ML20135E423

Rev 0 to Fire & Hose Stream Test of 8-Inch Thick Specimen of TCO-002 Medium Density Silicone Elastomer Used in Electrical Sleeve Opening Penetrated by Extended Aluminum Conduit

ML20135E423
Person / Time
Site:	Millstone
Issue date:	03/29/1985
From:	Alexander B, Jarosz G TRANSCO, INC.
To:
Shared Package
ML20135E415	List: B11669, Requests Four Deviations from Branch Technical Position Cmeb 9.5.1 Re Penetration Seals,Fire Barriers,Concealed Spaces & Internal Sealing of Conduits.Transco,Inc Test Repts TR-193,Rev 0 & TR-194,Rev 0 Encl ML20135E423 ML20135E434
References
TR-193, TR-193-R, TR-193-R00, NUDOCS 8509160392
Download: ML20135E423 (41)

Text

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Test Report: *TR-193 Revision: 0 Date: 03/25/F5 Transco Products Inc. Test Report: #TR-193 Fire and Hose Stream Test of an 8" thick specimen of !TCO-002 Medium Density Sili-cone Elastomer used in an electrical sleeve opening penetrated by an extended aluminum conduit.

For Millstone Nuclear Power Station, Unit 3 Northeast Utilities Service Company Contract No. 2400.000-680 (J.O. 12179) s This Report is the property of:

Northeast Utilites Service Company Millstone Nuclear Power Station, Unit 3 By: W, vv

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j Gregory J. Jaros:

) Manager of Technical Development 1

Transco Products Inc.

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Brian Alexander Quality Control 4

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Table of Contents Test Report: #TR-193 Revision: 0 Date: 03/25/85 TABLE OF CONTENTS:

Section "A", Synopsis: .......................... Page 1 Section "B", Test Slab: ......................... Page 2 Section "C", Penetrating Elements: .............. Pages 2 -

3 4

Section "D", Seal Installation: ................. Page Section "E", Thermocouples: ........... ......... Page 5 Section "F", Test: .............................. Page 6 Section "G", Hose Stream Tests: ................. Page 7 Section "H", Laboratory Notes and Data: ......... Pages 8 - 14 Section "I", Post Test Observations: ............ Page 15 Attachaent "A", Specimen Drawings: .............. Page 1 of 1 Attachment "B", Furnace Drawings: ............... Pages 2 of 2 Attachment "C", Thermocouple Map: ............... Page 1 of 1 Attachme'nt "D", Seal, Installation Procedure: .... Pages 8 of 8 Attachment "E", QC Installation Records: ........ Pages 12 of 12 i

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f Test Report: #TR-193 Revision: 0 Date: 03/25/85 Page: 1 of 15 SECTION "A" SYSOPSIS:

The purpose of this test was to demonstrate the ability of an eight (8) inch thick firestop of #TCO-002 Medium Density Silicone Elastomer penetrated by an extended aluminum conduit (and seal within the conduit) to withstand a three (3) hcur fire test as defined by ANI and IEEE 634 The test was performed 03/18/85 at Portland Cemer.t Association (Skokie, Illinois) on a representative floor spe:imen. At the conclusion of the fire test, the seal specimen was subjected to a hose stream test in accordance with ANI requirements (along with two additional hose stream test performed for informational pur-poses).

The penetrating element used in this test was arranged as shown in Attachment "A". The single piece aluminum conduit extended a minimum of 12" below and 40" above the surrounding firestop. The conduit was filled with cables to 55.25% of its cross-sectional area. Cable sizes tested were in accordance with ANI and IEEE 634 requirements and included both copper and aluminum power cables.

The conditions demonstrated in this fire test are as follows:

1.) 5" dia. x 60" long aluminum conduit using a 55.25% by cross-sectional cable fill consisting of approximately 1/3 power, 1/3 control and 1/3 instrument cables sealed with 8" of #TCO-002 Medium Density Silicone Elastomer (plus 2" of #TCO-026

' Ceramic Blanket) at the unexposed end of the conduit.

2.) Representative cable types and percentages of fills found at Millstone Nuclear Station, Unit 3.

3.) 8" thick #TCO-002 Medium Density Silicone Elastomer seal around the conduit installed flush with the slab's exposed surface.

4.) A conduit penetrating a steel sleeve opening.

, INFORMATION ONLY 1

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Test Report: #TR-193 Revision: 0

. Date: 03/25/35 Page: 2 of 15 SECTION "B" TEST SLAB:

The concrete test slab used for this test measured 48" x 4S" x 12" thick and was penetrated by four 12" diameter steel sleeves.

One of these four 12" diameter steel sleeves was used for the test. The test slab was designed and fabricated by PCA/CTL.

SECTION "C" PENETEATING ELEMENTS:

The 5" diameter by 60" long single piece conduit was located on center to the 12" diameter sleeve opening. The conduit extended 12" below and 40" above the firestop. The exposed end of the conduit (beneath the slab) was capped with a steel connector and plug,.

The conduit was filled with representative cable types and per-centages of fills found at Millstone Nuclear Power Station, Unit

3. The cable sizes tested were in accordance with ANI and IEEE requirements.

The conduit was filled to 55.25% of its cross-sectional area with approximately 1/3 power, 1/3 control, and 1/3 instrument cables. Power cables included both copper and aluminum conductors.

The cables extended approximately 12" below and not less than 36" above'the test slab (40" above the firestop).

Cable fills are found on page number 3 of this report.

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Test Report: #TR-193 Revision: 0

' Date: 03/25/65 Page: 3 of 15 SECTION "C" (Cont.)

PENETRATING ELEMENTS:

The cable fill of the conduit was as follows:

Man. Mark #:

Description:

Con.: Dia. Area: Qty.: Total

(") ("2) Area:

(power cables:)

Kerite NHP-18 1/C 500 MCM Cu 1.25 1.2271 1 1.2271 Eerite NHP 42 1/C 500 MCM Al 1.76 2.4326 1 2.4328 (total power cables: 3.6599) s (control cables:)

Eerite NHh-05 7/C #14 Cu 0.76 0.4536 1 0.4536 Okonite NHT-24 1/C #14 Cu 0.21 0.0346 1 0.0346 Okonite NHT-37 9/C #14 Cu 0.81 0.5153 1 0.5153 Okonite NHT 40 12/C #14 Cu 0.97 0.7389 1 0.7389 Okonite NHT-59 12/C #12 Cu 1.05 0.8659 1 0.86i9 Okonite NHT-66 2/C #8 Cu 0.72 0.4072 1 0.4072 Rockbestos None 5/C #12 (ALS) Cu 0.73 0.4185 1 0.4185 Brand Rex None 1/C #4 (SIS) Cu 0.40 0.1257 1 0.1257 (total control cables: 3.5597)

(instrument cables:)

BIW NHS-97 9/C #14 Cu 0.81 0.5153 1 0.5153 EIW NHQ-20 4/C #16 Cu 0.55 0.2376 1 0.2376 EIW NHQ-61 Triax Cu 0.55 0.2376 1 0.2376 BIW NHQ 49 Thermocouple Cu 0.50 0.1963 1 0.1963 BIW NHQ-12 3/C #16 Cu 0.50 0.1963 1 0.1963 (NUSCO) NHS-69 5/C #10 Cu 0.65 0.3318 1 0.3318 BIW NHQ-15 10 pr. #18 Cu 1.40 1.5394 1 1.5394 (RCI) NHQ 47 24/C #16 Cu 0.69 0.3739 1 0.3739 (total instrument cables: 3.6282)

(total all cables used: 10.8478) god *co*OM

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. Test Report: #TR-193 Revision: 0

' Date: 03/25/85 Page: 4 of 15 SECTION "D" SEAL INSTALLATION:

The #TCO-002 Medium Density Silicone Elastomer seals were installed using applicable portions of Transco Products Inc.'s installation and QC procedure PSQAP 9.10, Rev. 1 (Attachment "D").

The medium density silicone elastomer was installed 8" (max.)

deep in the unexposed end of the conduit and space around the conduit. Prior to sealing the conduit, 2" (max.) of #TCO-026 Ceramic Blanket (Johns-Manville's 4 lb. "Cerawool") was installed 8" below the unexposed end of the conduit and served as perma-

'nent damming which was left in place for the test.

Inhibition of cure occured at the cables / conduit seal interfaces and was left unrepaired for the test. TPI QC records for the seal installation work can be found in Attachment "E".

Prior to conducting the test, the unexposed cable ends were capped with Dow Corning #96-081 Silicone Adhesive.

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Test Report: #TR-193

, Revision: 0 Date: 03/25/S5 Fage: 5 of 15 SECTION "E" THERMOCOUPLES:

Thermocouples were counted to the slab to gather temperature data throughout the test. Temperatures were documented at five minute intervals for the first two hours and then at ten minute incre-rents for the remaining hour of the test.

Thermocouples 21-26, and 31 were tied with brass wire to their respective items at the seal / item interfaces. Seal surface thermocouples 30, 46, and 47 (along with sleeve thermocouple 48) were laid onto their respective surfaces and weighted for con-tact.

Thercocouples 32 through 45 were tied with brass wire directly to the conduit and were covered with 1" x 1" x 1/8" thick ceramic fiber pads. These theimocouples were mounted in groups of two (180 degrees apart from each other) starting flush with the surrounding seal and extending up every 6" to the top of the conduit.

Furnace atmosphere temperatures were monitored and documented in accordance with ASTM E-119 requirements. Three thermocouples are permanently counted inside of the furnace 12" below the specimen for this purpose.

Ther=ocouples were counted as follows:

T/C #:

Description:

Degree F at 3 Hrs.:

21 1/C #14 (SIS) cable: ...................... 161 22 5/C *12 (ALS) cable: ...................... 170 23 9/C #14 ( BIk') cable: ...................... 160 24 1/C #14 cable: ............................ T/C malfunction 25 10 pr. #18 cable: ......................... 148 26 Triax cable: .............................. 192

'30 Conduit seal surface: ..................... 144 31 Conduit (unexposed end): .................. 161 32 Conduit (0" fro: sur. seal surface): ...... 627 33 Conduit (0" from sur. seal surface): ...... 668 34 Conduit (6" fro = sur. seal surface): ...... 454 35 Conduit (6" fro = sur. seal surface): ...... 475 36 Conduit (12" from sur. seal surface): ..... 334 -

37 Conduit (12" from sur. seal surface): ..... 354 38 Conduit (18" from sur. seal surface): ..... 267 39 Conduit (18" from sur. seal surface): ..... 271 40 Conduit (24" from sur. seal surface): ..... 224 41 Conduit (24" from sur. seal surface): ..... 227 42 Conduit (30" from sur. seal surface): ..... 192 (cont.)

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Test Report: #TR-193 Revision: 0 Date: 03/25/E5 Page: 6 of 15 SECTION "E" (cont.)

THERMOCOUPLES:

T/C f:

Description:

Degrees F at 3 Hrs.:

43 Conduit (30" from sur. saal surface): ..... 196 44 Conduit (36" from sur. seal surface): ..... 165 45 Conduit (36" from sur. seal surface): ..... 171 46 Surrounding seal surface: ................. 303 47 Surrounding seal surface: ................. 269 48 Sleeve: ................................... IIS The thertocouples were placed and mapped by TPI QC, Thermocouple map can be found in Attacnment "C".

s SECTION "F" TEST:

The fire test was conducted in accordance eith the ASIM E-119 time / temperature curve for three hours. PCA/CTL perscnnel documented specimen thermocouple and furnace atmosphere tempera-tures and recorded test observations.

No smoke or other occurrences were noted during the test except for slight expansion (approximately 1/4") of the seal material beginning_at about one hour and ten minutes into the test.

The furnace draft pressure averaged -0.08" of water pressure throughout the test. Fdrnace drawings can te found in Attach-ment "B".

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Test Report: #TR-193 Revision: 0 Date: 03/25/S5 Page: 7 of 15 SECTION "G" HOSE STREAM TESTS:

After the conclusion of the fire test, the specimen was removed from the furnace and placed on its side for the hose stream test.

Although the specimen was required to be subjected to only the ANI hose stream test, two additional tests were conducted for informational purposes.

Each test was conducted for a minimum period of 24 seconds based on a 2.5 minute exposure for every 100 square feet of slab area.

Prior to conducting the test, TPI QC personnel verified the distance between the specimen and hose no::le. The tests were as follows:

1.) ANI: 75 psi hose stream delivered through a 1.5" diameter hose equipped with a fog nozzle set at a discharge angle of 15 degrees from a distance of 10 feet with a flow rate of 75 gpm.

2.) IEEE: Same as above except that the discharge angle is increased to 30 degrees.

3.) ASTM: 30 psi solid hose stream delivered through a 2.5" diameter hose equipped with a 1.125" tip set on a playpipe from a distance of 20 feet.

No water projected through the specimen's unexposed surface during any of the tests, ngoRWm0N M

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h e v i s i o r.: C, D e. ; e : 03/25/s5, Page f of 5 CR3573 - TRANSCO TR193 - 03/16/85 TEST COMMENTS 0:02:00 LIGHT SMOKE NOTED AT THE TOP OF FEN D PIPE 0:20:00 STEAM BEING BLOWN OFF AT THE YOP OF PEN D PIPE 0:25:00 SMOKE NO LONGER NOTED AT THE TOP OF PEN D PIPE 0: 45:00 BLACK LIQUID MATERIAL NOTED COMING FROM TOP OF PEN D AROUND THE PIPE 1:10:00 MINOR EXPANDSION HOTED IN SEAL IN PEN C HOSE STREAM TESTS:

HOSE STREAM NO WATER PROJECTED PEYOND THE UNEXEXPOSED SURFACE DURING ANI STREAM TEST FOR 24 SEC.

N3 WATER PROJECTED EEYOND THE UNEXEXPOSED SURFACE DURING IEEE-634 HOSE STREAM TEST FOR 24 SEC. ,

H3 WATER PROJECTED BEYOND THE UNEXEXPOSED SURFACE DURING ASTM E-119 HOSE S TREAM TEST FOR 24 SEC.

NJTES:

DtAFT RUN AT .06 NEC.

SMOKE CLASS L PIN A = TR196 PEN B = TR195 PIN C = TR193 PIN D = TR194 i

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s nev a sion: C, Date: v;/cp/ _, 3 race y c. 7 CR5573 - TRANSCO TR193 - 03/18/85 FURNACE RTMOSPHERE TEMPERATURE (DEC. F)

TEST TIME, FURNRCE ASTM E119 VARIATION FROM TEMP. TEMP. RSTM TEMP.

Hr: Min F F F 77 68 9 0:00 1000 1000 0 0:05 1375 1300 75 0:10 1441 1399 42 0:15 1429 1462 -33 0:20 1510 5 0:25 1515 '

1"50 8 0:30 1558 1593 1584 9 0:35 1605 1613 -8 0:40

' 1628 1638 -10 0: 45 1657 1661 -4 0:50 1675 1681 -6 0:55 1691 1700 -9 1:00 1712 1718 -6 1:05 1:10 1734 1735 -1 1745 1750 -5 1:15 1759 1765 -6 1:20 1:25 1767 1779 -12 1786 1792 -6 1:30 1795 1804 -9 1:35 1: 40 1804 1815 -11 1: 45 1813 1826 -13 1827 1835 -8 1:50 1:55 1642 1843 -1 1855 1850 5 2:00 1868 1862 6 2:10 2:20 1869 1875 -6 2:30 1886 1888 -2 1903 1900 3 ,

2: 40 2:50 1911 1912 -1 3:00 1922 1925 -3 RRER UNDER CURVE = 294597 DEG. F-MINUTES ARER UNDER ASTM E119 CURVE = 294600 DEG. F-MINUTES VARIRTION FROM RSTM CURVE = -0.0010  %

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E e v i s i o r. : O, Date: 03/2 /55, . age ;C cf 15 CR3973 - TRANSCO TR193 - 03/&B/83 UNEXPOSED TEMP. READINGS (DEG. F.)

TI'.S T T I ME , T/C NO.

20 21 22 23 24 Hi-: M i n 19 70 72 71 71 72 0:00 71 7 71 71 71 72 0:05 71 7- 71 71 71 72 0:10 71 73 72 71 71 0:15 71 0 75 74 72 69 0:20 72 1 72 79 77 72 67 0:25 73 73 84 81 74 65 0:30 75 75 89 86 75 63 0:35 77 77 93 90 76 61 0: 40 79 80 98 95 61 61 0: 45 83 64 102 99 85 57 0:50 6 s 88 105 103 SS 57 0:55 0 93 108 107 92 54 1:00 9 99 111 lie 96 53 1:05 9 105 114 114 100 52 1:10 105 112 117 117 103 52 1:15 109 118 120 120 107 50 1:20 114 124 123 124 110 46 1:25 119 131 125 127 113 51 1:30 12 138 127 130 116 47 1:35 1 8 130 133 120 44 1: 40 12 144 30 151 133 135 123 49 1: 45

• 158 134 138 126 46 1:50 141 164 137 141 129 43 1:55 145 171 139 143 131 45 2:00 150 159 82 142 148 137 42 2:10 13 146 153 142 41 2:20 166 22 150 158 147 41 2:30 174 21 154 162 151 41 2: 40 178 181 21 158 167 156 39 2:50 223 161 170 160 41 3:00 190 INFORMATION ONLY l

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F.e v i s i o r. : O, Late: 03/25/55, Fage ;; er 15 CR9973 - TRANSCO TR193 - 03/a8/85

• UNEXPOSED TEMP. READINGS (DEG. F.>

TEST TIME, T/C NC.

25 26 27 28 29 30 H:-: M i n 70 70 72 0:00 71 71 70f 72 71 0 70 0:05 71 7f 71 70 4 0:10 71 71 72 7 74 2 72 0:15 71 75 80 93 75 0:20 72 75 81 87 106 78 0:25 73 79 89 95 121 82 0:30 75 84 90 98 104 140 86 0:35 78 94 107 113 161 90 0*40 81 99 117 123 183 94 0: 45 84 103 126 133 198 97 0:50 87 106 135 142 204 100 0:55 91 109 145 152 217 103 1:00 94 112 153 60 229 105 1:05 97 115 161 1 241 108 1:10 100 103 119 167 1, 254  !!O 1:15 106 121 176 1 265 112 1:20 109 124 184 90 274 115 1:25 111 127 190 195 233 116 1:30 114 129 198 202 291 lie 1:35 116 131 203 208 299 120 1: 40 119 133 208 212 307 123 1: 45 135 214 217 313 123 1:50 121 123 137 218 224 321 126 1:55 125 147 223 229 328 127 2:00 129 168 237 235 344 129 2:10 134 176 246 246 58 132 2:20 137 181 25 255 73 136 2:30 141 186 2 261 37 138 2: 40 145 190 28 269 39 142 2:50 148 192 76 281 408 144

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O, Date: 03/25/55, Fage 12 cf 15 CRS$73 - TRANSCO TR193 - 03/18/85 UNEXPOSED TEMP. READINGS (DEG. F.)

T/C NO.

TEST TIME, ,

He: Min 31 32 33 34 35 36 72 70 70 71 71 71 0:00 71 98 111 79 83 74 0:05 71 156 178 112 122 91 0:10 73 222 248 160 175 124 0:15 77 275 294 200 2:4 149 0:20 82 311 329 228 241 168 0:25 67 342 361 252 264 184 0:30 93 368 389 271 285 197 0:35 97 388 410 287 299 207 0: 40 102 407 421 300 310 216 0: 45 106 s 423 437 309 319 221 0:50 0:55 109 435 450 318 328 227 112 447 464 327 339 234 1:00 1:e5 115 457 477 334 348 238 1:10 117 470 490 342 355 245 1:15 120 486 501 350 364 250 .

1:20 123 483 510 356 371 255 1:25 126 486 520 364 378 262 1:30 128 491 529 369 335 264 1:35 130 499 540 376 392 270 1: 40 133 509 550 383 399 275 1: 45 134 519 561 391 407 282 1:50 136 527 571 395 414 284 1:55 138 537 586 404 419 290 2:00 140 542 604 408 426 295 2:10 144 556 620 421 437 304 2:20 147 588 634 429 448 312 2:30 151 604 648 438 457 319 2: 40 155 618 661 447 466 325 2:50 158 624 664 452 470 331 1:00 161 627 666 454 475 334 INFORMATION OHL30 t

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Fevicidn: C, Date: C3/25/55, Fage 13 cf 1?

i CR5573 - TRrtHSCO TR193 - 03/16/e9 UNEXPOSED TEMP. READIN3S (DEG. F.)

TEST TIME. T/C NO.

37 38 39 40 41 42 Hr: Min 71 71 71 71 71 3:00 71 73 72 72 72 72 0:05 74 85 80 77 75 74 0:10 95 112 102 96 90 86 0:15 131 128 121 110 107 96 0:20 155 14B 135 122 121 106 0:25 173 153 147 133 131 116 0:30 189 156 140 137 122 0:35 204 161 167 164 144 143 127 0: 40 215 170 150 147 131 0: 45 223 0 230 180 176 153 151 134 0:50 237 194 100 155 154 136 0:55 244 189 185 159 158 140 1:00 251 193 190 162 161 143 1:05 258 199 194 165 165 145 1:10 264 201 199 169 168 149 1:15 1:20 270 206 203 173 172 152 275 211 208 176 175 155 1:25 1:30 281 209 212 179 179 158 1:35 286 212 216 182 182 159 1: 40 292 217 221 184 186 160 1: 45 ' 297 221 225 188 188 164 1:50 302 223 228 189 191 165 1:55 307 228 231 193 193 167 2:00 311 232 235 195 196 169 2:10 320 239 243 200 202 172 2:20 330 247 251 206 209 177 2:30 337 253 257 212 214 181 2: 40 344 258 263 216 219 185 2:50 349 263 268 221 223 189

3:00 354 267 271 224 227 192

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F. e v i E '. c r. : C, :ste: 03/2:fc5, face ; ;. er ,e CRS573 - TRANSCO TR193 - 03/18/e5 UNEXPOSED TEMP. READINGS (DEC. F.)

TEST TIME. T/C NC.

H-: Min d3 44 45 46 47 48 71 71 71 70 70 70 0:00 71 il 71 70 70 70 0:05 73 72 72 73 71 74 0:10 83 75 75 81 75 74 0:15 95 82 81 90 82 75 0:20 107 88 87 102 90 76 0:25 116 96 94 114 100 78 0:30 122 102 100 126 110 80 0:35 127 106 105 137 119 79 0: 40 131 110 110 150 128 81 0: 45 134 114 114 162 137 84 0:50 s 136 116 116 171 146 91 0:55 1:00 139 119 119 162 155 90 1:05 142 122 122 191 163 c5 145 124 125 199 170 96 1:10 1:15 149 126 128 20? 180 97 1:20 152 130 131 215 185 101 1:25 155 132 134 223 194 93 1:30 158 135 137 225 201 100 1:35 160 137 139 232 205 107 1: 40 162 139 141 241 214 98 1: 45 164 141 143 246 216 109 1:50 166 142 145 246 223 105 1:55 168 143 147 253 230 99 2:00 170 145 149 256 228 112 2:10 175 148 153 273 242 108 2:20 180 152 157 273 246 116 2:30 185 155 161 288 253 114 2: 40 189 159 165 293 261 109 2:50 193 163 168 301 266 117 3:00 196 165 171 303 269 118 gxOGlh w,  : 5 liiFOPJJKfl0N ONLY

Test Report: #TR-193 Revision: 0 Date: 03/25/55 Page: 15 of 15 SECTION "I" POST TEST OBSERVATIONS:

After the fire test, it was observed that seal's expored surface had expanded approximately 1" out of the penetration at the conduit. The conduit had burned away up to this point. No other damage was noted to the conduit beyond this point.

No damage was noted to the specimen on its unexposed surface.

The exposed surface of the seal had formed a hard char layer approximately 3" dcep into the seal.

The conduit seal and seal surrounding it passed both the fire and hose stream test' and met the performance requirements of ANI and IEEE 634 -

ON

TEST f:EPORT : OTR-193 CEvtSION; O DATE: 03/25/85 PAGE: 1OFI l

SLEEVE TEST PENETRATION A

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Attachment "B" Test Report: #TR-193 Reviaioa: 0 '

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TEST R E PORT . OT R - 195 C E VISION : O DATE: 03/25/83 P1GEIOF1 THERMOCOUPLE MAP 33,35,37,39, 41,43 8 45 24s ,30 25 46

,f 22 ,26

/

21 f D 23 \46 47 31 32,34,36,38, 40,42 8 44 s

TEST #TR-193 T/C" DESCRIPTION 21 SIS #4 22 ALS 23 9/C #14 24 1/C " 14 -

25 10 TW PR #18 26 TRIAX 30 SEAL SURFACE 31 CONDUlT 32 CONDUlT (O"UP FROM SUROUNDING SE AL) 33 a a a " a "

6" FROM BOTTOM ON CONDUlT

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44 45 36" o a a

't. J ' #

46 ANNULAR SEAL SURFACE 47 a a a 48 SLEEVE

H/,@'SCO I?HODUC i S INC. I m W ==

: = m m . v c: e i

No. PSQAP 9.10 ',

TITLE:

.

• SPECI A1. PROCESSES - SILICONE EI)STOER Page 1 of 8 l Revision 1 l

. l l

9 .1 PUF. POSE I

r This procedure defines the method of installing and inspecting 5 Silicone Elastomer Seals.

. 9.2 REFEF.ENCE S 7 ' '

100FF30 Appendix B

[ Penetration Seal Quality Assurance Program Manual PSQAP 8.0, 9.0, 10.0, 10.1, 15.0 5 9.3 FROCEDURE

. 9.3.1 'Tne Transco Field Superintendent and qualified craf t pe rs onnel

{ are responsible for the installation of Silicone Elastomer g I caterials in accordance with this procedure. Quality Control e Personnel are responsible for inspection activities per this

fy f.

7 4,f 9.3.2 procedure.

Prior to installing the seal caterials, the penetration shall i have been identified per PSQAP 8.0 and the datz!ng operations

[ g(. shall have b en corpleted per PSQAP.9.0.

9.3.3 The Transco Field Superintendent / Designee shall obt ain a cop)

I of the " Field Takeof f, Installation, and Inspection Record" 3 (Figure 1) f roc Quality Control uhich will indicate those

-r penetrations which are released for final sealing operations.

- This form is norcally obtained at the start of each work day or shift. Penetrations shall not be sealed unless release is y4r indicated on the form. An al t e rna t e release cethod/f orm c.ay be used if found to le more ef ficient in issuing releases to

- production, but all data required on the Tield Takeof f, Instal-lation, and Inspection Record form shall be co:pleted.

~

i 9.3.4 For traceability purposes, the caterial supplier has assigned

'h j g, unique nutbers for each lot of material c.anufactured. Each container of silicone, both parts A and B, is to have a lot nutber cicarly printed on it and a green stripe indicating it is

,2N 4}[, acceptable f or production use (per PSQAP 10.0). Cont a i r.e r a A a without a lot number and/or a green paint stripe are not to ic'

- used,'are to be segregated fro: acceptable caterials, and the 2 Quality Control Manager is to k notified.

• i. .

d 9.3.5 Installation of Silicone Elastomer can le accomplished by

$ . . utilizing dispensing equipment, or eay be hand mixed and applied

, as specific conditions dictate. *

,v '

9.3.6 Prior to installation of the Stitcone Elastomer, the field Installer shall complete the top portion of the "Tield Data Sheet" (rigure 2) indicating, among other information, the l

T,i Y

INFORMATION ONLY

____-_________-___-___O l

.. a

! HAI\!SCO PHUDUCTS INC.Fevu

$: c u NU Are Oc go, psgro 9.10

.T IT LE :

Page 2 of 8 i . ' SPECI A1. PROCESSES - SIL.1 CONE ELASTOKER Resis!on 1 1

g the batch number assigned to the Silicone Elastocer. A batch is defined as each time the material holding tanks are refilled with ma t eri al. Batch nuchers are assiE ned beginning with *00l* an!

{ continuing consecutively. Any time a batch remains in the

" the holding tanks at the end of a shif t or the end of the work day and the holding tanks are not refilled when work resuces, i

then a unique and consecutive batch letter shall be assignedletter j to the end of the existing batch number beginning with the "A*.

Example:

2 EV118009 - 005 i

5 EV118009 a 005A EV118009 - }!aterial supplier lot number 005 - The 5th batch used f rom lot EV118009 j ,

A = A stop in production and resueption without j

a caterial refill. ,

i h.Q

• 7 During the installation operations, all penetration numbers .

{. h

%j which receive a specific batch of Silicone Elastomer shall be 4 i

~

listed on the Field Data Sheet.

? .

I' ."l 4..

• In some cases, equipment cay be used which attaches directly to l- ~8 h'l

• the material containers instead of having " holding tanks". In these cases, the canufacturer supplied lot nueber alone is all l,

l f.

.- that, is required. .

s 9.3.7 Sacples of the Silicone Elasto=er are taken to verify that the

• - caterial is suitable for installation, j- -

n . .

a) Two samples are cade in two disposable saeple cups supplied by Quality Control Personnel. These two sa:ples shall be l

made for each lot / batch of Silicone Elasto:er used in the i

dispensing unit (also for lettered batches). These two

~

i saeple cups cust be filled suf ficiently to assure that cured

samples are at or above the top of the sa

ple cups.

} *

q) t b) The lot / batch number, insta11er's initials, and date shall be af fixed on the two sample cups by the installer. These two

, h * . samples are for Quality Control and shall be prop'erly stored until turned over to Quality Control Personnel, normally at O the end of the shift. .

I '* c) The field installer shall evaluate one of these saeples prio r ga s. to installation activities. This sample shall be flush with sample cup top. Using a gram scale, weigh the sample to the {

l nearest 1/10 of a gram. This weight is recorded on the Field y Data Sheet and should be within the following acceptable lJg

-+q

)

tolerancest 70-95 lbs. per cubic foot, unless othersise specified.

l M INFORMATION ONLY .

~

$ $$ L.??E .$.E -

No. PSQtf 9.10 I ,1 IT LE  : AE PDO SSES - SIL1 CON 6 ELa.STOMER S.*ECI Page 3 of 8 Revision 1 Should the sacple weight not y ac ceptable , Quality Cnotr ol Personnel are to be contacted icrediately and vori shall not pro-ceed.

2 2 9.3.8 During Silicone Elastomer installation, the QC Inspector shall perfort in process inspections at random stages of the instal-lation process. During these inspections , the QC Inspector shall j

observe specific installation procedures such as cicanliness,

- spreading of electrical cables, proper use of the Field Data Sheet, etc.. These inspections shall be docueented on the applicable Field Data Sheet using the " REMARKS ~ colutn to 2

indicate any ins t ructions for re processing of a penetration to 5 correct in process deficiencies. Upon satisf actory completion of required re-processing, the QC Inspector shall initial and date the rc processing noted previously on the Field Data Sheet as j' being complete.

} 9.3.9 Installation of the Silicone Elastocer shall be accomplished as follows:

=. %~ .-.

", 4 o a) Prior to installation, individual silicone cocponents shall i

be thoroughly cixed using a drill cotor and cixing paddle.

( N! .

b) Tne individual co=ponents, A and B, shall now k nixed i$

~

3 l. .

together in one container at a ratio of 1:1 by weight or i . voluce using a heavy duty mixer motor and mixing head for 3 approxicately two cinutes. If a dispensing unit is used, the A and E cocponents are not cixed together'but are poured into separate holding tanks in the dispensing unit, or are pucped y . directly from the caterial containers, as applicable.

o c) If dispensing units are used, consult the applicable,

instruction canuals as required - PROPRIETARY.

d) Sacples shall new be prepared and evaluated per 9.3.7 above.

e) Install the Silicone Elastocer into the penetration by using

$ the dispensing unit, hand pouring or pucping as the field

[ ,5 condition dictates. VATCli FOR LE/JJ.0E!

i

~

i" j f) Installed Silicone Elastomer shall be allowed to cure for a tinicum of twenty-f our hours at which tice all dae.nicg shall

,,h - be recoved, as applicable, and excess caterial recoved and L. -.

the penetration seal tricced flush with wall or floor ew a .. surface.

4

', g) General good housekeeping shall be caintained at all tices.

Alterations for additions to or deletions f rom previously sealed kh 9 .3.10 penetrations can be cade by carefully cutting out enough Stif cone Elastomer to permit the addition or deletion, or by using core boring equipment if space allows. In either case, extreme

~

s 1q INFOhATION ONLY

~

[ H/\i Q L U i i R>L/ U v t O tis v.: ,y13 en: c, p3 , _ _ - .

c:f;5jg , :3ye ef No. PSQAP 9.10 l ,T IT L E : Page 4 of E l . SPECI AL PF.DCESSES - SIL1 CONE ELASTOER Revision 1 1

, \

l caution cast be exercised wher. caking alt e rations to avoid da: age I

to any penetrating ite=s (i.e.; cables, ins t r u:ent tubi ng , etc .) c :

• to surrounding seal material. The added openleg should be made o straight through the seal and made only slightly larger than the item to be added. Deletions should be carefully pulled out and only a r.inical acount of Silicone Elastomer should be recoved in j order to facilitate the deletion.

9.3.11 Minor repairs are permissible by removing a sea 11 portion (l~-2-)

of the surrounding Silicone Elastomer to provide a good, clean Prepare, i

surface for the new Silicone Elastomer to bond to.

sa pic, and seal the altered area following the inst r uc? Ions l

2 outlined in 9.3.6 through 9.3.9 above.

~j 9.3.12- Per=anent identification of cocpleted penetration seals is  !

perf orced by production personnel and cust be doce prior to final inspection by Quality Control Personnel. The cethod for identifi-j t i; l J-{q cation cay be accocplished by any of the following cathods or as gj

-, specified by the cer to=er: ,.

a) Ea'nd printed next to the opening using a vaterproof

} flow carker.

i _-

3 j .

b) Stenciled next to the opening using paint applied by brush, f j

roll, or spray. l I

a c) Steel tags attached with adhesive next to the opening. -

t{l * . 9.3.13 Quality Control Personnel shall perform final inspection of the -

g co:pleted seals when released by production for inspection

' activities. 'Itecs to be considered during final inspection shall y ,* *

.be a minicut of the following: j l ..

i

.. q a) Te:p'orary da= dog, where applicable , is totally removed l ,

• - ' and disposed of. j

! r, b) Te=porary supports, where applicable, such as duct tape, il k4 .

vood shl=s, etc. , have been ~ recoved and disposed of.~

Seals are neatly tritzed where applicable to floor, vall,

( . c) ceiling, and penetration surfaces. ,l

'4-

?

.h' j d) Penetration fill is sufficient to completely fill or overfill !

.. the penetration to the specified fill depth, ard no visible  ;

. og *

, voids or openings exist. Seal caterial is cured (no wet or r

tacky caterial is present).

i v;p e) The proper materials were used for the sealing, daesing, and identification of the penetration.

@g sp JNFOllMAT10N OnLY ,

1,H/Wbt,U thiUl >UL. I b in.. sevic ron: h, ate. k/h/es,r ace .- .-_.

s o, s

( .-

TITLE: So. P51*J 9.10 Pa r, 5 of 6 SPEC 1 AL FIXES 5T.S - 5111 COW Fi* m "r' ]

Fevistoc f) Pe r c.a n e nt identification it. affi w.' ntar the penc: ration a n:'

is correct and is acceptably attached.

1 .

2 g) k'ork loca t ico is clean.

in the I h) The dispe:s f on of Silicone Elastocer around the cables penetration shall be inspected. If the Silicone Elastocer is

{~ not dispersed htveen the cables in a penetration, the seal shall be repaired per Section 9.3.11.

9.3.14 Quality Control Personnel shall inspec: the sarples of Silicone o Elastoner supplied to the by pr oduction (0.3.7b). One sa:ple shall F: cut open and cu rined for:

f 'a) Color - Dark grey to black (this ray vary based on additives j ~, used) 1 iQ b) Cell structure - Unifort and free frc elongated cells

" -d.): s . .

I4 .

c) Texture - Solid, set, fire, with no tackiness.

i i

[ l. Acceptable co:parison sa:ples shall be available fe r the Quality Control Inspector to ref erence for an acceptable Silicone Elas-

'I

'i i . ) toter product. This inspection shall be docucented on the QC Sa:ple It'spection Eecord (Figure 3). The second sa:ple shall be f

./ 3 flush vith the top of the sample cup and veighed on the gra:

scales. The sa=ple density shall then te de:ercined and docu ented per PSQAP 10.1.

~

9.3.15 Upon acceptance of the co:pleted Silicone Elasto:er seal and

,g testing sa ples, the final inspection activity (per this procedure and 10.1) is docutented on the Field Takeof f, Insts.lation, and Inspection Record indicating, among other l

d- A infor:ation, the date accepted and the inspector's initials. If the inspection results in a rejection st;i:us, a Report of 3 Fonconforcance is issued and the penetration is tagged with a  ;

h{,

"Rej e c t" tag p. r PSQAf 1$,0. The Field Takeof f, Installation, y and Inspec:f on Record is not initia11ed until all nonconf or-i J J cances have been resolved and corrective action cocpie:ed and 4 5 ,

accepted. ,

e 1

.4 l Q DOCD'.:.NTS / P.EC0 F35 ,

% 3 3 7 & 9.4.1 The nonpercanent documents applicable to this procedure are the

" "Tield Data Sheet' and the "QS Sa:ple Inspection Record".

I l

., 9.4.2 The permanent document applicable to this p rocedure is the 'Tield k,, .akeoff, Installation, and Inspection Eecord".

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Test Report: #TR-193 J Revision: 0 Date: 03/25/85 Fage: 1 of 12

[

] ATTACHMENT "E" j QC INSPECTION RECORDS:

1

! The follo' wing pages consist of the Quality Control records for this test. These pages are:

l a.) Receiving Inspection Reports: ...................... 2 pages i b.) Field Take-Off, Installation, and Inspection Report: 1 page c.) Batch Sample Density Measurement Records: .......... I page j d.) Field Data Sheets: ................................. I page e.) QC Sample Inspection Records: ...................... I page

f.) Handwritten notes regarding specimen fabrication, l cable loadings, etc.: .............................. 2 pages i g.) Mapping of thermocouple layout: .................... 3 pages 1

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