ML102350005

Attachment to 8/20/10 Email from Bbrrct - Data Provided by Sfwmd That Was Collected by FPL for Uprate of Units 3 & 4

ML102350005
Person / Time
Site:	Turkey Point
Issue date:	08/02/2010
From:	Atkins A Testamerica Labs
To:	Foster S Florida Power & Light Co, Office of New Reactors
Kugler A, NRO/DSER/RAP2, 415-2828
References
Job Number 660-35805-1
Download: ML102350005 (144)

Text

ANALYTICAL REPORT Job Number: 660-35805-1 SDG Number: 35805 Job

Description:

FPL Turkey Point Analytical Services For:

Florida Power & Light Company Technical Services - PGD Environmental Water Compliance/Permitting 700 Universe Blvd (JES/JB)

Juno Beach, FL 33408 Attention: Ms. Stacy Foster Approved for release.

Amy Atkins Project Manager I 8/2/2010 3:40 PM Amy Atkins Project Manager I amy.atkins@testamericainc.com 08/02/2010 cc:

Ms. Sharon Ewe Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282; TestAmerica Tallahassee E81005; TestAmerica Savannah E87052 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report.

The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 43

Job Narrative 660-35805-1 Receipt All samples were received in good condition within temperature requirements.

Metals Method 200.7: The following sample was received unpreserved and was preserved upon receipt to the laboratory: 061610-TPGW-5D (660-35805-1). Initial pH was adjusted to <2 with HNO3 lot 2MER0014. Regulatory documents require a 24-hour waiting period from the time of the addition of the acid preservative to the time of digestion.

Method 200.7 Rev 4.4: The following sample was diluted due to the nature of the sample matrix: 061610-TPGW-5D (660-35805-1).

Elevated reporting limits (RLs) are provided.

Method 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for Calcium in batch 96355 were outside control limits with the sample greater than 4x the spike level. The associated laboratory control sample (LCS) recovery met acceptance criteria.

General Chemistry DOC samples were field filtered and preserved in the lab.

Method 300.0: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for batch 96178 were outside control limits for Chloride.

The associated laboratory control sample (LCS) recovery met acceptance criteria.

Method SM 4500 S2 F: Insufficient sample volume was provided to perform batch matrix spike/matrix spike duplicate (MS/MSD) associated with batch 96052 The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.

Page 2 of 43

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35805-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35805 660-35805-1 061610-TPGW-5D SU Field Sampling 6.85 Field pH Degrees C Field Sampling 24.69 Field Temperature mg/L Field Sampling 4.0 Oxygen, Dissolved umhos/cm Field Sampling 29980 Specific Conductance NTU Field Sampling 0.46 Turbidity 5.0 mg/L 300.0 40 Bromide 500 mg/L 300.0 12000 Chloride 50 mg/L 300.0 1300 Sulfate 1.0 mg/L SM 2320B 220 Alkalinity 250 mg/L SM 2540C 21000 Total Dissolved Solids Dissolved 1.0 mg/L 9060 55 Dissolved Inorganic Carbon-Dissolved Total Recoverable 100 ug/L 200.7 Rev 4.4 220 Barium 500 ug/L 200.7 Rev 4.4 1600 Iron 500 ug/L 6010B 1100 Boron 5.0 mg/L 6010B 600 Calcium 10 mg/L 6010B 210 Potassium 50 ug/L 6010B 7800 Strontium 0.80 mg/L 6010B 750 Magnesium 100 mg/L 6010B 6500 Sodium TestAmerica Tampa Page 3 of 43

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35805-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35805 660-35805-2 061610-TPGW-5M SU Field Sampling 6.92 Field pH Degrees C Field Sampling 24.61 Field Temperature mg/L Field Sampling 1.1 Oxygen, Dissolved umhos/cm Field Sampling 21350 Specific Conductance NTU Field Sampling 0.16 Turbidity 5.0 mg/L 300.0 30 Bromide 500 mg/L 300.0 8900 Chloride 50 mg/L 300.0 860 Sulfate 1.0 mg/L SM 2320B 210 Alkalinity 250 mg/L SM 2540C 17000 Total Dissolved Solids Dissolved 1.0 mg/L 9060 54 Dissolved Inorganic Carbon-Dissolved Total Recoverable 10 ug/L 200.7 Rev 4.4 260 Barium 50 ug/L 200.7 Rev 4.4 5400 Iron 500 ug/L 6010B 580 Boron 5.0 mg/L 6010B 570 Calcium 10 mg/L 6010B 120 Potassium 50 ug/L 6010B 6800 Strontium 0.80 mg/L 6010B 540 Magnesium 100 mg/L 6010B 4900 Sodium TestAmerica Tampa Page 4 of 43

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35805-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35805 660-35805-3 061610-TPGW-5S SU Field Sampling 7.47 Field pH Degrees C Field Sampling 25.80 Field Temperature mg/L Field Sampling 1.2 Oxygen, Dissolved umhos/cm Field Sampling 958 Specific Conductance NTU Field Sampling 5.27 Turbidity 0.050 mg/L 300.0 0.74 Bromide 5.0 mg/L 300.0 210 Chloride 0.050 mg/L 300.0 0.051 Fluoride 0.50 mg/L 300.0 19 Sulfate 1.0 mg/L SM 2320B 240 Alkalinity 5.0 mg/L SM 2540C 690 Total Dissolved Solids Dissolved 1.0 mg/L 9060 62 Dissolved Inorganic Carbon-Dissolved Total Recoverable 10 ug/L 200.7 Rev 4.4 40 Barium 50 ug/L 200.7 Rev 4.4 560 Iron 50 ug/L 6010B 54 Boron 0.50 mg/L 6010B 130 Calcium 1.0 mg/L 6010B 7.7 Potassium 5.0 ug/L 6010B 1300 Strontium 0.080 mg/L 6010B 8.4 Magnesium 0.50 mg/L 6010B 110 Sodium TestAmerica Tampa Page 5 of 43

METHOD

SUMMARY

Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Preparation Method Method Lab Location Description Matrix:

Water EPA 200.7 Rev 4.4 Metals (ICP)

TAL TAL EPA 200.7 TAL TAL Preparation, Total Recoverable Metals SW846 6010B Metals (ICP)

TAL TAM SW846 3005A TAL TAM Preparation, Total Recoverable or Dissolved Metals MCAWW 300.0 Anions, Ion Chromatography TAL TAM SW846 9060 Carbon, Dissolved and Dissolved Inorganic TAL SAV FIELD_FLTRD TAL SAV Sample Filtration, Field SM SM 2320B Alkalinity TAL TAM SM SM 2540C Solids, Total Dissolved (TDS)

TAL TAM SM SM 4500 S2 F Sulfide, Total TAL TAM EPA Field Sampling Field Sampling TAL TAM Lab

References:

TAL SAV = TestAmerica Savannah TAL TAL = TestAmerica Tallahassee TAL TAM = TestAmerica Tampa Method

References:

EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa Page 6 of 43

METHOD / ANALYST

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35805-1 Method Analyst Analyst ID Sdg Number: 35805 Neal, Amanda J AJN EPA 200.7 Rev 4.4 Wallace, Tiffany B TBW EPA 200.7 Rev 4.4 Fox, Greg GF SW846 6010B Sampler, Field FS EPA Field Sampling Sengsouvanna, Dom DS MCAWW 300.0 Blackshear, Kim KB SW846 9060 Steward, Tiffany TS SM SM 2320B Oonnoonny, Thomas TO SM SM 2540C Mostafavifar, Efe EM SM SM 4500 S2 F TestAmerica Tampa Page 7 of 43

SAMPLE

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Client Sample ID Lab Sample ID Client Matrix Date/Time Sampled Date/Time Received 06/16/2010 1336 06/17/2010 0840 061610-TPGW-5D 660-35805-1 Water 06/16/2010 1445 06/17/2010 0840 061610-TPGW-5M 660-35805-2 Water 06/16/2010 1230 06/17/2010 0840 061610-TPGW-5S 660-35805-3 Water TestAmerica Tampa Page 8 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Client Sample ID:

Lab Sample ID:

061610-TPGW-5D Client Matrix:

660-35805-1 Water Date Sampled: 06/16/2010 1336 Date Received: 06/17/2010 0840 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70408 Instrument ID:

Preparation:

Prep Batch: 640-70149 Lab File ID:

062910.csv Dilution:

10 Initial Weight/Volume:

50 mL Date Analyzed:

06/29/2010 0856 Final Weight/Volume:

50 mL Date Prepared:

06/22/2010 1000 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 220 100 9.6 Barium 1600 500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-96428 Instrument ID:

Preparation:

Prep Batch: 660-96355 Lab File ID:

10F25A Dilution:

10 Initial Weight/Volume:

50 mL Date Analyzed:

06/25/2010 0909 Final Weight/Volume:

50 mL Date Prepared:

06/24/2010 0908 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 600 5.0 1.0 Calcium 210 10 1.9 Potassium 750 0.80 0.20 Magnesium Analyte Result (ug/L)

Qualifier MDL PQL 1100 500 100 Boron 7800 50 10 Strontium Method:

6010B Analysis Batch: 660-96428 Instrument ID:

Preparation:

Prep Batch: 660-96355 Lab File ID:

10F25A Dilution:

200 Initial Weight/Volume:

50 mL Date Analyzed:

06/25/2010 1025 Run Type:

DL Final Weight/Volume:

50 mL Date Prepared:

06/24/2010 0908 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 6500 100 62 Sodium TestAmerica Tampa Page 9 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Client Sample ID:

Lab Sample ID:

061610-TPGW-5M Client Matrix:

660-35805-2 Water Date Sampled: 06/16/2010 1445 Date Received: 06/17/2010 0840 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70371 Instrument ID:

Preparation:

Prep Batch: 640-70149 Lab File ID:

N/A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

06/28/2010 1320 Final Weight/Volume:

50 mL Date Prepared:

06/22/2010 1000 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 260 10 0.96 Barium 5400 50 4.6 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-96428 Instrument ID:

Preparation:

Prep Batch: 660-96355 Lab File ID:

10F25A Dilution:

10 Initial Weight/Volume:

50 mL Date Analyzed:

06/25/2010 0915 Final Weight/Volume:

50 mL Date Prepared:

06/24/2010 0908 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 570 5.0 1.0 Calcium 120 10 1.9 Potassium 540 0.80 0.20 Magnesium Analyte Result (ug/L)

Qualifier MDL PQL 580 500 100 Boron 6800 50 10 Strontium Method:

6010B Analysis Batch: 660-96428 Instrument ID:

Preparation:

Prep Batch: 660-96355 Lab File ID:

10F25A Dilution:

200 Initial Weight/Volume:

50 mL Date Analyzed:

06/25/2010 1031 Run Type:

DL Final Weight/Volume:

50 mL Date Prepared:

06/24/2010 0908 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 4900 100 62 Sodium TestAmerica Tampa Page 10 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Client Sample ID:

Lab Sample ID:

061610-TPGW-5S Client Matrix:

660-35805-3 Water Date Sampled: 06/16/2010 1230 Date Received: 06/17/2010 0840 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70371 Instrument ID:

Preparation:

Prep Batch: 640-70149 Lab File ID:

N/A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

06/28/2010 1325 Final Weight/Volume:

50 mL Date Prepared:

06/22/2010 1000 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 40 10 0.96 Barium 560 50 4.6 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-96375 Instrument ID:

Preparation:

Prep Batch: 660-96355 Lab File ID:

10F24A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

06/24/2010 1610 Final Weight/Volume:

50 mL Date Prepared:

06/24/2010 0908 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 130 0.50 0.10 Calcium 7.7 1.0 0.19 Potassium 8.4 0.080 0.020 Magnesium 110 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 54 50 10 Boron 1300 5.0 1.0 Strontium TestAmerica Tampa Page 11 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 General Chemistry Client Sample ID:

Lab Sample ID:

061610-TPGW-5D Client Matrix:

660-35805-1 Water Date Sampled: 06/16/2010 1336 Date Received: 06/17/2010 0840 Analyte Result Qual Units MDL PQL Dil Method Bromide 40 mg/L 2.7 5.0 100 300.0 Analysis Batch: 660-96235 Date Analyzed: 06/21/2010 2122 Chloride 12000 mg/L 200 500 1000 300.0 Analysis Batch: 660-96392 Date Analyzed: 06/23/2010 2159 Fluoride 0.040 U

mg/L 0.040 0.10 2.0 300.0 Analysis Batch: 660-96606 Date Analyzed: 06/29/2010 2107 Sulfate 1300 mg/L 20 50 100 300.0 Analysis Batch: 660-96235 Date Analyzed: 06/21/2010 2122 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 55 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-172887 Date Analyzed: 06/28/2010 1127 Alkalinity 220 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1355 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1355 Total Dissolved Solids 21000 mg/L 250 250 1.0 SM 2540C Analysis Batch: 660-96110 Date Analyzed: 06/18/2010 1330 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96052 Date Analyzed: 06/17/2010 1640 TestAmerica Tampa Page 12 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 General Chemistry Client Sample ID:

Lab Sample ID:

061610-TPGW-5M Client Matrix:

660-35805-2 Water Date Sampled: 06/16/2010 1445 Date Received: 06/17/2010 0840 Analyte Result Qual Units MDL PQL Dil Method Bromide 30 mg/L 2.7 5.0 100 300.0 Analysis Batch: 660-96235 Date Analyzed: 06/21/2010 2144 Chloride 8900 mg/L 200 500 1000 300.0 Analysis Batch: 660-96392 Date Analyzed: 06/23/2010 2220 Fluoride 0.040 U

mg/L 0.040 0.10 2.0 300.0 Analysis Batch: 660-96606 Date Analyzed: 06/29/2010 2125 Sulfate 860 mg/L 20 50 100 300.0 Analysis Batch: 660-96235 Date Analyzed: 06/21/2010 2144 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 54 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-172887 Date Analyzed: 06/28/2010 1127 Alkalinity 210 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1408 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1408 Total Dissolved Solids 17000 mg/L 250 250 1.0 SM 2540C Analysis Batch: 660-96110 Date Analyzed: 06/18/2010 1330 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96052 Date Analyzed: 06/17/2010 1640 TestAmerica Tampa Page 13 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 General Chemistry Client Sample ID:

Lab Sample ID:

061610-TPGW-5S Client Matrix:

660-35805-3 Water Date Sampled: 06/16/2010 1230 Date Received: 06/17/2010 0840 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.74 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96178 Date Analyzed: 06/19/2010 0958 Chloride 210 mg/L 2.0 5.0 10 300.0 Analysis Batch: 660-96101 Date Analyzed: 06/17/2010 1919 Fluoride 0.051 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96178 Date Analyzed: 06/19/2010 0958 Sulfate 19 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96178 Date Analyzed: 06/19/2010 0958 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 62 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-172887 Date Analyzed: 06/28/2010 1127 Alkalinity 240 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1414 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96198 Date Analyzed: 06/21/2010 1414 Total Dissolved Solids 690 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96110 Date Analyzed: 06/18/2010 1331 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96052 Date Analyzed: 06/17/2010 1640 TestAmerica Tampa Page 14 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

061610-TPGW-5D Client Matrix:

660-35805-1 Water Date Sampled: 06/16/2010 1336 Date Received: 06/17/2010 0840 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 6.85 SU 1.0 Field Sampling 660-97058 06/16/2010 1336 Field Temperature 24.69 Degrees C 1.0 Field Sampling 660-97058 06/16/2010 1336 Oxygen, Dissolved 4.0 mg/L 1.0 Field Sampling 660-97058 06/16/2010 1336 Specific Conductance 29980 umhos/cm 1.0 Field Sampling 660-97058 06/16/2010 1336 Turbidity 0.46 NTU 1.0 Field Sampling 660-97058 06/16/2010 1336 TestAmerica Tampa Page 15 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

061610-TPGW-5M Client Matrix:

660-35805-2 Water Date Sampled: 06/16/2010 1445 Date Received: 06/17/2010 0840 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 6.92 SU 1.0 Field Sampling 660-97058 06/16/2010 1445 Field Temperature 24.61 Degrees C 1.0 Field Sampling 660-97058 06/16/2010 1445 Oxygen, Dissolved 1.1 mg/L 1.0 Field Sampling 660-97058 06/16/2010 1445 Specific Conductance 21350 umhos/cm 1.0 Field Sampling 660-97058 06/16/2010 1445 Turbidity 0.16 NTU 1.0 Field Sampling 660-97058 06/16/2010 1445 TestAmerica Tampa Page 16 of 43

Analytical Data Client: Florida Power & Light Company Job Number: 660-35805-1 Sdg Number: 35805 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

061610-TPGW-5S Client Matrix:

660-35805-3 Water Date Sampled: 06/16/2010 1230 Date Received: 06/17/2010 0840 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 7.47 SU 1.0 Field Sampling 660-97058 06/16/2010 1230 Field Temperature 25.80 Degrees C 1.0 Field Sampling 660-97058 06/16/2010 1230 Oxygen, Dissolved 1.2 mg/L 1.0 Field Sampling 660-97058 06/16/2010 1230 Specific Conductance 958 umhos/cm 1.0 Field Sampling 660-97058 06/16/2010 1230 Turbidity 5.27 NTU 1.0 Field Sampling 660-97058 06/16/2010 1230 TestAmerica Tampa Page 17 of 43

DATA REPORTING QUALIFIERS Client: Florida Power & Light Company Job Number: 660-35805-1 Lab Section Qualifier Description Sdg Number: 35805 Metals Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

J3 Indicates that the compound was analyzed for but not detected.

U The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

I General Chemistry Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

J3 Indicates that the compound was analyzed for but not detected.

U TestAmerica Tampa Page 18 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/28/2010 1149 Method Blank - Batch: 640-70149 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 640-70371 Prep Batch: 640-70149 06/22/2010 1000 50 mL 50 mL Units:

ug/L Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable N/A ICP2 MB 640-70149/1-A Analyte Result Qual MDL PQL 0.96 U

10 0.96 Barium 4.6 U

50 4.6 Iron Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/28/2010 1154 06/28/2010 1159 Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 640-70149 1.0 1.0 Water LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L 06/22/2010 1000 Prep Batch: 640-70149 Analysis Batch: 640-70371 50 mL 50 mL 50 mL 50 mL ug/L 06/22/2010 1000 Analysis Batch: 640-70371 Prep Batch: 640-70149 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable N/A N/A ICP2 ICP2 LCS 640-70149/2-A LCSD 640-70149/3-A Analyte LCSD Qual LCS Qual RPD Limit RPD Limit LCSD LCS

% Rec.

100 98 85 - 115 2

20 Barium 98 97 85 - 115 2

20 Iron TestAmerica Tampa Page 19 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/29/2010 0805 06/29/2010 0810 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 640-70149 10 10 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 640-70408 Analysis Batch: 640-70408 06/22/2010 1000 06/22/2010 1000 Prep Batch: 640-70149 Prep Batch: 640-70149 062910.csv 50 mL 50 mL 062910.csv 50 mL 50 mL Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 ICP2 660-35826-G-1-B MS 660-35826-G-1-C MSD Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

106 108 70 - 130 1

20 Barium 89 90 70 - 130 1

20 Iron ug/L Units:

Water Dilution:

10 Date Analyzed:

Duplicate - Batch: 640-70149 Lab Sample ID:

Client Matrix:

Date Prepared:

06/29/2010 0828 06/22/2010 1000 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 640-70408 Prep Batch: 640-70149 062910.csv 50 mL 50 mL Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 660-35826-G-2-B DU Analyte Qual Limit RPD Result Sample Result/Qual 85.5 110 26 20 I J3 Barium 1690 1700 1

20 Iron TestAmerica Tampa Page 20 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/24/2010 1421 Method Blank - Batch: 660-96355 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96375 Prep Batch: 660-96355 06/24/2010 0908 10F24A 50 mL 50 mL Units:

mg/L Method: 6010B Preparation: 3005A Total Recoverable ICPA MB 660-96355/1-A Analyte Result Qual MDL PQL 0.10 U

0.50 0.10 Calcium 0.19 U

1.0 0.19 Potassium 0.020 U

0.080 0.020 Magnesium 0.31 U

0.50 0.31 Sodium Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/24/2010 1421 Method Blank - Batch: 660-96355 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96375 Prep Batch: 660-96355 06/24/2010 0908 10F24A 50 mL 50 mL Units:

ug/L Method: 6010B Preparation: 3005A Total Recoverable ICPA MB 660-96355/1-A Analyte Result Qual MDL PQL 10 U

50 10 Boron 1.0 U

5.0 1.0 Strontium TestAmerica Tampa Page 21 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water 1.0 06/24/2010 1427 Date Analyzed:

Lab Control Sample - Batch: 660-96355 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

10F24A 06/24/2010 0908 Analysis Batch: 660-96375 Prep Batch: 660-96355 50 mL 50 mL Units:

mg/L Method: 6010B Preparation: 3005A Total Recoverable ICPA LCS 660-96355/2-A Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 1.01 101 75 - 125 Calcium 10.0 10.3 103 75 - 125 Potassium 1.00 1.01 101 75 - 125 Magnesium 10.0 10.2 102 75 - 125 Sodium Water 1.0 06/24/2010 1427 Date Analyzed:

Lab Control Sample - Batch: 660-96355 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

10F24A 06/24/2010 0908 Analysis Batch: 660-96375 Prep Batch: 660-96355 50 mL 50 mL Units:

ug/L Method: 6010B Preparation: 3005A Total Recoverable ICPA LCS 660-96355/2-A Analyte Qual Limit

% Rec.

Result Spike Amount 1000 1010 101 75 - 125 Boron 1000 1090 109 75 - 125 Strontium TestAmerica Tampa Page 22 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/24/2010 1446 06/24/2010 1452 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96355 1.0 1.0 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96375 Analysis Batch: 660-96375 06/24/2010 0908 06/24/2010 0908 Prep Batch: 660-96355 Prep Batch: 660-96355 10F24A 50 mL 50 mL 10F24A 50 mL 50 mL Method: 6010B Preparation: 3005A Total Recoverable ICPA ICPA 660-35887-E-1-B MS 660-35887-E-1-C MSD Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

246 233 75 - 125 0

20 J3 J3 Calcium 122 124 75 - 125 1

20 Potassium 108 110 75 - 125 0

20 Magnesium 111 101 75 - 125 1

20 Sodium Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/24/2010 1446 06/24/2010 1452 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96355 1.0 1.0 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96375 Analysis Batch: 660-96375 06/24/2010 0908 06/24/2010 0908 Prep Batch: 660-96355 Prep Batch: 660-96355 10F24A 50 mL 50 mL 10F24A 50 mL 50 mL Method: 6010B Preparation: 3005A Total Recoverable ICPA ICPA 660-35887-E-1-B MS 660-35887-E-1-C MSD Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

105 105 75 - 125 1

20 Boron 108 110 75 - 125 1

20 Strontium TestAmerica Tampa Page 23 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/17/2010 1531 Method Blank - Batch: 660-96101 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96101 Prep Batch: N/A 11.0000.TXT 5 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX 1 MB 660-96101/3 Analyte Result Qual MDL PQL 0.20 U

0.50 0.20 Chloride Water 1.0 06/17/2010 1549 Date Analyzed:

Lab Control Sample - Batch: 660-96101 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

12.0000.TXT N/A Analysis Batch: 660-96101 Prep Batch: N/A 5 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX 1 LCS 660-96101/4 Analyte Qual Limit

% Rec.

Result Spike Amount 10.0 10.6 106 90 - 110 Chloride Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/17/2010 1624 06/17/2010 1641 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96101 5.0 5.0 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96101 Analysis Batch: 660-96101 Prep Batch: N/A Prep Batch: N/A 14.0000.TXT 50 mL 15.0000.TXT 50 mL Method: 300.0 Preparation: N/A N/A N/A DIONEX 1 DIONEX 1 660-35696-G-5 MS ^5 660-35696-G-5 MSD ^5 Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

102 102 90 - 110 0

30 Chloride TestAmerica Tampa Page 24 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/19/2010 0516 Method Blank - Batch: 660-96178 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96178 Prep Batch: N/A 44.0000.TXT 1 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 MB 660-96178/3 Analyte Result Qual MDL PQL 0.027 U

0.050 0.027 Bromide 0.20 U

0.50 0.20 Chloride 0.020 U

0.050 0.020 Fluoride 0.20 U

0.50 0.20 Sulfate Water 1.0 06/19/2010 0538 Date Analyzed:

Lab Control Sample - Batch: 660-96178 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

45.0000.TXT N/A Analysis Batch: 660-96178 Prep Batch: N/A 1 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 LCS 660-96178/4 Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 0.975 98 90 - 110 Bromide 10.0 10.2 102 90 - 110 Chloride 1.00 1.01 101 90 - 110 Fluoride 10.0 10.0 100 90 - 110 Sulfate TestAmerica Tampa Page 25 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/19/2010 0831 06/19/2010 0853 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96178 10 10 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96178 Analysis Batch: 660-96178 Prep Batch: N/A Prep Batch: N/A 53.0000.TXT 50 mL 54.0000.TXT 50 mL Method: 300.0 Preparation: N/A N/A N/A DIONEX2 DIONEX2 660-35749-J-3 MS ^10 660-35749-J-3 MSD ^10 Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

110 110 90 - 110 0

30 Bromide 112 112 90 - 110 0

30 J3 J3 Chloride 104 105 90 - 110 1

30 Fluoride 105 105 90 - 110 0

30 Sulfate TestAmerica Tampa Page 26 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/21/2010 1745 Method Blank - Batch: 660-96235 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96235 Prep Batch: N/A 11.0000.TXT 1 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 MB 660-96235/3 Analyte Result Qual MDL PQL 0.027 U

0.050 0.027 Bromide 0.20 U

0.50 0.20 Sulfate Water 1.0 06/21/2010 1807 Date Analyzed:

Lab Control Sample - Batch: 660-96235 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

12.0000.TXT N/A Analysis Batch: 660-96235 Prep Batch: N/A 1 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 LCS 660-96235/4 Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 0.924 92 90 - 110 Bromide 10.0 9.37 94 90 - 110 Sulfate TestAmerica Tampa Page 27 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/21/2010 1850 06/21/2010 1912 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96235 25 25 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96235 Analysis Batch: 660-96235 Prep Batch: N/A Prep Batch: N/A 14.0000.TXT 50 mL 15.0000.TXT 50 mL Method: 300.0 Preparation: N/A N/A N/A DIONEX2 DIONEX2 660-35749-J-1 MS ^25 660-35749-J-1 MSD ^25 Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

102 105 90 - 110 4

30 Bromide 94 104 90 - 110 3

30 Sulfate TestAmerica Tampa Page 28 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/23/2010 2010 Method Blank - Batch: 660-96392 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96392 Prep Batch: N/A 43.0000.TXT 1 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 MB 660-96392/3 Analyte Result Qual MDL PQL 0.20 U

0.50 0.20 Chloride Water 1.0 06/23/2010 2137 Date Analyzed:

Lab Control Sample - Batch: 660-96392 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

44.0000.TXT N/A Analysis Batch: 660-96392 Prep Batch: N/A 1 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 LCS 660-96392/4 Analyte Qual Limit

% Rec.

Result Spike Amount 10.0 10.1 101 90 - 110 Chloride Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/24/2010 0157 06/24/2010 0219 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96392 100 100 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96392 Analysis Batch: 660-96392 Prep Batch: N/A Prep Batch: N/A 56.0000.TXT 50 mL 57.0000.TXT 50 mL Method: 300.0 Preparation: N/A N/A N/A DIONEX2 DIONEX2 660-35841-B-1 MS ^100 660-35841-B-1 MSD Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

105 108 90 - 110 3

30 Chloride TestAmerica Tampa Page 29 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/29/2010 1721 Method Blank - Batch: 660-96606 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96606 Prep Batch: N/A 11.0000.TXT 5 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX 1 MB 660-96606/3 Analyte Result Qual MDL PQL 0.020 U

0.050 0.020 Fluoride Water 1.0 06/29/2010 1838 Date Analyzed:

Lab Control Sample - Batch: 660-96606 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

12.0000.TXT N/A Analysis Batch: 660-96606 Prep Batch: N/A 5 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX 1 LCS 660-96606/4 Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 1.01 101 90 - 110 Fluoride Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/29/2010 1949 06/29/2010 2006 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96606 10 10 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96606 Analysis Batch: 660-96606 Prep Batch: N/A Prep Batch: N/A 16.0000.TXT 50 mL 17.0000.TXT 50 mL Method: 300.0 Preparation: N/A N/A N/A DIONEX 1 DIONEX 1 660-35863-I-7 MS ^10 660-35863-I-7 MSD ^10 Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

95 95 90 - 110 0

30 Fluoride TestAmerica Tampa Page 30 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/28/2010 1127 Method Blank - Batch: 680-172887 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 680-172887 Prep Batch: N/A 25 mL 25 mL N/A Units:

mg/L Method: 9060 Preparation: N/A N/A TOC3 MB 680-172887/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Dissolved Inorganic Carbon-Dissolved 1.0 U

1.0 1.0 Dissolved Carbon-Dissolved Water 1.0 06/28/2010 1127 Date Analyzed:

Lab Control Sample - Batch: 680-172887 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

N/A Analysis Batch: 680-172887 Prep Batch: N/A 25 mL 25 mL Units:

mg/L Method: 9060 Preparation: N/A N/A TOC3 LCS 680-172887/2 Analyte Qual Limit

% Rec.

Result Spike Amount 20.0 19.7 98 Dissolved Inorganic Carbon-Dissolved 20.0 19.7 98 Dissolved Carbon-Dissolved TestAmerica Tampa Page 31 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/21/2010 1342 Method Blank - Batch: 660-96198 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96198 Prep Batch: N/A 6.21.10a.txt 50 mL 50 mL N/A Units:

mg/L Method: SM 2320B Preparation: N/A MANTECH MB 660-96198/3 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Alkalinity Water 1.0 06/21/2010 1349 Date Analyzed:

Lab Control Sample - Batch: 660-96198 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

6.21.10a.txt N/A Analysis Batch: 660-96198 Prep Batch: N/A 50 mL 50 mL Units:

mg/L Method: SM 2320B Preparation: N/A MANTECH LCS 660-96198/4 Analyte Qual Limit

% Rec.

Result Spike Amount 118 120 101 80 - 120 Alkalinity mg/L Units:

Water Dilution:

1.0 Date Analyzed:

Duplicate - Batch: 660-96198 Lab Sample ID:

Client Matrix:

Date Prepared:

06/21/2010 1402 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96198 Prep Batch: N/A 6.21.10a.txt 50 mL 50 mL N/A Method: SM 2320B Preparation: N/A MANTECH 660-35805-1 Analyte Qual Limit RPD Result Sample Result/Qual 221 220 0

30 Alkalinity 1.0 1.0 U

NC 30 U

Carbonate Alkalinity as CaCO3 TestAmerica Tampa Page 32 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/18/2010 1324 Method Blank - Batch: 660-96110 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96110 Prep Batch: N/A 50 mL 50 mL N/A Units:

mg/L Method: SM 2540C Preparation: N/A N/A No Equipment Assigned MB 660-96110/1 Analyte Result Qual PQL PQL 5.0 U

5.0 5.0 Total Dissolved Solids Water 1.0 06/18/2010 1325 Date Analyzed:

Lab Control Sample - Batch: 660-96110 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

N/A Analysis Batch: 660-96110 Prep Batch: N/A 10 mL 50 mL Units:

mg/L Method: SM 2540C Preparation: N/A N/A No Equipment Assigned LCS 660-96110/2 Analyte Qual Limit

% Rec.

Result Spike Amount 10000 9950 100 80 - 120 Total Dissolved Solids mg/L Units:

Water Dilution:

1.0 Date Analyzed:

Duplicate - Batch: 660-96110 Lab Sample ID:

Client Matrix:

Date Prepared:

06/18/2010 1327 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96110 Prep Batch: N/A 50 mL 50 mL N/A Method: SM 2540C Preparation: N/A N/A No Equipment Assigned 660-35787-D-1 DU Analyte Qual Limit RPD Result Sample Result/Qual 1150 1100 0

20 Total Dissolved Solids TestAmerica Tampa Page 33 of 43

Quality Control Results Job Number: 660-35805-1 Client: Florida Power & Light Company Sdg Number: 35805 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/17/2010 1640 Method Blank - Batch: 660-96052 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96052 Prep Batch: N/A 1.0 mL 250 mL N/A Units:

mg/L Method: SM 4500 S2 F Preparation: N/A N/A No Equipment Assigned MB 660-96052/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Sulfide Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/17/2010 1640 06/17/2010 1640 Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 660-96052 1.0 1.0 Water LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

mg/L Prep Batch: N/A Analysis Batch: 660-96052 N/A 1.0 mL 250 mL 1.0 mL 250 mL mg/L Analysis Batch: 660-96052 Prep Batch: N/A Method: SM 4500 S2 F Preparation: N/A N/A N/A N/A No Equipment Assigned No Equipment Assigned LCS 660-96052/2 LCSD 660-96052/3 Analyte LCSD Qual LCS Qual RPD Limit RPD Limit LCSD LCS

% Rec.

98 98 75 - 125 0

25 Sulfide TestAmerica Tampa Page 34 of 43

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Page 40 of 43

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35805-1 SDG Number: 35805 Login Number: 35805 Question T / F/ NA Comment Creator: McNulty, Carol List Source: TestAmerica Tampa List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True 1.1 degrees C Cu-07 Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True no Hg required per PM Is the Field Sampler's name present on COC?

True There are no discrepancies between the sample IDs on the containers and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

True If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

True TestAmerica Tampa Page 41 of 43

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35805-1 SDG Number: 35805 Login Number: 35805 Question T / F/ NA Comment Creator: Daughtry, Beth List Source: TestAmerica Savannah List Creation: 06/18/10 12:27 PM List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

N/A There are no discrepancies between the sample IDs on the containers and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

True If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

N/A Samples do not require splitting or compositing.

N/A TestAmerica Tampa Page 42 of 43

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35805-1 SDG Number: 35805 Login Number: 35805 Question T / F/ NA Comment Creator: Archie, Datiska List Source: TestAmerica Tallahassee List Creation: 06/18/10 10:57 AM List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the sample IDs on the containers and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

N/A If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

N/A Samples do not require splitting or compositing.

N/A TestAmerica Tampa Page 43 of 43

ANALYTICAL REPORT Job Number: 660-35970-1 SDG Number: 35970 Job

Description:

FPL Turkey Point Analytical Services For:

Florida Power & Light Company Technical Services - PGD Environmental Water Compliance/Permitting 700 Universe Blvd (JES/JB)

Juno Beach, FL 33408 Attention: Ms. Stacy Foster Approved for release.

Amy Atkins Project Manager I 8/3/2010 1:30 PM Amy Atkins Project Manager I amy.atkins@testamericainc.com 08/03/2010 cc:

Ms. Sharon Ewe Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282; TestAmerica Tallahassee E81005; TestAmerica Savannah E87052 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report.

The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 47

Job Narrative 660-35970-1 Receipt All samples were received in good condition within temperature requirements.

6010B The matrix spike duplicate (MSD) recovery for Calcium in batch 660-96604 was outside control limits with the sample greater than 4x the spike level. The associated laboratory control sample (LCS) recovery met acceptance criteria.

300.0 The matrix spike / matrix spike duplicate (MS/MSD) recoveries for Chloride in batch 96989 were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria.

300.0 Due to analyst error the matrix spike / matrix spike duplicate (MS/MSD) was not analyzed with the parent sample at a dilution that was reportable. The associated laboratory control sample (LCS) recovery met acceptance criteria.

Page 2 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35970 660-35970-1 062510-TPGW-8M SU Field Sampling 7.06 Field pH Degrees C Field Sampling 25.29 Field Temperature mg/L Field Sampling 10.9 Oxygen, Dissolved umhos/cm Field Sampling 544 Specific Conductance NTU Field Sampling 1.18 Turbidity 0.050 mg/L 300.0 0.18 Bromide 0.50 mg/L 300.0 33 Chloride 0.050 mg/L 300.0 0.068 Fluoride 0.50 mg/L 300.0 43 Sulfate 1.0 mg/L SM 2320B 230 Alkalinity 5.0 mg/L SM 2540C 350 Total Dissolved Solids Dissolved 1.0 mg/L 9060 51 Dissolved Inorganic Carbon-Dissolved Total Recoverable 500 ug/L 200.7 Rev 4.4 550 Iron 50 ug/L 6010B 63 Boron 0.50 mg/L 6010B 110 Calcium 1.0 mg/L 6010B 9.2 Potassium 5.0 ug/L 6010B 1100 Strontium 0.080 mg/L 6010B 3.8 Magnesium 0.50 mg/L 6010B 20 Sodium TestAmerica Tampa Page 3 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35970 660-35970-2 062510-TPGW-8D SU Field Sampling 7.10 Field pH Degrees C Field Sampling 25.23 Field Temperature mg/L Field Sampling 1.6 Oxygen, Dissolved umhos/cm Field Sampling 599 Specific Conductance NTU Field Sampling 4.04 Turbidity 0.050 mg/L 300.0 0.26 Bromide 0.50 mg/L 300.0 47 Chloride 0.050 mg/L 300.0 0.047 I

Fluoride 0.50 mg/L 300.0 49 Sulfate 1.0 mg/L SM 2320B 220 Alkalinity 5.0 mg/L SM 2540C 370 Total Dissolved Solids Dissolved 1.0 mg/L 9060 49 Dissolved Inorganic Carbon-Dissolved Total Recoverable 100 ug/L 200.7 Rev 4.4 12 I

Barium 500 ug/L 200.7 Rev 4.4 310 I

Iron 50 ug/L 6010B 69 Boron 0.50 mg/L 6010B 110 Calcium 1.0 mg/L 6010B 8.5 Potassium 5.0 ug/L 6010B 1100 Strontium 0.080 mg/L 6010B 6.2 Magnesium 0.50 mg/L 6010B 31 Sodium TestAmerica Tampa Page 4 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35970 660-35970-3 062510-TPGW-9S SU Field Sampling 7.13 Field pH Degrees C Field Sampling 25.82 Field Temperature mg/L Field Sampling 2.6 Oxygen, Dissolved umhos/cm Field Sampling 556 Specific Conductance NTU Field Sampling 9.27 Turbidity 0.050 mg/L 300.0 0.30 Bromide 0.50 mg/L 300.0 23 Chloride 0.50 mg/L 300.0 18 Sulfate 1.0 mg/L SM 2320B 250 Alkalinity 5.0 mg/L SM 2540C 330 Total Dissolved Solids 1.0 mg/L SM 4500 S2 F 1.1 Sulfide Dissolved 1.0 mg/L 9060 62 Dissolved Inorganic Carbon-Dissolved Total Recoverable 100 ug/L 200.7 Rev 4.4 12 I

Barium 500 ug/L 200.7 Rev 4.4 190 I

Iron 50 ug/L 6010B 47 I

Boron 0.50 mg/L 6010B 120 Calcium 1.0 mg/L 6010B 11 Potassium 5.0 ug/L 6010B 990 Strontium 0.080 mg/L 6010B 2.9 Magnesium 0.50 mg/L 6010B 14 Sodium TestAmerica Tampa Page 5 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35970 660-35970-4 062510-TPGW-9M SU Field Sampling 6.99 Field pH Degrees C Field Sampling 25.10 Field Temperature mg/L Field Sampling 1.5 Oxygen, Dissolved umhos/cm Field Sampling 563 Specific Conductance NTU Field Sampling 8.49 Turbidity 0.050 mg/L 300.0 0.29 Bromide 0.50 mg/L 300.0 25 Chloride 0.050 mg/L 300.0 0.038 I

Fluoride 0.50 mg/L 300.0 24 Sulfate 1.0 mg/L SM 2320B 270 Alkalinity 5.0 mg/L SM 2540C 350 Total Dissolved Solids Dissolved 1.0 mg/L 9060 60 Dissolved Inorganic Carbon-Dissolved Total Recoverable 500 ug/L 200.7 Rev 4.4 600 Iron 50 ug/L 6010B 48 I

Boron 0.50 mg/L 6010B 120 Calcium 1.0 mg/L 6010B 6.7 Potassium 5.0 ug/L 6010B 990 Strontium 0.080 mg/L 6010B 3.1 Magnesium 0.50 mg/L 6010B 15 Sodium TestAmerica Tampa Page 6 of 47

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35970-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35970 660-35970-5 062510-TPGW-9D SU Field Sampling 6.99 Field pH Degrees C Field Sampling 25.09 Field Temperature mg/L Field Sampling 2.4 Oxygen, Dissolved umhos/cm Field Sampling 564 Specific Conductance NTU Field Sampling 0.83 Turbidity 0.050 mg/L 300.0 0.41 Bromide 0.50 mg/L 300.0 30 Chloride 0.050 mg/L 300.0 0.062 Fluoride 0.50 mg/L 300.0 33 Sulfate 1.0 mg/L SM 2320B 250 Alkalinity 5.0 mg/L SM 2540C 360 Total Dissolved Solids Dissolved 1.0 mg/L 9060 58 Dissolved Inorganic Carbon-Dissolved Total Recoverable 100 ug/L 200.7 Rev 4.4 23 I

Barium 500 ug/L 200.7 Rev 4.4 760 Iron 50 ug/L 6010B 48 I

Boron 0.50 mg/L 6010B 110 Calcium 1.0 mg/L 6010B 3.3 Potassium 5.0 ug/L 6010B 1100 Strontium 0.080 mg/L 6010B 3.6 Magnesium 0.50 mg/L 6010B 22 Sodium TestAmerica Tampa Page 7 of 47

METHOD

SUMMARY

Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Preparation Method Method Lab Location Description Matrix:

Water EPA 200.7 Rev 4.4 Metals (ICP)

TAL TAL EPA 200.7 TAL TAL Preparation, Total Recoverable Metals SW846 6010B Metals (ICP)

TAL TAM SW846 3005A TAL TAM Preparation, Total Recoverable or Dissolved Metals MCAWW 300.0 Anions, Ion Chromatography TAL TAM SW846 9060 Carbon, Dissolved and Dissolved Inorganic TAL SAV FIELD_FLTRD TAL SAV Sample Filtration, Field SM SM 2320B Alkalinity TAL TAM SM SM 2540C Solids, Total Dissolved (TDS)

TAL TAM SM SM 4500 S2 F Sulfide, Total TAL TAM EPA Field Sampling Field Sampling TAL TAM Lab

References:

TAL SAV = TestAmerica Savannah TAL TAL = TestAmerica Tallahassee TAL TAM = TestAmerica Tampa Method

References:

EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa Page 8 of 47

METHOD / ANALYST

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35970-1 Method Analyst Analyst ID Sdg Number: 35970 Wallace, Tiffany B TBW EPA 200.7 Rev 4.4 Fox, Greg GF SW846 6010B Sampler, Field FS EPA Field Sampling Sengsouvanna, Dom DS MCAWW 300.0 Blackshear, Kim KB SW846 9060 Steward, Tiffany TS SM SM 2320B Oonnoonny, Thomas TO SM SM 2540C Mostafavifar, Efe EM SM SM 4500 S2 F TestAmerica Tampa Page 9 of 47

SAMPLE

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID Lab Sample ID Client Matrix Date/Time Sampled Date/Time Received 06/25/2010 1225 06/26/2010 0830 062510-TPGW-8M 660-35970-1 Water 06/25/2010 1200 06/26/2010 0830 062510-TPGW-8D 660-35970-2 Water 06/25/2010 1030 06/26/2010 0830 062510-TPGW-9S 660-35970-3 Water 06/25/2010 0955 06/26/2010 0830 062510-TPGW-9M 660-35970-4 Water 06/25/2010 0930 06/26/2010 0830 062510-TPGW-9D 660-35970-5 Water TestAmerica Tampa Page 10 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID:

Lab Sample ID:

062510-TPGW-8M Client Matrix:

660-35970-1 Water Date Sampled: 06/25/2010 1225 Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 0941 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 9.6 U

100 9.6 Barium 550 500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1742 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1007 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 110 0.50 0.10 Calcium 9.2 1.0 0.19 Potassium 3.8 0.080 0.020 Magnesium 20 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 63 50 10 Boron 1100 5.0 1.0 Strontium TestAmerica Tampa Page 11 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID:

Lab Sample ID:

062510-TPGW-8D Client Matrix:

660-35970-2 Water Date Sampled: 06/25/2010 1200 Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 0944 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 12 I

100 9.6 Barium 310 I

500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1749 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1007 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 110 0.50 0.10 Calcium 8.5 1.0 0.19 Potassium 6.2 0.080 0.020 Magnesium 31 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 69 50 10 Boron 1100 5.0 1.0 Strontium TestAmerica Tampa Page 12 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID:

Lab Sample ID:

062510-TPGW-9S Client Matrix:

660-35970-3 Water Date Sampled: 06/25/2010 1030 Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 0948 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 12 I

100 9.6 Barium 190 I

500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1755 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1007 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 120 0.50 0.10 Calcium 11 1.0 0.19 Potassium 2.9 0.080 0.020 Magnesium 14 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 47 I

50 10 Boron 990 5.0 1.0 Strontium TestAmerica Tampa Page 13 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID:

Lab Sample ID:

062510-TPGW-9M Client Matrix:

660-35970-4 Water Date Sampled: 06/25/2010 0955 Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 0951 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 9.6 U

100 9.6 Barium 600 500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1801 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1007 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 120 0.50 0.10 Calcium 6.7 1.0 0.19 Potassium 3.1 0.080 0.020 Magnesium 15 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 48 I

50 10 Boron 990 5.0 1.0 Strontium TestAmerica Tampa Page 14 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Client Sample ID:

Lab Sample ID:

062510-TPGW-9D Client Matrix:

660-35970-5 Water Date Sampled: 06/25/2010 0930 Date Received: 06/26/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 0955 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 23 I

100 9.6 Barium 760 500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1807 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1010 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 110 0.50 0.10 Calcium 3.3 1.0 0.19 Potassium 3.6 0.080 0.020 Magnesium 22 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 48 I

50 10 Boron 1100 5.0 1.0 Strontium TestAmerica Tampa Page 15 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID:

Lab Sample ID:

062510-TPGW-8M Client Matrix:

660-35970-1 Water Date Sampled: 06/25/2010 1225 Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.18 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0629 Chloride 33 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0629 Fluoride 0.068 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0629 Sulfate 43 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0629 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 51 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 230 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1120 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1120 Total Dissolved Solids 350 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 16 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID:

Lab Sample ID:

062510-TPGW-8D Client Matrix:

660-35970-2 Water Date Sampled: 06/25/2010 1200 Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.26 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0651 Chloride 47 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0651 Fluoride 0.047 I

mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0651 Sulfate 49 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0651 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 49 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 220 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1125 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1125 Total Dissolved Solids 370 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 17 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID:

Lab Sample ID:

062510-TPGW-9S Client Matrix:

660-35970-3 Water Date Sampled: 06/25/2010 1030 Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.30 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0901 Chloride 23 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0901 Fluoride 0.020 U

mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0901 Sulfate 18 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0901 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 62 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 250 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1131 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1131 Total Dissolved Solids 330 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.1 mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 18 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID:

Lab Sample ID:

062510-TPGW-9M Client Matrix:

660-35970-4 Water Date Sampled: 06/25/2010 0955 Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.29 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0923 Chloride 25 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0923 Fluoride 0.038 I

mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0923 Sulfate 24 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0923 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 60 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 270 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1138 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1138 Total Dissolved Solids 350 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 19 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 General Chemistry Client Sample ID:

Lab Sample ID:

062510-TPGW-9D Client Matrix:

660-35970-5 Water Date Sampled: 06/25/2010 0930 Date Received: 06/26/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.41 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0945 Chloride 30 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0945 Fluoride 0.062 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0945 Sulfate 33 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-97030 Date Analyzed: 07/09/2010 0945 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 58 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 250 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1144 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1144 Total Dissolved Solids 360 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96652 Date Analyzed: 06/30/2010 1617 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 20 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062510-TPGW-8M Client Matrix:

660-35970-1 Water Date Sampled: 06/25/2010 1225 Date Received: 06/26/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 7.06 SU 1.0 Field Sampling 660-97058 06/25/2010 1225 Field Temperature 25.29 Degrees C 1.0 Field Sampling 660-97058 06/25/2010 1225 Oxygen, Dissolved 10.9 mg/L 1.0 Field Sampling 660-97058 06/25/2010 1225 Specific Conductance 544 umhos/cm 1.0 Field Sampling 660-97058 06/25/2010 1225 Turbidity 1.18 NTU 1.0 Field Sampling 660-97058 06/25/2010 1225 TestAmerica Tampa Page 21 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062510-TPGW-8D Client Matrix:

660-35970-2 Water Date Sampled: 06/25/2010 1200 Date Received: 06/26/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 7.10 SU 1.0 Field Sampling 660-97058 06/25/2010 1200 Field Temperature 25.23 Degrees C 1.0 Field Sampling 660-97058 06/25/2010 1200 Oxygen, Dissolved 1.6 mg/L 1.0 Field Sampling 660-97058 06/25/2010 1200 Specific Conductance 599 umhos/cm 1.0 Field Sampling 660-97058 06/25/2010 1200 Turbidity 4.04 NTU 1.0 Field Sampling 660-97058 06/25/2010 1200 TestAmerica Tampa Page 22 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062510-TPGW-9S Client Matrix:

660-35970-3 Water Date Sampled: 06/25/2010 1030 Date Received: 06/26/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 7.13 SU 1.0 Field Sampling 660-97058 06/25/2010 1030 Field Temperature 25.82 Degrees C 1.0 Field Sampling 660-97058 06/25/2010 1030 Oxygen, Dissolved 2.6 mg/L 1.0 Field Sampling 660-97058 06/25/2010 1030 Specific Conductance 556 umhos/cm 1.0 Field Sampling 660-97058 06/25/2010 1030 Turbidity 9.27 NTU 1.0 Field Sampling 660-97058 06/25/2010 1030 TestAmerica Tampa Page 23 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062510-TPGW-9M Client Matrix:

660-35970-4 Water Date Sampled: 06/25/2010 0955 Date Received: 06/26/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 6.99 SU 1.0 Field Sampling 660-97058 06/25/2010 0955 Field Temperature 25.10 Degrees C 1.0 Field Sampling 660-97058 06/25/2010 0955 Oxygen, Dissolved 1.5 mg/L 1.0 Field Sampling 660-97058 06/25/2010 0955 Specific Conductance 563 umhos/cm 1.0 Field Sampling 660-97058 06/25/2010 0955 Turbidity 8.49 NTU 1.0 Field Sampling 660-97058 06/25/2010 0955 TestAmerica Tampa Page 24 of 47

Analytical Data Client: Florida Power & Light Company Job Number: 660-35970-1 Sdg Number: 35970 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062510-TPGW-9D Client Matrix:

660-35970-5 Water Date Sampled: 06/25/2010 0930 Date Received: 06/26/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 6.99 SU 1.0 Field Sampling 660-97058 06/25/2010 0930 Field Temperature 25.09 Degrees C 1.0 Field Sampling 660-97058 06/25/2010 0930 Oxygen, Dissolved 2.4 mg/L 1.0 Field Sampling 660-97058 06/25/2010 0930 Specific Conductance 564 umhos/cm 1.0 Field Sampling 660-97058 06/25/2010 0930 Turbidity 0.83 NTU 1.0 Field Sampling 660-97058 06/25/2010 0930 TestAmerica Tampa Page 25 of 47

DATA REPORTING QUALIFIERS Client: Florida Power & Light Company Job Number: 660-35970-1 Lab Section Qualifier Description Sdg Number: 35970 Metals Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

J3 Indicates that the compound was analyzed for but not detected.

U The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

I General Chemistry Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

J3 Indicates that the compound was analyzed for but not detected.

U The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

I TestAmerica Tampa Page 26 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/13/2010 0852 Method Blank - Batch: 640-70571 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 640-70850 Prep Batch: 640-70571 07/06/2010 1100 071310.csv 50 mL 50 mL Units:

ug/L Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 MB 640-70571/1-A Analyte Result Qual MDL PQL 0.96 U

10 0.96 Barium 4.6 U

50 4.6 Iron Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/13/2010 0856 07/13/2010 0859 Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 640-70571 1.0 1.0 Water LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L 07/06/2010 1100 Prep Batch: 640-70571 Analysis Batch: 640-70850 071310.csv 50 mL 50 mL 071310.csv 50 mL 50 mL ug/L 07/06/2010 1100 Analysis Batch: 640-70850 Prep Batch: 640-70571 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 ICP2 LCS 640-70571/2-A LCSD 640-70571/3-A Analyte LCSD Qual LCS Qual RPD Limit RPD Limit LCSD LCS

% Rec.

102 101 85 - 115 1

20 Barium 103 102 85 - 115 1

20 Iron TestAmerica Tampa Page 27 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/13/2010 0910 07/13/2010 0913 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 640-70571 1.0 1.0 Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 640-70850 Analysis Batch: 640-70850 07/06/2010 1100 07/06/2010 1100 Prep Batch: 640-70571 Prep Batch: 640-70571 071310.csv 5.0 mL 50 mL 071310.csv 5.0 mL 50 mL Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 ICP2 660-36031-B-1-B MS 660-36031-B-1-C MSD MS Lab Sample ID:

MSD Lab Sample ID:

Analyte RPD Limit RPD Limit

% Rec.

MS MSD MS Qual MSD Qual 101 98 70 - 130 2

20 Barium 99 96 70 - 130 3

20 Iron ug/L Units:

Water Dilution:

1.0 Date Analyzed:

Duplicate - Batch: 640-70571 Lab Sample ID:

Client Matrix:

Date Prepared:

07/13/2010 0934 07/06/2010 1100 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 640-70850 Prep Batch: 640-70571 071310.csv 5.0 mL 50 mL Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 660-36031-B-2-B DU Analyte Qual Limit RPD Result Sample Result/Qual 123 130 2

20 Barium 8340 8600 3

20 Iron TestAmerica Tampa Page 28 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/15/2010 1250 Method Blank - Batch: 660-96604 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-97236 Prep Batch: 660-96604 06/30/2010 1004 10G15A 50 mL 50 mL Units:

mg/L Method: 6010B Preparation: 3005A Total Recoverable ICPA MB 660-96604/1-A Analyte Result Qual MDL PQL 0.10 U

0.50 0.10 Calcium 0.19 U

1.0 0.19 Potassium 0.020 U

0.080 0.020 Magnesium 0.31 U

0.50 0.31 Sodium Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/15/2010 1250 Method Blank - Batch: 660-96604 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-97236 Prep Batch: 660-96604 06/30/2010 1004 10G15A 50 mL 50 mL Units:

ug/L Method: 6010B Preparation: 3005A Total Recoverable ICPA MB 660-96604/1-A Analyte Result Qual MDL PQL 10 U

50 10 Boron 1.0 U

5.0 1.0 Strontium TestAmerica Tampa Page 29 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water 1.0 07/15/2010 1256 Date Analyzed:

Lab Control Sample - Batch: 660-96604 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

10G15A 06/30/2010 1004 Analysis Batch: 660-97236 Prep Batch: 660-96604 50 mL 50 mL Units:

mg/L Method: 6010B Preparation: 3005A Total Recoverable ICPA LCS 660-96604/2-A Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 1.05 105 75 - 125 Calcium 10.0 10.1 101 75 - 125 Potassium 1.00 1.03 103 75 - 125 Magnesium 10.0 9.85 98 75 - 125 Sodium Water 1.0 07/15/2010 1256 Date Analyzed:

Lab Control Sample - Batch: 660-96604 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

10G15A 06/30/2010 1004 Analysis Batch: 660-97236 Prep Batch: 660-96604 50 mL 50 mL Units:

ug/L Method: 6010B Preparation: 3005A Total Recoverable ICPA LCS 660-96604/2-A Analyte Qual Limit

% Rec.

Result Spike Amount 1000 1020 102 75 - 125 Boron 1000 1070 107 75 - 125 Strontium TestAmerica Tampa Page 30 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/15/2010 1314 07/15/2010 1320 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96604 1.0 1.0 Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-97236 Analysis Batch: 660-97236 06/30/2010 1004 06/30/2010 1004 Prep Batch: 660-96604 Prep Batch: 660-96604 10G15A 50 mL 50 mL 10G15A 50 mL 50 mL Method: 6010B Preparation: 3005A Total Recoverable ICPA ICPA 660-36004-B-9-B MS 660-36004-B-9-C MSD MS Lab Sample ID:

MSD Lab Sample ID:

Analyte RPD Limit RPD Limit

% Rec.

MS MSD MS Qual MSD Qual 93 250 75 - 125 1

20 J3 Calcium 111 113 75 - 125 2

20 Potassium 103 108 75 - 125 2

20 Magnesium 104 92 75 - 125 8

20 Sodium Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/15/2010 1314 07/15/2010 1320 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96604 1.0 1.0 Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-97236 Analysis Batch: 660-97236 06/30/2010 1004 06/30/2010 1004 Prep Batch: 660-96604 Prep Batch: 660-96604 10G15A 50 mL 50 mL 10G15A 50 mL 50 mL Method: 6010B Preparation: 3005A Total Recoverable ICPA ICPA 660-36004-B-9-B MS 660-36004-B-9-C MSD MS Lab Sample ID:

MSD Lab Sample ID:

Analyte RPD Limit RPD Limit

% Rec.

MS MSD MS Qual MSD Qual 104 105 75 - 125 1

20 Boron 107 109 75 - 125 2

20 Strontium TestAmerica Tampa Page 31 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/08/2010 2001 Method Blank - Batch: 660-96989 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96989 Prep Batch: N/A 21.0000.TXT 1 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 MB 660-96989/3 Analyte Result Qual MDL PQL 0.027 U

0.050 0.027 Bromide 0.20 U

0.50 0.20 Chloride 0.020 U

0.050 0.020 Fluoride 0.20 U

0.50 0.20 Sulfate Water 1.0 07/08/2010 2022 Date Analyzed:

Lab Control Sample - Batch: 660-96989 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

22.0000.TXT N/A Analysis Batch: 660-96989 Prep Batch: N/A 1 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 LCS 660-96989/4 Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 0.976 98 90 - 110 Bromide 10.0 10.2 102 90 - 110 Chloride 1.00 0.950 95 90 - 110 Fluoride 10.0 10.2 102 90 - 110 Sulfate TestAmerica Tampa Page 32 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/09/2010 0253 07/09/2010 0314 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96989 10 10 Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96989 Analysis Batch: 660-96989 Prep Batch: N/A Prep Batch: N/A 40.0000.TXT 50 mL 41.0000.TXT 50 mL Method: 300.0 Preparation: N/A N/A N/A DIONEX2 DIONEX2 660-36016-J-3 MS ^10 660-36016-J-3 MSD ^10 MS Lab Sample ID:

MSD Lab Sample ID:

Analyte RPD Limit RPD Limit

% Rec.

MS MSD MS Qual MSD Qual 104 101 90 - 110 3

30 Bromide 118 111 90 - 110 2

30 J3 J3 Chloride 110 108 90 - 110 2

30 Fluoride 109 103 90 - 110 3

30 Sulfate TestAmerica Tampa Page 33 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/09/2010 0818 Method Blank - Batch: 660-97030 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-97030 Prep Batch: N/A 55.0000.TXT 1 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 MB 660-97030/3 Analyte Result Qual MDL PQL 0.027 U

0.050 0.027 Bromide 0.20 U

0.50 0.20 Chloride 0.020 U

0.050 0.020 Fluoride 0.20 U

0.50 0.20 Sulfate Water 1.0 07/09/2010 0840 Date Analyzed:

Lab Control Sample - Batch: 660-97030 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

56.0000.TXT N/A Analysis Batch: 660-97030 Prep Batch: N/A 1 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 LCS 660-97030/4 Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 1.01 101 90 - 110 Bromide 10.0 10.2 102 90 - 110 Chloride 1.00 0.991 99 90 - 110 Fluoride 10.0 10.3 103 90 - 110 Sulfate TestAmerica Tampa Page 34 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/09/2010 0959 Method Blank - Batch: 680-173757 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 680-173757 Prep Batch: N/A 25 mL 25 mL N/A Units:

mg/L Method: 9060 Preparation: N/A N/A TOC3 MB 680-173757/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Dissolved Inorganic Carbon-Dissolved 1.0 U

1.0 1.0 Dissolved Carbon-Dissolved Water 1.0 07/09/2010 0959 Date Analyzed:

Lab Control Sample - Batch: 680-173757 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

N/A Analysis Batch: 680-173757 Prep Batch: N/A 25 mL 25 mL Units:

mg/L Method: 9060 Preparation: N/A N/A TOC3 LCS 680-173757/2 Analyte Qual Limit

% Rec.

Result Spike Amount 20.0 19.3 96 Dissolved Inorganic Carbon-Dissolved 20.0 19.3 96 Dissolved Carbon-Dissolved TestAmerica Tampa Page 35 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/07/2010 1023 Method Blank - Batch: 660-96877 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96877 Prep Batch: N/A 7.7.10a.txt 50 mL 50 mL N/A Units:

mg/L Method: SM 2320B Preparation: N/A MANTECH MB 660-96877/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Alkalinity Water 1.0 07/07/2010 1030 Date Analyzed:

Lab Control Sample - Batch: 660-96877 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

7.7.10a.txt N/A Analysis Batch: 660-96877 Prep Batch: N/A 50 mL 50 mL Units:

mg/L Method: SM 2320B Preparation: N/A MANTECH LCS 660-96877/2 Analyte Qual Limit

% Rec.

Result Spike Amount 118 117 99 80 - 120 Alkalinity mg/L Units:

Water Dilution:

1.0 Date Analyzed:

Duplicate - Batch: 660-96877 Lab Sample ID:

Client Matrix:

Date Prepared:

07/07/2010 1150 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96877 Prep Batch: N/A 7.7.10a.txt 50 mL 50 mL N/A Method: SM 2320B Preparation: N/A MANTECH 660-35970-5 Analyte Qual Limit RPD Result Sample Result/Qual 262 250 4

30 Alkalinity 1.0 1.0 U

NC 30 U

Carbonate Alkalinity as CaCO3 TestAmerica Tampa Page 36 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/30/2010 1617 Method Blank - Batch: 660-96652 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96652 Prep Batch: N/A 50 mL 50 mL N/A Units:

mg/L Method: SM 2540C Preparation: N/A N/A No Equipment Assigned MB 660-96652/1 Analyte Result Qual PQL PQL 5.0 U

5.0 5.0 Total Dissolved Solids Water 1.0 06/30/2010 1617 Date Analyzed:

Lab Control Sample - Batch: 660-96652 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

N/A Analysis Batch: 660-96652 Prep Batch: N/A 10 mL 50 mL Units:

mg/L Method: SM 2540C Preparation: N/A N/A No Equipment Assigned LCS 660-96652/2 Analyte Qual Limit

% Rec.

Result Spike Amount 10000 9990 100 80 - 120 Total Dissolved Solids mg/L Units:

Water Dilution:

1.0 Date Analyzed:

Duplicate - Batch: 660-96652 Lab Sample ID:

Client Matrix:

Date Prepared:

06/30/2010 1617 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96652 Prep Batch: N/A 50 mL 50 mL N/A Method: SM 2540C Preparation: N/A N/A No Equipment Assigned 660-35951-E-3 DU Analyte Qual Limit RPD Result Sample Result/Qual 58.0 56 4

20 Total Dissolved Solids TestAmerica Tampa Page 37 of 47

Quality Control Results Job Number: 660-35970-1 Client: Florida Power & Light Company Sdg Number: 35970 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/26/2010 1130 Method Blank - Batch: 660-96518 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96518 Prep Batch: N/A 1.0 mL 250 mL N/A Units:

mg/L Method: SM 4500 S2 F Preparation: N/A N/A No Equipment Assigned MB 660-96518/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Sulfide Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/26/2010 1130 06/26/2010 1130 Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 660-96518 1.0 1.0 Water LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

mg/L Prep Batch: N/A Analysis Batch: 660-96518 N/A 1.0 mL 250 mL 1.0 mL 250 mL mg/L Analysis Batch: 660-96518 Prep Batch: N/A Method: SM 4500 S2 F Preparation: N/A N/A N/A N/A No Equipment Assigned No Equipment Assigned LCS 660-96518/2 LCSD 660-96518/3 Analyte LCSD Qual LCS Qual RPD Limit RPD Limit LCSD LCS

% Rec.

98 96 75 - 125 2

25 Sulfide TestAmerica Tampa Page 38 of 47

Page 39 of 47

Page 40 of 47

Page 41 of 47

Page 42 of 47

Page 43 of 47

Page 44 of 47

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35970-1 SDG Number: 35970 Login Number: 35970 Question T / F/ NA Comment Creator: Volz, Charles List Source: TestAmerica Tampa List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True 2.5,2.7 Degrees C. CU-07 COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the sample IDs on the containers and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

False If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

True TestAmerica Tampa Page 45 of 47

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35970-1 SDG Number: 35970 Login Number: 35970 Question T / F/ NA Comment Creator: Kicklighter, Marilyn List Source: TestAmerica Savannah List Creation: 06/29/10 02:14 PM List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

N/A There are no discrepancies between the sample IDs on the containers and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

N/A If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

N/A Samples do not require splitting or compositing.

N/A TestAmerica Tampa Page 46 of 47

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35970-1 SDG Number: 35970 Login Number: 35970 Question T / F/ NA Comment Creator: Archie, Datiska List Source: TestAmerica Tallahassee List Creation: 06/30/10 09:30 AM List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the sample IDs on the containers and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

N/A If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

N/A Samples do not require splitting or compositing.

N/A TestAmerica Tampa Page 47 of 47

ANALYTICAL REPORT Job Number: 660-35950-1 SDG Number: 35950 Job

Description:

FPL Turkey Point Analytical Services For:

Florida Power & Light Company Technical Services - PGD Environmental Water Compliance/Permitting 700 Universe Blvd (JES/JB)

Juno Beach, FL 33408 Attention: Ms. Stacy Foster Approved for release.

Amy Atkins Project Manager I 8/2/2010 3:51 PM Amy Atkins Project Manager I amy.atkins@testamericainc.com 08/02/2010 cc:

Ms. Sharon Ewe Methods: FDEP, DOH Certification #: TestAmerica Tampa E84282; TestAmerica Tallahassee E81005; TestAmerica Savannah E87052 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report.

The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com Page 1 of 54

Job Narrative 660-35950-1 Receipt All samples were received in good condition within temperature requirements.

6010B The matrix spike duplicate (MSD) recovery for Calcium in batch 660-96604 was outside control limits with the sample greater than 4x the spike level. The associated laboratory control sample (LCS) recovery met acceptance criteria.

300.0 Due to sample matrix, 062410-TPGW-4D (660-35950-3) and 062410-TPGW-4M (660-35950-2) were diluted for Fluoride.

Page 2 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35950 660-35950-1 062410-TPGW-4S SU Field Sampling 7.31 Field pH Degrees C Field Sampling 24.99 Field Temperature mg/L Field Sampling 1.4 Oxygen, Dissolved umhos/cm Field Sampling 1750 Specific Conductance NTU Field Sampling 2.52 Turbidity 0.050 mg/L 300.0 1.7 Bromide 50 mg/L 300.0 490 Chloride 0.050 mg/L 300.0 0.055 Fluoride 0.50 mg/L 300.0 20 Sulfate 1.0 mg/L SM 2320B 200 Alkalinity 5.0 mg/L SM 2540C 1100 Total Dissolved Solids Dissolved 1.0 mg/L 9060 54 Dissolved Inorganic Carbon-Dissolved Total Recoverable 100 ug/L 200.7 Rev 4.4 24 I

Barium 500 ug/L 200.7 Rev 4.4 220 I

Iron 50 ug/L 6010B 64 Boron 0.50 mg/L 6010B 120 Calcium 1.0 mg/L 6010B 9.2 Potassium 5.0 ug/L 6010B 1300 Strontium 0.080 mg/L 6010B 19 Magnesium 5.0 mg/L 6010B 250 Sodium TestAmerica Tampa Page 3 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35950 660-35950-2 062410-TPGW-4M SU Field Sampling 6.88 Field pH Degrees C Field Sampling 25.66 Field Temperature mg/L Field Sampling 2.3 Oxygen, Dissolved umhos/cm Field Sampling 32010 Specific Conductance NTU Field Sampling 2.0 Turbidity 5.0 mg/L 300.0 47 Bromide 500 mg/L 300.0 13000 Chloride 50 mg/L 300.0 1600 Sulfate 1.0 mg/L SM 2320B 210 Alkalinity 250 mg/L SM 2540C 28000 Total Dissolved Solids Dissolved 1.0 mg/L 9060 48 Dissolved Inorganic Carbon-Dissolved Total Recoverable 100 ug/L 200.7 Rev 4.4 150 Barium 500 ug/L 200.7 Rev 4.4 4700 Iron 500 ug/L 6010B 1400 Boron 5.0 mg/L 6010B 620 Calcium 10 mg/L 6010B 280 Potassium 50 ug/L 6010B 8300 Strontium 0.80 mg/L 6010B 900 Magnesium 100 mg/L 6010B 7200 Sodium TestAmerica Tampa Page 4 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35950 660-35950-3 062410-TPGW-4D SU Field Sampling 6.92 Field pH Degrees C Field Sampling 25.29 Field Temperature mg/L Field Sampling 2.4 Oxygen, Dissolved umhos/cm Field Sampling 37010 Specific Conductance NTU Field Sampling 0.02 Turbidity 50 mg/L 300.0 54 Bromide 500 mg/L 300.0 16000 Chloride 50 mg/L 300.0 1900 Sulfate 1.0 mg/L SM 2320B 200 Alkalinity 250 mg/L SM 2540C 33000 Total Dissolved Solids Dissolved 1.0 mg/L 9060 45 Dissolved Inorganic Carbon-Dissolved Total Recoverable 100 ug/L 200.7 Rev 4.4 140 Barium 500 ug/L 200.7 Rev 4.4 5900 Iron 500 ug/L 6010B 2200 Boron 5.0 mg/L 6010B 620 Calcium 10 mg/L 6010B 420 Potassium 50 ug/L 6010B 8800 Strontium 0.80 mg/L 6010B 1100 Magnesium 100 mg/L 6010B 8600 Sodium TestAmerica Tampa Page 5 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35950 660-35950-4 062410-TPGW-7S SU Field Sampling 7.22 Field pH Degrees C Field Sampling 24.80 Field Temperature mg/L Field Sampling 2.0 Oxygen, Dissolved umhos/cm Field Sampling 483 Specific Conductance NTU Field Sampling 3.81 Turbidity 0.050 mg/L 300.0 0.18 Bromide 0.50 mg/L 300.0 36 Chloride 0.050 mg/L 300.0 0.17 Fluoride 0.50 mg/L 300.0 27 Sulfate 1.0 mg/L SM 2320B 210 Alkalinity 5.0 mg/L SM 2540C 300 Total Dissolved Solids Dissolved 1.0 mg/L 9060 44 Dissolved Inorganic Carbon-Dissolved Total Recoverable 500 ug/L 200.7 Rev 4.4 340 I

Iron 50 ug/L 6010B 53 Boron 0.50 mg/L 6010B 91 Calcium 1.0 mg/L 6010B 9.9 Potassium 5.0 ug/L 6010B 910 Strontium 0.080 mg/L 6010B 4.0 Magnesium 0.50 mg/L 6010B 20 Sodium TestAmerica Tampa Page 6 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35950 660-35950-5 062410-TPGW-7M SU Field Sampling 7.19 Field pH Degrees C Field Sampling 25.05 Field Temperature mg/L Field Sampling 1.5 Oxygen, Dissolved umhos/cm Field Sampling 500 Specific Conductance NTU Field Sampling 2.29 Turbidity 0.050 mg/L 300.0 0.17 Bromide 0.50 mg/L 300.0 35 Chloride 0.050 mg/L 300.0 0.23 Fluoride 0.50 mg/L 300.0 25 Sulfate 1.0 mg/L SM 2320B 200 Alkalinity 5.0 mg/L SM 2540C 310 Total Dissolved Solids Dissolved 1.0 mg/L 9060 47 Dissolved Inorganic Carbon-Dissolved Total Recoverable 100 ug/L 200.7 Rev 4.4 11 I

Barium 500 ug/L 200.7 Rev 4.4 360 I

Iron 50 ug/L 6010B 53 Boron 0.50 mg/L 6010B 91 Calcium 1.0 mg/L 6010B 9.4 Potassium 5.0 ug/L 6010B 920 Strontium 0.080 mg/L 6010B 4.1 Magnesium 0.50 mg/L 6010B 21 Sodium TestAmerica Tampa Page 7 of 54

EXECUTIVE

SUMMARY

- Detections Client: Florida Power & Light Company Job Number: 660-35950-1 Analyte Result / Qualifier Reporting Limit Units Method Lab Sample ID Client Sample ID Sdg Number: 35950 660-35950-6 062410-TPGW-7D SU Field Sampling 7.19 Field pH Degrees C Field Sampling 25.12 Field Temperature mg/L Field Sampling 2.3 Oxygen, Dissolved umhos/cm Field Sampling 510 Specific Conductance NTU Field Sampling 1.34 Turbidity 0.050 mg/L 300.0 0.21 Bromide 0.50 mg/L 300.0 41 Chloride 0.050 mg/L 300.0 0.14 Fluoride 0.50 mg/L 300.0 29 Sulfate 1.0 mg/L SM 2320B 200 Alkalinity 5.0 mg/L SM 2540C 320 Total Dissolved Solids Dissolved 1.0 mg/L 9060 47 Dissolved Inorganic Carbon-Dissolved Total Recoverable 500 ug/L 200.7 Rev 4.4 280 I

Iron 50 ug/L 6010B 51 Boron 0.50 mg/L 6010B 91 Calcium 1.0 mg/L 6010B 4.8 Potassium 5.0 ug/L 6010B 880 Strontium 0.080 mg/L 6010B 3.7 Magnesium 0.50 mg/L 6010B 26 Sodium TestAmerica Tampa Page 8 of 54

METHOD

SUMMARY

Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Preparation Method Method Lab Location Description Matrix:

Water EPA 200.7 Rev 4.4 Metals (ICP)

TAL TAL EPA 200.7 TAL TAL Preparation, Total Recoverable Metals SW846 6010B Metals (ICP)

TAL TAM SW846 3005A TAL TAM Preparation, Total Recoverable or Dissolved Metals MCAWW 300.0 Anions, Ion Chromatography TAL TAM SW846 9060 Carbon, Dissolved and Dissolved Inorganic TAL SAV FIELD_FLTRD TAL SAV Sample Filtration, Field SM SM 2320B Alkalinity TAL TAM SM SM 2540C Solids, Total Dissolved (TDS)

TAL TAM SM SM 4500 S2 F Sulfide, Total TAL TAM EPA Field Sampling Field Sampling TAL TAM Lab

References:

TAL SAV = TestAmerica Savannah TAL TAL = TestAmerica Tallahassee TAL TAM = TestAmerica Tampa Method

References:

EPA = US Environmental Protection Agency MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa Page 9 of 54

METHOD / ANALYST

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35950-1 Method Analyst Analyst ID Sdg Number: 35950 Wallace, Tiffany B TBW EPA 200.7 Rev 4.4 Fox, Greg GF SW846 6010B Sampler, Field FS EPA Field Sampling Sengsouvanna, Dom DS MCAWW 300.0 Blackshear, Kim KB SW846 9060 Steward, Tiffany TS SM SM 2320B Oonnoonny, Thomas TO SM SM 2540C Mostafavifar, Efe EM SM SM 4500 S2 F TestAmerica Tampa Page 10 of 54

SAMPLE

SUMMARY

Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID Lab Sample ID Client Matrix Date/Time Sampled Date/Time Received 06/24/2010 1500 06/25/2010 0830 062410-TPGW-4S 660-35950-1 Water 06/24/2010 1330 06/25/2010 0830 062410-TPGW-4M 660-35950-2 Water 06/24/2010 1300 06/25/2010 0830 062410-TPGW-4D 660-35950-3 Water 06/24/2010 1655 06/25/2010 0830 062410-TPGW-7S 660-35950-4 Water 06/24/2010 1715 06/25/2010 0830 062410-TPGW-7M 660-35950-5 Water 06/24/2010 1800 06/25/2010 0830 062410-TPGW-7D 660-35950-6 Water TestAmerica Tampa Page 11 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID:

Lab Sample ID:

062410-TPGW-4S Client Matrix:

660-35950-1 Water Date Sampled: 06/24/2010 1500 Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 1019 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 24 I

100 9.6 Barium 220 I

500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1427 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 120 0.50 0.10 Calcium 9.2 1.0 0.19 Potassium 19 0.080 0.020 Magnesium Analyte Result (ug/L)

Qualifier MDL PQL 64 50 10 Boron 1300 5.0 1.0 Strontium Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

10 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1519 Run Type:

DL Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 250 5.0 3.1 Sodium TestAmerica Tampa Page 12 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID:

Lab Sample ID:

062410-TPGW-4M Client Matrix:

660-35950-2 Water Date Sampled: 06/24/2010 1330 Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 1022 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 150 100 9.6 Barium 4700 500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

10 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1433 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 620 5.0 1.0 Calcium 280 10 1.9 Potassium 900 0.80 0.20 Magnesium Analyte Result (ug/L)

Qualifier MDL PQL 1400 500 100 Boron 8300 50 10 Strontium Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

200 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1525 Run Type:

DL Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 7200 100 62 Sodium TestAmerica Tampa Page 13 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID:

Lab Sample ID:

062410-TPGW-4D Client Matrix:

660-35950-3 Water Date Sampled: 06/24/2010 1300 Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 1026 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 140 100 9.6 Barium 5900 500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

10 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1440 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 620 5.0 1.0 Calcium 420 10 1.9 Potassium 1100 0.80 0.20 Magnesium Analyte Result (ug/L)

Qualifier MDL PQL 2200 500 100 Boron 8800 50 10 Strontium Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

200 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1531 Run Type:

DL Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 8600 100 62 Sodium TestAmerica Tampa Page 14 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID:

Lab Sample ID:

062410-TPGW-7S Client Matrix:

660-35950-4 Water Date Sampled: 06/24/2010 1655 Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 1033 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 9.6 U

100 9.6 Barium 340 I

500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1537 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 91 0.50 0.10 Calcium 9.9 1.0 0.19 Potassium 4.0 0.080 0.020 Magnesium 20 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 53 50 10 Boron 910 5.0 1.0 Strontium TestAmerica Tampa Page 15 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID:

Lab Sample ID:

062410-TPGW-7M Client Matrix:

660-35950-5 Water Date Sampled: 06/24/2010 1715 Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 1029 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 11 I

100 9.6 Barium 360 I

500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1543 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 91 0.50 0.10 Calcium 9.4 1.0 0.19 Potassium 4.1 0.080 0.020 Magnesium 21 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 53 50 10 Boron 920 5.0 1.0 Strontium TestAmerica Tampa Page 16 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Client Sample ID:

Lab Sample ID:

062410-TPGW-7D Client Matrix:

660-35950-6 Water Date Sampled: 06/24/2010 1800 Date Received: 06/25/2010 0830 200.7 Rev 4.4 Metals (ICP)-Total Recoverable Method:

200.7 Rev 4.4 Analysis Batch: 640-70850 Instrument ID:

Preparation:

Prep Batch: 640-70571 Lab File ID:

071310.csv Dilution:

1.0 Initial Weight/Volume:

5.0 mL Date Analyzed:

07/13/2010 1036 Final Weight/Volume:

50 mL Date Prepared:

07/06/2010 1100 200.7 ICP2 Analyte Result (ug/L)

Qualifier MDL PQL 9.6 U

100 9.6 Barium 280 I

500 46 Iron 6010B Metals (ICP)-Total Recoverable Method:

6010B Analysis Batch: 660-97236 Instrument ID:

Preparation:

Prep Batch: 660-96604 Lab File ID:

10G15A Dilution:

1.0 Initial Weight/Volume:

50 mL Date Analyzed:

07/15/2010 1724 Final Weight/Volume:

50 mL Date Prepared:

06/30/2010 1004 3005A ICPA Analyte Result (mg/L)

Qualifier MDL PQL 91 0.50 0.10 Calcium 4.8 1.0 0.19 Potassium 3.7 0.080 0.020 Magnesium 26 0.50 0.31 Sodium Analyte Result (ug/L)

Qualifier MDL PQL 51 50 10 Boron 880 5.0 1.0 Strontium TestAmerica Tampa Page 17 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID:

Lab Sample ID:

062410-TPGW-4S Client Matrix:

660-35950-1 Water Date Sampled: 06/24/2010 1500 Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 1.7 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2149 Chloride 490 mg/L 20 50 100 300.0 Analysis Batch: 660-96938 Date Analyzed: 07/08/2010 0000 Fluoride 0.055 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2149 Sulfate 20 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2149 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 54 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173756 Date Analyzed: 07/08/2010 1654 Alkalinity 200 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1036 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1036 Total Dissolved Solids 1100 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0948 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 18 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID:

Lab Sample ID:

062410-TPGW-4M Client Matrix:

660-35950-2 Water Date Sampled: 06/24/2010 1330 Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 47 mg/L 2.7 5.0 100 300.0 Analysis Batch: 660-96938 Date Analyzed: 07/08/2010 0021 Chloride 13000 mg/L 200 500 1000 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2211 Fluoride 0.10 U

mg/L 0.10 0.25 5.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0503 Sulfate 1600 mg/L 20 50 100 300.0 Analysis Batch: 660-96938 Date Analyzed: 07/08/2010 0021 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 48 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 210 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1049 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1049 Total Dissolved Solids 28000 mg/L 250 250 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0949 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 19 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID:

Lab Sample ID:

062410-TPGW-4D Client Matrix:

660-35950-3 Water Date Sampled: 06/24/2010 1300 Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 54 mg/L 27 50 1000 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2316 Chloride 16000 mg/L 200 500 1000 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2316 Fluoride 0.10 U

mg/L 0.10 0.25 5.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/09/2010 0524 Sulfate 1900 mg/L 20 50 100 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2338 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 45 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 200 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1055 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1055 Total Dissolved Solids 33000 mg/L 250 250 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0949 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 20 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID:

Lab Sample ID:

062410-TPGW-7S Client Matrix:

660-35950-4 Water Date Sampled: 06/24/2010 1655 Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.18 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2044 Chloride 36 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2044 Fluoride 0.17 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2044 Sulfate 27 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2044 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 44 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 210 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1101 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1101 Total Dissolved Solids 300 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0950 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 21 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID:

Lab Sample ID:

062410-TPGW-7M Client Matrix:

660-35950-5 Water Date Sampled: 06/24/2010 1715 Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.17 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2106 Chloride 35 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2106 Fluoride 0.23 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2106 Sulfate 25 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2106 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 47 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 200 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1107 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1107 Total Dissolved Solids 310 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0950 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 22 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 General Chemistry Client Sample ID:

Lab Sample ID:

062410-TPGW-7D Client Matrix:

660-35950-6 Water Date Sampled: 06/24/2010 1800 Date Received: 06/25/2010 0830 Analyte Result Qual Units MDL PQL Dil Method Bromide 0.21 mg/L 0.027 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2128 Chloride 41 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2128 Fluoride 0.14 mg/L 0.020 0.050 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2128 Sulfate 29 mg/L 0.20 0.50 1.0 300.0 Analysis Batch: 660-96989 Date Analyzed: 07/08/2010 2128 Analyte Result Qual Units PQL PQL Dil Method Dissolved Inorganic Carbon-Dissolved 47 mg/L 1.0 1.0 1.0 9060 Analysis Batch: 680-173757 Date Analyzed: 07/09/2010 0959 Alkalinity 200 mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1113 Carbonate Alkalinity as CaCO3 1.0 U

mg/L 1.0 1.0 1.0 SM 2320B Analysis Batch: 660-96877 Date Analyzed: 07/07/2010 1113 Total Dissolved Solids 320 mg/L 5.0 5.0 1.0 SM 2540C Analysis Batch: 660-96479 Date Analyzed: 06/28/2010 0951 Sulfide 1.0 U

mg/L 1.0 1.0 1.0 SM 4500 S2 F Analysis Batch: 660-96518 Date Analyzed: 06/26/2010 1130 TestAmerica Tampa Page 23 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062410-TPGW-4S Client Matrix:

660-35950-1 Water Date Sampled: 06/24/2010 1500 Date Received: 06/25/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 7.31 SU 1.0 Field Sampling 660-97058 06/24/2010 1500 Field Temperature 24.99 Degrees C 1.0 Field Sampling 660-97058 06/24/2010 1500 Oxygen, Dissolved 1.4 mg/L 1.0 Field Sampling 660-97058 06/24/2010 1500 Specific Conductance 1750 umhos/cm 1.0 Field Sampling 660-97058 06/24/2010 1500 Turbidity 2.52 NTU 1.0 Field Sampling 660-97058 06/24/2010 1500 TestAmerica Tampa Page 24 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062410-TPGW-4M Client Matrix:

660-35950-2 Water Date Sampled: 06/24/2010 1330 Date Received: 06/25/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 6.88 SU 1.0 Field Sampling 660-97058 06/24/2010 1330 Field Temperature 25.66 Degrees C 1.0 Field Sampling 660-97058 06/24/2010 1330 Oxygen, Dissolved 2.3 mg/L 1.0 Field Sampling 660-97058 06/24/2010 1330 Specific Conductance 32010 umhos/cm 1.0 Field Sampling 660-97058 06/24/2010 1330 Turbidity 2.0 NTU 1.0 Field Sampling 660-97058 06/24/2010 1330 TestAmerica Tampa Page 25 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062410-TPGW-4D Client Matrix:

660-35950-3 Water Date Sampled: 06/24/2010 1300 Date Received: 06/25/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 6.92 SU 1.0 Field Sampling 660-97058 06/24/2010 1300 Field Temperature 25.29 Degrees C 1.0 Field Sampling 660-97058 06/24/2010 1300 Oxygen, Dissolved 2.4 mg/L 1.0 Field Sampling 660-97058 06/24/2010 1300 Specific Conductance 37010 umhos/cm 1.0 Field Sampling 660-97058 06/24/2010 1300 Turbidity 0.02 NTU 1.0 Field Sampling 660-97058 06/24/2010 1300 TestAmerica Tampa Page 26 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062410-TPGW-7S Client Matrix:

660-35950-4 Water Date Sampled: 06/24/2010 1655 Date Received: 06/25/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 7.22 SU 1.0 Field Sampling 660-97058 06/24/2010 1655 Field Temperature 24.80 Degrees C 1.0 Field Sampling 660-97058 06/24/2010 1655 Oxygen, Dissolved 2.0 mg/L 1.0 Field Sampling 660-97058 06/24/2010 1655 Specific Conductance 483 umhos/cm 1.0 Field Sampling 660-97058 06/24/2010 1655 Turbidity 3.81 NTU 1.0 Field Sampling 660-97058 06/24/2010 1655 TestAmerica Tampa Page 27 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062410-TPGW-7M Client Matrix:

660-35950-5 Water Date Sampled: 06/24/2010 1715 Date Received: 06/25/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 7.19 SU 1.0 Field Sampling 660-97058 06/24/2010 1715 Field Temperature 25.05 Degrees C 1.0 Field Sampling 660-97058 06/24/2010 1715 Oxygen, Dissolved 1.5 mg/L 1.0 Field Sampling 660-97058 06/24/2010 1715 Specific Conductance 500 umhos/cm 1.0 Field Sampling 660-97058 06/24/2010 1715 Turbidity 2.29 NTU 1.0 Field Sampling 660-97058 06/24/2010 1715 TestAmerica Tampa Page 28 of 54

Analytical Data Client: Florida Power & Light Company Job Number: 660-35950-1 Sdg Number: 35950 Field Service / Mobile Lab Client Sample ID:

Lab Sample ID:

062410-TPGW-7D Client Matrix:

660-35950-6 Water Date Sampled: 06/24/2010 1800 Date Received: 06/25/2010 0830 Result Qual Units Dil Method Analysis Date Analyzed Date Prepared Analyte Batch Field pH 7.19 SU 1.0 Field Sampling 660-97058 06/24/2010 1800 Field Temperature 25.12 Degrees C 1.0 Field Sampling 660-97058 06/24/2010 1800 Oxygen, Dissolved 2.3 mg/L 1.0 Field Sampling 660-97058 06/24/2010 1800 Specific Conductance 510 umhos/cm 1.0 Field Sampling 660-97058 06/24/2010 1800 Turbidity 1.34 NTU 1.0 Field Sampling 660-97058 06/24/2010 1800 TestAmerica Tampa Page 29 of 54

DATA REPORTING QUALIFIERS Client: Florida Power & Light Company Job Number: 660-35950-1 Lab Section Qualifier Description Sdg Number: 35950 Metals Estimated value; value may not be accurate. Spike recovery or RPD outside of criteria.

J3 Indicates that the compound was analyzed for but not detected.

U The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

I General Chemistry Indicates that the compound was analyzed for but not detected.

U TestAmerica Tampa Page 30 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/13/2010 0852 Method Blank - Batch: 640-70571 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 640-70850 Prep Batch: 640-70571 07/06/2010 1100 071310.csv 50 mL 50 mL Units:

ug/L Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 MB 640-70571/1-A Analyte Result Qual MDL PQL 0.96 U

10 0.96 Barium 4.6 U

50 4.6 Iron Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/13/2010 0856 07/13/2010 0859 Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 640-70571 1.0 1.0 Water LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L 07/06/2010 1100 Prep Batch: 640-70571 Analysis Batch: 640-70850 071310.csv 50 mL 50 mL 071310.csv 50 mL 50 mL ug/L 07/06/2010 1100 Analysis Batch: 640-70850 Prep Batch: 640-70571 Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 ICP2 LCS 640-70571/2-A LCSD 640-70571/3-A Analyte LCSD Qual LCS Qual RPD Limit RPD Limit LCSD LCS

% Rec.

102 101 85 - 115 1

20 Barium 103 102 85 - 115 1

20 Iron TestAmerica Tampa Page 31 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/13/2010 0910 07/13/2010 0913 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 640-70571 1.0 1.0 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 640-70850 Analysis Batch: 640-70850 07/06/2010 1100 07/06/2010 1100 Prep Batch: 640-70571 Prep Batch: 640-70571 071310.csv 5.0 mL 50 mL 071310.csv 5.0 mL 50 mL Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 ICP2 660-36031-B-1-B MS 660-36031-B-1-C MSD Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

101 98 70 - 130 2

20 Barium 99 96 70 - 130 3

20 Iron ug/L Units:

Water Dilution:

1.0 Date Analyzed:

Duplicate - Batch: 640-70571 Lab Sample ID:

Client Matrix:

Date Prepared:

07/13/2010 0934 07/06/2010 1100 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 640-70850 Prep Batch: 640-70571 071310.csv 5.0 mL 50 mL Method: 200.7 Rev 4.4 Preparation: 200.7 Total Recoverable ICP2 660-36031-B-2-B DU Analyte Qual Limit RPD Result Sample Result/Qual 123 130 2

20 Barium 8340 8600 3

20 Iron TestAmerica Tampa Page 32 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/15/2010 1250 Method Blank - Batch: 660-96604 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-97236 Prep Batch: 660-96604 06/30/2010 1004 10G15A 50 mL 50 mL Units:

mg/L Method: 6010B Preparation: 3005A Total Recoverable ICPA MB 660-96604/1-A Analyte Result Qual MDL PQL 0.10 U

0.50 0.10 Calcium 0.19 U

1.0 0.19 Potassium 0.020 U

0.080 0.020 Magnesium 0.31 U

0.50 0.31 Sodium Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/15/2010 1250 Method Blank - Batch: 660-96604 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-97236 Prep Batch: 660-96604 06/30/2010 1004 10G15A 50 mL 50 mL Units:

ug/L Method: 6010B Preparation: 3005A Total Recoverable ICPA MB 660-96604/1-A Analyte Result Qual MDL PQL 10 U

50 10 Boron 1.0 U

5.0 1.0 Strontium TestAmerica Tampa Page 33 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water 1.0 07/15/2010 1256 Date Analyzed:

Lab Control Sample - Batch: 660-96604 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

10G15A 06/30/2010 1004 Analysis Batch: 660-97236 Prep Batch: 660-96604 50 mL 50 mL Units:

mg/L Method: 6010B Preparation: 3005A Total Recoverable ICPA LCS 660-96604/2-A Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 1.05 105 75 - 125 Calcium 10.0 10.1 101 75 - 125 Potassium 1.00 1.03 103 75 - 125 Magnesium 10.0 9.85 98 75 - 125 Sodium Water 1.0 07/15/2010 1256 Date Analyzed:

Lab Control Sample - Batch: 660-96604 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

10G15A 06/30/2010 1004 Analysis Batch: 660-97236 Prep Batch: 660-96604 50 mL 50 mL Units:

ug/L Method: 6010B Preparation: 3005A Total Recoverable ICPA LCS 660-96604/2-A Analyte Qual Limit

% Rec.

Result Spike Amount 1000 1020 102 75 - 125 Boron 1000 1070 107 75 - 125 Strontium TestAmerica Tampa Page 34 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/15/2010 1314 07/15/2010 1320 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96604 1.0 1.0 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-97236 Analysis Batch: 660-97236 06/30/2010 1004 06/30/2010 1004 Prep Batch: 660-96604 Prep Batch: 660-96604 10G15A 50 mL 50 mL 10G15A 50 mL 50 mL Method: 6010B Preparation: 3005A Total Recoverable ICPA ICPA 660-36004-B-9-B MS 660-36004-B-9-C MSD Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

93 250 75 - 125 1

20 J3 Calcium 111 113 75 - 125 2

20 Potassium 103 108 75 - 125 2

20 Magnesium 104 92 75 - 125 8

20 Sodium Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/15/2010 1314 07/15/2010 1320 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96604 1.0 1.0 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-97236 Analysis Batch: 660-97236 06/30/2010 1004 06/30/2010 1004 Prep Batch: 660-96604 Prep Batch: 660-96604 10G15A 50 mL 50 mL 10G15A 50 mL 50 mL Method: 6010B Preparation: 3005A Total Recoverable ICPA ICPA 660-36004-B-9-B MS 660-36004-B-9-C MSD Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

104 105 75 - 125 1

20 Boron 107 109 75 - 125 2

20 Strontium TestAmerica Tampa Page 35 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/07/2010 1246 Method Blank - Batch: 660-96938 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96938 Prep Batch: N/A 10.0000.TXT 1 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 MB 660-96938/3 Analyte Result Qual MDL PQL 0.027 U

0.050 0.027 Bromide 0.20 U

0.50 0.20 Chloride 0.20 U

0.50 0.20 Sulfate Water 1.0 07/07/2010 1307 Date Analyzed:

Lab Control Sample - Batch: 660-96938 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

11.0000.TXT N/A Analysis Batch: 660-96938 Prep Batch: N/A 1 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 LCS 660-96938/4 Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 1.00 100 90 - 110 Bromide 10.0 10.1 101 90 - 110 Chloride 10.0 10.2 102 90 - 110 Sulfate TestAmerica Tampa Page 36 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/07/2010 2211 07/07/2010 2233 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96938 10 10 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96938 Analysis Batch: 660-96938 Prep Batch: N/A Prep Batch: N/A 32.0000.TXT 50 mL 33.0000.TXT 50 mL Method: 300.0 Preparation: N/A N/A N/A DIONEX2 DIONEX2 660-35992-B-3 MS ^10 660-35992-B-3 MSD ^10 Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

102 104 90 - 110 1

30 Bromide 102 105 90 - 110 1

30 Chloride 103 104 90 - 110 1

30 Sulfate TestAmerica Tampa Page 37 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/08/2010 2001 Method Blank - Batch: 660-96989 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96989 Prep Batch: N/A 21.0000.TXT 1 mL N/A Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 MB 660-96989/3 Analyte Result Qual MDL PQL 0.027 U

0.050 0.027 Bromide 0.20 U

0.50 0.20 Chloride 0.020 U

0.050 0.020 Fluoride 0.20 U

0.50 0.20 Sulfate Water 1.0 07/08/2010 2022 Date Analyzed:

Lab Control Sample - Batch: 660-96989 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

22.0000.TXT N/A Analysis Batch: 660-96989 Prep Batch: N/A 1 mL Units:

mg/L Method: 300.0 Preparation: N/A DIONEX2 LCS 660-96989/4 Analyte Qual Limit

% Rec.

Result Spike Amount 1.00 0.976 98 90 - 110 Bromide 10.0 10.2 102 90 - 110 Chloride 1.00 0.950 95 90 - 110 Fluoride 10.0 10.2 102 90 - 110 Sulfate TestAmerica Tampa Page 38 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

07/08/2010 2233 07/08/2010 2254 Water Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 660-96989 1000 1000 MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Analysis Batch: 660-96989 Analysis Batch: 660-96989 Prep Batch: N/A Prep Batch: N/A 28.0000.TXT 50 mL 29.0000.TXT 50 mL Method: 300.0 Preparation: N/A N/A N/A DIONEX2 DIONEX2 660-35950-2 660-35950-2 Analyte MSD Qual MS Qual RPD Limit RPD Limit MSD MS

% Rec.

104 106 90 - 110 1

30 Bromide 104 105 90 - 110 0

30 Chloride 109 101 90 - 110 8

30 Fluoride 101 101 90 - 110 0

30 Sulfate TestAmerica Tampa Page 39 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/08/2010 1654 Method Blank - Batch: 680-173756 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 680-173756 Prep Batch: N/A 25 mL 25 mL N/A Units:

mg/L Method: 9060 Preparation: N/A N/A TOC3 MB 680-173756/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Dissolved Inorganic Carbon-Dissolved 1.0 U

1.0 1.0 Dissolved Carbon-Dissolved Water 1.0 07/08/2010 1654 Date Analyzed:

Lab Control Sample - Batch: 680-173756 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

N/A Analysis Batch: 680-173756 Prep Batch: N/A 25 mL 25 mL Units:

mg/L Method: 9060 Preparation: N/A N/A TOC3 LCS 680-173756/2 Analyte Qual Limit

% Rec.

Result Spike Amount 20.0 19.7 98 Dissolved Inorganic Carbon-Dissolved 20.0 19.7 98 Dissolved Carbon-Dissolved TestAmerica Tampa Page 40 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/09/2010 0959 Method Blank - Batch: 680-173757 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 680-173757 Prep Batch: N/A 25 mL 25 mL N/A Units:

mg/L Method: 9060 Preparation: N/A N/A TOC3 MB 680-173757/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Dissolved Inorganic Carbon-Dissolved 1.0 U

1.0 1.0 Dissolved Carbon-Dissolved Water 1.0 07/09/2010 0959 Date Analyzed:

Lab Control Sample - Batch: 680-173757 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

N/A Analysis Batch: 680-173757 Prep Batch: N/A 25 mL 25 mL Units:

mg/L Method: 9060 Preparation: N/A N/A TOC3 LCS 680-173757/2 Analyte Qual Limit

% Rec.

Result Spike Amount 20.0 19.3 96 Dissolved Inorganic Carbon-Dissolved 20.0 19.3 96 Dissolved Carbon-Dissolved TestAmerica Tampa Page 41 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

07/07/2010 1023 Method Blank - Batch: 660-96877 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96877 Prep Batch: N/A 7.7.10a.txt 50 mL 50 mL N/A Units:

mg/L Method: SM 2320B Preparation: N/A MANTECH MB 660-96877/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Alkalinity Water 1.0 07/07/2010 1030 Date Analyzed:

Lab Control Sample - Batch: 660-96877 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

7.7.10a.txt N/A Analysis Batch: 660-96877 Prep Batch: N/A 50 mL 50 mL Units:

mg/L Method: SM 2320B Preparation: N/A MANTECH LCS 660-96877/2 Analyte Qual Limit

% Rec.

Result Spike Amount 118 117 99 80 - 120 Alkalinity mg/L Units:

Water Dilution:

1.0 Date Analyzed:

Duplicate - Batch: 660-96877 Lab Sample ID:

Client Matrix:

Date Prepared:

07/07/2010 1042 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96877 Prep Batch: N/A 7.7.10a.txt 50 mL 50 mL N/A Method: SM 2320B Preparation: N/A MANTECH 660-35950-1 Analyte Qual Limit RPD Result Sample Result/Qual 204 200 2

30 Alkalinity 1.0 1.0 U

NC 30 U

Carbonate Alkalinity as CaCO3 TestAmerica Tampa Page 42 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/28/2010 0937 Method Blank - Batch: 660-96479 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96479 Prep Batch: N/A 50 mL 50 mL N/A Units:

mg/L Method: SM 2540C Preparation: N/A N/A No Equipment Assigned MB 660-96479/1 Analyte Result Qual PQL PQL 5.0 U

5.0 5.0 Total Dissolved Solids Water 1.0 06/28/2010 0938 Date Analyzed:

Lab Control Sample - Batch: 660-96479 Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

N/A Analysis Batch: 660-96479 Prep Batch: N/A 10 mL 50 mL Units:

mg/L Method: SM 2540C Preparation: N/A N/A No Equipment Assigned LCS 660-96479/2 Analyte Qual Limit

% Rec.

Result Spike Amount 10000 9910 99 80 - 120 Total Dissolved Solids mg/L Units:

Water Dilution:

1.0 Date Analyzed:

Duplicate - Batch: 660-96479 Lab Sample ID:

Client Matrix:

Date Prepared:

06/28/2010 0951 Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96479 Prep Batch: N/A 50 mL 50 mL N/A Method: SM 2540C Preparation: N/A N/A No Equipment Assigned 660-35950-6 Analyte Qual Limit RPD Result Sample Result/Qual 314 320 1

20 Total Dissolved Solids TestAmerica Tampa Page 43 of 54

Quality Control Results Job Number: 660-35950-1 Client: Florida Power & Light Company Sdg Number: 35950 Water Client Matrix:

1.0 Dilution

Date Analyzed:

Lab Sample ID:

06/26/2010 1130 Method Blank - Batch: 660-96518 Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-96518 Prep Batch: N/A 1.0 mL 250 mL N/A Units:

mg/L Method: SM 4500 S2 F Preparation: N/A N/A No Equipment Assigned MB 660-96518/1 Analyte Result Qual PQL PQL 1.0 U

1.0 1.0 Sulfide Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

06/26/2010 1130 06/26/2010 1130 Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 660-96518 1.0 1.0 Water LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix:

Water Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

mg/L Prep Batch: N/A Analysis Batch: 660-96518 N/A 1.0 mL 250 mL 1.0 mL 250 mL mg/L Analysis Batch: 660-96518 Prep Batch: N/A Method: SM 4500 S2 F Preparation: N/A N/A N/A N/A No Equipment Assigned No Equipment Assigned LCS 660-96518/2 LCSD 660-96518/3 Analyte LCSD Qual LCS Qual RPD Limit RPD Limit LCSD LCS

% Rec.

98 96 75 - 125 2

25 Sulfide TestAmerica Tampa Page 44 of 54

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Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35950-1 SDG Number: 35950 Login Number: 35950 Question T / F/ NA Comment Creator: McNulty, Carol List Source: TestAmerica Tampa List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True 4.1, 4.5 degrees C Cu-07 Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the sample IDs on the containers and the COC.

True 245.1 on coc-not in project, 200.7 to tally in proj.

but not checked off on coc Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

True If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

True TestAmerica Tampa Page 52 of 54

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35950-1 SDG Number: 35950 Login Number: 35950 Question T / F/ NA Comment Creator: Kicklighter, Marilyn List Source: TestAmerica Savannah List Creation: 06/29/10 02:14 PM List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

N/A There are no discrepancies between the sample IDs on the containers and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

True If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

N/A Samples do not require splitting or compositing.

False TestAmerica Tampa Page 53 of 54

Login Sample Receipt Check List Client: Florida Power & Light Company Job Number: 660-35950-1 SDG Number: 35950 Login Number: 35950 Question T / F/ NA Comment Creator: Archie, Datiska List Source: TestAmerica Tallahassee List Creation: 07/02/10 12:06 PM List Number: 1 Radioactivity either was not measured or, if measured, is at or below background N/A The cooler's custody seal, if present, is intact.

True The cooler or samples do not appear to have been compromised or tampered with.

True Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the sample IDs on the containers and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

N/A If necessary, staff have been informed of any short hold time or quick TAT needs True Multiphasic samples are not present.

N/A Samples do not require splitting or compositing.

N/A TestAmerica Tampa Page 54 of 54