ML17058A956

Rev 5 to Administrative Procedure AP-3.7.1, Unit 2 Radwaste Process Control Program.

ML17058A956
Person / Time
Site:	Nine Mile Point
Issue date:	05/02/1991
From:	Mccormick M NIAGARA MOHAWK POWER CORP.
To:
Shared Package
ML17058A955	List: ML17058A954 ML17058A956 ML18038A369
References
AP-3.7.1, NUDOCS 9109090105
Download: ML17058A956 (86)

Text

NIAGARA HOHAWK POWER CORPORATION NINE MILE POINT NUCLEAR STATION ADMINISTRATIVE PROCEDURE

~P- ~l V I N NIT RADWA T P NTR L RAH Approved By:

H. J. HcCormick, Jr. Pi ant a gb r~'i 2 2 Date Effective Date:

NOT TO BE USED AFTER Pla 1993 SUBJECT TO PERIODIC REVIEW

'9SOSOVOZOS VXasZv PDR ADOCK 050004i0 R PDR

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~" ""Procecfiii'e'fnformattok

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~ The attached pre caduii le routed for your atguature.

Procedure No.: -3.'-""7, / Revision:

Ownership Department Supervisor:

The attached procedure has been approved. Please arrange for training as required in accordance with AP-20, Section 72.1, and assign an effective date.

When assigning an effective date, please add at least 3 working days for Procedures Department to process, lf this procedure has an 'emergency" status, assign the appropriate effective date and fillout section below.

To ensure timely delivery, place procedures in appropriate 'Hand Carry'ray located in the various mail rooms.

This procedure cannot be given three (3) working days for pr essing due to:

p, Please perform the followfng before assfgning an effective date:

1. Check master copy and make sure that all TCN's are incorporated.

2 Whenever TCN's are incorporated in a procedure make sure that the cover sheet has the statement 'This revision supercedes TCN's 'nd state the TCN numbers.

3. State the system expert:

4. State if procedure is upgraded per Ste Writers Guide........... Ches C3 No

5. State if procedure is safety related...............,...............,....,.. 0 Yes LM

6. State if procedure Is Tech Spec related.................................~es ClNo Effecttve

7. State if procedure satisfies EQ requirements......................... Cl Yes CWo 3 jsS Dat: + y PROCEDURES OEP .

ODH or Designee Signature

+ Ru-s tC CQEaamGZ cv&'ay ksfJ Please Return to Proceduree"

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saFEpr uN.YSS AwconoANCE VNH to CFRSOsO (QecNnaoS thN nxpfre Plant Manage Appravaf per Tech Spec 8$ )

Ralston No. 05 Date ~ n For Documents@

The Author (A) and Sk member(Nnlmtin-8 regular members, 2 Iftarnatee) are to respond to each of the@estlona below. Ho Yes Does the dccument / revision result in a change to the facility or procedures described in the FSAR? A CI CI t CI Cl 20 CI 3 CI'l 40 CI s0 Cl Does the document / revision deviate from compliance to Tech Specs, or is the margin of AEf 0 safety defined in the basis reduced? ~CI 0 2 CI Cl 30 0 40 0 sg 0 Does the document / revision increase the probabiTCy of occurrence, or the consequences of an A'8 CI accident, or malfunction of equipment important to safety (Class 1) evaluated in the FSAR increased? <0 0 2 CI Cl

~ .

s0 40 0 sCI 0 Does the document / revision create the possibility for an accident or malfunction of a different AC3 0.

type than any evahated in the FSAR? t Cl Cl 2 Cl Cl

~CI 0

• A MAYBE"constitutes a YES response.

40 0 sCl 0

{~g Recommend Nudear SOB C a mS

'ch

~W Support)terfcrm a safety ANALYSISto present to ot Sa Sae quesaai>

1 0

2 C3 3

CJ Recommend fui SORC otmtm~ivfetr fia Evttfua5tN of Need for Safaty Analysis. Cl Cl Cl Recommend Approvaf - Tlis doctinent does not involve Nt ureviewed safety quesiorL Cl Cl Cl 2

SORC Meeting No.

(if repaired)

QH9 UNIT 2

~ >-.<4. pgLj@~jL4etWIRt~

Ak. REVIEW AND Document No. Rev. Ha 'Rd Rev,NC Cl Title Author Date DeSCriptlOn Of ChNlQ8$ (itemize the nature/ reason of general changes)

See attached Procedure Development Form Modification Related Changes? Yes 0 No 8 Mod. Control No.:

'f a periodic review with no changes (Prd Rev, NC), use the last published revision number and continue review process.

intradlscl plinary Review (minimum of one person required)

Dept. Name Title Signat e Date R'caw ~ cot R CrE,va SV. 4 el'K t1 t Cross. Dlsclpllrtary Review

~S Dept. Name QISO t-tAAA'=

(rf not required, use lines for justification statement)

Titie g L)Ill ITC.

Signature c- C t5:~ 'u ~

nest Date If not in concurrence, do not sign but return document to the author with comments.

Routed to Quality Assurance for eq'd for APs, EOPs, and SQPs): Yes& N/RQ QA Representative QA. Rep (for Site) Date & comments 0 Routed to A.LARA.forritrhw: Yes Q No JZ if No, reason: P 8 e e ed, Radiological conditio~Wll not,.be adversly affected, the amount of Radwaste will not be increas t

A.L.A.RA. Representative" QA Date 4 comments are attached 0 A.L.A.RA. Rep (for Site) Date 8 comments CI

<<<<<<<<<<<<<<<<<<<<<<<<<<Route To Author / 0 nit Supertrieer Safely Analysia flequiredf Ne G Ye> CI (See Aaa>al) if Yes, Analysis assigned to: Site Q, or to Engineerfng CI, Date:

Revfew of the sub)ect document has been completed and approval ls recommended

'Approv~hall sitfnlfy approval on the procedure cover sheet)

Ef.

DocumenthefdforSORC Meett NNo. 'fl- ).Approved, Yes& NoCL Ownership Dept. Supv. OIPL ~lt ~o 4 tk.~l

AND l HEI:KREHCK MCNIBIIS The gems entiredbefow have 5sen fnchded In the preparation andfor review of the attached reference document

'IJI'

.

and are prieentedh ~ataspecf5c check sheet $ 'or the docurmlt.

The foffoelny perlone~ consulted about Procedure fs fn complfance wlh the fotlowhg this procedure: Technical Specfffcstfons and Bases:

NAME:i'ITLE BY . SECTION AMENDMENT BY 4 -'0:

) I l. ~R Compliance with: CFR I U&4RC Comp f lance with:

REGULATORY GUIDE (S) DATED BY ANSI STANDARD (S) DATED BY A Icg

~S 4>>4 - H ~SI444 444 Complfance wfth: ASME Boiler and Pressure ls consistent with the following Station or Vessel Code (s) Site Procedures:

SECTION ADDENDUM BY NUMBER REY BY A -'2 C) 4(

4%-l.a

@l7-~cA wl Compliance with:

Other Information Sources Consulted BY FSAR I USAR REQUIREMENTS DATED BY LIQIE: Mc OE C 5 ( I CF" gc' Q)$

Procedure Evaluation Fomti Closed Out By This Revision PEF NNQKR BY PEF NUMBER BY AUTHOR i~~M ~ 'L~ DAm REVIEWED BY 'DATE

m wgfc7aPa'v c dc i,v m

ca@ ~c"p c as~) v vvc c .> 'jr ~

Vv REVlEN CHECK LIST To bo propsrod by Author Check List for Document ~'. - 7 l Rev. <~ Date "0" Only boxes thlt apply Yea NIA All references needed to implement the procedle are cfeaify identified and avalabfe. ~ P 0 The procedure contains adequate equipment lists, precautions and limitations, prerequisites, graphs, diagrams or data sheets as required ~ !P' Surveillance and Maintenance Procedure utilizes PLANT IMPACT statement associated with approval I permission for use.- ~ . ~ ~ ~ 0 KY As appropriate, procedure addresses use of MARKUPs..

If appropnate, procedure requires use of fire pmtection measures (ie., burning permits, etc,),-

If leads are lifted, jumpers placed or blocks used h the procedure, the PLANT IMPACT statement acknowledges such use.. - ~ - ~ ~ 0 G As appropriate, procedure notiTies other affected departments, such as Q.L,Openeons, Maintenance, and Rad Protection. - . - . - . --<<'0 Q If Technical Specification is exceeded, appropriate action is identified,. ~ .'0 When encountered, E.Q. related equipment is identrlied as such.

Procedure sleps are dear and accurate. They are not Neecessanly difficultto implement.

R( E3 The procedle reflects work as it is to be done at the statforL.

Procedle removes any jumpers e blocks and restores Htedieads used to effect the wortt.- ~ ~ 0 Ef "RRTURR TO ssllvlcs'us sUrgiitivmilicescnendblenlses aimdTvmbeing vedssd, ~

hRIIRITDII5CE' Wt PCS'ISIINCE TESTe references a reqwed test.- . 0 H MARKUPs ae cfeared e stmendeeL. ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ P ~ ~ ~ ~ ~ 0 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ - ~ 0 H "ACCEPTANCE CAfTERN iderkfies 0 ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ 0 Techrical spmilhuicns, smoa UsARIFRAR aml appleebieRegulssuy Guidsahave beenmvmmuiicccmpsance " ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ 0 cl

NIAGARA MOHAWK POWER CORPORATION NINE MILE POINT NUCLEAR STATION ADMINISTRATIVE PROCEDURE EVI T R DWA TE PR E T RAM Approved By:

M. J. HcCormick, Jr. Plant a . hit 2 Date Effective Date:

NOT TO BE USED AFTER Ra 1993 SUB J ECT TO PERIODIC REVIEW

F FF T VE PA

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~P~N. ~ggJtg.:

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~ ~ ~ ~ 23 24 2 25 3 ~ ~ 26 4 27 5 ~ ~ ~ ~ 28 29 7 0 ~ ~ 30 .

8 ~ ~ ~ ~ 31 9 32 10 . 33 ll 34 12 13 14 15 16 17 18 19 .

20 .

21 Page i AP-3.7.1 Rev 05

TABLE F QE~TI~N PA E 1.0 PURPOSE............. ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ \ ~ ~ ~ ~ 1

2.0 REFERENCES

AND COMMITMENTS..

3.0 DEFINITIONS...........

4.0 RESPONSIBILITIES 5 5.0 PROCEDURE 5.1 System Description 7 5.2 Asphalt Volume Reduction System.

5.3 Administrative Controls. 18 6.0 RECORD REVIEH AND DISPOSITION. 21 : Unit 2 Radwaste Process Control Program Implementing Procedures. 22 : Solid Haste Sources. 24 : Process Control Flowpath. 26 : System Flow Schematic 27 : Operator Horksheet 28 : Temperature Profile Log... ~ ...... 30 : Barnwell Manifest 31 : US Ecology Manifest............, 33 Page ii AP-3.7.1 Rev 05

1. 0 ~PRP~O 1.0.1 To describe the methods for processing, packaging and transportation of low-level radioactive waste and provide assurance of complete solidification of various radioactive "wet wastes" in accordance with applicable NRC regulations and guidelines.

1.0.2 To satisfy the Nuclear Regulatory Commission's Low-Level Waste and Uranium Recovery Projects Branch (HMLU) requirement and establish process parameters within which the Herner 0 Pfleiderer Corporation Volume Reduction System (HPC-VRS) must be operated to ensure complete solidification.

1.0.3 Waste process under this program using asphalt as the media is limited to Class A Waste.

~NTE: Conformance with WMLU requirements provides assurance that the requirements identified in 10CFR61, Sub Part D, Technical Requirements for Land Disposal Facilities and Final Haste

,Classification and Haste Form Technical Position Papers, which requires that Class A Waste shall be a free standing monolith with < .05 / free standing liquid.

1 i1 i This procedure applies to the Unit 2 Radwaste Process Control Program for solidification and transportation of radioactive waste.

2.0 AND MM TM NT 21 Li n D a i 2.1.1 QATR-1, Quality Assurance Program Topical Report for Nine Mile Point Nuclear Station Operations, Section 17.0, Quality Assurance Records 2.1..2 nit 2 T chn e ifi ti

a. Section 3.11.3-Action a, Solid Radioactive Wastes

b. Section 3.11.3-Action b, Solid Radioactive Wastes

c. Section 4.11.3.a, Solid Radioactive Wastes

d. Section 4.11.3.b, Solid Radioactive Wastes

e. Section 6.5.2.11, Review and Audit, Technical Review and Control Activities Page 1 AP-3.7.1 Rev 05

0 2.1.2 (Cont)

f. Section 6.5.3.8.i, Review and Audit, Safety Review and Audit Board

g. Section 6.F 1.8, Semi-Annual Radioactive Effluent Release Report

h. Section 6.13, Process Control Program 2.2 nd rd R 1 ti ns 2.2.1 ANSI/ANS 55.1, 1979, American National Standard for Solid Radioactive Haste Processing System for Light Water Cooled Reactor Plants 2.2.2 10CFR20.311, Transfer for Disposal and Manifest 2.2.3 10CFR20.311.d.3, Transfer for Disposal and Manifest 2'.2.4 10CFR61, Sub Part D, Technical Requirements for Land Disposal Facilities and Final Waste Classification and Haste Form Technical Position Papers 2.2.5 10CFR61.55, Haste Classification 2.2 ' 10CFR61.56, Haste Characteristics 2.2.7 10CFR71, Packaging and Transportation of Radioactive Material 2.2.8 49CFR173.l.b, Transportation 2.2.9 49CFR173.425, Transport Requirements for Low Specific Activity (LSA) Radioactive Materials 2.2,10 NUREG-0123, Standard Radiological Effluent Technical Specifications for Boiling Water Reactors 2.2.11 NUREG-0800,'.

Section 11.2, Standard Review Plan for Liquid Haste Management Systems

b. Section 11.4, Standard Review Plan for Solid Haste Management Systems 2.2.12 Resource Conservation and Recovery Act (RCRA) of 1976 (Ref.

Corporate Guide to Hazardous Waste Disposal and Spill Reporting) 2.2.13 Regulatory Guide 1.143, Rev. 0, Design Guidance for Radioactive Waste Management Systems, Structures, and Components Installed in Light Hater Cooled Nuclear Power Plants Page 2 AP-3.7.1 Rev 05

2.3 Pol i r nd Pr c r s 2.3.1 NIP-ECA-01, Deviation Event Report 2.3.2 AP-2.0, Production and Control of Procedures 2.3.3 AP-3.3.1, Site ALARA Program 2.3.4 AP-7.2, Control of Material Storage Areas 2.3.5 AP-9.0, Administration of Training 2.3.6 AP-10.1, Management of Station Records

2. 3". 7 N2-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2 2.3.8 N2-0P-41, Asphalt Solidification Operating Procedure 2.3.9 N2-NTP-13, Nuclear Department Training Manual 2.3.10 N2-WHP-l, Required Documents Concerning Packaging and Shipping of Radioactive Wastes 2.F 11 N2-WHP-2, Paperwork for a Radioactive Waste Shipment 2.3.12 N2-WHP-4, Cask Loading Procedure 2.3.13 N2-WHP-88, Flatbed Loading Procedure 2.3.14 N2-WHP-9, Asphalt Solidification 2.3.15 N2-WHP-9A, Operating Procedure Vendor Solidification 2.3.16 N2-WHP-98, Process Control LN Cement Solidification

'2.3.17 N2-WHP-10A, Process Control Oil/Cement Solidification Procedure 2.3.18 N2-WHP-108, Cement/Oil Solidification Procedure 2.3.19 N2-WHP-ll, Process Control Dry Solid Waste 2.3.20 N2-WHP-12, Solid Dry Waste Collection and Compaction 2.3.21 N2-WHP-14, Solidified Liner Inspection Program 2.3.22 NTP-l, Training and Continued Training of Chemistry and Radiochemistry Technicians 2.3.23 NTP-13, Training and Continued Training of Radwaste Operators 2.3.24 NTP-14, Training and Continued Training of Radiation Protection Technicians Page 3 AP-3.7.1 Rev 05

2.3.25 S-RPIP-7.1, Movement and Storage of Radioactive Material on Si te 2.3.26 S-RP IP-7. 2, Receipt of Radioactive Material 2.3.27 S-RPIP-7.3, Determination of Shipment Type 2.3.28 S-RPIP-7.4, Cask Shipments 2.3.29 S-RPIP-7.5, Van/Flatbed Shipments 2.3.30 S-RPIP-7.6, Activated Materials Shipments 2.3.31 S-RPIP-7.7, Non-Haste Radioactive Shipments 2.3.32 S-RPIP-7.8, Shipping Documents 2.4 Su le en 2.4.1 South Carolina Department of Health and Environmental Control, Radioactive Material License 097, as amended 2.4.2 State of Washington Radioactive Material License No.

HN-I019-2, as amended 2.4.3 Herner and Pfleiderer Corporation Topical Report No.

HPC-VRS-001, November 1976, Rev. 1, May 1978, Appendix B, Solid Content 2.4.4 NRC Special Nuclear Material License No. 12-13536-02, as amended, for Barnwell, SC 2.4.5 NRC Special Nuclear Material License No. 16-19204-01, as amended, for Richland, WA 2.4.6 Nuclear Regulatory Commission Branch Technical Position on Haste Classification and Waste Form, May 1983

.5 ~C Sequence NCTS NumluNr /goer D ri i n None Page '4 AP-3.7.1 Rev 05

3.0 DEFINITION n n 3.1 Waste usually segregated from other waste classes at the disposal site. The physical form and characteristics shall meet the minimum requirements of 10CFR61.56, Waste Characteristics.

3' 1 "B" W ste Waste meeting more rigorous waste form requirements to ensure stability after disposal. Class B waste form shall meet both the minimum and stability requirements of 10CFR61.56, Waste Characteristics."

3.3 1

" " W e Waste meeting Class 8 standards and requiring additional measures at the disposal facility to prevent inadvertent intrusion.

4.0 ~EN 4.1 The Plant Manager shall:

4.1.1 Review and approve changes to the Unit 2 Radwaste Process Control Program in accordance with Unit 2 Technical Specification, Section 6.5.2.11, Review and Audit, Technical Review and Control Activities.

4.1.2 Ensure the Unit 2 Radwaste Process Control Program provides for the health and safety of the general public as it applies to Radwaste Management.

4.2 nr rv r R dwa e The General Supervisor Radwaste shall:

4.2.1 Implement the Radwaste Process Control Program.

4.2.2 Interface with the Manager Chemistry on matters concerning radwaste processing and disposal, as required.

4.2 ' Interface with the Manager Radiation Protection on matters concerning radwaste processing and disposal, as required.

4.2.4 Supervise activities related to radwaste collection, processing, packaging, storage, transportation, and disposal.

Page 5 AP-3.7.1 Rev 05

4.2.5 Review Radwaste Process Control Program implementing procedures to ensure validity of technical content and compliance with applicable Federal and State Regulations, Technical Specifications, Company Policies, and the Station Operating License.

4.2.6 Ensure compliance with Federal and State Regulations governing the transportation and disposal of radioactive material.

4.2.7 Ensure Radwaste Operators complete required training and qualification and maintain proficiency, as required.

4.3 Mana r h mi str The Manager Chemistry shall:

4. 3.1 Interface with the General Supervisor Radwaste on matters concerning radwaste processing and disposal, as required.

4.3.2 Ensure Chemistry Technicians complete required training and qualification and maintain proficiency, as required.

4.3.3 Ensure Chemistry Technicians calculate and determine Haste-to-Asphalt flow rates and contents in accordance with established procedures.

4.4 Man er ia i Pr ecti n The Manager Radiation Protection shall:

4.4.1 Interface with the General Supervisor Radwaste on matters concerning radwaste processing and disposal, as required.

4.4.2 Ensure Radiation Protection Technicians complete required training and qualification and maintain proficiency, as required.

4.5 he T hni i Chemistry Technicians shall perform analysis of radioactive waste samples.

4.6 Ra i i Pr ion Techni Radiation Protection Technicians shall perform radiological controls monitoring on radwaste shipments.

4.7 d Radwaste Operators shall perform operations associated with radwaste processing.

Page 6 AP-3.7.1 Rev 05

5.0 ~PR QE~DRI..

5.1 S stem Descri 10 5.1.1 ~n~~rl The Solid Haste Management System (SHMS), implemented by the procedures identified in the Unit 2 Radwaste Process Control Program Implementing Procedures (Attachment 1) collects, reduces the volume, solidifies, and packages wet and dry types of radioactive waste in preparation for shipment off-site to a licensed burial site.

b. Types of solid waste sources are identified in Solid Haste Sources (Attachment 2).

C. Radwaste Process Control Flowpath (Attachment 3) and System Flow Schematic (Attachment 4) are provided for the Unit 2 SHMS.

d. The Solid Haste Management System accepts dry solid trash which is, when physically possible, compacted with a trash compactor.

Bead resins or powdered resins are dewatered in high integrity containers or processed along with evaporator bottoms through the extruder evaporator.

When required, Unit 2 will use the services of a vendor to solidify waste.

5.1.2 fv r or a ~ The extruder/evaporator is a one-step volume reduction and solidification process.

b. Two screws inside the twin screw extruder/evaporator convey the waste/asphalt mixture along the length, continually shearing and mixing the waste/asphalt.

c ~ The screw speed can be regulated to control the evaporating capacity and residence time of the waste.

d. The extruder/evaporator discharges a homogeneous mixture of asphalt and waste containing 59 free standing water.

e. The solid radwaste system uses the extruder/ evaporator to process waste fed from two inputs; the evaporator bottoms tank or the waste sludge tank. The waste is mixed with asphalt in the extruder. Only one waste feed path can be processed at a time.

Page 7 AP-3.7.1 Rev 05

(Cont)

f. Operation of the extruder/evaporator is detailed in N2-0P-41, Asphalt Solidification Operating Procedure.

a. The evaporator bottoms tank and lines are electrically heat traced to prevent crystallization of waste salts.

b. The contents of the tank are fed to the extruder/

evaporator via a transfer pump that supplies redundant metering pumps.

c. The waste flow rate is controlled manually by adjusting the flow rates on the metering pumps.

1 e T

a. The contents of the waste sludge tank are fed to the extruder/evaporator by a separate system from the evaporator bottoms feed system. This system has redundant waste sludge metering pumps.

b. The waste sludge tank is supplied by waste from three sources: the radwaste filters, the floor drain filter, and the spent resin tank.

c. The waste flow rate is controlled manually by adjusting the flow rates on the metering pumps.

d. The waste sludge tank has the ability for decantation.

A decant pump takes a suction off the sludge tank and discharges to the spent resin tank.

The contents of the asphalt tank is fed to the extruder/evaporator via redundant recirculation pumps, strainers, and metering pumps.

b. The asphalt flow rate is automatically adjusted to yield the proper ratio of asphalt to solids.'he C. asphalt tank and lines are continuously steam heated to keep the asphalt in a liquid state for ease in pumping.

Page 8 AP-3.7.1 Rev 05

ri dw a 0 As the waste/asphalt mixture moves through the extruder/evaporator, the mixture is heated by steam from the electric radwaste bo'iler.

b. The boiler is a skid mounted boiler'ystem which uses electricity for steam production.

P C. The boiler is a closed system, therefore, most of the water used for steam is returned to the boiler as condensate via the boiler feedwater system.

d. The boiling vessel is capable of supplying 1400¹/hr of steam at 233 psig and 400'F.

e. The steam applied to the extruder is used in six separate heating zones for moisture evaporation.

Each zone has a separate temperature controller for optimum operating conditions.

Dv 1 1 or Three devolatizati'on ports along the extruder allow for water vapor to separate from the product and enter the three steam domes.

A predetermined amount (4 gal.) of demineralized water is used, which dissolves and boils out salt sediment at the devolatization port ~

The vapors are condensed in the steam domes using turbine building closed loop cooling and drained to the distillate collection system.

11 lie i

a. The distillate collection system is a recirculating system used to continuously filter and cool the condensate from the extruder/evaporator steam domes.

b. The condensate is recirculated from the distillate collection tank through the distillate pumps, roughing filter, and the distillate cooler, then routed back to the collection tank.

The level controller maintains collection tank level and system flow.

Page 9 AP-3.7.1 Rev 05

5.1.9 V n i i n te a ~ A forced circulation ventilation system is incorporated into this system.

The system consists of a vent hood over the extruder/

evaporator turntable, a fan which draws air from the plant ventilation system across the extruder/evaporator turntable, and liner cool down areas.

5.1.10 ~Lin r The extruder/evaporator product empties into 50 cubic feet liners.

The liners are placed on the fill station turntable.

The operator indexes (turns) the turntable via a control switch, placing a liner under the discharge chute of the extruder/evaporator.

c ~ The turntable holds three liners. When the liner level reaches a predetermined level, a high level alarm sounds to inform the operator it is time to index the container.

Liners are indexed without shutting down the extruder/evaporator. Using control switches, the operator, via a pneumatic carrier, extends a drip pan under the extruder/evaporator discharge chute. The operator then indexes the turntable.

e. Once the new liner is in place under the extruder/

evaporator discharge chute, the pneumatically operated carrier is withdrawn.

During this withdrawal operation, the drip pan is removed from the carrier by a stationary arm as the carrier retracts past the arm and drops the drip pan into the new liner.

5.1.11 ~r e a ~ Full liners are removed from the turntable to the cooldown area via a radio controlled/operated crane.

b. After cooldown is completed, the liners are moved by crane to the storage area using a ceiling grid coordinated system for placement of the liner.

C. When the liners are to be shipped, the liners are moved to the capping station and capped just before shipment then loaded for transportation to the burial location.

Page 10 AP-3.7.1 Rev 05

5.2 As h 1 V m edu i n m 5.2.1 Radwaste Operators shall ensure proper equipment is available before beginning radwaste processing. Radwaste Operators may process wastes through the extruder/evaporator when the following equipment is operable:

a. Closed circuit television system at the asphalt loading stations

b. Calibrated temperature profile monitoring instrumentation

c. Operational asphalt and waste metering equipment

d. Solid radwaste sampling stations.

5.2.2 V i 1 Inf1 Pr Radwaste Operators shall control the following variables to ensure the final waste product is a free standing monolith with essentially ~N free standing water:

a. Asphalt type

b. Waste chemical species being incorporated into the asphalt matrix/water content

c. Ratio of waste-to-asphalt

d. Process temperature

e. Additional process variables. such as pH, that do 5QT affect the ability of the waste product to form a solid free standing monolith upon cooling .

5.2.3 h 1 T e Radwaste Operators shall:

Use an oxidized petroleum-based asphalt, conforming to ASTM-D-312-71, Type III requirements with the following properties:

1. Has a low residual volatile content

2. Has a high molecular weight

3. At room temperature, or ambient conditions, is a free standing monolith

4. Specify Witco Pioneer 221, or an equivalent asphalt Page ll AP-3.7.1 Rev 05

5.2.3 (Cont)

~NTE. Consult Werner and Pfleiderer Corporation if an alternate asphalt material is to be used.

b. Ensure verification of asphalt type is conducted per N2-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2.

5.2.4 W h mi 1 Radwaste Operators shall ensure:

a. Testi'ng is performed to determine the oil content and physical properties of the waste to be solidified per N2-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2.

b. Adherence to the Werner and Pfleiderer limit of 1.0/.

oil and organic contaminants in the waste feed stream for process control.

Type and relative quantity (waste-to-asphalt) of waste chemicals being incorporated in the asphalt matrix has a direct influence on the properties of the final product:

l. Encapsulation of inorganic salts and solids typically "stiffen" and harden the waste product.

2. Encapsulation of organic liquids typically softens the waste product.

5.2.5 h 1 Radwaste Operators shall use the following waste-to-asphalt ratios:

gOOE;: Optimum values depend on type and quantity of contaminants present.

a. Evaporator Concentrates 40/60 to 50/50

b. Spent Resins 45/55 to 50/50

c. filter Sludge 40/60 to 50/50 Page 12 AP-3.7.1 Rev 05

When the ratio of waste-to-asphalt is increased above the range specified above, the end product viscosity will increase and may exhibit a grainy texture. This could lead to "pyramiding" of the product in the container, thereby decreasing the container filling efficiency.

W - - hl Fl w

a. Radwaste Operators shall set the initial proportion of waste-to-asphalt flow based on Chemistry Department calculations.

b. The Chemistry Department shall determine the solids content of the waste feed by sampling.

c. The Chemistry Department shall:

1. Determine the proper feed control settings in accordance with N2-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2, for flow rate calculations.

2. Calculate flow rates based on the information supplied in Werner and Pfleiderer Corporation Topical Report No. WPC-VRS-001, November 1976, Rev. 1, May 1978 Appendix 8 Solid Content.

Radwaste Operators shall visually confirm the proper ratios are being maintained on the Solid Radwaste Control Panel.

1. A closed circuit television camera may be used to view the discharge from the extruder/evaporator.

2. The television monitor located .in the control room allows observation of the physical consistency as the product is discharged into the container.

Radwaste Operators shall:

a ~ Ensure a proper temperature profile is maintained along the length of the extruder/evaporator to provide adequate evaporative (process) capacity.

Ensure free water is ~T discharged from the machine.

Page 13 AP-3.7.1 Rev 05

(Cont) 5QT~: 1. Low temperature alarms are provided to alert the operator to a low temperature off-normal condition which could lead to the discharge of free water.

2. Low temperature alarms are typically based on a z10'F deviation from setpoint. The above can be adjusted up to z25/. (+75'F) of the instrument range.

c. Adhere to the following (approximate) temperature profiles:

1, Evaporator Concentrates:

Zone 1 165'F Zone 2 265'F Zone 3 300'F

~ Zone 4 330'F

~ Zone 5/6 375'F Zone 7 350 F.

2. Spent Resins, Filter Sludge:

~ Zone 1 165'F Zone 2 265'F Zone 3 285'F

~ Zone 4 300 F

~ Zone 5/6 285'F

~ Zone 7 230'F.

d. Log temperature profiles every two hours during equipment operating run time.

i I n i r The General Supervisor Radwaste shall ensure:

a. High Integrity Containers (HIC) are used for dewatering to satisfy the stability requirements.

Page 14 AP.-3.7.1 Rev 05

5.2.8 (Cont)

b. Each HIC is accompanied by a certificate of compliance.

c. Dewatering procedures based on an NRC approved vendor process control program or "Topical Report" are part of N2-WHP-4, Cask Loading Procedure.

d. Documentation of adherence to procedures are maintained as records.

5.2.9 in ed Oi s The General Supervisor Radwaste shall ensure:

a. Contaminated oils are stored in containers at designated areas within the plant.

b. A vendor with an approved process control program acceptable at the selected burial site is used to solidify the oil.

c. NZ-WHP-10A, Process Control Oil/Cement Solidification Procedure, is used for operating the portable oil solidification system.

d. N2-WHP-108, Cement/Oil Solidification Procedure, is used to sample production level.

5.2.10 Tem r R w Processin The General Supervisor Radwaste shall ensure:

a. The vendor is NRC approved and has demonstrated a commitment to 10CFR61, Sub Part D, Technical Requirements for Land'isposal Facilities and Final Waste Classification and Waste Form Technical Position Papers stability requirements.

b. The vendor has completed Class 8 and C waste testing or has provided a schedule of completion.

c. The vendor has an approved procedure to process Class A waste (Dewatering, Solidification).

d. Vendor procedures are acceptable if:

1. Vendor procedures are reviewed and approved in accordance with AP-2.0, Production and Control of Procedures.

2. A production sample level process control procedure is implemented.

Page 15 AP-3.7.1 Rev 05

5.2.10.d (Cont)

3. The vendor is provided samples in accordance with N2-0P-41, Asphalt Solidification Operating Procedure, and N2-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2.

5.2.11 Dr iv W e DAW The General Supervisor Radwaste shall ensure:

a. The proper and safe steps are performed to collect and prepare low specific activity (LSA) DAW in accordance with N2-HHP-12, Solid Dry Haste Collection and Compaction.

b. Items most directly influencing the quality of the end product are identified and controlled in accordance with N2-WHP-ll, Process Control Dry Solid Haste.

C. DAH is examined for liquids or items that would compromise the integrity of the package or violate the burial site license and/or criteria before compacting is removed or separated.

d. DAW is shipped in containers meeting the transport requirements of 49CFR173.425, Transport Requirements for Low Specific Activity (LSA) Radioactive Materials.

Waste precluded from disposal in LSA boxes or drums due to radiation limits is disposed of in liners in accordance with N2-HHP-4, Cask Loading Procedure.

5.2.12 ~~lin Radwaste Operators and the Chemistry Department shall ensure:

a. The evaporator bottoms tank (Tk10) and the waste sludge tank (Tk8) are isolated from further input when preparing to process waste and a batch number is assigned in accordance with the Operator Worksheet (Attachment 5).

b. The evaporator bottoms tank (TklO) is recirculated to ensure a homogeneous mixture.

c ~ The waste sludge tank (Tk8) is agitated to ensure a homogeneous mixture.

A sample is obtained from the tank(s) to be processed in accordance with N2-0P-41, Asphalt Solidification Operating Procedure and N2-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2.

Page 16 AP-3.7.1 Rev 05

5.2.12 (Cont)

e. The sample from the tank(s), to be processed is analyzed and the sample data sheet form in N2-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2, is completed.

f. The Chemistry Department shall determine the chemical and radionuclide content of each sample.

g. Completion of the Operator Horksheet (Attachment 5).

h. Completion of the Temperature Profile Log (Attachment

6) during processing.

After obtaining feed rate data from the Chemistry Department, the given feed rates for introduction into the extruder/evaporator are selected.

j. If batch processing is interrupted, the Radwaste Operator shall isolate the source tank until processing can resume.

~ ~

5.2.13 H 1

a. The Unit 2 Radwaste Process Control Program assures that wastes determined acceptable for near surface disposal are properly classified.

b. Haste classification is performed consistent with the guidance provided in the Branch Technical Position .

pertaining to Haste Classification and is based upon the concentration of certain radionuclides in the waste form as given in 10CFR61.55, Waste Classifica- tion, and 10CFR61.56, Haste Characteristics.

The methods used by Unit 2 and the frequency for determining the radionuclide concentration of the final waste form are conducted in accordance with NZ-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2.

C. The General Supervisor Radwaste shall ensure:

The minimum waste characteristic requirements identified in 10CFR61.56, Waste Characteristics, are satisfied by implementation of applicable S-RPIPs for the packaging and transportation of radioactive material.

2. The radionuclide concentration determin'ation methods and frequency are conducted in accordance with N2-CSP-14, Solid Radwaste Chemical Surveillance at Unit 2.

Page 17 AP-3.7.1 Rev 05

5.2.13 (Cont)

d. The Manager Chemistry and Manager Radiation Protection shall ensure classification of waste is performed in accordance with S-RPIP-7.3, Determination of Shipment Type.

5' Administra ive Control gQTT,: -The Manager, Nuclear QA, Operations has the authority to stop work when significant conditions adverse to quality exist and require corrective action.

5.3.1 gua A rc re r r r

~re uire:

a. Ongoing review, monitoring, and audit functions.

b. Performance of audits, under the cognizance of the SRAB, of the Process Control Program and implementing procedures for processing,and packaging of radioactive waste at least once every 24 months as required by Unit 2 Technical Specification 6.5.3.8.i, Review and Audit, Safety Review and Audit Board.

c. Compliance with the waste classification and characterization requirements of 10CFR61.55, Waste Classification and 10CFR61.56, Haste Characteristics.

d. Quality Assurance Inspectors performing radwaste inspections have documented training in Department of Transportation and NRC radwaste regulatory requirements.

e. Quality Assurance review of vendor procedures.

f. Quality Assurance review of vendor programs to ensure compliance with 10CFR71, Packaging and Transportation of Radioactive Materials, Quality Assurance requirements.

5.3.2 Trainin ro e ure Tr ini Pro r r ~uir  :

a 0 Radwaste Operator qualification by completion of the Radwaste Operations Unit 2 Plant Training Program with:

l. An average grade of 80 percent or above.

2. On-the-job training in conjunction with classroom instruction to ensure each radwaste operator maintains an acceptable level of skill and familiarity associated with radwaste controls and operational procedures.

Page 18 AP-3.7.1 Rev 05

5.3.2.a (Cont)

3. Training in accordance with NTP-13, Training and Continued Training of Radwaste Operators.

b. Training of Radwaste Operators includes, but is ~N T limited to, familiarity with the following radwaste components or related systems:

1. Liquid-drains, collection tanks with subsystems, waste and regeneration evaporators, and seal water

2. Solid-Extruder/evaporator and associated support systems

3. LWS-Computer operation and interfaces

4. Waste handling procedures for packaging and shipping of radioactive materials

5. Condensate demineralizer system

6. Spent fuel and phase separators subsystem

7. Steam supplies Chemistry Technicians are trained in accordance with  !

NTP-l, Training and Continued Training of Chemistry and Radiochemistry Technicians.

-

d. Radiation Protection Technicians are trained in accordance with NTP-14, Training and Continued Training of Radiation Protection Technicians.

e. A formal classroom Radwaste Training Program is scheduled based on the needs of Radwaste Operations personnel.

~N T : This training may be covered in a continuous cycle or as part of the normal rotating shift schedule.

Retraining of Radwaste Operator personnel on an annual basis identifies individual needs for retraining.

Personnel demonstrating a significant deficiency in a given area of knowledge and proficiency are placed in a remedial training program as directed by the General Supervisor Radwaste.

Page 19 AP-3.7.1 Rev 05

5.3.2.f (Cont)

2. Successful completion of the accelerated training program is evaluated by a written and/or oral examination as directed by the General Supervisor Radwaste.

NOTE: The Requalification Training Program covers a fundamental review of system modifications, revisions or changes to procedures, and changes or experiences in the nuclear industry.

g. Training records:

1. Are maintained for audit and inspection purposes.

2. Are considered permanent records.

3. Shall meet the applicable requirements of QATR-l, Quality Assurance 'Program Topical Report for Nine Mile Point Nuclear Station Operations, Section 17.0, Quality Assurance Records, AP-9.0, Administration of Training, and AP-10.1, Management of'tation Records.

5.3.3 i n n e r n

a. Station management shall evaluate QA program audits of waste classification records to satisfy the requirements of 10CFR20.311.d.3, Transfer for Disposal and Manifests.

b. Personnel shall forward changes affecting operating procedures to Nuclear-QA for review in parallel with the NMPC Operations review as required.

c. Site Records Management shall maintain waste management records in accordance with the appropriate administrative procedures.

5.3.4 ~Li n -i i i 2 w n r r r

a. Are submitted to the Commission by the method and containing the information as required by Technical Specification 6.13, Process Control Program.

b. Become effective upon review and acceptance by the SORC.

Page 20 AP-3.7.1 Rev 05

5.3.5 T 1 rvi r w Shipping manifests are completed and tracked to satisfy the requirements of 10CFR20.311, Transfer for Disposal and Manifests, in accordance with Waste Handling Procedures.

b. Radwaste Management monitors the status of the manifests in accordance with N2-WHP-2, Paperwork for a Radioactive Waste Shipment.

Temporary storage of solid radioactive material awaiting shipment in an area other than a designated area is done in accordance with AP-7.2, Control of Material Storage Areas.

6.0 REC RD REVIEW AND DISPOSITION Ensure the following records are retained in accordance with'AP-10.1, Management of Station Records.

Operator Worksheets

~ Temperature Profile Logs Page 21 AP-3.7.1 Rev 05

ATTACHMENT 1 UNIT 2 RADWASTE PROCESS CONTROL PROGRAM I PLEMENT N P EDU E (Sheet 1 of 2)

W e H n lin Pr r (WHPs N2-WHP-1 Required Documents Concerning Packaging and Shipping of Radioactive Wastes N2-WHP-2 Paperwork for a Radioactive Waste Shipment N2-WHP-3 Cask Handling Procedure NZ-WHP-4 Cask Loading Procedure I

N2-WHP-6 Van Handling Procedure N2-WHP-7 Van Loading Procedure N2-WHP-8A Flatbed Handling Procedure N2-WHP-8B Flatbed Loading Procedure N2-WHP-9 . Asphalt Solidification N2-WHP-9A Cement Solidification Procedure N2-WHP-9B Process Control LN Cement Solidification N2-WHP-10A Process Control Oil/Cement Solidification Procedure N2-WHP-108 Cement/Oil Solidification Procedure N2-WHP-ll Process Control Dry Solid Waste N2-WHP-12 Solid Dry Waste Collection and Compaction N2-WHP-14 Solidified Liner Inspection Procedure di i n Pr te i Pr c u e S-RPIP-7.1 Movement and Storage of Ra'dioactive Material on Site S-RPIP-7.2 Receipt of Radioactive Material S-RPIP-7.3 Determination of Shipment Type S-RPIP-7.4 Cask Shipments S-RPIP-7.5 Van/Flatbed Shipments Page 22 AP-3.7.1 Rev 05

ATTACHMENT 1 UNIT 2 RADWASTE PROCESS CONTROL PROGRAM IMP EMENTIN PR ED (Sheet 2 of 2)

R i ti n Pr i n Pr ce r PI (Cont)

S-RPIP-7.6 Activated Materials Shipments S-RPIP-7.7 Non-Waste Radioactive Shipments S-RPIP-7.8 Shipping Documents h i r Prcd P N2-CSP-14 Solid Radwaste Chemical Surveillance at Unit 2 li A r eP r P QAP-10.03 QAD Surveillance Activities for Operations QAP-10.30 QAD Inspection Acti vi ties QAP-18.10 QAD Audits i Pr N2-OP-40 Liquid Radwaste Operating Procedures N2-OP-41 Asphalt Solidification Operating Procedure mi i AP-10.1 Management of Station Records AP-3.3 Radiation Protection Program AP-3.3.2 Radiation Work Permit AP-3.3.3 Radiation Worker Conduct 1 r D'vi i n In rf in Pro ed r I NIP-ECA-Ol Deviation Event Report Page 23 AP-3.7.1 Rev 05

ATTACHMENT 2 OLID WA T E (Sheet 1 of 2) 1.1 Mechanical radwaste filters filter resin and crud (backwash material) from the waste collector sub-system.

1.2 When a filter reaches a pre-determined differential pressure, the filter backwashes the material into the backwash tank, which is. then pumped to the spent resin tank.

2.0 RADWA TE DE I E L ZE 2.1 The radwaste demineralizers are used as an ionic exchange media for processing high quality water from the waste collector tanks.

2.2 When determined the resin can gQ longer be regenerated, the depleted resin is pumped to the spent resin tank.

3.0 ND TE D I 3.1 The condensate demineralizers remove soluble and insoluble impurities from the condensate water to maintain reactor feedwater purity.

3.2 After it is determined these resins can gO longer be regenerated, the depleted resins are pumped to the spent resin tank.

4.0 LO D I IL 4.1 The floor drain filter contributes to solid waste because the filter uses diatomaceous earth to process liquid waste of low quality. Input to the filter is from the floor drain system and the regeneration waste tank.

4.2 When the filter reaches a pre-determined pressure drop the filter backwashes to the waste sludge tank for processing through the extruder/evaporator.

5.0 PENT F PHA E A A These tanks receive the exhausted powdered filter media (resins) from the fuel pool cleanup system which is subsequently pumped to the spent resin tank.

6.0 W PH P T These separator tanks receive exhausted powdered filter media (resins) from the water cleanup system which is subsequently pumped to the spent resin tank.

Page 24 AP-3.7.1 Rev 05

ATTACHMENT 2 llua~t (Sheet 2 of 2) 7.0 NTAMINAT D I Oil from sources within Unit 2 that become contaminated are stored in containers to be solidified by a vendor with an approved procedure.

8.0 0 PA IB D 8.1 Compactible low level trash is processed and compacted in a hydraulically operated box compactor.

8.2 Shoe covers, trash, contaminated paper from the chemistry lab, and similar materials are included in this category.

9.0 FIL E ND I ELLANE ITEM Solid items with high dose rates are handled on a case-by-case basis, being disposed of by methods acceptable to the burial site.

10.1 The waste evaporator processes low quality waste from the floor drain collector system and, as an option, waste from the waste discharge tanks.

10.2 The waste evaporator is designed to concentrate the waste to a 25%

solid concentration. The concentrates are then discharged to the evaporator bottoms tank for processing through the extruder/evaporator.

11.0 RE ENERANT EV RAT 11.1 The regenerant waste evaporator receives regeneration solutions from the condensate demineralizer system and radwaste demineralizer resin regeneration system as well as the radwaste regeneration sump.

11.2 The regenerant waste evaporator is designed to concentrate to a 25% by weight solid concentration of sodium sulfate.

11.3 The concentrates are then discharged to the evaporator bottoms tank to be processed through the extruder/evaporator.

12.0 PENT N T RA E T 12.1 Exhausted resin from the condensate demineralizer, the radwaste demineralizer, RNCU phase separator, the spent fuel pool phase separator, and the radwaste filter backwash tanks are sluiced to the spent resin storage tank.

12.2 The waste from the spent resin storage tank is pumped to the waste sludge tank for processing through the extruder/evaporator.

Page 25 AP-3.7.1 Rev 05

ATTACHMENT 3 PR E NT L L W Start Pro Rett Asar>>tt Sampted.HASP.ti ItZ

> and Ms Sempre Was>> NZ.WHP.OB Form Chsmcat Analysts N2.WH P-10 8 -NZ<P-41 Nz wHp.o M2 wHp 08 NZ WHP 0* N2 WHPR Propose Was>> Form NZ WHP.OB NZ WHP 11 MZ WHP 12 S RPIP 7,1 S RPIP 7.3 To Storaae P. T. Ctssst ty, Label and or SNp lor N2 WHP.O S RPIP 7o4 Store Wes>> Form Ctspo eel N2 CSP.11 S RPIP-7.$ MZ WHP 2 S RPIP 7.8 NZ WHP.Z N2.WHP 2 NZ-WHP.2 S-RPIP-7.3 S RPIP-7 ' S-RPIP 7.4 S RPIP 7.8 S-RPIP-7 ' Was'>> Roe&ed Invesdaate N2 WHP 2 At IXsposal St>> Itspoeat St>> N2 WHP 2 Page 26 AP-3.7.1 Rev 05 ATTACHNENT 4 Y W Reactor Water Ctean Up Phase Separator Spent Fuel Phase Sepsraatr Condensate Radwaste Demtneralzsrs Radwaste Demlneratlzers Radwsste Roor Drain Filter Filters To Floor Drain Waste Sudge Waste FLT Tank Evaporator R.T Waste Tank er Evsp. Sludge Bonoms Meter lnQ Ptltp Distigate Collection Tank Steam Domes Evaporator EvaP am Bonoms Metering Bonoms Vent Et GRLREAKVAPORATOR be ai sphal Pumps ank Cool Down Lube ON Filter Fill Area Tank Stadon 0 Asphalt Metering oAw. comparer ~ ~LS DA.W. Storage A Solid Waste Storage Page 27 AP-3,7.1 Rev 05 ATTACHMENT 5 ILEPlLODB~E (Sheet 1 of 2) FIGURE I Operator Horksheet Batch Number Date A batch is considered (1) A Sampled Sludge TK, or (2) a sampled Evaporator Bottoms Tank with no waste being added to the tank during the processing of that batch. ~NOT Batch number will consist of; BA (Batch Asphalt), year, and a four-digit successive number, (beginning with 0001). JI4 Unit Year Batch Number

b. Type of Haste Resin Filter Media Concentrate Haste

1. Waste Temperature 'F

2. Rad Level

3. Specific Gravity

4. pH

5. / Oil

6.  % Solid

7. Activity M/Ci /ml C. QA to verify chemistry results and flow settings prior to starting E/E QA Date

d. Feed Flow Settings

l. Asphalt feed flow settings

2. Haste feed flow settings

e. Radioactive materials classification

1. Radioactive materials LSA

2. Other Page 28 AP-3.7.1 Rev 05

ATTACHMENT 5 gP ERATOR~Wf~HQT (Sheet 2 of 2) fIGURE I (Cont)

f. Waste container labeled in respect to S-RPIP-7 ~ 3

1. Labels with the appropriate data will be supplied to the Radwaste Operator by the Radiation Protection Department/

Chemistry Department.

2. The operator must label container.

g. Radioactive waste classification

1. Class A Waste

2. Class B Waste

3. Class C Waste

h. Was container labeled in respect to S-RPIP-7.3

1. The Radwaste Operator will label the container with labels he received from the Radiation Protection Department.

Temperature Profile the radwaste operator must monitor the temperature profile while processing waste. The profile must be logged every 2 hours2.314815e-5 days <br />5.555556e-4 hours <br />3.306878e-6 weeks <br />7.61e-7 months <br /> of operations. In addition, the operator must include liner numbers that were solidified in that batch, and record time it took to fill each container of a particular batch. See a. (Figure II). After completion of the Operator Worksheet and temperature profile log, a copy will be returned to the Radiation Protection Department and the original returned to Radwaste Supervision for permanent records. The radwaste operator will retain a copy in the Radwaste Control Room. Page 29 AP-3.7.1 Rev 05 C 8 ATTACHMENT 6 FIGURE II

a. Temperature Profile Log Record of Temperature in Degree F every two hours of Run Time for a particular batch. II TYPE OF WASTE BATCH ¹ START TIME

'2 4 Ini Bead Resin = Precoat Filtercake 200 280 320 350 300 190 w/Powered Resin-Mixed Resin and il Precoat Filtercake w/Diatomaceous Earth- 200 280 320 350 350 280 Evaporator Concentrates D n f r 4 r f r H r f r 1 H r f r 1 r r 1 H r Af r 2

b. Did temperature profile remain within li,mits?

NINTH: The temperature profile should be monitored constantly but must be logged every second hour of Run Time. n in r um r 1 Tim Page 30 AP-3.7.1 Rev 05 ATTACHHENT 7 1A F (Sheet 1 of 2) (3) (I) GFNEAATOR'NAME BARNWELLWASTE MANAGEMENTFACILITY CAAAIER ADDRESS FACtllTV Operated by CHEM NUCLEAR SYSTEMS, INC. TELEPHONE SIOPPOIG OAIE ADDRESS PO Box 726. Barnweg, South Caro))tta 29812 (803) 259-(781 SIOPMENT 1YPE SIOIM(h( SUIUAC((XFOSUIIE mR.lv ZIP RADIOACTIVESHIPMENT MANIFEST FORM CAY S'lA'IE CODE CASK IDENTIFCATION NO. USA (3A) RADIOACTIVEWASTE TRANSPORTAT)ON PEALUT NO. CONTACT PHONE ( ) SIOPMENT NO. LPIER 1YPE EME AGE HCY RESPONSE CONTACA (C) USE THIS NUMSEA ON SIOPMENT LD. NUMSEA PAGE LPIEA SERIAL NO. PHONE ( ) AILCCNT INUATICNPAGES OF (3) SILL T(k DRIVER SIGNATURE DATE (38) NUMSEA OP GENEAATORS (S) TOTAL FOR PROPER SISPPINO NAME ~ HA?AAO CIASS I O. SHSrMENT TOTALS (s) TOTAL SNM EACH CLASS (PERsgcFRtn toU NUMSEA Tcxsl Source Grams so Pattsrt ACTIVAY(I OCFR30 311) No. d Iaasurtes (Pounds) ~ hhsceve vs!Vie tscttcs Pacaages soeecev ~ l4rwut erato no a stseewceve vsrerut tatters Trtaurn C Ie TC gg I I sg votre lie ne sooecev ~ l4soeecevevsroesc s 4 a l reesceve vswnm Total IVchhscte ~ V Sense h S a ~ setose<<e Vetwul cscrs I 0 asseecev ~ strrehrt no a.. Awsmmm vsrmu toasts (10) (11) nlectcsvo vrreerr mstlllwes mo selects 'cceeceve vswhm tsrts lr MtrpMUMwAETE SOLEXFCATION NUMSER ANO TYPE PACKAGE Ss Fkl AGENT OF CONTAPIERS (13) PHVSCAL (I a) BS) (ISA) (12) WASTE DESCRIPTION FOAM CHEMCAL NAME AND Sc OF WASTE FORM CLASS (la8) )ves ( FOAM CHELATUIOAGENT(S) OAU CI AS 08 OC ( ) No Tht ~ waste(sl must ba dllpostd In south cocoons Department ol Heahh and Ehvuonmehtal control Approved structurv ov alpaca( ~ ) lo meet stsbacy root<<oments. (I g) 'ceoacaocm 4 h<<eby made to Ao sash calosha oattmocs d Heath snd E tlcmmol>>I coned that Ats sh'pmera ol tow revet Ilyl ( I yes I ) No THIS VEHIClE IS CONSK)NED EXCLUSIVE USE. lOADINO AND UNlOADING MUST rcsoaarhvs waste h>> bosn Inspeaod In acoordahco we Ae requirements d Stum Carolmo Asdoaalvt Matenal Uctnse No 0) ~ mended ahd Ihe Nude<<Regulatory Commlsserrys License No. 13 I 33)d 01 ss amended. and Ihe oeecsve 8amwoa seo D roose SE ACCOMPLISHED 8Y CONSIGNOR OR CONSK)NEE OR HIS DESIGNATED AGENT. Ctaona wroth la bouts ptcu lo shpmohL <<ld arrlhor c<<sllcasoh Is made Ihsl At Ihspocooh revealed ho Norns ol hohoompsshct (Is) IMpoRTANT: TNs Is Io colory Ihsl Iha above named mvortvs <<o poporty dasslaecL descrtb<<L pscaagtd. wah as appacab ~ Mws. nasa and rogulasons. m<<socL ahd Mbotocl ahd <<e ln pop<<cohdoorl atl pshsportaoon ccooYcshg lo lht appscaat logcpaaohs ol Ihe Depsrtmsrx ol Transponaeotu Date Stgnstulo DISPOSAL SITE COPY F<<m No. CNS 301 1)ae Snd (hganttattcm (I (10) scl ersrrsrcrrorrs cw revl n\l soe Telephone Nh ( ) toe r si wo mrr Iles roeu - Q Tres mvohv moots as scenes Q Thts mst<<tv wss deposed d sl r~ ~ we scenes. CNSI USE ONLY Forsstt Polsohhd Q Q Anted Date Q (Xsaop<<cy. H P astral Waste CMSS Code Trench No. Date W>>te Crass Code AOAonted Sgnatule Tete Peltohnel Er poscso Page 31 AP-3.7.1 Rev 05 ATTACHMENT 7 B RNNELL MA IFE T (Sheet 2 of 2) BARNWELL WASTE MANAGEMENT FACILITY Operated by: CHEM.NUCLEAR SYSTEMS, INC. CISE TNIS NUM8EA ON STAflgfrrle TAAAKA GENERATOR NAllE CONTINUATION SHEET ALL CONrerUArION PAGES PAGE OF 01 I 0TI 0ll 0TI Oll 0ll 04 fACTCC ACTA\ Cf ~ CTATTT CA ~ CTATTT llCA CTAffCAT TCTAT f141 CTWTAAAA CTWTkAAA Wl CNl 01 CTWTfAKA f4TAT lfATTV ~Of CTWllAl4 Afffl~ Tf Cf TCAIATT CTATT ~ TAATWCC TTCTT CCATffff4 VICl44 CTA TJAAC fCA TT I TMfAACT j MAA ~ ~ AT0 fCT AT PAGE tOEALS DISPOSAL SITE COPY Page 32 AP-3.7.1 Rev 05 C ~ ' ~ ~ ~azz~mrzm RZSESHFa5 ~ M~~~R& ~ ~ ~ 'KIREWKSREI KBSWRWR ~ ~ ATTACHMENT 8 Y MA IFE (Sheet 2 of 2) T¹EC>>ogy No ss srlstoa>>s l5Ecology Nuckar ~ srgc>>e e>>o csoogosg lor gsro gogo: NAN>>EST ~ CI TNI gogo oeocsc>>o OIKCESSEO ws>>o TIENETTATOTT NANE: CONTINUATION SHEET CI lies gogo rso>>sc>>o cxTEOTED woNt AGENT/BROKE TT: llg >>o ososw l>>N Cower IIO >>As>> IITIW Ical NOO¹W la orle>>>> Ossa>>i oeseo Alee Isxso¹ ills Ioe II>> oo aw>> IVI o<>s Cjo n w Ow>> lao>>W l<< 1 I I ~ ll lg Iles>> sewer >> I Sswr Oseol gas l>> Cl sr>>l Ioo lcorgoltg crrcocg lro II>> no gl O Ass Tg loll la nrsc O ON>> 1 >><<stew<< I.awwewe<<awe>>wwe>>see.wwsw ~ ~~ ~ IN I>><< ~ \ S<<e<<>>WW n c<<<<<<<<s<<e<<s le<<e e>> a <<wscec cwh ew<< ee>> n <<<<<<a<<N oe asw w<<al Iew ~ ooo sass<< scow I see<<sew N O<<wa<<WI>>ee <<<<wae u a<<aaaws>>w le<< ~ oao I sewn N e<<T sw wwl awe~el ee la\<< wo To II Cww ~ >> n raw>> swee>> ~ we<<a oee>>wa oea<<w a<<cwa ees>> ae>>ss>> aeoseeo >>owl I ~ a>>ere<< ~ o<<>>a N C<< N swaw N ~~ N ew<< N rwwe n >>e<<<<ee <<we<<wree>>N N awwsw ~ NW<<>>>> ~ COol <Sw>> sl >> Dwr Ivws I ee ~ N W>>S ~ l cee >>ewe>> s>>a' ~ als I <<w 0<<\ Cewww ww W<<o>>we<<<<a'olg w les <<w N le>> ew<<w c<<<< c<<w Csea O. sr<<alla N neo<<w'eel ~ as CONSIGNEE ORIGINAL COPY a<<c<<we<<<<<< I asw<<N<<ewwea sl rrr<< as s>>w lew'olo ~ >> oa ~ \ CWWN SW<> I ~ Cww rw<<>>N ~ Cs<<>>e>> o W n ~ ~ ~ Ca<<e<<a>><< Iee'<<ww Il oew<<>>wee N Oe ~S SWN I s>><<a ~ N ~ N I Oe le sees Craw <<a ~ ee Ose<< IW<<W W I (MUST ACCOMPANY WASTE IN TRANSIT) I os as n w>>wa N n ose>> Os>>>>a N Iae<<w AINling Oo Oslrgsl Al A glsoVIICN Nr¹T oCLIIC>> A wllrlTCNA>>O OSIICO EIIIAIIAIIO>>ATTACI>>O TO Iles NAI>>ill. Page 34 AP-3.7.1 Rev 05 '7' ~ 'l (-, c (