ML20135E434

Rev 0 to Fire & Hose Stream Test of 8-Inch Thick Specimen of TCO-002 Medium Density Silicone Elastomer Used in Electrical Sleeve Opening Penetrated by Extended Steel Conduit

ML20135E434
Person / Time
Site:	Millstone
Issue date:	03/27/1985
From:	Alexander B, Jarosz G TRANSCO, INC.
To:
Shared Package
ML20135E415	List: B11669, Requests Four Deviations from Branch Technical Position Cmeb 9.5.1 Re Penetration Seals,Fire Barriers,Concealed Spaces & Internal Sealing of Conduits.Transco,Inc Test Repts TR-193,Rev 0 & TR-194,Rev 0 Encl ML20135E423 ML20135E434
References
TR-194, TR-194-R, TR-194-R00, NUDOCS 8509160395
Download: ML20135E434 (42)

Text

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Test Report: #TR-194

- Revision: 0 f Date: 03/25/85

,e Transco Products Inc. Test Report: #TR-194 Fire and Hose Stream Test of an 8" thick specimen of #TCO-002 Medium Density Sili-cone Elastomer used in an electrical sleeve opening penetrated by an extended steel conduit.

For Millstone .;uclear Power Station, Unit 3 Northeast Utilities Service Company Contract No. 2400.000-680 (J.0. 12179)

This Report is the property of:

Northeast Utilites Service Company Millstone Nuclear Power Station, Unit 3 By: A> m Date: ct3/$7!87 va o Gregory J. Jarosz Manager of Technical Development Transco Products Inc.

QC Approval by:

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[Gt , Date: I/87 28 i l Brian Alexander Quality Control O N LY h u'""

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Cnetruction technology laborotorier m: : : :-: r: ::3: s- > e .: : s e::- a2: . : cre 2;: M5 sac May 1, 1985 Mr. Gregory J. Jarosz Manager of Technical Development Transco Products, Inc.

55 East Jackson Blvd.

Chicago, Illinois 60604 Transco Fire Test Report 4TR-194

Dear Mr. Jarosz:

We have received a copy of your Test Report STR-194, dated March 25, 1985, describing fire and hose stream tests of ITCO-002 Medium Density Silicone Elastomer seals. This test was per-formed on March 18, 1985, at the fire research facilities of construction Technology Laboratories.

After review, we find that the report accurately describes test procedures, observations during test, and quantitative results.

Very truly yours, aWgH+ -

Michael Gillen Senior Research Engineer Fire Research Section MG/sr Copy to-- bh Y _ O1NQ W. G. Corley E. A. B. Salse T. J. Rowe Central Files CR5573-4324 l

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Table of Contents Test Report: dTR-194 Revision: 0 )

. Date: 03/25/55 )

TA3LE OF CONTENTS:

dection ,,A,,, ccynopsis: .......................... Page 1 Section "3", Test Slab: ......................... Page 2 Section "C", Penetrating Elements: .............. Pages 2 -3 Section "D", Seal Installation: ................. Page 4 Section "E", Thermocouples: ..................... Page 5 Section "F", Test: .............................. Page 6 Section "G", Hose Stream Tests: ................. Page 7 Section "H", Laboratory Notes and Data: ......... Pages S - 14 Section "I", Post Test Observations: ............ Page 15 Attachment "A", Specimen Drawings: .............. Page 1 of 1 Attachment "3", Furnace Drawings: ............... Pages 2 of 2 Attachment "C", Thermocouple Map: ............... Page 1 of 1 Attachment "D", Seal Installation Procedure: .... Pages 5 of 8 Attachment "E", QC Installation Records: ........ Pages 12 of 12

$blU,fATION ONLY

Test Report: #TR-194 Revision: 0 Date: 03/25/85

- Page: 1 of 15 SECTION "A" SYNOPSIS: ,

The. purpose of this test was to demonstrate the ability of an eight (8) . inch thick firestop of #TCO-002 Medium Density Silicone Elastomer penetrated by an extended steel conduit (and seal within the conduit) to withstand a three (3) hour fire test as defined by ANI and IEEE 634 The test was performed 03/18/85 at' Portland Cement Association 4

(Skokie, Illinois) on a representative floor specimen. At the conclusion of the fire test, the seal specimen sas subjected to a hose stream test in accordance with ANI requirements (along with two additional hose stream tests performed for informational pur-i poses).

i The penetrating ele =ent used in this test was arranged as shown in Attachment "A". The single piece steel conduit extended a minimum of 12" below and 40" above the surrounding firestop. The l

conduit was filled with cables to 55.25% of its cross-sectional i area. Cable sizes tested were in accordance with ANI and-IEEE 634 requirements and included both copper and aluminum power cables.

The conditions demonstrated in this fire test are as follows:

1.) 5" dia. x 60" long steel conduit using a 55.25% by cross-sectional cable fill consisting of approximately 1/3 power, l- 1/3 control and 1/3 instrument cables sealed with 8" of #TCO-

002 Medium Density Silicone Elastomer (plus_2" of #TCO-026 ,

Ceramic Blanket) at the unexposed end of the conduit.

r 2.) Representative cable types and percentages of fills found at Millstone Nuclear Station , Unit 3. ,

3.) 8" thick #TCO-002 Medium Deneity Silicone Elastomer seal i around the conduit installed flush with the slab's exposed surface.

4 4.) A conduit penetrating a steel sleeve opening.

i INFORMATiON ONLY l  :

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. Test Report: #TR-194 Revision: 0 Date: 03/25/S5 Page: 2 of 15 SECTION "B" TEST SLAB:

The concrete test slab used for this test measured 48" x 48" x 12" thick and was penetrated by four 12" diameter steel sleeves.

One of these four 12" diameter steel sleeves was used for the test. The test slab was designed and fabricated by PCA/CTL.

SECTION "C" PENETRATING ELEMENTS:

The 5" diameter by 60" long single piece conduit was located on center to the 12" diameter sleeve opening. The conduit . extended 12" below and 40" above the firestop. The exposed end of the conduit (beneath the slab) was capped with a steel connector and plug.

The conduit was filled with representative cable types and per-centages of fills found at Millstone Nuclear Power Station, Unit

3. The cable sizes tested were in accordance with ANI and IEEE requirements.

The conduit was filled to 55.25% of its cross-sectional area with approximately 1/3 power, 1/3 control, and 1/3 instrument cables. Power cables included both copper and aluminum conductors.

The cables extended approximately 12" below and not less than 36" above the test slab (40" above the firestop).

Cable fills are found on page number 3 of this report.

)$ FORMATION ONLY t

Test Report: #TR-194 Revision: 0 Date: 03/25/85 Page: 3 of 15 SECTION "C" (Cont.)

PENETRATING ELEMENTS:

The cable fill of the conduit was as follows:

Man. Mark #:

Description:

Con.: Dia. Area: Qty.: Total

(") ("2) Area:

(power cables:)

Kerite NHP-18 1/C 500 MCM Cu 1.25 1.2271 1 1.2271 Kerite NHP 42 1/C 500 MCM Al 1.76 2.4328 1 2.4328 (total power cables: 3.6599)

(control cables:)

Kerite NHN-05 7/C #14 Cu 0.76 0.4536 1- 0.4536 Okonite NHT-24 1/C #14 Cu 0.21 0.0346 1 0.0346 Okonite NHT-37 9/C #14 Cu 0.81 0.5153 1 0.5153 Okonite NHT 40 12/C #14 Cu 0.97 0.7389 1 0.7389 Okonite NHT-59 12/C #12 Cu 1.05 0.8659 1 0.8659 Okonite NHT-66 2/C #8 Cu 0.72 0.4072 1 0.4072 Rockbestos None 5/C #12 (ALS) Cu 0.73 0.4185 1 0.4185 Brand Rex Not.e 1/C #4 (SIS) Cu 0.40 0.1257 1 0.1257 (total control cables: 3.5597)

(instrument cables:)

BIW NHS-97 9/C #14 Cu 0.81 0.5153 1 0.5153 BIW NHQ-20 4/C #16 Cu 0'.55 0.2376. 1 0.2376 BIW NHQ-61 Triax Cu 0.55 0.2376 1 0.2376 BIW NHQ 49 Thermocouple Cu 0.50 0.1963 1 0.1963 BIW NHQ-12 3/C #16 Cu 0.50 0.1963 1 0.1963 (NUSCO) NHS-69 5/C *10 Cu 0.65 0.3318 1 0.3318 BIW NHQ-15 10 pr. #18 Cu 1.40 1.5394 1 1.5394 (RCI) NH1 47 24/C #16 Cu 0.69 0.3739 1 0.3739 (total instrument cables: 3.6282)

(tota; all cables used: 10.8478)

INFORMAT1ON ONLY

Test Report: #TR-194 Revision: 0 Date: 03/25/85 Page: 4 of 15 SECTION "D" SEAL INSTALLATION:

The #TCO-002 Medium Density Silicone Elastomer seals were installed using applicable sections of Transco Products Inc.'s

.nstallation and QC procedure PSQAP 9.10, Rev. 1 (Attachment "D").

The medium density silicone elastomer was installed 8" (max.)

deep in the unexposed end of the conduit and space around the conduit. Prior to sealing the conduit, 2" (max.) of #TCO-026 Ceramic Blanket (Johns-Manville's 4 lb. "Cerawool") aas installed 8" below the unexposed end of the conduit and served as perma-nent damming which was left in place for the test.

Inhibition of cure occured at the cables / conduit seal interfaces and was left unrepaired for the test. TPI QC records for the seal installation wo'rk c'an be found in Attachment "E".

Prior to conducting the test, the unexposed cable ends were capped with Dow Corning #96-081 Silicone Adhesive.

JNFOIUdAhs q

Test Report: #TR-194 Revision: 0 Date: 03/25/85 Page: 5 of 15 SECTION "E" THERMOCOUPLES:

Thermocouples were mounted to the slab to gather temperature data throughout the test. Temperatures were documented at five minute intervals for the first two hours and then at ten minute incre-ments for the remaining hour of the test.

Thermocouples 49-54, and 56 were tied with brass wire to their ,

respective items at the seal / item interfaces. Seal surface l thermocouples 27, 28, and 55 (along with sleeve thermocouple 29) i were laid onto their respective surfaces and weighted for con-tact.

! Thermocouples 57 through 70 were tied with brass wire directly to 1

the conduit and were covered with 1" x 1" x 1/8" thick ceramic l j fiber pads. These thermocouples were mounted in groups of two  ;

j (180 degrees apart from each other) starting flush with the surrounding seal and extending up every 6" to the top of the ~

conduit. l 1 i Furnace atmosphere temperatures were monitored and documented in l

! accordance with ASTM E-119 requirements. Three thermocouples are l permanently mounted inside of the furnace 12" below the specimen for this purpose. l Thermocouples were mounted as follows: [

i T/C #:

Description:

Degree F at 3 Hrs.:  ;

27 Surrounding seal surface: .... ........... 276  ;

25 Surrounding seal surface: ................. 281  !

29 Sleeve: ..........................:........ 408 49 1/C #4 SIS cable: ......................... 116  !

50 5/C #12 ALS cab 1e:......................... 117 -

i 51 9/C #14 (BIW) cable: ...................... 114 l 52 1/C #14 cable: ............................ 113 53 10 pr. #18 cable: ......................... 102  :

54 Triax cable: .............................. 113 t 55 Conduit seal surface: ..................... 109  !

56 Conduit: .................................. 115 l 57 Conduit (0" from sur. seal surface): ...... 450  ;

, 58 Conduit (0" from sur. seal surface): ...... 430 [

59 Conduit (6" from sur. seal surface): ...... 256 60 Conduit (6" from sur. seal surface): ...... 272 I 61 Conduit (12" from sur. seal surface): ..... 188 i 62 Conduit (12" from sur. seal surface): ..... 218 i 63 Conduit (18" from sur. seal surface): ..... 182  !

64 Conduit (18" from sur. seal surface): ..... 184 (cont.) i t

R4 FORMATION ONLY l i

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1 Test Report: STR-194 Revision: 0 Date: 03/25/S5 Page: 6 of 15 SECTION "E" (cont.)

THERMOCOUPLES:

T/C #:

Description:

Degrees F at 3 Hrs.:

65 Conduit (24" from sur. seal surface): ..... 167 66 Conduit (24" from sur. seal surface): ..... 172 67 Conduit (30" from sur. seal surface): ..... 140 68 Conduit (30" from sur. seal surface): ..... 144 69 Conduit (36" from sur. seal surface): ..... 119 70 Conduit (36" from sur. seal surface): ..... 122 The thermocouples were placed and mapped by TPI QC. Thermocouple map can be found in Attachment "C".

SECTION "F" TEST:

The fire test was conducted in accordance with the ASTM E-119 time / temperature curve for three hours. PCA/CTL personnel documented specimen thermocouple and furnace. atmosphere tempera-tures and recorded test observations.

Light smoke began at the unexposed end of the conduit at 2 minutes and lasted an additional 23 minutes. At 45 minutes into the test, liquid inhibited silicone from the seal / cable interfaces began to drip down the conduit. No other occurrences were noted.

The furnace draft pressure averaged -0.08" of water pressure throughout the test. Furnace drawings can be found in Attach-ment "B".

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Test Report: *TR-19' Revision: 0 Date: 03/25/S5 Page: 7 of 15 SECTION "G" HOSE STREAM TESTS:

After the conclusion of the fire test, the specimen was removed from the furnace and placed on its side for the hose stream test.

Although the specimen was required to be subjected to only the ANI hose stream test, two additional tests were conducted for informational purposes.

Each test was conducted for a minimum period of 24 seconds based on a 2.5 minute exposure for every 100 square feet of slab area.

Prior to conducting the test, TPI QC personnel verified the distance between the specimen and hose nozzle. The tests were as follows:

1.) ANI: 75 psi hose stream delivered through a 1. " diameter hose equipped with a fog nozzle set at a 21scharge angle of 15 degrees from a distance of 10 feet with a flow rate of 75 gpm.

2.) IEEE: Sa=e as above except that t discharge angle is increased to 30 degrees.

3.) ASTM: 30 psi solid hose stream delivered through a 2.5" diameter hose equipped with a 1.125" tip set on a playpipe from a distance of 20 feet.

No water projected through the specimen's unexposed surface during any of the tests, s

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" Revision: 0, Date: 03/25/35, Page 3 er 15 CR5573 - TRANSCO TR193 - 03/18/85 TEST COMMENTS 0:00:00 LIGHT SMOKE NOTED RT THE TOP OF PEN D PIPE 0:20:00 STERM BEING BLOWN OFF RT THE TOP OF PEN D PIPE 0:25:00 SMOKE NO LOHCER HOTED.RT THE TOP OF PEN D PIPE 0: 45:00 BLACK LIQUID MRTERI AL NOTED COMING FROM TOP OF PEN D AROUND THE PIPE 1:10:00 MINCR EXPANDSIGH NOTED IN SEAL IN PEH C HOSE STREAM TESTS:

HOSE STREAM N0 WRTER PROJECTED BEYOHD THE UNEXEXPOSED SURFRCE DURIHC RHI STREAM TEST FOR 24 SEC.

IEEE-634 HOSE H0 WRTER PROJECTED BEYOND THE UNEXEXPOSED SURFACE DURING STREAM TEST FOR 24 SEC.

E-119 HOSE H0 WATER PROJECTED BEYOND THE UNEXEXPOSED SURFRCE DURING RSTM STREAM TEST FOR 24 SEC.

H0TES:

D:tRFT RUN RT .08 NEG.

S:10KE CLASS L PEN R = TR196 PEN 3 = TR195 PEN C = TR193 PEN D = TR194 1

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" Revision: 0, Date: 03/2,5/35, Page 9 of 15 CR5573 - TRANSCO TR193 - 03/18/85 FURNRCE RTMOSPHERE TEMPERATURE (DEC. F)

FURNRCE ASTM E119 VARIATION FROM TEST TIME, TEMP. TEMP. RSTM TEMP.

Hr: Min F F F 77 68 9 0:00 1000 0 0:05 1000 1375 1300 75 0:10 1441 1399 42 0:15 1429 1462 -33 0:20 1510 5 0:25 1515 1550 8 0:30 1558 1584 9 0:35 1593 1613 -8 0: 40 1605 1628 1630 -10 0: 45 1661 -4 0:50 1657 1675 1681 -6 0:55 1691 1700 -9 1:00 1712 1718 -6 1:05 1734 1735 -1 1:10 1745 1750 -5 1:15 1759 1765 -6 1:20 1767 1779 -12 1:25 ~

1786 1792 -6 1:30 1795 1804 -9 1:35 1804 1815 -11 1: 40 1813 1826 -13 1: 45 1827 1835 -8 1:50 1842 1843 -1 1:55 1855 1850 5 2:00 1868 1862 6 2:10 1869 1875 -6 2:20 1886 1888 -2 2:30 1983 1900 3 2: 40 1912 -1 2:50 1911 1922 1925 -3 3:00 RRER UNDER CURVE = 294597 DEG. F-MINUTES 1 RRER UNDER ASTM E119 CURVE = 294600 DEG. F-MINUTES VARIATION FROM RSTM CURVE = -0.0010  %

l JNFORhMTION ONLY

Section "H" to Test Repo:: ??E '

' Revision: 0, Date: 03/25/85, Page 10 of 15 CR5573 - TRANSCO TR193 - 03/10/89 UNEXPOSED TEMP. READINGS (DEC. F.)

TEST TIME, T/C NO.

Hr: Min 25 26 27 28 29 30 71 7 70 70 70 72 0:00 71 7 70 70 70 72 0:05 71 1 70 70 74 71 0:10 71 2 72 74 82 72 0:15 72 75 75 GO 93 75 0:20 73 79 81 87 106 78 0:25 84 89 95 121 2 0:30 75 78 90 98 104 140 6 0:35 94 107 113 161 0 0: 40 81 0: 45 4 99 117 123 183 9 0:50 7 103 126 133 198 9 0:55 9 106 135 142 204 10 1:00 9 109 145 152 217 103 1:05 97 112 153 160 229 105 100 115 161 167 241 108 1:10 1:15 103 119 167 175 254 110 1:20 106 121 176 182 265 112 1:25 10. 124 184 190 274 115 1:30 11 127 190 195 283 116 1:35 1'4 129 198 202 291 118 1: 40 16 131 203 208 299 120 1: 45 13 133 203 212 307 12 1:50 21 135 214 217 313 12 1:55 123 137 218 '

224 321 12 l 2:00 125 47 223 229 328 1 2:10 129 1 8 237 235 344 1 9 2:20 134 1 6 246 246 358 1 2 2:30 137 18 251 255 373 1 6 141 18 260 261 387 38 2: 40 .

145 190 268 269 395 42 2:50 276 281 408 !144

3:00 148 192 i

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Section "H" to Test Reper eTR Revision: 0, Date: 03/25/35, Page 11 of 15 CR5573 - TRANSCO TR193 - 03/18/85 UNEXPOSED TEMP. READINGS (DEG. F.)

TEST TIME, T/C NO.

Hi-: Min 49 50 51 52 53 54 0:00 72 72 71 72 73 71 71 71 71 71 73 71 0:05 71 71 71 71 73 71 0:le 71 71 71 72 73 71 0:15 0:20 72 72 72 72 73 72 73 73 72 73 73 72 s 0:25 0:30 74 74 73 74 74 73 0:35 75 75 73 75 75 75 0: 40 76 77 74 76 76 76 0: 45 78 78 75 78 78 77 0:50 79 80 77 79 79 79 0:55 81 81 78 80 80 80 1:00 82 83 79 82 81 82 1:05 84 85 80 83 82 83 1:10 86 86 82 84 83 84 1:15 87 88 84 86 84 86 1:00 89 89 86 87 84 87 1:25 90 90 87 89 85 89 1:30 91 S2 89 90 86 90 1:35 93 93 90 91 87 91 1: 40 94 95 92 93 88 93 1: 45 95 96 93 93 89 94 1:50 96 97 94 95 89 95 1:55 98 98 95 - 96 90 96 2:00 99 99 96 96 91 97 2:10 102 102 100 180 93 99 2:20 105 106 103 103 95 102 2:30 108 109 105 105 97 106 2: 40 111 112 108 108 99 109 2:50 114 115 111 110 100 111 l

3:00 116 117 114 113 102 113 l

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-dection ' '.. ;c .es. .: pert ... .y-hevis' ion: 0, Cate: 03/25/E , Fa6e 12 Of 15 CR5573 - TRANSCO TR193 - 03/18/85 UNEXPOSED TEMP. READINGS (DEG. F.)

TEST TIME, T/C NO.

55 56 57 58 59 60 Hi-: M i n 72 70 70 71 71 0:00 72 71 74 73 71 72 0:05 72 71 89 91 74 84 0:10 71 71 130 120 91 118 0:15 72 72 72 202 144 120 133 0:20 73 72 239 162 149 137 0:25 73 257 181 162 144 0:30 73 75 269 201 169 156 0:35 74 76 274 219 172 170 0: 40 74 76 77 290 232 179 182 0: 45 77 79 306 247 136 189 0:50 79 80 310 257 191 195 0:55 80 82 309 266 192 202 1:00 82 84 308 276 196 207 1:05 83 86 311 284 200 213 1:10 85 87 315 291 205 218 1:15 86 89 319 298 209 222 1:20 88 90 323 305 214 226 1:25 89 91 329 310 217 229 1:30 90 93 335 314 218 233 1:35 91 94 339 319 221 234 1: 40 92 95 343 324 222 236 1: 45 93 96 351 331 224 236 l 1:50 95 98 358 s 336 227 236 1:55 95 99 367 339 228 238 2:00 98 102 384 355 230 243 2:10 100 105 401 377 237 249 2:20 103 108 412 391 241 256 2:30 110 424 406 245 261 2: 40 105 113 436 416 251 266 2:50 107 115 450 430 256 272

~3:00 109 hsjal uk kkiL A UY eY l

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3evision: 0, Oa e: 03/25/35, Page 13 of 15 CR5573 - TRANSCO TR193 - 03/18/85 UNEXPOSED TEMP. READINGS (DEC. F.)

TES T TIME, T/C NO.

61 62 63 64 65 66 Hr: Min 71 71 71 71 72 72 0:00 71 72 71 71 71 72 0:05 73 77 72 73 72 73 0:10 89 98 86 83 78 83 0:15 107 114 96 95 OS 91 0:20 129 120 112 105 94 93 0:25 137 128 122 113 103 105 0:30 141 134 127 120 108 110 0:35 137 142 124 122 107 109 0: 40 143 152 128 127 108 111 0: 45 149 161 131 133 115 118 0:50 151 168 134 141 118 123 0:55 151 172 139 146 121 126 1:00 155 177 141 146 121 124 d

1:05 1:10 160 181 142 146 121 124 156 184 143 146 121 123 1:15 1:20 164 190 145 148 122 124 1:25 171 196 148 152 123 125 1:30 172 198 153 157 125 127 1:35 177 203 160 164 127 130 1:40 179 207 165 169 131 133 1: 45 179 208 171 176 134 137 1:50 181 206 175 183 139 142 1:55 182 203 175 s 185 146 149 2:00 180 203 175 186 152 156 2:10 181 205 176 185 157 160 2:20 183 207 178 183 159 161 2:30 182 210 180 181 161 163 2: 40 185 213 180 183 162 165 2:50 186 215 181 183 164 168

3:00 188 218 182 184 167 172 J r g Q L. ,. r .rr y ' @ h I

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R e v i s i*c n : 0, tate: 03/25/55, pag, ;; of ;5

' CR5573 - TRANSCO TR193 - 03/18/85 UNEXPOSED TEMP. READINGS (DEC. F.)

TEST TIME, T/C NO.

67 68 69 70 H;-: Mi n 72 72 72 72 0:00 71 71 71 0:05 71 71 72 71 71 0:10 76 72 72 0:15 73 30 72 73 0:20 77 82 87 74 74 0:25 93 75 77 0:30 89 92 95 78 79 0:35 93 95 79 81

, 0: 40 93 95 80 83

! 0: 45 96 99 82 84 0:50 98 101 83 86 j

0:55 100 103 85 88 l 1:00 101 104 87 89 j 1:05 102 104 89 90 2 1:10 102 105 90 91 f 1:15 103 106 91 93 j 1:20 104 106 92 94 1:25 106 108 94 S5 1:30 107 109 95 97 3

1:35 0 112 9 9 1 45 112 115 98 100 1:50 115 117 100 102 1:55 119 120 101 103

2

00 124 126 105 187 2:10 129 131 188 110 2:20 132 134 111 114 2:30 134 138 114 117 2: 40 137 141 116 119 2:50 140 144 119 122 3:00

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i INFORMATION ONLY I

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Test Report: 4TR-194 Revision: 0 Date: C3/25/S5 Page: 13 of 13 SECTION "I" POST TEST OBSERVATIONS:

After the fire test, it was observed that seal's exposed surface had expanded approximately 1" out of the penetration at the conduit. The conduit was still intact but discolored from the fire. No other damage to the conduit was noted.

No visual changes were noted to the specimen on its unexposed surface (except for where inhibited silicone had dripped down the conduit). The exposed surface of the seal had formed a hard char layer approximately 3" deep into the seal.

The conduit seal and seal surrounding it had passed both the fire and hose stream tests and met the performance requirements of ANI and IEEE 634 s

JNFORMATION ONLY

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TEST REPOAT: #TR194 REVISION: 0 DATE: 03/25/85 PAGE: 1OF1 I

x SLEEVE TEST PENETRATION A A t_ g ,

3 SEAL 5"DIA. CONDUIT I

PLAN CABLES (TYPtCAL)

TCO-OO2 MEDIUM DENSITY

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SILICONE ELASTOMER SECTION "A-A" TEST W TR-194 7C0-002 MEDIUM DENSITY SILICONE ELASTOMER SEAL FOR STEEL CONDUE t--

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- Test Report: #TR-194 Revision: 0 Date: 03/25/85

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OF FURNACE

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ATTAOMM ENT "O" TEST REPORT;88TR-!94

% AEVISION: O DATE: 03/25/85

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58,60,62,64, 29 66,68 8 70 TEST #TR-194 T/C" DESCRIPTION 27 ANNULAR SEAL SURFACE ,

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29 SLEEVE 49 SIS #4 50 ALS 51 9/C ,#14 52 1/C 14 53 10 TW PR #18 54 TRIAX 55 SEAL SURFACE 56 CONDUlT 57 CONDUIT (O" UP FROM SURROUNDING SEAL) 58 a a a a a a 59 6" FROM BOTTOM ON CONDUIT 60 a a a a a a

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RANSCO PRODUCTS INC. CiHlU' oms 11DJ]BM C : -

' No. PSQAP 9.10 TITLE:

Page 1 of 8 SPECIA1. PROCESSES - SILICONE ELASTOMER Revision 1 9 .1 ; PUFJOSE_

- This procedure defines the method of installing and inspecting o Silicone Elas tome r Seals.

9.2 l .

P.EFEFINCES E

10CFR50 Appendix 3 Penetration Seal Quality Assurance Program Manual PSQAP 8.0, 9.0, 10.0, 10. I , 15.0 :

i c 9.3 PROCEDUFI 9.3.1 The Transco Field Superintendent and qualified craf t pe rs onnel

{. are responsible for the installation of Silicone Elastomer

~

caterials in accordance with this proceddre. Quality Control j Fersonnel are responsible for inspection activities per this I.y procedure.

a-~;s.

! 4, . 9.3.2 Prior to installing the seal materials, the penetration shall have been identified per PSQAP 8.0 and the da= ing operations shall have been cocpleted per PSQAP 9.O.

i[

[

9.3.3 The Transco Field Superintendent / Designee shall obtain a copy

_1 of the " Field Takeoff, Installation, and Inspection Record" 3 (Figure 1) f roc Quality Control which will indicate those penetrations which are released for final sealing operations.

This form is nor= ally obtained at the start of each work day or shift. Penetrations shall not be sealed unless release is e

~

indicated on the form. An alternate release method /fors may te used if found to be more efficient in issuing releases to production, but all data required 'on the Field Takeof f, Ins tal-N '

lation, arid Inspection Record form shall be completed.

9.3.4 For traceability purposes, the caterial supplier hac assigned unique numbers for each lot of material manufactured. Each hjt, container of silicone, both parts A and B, is to have a lot yyj, nu'eber clearly printed on it and a green stripe indicating it is acceptable for production use (per PSQAP 10.0). Containers a without a lot number and/or, a green paint stripe are not to be~

used,'are to be segregated from acceptable caterials, and the D Quality Control Manager is to be notified.

• ~i. e o 9.3.5 Installation of Silicone Elastomer can be accomplished by 3 utilizing dispensing equipcent, or may be hand mixed and applied as specific conditions dictate.

s 9.3.6 Prior to installation of the Silicone Elastomer, the field installer shall complete the top portion of the " Field Data 6

Sheet" (Figure 2) indicating, among other information, the l MM '

INFORMATION ONLY

_ I HAljSUU PHOUUCTS INC.aedst=: o, :ne: O m s/ss, P ue 2 or e TITLE: No. PSQAv 9.10 Page 2 of 8 SPECI AL PROCESSES - SILICONE ELASTO.T.:.R

' Revision 1

, the batch number assigned to the Silicone Elastocer. A batch is defined as each ti=e the =aterial holding tanks are refilled with Batch numbers are assigned beginning with ~001 ard ma t e ri al.

3 continuing consecutively. Any time a batch re=ains in the the holding tanks at the end of a shif t or the end of the work day and the holding tanks are not refilled when work resu:es, t hen a unique and consecutive batch letter shall be assigned i to the end of the existing batch number beginning with the letter A".

Example:

2, EV118009 - 005 EV118009 - 005A EV118009 = P.aterial supplier lot nu ber

- 005 = The 5th batch used from lot EV118009

'E A = A stop in production and resu ption without I

j a caterial refill. .

ii 9 -

r .c-a L During the installation operations, all penetration numbers .

- Qn 3 J.

)9 which receive a specific batch of Silicone Elasto=er shall be j i

~

listed on the Field Data Sheet.

I 3d In so=e cases, equip:ent may be used which attaches directly to j $'I of .

the caterial containers 'instead of having " holding tanks". In these cases, the canufacturer supplied lot nueber alone is all j

• that.is required. .

9.3.7 Sa=ples of the Silicone Elasto=er are taken to verify that the

{ caterial is suitable for installation.

a) Two sacples are cade in two disposable sacple cups supplied

_\ by quality Control Personnel. These two saeples shall be s made for each lot / batch of Silicone Elastomer used in the dispensing unit (also for lettered batches). These two

.C sample cups must be filled sufficiently to assure that cured a samples are at or above the top of the sacple cups.

c .

,y , j b) The lot / batch nucher, insta11er's initials, and date shall be af fixed on the two sacple cups by the installer. These two i g,

,V samples are for Quality Control and shall be properly stored

' until turned over to quality Control Personnel, normally at N the end of the shif t.

Sa :.

3 a -

c) The field installer shall evaluate one of these samples prior to installation activities. This sample shall be flush with sample cup top. Using a gram scale, weigh the sample to the nearest 1/10 of a gram. This weight is recorded on the Field 7 Data Sheet and should be within the following acceptable d'-,) tolerances:

70-95 lbs. per cubic foot, unless otherUise specified.

-Q L

M INF_ORMATION ONLY

b -

. ic O, Da- : f 2h f ', I - :

TITLE: No. PSQAP 9.10 Page 3 of 8

' SPECI A1 ?ECCESSES - SILICONE ELASTOMER ~

Revision 1 Should the sa:ple weight not ,be acceptable , Quality Control ,

Personnel are 'to be contacted ic=ediately and work shall not pro-ceed.

9.3.S During Silicooe Elastomer installation, the QC Inspector shall perfor:: in process inspections at random stages of the instal-lation process. During these inspections , the QC Inspector shall j

observe specific installation procedures such as cleanliness, spreading of electrical cables, proper use of the Field Data Sheet, etc.. These inspections shall be documented on the

- applicable Field Data Sheet using the ~ REMARKS colucn to 2 indicate any instructions for re processing of a penetration to 5 correct in-process deficiencies. Upon satisfactory cospletion of required re processing, the QC Inspector shall initial and date the re processing noted previously on the Field Data Sheet as i

7 being co=plete.

7 i 9.3.9 Installation of the Silicone Elastocer shall be accomplished as j@ follows:

1h i '-.

10 ,3 a) Prior to installation, individual silicone cosponents shall j be thoroughly cixed using a drill motor'and mixing paddle.

L -

'2 3

~

b) The individual cocponents, A and B, shall now be mixed j todether in one container at a ratio of 1:1 by weight or j voluce using a heavy duty mixer motor and mixing head for

• approxicately two minutes. If a dispensing unit is used , the A and 3 cocponents are not mixed together'but are poured into separate holding tanks in the dispensing unit, or are pumped

,q g directly from the material containers, as applicable.

O c) If dispensing units are used,sconsult the applicable,

' instruction manuals as required - PROPRIETARY.

d) Samples shall now be prepared and evaluated per 9.3.7 above.

e) Install the Silicone Elastocer into the penetration by using

[f, the dispensing unit, hand pouring or pumping as the field g,I} condition dictatn. WATC11 FOR LEAKACE!

%5 X - f) Installed Silicone Elastomer shall be allowed to cure for a minimum of twenty-four houcs at which time all damming shall be re=oved, as applicable, and excess material removed and

[t. -.

the penetration seal trimmed flush with wall or floor

~

5 .. surface.

4 i g) Ceneral good housekeeping shall be maintained at all times.

I y%) i 9.3.10 Alterations for additions to or deletions f rom previously sealed penetrations can be made by carefully cutting out enough Silicone Elastomer to permit the addition or deletion, or by using core boring equipment if space allows. In either case, etgeg Q$; INFORMATION ONLY W"

I HANWU vnuuvo i d om. T _ ate: . ,3/25/h_, Page i of 8

. _._ Le-zis.vn: C, s

' 30, psqf,p 9,to TITLE: 4 of 8 Page  ;

SPECI AL PROCESSES - SILICOST. ELASTO."IP. Ite vi s ion 1 caution must be exercised when making alte rat tor.s to avoid da: age to any penetrating ite=s (i.e.; cables, ins tru:e ct tubing, etc.) cc a to surrounding seal material. The added opening should be made o straight through the seal and made only slightly larger than the ites to be added. Deletions should be carefully pulled out and only a mini =al a:ount of Silicone Elastomer should k removed in i_

order to facilitate the deletion.

9.3.11 Minor repairs are permissible by removing a small portion (1 -2")

of the surrounding Silicone Elastocer to provide a good, clean Prepare,

• surface for the ces Silicone Elastomer to bond to.

sa:ple, and seal the altered area following the instructions outlined in 9.3.6 through 9.3.9 above.

i 9.3.12 Per=anent identification of completed pene tratica seals is 3 final j' perf orced by production personnel and cust be doce prior to inspection by Quality Control Personnel. The :ethod for identifi-cation cay be accocplished by any of the folloviq cethods or as i[-[n ,

specified by the custocer: ,

]Ij i

a) Hand printed next to the opening using a waterproof g

flow =ar .ce r .

g gw .

Stenciled next to the opening using paint applied by brush, f

j b) roll, or spray.

c) Steel tags attached with adhesive next to the opening. .

>~ 9.3.13 Quality Control Personnel shall perfors final inspection of the N cocpleted seals when released by production for inspection k.: -

activities. Ite=s to be considered during final inspection shall

,be a minicus of the following:

a) Temporary dae:: ting, ,where applicable , is totally removed

and disposed of.

b Temporary supports, where applicable, such as duct tape, E1 .

b) vood shics, etc. , have ken recoved and disposed of.'

Seals are teatly trimmed where applicable to floor, vall,

[ . c) ceiling, and penetration surfaces.

.%y D

• d) Penetration fill is sufficient to co=pletely fill or overfill the penetration to the specified fill depth, ard no visible h" ..

, volds or openings exist. Seal material is cured (no wet or tacky material is present).

=a

- " e) The proper materials were used for the sealing, damaing, and identification of the penetration.

INFORMATION ONLY la . - .- .-

l HANSUU l>HUUUC FS INC.tevision: C, late: C m sfes, Psd i cf 5 TITLE: No. PsqAP 9.10

, SPECI AL PTt0 CESSES - SILICONE ELASTO."ER Page 5 of 8 Revision I

)

f)' Permanent identification is affixed near the penetration and is correct and is acceptably attached.

d: g) Work location is clean. ~,

b) The dispersion of Silicone Elastocer around the cables in the penetration shall be inspected. If the Silicone Elastomer is

-i not dispersed between the cables in a penetration, the seal shall be repaired per Section 9.3.11.

• 9.3.14 Quality Control Personnel shall inspect the samples of Silicone Elasto=er supplied to them by production (9.3.7b). One sa:ple shall be cut. open and exa:Ined for: -

f -

a) Color - Dark grey to black (this may vary based on additives

~

j used) fQ b) Cell' structure - Uniform and free from elongated cells

". ~i.  %

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[. 4 c) Textu re - Solid , se t , firm, with no tackiness.

k . Acceptable cocparison sacples shall be available for the Quality

'I Control Inspector to reference for an acceptable Silicone Elas- -

3 ,

tocer product. This' inspection shall be docu=ented on the QC f . Sacple Inspection Record (Figure 3). The second sample shall be 3 flush with the top of the saeple cup and weighed on the gram scales. The sample density shall then be deterzined and documented per PSQAP 10.1.

9 - -

9.3.15 Upon acceptance of the completed Silicone Elastocer seal and testing sa=ples, the final inspection activity (per this procedure and 10.1) is docucented on the Field Takeoff, y

Installation, and Inspection Record indicating, among other s information, the date accepted and the inspector's initials. If

4 the inspection results in a rejection status, a Report of No nconf o r=a nce is issued and the penetration is tagged with a "Rej e ct" tag pe r PSQAP 15.0. The Field Takeoff, Installation, j j ,

}

and Inspection Record is not initia11ed until all noaconfor-l

%g 4 mances have been resolved and corrective action completed and 5 .

accepted.

Q  : 4 Doct;"ENTS/ RECORDS

'h  !

5 9.4.1 The nonpermanent docueents applicable to this procedure are the

" " Field Data Sheet" and the "QC Sample Inspection Record".

9.4.2 The permanent document applicable to this procedure is the " Field

k. - Takeof f, Installation, and Inspection Record".

r

.. . INFORM!JrION ONLY WI .

= *** "

R---AN S CO PRO D U_C. T_.S IN_C.e Ce'?.s;!."on?. 'O ,"";a'te: c /25/c _ - . a, "-a J "e.c9-or c -

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Attachment "E" Test Report: #TR-194 Revision: 0 Date: 03/25/85 Page: 1 of 12 ATTACHMENT "E" QC INSPECTION RECORDS:

The following pages cons.ist of the Quality Control records for this test. These records are:

a.) Receiving Inspection Reports: ...................... 2 pages b.) Field Take-Off, Installation, and Inspection Record: ............................................ 1 page c.) Batch Sample Density Measurement Records: .......... I page d.) Field Data Sheets: ................................. 1 page e.) QC Sample Inspection Record: ....................... I page f.) Handwritten notes regarding specimen fabrication, cable loadings, etc.: .............................. 2 pages g.) Mapping of thermocouple layouts: ................... 3 pages

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