 Modified4.33E-015.83E-026.23E-028.32E-02pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Lead-214LANL ER-130 Modified3.29E-011.49E-011.50E-011.23E-01pCi/g17-03011-16TRGL310301AFIGS017SS-A06/14/16 13:403/3/20173/7/201717-03011Thallium-208LANL ER-130 Modified2.56E-018.59E-028.69E-021.05E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank; DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:24 PMPage 1 of 2SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a m pleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnits17-10053-01LCSKNOWN10/11/17 00:0010/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified1.35E+025.27E+00pCi/g17-10053-01LCSKNOWN10/11/17 00:0010/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified8.44E+013.38E+00pCi/g17-10053-01LCSSPIKE10/11/17 00:0010/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified1.30E+027.87E+001.03E+019.20E-01pCi/g17-10053-01LCSSPIKE10/11/17 00:0010/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified8.23E+011.01E+011.09E+011.58E+00pCi/g17-10053-02MBLBLANK10/11/17 00:0010/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified1.49E-021.43E-021.43E-022.53E-02UpCi/g17-10053-02MBLBLANK10/11/17 00:0010/11/201710/13/201717-10053Cesium-134EPA 901.1 Modified1.20E-049.67E-039.67E-032.25E-02UpCi/g17-10053-02MBLBLANK10/11/17 00:0010/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified3.18E-031.51E-021.51E-022.46E-02UpCi/g17-10053-02MBLBLANK10/11/17 00:0010/11/201710/13/201717-10053Potassium-40EPA 901.1 Modified8.01E-021.97E-011.97E-013.19E-01UpCi/g17-10053-03DUPL310213AFRGS006SSB04/13/16 13:1510/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified3.20E-024.42E-024.42E-025.93E-02UpCi/g17-10053-03DUPL310213AFRGS006SSB04/13/16 13:1510/11/201710/13/201717-10053Cesium-134EPA 901.1 Modified-7.97E-012.03E-012.07E-018.98E-02UpCi/g17-10053-03DUPL310213AFRGS006SSB04/13/16 13:1510/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified3.32E-017.60E-027.79E-029.44E-02pCi/g17-10053-03DUPL310213AFRGS006SSB04/13/16 13:1510/11/201710/13/201717-10053Potassium-40EPA 901.1 Modified1.40E+011.57E+001.73E+007.85E-01pCi/g17-10053-04DOL310213AFRGS006SSB04/13/16 13:1510/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified4.93E-024.81E-024.82E-025.54E-02UpCi/g17-10053-04DOL310213AFRGS006SSB04/13/16 13:1510/11/201710/13/201717-10053Cesium-134EPA 901.1 Modified1.42E-023.07E-023.07E-029.48E-02UpCi/g17-10053-04DOL310213AFRGS006SSB04/13/16 13:1510/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified3.42E-017.70E-027.89E-029.48E-02pCi/g17-10053-04DOL310213AFRGS006SSB04/13/16 13:1510/11/201710/13/201717-10053Potassium-40EPA 901.1 Modified1.37E+011.67E+001.81E+001.20E+00pCi/g17-10053-05TRGL310219BFRGS007SSA09/27/16 10:0510/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified-2.85E-032.42E-022.42E-023.05E-02UpCi/g17-10053-05TRGL310219BFRGS007SSA09/27/16 10:0510/11/201710/13/201717-10053Cesium-134EPA 901.1 Modified-2.56E-031.67E-021.67E-023.83E-02UpCi/g17-10053-05TRGL310219BFRGS007SSA09/27/16 10:0510/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified2.13E-022.21E-022.22E-023.62E-02UpCi/g17-10053-05TRGL310219BFRGS007SSA09/27/16 10:0510/11/201710/13/201717-10053Potassium-40EPA 901.1 Modified4.71E+006.50E-016.93E-013.92E-01pCi/g17-10053-06TRGL310223AFRGS003SSB04/25/16 13:2010/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified2.96E-024.43E-024.44E-026.13E-02UpCi/g17-10053-06TRGL310223AFRGS003SSB04/25/16 13:2010/11/201710/13/201717-10053Cesium-134EPA 901.1 Modified-6.71E-033.68E-023.68E-028.99E-02UpCi/g17-10053-06TRGL310223AFRGS003SSB04/25/16 13:2010/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified3.67E-017.80E-028.02E-029.46E-02pCi/g17-10053-06TRGL310223AFRGS003SSB04/25/16 13:2010/11/201710/13/201717-10053Potassium-40EPA 901.1 Modified6.97E+001.04E+001.10E+006.48E-01pCi/g17-10053-07TRGL310223AFRGS004SSB04/25/16 13:1510/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified2.37E-024.44E-024.44E-025.95E-02UpCi/g17-10053-07TRGL310223AFRGS004SSB04/25/16 13:1510/11/201710/13/201717-10053Cesium-134EPA 901.1 Modified1.77E-021.71E-021.71E-027.22E-02UpCi/g17-10053-07TRGL310223AFRGS004SSB04/25/16 13:1510/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified2.07E-023.81E-023.81E-025.62E-02UpCi/g17-10053-07TRGL310223AFRGS004SSB04/25/16 13:1510/11/201710/13/201717-10053Potassium-40EPA 901.1 Modified6.62E+009.64E-011.02E+006.62E-01pCi/gZion, IL 60099Work Order Details:67149817-10053SOENVI RONMENTALFinal Report of AnalysisReport To:Alex Bohacheff Z i o n Solutions101 Shiloh BlvdCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect Printed: 6/12/2018 3:24 PMPage 2 of 2SDG:Purchase Order:Analysis Category:Sample Matrix:Lab I D S a m pleTypeClientIDSampleDateReceiptDateAnalysisDateBatchIDAnalyteMethodResultCUCSUMDAQualifierReportUnitsZion, IL 60099Work Order Details:67149817-10053SOENVIRONMENTALFinal Report of AnalysisReport To:Alex Bohacheff Z i o n Solutions101 Shiloh Blvd17-10053-08TRGL310223AFRGS005SSA04/25/16 13:0010/11/201710/13/201717-10053Cobalt-60EPA 901.1 Modified9.45E-032.47E-022.47E-023.15E-02UpCi/g17-10053-08TRGL310223AFRGS005SSA04/25/16 13:0010/11/201710/13/201717-10053Cesium-134EPA 901.1 Modified-5.75E-031.89E-021.90E-024.35E-02UpCi/g17-10053-08TRGL310223AFRGS005SSA04/25/16 13:0010/11/201710/13/201717-10053Cesium-137EPA 901.1 Modified1.83E-022.26E-022.26E-023.79E-02UpCi/g17-10053-08TRGL310223AFRGS005SSA04/25/16 13:0010/11/201710/13/201717-10053Potassium-40EPA 901.1 Modified4.77E+006.79E-017.22E-014.80E-01pCi/g17-10053-01LCSKNOWN10/11/17 00:0010/11/201710/18/201717-10053Nickel-63ASTM 3500-Ni Modified1.59E+034.78E+01pCi/g17-10053-01LCSSPIKE10/11/17 00:0010/11/201710/18/201717-10053Nickel-63ASTM 3500-Ni Modified1.71E+031.02E+011.01E+022.33E+00pCi/g17-10053-02MBLBLANK10/11/17 00:0010/11/201710/18/201717-10053Nickel-63ASTM 3500-Ni Modified-2.82E-011.35E+001.35E+002.32E+00UpCi/g17-10053-03DUPL310213AFRGS006SSB04/13/16 13:1510/11/201710/18/201717-10053Nickel-63ASTM 3500-Ni Modified-2.01E-017.18E-017.19E-011.24E+00UpCi/g17-10053-04DOL310213AFRGS006SSB04/13/16 13:1510/11/201710/18/201717-10053Nickel-63ASTM 3500-Ni Modified2.91E-017.05E-017.06E-011.20E+00UpCi/g17-10053-05TRGL310219BFRGS007SSA09/27/16 10:0510/11/201710/18/201717-10053Nickel-63ASTM 3500-Ni Modified-2.31E-016.62E-016.62E-011.14E+00UpCi/g17-10053-06TRGL310223AFRGS003SSB04/25/16 13:2010/11/201710/18/201717-10053Nickel-63ASTM 3500-Ni Modified4.49E-026.47E-016.47E-011.11E+00UpCi/g17-10053-07TRGL310223AFRGS004SSB04/25/16 13:1510/11/201710/18/201717-10053Nickel-63ASTM 3500-Ni Modified-4.17E-016.58E-016.59E-011.14E+00UpCi/g17-10053-08TRGL310223AFRGS005SSA04/25/16 13:0010/11/201710/19/201717-10053Nickel-63ASTM 3500-Ni Modified-1.42E-016.79E-016.79E-011.17E+00UpCi/g17-10053-01LCSKNOWN10/11/17 00:0010/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified6.89E+013.86E-01pCi/g17-10053-01LCSSPIKE10/11/17 00:0010/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified7.40E+011.95E+001.03E+011.04E+00pCi/g17-10053-02MBLBLANK10/11/17 00:0010/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified2.17E-011.94E-011.97E-013.90E-01UpCi/g17-10053-03DUPL310213AFRGS006SSB04/13/16 13:1510/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified5.95E-012.43E-012.57E-014.58E-01pCi/g17-10053-04DOL310213AFRGS006SSB04/13/16 13:1510/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified4.41E-012.17E-012.25E-014.14E-01pCi/g17-10053-05TRGL310219BFRGS007SSA09/27/16 10:0510/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified3.37E-012.24E-012.28E-014.41E-01UpCi/g17-10053-06TRGL310223AFRGS003SSB04/25/16 13:2010/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified5.26E-012.47E-012.58E-014.76E-01pCi/g17-10053-07TRGL310223AFRGS004SSB04/25/16 13:1510/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified2.44E-012.14E-012.17E-014.32E-01UpCi/g17-10053-08TRGL310223AFRGS005SSA04/25/16 13:0010/11/201710/19/201717-10053Strontium-90EIChroM SRW01 Modified5.66E-012.11E-012.25E-013.89E-01pCi/gCU=Counting Uncertainty;CSU=Combined Standard Uncertainty (2-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

ML19178A101

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