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Rev 5 to Health Physics Procedure HP 10.10, Palisades Radiological Environ Program Sample Collection & Shipment.
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Issue date:	02/11/1997
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Procedure No HP 10.10 Revision 5 Issued Date 2/ 12/97 PALISADES NUCLEAR PLANT HEALTH PHYSICS PROCEPURE TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT

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~-7 Date TPNeal t 2/26/96 Technical Reviewer Date SCSunday I 2/6/96 User Reviewer Date q7osooA0Dgg~ 6§865~ss i*

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PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page i TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT Table of Contents

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1 .0 PURPOSE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

2. 0 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 2.1 SOURCE DOCUMENTS . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 2.2 REFERENCE DOCUMENTS .......................... 1 3.0 PREREQUISITES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

4. 0 PRECAUTIONS AND LIMITATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . 2 5.0 PROCEPURE . . . . . . . . . . . . . . *............................ 3

5. 1 CONTROL AND OVERSIGHT OF SAMPLING FOR THE RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM 3 5.2 REMP AIR SAMPLE COLLECTION ..................... 4

5. 2. 1 Precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 5.2.2 Prerequjsjtes . . . . . . . . . . . . . . . . . *. . . . . . . . . . . 4 5.3

REMP LAKE (DRINKING) WATER SAMPLE COLLECTION-SOUTH HAVEN, MICHIGAN . . . . . . . . . . . . . . 7

5. 3. 1 Preregujsjtes . . . . . . . . . . . . . . . : . . . .. . . . . . . . .

7 5.4. REMP WELL WATER SAMPLE COLLECTION ............ 8 5.4.1 Preregyjsjtes . . . . . . . . . . . . . . . . . . . . . * ....... 8 5.5 REMP MILK SAMPLE COLLECTION . . . . . . . . . . . . . . . . . . . 9

. . -

5. 5. 1 Precaytjons . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

5. 5. 2 Preregyjsjtes . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

5. 6 REMP AQUATIC BIOTA COLLECTION . . . . . . . . . . . . . . . . 10 5.6.1 Precaytjons . . . . . . . . . . . . . . . . . ; . . . . . . . . . 10

5. 6. 2 Preregyjsjtes . . . . . . . . . . . . . . .* . . . . . . . . . . . . 10

PALISAPES NUCLE;AR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page ii

TITLE:. PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT Table of Contents

5. 7 REMP SEDIMENT SAMPLE COLLECTION ..... : ........ 12

5. 7. 1 Prerequisites . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 2 5.8 REMP FOOD PRODUCT SAMPLE COLLECTION ......... 13

5. 9 REMP TLD SAMPLE COLLECTION .............. *... , *. 14

5. 9. 1 Prerequisites .. . . . . . . . . . . . . . . . . . . . . . . . . . . 14

5. 10 MISCELLANEOUS SAMPLES . . . . . . . . . . . . . . . . . . . . . . 1 5

5. 10. 1 Ludington - Control Station . . . . . . . . . . . . . . . . . 1 5

5. 10. 2 Palisades Daily Samples . . . . . . . . . . . . . . . . . . . 15 6.0 ACCEPTANCE CRITERIA ...............................: .. 16 7.0 ATTACHMENTS ANP RECORDS . . . . . . . . . . . . . . . . . . . . . . . . . . 16 7.1 ATTACHMENTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 7.2 RECORDS . . . . . . . . . . . . . . . . . . . . . . , ............. 16

. ATTACHMENTS Attachm~nt 1, "Environmental Sample Collection Schedule" Attachment 2, "Sample Locations" Attachment 3, "Sample Identification" -

Attachment 4, "Sample Packaging and Shipment" Attachment 5, "Palisades Sample Collection Forms and Records"

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5

Page 1 of 16 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT USER ALERT INFORMATION USE PROCEDURE The activities covered by this procedure may be performed from memory.

1.0 PURPOSE To provide methodology for collection of environmental samples in support of the Radiological Environmental Monitoring Program (REM Pl.

2. 0 REFERENCES 2.1 SOURCE DOCUMENTS 2.1 .1 Reg _Guide 4.15(7) 2.1 .2 1OCFR50, Appendix I

2.1.3 Palisades Administrative Procedure 7 .08, "Nuclear Plants Radiological Environmental Monitoring Program" 2.1 .4 REMP Sample Shipping Manual, Teledyne Isotopes Midwest Laboratory 2.1.5 Palisades Health Physics Procedure 10.1, "Radiological Environmental Monitoring Program Surveillance"

2. 2 REFERENCE DOCUMENTS 2.2.1 Palisades ODCM, Appendix A, Sections 111.J, *1v:c, and Tables E-1 and E-2 2.2.2 *Palisades Administrative Procedure 10.46, "Plant Records" 3.0 PREREQUISITES As indicated in procedure .

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 2 of 16

4.0 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT PRECAUTIONS AND LIMITATIONS

~I 4.1 This procedure shall be applicable to Palisades/C&RSD HP, Environmental Department, and any contractual personnel assigned to collect or evaluate REMP .samples.

4.2 Any revisions to this procedure shall be reviewed against Palisades ODCM Specifications to verify compliance to all requirements.

4.3 Deviations from the required sampling schedule shall be documented in the Annual Radiological Environmental Operating Report.

4.4 Every effort shall be made to complete corrective action on malfunctioning sampling equipment prior to the end of the next sampling period.

4.5 If it is not possible to obtain the required samples, suitable alternative

* .4.6 media and locations shall be substituted withi". 30 days.

Samples shall be collected, prepared, and shipped for analysis in a timely

manner to preserve integrity. Other specific handling precautions for sample media are indicated in Section 5.0 as required.

4.*7 Obtain best available replacement sample for any missing sample. Notify e..1 Palisades C&RSD Radiological Environmental contact with description and location of the replacement sample. Some samples are not replaceable

. (TLDs, air samples, etc), however, water, milk, crop samples, etc, should be.

4.8 Document any missing samples or malfunctioning equipment on sample data collection sheets .

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5

TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT Page 3 of 16 5.0 PROCEDURE USER ALERT INFORMATION USE PROCEDURE The activities covered by this procedure may be performed from memory.

5.1 CONTROL AND OVERSIGHT OF SAMPLING FOR THE RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM

5. 1 . 1 Sampling techniques described by this procedure must be strictly adhered.

with .

a.

b.

This includes use of forceps for air sample media change out to ensure the collected media is not disturbed.

Recorded data should be verified including verification of transcribed data to avoid errors.

c.. All deviations from performance requirements, unavailable samples, or other sampling anomalies must be reported to the C&RSD I e:,,

Radiological Environmental Contact.

5.1.2 Failure of sample collectors to comply with sampling and reporting requirements may result in remedial training, disciplinary action, or reassignment of sampling duties.

5.1.3 The C&RSD radiological environmental contact shall conduct periodic (annual) audits of sampling activities.

a. These audits shall include observation of collection techniques, verification of procedural compliance and review of equipment condition.

b. Audits should specifically address air sample collection and should

. include observation of all individuals involved in sample changeout.

c. Audit of collection of. other sample media may be performed at the discretion of the C&RSD environmental contact.

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 4 of 16

TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM d.

SAMPLE COLLECTION AND SHIPMENT Results of the audits and any follow up action should* be documented in the REMP file.

Collect samples using the following methodology in accordance with schedule and location data described in Attachments 1 and 2.

5.2 REMP.AIR SAMPLE COLLECTION

5. 2. 1 Precautions

a. New filters and cartridges should be transported and handled such that potential contami_nation of them is minimized (ie, placed.in clean plastic bags, etc).

b. If an air sampling unit is discovered not operating, attempt to find the cause and repair. If this cannot be done, replace applicable

. component and document o~ air sample collection data sheet.

c. Airflow meters shall be calibrated annually by General Meter. All in service calibrated meters will have affixed a valid calibration sticker/card stating date of calibration and calibration due date.

d. Airflow meters shall be changed out prior to the expiration of calibration dates. Replacement ~ir meters are available from Plant

e. I C&RSD Environmental contact.

e. Air station leakage shall be < 0.1 CFM.

If the replaqement'*of air station components is required due to air leakage, document on air sample collection data sheet.

5.2.2 Preregujsjtes

a. Glass fiber (particulate) air filters

b. Charcoal cartridges for iodine sampling (prelabeled *for each air sampler)

c. Glassine or plastic envelopes (prelabeled for each air sampler)

d.

e.

REMP Air Sample Data Sheet (containing installation data)

Replac~ment air sample meters (as required)

PALISADES NUCLEAR PLANT Proc No HP 10. 10 HEALTH PHYSICS PROCEDURE Revision 5 Page 5 of 16 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT

f. Forceps

g. Stop Watch

h. Step Ladder_

NOTE:_ The Control Stations 10-GR, 11-KZ, and 12-DG are changed out weekly by three independent collectors, and mailed in separately. The prelabeling of cartridges and envelopes, detailed below, is not required for these stations as sample mix-up is not possible. In addition; for these control stations, the Palisades Sample Collection Form and Records (Page 1 of Attachment 5) is completed by the Technician changing out the nine local stations by transferring the recorded data provided by the independent collectors.

5.2.3 Perform the following weekly at each sample location:

a.

b.

Open the protective cover on the air sample station and verify the sampling location number written on the inside of the door is the same as the prelabeled sample change-out package.

Verify that the meter serial number and calibration due date are correctly documented on Palisades Plant Environmental Monitor Operability Check and Sample Collection data form (Page 1 of Attachment 5.)

c. Determine and record the "As Found Flow" rate (seconds for one cubic foot of volume).

d. Determine and record the "As Found Leak" rate by placing hand -

over filter housing inlet to form a seal. While holding hand over the inlet, determine if air leakage is evident by checking the air flow meter needle for movement (leakage). If air leakage is less than

-0.1- CFM, record as < 0.1; If air leakage is greater than or equal to_

0. 1 CFM, record the amount (in a fraction of CFM). If leakage is

> 0.1 CFM determine the cause and repair as soon as possible.

e. Unplug or turn off the air pump and record the "REMOVED 1e MONTH/DAY/YEAR," "REMOVED TIME," and "GAS METER READING REMOVED."

f. Remove the prelabeled charcoal cartridge and place in zip lock bag.

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 6 of 16

TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM g.

SAMPLE COLLECTION AND SHIPMENT Using tweezers, carefully remove particulate filter from the sampler head and place in the prelabeled glassine envelope or plastic envelope.

h. Clean out any residue or moisture buildup in sampler head before replacement filter is installed. Check the condition of the sampler head o-rings. Replace cracked o-rings as necessary to prevent air leakage.

1. . Install new particulate filter and charcoal cartridge and ensure that both are properly centered iri sampler head to prevent air leakage.

Ensure the fiber side of the particulate filter is facing out (smooth side facing inward).

e. I j. Restart air pump. Place hand over the filter housing inlet to form a seal, determine if air leakage is evident by checking air flow meter needle movement. If air leakage is less than 0.1 CFM, record as

. < 0.1 CFM. If air leakage is greater than 0.1 CFM, determine the cause of the leakage (filter not centered in holder properly or cracked o-ring) and correct problem as soon as possible, restoring to less than 0.1 CFM leakage.

k. Determine and record "As Left" flow rate... If greater than ..

90 seconds are required for one cubic foot of volume, the sample pu.mp is degrading. Replace pump as soon as possible to avoid failure to.reach minimum sample volume. (5000 ft 3 ).

I. If an airflow meter must be replaced, record this in the "Comments" column. Record replacement meter data in the read_ing on the upcoming week's sample collection data sheet.

m. Close the protective cover on the air sample station.

n. Calculate and record "SAMPLE VOL (FT3)," ALSO ensure all pertinent data is recorded. *

.. . -

e. I o. Proceed to the next station. Date and sign the current weeks data I . sheet upon completion of the entry of all current data.

p. Transcribe the "REMOVED MONTH/DAY/YR" and "GAS METER READING REMOVED" taken in Step 5.2.3e to the "INSTALLED" reading columns on the sample collection sheet to be used for the upcoming week's air sample collection. Also transcribe the meter serial number and calibration due date to the upcoming week's sample collection sheet.

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5

TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT Page 7 of 16 5.3 REMP LAKE (DRINKING) WATER SAMPLE COLLECTION-SOUTH HAVEN, MICHIGAN

5. 3. 1 Preregujsjtes

a. Four clean one-gallon plastic containers labeled with sample type, location, amount, and date (or collection period)

b. REMP Misce'llaneous Data Sheet (Attachment 3)

I e.

5.3.2 Perform the following sample collection monthly:

a. Leave four containers with the Plant Superintendent at the South Haven Municipal Water Treatment Plant. New water sample containers should be left at the South Haven Water Treatment

.Plant upon pickup of end-of-month composite samples .

b. Instruct the Plant Superintendent to add approximately 300 ml per day of raw water to container labeled "RAW," and approximately 300 ml per day of treated water to container labeled "TREATED,'.'

or "TAP."

c. Return at end of month to collect containers. Obtain verbal verification that Step 5.3.2b was carried out. Note any deviations in "Remarks" column of data sheet.

d. . Label containers with sample type, amount, location, and collection period.

e. Package and ship samples per Attachment 4.

f. Record location, sample types (raw and treated), and amount on sample identification data sheet (Attachment 3). Sign and date data sheet .

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 8 of 16 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT 5.4 REMP WELL WATER SAMPLE COLLECTION 5.4.1 Prerequisites

a. Clean, one-gallon plastic containers el b. REMP Miscellaneous Data Sheet (Attachment 3) 5.4.2 Perform the following sample collection monthly:

NOTE: During the winter months, the State and Township Park wells may be out of service. When this occurs, note the unavailability of the water samples and document on sample data sheet.

a. Turn on water supply (or begin puniping water) and allow water to run for approximately one minute to purge the lines.

b. Fill tw.o clean; one-gallon plastic containers with well water from each sample location.

c. Label containers with sample type, amount, location, and collection date.

d. Pa~kage and ship samples per Attachment 4.

e.I e. Record on data sheet (Attachment 3) location, type, date, amount,_

and under "Remarks" any pertinent information. Sign form in space provided .

PALISADES NUCLEAR PLANT Proc No HP 10. 10 HEALTH PHYSICS PROCEDURE Revision 5

TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT Page 9 of 16

5. 5 REMP MILK SAMPLE COLLECTION

5. 5. 1 Precautions

a. Milk samples shall be sent to the laboratory as soon as possible because of the short half-life of 1-1 31 . Any undue delay may cause ODCM, Appendix A, Table E-3 analytical LLD requir~ments to be violated.

b. Obtain best available replacement sample for any missing milk sample(s). Identify new sample location(s) and notify Palisades C&RSD Radiological Environmental contact as soon as possible. 1~

c. If milk samples are unavailable, then samples of three different kinds of broad leaf vegetation grown nearest to Palisades in each of two different offsite locations of the highest predicted average ground level D/Q (SE or SSE sectors near site), and one sample of each kind of similar broad leaf vegetation grown 1 5-30 km distant from Palisades in the least prevalent wind direction (SSW or S sectors) may be used as replacement samples. The new sample locations shall be identified and the REMP procedures revised within 30 days to reflect sampling changes. Collect approximately one kilogram (2.2 lb) of each sample type.

5.5.2 Preregujsjtes

a. Two clean, plastic one-gallon containers for each sample location

b. Sodium bisulfite preservative (approximately 40 gm per gallon of milk required)

c. Miscellaneous sample data form (Attachment 3) I e...

5.5.3 Perform the following monthly at each specified sample collection_

location:

a. Obtain two one-gallon grab samples of raw milk as specified in Attachments 1 and 2.

b. If problems are encountered in obtaining a sufficient quantity of milk sample, notify the Palisades C&RSD Radiological Environmental contact.

PALISADES NUCLfAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 10 of 16 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT

c. Add approximately 40 gm of sodium bisulfite to each one-gallon container of milk and thoroughly mix. The sodium bisulfite can either be in prepared packets or "scooped" with a volumetric measure from its container.

d. Label containers with sample type, amount, location, date, and time.

e. Package and ship samples as per Attachment 4.

el f. Record on Sample Data Form (Attachment 3), the location, type, date, and amount of samples. Under "Remarks," note any other pertinent information. Sign form in space provided.

5. 6 REMP AQUATIC BIO! A COLLECTION

5. 6. 1 Precaytjoos

a. Collection to be coordinated between Radiological Services Department RMC Section and the Environmental Department. At least one individual in the collection party is required to have MDNR Cultural and Scientific Fish Collectors Permit.

b. If logisti~al problems prevent use of a boat to set gill nets from the lake side of Palisades,* then the nets can be set offshore from the site. boundary (by wading). Notify Security prior to using offshore wading method for beach access.

5.6.2 Preregyjsjtes

a. Boat with required safety equipment, or waders

b. Gill nets (of varying. size mesh) and weights and floats c.* * -Plastic one-liter wide-mouth bottles e- I d. REMP Miscellaneous Data Sheet (Attachment 3)

e. 10% formaldehyde solution

f. Fillet knives

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 11 of 16

TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM g.

SAMPLE COLLECTION AND SHIPMENT Black permanent felt markers for sample identification on containers

h. Notify district MDNR Fisheries biologist prior to sample collection 5.6.3 Collect samples twice during the season of greatest abundance (typically May through October) as follows:

a. Gill nets are placed at the locations specified in Attachment '1 to collect at least two species of commercially and/or recreationally important fish in the vicinity of the Plant discharge area and the same species in an area not influenced by the Plant discharge (Ludington Pump Storage Plant). One liter of flesh should be I e..

collected for each species caught for analysis accuracy. Fish samples from the same area may be combined, if necessary, to make a one-liter composite sample.

b. Filamentous algae samples are not required, but,may be collected from driftwood or shoreline protection structures at vicinity of discharge if available.

c. . Periphyton samples are not required, but may be collected if available. Scrape periphyton from rocks into a pail. When sufficient sample is collected, excess water is gently poured off.

The partially solidified periphyton is then transferred to a liter sample bottle.

d. Crayfish (invertebrates) samples are not typically available at Palisades but shall be collected if available. Collect crayfish by hand picking or spearing.

e. Label all containers with sample type, amount, location, and date.

f. Package and ship samples per Attachment 4.

g. Record on data sheet (Attachment 3) location, type, date, amount, I...

and under "Remarks" indicate any pertinent information. Sign form in space provided .

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 12 of 16

5. 7 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT REMP SEDIMENT SAMPLE COLLECTION

5. 7. 1 Prerequisites

a. One-liter, wide-mouth plastic sample bottles el b. Miscellaneous Data Sheet (Attachment 3) 5.7.2 Collect sediment samples semiannually at collection locations specified in e, I Attachment 1 (includes control sample at the Ludington Pump Storage I Plant). Palisades C&RSD and/or Environmental Department personnel shall collect these sediment samples.

a. Label containers with sample type, amount, location, and date.

b. Package and ship samples per Attachment 4.

e, I c. Record on Sample Data Sheet (Attachment 3) location, type, date, and amount of sample. Note any other pertinent information in the "Remarks" section. Sign form in space provided.

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5

TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT Page 13 of 16

5. 8 REMP FOOD PRODUCT SAMPLE COLLECTION

a. Sample containers

b. Miscellaneous Data Sheet (Attachment 3) 1e 5.8.1 Collect food samples monthly during the harvest season, as per ODCM,.

Appendix A, Table E-1. Blueberries and apples must be collected. Other crop samples can be collected on availability.

a. Sample selection of the following crops if available:

Strawberries Turnips "Grapes Cauliflower Peaches Cabbage - outer leaves only Pears Broccoli Collard greens

b. Collect approximately one kilogram (2.2 lb) of each sample type.

Samples are not to be washed, shaken, or cleaned. Samples should not be collected from a single source, but at random from the entire orchard or field.

c. Label all containers with sample type, amount, location, and date.

d. Package and ship samples per Attachment 4.

e. Record on data sheet (Attachmerit 3) location, type, date, amount, I e, and under "Remarks" note any unusual conditions. Sign form in space provided.

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 14 of 16

- 5. 9 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT REMP TLD SAMPLE COLLECTION

5. 9. 1 Prerequisites

a. TLDs g, I b. TLD Data Sheet (Attachment 5) 5.9.2 Monthly TLDs are to be changed each month; quarterly TLDs during January, April, July, and October; and annual TLDs during January.

5. 9. 3 Monthly, quarterly, and annually at each sample location perform the following:

a. Upon receipt of TLDs fro_m the laboratory contractor, all TLDs shall be inventoried and immediately placed in the lead cave (at offsite sample collector's residence). Note date of receipt and inventory on TLD data sheet.

b. Field TLDs shall only be removed from the lead cave for delivery to their proper locations. All control TLDs remain in the lead cave throughout the entire exposure period.

c. Remove and replace TLDs at each .sample location.

d. For ~my missing TLDs, perform the following:

1. Search immediate area.

2. If lost TLD is found, collect it and perform standard change out procedure.

3. If lost TLD is not found, post the new TLD in proper location.

4. Record in "Remarks" column of data sheet any of the above circumstances.

e. Store collected field TLDs in lead cave along with control TLDs until

ready for mailing to laboratory contractor. Mark Do not x-ray" on

.TLD package.

PALISADl:S NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5

Page 15 of 16 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT

f. Transportation control TLDs are to be stored in a special lead shield provided by laboratory contractor .fil1.fil the field TLDs are posted.

Ensure that designated transportation control TLDs are included with the correct TLD package being mailed to laboratory contractor.

Also ensure that laboratory contractor's TLD data sheet is

completed and enclosed with shipment.

g. Record TLD *c-ollection date and the date that the TLDs are returned to the vendor. Initial/sign the data sheet (Attachment 5). Record I e.

the installation date for the new TLDs on the appropriate data sheet.

h. Package and ship samples per Attachment 4.

5.10 MISCELLANEOUS SAMPLES I I

5.10.1 Ludington - Control Station I I

NOTE: Aquatic Biota and Sediment samples are also collected at Ludington Pump I Storage Plant per Sections 5.6 and 5. 7 of this procedure. I I

a. Ludington Lake In & Well Water composites are collected daily and I shipped to Palisades on a monthly basis. I I

b. Palisades RETS/REMP personnel record appropriate data on the I Sample Identification Form (Attachment 3), and deliver samples to I the local Teledyne sample collector for shipment to Teledyne I

_Midwest Laboratory. I I

5.10.2 Palisades Daily Samples I I

a. Palisades Lake In, Lake Out, Site Well Water, Service Water, and I Turbine Sump effluent sampl.es are collected on a daily basis per I Palisades per Health Physics Procedure HP 6.52, "Palisades I' (Onsite} Radiological Environmental Program Sample Collection." I I

b. Palisades RETS/REMP personnel record appropriate data on the I

Sample Identification Form (Attachment 3), label all samples, and deliver samples to the local Teledyne sample collector for shipment to Teledyne Midwest Laboratory.

I I

I

PALISADES NUCLEAR PLANT Proc No HP 10.10 HEALTH PHYSICS PROCEDURE Revision 5 Page 16 of 16

6. 0 TITLE: PALISADES RADIOLOGICAL ENVIRONMENTAL PROGRAM SAMPLE COLLECTION AND SHIPMENT ACCEPTANCE CRITERIA Proper completion of procedure.

7.0 ATTACHMENTS AND RECORDS 7.1 . ATTACHMENTS 7 .1 .1 Attachment 1, "Environmental Sample Collection Schedule" 7.1.2 Attachment 2, "Sample Locations" 7.1.3 Attachment 3, "Sample Identification" 7.1.4 Attachment 4, "Sample Packaging and Shipment" 7.1.5 Attachment 5, "Palisades Sample Collection Forms and Records"

7.2 7.2.1 RECORDS Distribution of Sample Collection Data Sheet as per Attachment 4.

7.2.2 All Radiological Environmental Monitoring Program Records shall be considered complete when the Annual Radiological Environmental Operating Report is submitted to the NRC. Records shall be retained in accordance with Palisades Administrative Procedure 10.46, "Plant Records."

PAL 950/24*03*1 OLP

Proc No HP 10.10 ENVIRONMENTAL SAMPLE COLLECTION SCHEDULE Attachment 1 Revision 5 Palisades Nuclear Plant Page 1 of 2 Exposure Pathway Number of Samples

Collection and/or Sample and Locations* Sample Type Frequency Airborne: 1 - Onsite Continuous at Weekly 8 - Within a 10 km approximately Particulates Radius 1 cfm (may be 3 - 25 to 89 km Distant less due to dust loading)

Iodines Same as Particulates Same as Weekly particulates Waterborne: 1 - Intake Daily compqsite Monthly 1 - Discharge to obtain a Lake Water 1 - Intake (Ludington two-gallon sample Control)

Drinking ., - S Haven Municipal System - Raw Water 1 - S Haven Municipal System - Treated

Well Water 6 - Plant Site Locations Two-gallon grab Monthly 1 - State Park sample 1 ~ Township park 1 - Ludington Control Sediment 1 - Within 1 52.4 m of One-liter grab Semiannually discharge ( 500 ft) sample 1 - 0.8 km North of discharge 1 - 0.8 km South of discharge 1 - 8.9 km North 1 - Ludington control (2 recommended)

Ingestion: 3 - From 5 to 1 3 km Two-gallon grab Monthly 1* - Control from sample

Milk 15 to 30 km

If samples are unavailable at the specified location, an attempt should be made to sample at an alternate location* (Refer to Step 4. 5).

Proc No HP 10.10 ENVIRONMENTAL SAMPLE COLLECTION SCHEDULE Attachment 1 Revision 5 Palisades Nuclear Plant Page 2 of 2 Exposure Pathway Number of Samples Collection and/or Sample and Locations* Sample Type Frequency NQTE: If milk samples are unavailable, see Step 5.4.1.

.~~ ... ~---: -~.:=*:;..;;,,," *:.. *-.. -~ *'~:: .~:.:;.L_~~.:.~>-;,,:.;:-::* -..

Food Products 1 - Each of two Two-pound gral::> At time of principal fruit crops sample harvest (blueberries and apples).

Fish and 2 - Location in vicinity One-liter fish flesh Twice in Invertebrates of Plant discharge from each season 2 - Ludington control available species, two species required.

Attempt to obtain the same species from the control location.

Direct: l On site Continuous Monthly 16 - Site boundary Quarterly arid TLD 9 - Within 12 km Annually radius 3 - Control stations 1 Control in lead

. cave (C.ontractor's House)

*If samples are unavailable at the specified location, an .attempt should be made to sample at an alternate location (Refer to Step 4.5).

SAMPLE LOCATIONS Proc No HP - 0 Attachment 2 Revision 5 Palisades Nuclear Plant Page 1 of 10

'

Air Air lake Well Station Code .location Particulates Iodine Water Water Milk Crops Sediment TLD Fish

t ST Palisades Nuclear Plant Mounted onsite, 500 ft east of x x x x x x x main gate. 25 ft south of access road next to well.

2 TH RR 3 Along 48th Ave, 500 ft east of x x x x Coloma, Ml 80th St, 25 ft off north side of 5 miles south road.

3 HS 76182 48th Ave Along 48th Ave, 1 /4 mile west x x x Covert, Ml 5 miles south of 76th St. In barnyard 50 yds off north side of road. .

4 JS 36197 M-140 Hwy Along 36th Ave, 1 /2 mile east. x x x x Covert, Ml of M-140 1 5 ft off south side 3-1 /2 miles SE of road.

5 PR 72723 CR 378 Along CR 378, 3/4 mile east of x x x x Covert, Ml M-140, 30 ft off north side of ,,

3-1 /2 miles ESE road.

6 RB RR 3 Along 12th Ave, 1 /4 mile west x x x x South Haven, Ml of M-43, 30 ft off south side of 4-1 /2 miles NE road.

7 SD Sherman Dairy Along Phoenix Rd, directly x x South Haven, Ml behind Sherman Dairy. 1/4 6 miles NNE mile east of 1-196 and Phoenix Rd on porth side.

7a SN35 Emergency Siren 35 On Monroe Blvd. x 4-3/4 mil~s NNE 8 SP State Park Onsite along the dump road, x x x x 1 mile N north of Plant. One.mile from main gate. Near State Park boundary, on side of road as road turns west.

Plant Site Well #2 or #3

SAMPLE LOCATIONS Palisades Nuclear Plant Proc No H Attachment 2 Revision 5 Page 2 of 10 Air Air Lake Well Station Code Location Particulates Iodine Water Water Milk Crops Sediment TLD Fish 9 TP Covert Township Park Along 32nd Ave, 1 /4 mile west x x x x 1-1 /2 miles SSW of Blue Star Hwy. 5 ft off south side of road.

10 GR Grand Rapids, Ml Control TLD and air sample. x x x 55 miles NNE 11 KZ Kalamazoo, Ml Control TLD and air sample. x x x 35 miles SSE 12 DG Dowagiac, Ml Control TLD and air sample. x x x 30 miles SSE 13 ST Perimeter of Palisades Past #8 along dump road. x Proceed west up dune path at right of containment test structure. At first crest, turn north and proceed up adjacent hill .to # 13 at top {approx 50 yds from crest}. Near State Park fence line.

14 ST Perimeter of Palisades Along dump road to point x where fence divides old Blue Star Hwy, 25 yds to east of road.

SAMPLE LOCATIONS Palisades Nuclear Plant

'.Proc No HP

,'Attachment 2.

Revision 5 Page 3 of 10 Air Air Laka Well Station Code Location Particulates Iodine Water Water Milk Crops Sediment TLD Fish 15 ST Perimeter of Palisades North along Blue Star Hwy, x

0. 75 mile.s from access road,

10 h off west side of road.

16 ST Perimeter of Palisades North along Blue Star Hwy, 0.4 x miles from access road, 50 ft off west side of road.

17 ST Perimeter of Palisades Along access road, 25 yds x south of southern power line, 15 yds off east side of road.

18 ST Perimeter of Palisades 20 yds from a*ccess road along x south road. 40 yds off south road.

19 ST Perimeter of Palisades 0.2 miles along south. road x from access road, 30 ft off north side of road.

20 ST Perimeter of Palisades 0.4 miles along south road x from access road, 20 ft off south side of road.

21 ST Perimeter of Palisades 0. 7 miles along south road x from access road. 5 ft off east side of road. Near Lake Michigan Bluff.

22 JS Jerry Sarno Control TLD in lead cave inside x 36197 M-140 Hwy garage at Station 4.

Covert, Ml 3-1 /2 miles SE

SAMPLE LOCATIONS Palisades Nuclear Plant Proc No H-.10 Attachment 2 Revision 5 Page 4 of 10 Air Air lake Well Station Code location Particulates Iodine Water Water Milk Crops Sediment TLD fish 23 SN25 Emergency On CR 380 x Siren 25 3 miles ENE 24 SN22 Emergency On 24th Ave x Siren 22 4-1/2 miles E 25 SH South Haven, Ml South Haven Water Treatment x x 5-1 /2 miles NNE Plant 26 AK Allen Karr x 31110 68th St e Covert, Ml

5. 75 miles ESE 27 KK Kenneth. Kemp x Rt 4, Box 32 South Haven, Ml 8 miles NE 28 DC Danny Carpenter x 64015 M-43 Bangor.-MI 7.25 miles E 29 ws William Shine x 60364 M-43 West Bangor, Ml 10 miles E 30 STN 1 /2 mile N of discharge x 31 STS 1/2 mile S of discharge x 32 LP Ludington Pumped x x x x Storage 33 ST Perimeter of Palisades Onsite along dump road, just x 5 yards east of Air Station BSP

'

SAMPLE LOCATIONS Proc No HP4'10 Attachment 2 Revision 5 Palisades Nuclear Plant Page 5 of 10 Air Air laka Well Station Code location Particulates Iodine Water Water Milk Crops Sediment TLD Fish 34 ST Perimeter of Palisades Along dump road to area where x fence divides old Blue Star Hwy, 26 yards east of road, near Station 14 36 ST Perimeter of Palisades Located on the main post x directly across the storeroom, near Training Building 36 ST Perimeter of Palisades North along Blue Star Hwy, x 0.15 miles from access road, near old RR spur. 50 ft off West side of road 37 ST Perimeter of Palisades North along Blue Star Hwy, x 0.6 miles from access road, 50 Ft off West side of road 38 ST Perimeter of Palisades North along Blue Star Hwy, x 0.9 miles from access road, 50 Ft off West side of road 39 ST Plant Site Wells 111 or x 119 (Warehouse) 40 ST Plant Site Wells 1111, x 12, 13 (Outage Building I 41 ST Plant Site Monitoring x Well /114 42 ST Plant Site Monitoring x Well #15 43 ST Plant Site Monitoring x Well #16

Proc No HP 10.10

- SAMPLE LOCATIONS Palisades Nuclear Plant Attachment 2 Revision 5 Page 6 of 10

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Proc No HP 10.10 Attachment 2

SAMPLE LOCATIONS Palisades Nuclear Plant Revision 5 Page 7 of ~O

NOT SHOWN !Control Locations)

Grand Rapids (55 mi NNE)

Kalamazoo (35 mi SSE)

Dowagiac (30 mi SSE) 22 Control TLD placed in lead cave at Location 4 29 William Shine (WS - 1 0 mi E)

Proc No HP 10.10 Attachment 2 SAMPLE LOCATIONS Revision 5

Palisades Nuclear Plant Page 8 of 10 SAMPLING STATIONS Ludi:i~ton ?umped

. Sto~oge Project N

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Proc No HP 10.10 Attachment 2

REMP SAMPLING NO

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1 SAMPLE LOCATIONS Palisades Nuclear Plant WELL. SIAI!.!S Abandon NA LOCATION Revision 5 Page 9 of 10 YES #2 In Service North side of Support Building. Supports Plant site.

YES (Note 1) #3 Active *Across from East-Radwaste (South Side) backup for well #2.

NO #4 Abandon NA NO #5 Abandon NA NO #6 Active Located - 145 ft west of Blue Star Hwy. Used for training trailers, well capped when not in service and well is outside of Westerly Groundwater Flow to Plant and interim storage facility.

YES #7 In Service Just to the west & between outage building and interim storage facility: Water is nonpotable and used in warehouse restrooms (later to be used for fire system only).

NO #8 Abandon NA YES (Note 21 #9 Active Located at junction of access and warehouse road, domestic water supply for warehouse when it is put in service.

NO #10 Abandon NA YES (Note 3) #11 In Service North of access road and east of construction road,

12 In Service supplies domestic water for outage building, all

13 In Service in one tie-in.

YES #14 Active East of Interim Storage Facility, used for REMP monitoring well.

YES #15 Active Southwest of Interim Storage Facility, used for REMP monitoring well.

YES #16 Active Northwest of Interim Storage Facility, used for REMP monitoring well. '

NOTES: .1. When well #2 is out of service, well #3 is put in service with same sample point as well

2, only one sample required in combination of wells #2 and #3.

2. Sample point will be same as well #7 (in warehouse restroom) when well is put in service.

3. Wells #11, #12, and #13 all have a common line which supplies domestic water to outage building, only one sample required in conjunction with all 3 wells.

Proc No HP 10.10 Attachment 2 SAMPLE LOCATIONS Revision 5 Palisades Nuclear Plant Page 10 of 10 WEST 110' 114

Proc No HP 10.10 Attachment 3 Revision 5 SAMPLE IDENTIFICATION Page 1 of 1 Collector: - - - - - - - -

___________________ PLANT Miscellaneous. Radiological Environmental Samples SAMPLE DATE TIME AMOUNT . REMARKS Location Type r

Proc No HP 10.10 Attachment 4

SAMPLE PACKAGING AND SHIPMENT Revision 5 Page 1 of 1

1. Label samples clearly per Attachment 3.

2. Seal all liquid, biota, fish, and sediment sample containers with tape to prevent leakage.

3. Ship liquid samples separately from air particulate and air iodine samples and TLDs.

4. Use sufficient packing material (ie, crumpled newspaper) to avoid possible sample container damage during shipment.

5. Package air filters in glassine or plastic envelopes.

J3. For TLO shipments, make sure that laboratory contractor's own TLD data sheet is enclosed with package.

7. Ship milk samples as soon as possible. Be sure to add a sufficient amount of sodium bisulfite (40 grams) as preservative to each sample.

8. Ship food products as soon as possible after collection.

9. Ship fish and biota samples with a 10% formaldehyde solution adqed (preservative). Only 10 milliliters is required per sampie. Samples should be shipped as soon as possible after processing.

10. Distribute copies of the Sample Collection Data Sheet{s) to the:

Analytical laboratory Radiological Services Department Environmental Contact (Palisades)

Sample Collector 11 . Send samples to the following address:

Teledyne Brown Engineering Services Midwest Laboratory Att: laboratory Manager 700 Landwehr Road Northbrook, IL 60062

12. Ship all samples to the laboratory contractor with minimal delay after collection so as to avoid elevated analytical levels of detection.

Proc No HP 1 .

Attachment 5 Revision 5 PALISADES SAMPLE COLLECTION FORMS AND RECORDS Page 1 of 2 PALISADES PLANT ENVIRONMENTAL MONITOR OPERABILITY CHECK AND SAMPLE COLLECTION REPLACEMENT METER METER FLOW TEST GAS METER READING SERIAL SERIAL NO AS FOUND AS LEFT NUMBER SAMPLE INSTALLED REMOVED REMOVED INSTALLED REMOVED CAL FLOW LEAK FLOW LEAK CAL DUE CALIB VOL (MO/DA/YR) (MO/DA/YR) TIME (Ft 3) (Ft 3) DUE (SEC/Ft3) (CFM) (SEC/Ft3) (CFM) DATE ACCURACY (Ft 3) COMMENTS DATE ACCEPTABLE lST 2TH 3HS 4JS 5PR 6RB 7SD BSP 9TP lOGR 11KZ 12DG TEST PERFORMED B Y : - - - - - - - - - - - - - - DATE:----

REVIEWED B Y : - - - - - - - - - - - - - - DATE:----

Proc No HP 10.10 Attachment 5

PALISADES SAMPLE COLLECTION FORMS AND RECORDS

. Revision 5 Page 2 of 2 CONSUMERS POWER COMPANY PALISADES ENVIRONMENTAL TLD REPORT 0 MONTHLY n QUARTERLY Collector QANNUAL I

I STATION - LOCATION I INSTALLED I COLLECTED REMARKS DATE TIME DATE TIME I I I I C-1 II C-2 I I I

ST22 ST I

ST5 PR I

STS RB ST24 SN21 ST23 SN25 ST7a SN35 ST16 ST*

ST15 ST ST1 ST ST14 ST STB SP ST13 ST ST17 ST ST18 ST ST19 ST ST20 ST ST21 ST ST9 TP ST12 DG ST3 HS ST2 TH ST4 JS ST10 GR ST11 KZ ST-33 ST ST-34 ST ST-35 ST ST-36 ST ST-37 ST I

ST-38 ST I

I I Data Received From Vendor (With lntranalt Date TLD* Inventoried end Placed In Lead Cave I Data TLDa Returned to Vendor For Analyala TLDa) and lnltlela (With lntranalt TLDa) and lnltlail (With lntranalt TLDa) and lnltilil I

ML18067A515: Difference between revisions

Revision as of 17:34, 21 October 2019

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