Latest revision as of 20:50, 11 March 2020

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Attachment to 8/20/10 Email from Bbrrct - Data Provided by Sfwmd That Was Collected by FPL for Uprate of Units 3 & 4
	ML102350005
Person / Time
Site:	Turkey Point
Issue date:	08/02/2010
From:	Atkins A; Testamerica Labs
To:	Foster S; Florida Power & Light Co, Office of New Reactors
	Kugler A, NRO/DSER/RAP2, 415-2828
References
	Job Number 660-35805-1
	Download: ML102350005 (144)
	v • d • e

ANALYTICAL REPORT Job Number: 660-35805-1 SDG Number: 35805 Job

Description:

FPL Turkey Point Analytical Services For:

Florida Power & Light Company Technical Services - PGD Environmental Water Compliance/Permitting 700 Universe Blvd (JES/JB)

Juno Beach, FL 33408 Attention: Ms. Stacy Foster Approved for release.

Amy Atkins Project Manager I 8/2/2010 3:40 PM Amy Atkins Project Manager I amy.atkins@testamericainc.com 08/02/2010 cc: Ms. Sharon Ewe Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282; TestAmerica Tallahassee E81005; TestAmerica Savannah E87052 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report.

The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 43

Job Narrative 660-35805-1 Receipt All samples were received in good condition within temperature requirements.

Metals Method 200.7: The following sample was received unpreserved and was preserved upon receipt to the laboratory: 061610-TPGW-5D (660-35805-1). Initial pH was adjusted to <2 with HNO3 lot 2MER0014. Regulatory documents require a 24-hour waiting period from the time of the addition of the acid preservative to the time of digestion.

Method 200.7 Rev 4.4: The following sample was diluted due to the nature of the sample matrix: 061610-TPGW-5D (660-35805-1).

Elevated reporting limits (RLs) are provided.

Method 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for Calcium in batch 96355 were outside control limits with the sample greater than 4x the spike level. The associated laboratory control sample (LCS) recovery met acceptance criteria.

General Chemistry DOC samples were field filtered and preserved in the lab.

Method 300.0: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 96178 were outside control limits for Chloride.

The associated laboratory control sample (LCS) recovery met acceptance criteria.

Method SM 4500 S2 F: Insufficient sample volume was provided to perform batch matrix spike/matrix spike duplicate (MS/MSD) associated with batch 96052 The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.

Page 2 of 43

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35805-1 061610-TPGW-5D Field pH 6.85 SU Field Sampling Field Temperature 24.69 Degrees C Field Sampling Oxygen, Dissolved 4.0 mg/L Field Sampling Specific Conductance 29980 umhos/cm Field Sampling Turbidity 0.46 NTU Field Sampling Bromide 40 5.0 mg/L 300.0 Chloride 12000 500 mg/L 300.0 Sulfate 1300 50 mg/L 300.0 Alkalinity 220 1.0 mg/L SM 2320B Total Dissolved Solids 21000 250 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 55 1.0 mg/L 9060 Total Recoverable Barium 220 100 ug/L 200.7 Rev 4.4 Iron 1600 500 ug/L 200.7 Rev 4.4 Boron 1100 500 ug/L 6010B Calcium 600 5.0 mg/L 6010B Potassium 210 10 mg/L 6010B Strontium 7800 50 ug/L 6010B Magnesium 750 0.80 mg/L 6010B Sodium 6500 100 mg/L 6010B TestAmerica Tampa Page 3 of 43

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35805-2 061610-TPGW-5M Field pH 6.92 SU Field Sampling Field Temperature 24.61 Degrees C Field Sampling Oxygen, Dissolved 1.1 mg/L Field Sampling Specific Conductance 21350 umhos/cm Field Sampling Turbidity 0.16 NTU Field Sampling Bromide 30 5.0 mg/L 300.0 Chloride 8900 500 mg/L 300.0 Sulfate 860 50 mg/L 300.0 Alkalinity 210 1.0 mg/L SM 2320B Total Dissolved Solids 17000 250 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 54 1.0 mg/L 9060 Total Recoverable Barium 260 10 ug/L 200.7 Rev 4.4 Iron 5400 50 ug/L 200.7 Rev 4.4 Boron 580 500 ug/L 6010B Calcium 570 5.0 mg/L 6010B Potassium 120 10 mg/L 6010B Strontium 6800 50 ug/L 6010B Magnesium 540 0.80 mg/L 6010B Sodium 4900 100 mg/L 6010B TestAmerica Tampa Page 4 of 43

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35805-3 061610-TPGW-5S Field pH 7.47 SU Field Sampling Field Temperature 25.80 Degrees C Field Sampling Oxygen, Dissolved 1.2 mg/L Field Sampling Specific Conductance 958 umhos/cm Field Sampling Turbidity 5.27 NTU Field Sampling Bromide 0.74 0.050 mg/L 300.0 Chloride 210 5.0 mg/L 300.0 Fluoride 0.051 0.050 mg/L 300.0 Sulfate 19 0.50 mg/L 300.0 Alkalinity 240 1.0 mg/L SM 2320B Total Dissolved Solids 690 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 62 1.0 mg/L 9060 Total Recoverable Barium 40 10 ug/L 200.7 Rev 4.4 Iron 560 50 ug/L 200.7 Rev 4.4 Boron 54 50 ug/L 6010B Calcium 130 0.50 mg/L 6010B Potassium 7.7 1.0 mg/L 6010B Strontium 1300 5.0 ug/L 6010B Magnesium 8.4 0.080 mg/L 6010B Sodium 110 0.50 mg/L 6010B TestAmerica Tampa Page 5 of 43

METHOD

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Description Lab Location Method Preparation Method Matrix: Water Metals (ICP) TAL TAL EPA 200.7 Rev 4.4 Preparation, Total Recoverable Metals TAL TAL EPA 200.7 Metals (ICP) TAL TAM SW846 6010B Preparation, Total Recoverable or Dissolved Metals TAL TAM SW846 3005A Anions, Ion Chromatography TAL TAM MCAWW 300.0 Carbon, Dissolved and Dissolved Inorganic TAL SAV SW846 9060 Sample Filtration, Field TAL SAV FIELD_FLTRD Alkalinity TAL TAM SM SM 2320B Solids, Total Dissolved (TDS) TAL TAM SM SM 2540C Sulfide, Total TAL TAM SM SM 4500 S2 F Field Sampling TAL TAM EPA Field Sampling Lab

References:

TAL SAV = TestAmerica Savannah TAL TAL = TestAmerica Tallahassee TAL TAM = TestAmerica Tampa Method

References:

EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa Page 6 of 43

METHOD / ANALYST

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Analyst Analyst ID EPA 200.7 Rev 4.4 Neal, Amanda J AJN EPA 200.7 Rev 4.4 Wallace, Tiffany B TBW SW846 6010B Fox, Greg GF EPA Field Sampling Sampler, Field FS MCAWW 300.0 Sengsouvanna, Dom DS SW846 9060 Blackshear, Kim KB SM SM 2320B Steward, Tiffany TS SM SM 2540C Oonnoonny, Thomas TO SM SM 4500 S2 F Mostafavifar, Efe EM TestAmerica Tampa Page 7 of 43

SAMPLE

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Date/Time Date/Time Lab Sample ID Client Sample ID Client Matrix Sampled Received 660-35805-1 061610-TPGW-5D Water 06/16/2010 1336 06/17/2010 0840 660-35805-2 061610-TPGW-5M Water 06/16/2010 1445 06/17/2010 0840 660-35805-3 061610-TPGW-5S Water 06/16/2010 1230 06/17/2010 0840 TestAmerica Tampa Page 8 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Client Sample ID: 061610-TPGW-5D Lab Sample ID: 660-35805-1 Date Sampled: 06/16/2010 1336 Client Matrix: Water Date Received: 06/17/2010 0840 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70408 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70149 Lab File ID: 062910.csv Dilution: 10 Initial Weight/Volume: 50 mL Date Analyzed: 06/29/2010 0856 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000 Analyte Result (ug/L) Qualifier MDL PQL Barium 220 9.6 100 Iron 1600 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-96428 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96355 Lab File ID: 10F25A Dilution: 10 Initial Weight/Volume: 50 mL Date Analyzed: 06/25/2010 0909 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Result (mg/L) Qualifier MDL PQL Calcium 600 1.0 5.0 Potassium 210 1.9 10 Magnesium 750 0.20 0.80 Analyte Result (ug/L) Qualifier MDL PQL Boron 1100 100 500 Strontium 7800 10 50 Method: 6010B Analysis Batch: 660-96428 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96355 Lab File ID: 10F25A Dilution: 200 Initial Weight/Volume: 50 mL Date Analyzed: 06/25/2010 1025 Run Type: DL Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Result (mg/L) Qualifier MDL PQL Sodium 6500 62 100 TestAmerica Tampa Page 9 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Client Sample ID: 061610-TPGW-5M Lab Sample ID: 660-35805-2 Date Sampled: 06/16/2010 1445 Client Matrix: Water Date Received: 06/17/2010 0840 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70371 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70149 Lab File ID: N/A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 06/28/2010 1320 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000 Analyte Result (ug/L) Qualifier MDL PQL Barium 260 0.96 10 Iron 5400 4.6 50 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-96428 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96355 Lab File ID: 10F25A Dilution: 10 Initial Weight/Volume: 50 mL Date Analyzed: 06/25/2010 0915 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Result (mg/L) Qualifier MDL PQL Calcium 570 1.0 5.0 Potassium 120 1.9 10 Magnesium 540 0.20 0.80 Analyte Result (ug/L) Qualifier MDL PQL Boron 580 100 500 Strontium 6800 10 50 Method: 6010B Analysis Batch: 660-96428 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96355 Lab File ID: 10F25A Dilution: 200 Initial Weight/Volume: 50 mL Date Analyzed: 06/25/2010 1031 Run Type: DL Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Result (mg/L) Qualifier MDL PQL Sodium 4900 62 100 TestAmerica Tampa Page 10 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Client Sample ID: 061610-TPGW-5S Lab Sample ID: 660-35805-3 Date Sampled: 06/16/2010 1230 Client Matrix: Water Date Received: 06/17/2010 0840 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70371 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70149 Lab File ID: N/A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 06/28/2010 1325 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000 Analyte Result (ug/L) Qualifier MDL PQL Barium 40 0.96 10 Iron 560 4.6 50 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-96375 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1610 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Result (mg/L) Qualifier MDL PQL Calcium 130 0.10 0.50 Potassium 7.7 0.19 1.0 Magnesium 8.4 0.020 0.080 Sodium 110 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 54 10 50 Strontium 1300 1.0 5.0 TestAmerica Tampa Page 11 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 General Chemistry Client Sample ID: 061610-TPGW-5D Lab Sample ID: 660-35805-1 Date Sampled: 06/16/2010 1336 Client Matrix: Water Date Received: 06/17/2010 0840 Analyte Result Qual Units MDL PQL Dil Method Bromide 40 mg/L 2.7 5.0 100 300.0 Analysis Batch: 660-96235 Date Analyzed: 06/21/2010 2122 Chloride 12000 mg/L 200 500 1000 300.0 Analysis Batch: 660-96392 Date Analyzed: 06/23/2010 2159 Fluoride 0.040 U mg/L 0.040 0.10 2.0 300.0 Analysis Batch: 660-96606 Date Analyzed: 06/29/2010 2107 Sulfate 1300 mg/L 20 50 100 300.0 Analysis Batch: 660-96235 Date Analyzed: 06/21/2010 2122 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 55 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-172887 Date Analyzed: 06/28/2010 1127 Alkalinity 220 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1355 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1355 Total Dissolved Solids 21000 mg/L 250 250 1.0 SM 2540C Analysis Batch: 660-96110 Date Analyzed: 06/18/2010 1330 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96052 Date Analyzed: 06/17/2010 1640 TestAmerica Tampa Page 12 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 General Chemistry Client Sample ID: 061610-TPGW-5M Lab Sample ID: 660-35805-2 Date Sampled: 06/16/2010 1445 Client Matrix: Water Date Received: 06/17/2010 0840 Analyte Result Qual Units MDL PQL Dil Method Bromide 30 mg/L 2.7 5.0 100 300.0 Analysis Batch: 660-96235 Date Analyzed: 06/21/2010 2144 Chloride 8900 mg/L 200 500 1000 300.0 Analysis Batch: 660-96392 Date Analyzed: 06/23/2010 2220 Fluoride 0.040 U mg/L 0.040 0.10 2.0 300.0 Analysis Batch: 660-96606 Date Analyzed: 06/29/2010 2125 Sulfate 860 mg/L 20 50 100 300.0 Analysis Batch: 660-96235 Date Analyzed: 06/21/2010 2144 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 54 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-172887 Date Analyzed: 06/28/2010 1127 Alkalinity 210 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1408 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1408 Total Dissolved Solids 17000 mg/L 250 250 1.0 SM 2540C Analysis Batch: 660-96110 Date Analyzed: 06/18/2010 1330 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96052 Date Analyzed: 06/17/2010 1640 TestAmerica Tampa Page 13 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 General Chemistry Client Sample ID: 061610-TPGW-5S Lab Sample ID: 660-35805-3 Date Sampled: 06/16/2010 1230 Client Matrix: Water Date Received: 06/17/2010 0840 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.74 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96178 Date Analyzed: 06/19/2010 0958 Chloride 210 mg/L 2.0 5.0 10 300.0 Analysis Batch: 660-96101 Date Analyzed: 06/17/2010 1919 Fluoride 0.051 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96178 Date Analyzed: 06/19/2010 0958 Sulfate 19 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96178 Date Analyzed: 06/19/2010 0958 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 62 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-172887 Date Analyzed: 06/28/2010 1127 Alkalinity 240 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1414 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1414 Total Dissolved Solids 690 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96110 Date Analyzed: 06/18/2010 1331 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96052 Date Analyzed: 06/17/2010 1640 TestAmerica Tampa Page 14 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Field Service / Mobile Lab Client Sample ID: 061610-TPGW-5D Lab Sample ID: 660-35805-1 Date Sampled: 06/16/2010 1336 Client Matrix: Water Date Received: 06/17/2010 0840 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 6.85 SU 1.0 Field 660-97058 06/16/2010 1336 Sampling Field Temperature 24.69 Degrees C 1.0 Field 660-97058 06/16/2010 1336 Sampling Oxygen, Dissolved 4.0 mg/L 1.0 Field 660-97058 06/16/2010 1336 Sampling Specific Conductance 29980 umhos/cm 1.0 Field 660-97058 06/16/2010 1336 Sampling Turbidity 0.46 NTU 1.0 Field 660-97058 06/16/2010 1336 Sampling TestAmerica Tampa Page 15 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Field Service / Mobile Lab Client Sample ID: 061610-TPGW-5M Lab Sample ID: 660-35805-2 Date Sampled: 06/16/2010 1445 Client Matrix: Water Date Received: 06/17/2010 0840 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 6.92 SU 1.0 Field 660-97058 06/16/2010 1445 Sampling Field Temperature 24.61 Degrees C 1.0 Field 660-97058 06/16/2010 1445 Sampling Oxygen, Dissolved 1.1 mg/L 1.0 Field 660-97058 06/16/2010 1445 Sampling Specific Conductance 21350 umhos/cm 1.0 Field 660-97058 06/16/2010 1445 Sampling Turbidity 0.16 NTU 1.0 Field 660-97058 06/16/2010 1445 Sampling TestAmerica Tampa Page 16 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Field Service / Mobile Lab Client Sample ID: 061610-TPGW-5S Lab Sample ID: 660-35805-3 Date Sampled: 06/16/2010 1230 Client Matrix: Water Date Received: 06/17/2010 0840 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 7.47 SU 1.0 Field 660-97058 06/16/2010 1230 Sampling Field Temperature 25.80 Degrees C 1.0 Field 660-97058 06/16/2010 1230 Sampling Oxygen, Dissolved 1.2 mg/L 1.0 Field 660-97058 06/16/2010 1230 Sampling Specific Conductance 958 umhos/cm 1.0 Field 660-97058 06/16/2010 1230 Sampling Turbidity 5.27 NTU 1.0 Field 660-97058 06/16/2010 1230 Sampling TestAmerica Tampa Page 17 of 43

DATA REPORTING QUALIFIERS Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Lab Section Qualifier Description Metals J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

U Indicates that the compound was analyzed for but not detected.

I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

General Chemistry J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

U Indicates that the compound was analyzed for but not detected.

TestAmerica Tampa Page 18 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 640-70149 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable Lab Sample ID: MB 640-70149/1-A Analysis Batch: 640-70371 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70149 Lab File ID: N/A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 06/28/2010 1149 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000 Analyte Result Qual MDL PQL Barium 0.96 U 0.96 10 Iron 4.6 U 4.6 50 Lab Control Sample/ Method: 200.7 Rev 4.4 Lab Control Sample Duplicate Recovery Report - Batch: 640-70149 Preparation: 200.7 Total Recoverable LCS Lab Sample ID: LCS 640-70149/2-A Analysis Batch: 640-70371 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70149 Lab File ID: N/A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 06/28/2010 1154 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000 LCSD Lab Sample ID: LCSD 640-70149/3-A Analysis Batch: 640-70371 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70149 Lab File ID: N/A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 06/28/2010 1159 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000

% Rec.

Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual Barium 98 100 85 - 115 2 20 Iron 97 98 85 - 115 2 20 TestAmerica Tampa Page 19 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Matrix Spike/ Method: 200.7 Rev 4.4 Matrix Spike Duplicate Recovery Report - Batch: 640-70149 Preparation: 200.7 Total Recoverable MS Lab Sample ID: 660-35826-G-1-B MS Analysis Batch: 640-70408 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70149 Lab File ID: 062910.csv Dilution: 10 Initial Weight/Volume: 50 mL Date Analyzed: 06/29/2010 0805 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000 MSD Lab Sample ID: 660-35826-G-1-C MSD Analysis Batch: 640-70408 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70149 Lab File ID: 062910.csv Dilution: 10 Initial Weight/Volume: 50 mL Date Analyzed: 06/29/2010 0810 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Barium 106 108 70 - 130 1 20 Iron 89 90 70 - 130 1 20 Duplicate - Batch: 640-70149 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable Lab Sample ID: 660-35826-G-2-B DU Analysis Batch: 640-70408 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70149 Lab File ID: 062910.csv Dilution: 10 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 06/29/2010 0828 Final Weight/Volume: 50 mL Date Prepared: 06/22/2010 1000 Analyte Sample Result/Qual Result RPD Limit Qual Barium 110 85.5 26 20 I J3 Iron 1700 1690 1 20 TestAmerica Tampa Page 20 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96355 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: MB 660-96355/1-A Analysis Batch: 660-96375 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1421 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Result Qual MDL PQL Calcium 0.10 U 0.10 0.50 Potassium 0.19 U 0.19 1.0 Magnesium 0.020 U 0.020 0.080 Sodium 0.31 U 0.31 0.50 Method Blank - Batch: 660-96355 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: MB 660-96355/1-A Analysis Batch: 660-96375 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1421 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Result Qual MDL PQL Boron 10 U 10 50 Strontium 1.0 U 1.0 5.0 TestAmerica Tampa Page 21 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Lab Control Sample - Batch: 660-96355 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: LCS 660-96355/2-A Analysis Batch: 660-96375 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1427 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Spike Amount Result % Rec. Limit Qual Calcium 1.00 1.01 101 75 - 125 Potassium 10.0 10.3 103 75 - 125 Magnesium 1.00 1.01 101 75 - 125 Sodium 10.0 10.2 102 75 - 125 Lab Control Sample - Batch: 660-96355 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: LCS 660-96355/2-A Analysis Batch: 660-96375 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1427 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 Analyte Spike Amount Result % Rec. Limit Qual Boron 1000 1010 101 75 - 125 Strontium 1000 1090 109 75 - 125 TestAmerica Tampa Page 22 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Matrix Spike/ Method: 6010B Matrix Spike Duplicate Recovery Report - Batch: 660-96355 Preparation: 3005A Total Recoverable MS Lab Sample ID: 660-35887-E-1-B MS Analysis Batch: 660-96375 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1446 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 MSD Lab Sample ID: 660-35887-E-1-C MSD Analysis Batch: 660-96375 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1452 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Calcium 246 233 75 - 125 0 20 J3 J3 Potassium 122 124 75 - 125 1 20 Magnesium 108 110 75 - 125 0 20 Sodium 111 101 75 - 125 1 20 Matrix Spike/ Method: 6010B Matrix Spike Duplicate Recovery Report - Batch: 660-96355 Preparation: 3005A Total Recoverable MS Lab Sample ID: 660-35887-E-1-B MS Analysis Batch: 660-96375 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1446 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908 MSD Lab Sample ID: 660-35887-E-1-C MSD Analysis Batch: 660-96375 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96355 Lab File ID: 10F24A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 06/24/2010 1452 Final Weight/Volume: 50 mL Date Prepared: 06/24/2010 0908

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Boron 105 105 75 - 125 1 20 Strontium 108 110 75 - 125 1 20 TestAmerica Tampa Page 23 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96101 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-96101/3 Analysis Batch: 660-96101 Instrument ID: DIONEX 1 Client Matrix: Water Prep Batch: N/A Lab File ID: 11.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/17/2010 1531 Final Weight/Volume: 5 mL Date Prepared: N/A Analyte Result Qual MDL PQL Chloride 0.20 U 0.20 0.50 Lab Control Sample - Batch: 660-96101 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-96101/4 Analysis Batch: 660-96101 Instrument ID: DIONEX 1 Client Matrix: Water Prep Batch: N/A Lab File ID: 12.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/17/2010 1549 Final Weight/Volume: 5 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Chloride 10.0 10.6 106 90 - 110 Matrix Spike/ Method: 300.0 Matrix Spike Duplicate Recovery Report - Batch: 660-96101 Preparation: N/A MS Lab Sample ID: 660-35696-G-5 MS ^5 Analysis Batch: 660-96101 Instrument ID: DIONEX 1 Client Matrix: Water Prep Batch: N/A Lab File ID: 14.0000.TXT Dilution: 5.0 Initial Weight/Volume:

Date Analyzed: 06/17/2010 1624 Final Weight/Volume: 50 mL Date Prepared: N/A MSD Lab Sample ID: 660-35696-G-5 MSD ^5 Analysis Batch: 660-96101 Instrument ID: DIONEX 1 Client Matrix: Water Prep Batch: N/A Lab File ID: 15.0000.TXT Dilution: 5.0 Initial Weight/Volume:

Date Analyzed: 06/17/2010 1641 Final Weight/Volume: 50 mL Date Prepared: N/A

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Chloride 102 102 90 - 110 0 30 TestAmerica Tampa Page 24 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96178 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-96178/3 Analysis Batch: 660-96178 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 44.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/19/2010 0516 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Result Qual MDL PQL Bromide 0.027 U 0.027 0.050 Chloride 0.20 U 0.20 0.50 Fluoride 0.020 U 0.020 0.050 Sulfate 0.20 U 0.20 0.50 Lab Control Sample - Batch: 660-96178 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-96178/4 Analysis Batch: 660-96178 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 45.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/19/2010 0538 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Bromide 1.00 0.975 98 90 - 110 Chloride 10.0 10.2 102 90 - 110 Fluoride 1.00 1.01 101 90 - 110 Sulfate 10.0 10.0 100 90 - 110 TestAmerica Tampa Page 25 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Matrix Spike/ Method: 300.0 Matrix Spike Duplicate Recovery Report - Batch: 660-96178 Preparation: N/A MS Lab Sample ID: 660-35749-J-3 MS ^10 Analysis Batch: 660-96178 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 53.0000.TXT Dilution: 10 Initial Weight/Volume:

Date Analyzed: 06/19/2010 0831 Final Weight/Volume: 50 mL Date Prepared: N/A MSD Lab Sample ID: 660-35749-J-3 MSD ^10 Analysis Batch: 660-96178 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 54.0000.TXT Dilution: 10 Initial Weight/Volume:

Date Analyzed: 06/19/2010 0853 Final Weight/Volume: 50 mL Date Prepared: N/A

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Bromide 110 110 90 - 110 0 30 Chloride 112 112 90 - 110 0 30 J3 J3 Fluoride 104 105 90 - 110 1 30 Sulfate 105 105 90 - 110 0 30 TestAmerica Tampa Page 26 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96235 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-96235/3 Analysis Batch: 660-96235 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 11.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/21/2010 1745 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Result Qual MDL PQL Bromide 0.027 U 0.027 0.050 Sulfate 0.20 U 0.20 0.50 Lab Control Sample - Batch: 660-96235 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-96235/4 Analysis Batch: 660-96235 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 12.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/21/2010 1807 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Bromide 1.00 0.924 92 90 - 110 Sulfate 10.0 9.37 94 90 - 110 TestAmerica Tampa Page 27 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Matrix Spike/ Method: 300.0 Matrix Spike Duplicate Recovery Report - Batch: 660-96235 Preparation: N/A MS Lab Sample ID: 660-35749-J-1 MS ^25 Analysis Batch: 660-96235 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 14.0000.TXT Dilution: 25 Initial Weight/Volume:

Date Analyzed: 06/21/2010 1850 Final Weight/Volume: 50 mL Date Prepared: N/A MSD Lab Sample ID: 660-35749-J-1 MSD ^25 Analysis Batch: 660-96235 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 15.0000.TXT Dilution: 25 Initial Weight/Volume:

Date Analyzed: 06/21/2010 1912 Final Weight/Volume: 50 mL Date Prepared: N/A

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Bromide 102 105 90 - 110 4 30 Sulfate 94 104 90 - 110 3 30 TestAmerica Tampa Page 28 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96392 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-96392/3 Analysis Batch: 660-96392 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 43.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/23/2010 2010 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Result Qual MDL PQL Chloride 0.20 U 0.20 0.50 Lab Control Sample - Batch: 660-96392 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-96392/4 Analysis Batch: 660-96392 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 44.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/23/2010 2137 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Chloride 10.0 10.1 101 90 - 110 Matrix Spike/ Method: 300.0 Matrix Spike Duplicate Recovery Report - Batch: 660-96392 Preparation: N/A MS Lab Sample ID: 660-35841-B-1 MS ^100 Analysis Batch: 660-96392 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 56.0000.TXT Dilution: 100 Initial Weight/Volume:

Date Analyzed: 06/24/2010 0157 Final Weight/Volume: 50 mL Date Prepared: N/A MSD Lab Sample ID: 660-35841-B-1 MSD Analysis Batch: 660-96392 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 57.0000.TXT Dilution: 100 Initial Weight/Volume:

Date Analyzed: 06/24/2010 0219 Final Weight/Volume: 50 mL Date Prepared: N/A

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Chloride 105 108 90 - 110 3 30 TestAmerica Tampa Page 29 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96606 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-96606/3 Analysis Batch: 660-96606 Instrument ID: DIONEX 1 Client Matrix: Water Prep Batch: N/A Lab File ID: 11.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/29/2010 1721 Final Weight/Volume: 5 mL Date Prepared: N/A Analyte Result Qual MDL PQL Fluoride 0.020 U 0.020 0.050 Lab Control Sample - Batch: 660-96606 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-96606/4 Analysis Batch: 660-96606 Instrument ID: DIONEX 1 Client Matrix: Water Prep Batch: N/A Lab File ID: 12.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 06/29/2010 1838 Final Weight/Volume: 5 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Fluoride 1.00 1.01 101 90 - 110 Matrix Spike/ Method: 300.0 Matrix Spike Duplicate Recovery Report - Batch: 660-96606 Preparation: N/A MS Lab Sample ID: 660-35863-I-7 MS ^10 Analysis Batch: 660-96606 Instrument ID: DIONEX 1 Client Matrix: Water Prep Batch: N/A Lab File ID: 16.0000.TXT Dilution: 10 Initial Weight/Volume:

Date Analyzed: 06/29/2010 1949 Final Weight/Volume: 50 mL Date Prepared: N/A MSD Lab Sample ID: 660-35863-I-7 MSD ^10 Analysis Batch: 660-96606 Instrument ID: DIONEX 1 Client Matrix: Water Prep Batch: N/A Lab File ID: 17.0000.TXT Dilution: 10 Initial Weight/Volume:

Date Analyzed: 06/29/2010 2006 Final Weight/Volume: 50 mL Date Prepared: N/A

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Fluoride 95 95 90 - 110 0 30 TestAmerica Tampa Page 30 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 680-172887 Method: 9060 Preparation: N/A Lab Sample ID: MB 680-172887/1 Analysis Batch: 680-172887 Instrument ID: TOC3 Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL Date Analyzed: 06/28/2010 1127 Final Weight/Volume: 25 mL Date Prepared: N/A Analyte Result Qual PQL PQL Dissolved Inorganic Carbon-Dissolved 1.0 U 1.0 1.0 Dissolved Carbon-Dissolved 1.0 U 1.0 1.0 Lab Control Sample - Batch: 680-172887 Method: 9060 Preparation: N/A Lab Sample ID: LCS 680-172887/2 Analysis Batch: 680-172887 Instrument ID: TOC3 Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL Date Analyzed: 06/28/2010 1127 Final Weight/Volume: 25 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Dissolved Inorganic Carbon-Dissolved 20.0 19.7 98 Dissolved Carbon-Dissolved 20.0 19.7 98 TestAmerica Tampa Page 31 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96198 Method: SM 2320B Preparation: N/A Lab Sample ID: MB 660-96198/3 Analysis Batch: 660-96198 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 6.21.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/21/2010 1342 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Result Qual PQL PQL Alkalinity 1.0 U 1.0 1.0 Lab Control Sample - Batch: 660-96198 Method: SM 2320B Preparation: N/A Lab Sample ID: LCS 660-96198/4 Analysis Batch: 660-96198 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 6.21.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/21/2010 1349 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Alkalinity 118 120 101 80 - 120 Duplicate - Batch: 660-96198 Method: SM 2320B Preparation: N/A Lab Sample ID: 660-35805-1 Analysis Batch: 660-96198 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 6.21.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/21/2010 1402 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Sample Result/Qual Result RPD Limit Qual Alkalinity 220 221 0 30 Carbonate Alkalinity as CaCO3 1.0 U 1.0 NC 30 U TestAmerica Tampa Page 32 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96110 Method: SM 2540C Preparation: N/A Lab Sample ID: MB 660-96110/1 Analysis Batch: 660-96110 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/18/2010 1324 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Result Qual PQL PQL Total Dissolved Solids 5.0 U 5.0 5.0 Lab Control Sample - Batch: 660-96110 Method: SM 2540C Preparation: N/A Lab Sample ID: LCS 660-96110/2 Analysis Batch: 660-96110 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 10 mL Date Analyzed: 06/18/2010 1325 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Total Dissolved Solids 10000 9950 100 80 - 120 Duplicate - Batch: 660-96110 Method: SM 2540C Preparation: N/A Lab Sample ID: 660-35787-D-1 DU Analysis Batch: 660-96110 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/18/2010 1327 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Sample Result/Qual Result RPD Limit Qual Total Dissolved Solids 1100 1150 0 20 TestAmerica Tampa Page 33 of 43

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Method Blank - Batch: 660-96052 Method: SM 4500 S2 F Preparation: N/A Lab Sample ID: MB 660-96052/1 Analysis Batch: 660-96052 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/17/2010 1640 Final Weight/Volume: 250 mL Date Prepared: N/A Analyte Result Qual PQL PQL Sulfide 1.0 U 1.0 1.0 Lab Control Sample/ Method: SM 4500 S2 F Lab Control Sample Duplicate Recovery Report - Batch: 660-96052 Preparation: N/A LCS Lab Sample ID: LCS 660-96052/2 Analysis Batch: 660-96052 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/17/2010 1640 Final Weight/Volume: 250 mL Date Prepared: N/A LCSD Lab Sample ID: LCSD 660-96052/3 Analysis Batch: 660-96052 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/17/2010 1640 Final Weight/Volume: 250 mL Date Prepared: N/A

% Rec.

Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual Sulfide 98 98 75 - 125 0 25 TestAmerica Tampa Page 34 of 43

Page 35 of 43 Page 36 of 43 Page 37 of 43 Page 38 of 43 Page 39 of 43 Page 40 of 43 Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35805-1 SDG Number: 35805 Login Number: 35805 List Source: TestAmerica Tampa Creator: McNulty, Carol List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True 1.1 degrees C Cu-07 Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True no Hg required per PM Is the Field Sampler's name present on COC? True There are no discrepancies between the sample IDs on the containers and True the COC.

Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in True diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. True Samples do not require splitting or compositing. True TestAmerica Tampa Page 41 of 43

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35805-1 SDG Number: 35805 Login Number: 35805 List Source: TestAmerica Savannah Creator: Daughtry, Beth List Creation: 06/18/10 12:27 PM List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? N/A There are no discrepancies between the sample IDs on the containers and True the COC.

Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in True diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. N/A Samples do not require splitting or compositing. N/A TestAmerica Tampa Page 42 of 43

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35805-1 SDG Number: 35805 Login Number: 35805 List Source: TestAmerica Tallahassee Creator: Archie, Datiska List Creation: 06/18/10 10:57 AM List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the sample IDs on the containers and True the COC.

Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in N/A diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. N/A Samples do not require splitting or compositing. N/A TestAmerica Tampa Page 43 of 43

ANALYTICAL REPORT Job Number: 660-35970-1 SDG Number: 35970 Job

Description:

FPL Turkey Point Analytical Services For:

Florida Power & Light Company Technical Services - PGD Environmental Water Compliance/Permitting 700 Universe Blvd (JES/JB)

Juno Beach, FL 33408 Attention: Ms. Stacy Foster Approved for release.

Amy Atkins Project Manager I 8/3/2010 1:30 PM Amy Atkins Project Manager I amy.atkins@testamericainc.com 08/03/2010 cc: Ms. Sharon Ewe Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282; TestAmerica Tallahassee E81005; TestAmerica Savannah E87052 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report.

The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 47

Job Narrative 660-35970-1 Receipt All samples were received in good condition within temperature requirements.

6010B The matrix spike duplicate (MSD) recovery for Calcium in batch 660-96604 was outside control limits with the sample greater than 4x the spike level. The associated laboratory control sample (LCS) recovery met acceptance criteria.

300.0 The matrix spike / matrix spike duplicate (MS/MSD) recoveries for Chloride in batch 96989 were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria.

300.0 Due to analyst error the matrix spike / matrix spike duplicate (MS/MSD) was not analyzed with the parent sample at a dilution that was reportable. The associated laboratory control sample (LCS) recovery met acceptance criteria.

Page 2 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35970-1 062510-TPGW-8M Field pH 7.06 SU Field Sampling Field Temperature 25.29 Degrees C Field Sampling Oxygen, Dissolved 10.9 mg/L Field Sampling Specific Conductance 544 umhos/cm Field Sampling Turbidity 1.18 NTU Field Sampling Bromide 0.18 0.050 mg/L 300.0 Chloride 33 0.50 mg/L 300.0 Fluoride 0.068 0.050 mg/L 300.0 Sulfate 43 0.50 mg/L 300.0 Alkalinity 230 1.0 mg/L SM 2320B Total Dissolved Solids 350 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 51 1.0 mg/L 9060 Total Recoverable Iron 550 500 ug/L 200.7 Rev 4.4 Boron 63 50 ug/L 6010B Calcium 110 0.50 mg/L 6010B Potassium 9.2 1.0 mg/L 6010B Strontium 1100 5.0 ug/L 6010B Magnesium 3.8 0.080 mg/L 6010B Sodium 20 0.50 mg/L 6010B TestAmerica Tampa Page 3 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35970-2 062510-TPGW-8D Field pH 7.10 SU Field Sampling Field Temperature 25.23 Degrees C Field Sampling Oxygen, Dissolved 1.6 mg/L Field Sampling Specific Conductance 599 umhos/cm Field Sampling Turbidity 4.04 NTU Field Sampling Bromide 0.26 0.050 mg/L 300.0 Chloride 47 0.50 mg/L 300.0 Fluoride 0.047 I 0.050 mg/L 300.0 Sulfate 49 0.50 mg/L 300.0 Alkalinity 220 1.0 mg/L SM 2320B Total Dissolved Solids 370 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 49 1.0 mg/L 9060 Total Recoverable Barium 12 I 100 ug/L 200.7 Rev 4.4 Iron 310 I 500 ug/L 200.7 Rev 4.4 Boron 69 50 ug/L 6010B Calcium 110 0.50 mg/L 6010B Potassium 8.5 1.0 mg/L 6010B Strontium 1100 5.0 ug/L 6010B Magnesium 6.2 0.080 mg/L 6010B Sodium 31 0.50 mg/L 6010B TestAmerica Tampa Page 4 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35970-3 062510-TPGW-9S Field pH 7.13 SU Field Sampling Field Temperature 25.82 Degrees C Field Sampling Oxygen, Dissolved 2.6 mg/L Field Sampling Specific Conductance 556 umhos/cm Field Sampling Turbidity 9.27 NTU Field Sampling Bromide 0.30 0.050 mg/L 300.0 Chloride 23 0.50 mg/L 300.0 Sulfate 18 0.50 mg/L 300.0 Alkalinity 250 1.0 mg/L SM 2320B Total Dissolved Solids 330 5.0 mg/L SM 2540C Sulfide 1.1 1.0 mg/L SM 4500 S2 F Dissolved Dissolved Inorganic Carbon-Dissolved 62 1.0 mg/L 9060 Total Recoverable Barium 12 I 100 ug/L 200.7 Rev 4.4 Iron 190 I 500 ug/L 200.7 Rev 4.4 Boron 47 I 50 ug/L 6010B Calcium 120 0.50 mg/L 6010B Potassium 11 1.0 mg/L 6010B Strontium 990 5.0 ug/L 6010B Magnesium 2.9 0.080 mg/L 6010B Sodium 14 0.50 mg/L 6010B TestAmerica Tampa Page 5 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35970-4 062510-TPGW-9M Field pH 6.99 SU Field Sampling Field Temperature 25.10 Degrees C Field Sampling Oxygen, Dissolved 1.5 mg/L Field Sampling Specific Conductance 563 umhos/cm Field Sampling Turbidity 8.49 NTU Field Sampling Bromide 0.29 0.050 mg/L 300.0 Chloride 25 0.50 mg/L 300.0 Fluoride 0.038 I 0.050 mg/L 300.0 Sulfate 24 0.50 mg/L 300.0 Alkalinity 270 1.0 mg/L SM 2320B Total Dissolved Solids 350 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 60 1.0 mg/L 9060 Total Recoverable Iron 600 500 ug/L 200.7 Rev 4.4 Boron 48 I 50 ug/L 6010B Calcium 120 0.50 mg/L 6010B Potassium 6.7 1.0 mg/L 6010B Strontium 990 5.0 ug/L 6010B Magnesium 3.1 0.080 mg/L 6010B Sodium 15 0.50 mg/L 6010B TestAmerica Tampa Page 6 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35970-5 062510-TPGW-9D Field pH 6.99 SU Field Sampling Field Temperature 25.09 Degrees C Field Sampling Oxygen, Dissolved 2.4 mg/L Field Sampling Specific Conductance 564 umhos/cm Field Sampling Turbidity 0.83 NTU Field Sampling Bromide 0.41 0.050 mg/L 300.0 Chloride 30 0.50 mg/L 300.0 Fluoride 0.062 0.050 mg/L 300.0 Sulfate 33 0.50 mg/L 300.0 Alkalinity 250 1.0 mg/L SM 2320B Total Dissolved Solids 360 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 58 1.0 mg/L 9060 Total Recoverable Barium 23 I 100 ug/L 200.7 Rev 4.4 Iron 760 500 ug/L 200.7 Rev 4.4 Boron 48 I 50 ug/L 6010B Calcium 110 0.50 mg/L 6010B Potassium 3.3 1.0 mg/L 6010B Strontium 1100 5.0 ug/L 6010B Magnesium 3.6 0.080 mg/L 6010B Sodium 22 0.50 mg/L 6010B TestAmerica Tampa Page 7 of 47

METHOD

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Description Lab Location Method Preparation Method Matrix: Water Metals (ICP) TAL TAL EPA 200.7 Rev 4.4 Preparation, Total Recoverable Metals TAL TAL EPA 200.7 Metals (ICP) TAL TAM SW846 6010B Preparation, Total Recoverable or Dissolved Metals TAL TAM SW846 3005A Anions, Ion Chromatography TAL TAM MCAWW 300.0 Carbon, Dissolved and Dissolved Inorganic TAL SAV SW846 9060 Sample Filtration, Field TAL SAV FIELD_FLTRD Alkalinity TAL TAM SM SM 2320B Solids, Total Dissolved (TDS) TAL TAM SM SM 2540C Sulfide, Total TAL TAM SM SM 4500 S2 F Field Sampling TAL TAM EPA Field Sampling Lab

References:

TAL SAV = TestAmerica Savannah TAL TAL = TestAmerica Tallahassee TAL TAM = TestAmerica Tampa Method

References:

EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa Page 8 of 47

METHOD / ANALYST

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Analyst Analyst ID EPA 200.7 Rev 4.4 Wallace, Tiffany B TBW SW846 6010B Fox, Greg GF EPA Field Sampling Sampler, Field FS MCAWW 300.0 Sengsouvanna, Dom DS SW846 9060 Blackshear, Kim KB SM SM 2320B Steward, Tiffany TS SM SM 2540C Oonnoonny, Thomas TO SM SM 4500 S2 F Mostafavifar, Efe EM TestAmerica Tampa Page 9 of 47

SAMPLE

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Date/Time Date/Time Lab Sample ID Client Sample ID Client Matrix Sampled Received 660-35970-1 062510-TPGW-8M Water 06/25/2010 1225 06/26/2010 0830 660-35970-2 062510-TPGW-8D Water 06/25/2010 1200 06/26/2010 0830 660-35970-3 062510-TPGW-9S Water 06/25/2010 1030 06/26/2010 0830 660-35970-4 062510-TPGW-9M Water 06/25/2010 0955 06/26/2010 0830 660-35970-5 062510-TPGW-9D Water 06/25/2010 0930 06/26/2010 0830 TestAmerica Tampa Page 10 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID: 062510-TPGW-8M Lab Sample ID: 660-35970-1 Date Sampled: 06/25/2010 1225 Client Matrix: Water Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0941 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 9.6 U 9.6 100 Iron 550 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1742 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1007 Analyte Result (mg/L) Qualifier MDL PQL Calcium 110 0.10 0.50 Potassium 9.2 0.19 1.0 Magnesium 3.8 0.020 0.080 Sodium 20 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 63 10 50 Strontium 1100 1.0 5.0 TestAmerica Tampa Page 11 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID: 062510-TPGW-8D Lab Sample ID: 660-35970-2 Date Sampled: 06/25/2010 1200 Client Matrix: Water Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0944 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 12 I 9.6 100 Iron 310 I 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1749 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1007 Analyte Result (mg/L) Qualifier MDL PQL Calcium 110 0.10 0.50 Potassium 8.5 0.19 1.0 Magnesium 6.2 0.020 0.080 Sodium 31 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 69 10 50 Strontium 1100 1.0 5.0 TestAmerica Tampa Page 12 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID: 062510-TPGW-9S Lab Sample ID: 660-35970-3 Date Sampled: 06/25/2010 1030 Client Matrix: Water Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0948 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 12 I 9.6 100 Iron 190 I 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1755 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1007 Analyte Result (mg/L) Qualifier MDL PQL Calcium 120 0.10 0.50 Potassium 11 0.19 1.0 Magnesium 2.9 0.020 0.080 Sodium 14 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 47 I 10 50 Strontium 990 1.0 5.0 TestAmerica Tampa Page 13 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID: 062510-TPGW-9M Lab Sample ID: 660-35970-4 Date Sampled: 06/25/2010 0955 Client Matrix: Water Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0951 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 9.6 U 9.6 100 Iron 600 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1801 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1007 Analyte Result (mg/L) Qualifier MDL PQL Calcium 120 0.10 0.50 Potassium 6.7 0.19 1.0 Magnesium 3.1 0.020 0.080 Sodium 15 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 48 I 10 50 Strontium 990 1.0 5.0 TestAmerica Tampa Page 14 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID: 062510-TPGW-9D Lab Sample ID: 660-35970-5 Date Sampled: 06/25/2010 0930 Client Matrix: Water Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0955 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 23 I 9.6 100 Iron 760 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1807 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1010 Analyte Result (mg/L) Qualifier MDL PQL Calcium 110 0.10 0.50 Potassium 3.3 0.19 1.0 Magnesium 3.6 0.020 0.080 Sodium 22 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 48 I 10 50 Strontium 1100 1.0 5.0 TestAmerica Tampa Page 15 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID: 062510-TPGW-8M Lab Sample ID: 660-35970-1 Date Sampled: 06/25/2010 1225 Client Matrix: Water Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.18 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0629 Chloride 33 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0629 Fluoride 0.068 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0629 Sulfate 43 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0629 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 51 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 230 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1120 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1120 Total Dissolved Solids 350 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 16 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID: 062510-TPGW-8D Lab Sample ID: 660-35970-2 Date Sampled: 06/25/2010 1200 Client Matrix: Water Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.26 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0651 Chloride 47 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0651 Fluoride 0.047 I mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0651 Sulfate 49 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0651 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 49 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 220 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1125 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1125 Total Dissolved Solids 370 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 17 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID: 062510-TPGW-9S Lab Sample ID: 660-35970-3 Date Sampled: 06/25/2010 1030 Client Matrix: Water Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.30 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0901 Chloride 23 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0901 Fluoride 0.020 U mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0901 Sulfate 18 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0901 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 62 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 250 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1131 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1131 Total Dissolved Solids 330 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.1 mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 18 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID: 062510-TPGW-9M Lab Sample ID: 660-35970-4 Date Sampled: 06/25/2010 0955 Client Matrix: Water Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.29 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0923 Chloride 25 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0923 Fluoride 0.038 I mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0923 Sulfate 24 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0923 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 60 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 270 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1138 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1138 Total Dissolved Solids 350 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 19 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID: 062510-TPGW-9D Lab Sample ID: 660-35970-5 Date Sampled: 06/25/2010 0930 Client Matrix: Water Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.41 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0945 Chloride 30 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0945 Fluoride 0.062 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0945 Sulfate 33 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0945 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 58 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 250 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1144 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1144 Total Dissolved Solids 360 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 20 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID: 062510-TPGW-8M Lab Sample ID: 660-35970-1 Date Sampled: 06/25/2010 1225 Client Matrix: Water Date Received: 06/26/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 7.06 SU 1.0 Field 660-97058 06/25/2010 1225 Sampling Field Temperature 25.29 Degrees C 1.0 Field 660-97058 06/25/2010 1225 Sampling Oxygen, Dissolved 10.9 mg/L 1.0 Field 660-97058 06/25/2010 1225 Sampling Specific Conductance 544 umhos/cm 1.0 Field 660-97058 06/25/2010 1225 Sampling Turbidity 1.18 NTU 1.0 Field 660-97058 06/25/2010 1225 Sampling TestAmerica Tampa Page 21 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID: 062510-TPGW-8D Lab Sample ID: 660-35970-2 Date Sampled: 06/25/2010 1200 Client Matrix: Water Date Received: 06/26/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 7.10 SU 1.0 Field 660-97058 06/25/2010 1200 Sampling Field Temperature 25.23 Degrees C 1.0 Field 660-97058 06/25/2010 1200 Sampling Oxygen, Dissolved 1.6 mg/L 1.0 Field 660-97058 06/25/2010 1200 Sampling Specific Conductance 599 umhos/cm 1.0 Field 660-97058 06/25/2010 1200 Sampling Turbidity 4.04 NTU 1.0 Field 660-97058 06/25/2010 1200 Sampling TestAmerica Tampa Page 22 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID: 062510-TPGW-9S Lab Sample ID: 660-35970-3 Date Sampled: 06/25/2010 1030 Client Matrix: Water Date Received: 06/26/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 7.13 SU 1.0 Field 660-97058 06/25/2010 1030 Sampling Field Temperature 25.82 Degrees C 1.0 Field 660-97058 06/25/2010 1030 Sampling Oxygen, Dissolved 2.6 mg/L 1.0 Field 660-97058 06/25/2010 1030 Sampling Specific Conductance 556 umhos/cm 1.0 Field 660-97058 06/25/2010 1030 Sampling Turbidity 9.27 NTU 1.0 Field 660-97058 06/25/2010 1030 Sampling TestAmerica Tampa Page 23 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID: 062510-TPGW-9M Lab Sample ID: 660-35970-4 Date Sampled: 06/25/2010 0955 Client Matrix: Water Date Received: 06/26/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 6.99 SU 1.0 Field 660-97058 06/25/2010 0955 Sampling Field Temperature 25.10 Degrees C 1.0 Field 660-97058 06/25/2010 0955 Sampling Oxygen, Dissolved 1.5 mg/L 1.0 Field 660-97058 06/25/2010 0955 Sampling Specific Conductance 563 umhos/cm 1.0 Field 660-97058 06/25/2010 0955 Sampling Turbidity 8.49 NTU 1.0 Field 660-97058 06/25/2010 0955 Sampling TestAmerica Tampa Page 24 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID: 062510-TPGW-9D Lab Sample ID: 660-35970-5 Date Sampled: 06/25/2010 0930 Client Matrix: Water Date Received: 06/26/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 6.99 SU 1.0 Field 660-97058 06/25/2010 0930 Sampling Field Temperature 25.09 Degrees C 1.0 Field 660-97058 06/25/2010 0930 Sampling Oxygen, Dissolved 2.4 mg/L 1.0 Field 660-97058 06/25/2010 0930 Sampling Specific Conductance 564 umhos/cm 1.0 Field 660-97058 06/25/2010 0930 Sampling Turbidity 0.83 NTU 1.0 Field 660-97058 06/25/2010 0930 Sampling TestAmerica Tampa Page 25 of 47

DATA REPORTING QUALIFIERS Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Lab Section Qualifier Description Metals J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

U Indicates that the compound was analyzed for but not detected.

I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

General Chemistry J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

U Indicates that the compound was analyzed for but not detected.

I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

TestAmerica Tampa Page 26 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Blank - Batch: 640-70571 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable Lab Sample ID: MB 640-70571/1-A Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/13/2010 0852 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result Qual MDL PQL Barium 0.96 U 0.96 10 Iron 4.6 U 4.6 50 Lab Control Sample/ Method: 200.7 Rev 4.4 Lab Control Sample Duplicate Recovery Report - Batch: 640-70571 Preparation: 200.7 Total Recoverable LCS Lab Sample ID: LCS 640-70571/2-A Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/13/2010 0856 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 LCSD Lab Sample ID: LCSD 640-70571/3-A Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/13/2010 0859 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100

% Rec.

Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual Barium 101 102 85 - 115 1 20 Iron 102 103 85 - 115 1 20 TestAmerica Tampa Page 27 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Matrix Spike/ Method: 200.7 Rev 4.4 Matrix Spike Duplicate Recovery Report - Batch: 640-70571 Preparation: 200.7 Total Recoverable MS Lab Sample ID: 660-36031-B-1-B MS Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0910 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 MSD Lab Sample ID: 660-36031-B-1-C MSD Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0913 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Barium 101 98 70 - 130 2 20 Iron 99 96 70 - 130 3 20 Duplicate - Batch: 640-70571 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable Lab Sample ID: 660-36031-B-2-B DU Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Units: ug/L Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0934 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Sample Result/Qual Result RPD Limit Qual Barium 130 123 2 20 Iron 8600 8340 3 20 TestAmerica Tampa Page 28 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Blank - Batch: 660-96604 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: MB 660-96604/1-A Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1250 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result Qual MDL PQL Calcium 0.10 U 0.10 0.50 Potassium 0.19 U 0.19 1.0 Magnesium 0.020 U 0.020 0.080 Sodium 0.31 U 0.31 0.50 Method Blank - Batch: 660-96604 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: MB 660-96604/1-A Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1250 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result Qual MDL PQL Boron 10 U 10 50 Strontium 1.0 U 1.0 5.0 TestAmerica Tampa Page 29 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Lab Control Sample - Batch: 660-96604 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: LCS 660-96604/2-A Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1256 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Spike Amount Result % Rec. Limit Qual Calcium 1.00 1.05 105 75 - 125 Potassium 10.0 10.1 101 75 - 125 Magnesium 1.00 1.03 103 75 - 125 Sodium 10.0 9.85 98 75 - 125 Lab Control Sample - Batch: 660-96604 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: LCS 660-96604/2-A Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1256 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Spike Amount Result % Rec. Limit Qual Boron 1000 1020 102 75 - 125 Strontium 1000 1070 107 75 - 125 TestAmerica Tampa Page 30 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Matrix Spike/ Method: 6010B Matrix Spike Duplicate Recovery Report - Batch: 660-96604 Preparation: 3005A Total Recoverable MS Lab Sample ID: 660-36004-B-9-B MS Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1314 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 MSD Lab Sample ID: 660-36004-B-9-C MSD Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1320 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Calcium 93 250 75 - 125 1 20 J3 Potassium 111 113 75 - 125 2 20 Magnesium 103 108 75 - 125 2 20 Sodium 104 92 75 - 125 8 20 Matrix Spike/ Method: 6010B Matrix Spike Duplicate Recovery Report - Batch: 660-96604 Preparation: 3005A Total Recoverable MS Lab Sample ID: 660-36004-B-9-B MS Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1314 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 MSD Lab Sample ID: 660-36004-B-9-C MSD Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1320 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Boron 104 105 75 - 125 1 20 Strontium 107 109 75 - 125 2 20 TestAmerica Tampa Page 31 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Blank - Batch: 660-96989 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-96989/3 Analysis Batch: 660-96989 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 21.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 07/08/2010 2001 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Result Qual MDL PQL Bromide 0.027 U 0.027 0.050 Chloride 0.20 U 0.20 0.50 Fluoride 0.020 U 0.020 0.050 Sulfate 0.20 U 0.20 0.50 Lab Control Sample - Batch: 660-96989 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-96989/4 Analysis Batch: 660-96989 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 22.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 07/08/2010 2022 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Bromide 1.00 0.976 98 90 - 110 Chloride 10.0 10.2 102 90 - 110 Fluoride 1.00 0.950 95 90 - 110 Sulfate 10.0 10.2 102 90 - 110 TestAmerica Tampa Page 32 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Matrix Spike/ Method: 300.0 Matrix Spike Duplicate Recovery Report - Batch: 660-96989 Preparation: N/A MS Lab Sample ID: 660-36016-J-3 MS ^10 Analysis Batch: 660-96989 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 40.0000.TXT Dilution: 10 Initial Weight/Volume:

Date Analyzed: 07/09/2010 0253 Final Weight/Volume: 50 mL Date Prepared: N/A MSD Lab Sample ID: 660-36016-J-3 MSD ^10 Analysis Batch: 660-96989 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 41.0000.TXT Dilution: 10 Initial Weight/Volume:

Date Analyzed: 07/09/2010 0314 Final Weight/Volume: 50 mL Date Prepared: N/A

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Bromide 104 101 90 - 110 3 30 Chloride 118 111 90 - 110 2 30 J3 J3 Fluoride 110 108 90 - 110 2 30 Sulfate 109 103 90 - 110 3 30 TestAmerica Tampa Page 33 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Blank - Batch: 660-97030 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-97030/3 Analysis Batch: 660-97030 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 55.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 07/09/2010 0818 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Result Qual MDL PQL Bromide 0.027 U 0.027 0.050 Chloride 0.20 U 0.20 0.50 Fluoride 0.020 U 0.020 0.050 Sulfate 0.20 U 0.20 0.50 Lab Control Sample - Batch: 660-97030 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-97030/4 Analysis Batch: 660-97030 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 56.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 07/09/2010 0840 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Bromide 1.00 1.01 101 90 - 110 Chloride 10.0 10.2 102 90 - 110 Fluoride 1.00 0.991 99 90 - 110 Sulfate 10.0 10.3 103 90 - 110 TestAmerica Tampa Page 34 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Blank - Batch: 680-173757 Method: 9060 Preparation: N/A Lab Sample ID: MB 680-173757/1 Analysis Batch: 680-173757 Instrument ID: TOC3 Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL Date Analyzed: 07/09/2010 0959 Final Weight/Volume: 25 mL Date Prepared: N/A Analyte Result Qual PQL PQL Dissolved Inorganic Carbon-Dissolved 1.0 U 1.0 1.0 Dissolved Carbon-Dissolved 1.0 U 1.0 1.0 Lab Control Sample - Batch: 680-173757 Method: 9060 Preparation: N/A Lab Sample ID: LCS 680-173757/2 Analysis Batch: 680-173757 Instrument ID: TOC3 Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL Date Analyzed: 07/09/2010 0959 Final Weight/Volume: 25 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Dissolved Inorganic Carbon-Dissolved 20.0 19.3 96 Dissolved Carbon-Dissolved 20.0 19.3 96 TestAmerica Tampa Page 35 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Blank - Batch: 660-96877 Method: SM 2320B Preparation: N/A Lab Sample ID: MB 660-96877/1 Analysis Batch: 660-96877 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 7.7.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/07/2010 1023 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Result Qual PQL PQL Alkalinity 1.0 U 1.0 1.0 Lab Control Sample - Batch: 660-96877 Method: SM 2320B Preparation: N/A Lab Sample ID: LCS 660-96877/2 Analysis Batch: 660-96877 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 7.7.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/07/2010 1030 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Alkalinity 118 117 99 80 - 120 Duplicate - Batch: 660-96877 Method: SM 2320B Preparation: N/A Lab Sample ID: 660-35970-5 Analysis Batch: 660-96877 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 7.7.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/07/2010 1150 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Sample Result/Qual Result RPD Limit Qual Alkalinity 250 262 4 30 Carbonate Alkalinity as CaCO3 1.0 U 1.0 NC 30 U TestAmerica Tampa Page 36 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Blank - Batch: 660-96652 Method: SM 2540C Preparation: N/A Lab Sample ID: MB 660-96652/1 Analysis Batch: 660-96652 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/30/2010 1617 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Result Qual PQL PQL Total Dissolved Solids 5.0 U 5.0 5.0 Lab Control Sample - Batch: 660-96652 Method: SM 2540C Preparation: N/A Lab Sample ID: LCS 660-96652/2 Analysis Batch: 660-96652 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 10 mL Date Analyzed: 06/30/2010 1617 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Total Dissolved Solids 10000 9990 100 80 - 120 Duplicate - Batch: 660-96652 Method: SM 2540C Preparation: N/A Lab Sample ID: 660-35951-E-3 DU Analysis Batch: 660-96652 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/30/2010 1617 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Sample Result/Qual Result RPD Limit Qual Total Dissolved Solids 56 58.0 4 20 TestAmerica Tampa Page 37 of 47

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Method Blank - Batch: 660-96518 Method: SM 4500 S2 F Preparation: N/A Lab Sample ID: MB 660-96518/1 Analysis Batch: 660-96518 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/26/2010 1130 Final Weight/Volume: 250 mL Date Prepared: N/A Analyte Result Qual PQL PQL Sulfide 1.0 U 1.0 1.0 Lab Control Sample/ Method: SM 4500 S2 F Lab Control Sample Duplicate Recovery Report - Batch: 660-96518 Preparation: N/A LCS Lab Sample ID: LCS 660-96518/2 Analysis Batch: 660-96518 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/26/2010 1130 Final Weight/Volume: 250 mL Date Prepared: N/A LCSD Lab Sample ID: LCSD 660-96518/3 Analysis Batch: 660-96518 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/26/2010 1130 Final Weight/Volume: 250 mL Date Prepared: N/A

% Rec.

Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual Sulfide 96 98 75 - 125 2 25 TestAmerica Tampa Page 38 of 47

Page 39 of 47 Page 40 of 47 Page 41 of 47 Page 42 of 47 Page 43 of 47 Page 44 of 47 Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35970-1 SDG Number: 35970 Login Number: 35970 List Source: TestAmerica Tampa Creator: Volz, Charles List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True 2.5,2.7 Degrees C. CU-07 COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the sample IDs on the containers and True the COC.

Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in False diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. True Samples do not require splitting or compositing. True TestAmerica Tampa Page 45 of 47

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35970-1 SDG Number: 35970 Login Number: 35970 List Source: TestAmerica Savannah Creator: Kicklighter, Marilyn List Creation: 06/29/10 02:14 PM List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? N/A There are no discrepancies between the sample IDs on the containers and True the COC.

Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in N/A diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. N/A Samples do not require splitting or compositing. N/A TestAmerica Tampa Page 46 of 47

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35970-1 SDG Number: 35970 Login Number: 35970 List Source: TestAmerica Tallahassee Creator: Archie, Datiska List Creation: 06/30/10 09:30 AM List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the sample IDs on the containers and True the COC.

Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in N/A diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. N/A Samples do not require splitting or compositing. N/A TestAmerica Tampa Page 47 of 47

ANALYTICAL REPORT Job Number: 660-35950-1 SDG Number: 35950 Job

Description:

FPL Turkey Point Analytical Services For:

Florida Power & Light Company Technical Services - PGD Environmental Water Compliance/Permitting 700 Universe Blvd (JES/JB)

Juno Beach, FL 33408 Attention: Ms. Stacy Foster Approved for release.

Amy Atkins Project Manager I 8/2/2010 3:51 PM Amy Atkins Project Manager I amy.atkins@testamericainc.com 08/02/2010 cc: Ms. Sharon Ewe Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282; TestAmerica Tallahassee E81005; TestAmerica Savannah E87052 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report.

The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 54

Job Narrative 660-35950-1 Receipt All samples were received in good condition within temperature requirements.

6010B The matrix spike duplicate (MSD) recovery for Calcium in batch 660-96604 was outside control limits with the sample greater than 4x the spike level. The associated laboratory control sample (LCS) recovery met acceptance criteria.

300.0 Due to sample matrix, 062410-TPGW-4D (660-35950-3) and 062410-TPGW-4M (660-35950-2) were diluted for Fluoride.

Page 2 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35950-1 062410-TPGW-4S Field pH 7.31 SU Field Sampling Field Temperature 24.99 Degrees C Field Sampling Oxygen, Dissolved 1.4 mg/L Field Sampling Specific Conductance 1750 umhos/cm Field Sampling Turbidity 2.52 NTU Field Sampling Bromide 1.7 0.050 mg/L 300.0 Chloride 490 50 mg/L 300.0 Fluoride 0.055 0.050 mg/L 300.0 Sulfate 20 0.50 mg/L 300.0 Alkalinity 200 1.0 mg/L SM 2320B Total Dissolved Solids 1100 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 54 1.0 mg/L 9060 Total Recoverable Barium 24 I 100 ug/L 200.7 Rev 4.4 Iron 220 I 500 ug/L 200.7 Rev 4.4 Boron 64 50 ug/L 6010B Calcium 120 0.50 mg/L 6010B Potassium 9.2 1.0 mg/L 6010B Strontium 1300 5.0 ug/L 6010B Magnesium 19 0.080 mg/L 6010B Sodium 250 5.0 mg/L 6010B TestAmerica Tampa Page 3 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35950-2 062410-TPGW-4M Field pH 6.88 SU Field Sampling Field Temperature 25.66 Degrees C Field Sampling Oxygen, Dissolved 2.3 mg/L Field Sampling Specific Conductance 32010 umhos/cm Field Sampling Turbidity 2.0 NTU Field Sampling Bromide 47 5.0 mg/L 300.0 Chloride 13000 500 mg/L 300.0 Sulfate 1600 50 mg/L 300.0 Alkalinity 210 1.0 mg/L SM 2320B Total Dissolved Solids 28000 250 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 48 1.0 mg/L 9060 Total Recoverable Barium 150 100 ug/L 200.7 Rev 4.4 Iron 4700 500 ug/L 200.7 Rev 4.4 Boron 1400 500 ug/L 6010B Calcium 620 5.0 mg/L 6010B Potassium 280 10 mg/L 6010B Strontium 8300 50 ug/L 6010B Magnesium 900 0.80 mg/L 6010B Sodium 7200 100 mg/L 6010B TestAmerica Tampa Page 4 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35950-3 062410-TPGW-4D Field pH 6.92 SU Field Sampling Field Temperature 25.29 Degrees C Field Sampling Oxygen, Dissolved 2.4 mg/L Field Sampling Specific Conductance 37010 umhos/cm Field Sampling Turbidity 0.02 NTU Field Sampling Bromide 54 50 mg/L 300.0 Chloride 16000 500 mg/L 300.0 Sulfate 1900 50 mg/L 300.0 Alkalinity 200 1.0 mg/L SM 2320B Total Dissolved Solids 33000 250 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 45 1.0 mg/L 9060 Total Recoverable Barium 140 100 ug/L 200.7 Rev 4.4 Iron 5900 500 ug/L 200.7 Rev 4.4 Boron 2200 500 ug/L 6010B Calcium 620 5.0 mg/L 6010B Potassium 420 10 mg/L 6010B Strontium 8800 50 ug/L 6010B Magnesium 1100 0.80 mg/L 6010B Sodium 8600 100 mg/L 6010B TestAmerica Tampa Page 5 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35950-4 062410-TPGW-7S Field pH 7.22 SU Field Sampling Field Temperature 24.80 Degrees C Field Sampling Oxygen, Dissolved 2.0 mg/L Field Sampling Specific Conductance 483 umhos/cm Field Sampling Turbidity 3.81 NTU Field Sampling Bromide 0.18 0.050 mg/L 300.0 Chloride 36 0.50 mg/L 300.0 Fluoride 0.17 0.050 mg/L 300.0 Sulfate 27 0.50 mg/L 300.0 Alkalinity 210 1.0 mg/L SM 2320B Total Dissolved Solids 300 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 44 1.0 mg/L 9060 Total Recoverable Iron 340 I 500 ug/L 200.7 Rev 4.4 Boron 53 50 ug/L 6010B Calcium 91 0.50 mg/L 6010B Potassium 9.9 1.0 mg/L 6010B Strontium 910 5.0 ug/L 6010B Magnesium 4.0 0.080 mg/L 6010B Sodium 20 0.50 mg/L 6010B TestAmerica Tampa Page 6 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35950-5 062410-TPGW-7M Field pH 7.19 SU Field Sampling Field Temperature 25.05 Degrees C Field Sampling Oxygen, Dissolved 1.5 mg/L Field Sampling Specific Conductance 500 umhos/cm Field Sampling Turbidity 2.29 NTU Field Sampling Bromide 0.17 0.050 mg/L 300.0 Chloride 35 0.50 mg/L 300.0 Fluoride 0.23 0.050 mg/L 300.0 Sulfate 25 0.50 mg/L 300.0 Alkalinity 200 1.0 mg/L SM 2320B Total Dissolved Solids 310 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 47 1.0 mg/L 9060 Total Recoverable Barium 11 I 100 ug/L 200.7 Rev 4.4 Iron 360 I 500 ug/L 200.7 Rev 4.4 Boron 53 50 ug/L 6010B Calcium 91 0.50 mg/L 6010B Potassium 9.4 1.0 mg/L 6010B Strontium 920 5.0 ug/L 6010B Magnesium 4.1 0.080 mg/L 6010B Sodium 21 0.50 mg/L 6010B TestAmerica Tampa Page 7 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 660-35950-6 062410-TPGW-7D Field pH 7.19 SU Field Sampling Field Temperature 25.12 Degrees C Field Sampling Oxygen, Dissolved 2.3 mg/L Field Sampling Specific Conductance 510 umhos/cm Field Sampling Turbidity 1.34 NTU Field Sampling Bromide 0.21 0.050 mg/L 300.0 Chloride 41 0.50 mg/L 300.0 Fluoride 0.14 0.050 mg/L 300.0 Sulfate 29 0.50 mg/L 300.0 Alkalinity 200 1.0 mg/L SM 2320B Total Dissolved Solids 320 5.0 mg/L SM 2540C Dissolved Dissolved Inorganic Carbon-Dissolved 47 1.0 mg/L 9060 Total Recoverable Iron 280 I 500 ug/L 200.7 Rev 4.4 Boron 51 50 ug/L 6010B Calcium 91 0.50 mg/L 6010B Potassium 4.8 1.0 mg/L 6010B Strontium 880 5.0 ug/L 6010B Magnesium 3.7 0.080 mg/L 6010B Sodium 26 0.50 mg/L 6010B TestAmerica Tampa Page 8 of 54

METHOD

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Description Lab Location Method Preparation Method Matrix: Water Metals (ICP) TAL TAL EPA 200.7 Rev 4.4 Preparation, Total Recoverable Metals TAL TAL EPA 200.7 Metals (ICP) TAL TAM SW846 6010B Preparation, Total Recoverable or Dissolved Metals TAL TAM SW846 3005A Anions, Ion Chromatography TAL TAM MCAWW 300.0 Carbon, Dissolved and Dissolved Inorganic TAL SAV SW846 9060 Sample Filtration, Field TAL SAV FIELD_FLTRD Alkalinity TAL TAM SM SM 2320B Solids, Total Dissolved (TDS) TAL TAM SM SM 2540C Sulfide, Total TAL TAM SM SM 4500 S2 F Field Sampling TAL TAM EPA Field Sampling Lab

References:

TAL SAV = TestAmerica Savannah TAL TAL = TestAmerica Tallahassee TAL TAM = TestAmerica Tampa Method

References:

EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa Page 9 of 54

METHOD / ANALYST

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Analyst Analyst ID EPA 200.7 Rev 4.4 Wallace, Tiffany B TBW SW846 6010B Fox, Greg GF EPA Field Sampling Sampler, Field FS MCAWW 300.0 Sengsouvanna, Dom DS SW846 9060 Blackshear, Kim KB SM SM 2320B Steward, Tiffany TS SM SM 2540C Oonnoonny, Thomas TO SM SM 4500 S2 F Mostafavifar, Efe EM TestAmerica Tampa Page 10 of 54

SAMPLE

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Date/Time Date/Time Lab Sample ID Client Sample ID Client Matrix Sampled Received 660-35950-1 062410-TPGW-4S Water 06/24/2010 1500 06/25/2010 0830 660-35950-2 062410-TPGW-4M Water 06/24/2010 1330 06/25/2010 0830 660-35950-3 062410-TPGW-4D Water 06/24/2010 1300 06/25/2010 0830 660-35950-4 062410-TPGW-7S Water 06/24/2010 1655 06/25/2010 0830 660-35950-5 062410-TPGW-7M Water 06/24/2010 1715 06/25/2010 0830 660-35950-6 062410-TPGW-7D Water 06/24/2010 1800 06/25/2010 0830 TestAmerica Tampa Page 11 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID: 062410-TPGW-4S Lab Sample ID: 660-35950-1 Date Sampled: 06/24/2010 1500 Client Matrix: Water Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 1019 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 24 I 9.6 100 Iron 220 I 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1427 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Calcium 120 0.10 0.50 Potassium 9.2 0.19 1.0 Magnesium 19 0.020 0.080 Analyte Result (ug/L) Qualifier MDL PQL Boron 64 10 50 Strontium 1300 1.0 5.0 Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 10 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1519 Run Type: DL Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Sodium 250 3.1 5.0 TestAmerica Tampa Page 12 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID: 062410-TPGW-4M Lab Sample ID: 660-35950-2 Date Sampled: 06/24/2010 1330 Client Matrix: Water Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 1022 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 150 9.6 100 Iron 4700 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 10 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1433 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Calcium 620 1.0 5.0 Potassium 280 1.9 10 Magnesium 900 0.20 0.80 Analyte Result (ug/L) Qualifier MDL PQL Boron 1400 100 500 Strontium 8300 10 50 Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 200 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1525 Run Type: DL Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Sodium 7200 62 100 TestAmerica Tampa Page 13 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID: 062410-TPGW-4D Lab Sample ID: 660-35950-3 Date Sampled: 06/24/2010 1300 Client Matrix: Water Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 1026 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 140 9.6 100 Iron 5900 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 10 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1440 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Calcium 620 1.0 5.0 Potassium 420 1.9 10 Magnesium 1100 0.20 0.80 Analyte Result (ug/L) Qualifier MDL PQL Boron 2200 100 500 Strontium 8800 10 50 Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 200 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1531 Run Type: DL Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Sodium 8600 62 100 TestAmerica Tampa Page 14 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID: 062410-TPGW-7S Lab Sample ID: 660-35950-4 Date Sampled: 06/24/2010 1655 Client Matrix: Water Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 1033 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 9.6 U 9.6 100 Iron 340 I 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1537 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Calcium 91 0.10 0.50 Potassium 9.9 0.19 1.0 Magnesium 4.0 0.020 0.080 Sodium 20 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 53 10 50 Strontium 910 1.0 5.0 TestAmerica Tampa Page 15 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID: 062410-TPGW-7M Lab Sample ID: 660-35950-5 Date Sampled: 06/24/2010 1715 Client Matrix: Water Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 1029 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 11 I 9.6 100 Iron 360 I 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1543 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Calcium 91 0.10 0.50 Potassium 9.4 0.19 1.0 Magnesium 4.1 0.020 0.080 Sodium 21 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 53 10 50 Strontium 920 1.0 5.0 TestAmerica Tampa Page 16 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID: 062410-TPGW-7D Lab Sample ID: 660-35950-6 Date Sampled: 06/24/2010 1800 Client Matrix: Water Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method: 200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID: ICP2 Preparation: 200.7 Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 1036 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result (ug/L) Qualifier MDL PQL Barium 9.6 U 9.6 100 Iron 280 I 46 500 6010B Metals (ICP)-Total Recoverable Method: 6010B Analysis Batch: 660-97236 Instrument ID: ICPA Preparation: 3005A Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1724 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result (mg/L) Qualifier MDL PQL Calcium 91 0.10 0.50 Potassium 4.8 0.19 1.0 Magnesium 3.7 0.020 0.080 Sodium 26 0.31 0.50 Analyte Result (ug/L) Qualifier MDL PQL Boron 51 10 50 Strontium 880 1.0 5.0 TestAmerica Tampa Page 17 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID: 062410-TPGW-4S Lab Sample ID: 660-35950-1 Date Sampled: 06/24/2010 1500 Client Matrix: Water Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 1.7 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2149 Chloride 490 mg/L 20 50 100 300.0 Analysis Batch: 660-96938 Date Analyzed: 07/08/2010 0000 Fluoride 0.055 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2149 Sulfate 20 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2149 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 54 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173756 Date Analyzed: 07/08/2010 1654 Alkalinity 200 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1036 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1036 Total Dissolved Solids 1100 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0948 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 18 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID: 062410-TPGW-4M Lab Sample ID: 660-35950-2 Date Sampled: 06/24/2010 1330 Client Matrix: Water Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 47 mg/L 2.7 5.0 100 300.0 Analysis Batch: 660-96938 Date Analyzed: 07/08/2010 0021 Chloride 13000 mg/L 200 500 1000 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2211 Fluoride 0.10 U mg/L 0.10 0.25 5.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0503 Sulfate 1600 mg/L 20 50 100 300.0 Analysis Batch: 660-96938 Date Analyzed: 07/08/2010 0021 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 48 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 210 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1049 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1049 Total Dissolved Solids 28000 mg/L 250 250 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0949 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 19 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID: 062410-TPGW-4D Lab Sample ID: 660-35950-3 Date Sampled: 06/24/2010 1300 Client Matrix: Water Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 54 mg/L 27 50 1000 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2316 Chloride 16000 mg/L 200 500 1000 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2316 Fluoride 0.10 U mg/L 0.10 0.25 5.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0524 Sulfate 1900 mg/L 20 50 100 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2338 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 45 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 200 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1055 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1055 Total Dissolved Solids 33000 mg/L 250 250 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0949 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 20 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID: 062410-TPGW-7S Lab Sample ID: 660-35950-4 Date Sampled: 06/24/2010 1655 Client Matrix: Water Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.18 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2044 Chloride 36 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2044 Fluoride 0.17 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2044 Sulfate 27 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2044 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 44 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 210 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1101 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1101 Total Dissolved Solids 300 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0950 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 21 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID: 062410-TPGW-7M Lab Sample ID: 660-35950-5 Date Sampled: 06/24/2010 1715 Client Matrix: Water Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.17 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2106 Chloride 35 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2106 Fluoride 0.23 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2106 Sulfate 25 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2106 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 47 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 200 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1107 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1107 Total Dissolved Solids 310 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0950 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 22 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID: 062410-TPGW-7D Lab Sample ID: 660-35950-6 Date Sampled: 06/24/2010 1800 Client Matrix: Water Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.21 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2128 Chloride 41 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2128 Fluoride 0.14 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2128 Sulfate 29 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2128 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic 47 mg/L 1.0 1.0 1.0 9060 Carbon-Dissolved Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 200 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1113 Carbonate Alkalinity as CaCO3 1.0 U mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1113 Total Dissolved Solids 320 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0951 Sulfide 1.0 U mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 23 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID: 062410-TPGW-4S Lab Sample ID: 660-35950-1 Date Sampled: 06/24/2010 1500 Client Matrix: Water Date Received: 06/25/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 7.31 SU 1.0 Field 660-97058 06/24/2010 1500 Sampling Field Temperature 24.99 Degrees C 1.0 Field 660-97058 06/24/2010 1500 Sampling Oxygen, Dissolved 1.4 mg/L 1.0 Field 660-97058 06/24/2010 1500 Sampling Specific Conductance 1750 umhos/cm 1.0 Field 660-97058 06/24/2010 1500 Sampling Turbidity 2.52 NTU 1.0 Field 660-97058 06/24/2010 1500 Sampling TestAmerica Tampa Page 24 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID: 062410-TPGW-4M Lab Sample ID: 660-35950-2 Date Sampled: 06/24/2010 1330 Client Matrix: Water Date Received: 06/25/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 6.88 SU 1.0 Field 660-97058 06/24/2010 1330 Sampling Field Temperature 25.66 Degrees C 1.0 Field 660-97058 06/24/2010 1330 Sampling Oxygen, Dissolved 2.3 mg/L 1.0 Field 660-97058 06/24/2010 1330 Sampling Specific Conductance 32010 umhos/cm 1.0 Field 660-97058 06/24/2010 1330 Sampling Turbidity 2.0 NTU 1.0 Field 660-97058 06/24/2010 1330 Sampling TestAmerica Tampa Page 25 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID: 062410-TPGW-4D Lab Sample ID: 660-35950-3 Date Sampled: 06/24/2010 1300 Client Matrix: Water Date Received: 06/25/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 6.92 SU 1.0 Field 660-97058 06/24/2010 1300 Sampling Field Temperature 25.29 Degrees C 1.0 Field 660-97058 06/24/2010 1300 Sampling Oxygen, Dissolved 2.4 mg/L 1.0 Field 660-97058 06/24/2010 1300 Sampling Specific Conductance 37010 umhos/cm 1.0 Field 660-97058 06/24/2010 1300 Sampling Turbidity 0.02 NTU 1.0 Field 660-97058 06/24/2010 1300 Sampling TestAmerica Tampa Page 26 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID: 062410-TPGW-7S Lab Sample ID: 660-35950-4 Date Sampled: 06/24/2010 1655 Client Matrix: Water Date Received: 06/25/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 7.22 SU 1.0 Field 660-97058 06/24/2010 1655 Sampling Field Temperature 24.80 Degrees C 1.0 Field 660-97058 06/24/2010 1655 Sampling Oxygen, Dissolved 2.0 mg/L 1.0 Field 660-97058 06/24/2010 1655 Sampling Specific Conductance 483 umhos/cm 1.0 Field 660-97058 06/24/2010 1655 Sampling Turbidity 3.81 NTU 1.0 Field 660-97058 06/24/2010 1655 Sampling TestAmerica Tampa Page 27 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID: 062410-TPGW-7M Lab Sample ID: 660-35950-5 Date Sampled: 06/24/2010 1715 Client Matrix: Water Date Received: 06/25/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 7.19 SU 1.0 Field 660-97058 06/24/2010 1715 Sampling Field Temperature 25.05 Degrees C 1.0 Field 660-97058 06/24/2010 1715 Sampling Oxygen, Dissolved 1.5 mg/L 1.0 Field 660-97058 06/24/2010 1715 Sampling Specific Conductance 500 umhos/cm 1.0 Field 660-97058 06/24/2010 1715 Sampling Turbidity 2.29 NTU 1.0 Field 660-97058 06/24/2010 1715 Sampling TestAmerica Tampa Page 28 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID: 062410-TPGW-7D Lab Sample ID: 660-35950-6 Date Sampled: 06/24/2010 1800 Client Matrix: Water Date Received: 06/25/2010 0830 Analysis Date Analyzed Analyte Result Qual Units Dil Method Batch Date Prepared Field pH 7.19 SU 1.0 Field 660-97058 06/24/2010 1800 Sampling Field Temperature 25.12 Degrees C 1.0 Field 660-97058 06/24/2010 1800 Sampling Oxygen, Dissolved 2.3 mg/L 1.0 Field 660-97058 06/24/2010 1800 Sampling Specific Conductance 510 umhos/cm 1.0 Field 660-97058 06/24/2010 1800 Sampling Turbidity 1.34 NTU 1.0 Field 660-97058 06/24/2010 1800 Sampling TestAmerica Tampa Page 29 of 54

DATA REPORTING QUALIFIERS Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Lab Section Qualifier Description Metals J3 Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

U Indicates that the compound was analyzed for but not detected.

I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

General Chemistry U Indicates that the compound was analyzed for but not detected.

TestAmerica Tampa Page 30 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 640-70571 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable Lab Sample ID: MB 640-70571/1-A Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/13/2010 0852 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Result Qual MDL PQL Barium 0.96 U 0.96 10 Iron 4.6 U 4.6 50 Lab Control Sample/ Method: 200.7 Rev 4.4 Lab Control Sample Duplicate Recovery Report - Batch: 640-70571 Preparation: 200.7 Total Recoverable LCS Lab Sample ID: LCS 640-70571/2-A Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/13/2010 0856 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 LCSD Lab Sample ID: LCSD 640-70571/3-A Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/13/2010 0859 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100

% Rec.

Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual Barium 101 102 85 - 115 1 20 Iron 102 103 85 - 115 1 20 TestAmerica Tampa Page 31 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Matrix Spike/ Method: 200.7 Rev 4.4 Matrix Spike Duplicate Recovery Report - Batch: 640-70571 Preparation: 200.7 Total Recoverable MS Lab Sample ID: 660-36031-B-1-B MS Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0910 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 MSD Lab Sample ID: 660-36031-B-1-C MSD Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0913 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Barium 101 98 70 - 130 2 20 Iron 99 96 70 - 130 3 20 Duplicate - Batch: 640-70571 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable Lab Sample ID: 660-36031-B-2-B DU Analysis Batch: 640-70850 Instrument ID: ICP2 Client Matrix: Water Prep Batch: 640-70571 Lab File ID: 071310.csv Dilution: 1.0 Units: ug/L Initial Weight/Volume: 5.0 mL Date Analyzed: 07/13/2010 0934 Final Weight/Volume: 50 mL Date Prepared: 07/06/2010 1100 Analyte Sample Result/Qual Result RPD Limit Qual Barium 130 123 2 20 Iron 8600 8340 3 20 TestAmerica Tampa Page 32 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 660-96604 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: MB 660-96604/1-A Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1250 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result Qual MDL PQL Calcium 0.10 U 0.10 0.50 Potassium 0.19 U 0.19 1.0 Magnesium 0.020 U 0.020 0.080 Sodium 0.31 U 0.31 0.50 Method Blank - Batch: 660-96604 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: MB 660-96604/1-A Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1250 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Result Qual MDL PQL Boron 10 U 10 50 Strontium 1.0 U 1.0 5.0 TestAmerica Tampa Page 33 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Lab Control Sample - Batch: 660-96604 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: LCS 660-96604/2-A Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1256 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Spike Amount Result % Rec. Limit Qual Calcium 1.00 1.05 105 75 - 125 Potassium 10.0 10.1 101 75 - 125 Magnesium 1.00 1.03 103 75 - 125 Sodium 10.0 9.85 98 75 - 125 Lab Control Sample - Batch: 660-96604 Method: 6010B Preparation: 3005A Total Recoverable Lab Sample ID: LCS 660-96604/2-A Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Units: ug/L Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1256 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 Analyte Spike Amount Result % Rec. Limit Qual Boron 1000 1020 102 75 - 125 Strontium 1000 1070 107 75 - 125 TestAmerica Tampa Page 34 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Matrix Spike/ Method: 6010B Matrix Spike Duplicate Recovery Report - Batch: 660-96604 Preparation: 3005A Total Recoverable MS Lab Sample ID: 660-36004-B-9-B MS Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1314 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 MSD Lab Sample ID: 660-36004-B-9-C MSD Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1320 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Calcium 93 250 75 - 125 1 20 J3 Potassium 111 113 75 - 125 2 20 Magnesium 103 108 75 - 125 2 20 Sodium 104 92 75 - 125 8 20 Matrix Spike/ Method: 6010B Matrix Spike Duplicate Recovery Report - Batch: 660-96604 Preparation: 3005A Total Recoverable MS Lab Sample ID: 660-36004-B-9-B MS Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1314 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004 MSD Lab Sample ID: 660-36004-B-9-C MSD Analysis Batch: 660-97236 Instrument ID: ICPA Client Matrix: Water Prep Batch: 660-96604 Lab File ID: 10G15A Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 07/15/2010 1320 Final Weight/Volume: 50 mL Date Prepared: 06/30/2010 1004

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Boron 104 105 75 - 125 1 20 Strontium 107 109 75 - 125 2 20 TestAmerica Tampa Page 35 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 660-96938 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-96938/3 Analysis Batch: 660-96938 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 10.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 07/07/2010 1246 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Result Qual MDL PQL Bromide 0.027 U 0.027 0.050 Chloride 0.20 U 0.20 0.50 Sulfate 0.20 U 0.20 0.50 Lab Control Sample - Batch: 660-96938 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-96938/4 Analysis Batch: 660-96938 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 11.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 07/07/2010 1307 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Bromide 1.00 1.00 100 90 - 110 Chloride 10.0 10.1 101 90 - 110 Sulfate 10.0 10.2 102 90 - 110 TestAmerica Tampa Page 36 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Matrix Spike/ Method: 300.0 Matrix Spike Duplicate Recovery Report - Batch: 660-96938 Preparation: N/A MS Lab Sample ID: 660-35992-B-3 MS ^10 Analysis Batch: 660-96938 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 32.0000.TXT Dilution: 10 Initial Weight/Volume:

Date Analyzed: 07/07/2010 2211 Final Weight/Volume: 50 mL Date Prepared: N/A MSD Lab Sample ID: 660-35992-B-3 MSD ^10 Analysis Batch: 660-96938 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 33.0000.TXT Dilution: 10 Initial Weight/Volume:

Date Analyzed: 07/07/2010 2233 Final Weight/Volume: 50 mL Date Prepared: N/A

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Bromide 102 104 90 - 110 1 30 Chloride 102 105 90 - 110 1 30 Sulfate 103 104 90 - 110 1 30 TestAmerica Tampa Page 37 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 660-96989 Method: 300.0 Preparation: N/A Lab Sample ID: MB 660-96989/3 Analysis Batch: 660-96989 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 21.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 07/08/2010 2001 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Result Qual MDL PQL Bromide 0.027 U 0.027 0.050 Chloride 0.20 U 0.20 0.50 Fluoride 0.020 U 0.020 0.050 Sulfate 0.20 U 0.20 0.50 Lab Control Sample - Batch: 660-96989 Method: 300.0 Preparation: N/A Lab Sample ID: LCS 660-96989/4 Analysis Batch: 660-96989 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 22.0000.TXT Dilution: 1.0 Units: mg/L Initial Weight/Volume:

Date Analyzed: 07/08/2010 2022 Final Weight/Volume: 1 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Bromide 1.00 0.976 98 90 - 110 Chloride 10.0 10.2 102 90 - 110 Fluoride 1.00 0.950 95 90 - 110 Sulfate 10.0 10.2 102 90 - 110 TestAmerica Tampa Page 38 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Matrix Spike/ Method: 300.0 Matrix Spike Duplicate Recovery Report - Batch: 660-96989 Preparation: N/A MS Lab Sample ID: 660-35950-2 Analysis Batch: 660-96989 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 28.0000.TXT Dilution: 1000 Initial Weight/Volume:

Date Analyzed: 07/08/2010 2233 Final Weight/Volume: 50 mL Date Prepared: N/A MSD Lab Sample ID: 660-35950-2 Analysis Batch: 660-96989 Instrument ID: DIONEX2 Client Matrix: Water Prep Batch: N/A Lab File ID: 29.0000.TXT Dilution: 1000 Initial Weight/Volume:

Date Analyzed: 07/08/2010 2254 Final Weight/Volume: 50 mL Date Prepared: N/A

% Rec.

Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual Bromide 104 106 90 - 110 1 30 Chloride 104 105 90 - 110 0 30 Fluoride 109 101 90 - 110 8 30 Sulfate 101 101 90 - 110 0 30 TestAmerica Tampa Page 39 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 680-173756 Method: 9060 Preparation: N/A Lab Sample ID: MB 680-173756/1 Analysis Batch: 680-173756 Instrument ID: TOC3 Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL Date Analyzed: 07/08/2010 1654 Final Weight/Volume: 25 mL Date Prepared: N/A Analyte Result Qual PQL PQL Dissolved Inorganic Carbon-Dissolved 1.0 U 1.0 1.0 Dissolved Carbon-Dissolved 1.0 U 1.0 1.0 Lab Control Sample - Batch: 680-173756 Method: 9060 Preparation: N/A Lab Sample ID: LCS 680-173756/2 Analysis Batch: 680-173756 Instrument ID: TOC3 Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL Date Analyzed: 07/08/2010 1654 Final Weight/Volume: 25 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Dissolved Inorganic Carbon-Dissolved 20.0 19.7 98 Dissolved Carbon-Dissolved 20.0 19.7 98 TestAmerica Tampa Page 40 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 680-173757 Method: 9060 Preparation: N/A Lab Sample ID: MB 680-173757/1 Analysis Batch: 680-173757 Instrument ID: TOC3 Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL Date Analyzed: 07/09/2010 0959 Final Weight/Volume: 25 mL Date Prepared: N/A Analyte Result Qual PQL PQL Dissolved Inorganic Carbon-Dissolved 1.0 U 1.0 1.0 Dissolved Carbon-Dissolved 1.0 U 1.0 1.0 Lab Control Sample - Batch: 680-173757 Method: 9060 Preparation: N/A Lab Sample ID: LCS 680-173757/2 Analysis Batch: 680-173757 Instrument ID: TOC3 Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 25 mL Date Analyzed: 07/09/2010 0959 Final Weight/Volume: 25 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Dissolved Inorganic Carbon-Dissolved 20.0 19.3 96 Dissolved Carbon-Dissolved 20.0 19.3 96 TestAmerica Tampa Page 41 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 660-96877 Method: SM 2320B Preparation: N/A Lab Sample ID: MB 660-96877/1 Analysis Batch: 660-96877 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 7.7.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/07/2010 1023 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Result Qual PQL PQL Alkalinity 1.0 U 1.0 1.0 Lab Control Sample - Batch: 660-96877 Method: SM 2320B Preparation: N/A Lab Sample ID: LCS 660-96877/2 Analysis Batch: 660-96877 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 7.7.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/07/2010 1030 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Alkalinity 118 117 99 80 - 120 Duplicate - Batch: 660-96877 Method: SM 2320B Preparation: N/A Lab Sample ID: 660-35950-1 Analysis Batch: 660-96877 Instrument ID: MANTECH Client Matrix: Water Prep Batch: N/A Lab File ID: 7.7.10a.txt Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 07/07/2010 1042 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Sample Result/Qual Result RPD Limit Qual Alkalinity 200 204 2 30 Carbonate Alkalinity as CaCO3 1.0 U 1.0 NC 30 U TestAmerica Tampa Page 42 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 660-96479 Method: SM 2540C Preparation: N/A Lab Sample ID: MB 660-96479/1 Analysis Batch: 660-96479 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/28/2010 0937 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Result Qual PQL PQL Total Dissolved Solids 5.0 U 5.0 5.0 Lab Control Sample - Batch: 660-96479 Method: SM 2540C Preparation: N/A Lab Sample ID: LCS 660-96479/2 Analysis Batch: 660-96479 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 10 mL Date Analyzed: 06/28/2010 0938 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Spike Amount Result % Rec. Limit Qual Total Dissolved Solids 10000 9910 99 80 - 120 Duplicate - Batch: 660-96479 Method: SM 2540C Preparation: N/A Lab Sample ID: 660-35950-6 Analysis Batch: 660-96479 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 50 mL Date Analyzed: 06/28/2010 0951 Final Weight/Volume: 50 mL Date Prepared: N/A Analyte Sample Result/Qual Result RPD Limit Qual Total Dissolved Solids 320 314 1 20 TestAmerica Tampa Page 43 of 54

Quality Control Results Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Method Blank - Batch: 660-96518 Method: SM 4500 S2 F Preparation: N/A Lab Sample ID: MB 660-96518/1 Analysis Batch: 660-96518 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/26/2010 1130 Final Weight/Volume: 250 mL Date Prepared: N/A Analyte Result Qual PQL PQL Sulfide 1.0 U 1.0 1.0 Lab Control Sample/ Method: SM 4500 S2 F Lab Control Sample Duplicate Recovery Report - Batch: 660-96518 Preparation: N/A LCS Lab Sample ID: LCS 660-96518/2 Analysis Batch: 660-96518 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/26/2010 1130 Final Weight/Volume: 250 mL Date Prepared: N/A LCSD Lab Sample ID: LCSD 660-96518/3 Analysis Batch: 660-96518 Instrument ID: No Equipment Assigned Client Matrix: Water Prep Batch: N/A Lab File ID: N/A Dilution: 1.0 Units: mg/L Initial Weight/Volume: 1.0 mL Date Analyzed: 06/26/2010 1130 Final Weight/Volume: 250 mL Date Prepared: N/A

% Rec.

Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual Sulfide 96 98 75 - 125 2 25 TestAmerica Tampa Page 44 of 54

Page 45 of 54 Page 46 of 54 Page 47 of 54 Page 48 of 54 Page 49 of 54 Page 50 of 54 Page 51 of 54 Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35950-1 SDG Number: 35950 Login Number: 35950 List Source: TestAmerica Tampa Creator: McNulty, Carol List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True 4.1, 4.5 degrees C Cu-07 Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the sample IDs on the containers and True 245.1 on coc-not in project, 200.7 to tally in proj.

the COC. but not checked off on coc Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in True diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. True Samples do not require splitting or compositing. True TestAmerica Tampa Page 52 of 54

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35950-1 SDG Number: 35950 Login Number: 35950 List Source: TestAmerica Savannah Creator: Kicklighter, Marilyn List Creation: 06/29/10 02:14 PM List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? N/A There are no discrepancies between the sample IDs on the containers and True the COC.

Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in True diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. N/A Samples do not require splitting or compositing. False TestAmerica Tampa Page 53 of 54

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35950-1 SDG Number: 35950 Login Number: 35950 List Source: TestAmerica Tallahassee Creator: Archie, Datiska List Creation: 07/02/10 12:06 PM List Number: 1 Question T / F/ NA Comment Radioactivity either was not measured or, if measured, is at or below N/A background The cooler's custody seal, if present, is intact. True The cooler or samples do not appear to have been compromised or True tampered with.

Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the sample IDs on the containers and True the COC.

Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs VOA sample vials do not have headspace or bubble is <6mm (1/4") in N/A diameter.

If necessary, staff have been informed of any short hold time or quick TAT True needs Multiphasic samples are not present. N/A Samples do not require splitting or compositing. N/A TestAmerica Tampa Page 54 of 54

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ML102350005: Difference between revisions

Latest revision as of 20:50, 11 March 2020

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