ML20053C445
| ML20053C445 | |
| Person / Time | |
|---|---|
| Site: | LaSalle  |
| Issue date: | 03/19/1982 |
| From: | COMMONWEALTH EDISON CO. |
| To: | |
| Shared Package | |
| ML20053C431 | List: |
| References | |
| PROC-820319-04, NUDOCS 8206020151 | |
| Download: ML20053C445 (66) | |
Text
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. I INDEX PAGE y ;
f7 8/17/81 LZP i Wi REV. AEV OATE CISAETT{
PROC. No. TITLE
[
.. t
.u 03
- i.ZP- 1330-24 DETERMINATION OF REACTOR COOLANT 00 to/8l i HYOROGEN C0t* CENTRATION AT THE HIGH (
s RADIATION SAMPLING SYSTEM h
Lu 03 V
LZP 1330-25 SAMPLING OF REACTOR COOLANT AT THE HIGH Qi ,
3/D l m
Pr; RADIATION SAMPLE SYSTEM 'f
$ 01 3/gd 03 f MZP 1330-26 SAMPLING OF CONTAINMENT AIR AT THE HIGH RADIATION SAMPLING SYSTEM 1330-27 SAMPLING OF REACTOR COOLANT OFF-GAS AT Of .3/g;) 03 f' QZP 5 b THE HIGH RADIATION SAMPLE SYSTEM h 01 3/ 85L 03 {
6.ZP 1330-28 SAMPLING OF PROCESS WATERS CONTATNIMt D_AnIn_
i
. 'r ACTIVITY AT THE HIGH RADIATION SA'iPLING SYSTDi 03 1330-29 SAMPLING AT THE HIGH RADIATION CO 0/00 }
~l 2 P &
SAMPLING SYSTEM (VALVE OPERATION AT T THE VALVE CONTROL PANEL)
D bR a /61 03 !
TR Ar.SFER OF W ASTE FROM THE HRSS WASTE 00 LZP 1330-30 >
TANK AND WASTE PUMP f:]
[j?.ZP 1330-31 & 50 See next pace '
IMPLEMENTING PROCEDURE FOR FIRE: Of 9/B/ 02 ;
LZP 1390-1 FIRE MARSHALL 0I 9/6/ 02
%.ZP 1340-2 IMPLEMENTING PROCEDURE FOR FIRE:
FIRE CHIEF (OESIGNATED Sr11FT FOREMAN) ,
F7?
b2P 1340-3 IMPLEMENTING PROCEDURE FOR FIRE: 01 9/6/ 02 [
FIRE OFFICER ::1 (COGNIZANT MAINTENANCE i-m FOREMAN)
% 0t 9/8/ 02
$2P 1340-4 IMPLEMENTING PROCEDURE FOR FIRE:
FIRE BRIGADE t
01 8/81 02 !
.i. Z P 1340-5 IMPLEMENTING PROCEDURE FOR FIRE:
FIRE COMPANY NO. 1 (MAINTENANCE PERSONNEL) h q t.
R 03 7/81 02 i~
" LIP 1360-1 PROTECTIVE MEASURES FOR ON-SITE PERSONNEL r :
% USE OF POTASSIUM IODIDE (KI) AS A 00 7/61 03 t-RZP 1360-2 THYROID BLOCKING AGENT
$ZI' 1360-4 SEE NEXT PAGE RESCUE 00 10/80 02 h
@ZP 1370-1 t 01 11/80 02 g.Z P 1370-2 ' RSONNEL INJURIES ,
FIRST AID, OECONTAMINATION ANC 00 10/80 02 ZP 1370-3 EVACUATION Cc EXPOSED AND/OR t
er CONTAMINATEC CASUALTIES t k**
& on CONTROL OF OIL SPILLS CO 10/80 02 f LZP 1 8206020151 820525
[.
t-PDR ADOCK 05000373 F P_DR p #,
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b LZP-1330-25 [
Revisicn 1 Maren 18, 1982 j[
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SAMPLING OF REACTOR CCOLANT AT THE HIGH RADIATION SAMPLE SYSTEM l p ;-
li i A. PgSj ('
?? p E
d." The purpose of this procedure i s to celineate a metnoo of obtaining liquia samples at the High Raolation Sample f::
g System (HRSS) during normal anc post-accident operations, [
y incluaing grad, diluted (1000:1), and unciluteo (15 mi) samples. g e
s B. REFERENCES [
[}' t
- 1. Sentry Equipment Corporation, Post-Accicent Sample i b
System, volume 1. ,
r LT 93
- 2. LZP 1330-29, "Sampiing at the High Radiation Sampiing ;
I System (Valve Operation at the HRSS Valve Control {i f
,_{ {..
Panel)." (
- 3. LZP 1330-31, "HRSS Sample Movement." .
- 4. AAIS-CCP-0031, "BWR Coolant Radionuciide Analysis." h' b
LCP 410-1, " Preparation of S4mples for Gamma Ray o 5.
Spectroireter Neasurements."
C. PREREQUISITES [
- 1. The Operator should be fami1iar with the cperation of the FRSS panels. t I-
- 2. Verify tnat nitrogen, approximately 100 psig, is
- availaole at the Liquid Sampling Panel (LSP), OPL0dJ.
t.
3 Establish communications eith the Unit Nuclear [
(' Station Operator (NS0). lE 1 f
- 4. Equipmen**
y b-
- a. Clean one liter polyetnylene octtles witn caps. [v.
4 m
O D. Paper towels. l' 4.
- c. Plastic cr ruoner gloves.
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- t LZP-1330-25 I; V
'k" Revisioni March 18, 1982 ij 2 L
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- a. Sample tote tray. ((-
k
- e. Survey instruments, as appropr i ate. 1 e
e
- f. Shielded syringe assembly. -
b-N The sample must have been obtained in accordance I l'n' 5.
k
- with Reference 2 prior to performing this procecure.
h g{T D. PR,ELAUTTOM f.
k,
- 1. A Regulatory Guide 1.3 or 1.4 release of fission i;
- k. proaucts implies extremely high levels of #'
L radioactivity. Oose rates may be high encugh to prevent entry into many areas of the plant tnat are 6 normal 1y habitabie. Rad /Cnem Supervision shoulo De E p contacted prior to entry into any area unen such a f';
b release of fission products is suspected. F.
J
, e wear raciation dosimetry as reccmmenced Dy Rac/ Chem !;
.t 2. K Supervision. '
- 3. wear protective clotning and respiratory protection F.#is as recommended by Rad / Chem Supervision. (f h
E
- n. 4. Appropriate survey i nstr uments shoul d De available h, e for monitoring curing this procecure.
. . s., '.
- 5. The splash box door of the Liquid Sample Panel (LSP), f.
OPLD8J, must be closec during panel 1ine purge and j.
%, g En grao sample collection operations.
h
[
z E. LIMITATIONS AND ACTIONS b i #
- l. Nctify Chemistry Supervision if any proclems are >
encountered at tne HRSS panel s.
'b
- 2. This procedure, though intended for use uncer post-accident conditions, can De usea for sampling at
{c T
T the HRSS panels during normal operaticns, ouring 6 which the precautions may' nave limiteo applications.
However, normal routine sampling precauticns snould ce ooserved. F.
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II LZP-1330-25 Revision 1
{ March 18, 1982 3
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53 For noun names associated with the valves operatec bN in this procecure, refer to Attachment A.
- l. Verify the following valve lineup at the LSP. OPLO8J' .
(('
ut
- a. RC-V-1 1 (closed). {
n?
- o. RC-V-1.2 (closed).
{.} _
- c. RC-V-1.3 (closec).
?.*
(d'n c. RC-V-1 4 (closec).
- 7 e. RC-V-1 5 (closed).
6
- f. RC-DV-1 (BYPASS).
I PI g. RC-V-19 (8YPASS).
- 2. Connect the flusn water nose to RC-C-1 at the LSP, y gp OPLD8Je and open the fl ush water valve. l L
p~b
- 3. To ootain a dilutec (1000:1) reactor coolant sample, proceed to step F.5. To ootain an uncilutea reactor s coolant sample (15 ml), proceed to step F.4. To l obtain a reactor coolant grac sample, proceec in i.
l accordance with the following at tne LSP, OPLO8J or i na as otherwise directed: r gi a. Verify the following valve lineup:
f l
- 1) RC-V-5.1 (closec). .
h(
as g
- 2) RC-V-5.2 (closec). r s.
59
(( 3) RC-V-17 (closed). f._
i
- 4) RC-V-17 (closec). y gy I
3-.
ch 5) RC-V-4 (closec). [.
r pf 6) RC-V-ll (closec). [h i
Ch !
- 7) RC-V-9 (closec). i' i
- 19. ,
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' " LZP-1330-25
. t.
Revision 1 Marcn 18. 1982 4
- C# ,
i
- 8) RC-V-8.2 (closeo).
ca
- 9) RC-V-8.1 (closed). a
- 6/ ;
- 10) RC-V-16 (closed).
p.
~ h.. 11) RC-V-18 (6 o' clock).
- 12) RC-V-22 (TO WASTE). r
, 7, .
00tain the sample in accordance with the b LL b.
following: ,
j', .. t s 1) Open RC-V-3.
- 2) Open RC-V-2.
- f U 3) Select one of the sample sources ano open its' corresponding valve, RC-V-1.1 (-1 2, ,
+
b -1 3, -1.4, -1.5).
,E , t Lu
- 4) Slowl y open RC-VREL-1 until RC-FI-l reaos ;
35-40 inches of water. Allow tc purge
- m. - -
b for a minimum of five (5) minutes. >
b L2:
- 5) Sl owl y close RC-VREL-1 until RC-FI-1 reacs 5 12-15 inches of water. Continue tne purge b
((
for a minimum of one (1) minute. !
bd I.
pp 6) Cl ose RC-V-3. {,
?> !
- 7) Open RC-V-7.
- 5. 8) Slowly open RC-VREL-2 until RC-FI-2 reaos ,
W 18-22 inches of water. Allow tc purge f-l for three (3) minutes. l-1 l !%
l
(( 9) Align RC-V-16 to the 3 o' clock position. [l
- 10) Open RC-V-17, acjust RC-VREL-2 until RC- ;
fr A FI-2 reacs 18-22 incnes of water or RC-G- 1 f
~ minutes. ;
'!_ 11) .Close RC-V-17 anc place a sample Dottle under the sample tap.
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r0 LZP-1330-25 4 Revision .I g;3 March 18, 1982 ;
5 :
ty F Ootain sufficient sample 5
- 12) Open RC-V-17.
to rinse the sample cottle.
b f
d, 13) Close RC-V-17 and empty the sample bottle {
into the tray.
II r-r: I
((:?. 14) Replace the sample bottle under the sample
'" tap and open RC-V-17. h L
Fill the sample cottle to overflow and i$
I 15) U I.id screw the cap on 1oosely.
W:
1 m 16) Gentl y squeeze tne bottle to ef fect U E
b over fl ow, then immeciately tighten tne D.
cap.
p
, (2:' NOH -
,:u The physical shape of the polyethylene bottle should .k
,{ be somewhat distorted after step F.3.b.16). {
b.
C:s p
- 17) Close RC-V-17. ;.
M:
- 18) Wipe tne bottie ory with paper towels.
{ Label the bottie witn the fclIowing [
19) information: L:
Ef b$ "
- a. Sample point. -
ry. Cate sampiea.
<- b.
ii+.i
- c. Time sampled. g,
,q/
rig o. Initials of person sampling. >
nn $3 ;
M' Tnis labeling may De cone prior to taking the sample. [.
?:
- 20) Tag the sample cottle with tne appropriate
[~ sticker i f the sample contains racionucl ioes. {(
(;
fr $3 1
This tagging may De cone prior to taking tne sample.
- 21) Place the cottle in the tote tray for NY bL transport to tne chemica) 1accratory.
l-r !
- - J.
L4 :
9
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,f 7m LZP-1330-25 te; GU Revision 1 [
Marcn 16, 1982 f:
6
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- c. Flush ano secure the system in accordance witn (
tne f ollowing: g y i.
p*l
- 1) At the Valve Control Panel, OPLC9J, secure [ '
the sampling lineup in accordance with Reference 2, steps F.1.d.6) througn
[10 f' .c l.d.7).
- 2) Close the sample valve, RC-V-1.1 (-1.2. [..
p7 -1.3, -1.4, -1.5). p gg ..
L Open RC-V-4 ;'
3) n i-MJ 4) Open RC-V-17, adjust RC-VREL-2 until RC- [
FI-2 reads 18-22 inches of water. Flush [
T+ with demineralized water for a n.inimum of three (3) minutes. f i
E
- 5) Close RC-V--17. -
l
(( Al i gn RC-V-18 to the 6 o' clock position, Lc 6) adjust RC-VREL-2 until RC-FI-2 reads lo- [
"T 22 inches of water. Flush with cemineralizea [
hkl water for a minimum of three (3) minutes. {y.
, 7) Close RC-V-7. f'
.i i
- 8) Open RC-V-3. ,
y 9) Adjust RC-VREL-1 until RC-FI-l reacs 35- fL 40 inches of water. Flush with demineralizec e
V water for a minimum of one (1) minute. I I
l -
- 10) Cl ose RC-V-3.
Open tne sample valve, RC-y-l.1 (-1.2, - [
- 11) ;
1 3, -1.4, -1 5), flush with cerineralizea
-g [
4 water for five (5) minutes.
I i
Close the sample valve, RC-9-1.1 (-1.2, f m
12)
-1 3, -1.4, -1.5).
CJ I
- 13) Close RC-V-4. y C 1*) Close RC-VREL-1 and RC-VREL-2.
L.
I
- 15) Close the flusn water valve and disconnect ;
the flusn water nose f rom RC-CV-1. i
[S'W:
I
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- LZP-1330-25 L Ni Revision I h
'Ul March 18, 1982 6 7 k:
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gg 16) Secure tne system in accordance with h Reference 2, steps F.1.d.8) through F.1.f.
{-
- 4. To oDtain an undiluted (15 ml) reactor coclant fa.I sample, proceed in accordance .#ith the following at f.'
g' the LSP, CPLD8J or as otherwise directeo: r Et-F');
g a. Verify the following valve lineup: 5
- 1) RC-V-5.1 (closed). A:
N.;. W G
- 2) RC-V-5.2 (closed).
[v De 3) RC-V-17 (closec). h g y
- 4) RC-V-4 (closed). {
e
'I w${..
u
- 5) RC-V-7 (closed). D.
(
1:
- 6) RC-V-ll (closed). [
y g- p 4 7) RC-V-9 (closeo). E i-ps 8) RC-V-11 (closed). k W V
- 9) RC-V-8.1 (closed). h
- 10) RC-V-16 (c)osed).
'r.
- 11) RC-V-18 (6 o' clock). ['
Ks
- 12) RC-V-22 (TO nASTE). r.
D. Prepare tne sample Dottle in accercance witn tne following:
- 1) Place the cottle on the cart / cask assembly cavity piston.
- 2) Turn the di rection val ve for the hydraulic ofston in the DOWN position and 1ower the h Octtle into tne cask cavity. fr'
- 3) Close and open the cask tc verify that -
E, the cover is working prcper1y. [
ric "
- 4) Turn en the L5P undiluteo reactor coolant
$* sample fill station lignts.
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.. - + *
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b LZP-1330-25' h.
Revision 1 F Maren 18, 1982 b 8 O C; l k 4 5) Pcsition the casx/ cart under the LSP ff f undiluteo reactor ccolant sample fill )f
~
station needles and set tne brake. tf f
Turn tne direction valve for the hydraulic h
- 6) I piston in the UP positicn and raise the e-
~
bottle onto the needles. :
h e
Obtain the sample in acccraance with the y
- c. b following: e C
- t. .
(b
- 1) Open RC-V-3. k
~~
y
' T:'
Open RC-V-2. J jc< 2)
- 3) Select one of the sample sources anc open [
- r. ,
its' corresponding valve. RC-V-1.1 (-1.2, [..
p -1.3, -1.4, -1.5). :~
h-r' ~ 4) Slowly open RC-VREL-1 ur.til RC-FI-l reads ;,
35-40 inches of water. Allcw tc purge [
b:.__ for a minimum of five (5) minutes. P h
,,.7
- 5) Slowly close RC-VREL-1'until RC-FI-l reacs p; 12-15 inches of water. Continue tne purge i:
for.a minimum of cne (1) sinute. "ff;
~
ff n~ 6) Close RC-V-3. g
$k rA y 7) Open RC-V-7. 3:
- n 5
- 8) Slowl y open RC-VREL-2 until RC-FI-2 reads 18-22 inches of water. AllCw tC purge for three (3) minutes. 4{
p g //-
r .-
- 9) Turn RC-V-19 to SAMPLE. V
[ -.
- 10) Adjust RC-VREL-2 until RC-FI-2 reads id- k l h~. 22 incnes of water or RC-G-3 reads 20 )
PSIG. DO NOT exceed 20 PSIG cn RC-G-3.
! f. ' '.
Allow to purge for two (2) minutes. (
E l
- 11) Cl ose RC-V-7. Let RC-G-3 return to O PSIG If tnen wait 30 seconds to allow the sample i
,y
' Octtle to cepressurize. 2 Y
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LZP-1330-25 rr Revision 1 7 I Maren 18, 1982 7' 9 .
B
{', 12) Turn RC-V-19 to BYPASS.
. D
- 13) Turn the direction valve for the cart / cask g'- hydraul ic plunger to the 00hN pcs i tion.
Lower the sample cottle intc the cask and close tne cask. [ -
> r
' L, 14) At tne Valve Control Panel, OPLC9J, secure 6" the sampl i ng l ineup in accordance with y Reference 2. steps F.1.d.6) thrcugn
{
[",
F.1.d.7). ,
i:> f
- d. Flush and secure the system in accorcance with [
tne following:
73
,u
- 1) Close the sampl e val ve, RC-y-1 1 (-1 2, ,
-1.3, -1.4, -1.5). j
- c. '.r, t 2) Open RC-V-7.
- 3) Open RC-V-4.
, pl _
'+" - *
- 4) Adjust RC-VREL-2 until RC-FI-2 reads 18- '
22 inches of water. Flush with demineralized E" water for a minimum of three (3) minutes. E i L
- 5) Close RC-V-7. b
+
p$g Open RC-V-3. I:
[h 6)
I:.
- 7) Adjust RC-VREL-1 until RC-FI-l reads 35- 0 40 inches of water. Flush with demineralized k E7 b1 water for a minimum of one (1) minute. h L
er 8) Close RC-V-3. l W: h*
- 9) Open the sample valve, RC-V-1.1 (-1.2, - t 1.3, -1.4, . 5), and flusn fcr a minimum }
c' (c .
of five (5) minutes. [
t
- 10) Close the sample valve, RC-V-1.1 (-1.2, [
-1.3, -1.4, -1.5).
Pd i(-
i.
- 11) Release the Drake anc remcVe tne cart / cask .-
from tne sample station. [.
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1.
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LIP-1330-25
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- k. Revision 1 March 18, 1962 '
10 y p- k
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k' Install and secure tne auxiliary sni el a. fj 12) t Install and secure tne needle flush tool . r 13)
"b~? f[
- 14) Open RC-V-8 1.
l'l
- 15) Open RC-y-8.2. #
[9?<2 ,
r <
- 16) Adjust RC-VREL-2 until RC-FI-2 reaas 18 t.
7 22 inches of water. Flush with demineralizeo !
y{u<.y f.
a water for one (1) minute. ;
P3 17) Turn RC-V-19 to SAMPLE. :
(i '
~
- 18) Adjust RC-VREL-2 until RC-FI-2 reads 18- ,
22 inches of water or RC-G-3 reads 20 I hs.:. PSIG. DO NOT exceed 20 PSIG on RC-G-3. '
" Allow to flush with demineralizea water for two (2) m i nu te s. f, o em ,
h, 19) Close RC-V-2.
t
- n 20) Allow RC-G-3 return to O PSIG then wait
{;: 30 seconds to allow the bottle to _
depressurize.
Turn RC-V-19 to BYPASS. j
}$ 21) c; f
- 22) Close RC-V-8.2.
[
h hy 23) Close RC-V-8.1.
y 9;
- 24) Close RC-V-4. r 53 25) Remove the needl e flush tool . }<
Turn off tne LSP unoiluted reatcr coolant rc 26)
([ sample fill station lights.
- 27) Close the flush water valvo and disconnect , 7' F
the flush water nose from RC-CV-1. '
[
I 28) Secure the system in accordance with t; Reference 2, steps F.1.d.8) thrcugn F.1.f. !
{J '
I
- 5. To ootain a diluted (1000:1) reactor cociant sampl e, - ;
r proceed in accordance with the following at tne LSP, !
' k--
OPLOSJ or as otnermise directed: /
c e-t i I #
- w. e, I . - . , e..
- -. 7,._ e . -
- . - . . . . .. w . a. ~ .. ......=:.-..u.s....-~..~ .
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LZP-1330-25 {t <
m Revision .1 i
'E '
Marcn 18, 1982 t-gg lx,
. F
- a. Fill reservoir RC-R-1 with demineralized water. t
,' ic:.[s ,-
t o. Open RC-V-20 then cpen RC-V-21. Adjust reservcir
-g RC-R-1 until the water level in graduatec b_
d ',
i cylinder RC-C-1 1s:125 ml. !
g.
- c. Close RC-V-21. [y
{7 "
f
- d. Close RC-V-20.
4
[
e.
- e. Verify the following valwe 1ineup:
{.'
- 1) RL-V-5 1 (closed). ?
re k I."
w 2) RC-V-5.2 (closed). '
I
};
m, 3) RC-V-17 (cicsed).
it Le 4) RC-V-4 (closed). [
- 5) RC-V-2 (closed). [
>p ..
Ee I
- 6) RC-V-7 (closed). f.
- k. 7)* RC-V-11 (closed).
L
- 8) RC-V-9 (closed).
C g 9) RC-V-16 (closed).
a
- 10) RC-V-18 (6 o' clock). "
i E.d s
, 11) RC-V-19 (BYPASS).
s:
l oi 12) RC-V-22 (TO WASTE).
- W- ,
- f. Prepare the sample Dottle,in accordance with the foilowing:
7 ZT
- 1) Insert the needl e of the hand operated vacuum pump in c the septum of the dilutea .
5 reactcr coolant sample cottle. Evacuate
[i, s to the maximum vacuum achievable witn the j
- a hanc operated pump. . Tne vacuum MUST oe t at LEAST 15 incnes of Hg. ;
t.
', 2) Keep the hana operated vacuum pump connected I
,. to ne evacuatec oottle for three (3) }-
g i A {
C# I.
D.,
'a d -
L - .- - ..
..s. . ~- .. _ . _ _ -
7 . , _ _ _ . _ _ _
i 1
w .
,w A W^ LZP-1330-25 ;
- .g.
Revision 1 '
Parcn 18, 1982 I IF j N-minutes to assure that tne bottle retains ,
the vacuum. 7 f.
TP Remove the cottle from tne hand operatec i.
[i 3) !
vacuum pump and place the octtle on tne cart / cask assemD1y Cavity piston. f "U 4) Turn tne cirection valve for tne nyaraulic piston to the DOWN position and lower the [-
Dottle into the cask cavity. [
fl m?
I-
- 5) Close and open tne cask tc verify that [
the cover is working properly. t
- .- V
- 6) Turn on the LSP diluted reacter coolant I sample fill station lights. [
rr ..
pv Position the cask / cart unoer the LSP l uh 7) olluted reactor coolant sample fill station j
, 3; neeole and set the Drake.
w
"^ Turn the direction vaise for the hyoraulic 8) piston to the VP position and raise the f octtle onto the neeole. {
- g. Sample in accordance with the following: I L
I 1) Open RC-V-8 1.
- 2) Open RC-V-8.2.
@ Open RC-V-3.
3)
- 4) Select orse of the sample sources ano open
{p gi its' correcponcing valve, RC-V-1.1 (-1.2, . _ _ ,
-1.3, -1 4, -1.5).
ll
- 5) Slowly open RC-VREL-1 until RC-F1-1 reaos 35-40 inches of water. Purge for a minimum of five (5) m i nute s.
$b 6) Slowly close RC-vREL-1 until RC-FI-1 reads j 12-15 incnes of water. Ccntinue the purge [
l .
7 for a minimum of cne (1) minute. j-
- 7) Cl ose RC-V-3. ,
V IL v-: *!
4 wu
- m. _ _ _
. .. .. . .. - .. .m..
.. m w: 'e,-
'^
c,'
W
. k I
t i
LZP-1330-25 }
- r. ' Revision 1 :
I" March 18, 1982 !
'^
13 :
,- 4
- 8) Open RC-V-2. [
u (
- 9) Slowly open RC-vREL-2 until RC-FI-2 reacs [
p' 18-22 inches of water. Purge for three -
[; (3) minutes. !
s ,-. 10) Close RC-V-8.1. I 6
I 11) Turn RC-DV-1 to SAMPLE.
- 12) Close the sample source i sol aticn valve. :
{'"
ti .
- 13) At the Valve Control Panel, OPLC9J, secure the sampling lineup in accordance witn ;
p[y- Reference 2, steps F.1.c.6) througn F
~~
F.1.d.7).
f5 14) Close the sample valve, RC-V-1 1 (-1 2, i LL -1.3, -1.4, -1.5).
, g, r, n. F*,ush and secure the system in acccraance with l Q
the following: j
- 1) Open RC-V-7.
77
- 2) Open RC-V-4.
.- 3) Adjust RC-VREL-2 until RC-FI-2 reacs 18-
{3 b 22 inches of water. Flush with cemineralizeu ,
water for a minioum of three (3) minutes.
[&
- 4) Close RC-V-7.
I
- 5) Open RC-V-3. p T* [
13 6) Adjust RC-VREL-1 until RC-FI-1 reads 35- [
40 inches of water. Flush with demineralized i-gp water for a minimum of cne (1) minute. 5
'h$
- 7) Close RC-V-3. [
t EY 8) Open RC-V-21 [
bl 7
- 9) Crack open RC-y-21, and aca 24 el of water j
., y from RC-C-1 to tne sample octtle, then j gg close RC-V-21.
re i L; t
--~ -
. . . . . . . .-... - -,s-. .- . . , .
r,' '
e.
?- t1 i
- LZi'-1330-25 I I
I Revision 1 Marcn 18, 1982 14 !
(
$5 l
,~ The ollution volume may oe changea as assired oy l ~
it Rao/ Chem Supervision.
u.
- , 10) Turn RC-DV-1 to BYPASS. .
V4 11) Open RC-V-8.1. l p- 12) Adjust RC-VREL-2 until RC-FI-2 reads 18- ;
A 22 inches of water. Flush witn demineralizea water for one (1) minute.
Eb 13) Close RC-V-2. ;
L: '
- 14) Open the sample valve, RC-V-1.1 (-1 2, -
F 1.3, -1.4, -1.5) anc flush with aemineralized
(; water f or a mi ni mum of five (5) minutes.
-. 15) Close the sample valve, RC-V-1 1 (-1.2, ,
' E' -1.3, -1.4, -1.5).
L i
- 16) Close RC-V-8.2.
f',
> (j 17) Close RC-V-8.1.
4 l ILq 18) Close RC-V-4 {
- i. Remove the sample and casx/ cart assencly and f secure the system in accorcance with the ,
l r:5 following: t t $;- i l i) Place the direction valve for the nyaraulic f 7, plunger in tne 00hN position.
L.1' 2) Lower the Dottle into the cask. l i
l [,[ 3) Close the cask. !
l- $.
- 4) Release tne Drake and remcVe the cart / Cask )
,.r from the sample station. [
i * ' 1 Install and secure tne auxiliary snielo. !
5) l 6) Turn off the LSP dilutec reactor coolant
[h k sample fill station lights. -;
r
? 7) Close tne fluin mater valve and disconnect 8 l J, tne riusn water nose frc RC-cv-1. -
i b
t
[;
p'
- Y LZP-1330-25 ,
I Revision 1 Marcn 18, 1982 1 15
- 8) Secure the system in accordance with ,
Reference 2, steps F.1.d.8) througn F.1.f. V IS 6. Transport the samples to the sample preparation area
- k in accordance with Reference 3.
- 7. Prepare the sample frem Step F.4. or F.5. for anal ysis i 7'
- k. in accordance witn the following:
h.
' ?
- a. Place a 47 mm fiber filter in a new petri oisn fc, and place behino a shielced are= witn the cover '
- off.
.' $U '
tu-If less than 500 ul (0.5 ml) of sample is usea, p- campen the fiber filter with celonizea water prior CN to placing the sample on the fil ter. ,
L2 4, D. Recove the small shield. plug from the top of p [i- the shielo cask. .
L '
- c. Using the syringe assemoly, witncraw 20 ul of the sample and immediately replace the shielo ,
plug.
((? ;
- n. . $U !
d Sample volume and geometry may be changed at the t discretion of Rad / Chem Supervision to f acili tate f
, 5". anal ysis of samples.
f' 1-L Discharge tne sample ontc the fiber filter in
- d. '
p.
the petri cish in sucn a manner tnat the sample qi is evenly aepositeo over the entire ficer fil ter
surface.
- e. Place the cover on the petri aish anc tape it i
^['
closed.
I m f. wrap the petri dish in plastic wrap ano seal it.
33
- g. Label the sample in accorcance with tne following:
ar 1) System sampled and sample location.
(a .
NE.
r k.
[
. F
. I'
- ?.
?
G LZP-1330-25 Revision 1 [';
Marcn 18, 1982 16 r- ,
- 2) Time of sampling.
- r. 3) Date of sampiing.
- 4) Sample volure, refer to Step F.8.
E' 5) Initials. i
- 6) Survey results. <
W "
y.
' ^ ~
- 8. The sample volume for undiluted samples is the same as the syringa volume oiscnarged. For a o8 luteo !-
sample, calculate the actual volure of sample on ,
p the floer filter in accordance with the following:
%. m V = b2 # ,
- r. , y b,k l-where: V = The actual volume of rcactor water f
_. to De analyzec on the filter paper in ml.
{ l.
S = The volume of the diluted sample in
$' the syringe in rl. t L:
A = The valve aliquot of sample collected
- g. in the cask Dottle in ml. ,
'# T = The total volume in the cask oottle, .
the valve aliquot of the sarple plus [
the water added from the graduated cylinder p g in ml. -
g- 9. Anal yze the samples in accordance with Reference 4
- Q Report the sample results to the Rao/ Chem Director t
10.
for evaluation.
-n n s.
f{$
- d. 11. Route al1 output oata and calcuiatians to Rad / Chem -
Supervision for review. l p 1.
E G- Ctf21.1111 l
, 1. None.
L L H. TECHNICAL SPECIFIQ TION REFERQ g l ;
m-c' i 4.- f i* k
~
,. _ . ...r. _ .-
wM
(
. e v
' t:
. s.
2 5
LZP-1330-25 Revision 1 i March 18, 1982 17
- 1. None.
k t
- 1. . -
i.
i 5
e.p.+
i .
ki .
rw
~
s IO 5
8 5
F3' I
-3 i.
L, 1: .
=
?
- F
,, v
- d. F' p.
a i
% S JE, .
id
- L,,"
T F
ue t
X-5.
G I
s, M6 E,
e
.k .' .
+:+
f Li
I e
-. . a. . = = ~ ;- =. r- .-- - - = -. = : -- - - :
- _ ;= . .- _
=::= - := : = = - .:
LZP 1330-25 RevIsl'on 1 L March 18, 1982 [
i8 1 ATTACHMENT A VALVE LISTING RC-V-1.1 Reactor Recire. Loop B Sample Cutout Valve l Y
+
I. .. RC-V-1.2 RT Domin. Inlet Sample Cutout Valve c-- RC-V-1.3 RHR Loop A Sample Cutout Valve l t
^'
RC-V-1.4 RHR Loop B Sample Cutout Valve :
l RT Demin. Outlet Sample Cutout Valve :
I' RC-V-1.5 '
c.
RC-V-2 Sample Source isolation Valve :
re Sample Purge Cutout Valve RC-V-3
{
- RC-V-4 81ushing Vater Isolation Valve P'
p.
- 6. RC-V-5.1 Pressurized Sample inlet isolation Valve Pressurized Sample Outlet isolation Valve ;
,g, RC 'i 5.2 i: . L RC-V-7 Diluted Sample Bypass Valve \
7 RC-V-8.1 RC-SF-1.2 inlet Isolation Valve [
iC. '
RC-V-8.2 RC-SF-1.2 Outlet isolation Valve e
2 RC-V-9 RC-EV-1 Isolation Valve [
w RC-V-10 RC-EV-1 Evacuation Cutout Valve [6 M' I' LV. RC-V-11 Off-gas 4-way Valve Argon to Air Ejector Cutout Valve
,j RC-V-12 '
.x i Off gas Vial Evacuation Cutout Valve RC-V-13 i
RC-V-14 Argon Supply to Off-gas Vial Cutout Valve RC-V-15 Off gas Sample to Gas Chromatograph Isolation Valve ]
t' RC-V-16 RC-SF-1.2 Argon Purge Cutout Valve RC-V-17 Reactor Ccolant Grab Sample Cutout Valve
,w
[3 7 .,
-w
r f
y
' L _*_ _ .
t 6
LIP 1330-25 i
~
Revision :) ;
e.
~- March 18,- 1982 ,
f.
19 (Final)
ATTACHMENT A l
[
(Continued) e :
t:
- k. .
Reactor Coolant Undiluted Sample Backflush Cutout Valve b RC-V-18 d
?l' Reactor Coolant Undiluted Sample injection Valve [
f~ RC-V- 19 t
RC-V-20 RC-C-1 Fill Valve -
r-y:
E-- RC-V-21 RC-C-1 Isolation Valve b
'a RC-V-22 Liquid Sample to CAP lsolation Valve .
f RC-DV-1 Reactor Coolant Olluted Sample injection Valve
.. w Of f gas Sample injection Valve 1J RC-DV-2 Cv RC-VREL-1 Reactor Coolant Purge Throttle Valve '.
y <
g RC-VREL-2 Reactor Coolant Sample Throttle Valve p TTc: ?
c sr._.
?
I*
1 C4
.S m
>8._
O-CJ' t ,
CL 9 4
i
,3c =
1 p :
EL V 4 l
t- ,
i e 6
' ~ ' ' -~ ' *~~: :# * *~ :
a .. .
f1
- e. % 1 E
r LZP-1330-26 -
Revision 1 March 18, 1982 1 1
- SAMPLING CF CONTAINMEhT AIR AT THE HIGH p RADIATION SAMPLING SYSTEM w..
A. f,U,3P_91) c' O ,
U The purpose of this procedure i s to delineate a metnod {
of obtaining a containment air sample at the High Radiation y F Sampling System (HRSS) suppl ement i ng the containment [
[;
monitors during normal and post-accident concitions.
e YJ B. REEERENCES l
L1
- 1. Sentry Equipment Corporation, Post-Accicent Sample I System, Volume 1. -
{7" ..
- 2. LZP 1330-29, " Sampling at the High Radiation Sampling -
c ..
System (Valve Operation at tne HRSS Valve Control g Panel)." ;
a- t.
i
- 3. LZP 1330-31, "HRSS Sampl e Movement."
IE*
AAIS-CCP-0002, " General Radionuclide Analysis of a !
Li 4.
Gas Sample." [
p h, 5. AAIS-CCP-00C3, " Particulate Radionuclide Analysis."
t-!
- 6. AAIS-CCP-0004, " Iodine Radionuclide Analysis." I
! . 52 h
N
! $N 7. Action Item Record (AIR), 1-81-494.
- 8. Hewlett Packard Program Instructions, "I-131 Equivalent [
! gy l
gg. Concentration." {
- 9. GSEP Environmental Director Energency Plan Implementing Procedure EC-16, " Quick Estimate of Offsite Dose
)_k Wu From Unplannec Release: Liquid and Gaseous." .
- 10. Calculatiogj of Distance FdStprj for Powgg ggo Tgs3 '
((d L
Reactor Siter, Chemical Infcrmation Document, Division of Licensing anc Regulations, Washington, D.C., 23 TIC 14844, Taole III.
! rr March 62.
h0" C. PRgREQUISITES
- 1. Verify tnat nitrogen pressure, apprcximately 100
{I w; psig, is available at the Containment Air Control '
l Panel (CCP), OPLE2J.
- u. .
6
. o .
[.
(
l s
b.
r p.
LIP-1330-26 h Revision 1 March 16, 1982 i 2
- 2. Verify that the CCP printer power is GN and the ; ,
printer is set to the proper date and time.
i 9
6
- 3. Set the CCP FUNCTION SELECT to tne SF1-SF3/GGD
- position and cbserve the following at the CCP, CPLE2J: p L.'
- a. The POWER CN 1ight turns on.
- . Annunciator Windcws glow steady in:
' t. : o.
"; ROh COL ,'
+
1 2 -
r.
- 1. , 1 3
" 2 2
]
The flow monitor 20% and 100% ficw 1ights turn ;'
C c.
b on for approximatel y 25 seconds af ter poner is ;
first applieo.
-. \
$5 L
There is no flow at this time. '
~. ,
, di C. The 20 minute Gross Gamma Detector (GGD) timer g; b.
is energized. f-t*,
M [-
I Pt M
There is no GGD incluced in this system, nowever,
, M the steps were incluced to ciarify tne tir.er l b; sequencing. _
gm 4. Press the annunciator RESET pushoutton to turn off lg all lighted annunciator wincows.
' 5 Verify tne timers on the CCP. OPLE2J, are set as ;
fh follows: ,
,u l
t
- a. Pre-sample Dack flush - two minutes. ,
l tin lg( D. Sample capture / residual gas removal -
tnree ,
s minutes. r l a w
I l
(
l s .;
l l . , . . . . . _ - .. . . , . - , _ . _ . -
- - , - .n - -. - - ,
t e
g r
LZP-1330-26 Revision 1 Marcn 18, 1982 e 3 m
- c. Sample flask line flush - tnree mir.utes.
i' d. Equilibrate flask pressure and post sample oack -
flush - fifteen seconds.
I e. Time between SF1 and SF2 - twenty minutes. {
!! L
- f. Time between GGO exercises - twenty minutes. l 7'
(( g. Time between SF2 and SF3 - 120 minutes. E r 6. Verify all air and solenoid valve selector switenes [
!E on the CCP, OPLE2J, are positionec to AUTO. [
Lk z
- 7. Press the PILOT LIGHT TEST pushbutton on tne CCP, I" OPLE2J, and observe all pilot lights are functiona.l.
- 8. Press the annunciator TEST outton on the CCP', OPLE2J, and verify the following:
, 7r
" a. Horn sounds.
- b. Annunciator winoows flash on and off in: '.
n.
ROW COL 1 1 i
~
1 2 {
1 3
- c. Annunciator windcw in ROW 2, COL 1 lights up ;
p:3 and remains l ighted. '
ki Annunciator windcw in R0h 2, COL 3 is off.
d.
Tnis position has no operator functicn. i i 9. Release the annunciator TEST pusnbutton. Verify that the annunciator windcw in R0h 2, COL 1 turns,
?. ? off and remains off. -
C.:
- 10. Press the annunciator ACKNOWLEDGE pushbutton en the
- y- CCP, OPLE2J. Verify tne following
! fla. '"
l a. Horn turns off.
l 97 s
V W:
.._ .m. . - _ .
k t
f:
f LZP-1330-26 5-Revision 1 ,
Marcn 18, 1982 T
-.. 4 p
- [
- 0. All flashing winoows change to a stedoy glow. 0(
t
.N,plj {
'l ' t If desired, push tne TEST pushoutton to retest ROW (
2 COL 1 lamps. ROW 2, COL 1 lamps remain 1ignteo ).
The I; as long as tne TEST pushcutton is presseo.
other windows vill maintain a steady gicw. [
[ j, 11. Press the annunciator RESET pushbutton en the CCP, fs Verify that all annunciator windcws return !
OPLE2J.
e to the normal (off) condition. .
I "
- 12. At the Containment Air Sampiing Panel (CASP), CPLO9J, f;'
verify the following: f:
1 3a a. The green INACTIVE pilot light is on. .
t D. All four green SAMPLE FLASK INACTIVE pilot _t
,r 1Ights are on. )
I-Ls ,
- c. Sarple flasks are properly coupled and lockeo I' to the CASP, OPLO9J.
E I
- o. All sample flask inlet and outl et valves are
- y. opened. [
6 L e. All sample flask bypass valves are closed. {
jn E' 13. Datain the sample in accordance with Reference 2 r t.
prior to performing this procedure.
I r
- 14. Equipment: p E. i C
- a. Reach rods. }L g, .
p b b. Sample flask assemolles. .
- c. Partioner sampling assembly.
{f L
- 15. The operator should be faciliar with tne cperation .
of the hRSS panel s.
- g. '
g.
- 17. Establisn communications with the Unit huclear Station Operator (NS0). j f-e' .
- p. l, e 5
E 4 h.
.-a. .
l' n..._. .. . . _ _ _ _ . .. .._
V i, h b yrr N
u .- t LZP-1330-26
((
M Revision 1
[
March 18, 1982 I
TT' 5 7
?/
sa D. EBILA2119El .
m t 1. A Regulatory Guide 1 3 or 1 4 release of fission .
- products implies extremely high levels of ;
racioactivity. Oose rates may oe nigh enougn to
' G3 prevent entry into,many areas of the plant that are -
50 normall y habitable. Rac/Cnem Supervision shoulo be ;.
t-contacted pricr to entry into any area wnen such a release of fission products is suspected.
[gy S 2. Wear radiation aosimetry as recommended by Rao/Cnem f Supervision.
Sb 3. Wear protective clothing and respiratcry protection as recommended by Rad / Chem Supervision.
m '
k,, 4 Appropriate survey instruments should De available ,
for monitoring during this procedure.
)
f 5. Under no circumstances snould the sample fl a s k Ei assemblies be uncoupled from the CASP, OPLD9J, t witnout either verifying tnat the "sasple flask flushing exercise complete" indicating lignts are i
[{
tg on or performing a manual flushing operation.
Reach roos should be used to cpen and close the i 6.
valves on the sample fl a sk assemblies for nign radiation level samples. e
- 7. A LOW NEGATIVE CABINET PRESSURE ALARM, at the ;;
M{ Containment Air Control Panel, OPLE2J, implies a [
L' potential for airborne activity leaking into tne 'J y HRSS room. Investigate and correct the proolem [
pj immediately to precluoe contamination of the area.
E. LIMITATIONS AND AgTIONS kh l !.
lT After the "SF3 exercise complete" indicatcr lights, I dA 1.
the START pushoutton becomes inocerative until tne v
& CCP SYSTEM RESET outton is pusneo. This resets the (c.
j[ automatic sample sequence program.
- 2. After the "SF4 exercisa complete" indicatcr liynts, re. the START pushoutton oecomes inoperative until the
{6 i CASP SF4 RESET button is pushed. This signifies that the operator has removed the filleo sample ;
flask and replaced it with an empty one. p n[E
- w. ,
i
- n. t E
<c :
.w p i'
. . ..~.
'f'
? ' .. L \
v.; t
[! ,
n h!
hE. '
r'
?
[
LZP-1330-26 f.
Revision 1 b Marcn 18, 19d2 [
OS 0 t'
,ix c.
- 3. The exercise stop pushoutton, when pusheo, will stop [,
automatic sequencing and disaole tne start pusnoutton. p
"? i
- 4. If any proolems are encountereo at the HRSS panels. (
contact Rad / Chem Supervision. !
g.
9
- This procedure, though intenced far use uncer post- t 5.
accident conditions, can be used for sampling at [_
f; the HRSS panels during normal operations, during j f[{ which the precautions l i sted may have limited C However, normal routine sampling [
applicatioits. P precautions should be observed. !
'.i;
- 6. S51 may be replaced with the post-accident sample [
partitioner. For purposes of this procedure. SF1 e
is equal to the post-accicent sample partitioner. [
E To obtain a sample in the sample partitioner, proceeo {s El in accordance with Step F.1. 1 L
F. PROCEDURE g 7{(r L US.I.5 !
m 0 4
& For noun names associated with the valves operated [
in this procedure, refer to Attachment A.
{.
rt h 1. Obtain iodine, particulate and noble gas samples in (
the post-accident sampie partitioner in accordance t E
with the following:
h i
- a. Install tne sampler unit in the sample {
partitioner.
- b. Slide the positioner over tne top cf the sampler h unit.
~
[
- c. Remove the neeole guard.
P
- o. Place the noble gas vial with septum in its u protective housing and place the lid on the p' R
E vial housing. ,
i
- e. Install the vial and nousing in the partitioner g l-v oevice.
G #
i b,, regulator PC-1 until the pressure gauge reads I G 100 psi.
I l-w 9-f io2:
I .-
~ . . .. ..
- . ,. ~ _ . . . . . . . .
+
p5. . - . . - - - ., - .m.
e '
c, i
iI f.A ,.
Y I[E L Z P- 133 0-26
'{,' Revision 1 Marcn 18, 1982 '
sn 7 .
b Se
- g. Press the SYSTEM RESET button to initialize .
the automatic sample fl a sk filling program. ~
f..*.) t' kJ n. Press the exercise RESET button and then exercise START button to initiate the automatic sample .
acquisition sequence. 4
{ The CCP, OPLE2J, will control the collection 3]
i.
of a sample automatically. Iil
%L J. Wnen the ISOLATE S AMPLE FLASK annu.; iator windcw h t
flashes, press the exercise STOP outton. This F5[ freezes the program in the PAUSE mode. {
sw h p
- k. At the partitioner controller, set the counter to the number of aliquots of the sample to ce .
$5 taken as designated by Rad / Chem Supervision, ;
LU
- then start the sampling sequence oy depressing ,
y 70 the START button. v.
R
~
EE f r, .
- d4
/j" The sample tire will be determined by the time of
'and sampl e injection valve turning and injecting t the sample into the partitioner. k FP-
- 1. At the completion of the sampling sequence, "h k(I the vial and housing will pop up. At the CCP, p OPLE2J, release the exercise STOP pusnbutton i and press the exercise START pushoutton. fy' Pressing the START button initiates a tnree t minute sample flask line flush. When the flush is complete, the programr.er returns to the home 3
'N
' position and turns on the TIME BETWEEN SF1 - I LE SF2 timer.
li li l$
Et If the sample lines are not flusned dur ing automatic I[
i fg sample acquisition, a manual line flusn must ce g 8
, E. performed before the sampler unit can ce removed F.: .
' from the CASP, OPLO9J. Proceed immediately to Step f-p F.4. for manual sample l ine flusn. t n
(;
- m. When the TIME BETWEEN SF1 - SF2 tirer times out, (20 min.) tne programmer will repeat tne j $d sampl e acqui s i ti on sequence of Step F.1.h. for SF2. If a sample in SF2 is.casirec, proceea
[E r0 l
in accordance witn Step F.2. If nc furtner [
l
t F, . _ _ . . _ _ _ . _ _ _ _ _ _ . _ _ . _ _ _ . . _ _ . . _
I y .
L
,7-LZP-1330-26 Revision 1 Marcn 18, 1982
,. 8 c
1, samples are desired proceed in accoroance with Steps F.5.c. through F.5.f.
- 2. To obtain a continament air sample in sample flask (SF) 02, or 03, proceea in accordance with the following at the CCP, OPLE2J, or as otherwise
~
be directed:
7 a. When the ISOLATE SAMPLE FLASK annunciator windcw flashes, press the exercise STOP outton. This
{f( freezes the program in the PAUSE mode.
e.
c O. At the CASP, OPLD9J, close the inlet and outlet ,
[d
' valves for the sample flask, SF2, anc open the bypass valve.
- m. um Reach rods should be used to open and close the y [rn valves on the sample fl ask assemolles for hign
- - - radiation level samples.
? c. At the CCP, OPLE2J, release the exercise STOP '
K2 pusncutton ano press the exercise START pusnbutton. Pressing the START butten initiates 3.
a three-minute sample fissK line flush.
gv -
(d~
t!95 f
If the SF lines are not fl ushed during automatic <
75
- s4 sample acquisition, a manual line flusn must be performed later before the SF can be removed from the CASP, OPLD9J. Refer to Step F.4.
P: -
- c. When the SF2 exercise has endec, the programmer returns to the home position and turns on tne f ol l ow i ng: {
TIME BETWEEN GGO EXERCISES timer (20 min.). b 1) ry
- 2) TIME BETWEEN SF2-SF3 timer (120 min.). b bl
,, e. Four GGD exercises will be accomplishea oefore 7i the TIME BETWEEN SF2-SF3 timer times out. At
" the completion of tne four GGO exercises, tne CCP, OPLE2J. will collect the SF3 sample. If tne TIME SETWEEN SF2 and SF3 timer times out F?.?C cefore completion of a GGD exercise tne GGD exercise will continue to compl etion ano tr.en i
F L. '
r
.; . . . - . . ..-~. u . .
rs ,
r L Z P- 133 0-26 i Revision 1 March 18, 1982 9
f~
\c .
the SF3 exercise will Degin. Perform Steps
. , F.2.a. through F.2.c.
i i
- f. Observe that all SF EXERCISE COMPLETE incicators, for sample flasks SF1, SF2, and SF3 cn the CCP,
[~ OPLE2J, are l i ghted. If all inoicators are e lightea, proceed to Step F.5. for system shutcown ano cart / cask removal. If all exercise '
e ." complete indicators are not lightec, proceed immediately to Step F.4 for manual sample flask !
I.
l ine flusning. CO NOT uncouple the sampling ,
flasks at th i s ti .ne .
r-I
- 3. To obtain a containment air sample in sample flask i
- 4, SF4, proceed in accordance with the following ,
i at the CCP, OPLE2J, or as otherwise directed-
". c !
~
o 7. y l
k b. Place the CCP Function Select Switch to tne !
SF4 position. [
W ,
[j c. Press the exercise RESET outton anc then exercise !
START button to initiate sampling. i p_.
I
- d. The CCP, OPLE2J, will control the collection [;
{~. of a sample automatically through tne following sequential operations: ,
in 1) Two-minute pre-sample Dackflush. [.
cy 2) Three-minute sample capture. :
b ..
" Fifteen-secona equilibrate flask pressure.
3)
- ) Three-minute resiaual gas removal. f-
- 5) Fifteen-seconc post-sample Dackflusn. ,
7-:
(( 6) Fifteen-second post-sample backflusn.
- e. When the ISOLATE SAMPLE FLASK annunciator winaca !
flashes, press the exercise STOP Dutton. Tnis j f_
5- freezes the program in the PAUSE mcoe.
l
% f. At the CASP, OPLC9J, close the inlet and outlet !
valves for the sample flask, SF4, anc open the l
[L bypass valves. !
-q _ , , , ,, . . _ , _ - - . - _ . -
s
.i
. _ . ~ . . . - _ _ . _ _
- 7. ,_ m_.____. t
('
L
< r-,.
o f' '
LZP-1330-26 Revision 1
-. March 18, 1982 10 e 13 '
- g. At the CCP, OPLE2J, release the exercise STOP pushbu+, ton and press the exercise STAAT I3, pushbutton. The CCP, OPLEZJ+ will initiate a
- r. - three-minute sample flask line flusn to complete the sampling sequence.
rv L@, NOH If the SF lines are not flushec during automatic f.", sample acquisition, a manual line flusn must be U" performed later Defore tne sample flask can De Refer to Step F.4.
removed from CASP, OPLD9J.
gn
[i h. Observe tnat the SF4 exercise complete incicator is lightea. If tne inoicator is lighted, w proceed to Step F.5 for system shutocwn ano k;, cart / cask removal. If the indicator is not
-' lighted, proceed to Step F.4 to perfcrm a manual flushing operation prior to further action.
DO NOT uncouple the sampling flasks at tnis
)f time.
6.
e 4. To perform a manual sample flask line flush, proceso in accordance with the following at the CCP, OPLE2J:
{.{
- a. Turn all air operated and solenoid valves to I2 the CLOSED position. ,
YU I D. Turn the f ollowing valves to the 3 PEN position.
I 1) SV-10.
SV-1.2 and AV-1 for SF-1 flushing. r
- 2) ,
.Y?
SV-2.1 and SV-2.2 for SF-2 flushing.
G; 3) 1 rp 4) SV-3.1 and SV-3.2 for SF-3 flushing.
b 5) SV-4.1 anc SV-4.2 for SF-4 flushing.
m.
- . " c. Flush the sampl e fl ask lines for a period of we three-minutes and close SV-lO anc the inlet and outlet sampling line valves previously F" openec in Step F.4 0.
\
N. c. Proceea to Step F.5. for system snutcown ana j gr.
cart / cask removal.
n we ,
t A .'
. ,,,.,,,w.,.,
- ~
- m~*
-..asm-,, mn. .
ff k'
E b ..
i u- '
i k- f' i g si ,
LZP-1330-26 f*
- f. Revision 1 March 18, 1982
-e LL f
y y
- 5. To temove the partitioned sample proceec to Step g
'F.6. To remove the cart / cask and shut the system y, down, proceed in accordance with the following at f.
b the CASP, OPLC9J, or as otnerwise directed:
LC t
r't ' a. Unl ock the quick disconnects from the flusheo [
cask or casks. Remove the cart / cask assemoly y k3 to the laooratory area in accordance witn F Reference 3. [
g i
L# CAUTION a Reach rods should De used to unl ock the quick [
7[ disconnects on tne sample cask assemblies for nigh _
go level radiation samples. [
f s
Install the backup cart / cask assemoly.
f O.
- c. Pusn the RESET outton at the CASP, OPLD9J. to L
)
"" clear sampling flusn indicator l ights f rom .
ACTIVE to INACTIVE status. !
I-Push the SYSTEM RESET button at the CCP, OPLE2J.
pg d.
to return electro-programmer to initial startup I I"9' moce. f t-P
- e. At the CCP, OPLE2J, turn FUNCTION SELECT to k
- OFF, and remove the tape output frcm the printer. h" The tape output snould acccmpany the samples '
to the chemical l acor ator y.
p; i i
( be Upon completion of the sampling operations, I
f.
secure the sampling lineup in accordance witn !
Reference 2. Steps F.4 0 6) through F.4.c. ,
- 6. Tc remove the partioned sample, proceed in accorcance y..
with tne following:
- a. Remove the vial ano nousing from the partitioner.
I
' Log tne following information (as appropriate) [
b
- for entry into the A.A.I.S.: p I
- 1) System sampled ano unit. l.
F [
- 2) Sampl e l ocati on.
kb L T
t
, 7 t l T -
tv
--n.- .,-.....n w-
,, o . L r:
- k . b
~
- n
! h.
N g p- LZP-1330-26 i~ Revision 1 ,'
" Maren 18, 1982 P 12 I;l r e f 3) Sample time on. ,'
Yi p(,,;
- 4) Sample time off (this time will oe tne same as time on).
fg; g
b
- 5) Sample cate on. fp
.t.
I 6) Sample date off (this date will De tne r same as date on). '.
- 7) Reactor power, megawatts thermal. -
F
- 8) Reactor power, megawatts electric.
g ,
- 9) Initials. k.
I.
P.? o. Remove the protective housing from the noole E 3] gas vial and determi ne the radi aticn level of the sample. If radiation l evel s warrant, place [i
,p the vial in a lead shielo for transpcrting to i
- y. the analytical area. y V
- c. Remove the protective housing from the particulate r and iodine cartridges. l.
b l
- d. Remove neeole from the sampier unit. ll
- e. Remove the particulate and iodine cartridges.
f.
, fe Transport the samples to the sample preparation .
A area in accordance witn Reference 3. F Lis i
- g. Separate the particulate filter anc iocine l; y, cartriage utilizing a knife to cut the ccnnectcrs. {
p Cut relatively close to the top anc Dottom of F the samples i n oraer to set tnem flat in secondary containers.
- i. Place the particulate filter inlet side up in '
a plastic petri disn. .
w j' y
- j. 'w r a p tne sample containers in plastic wrap or J.
seal in plastic bag. [
t
- k. LaDel the samples i n acccrdance witn the
.1 following: p t-t-
A h-g.em q=w - esdery ey 9gae.g-O
- e.m ey u ,a ,,,,y,ge
- 4.*.n.a
I
.~_
- . ?
L .e r,. ,
w.
LZP-1330-26 r-i~ Revision 1
" ~ ' March 18, 1982 ,
13 Q )
[2 t 1) System sampleo ant unit.
rf: 2) Sample location. p
- 3) Sample time.
t b 4) Sampie cate. b k y;
- 5) Sample volunte. [O R
O' 6) Survey results. $
'"'' ~
t fn.
$" 1. Prepare the post-acci dent sample partitioner [t for further sampling in accordance with Steps
" F.1.a. througn F.1.e. f
- e. t;
- 7. Perform the racioactive anal ysis for each sample in y, accordance with Reference 4, 5, or 6, as apprcpriate. h.'
V w T C' 8. Determine the I-131 equi valent concentration using 3 th Hewlett Packard Calculator program in accordance f-with Reference 8.
7:
- 9. If the Hewlett Packaro calculator or calculatcr [
g program "I-131 Equivalent Concentration" is not I g available, calculate the I-131 equivalent concentration of the containment ai r sarr.ple in accordance with
[4 p
Attachment B.
- 10. Calculate the iodine, particulate, and nocle gases r
curie content in tne primary containment in accorcance with the following: p w
!!.9.I.E i-Calculations should De perforzeo on the isotopic I anal ysis hard copy printer output. ;
2
- a. Calculate tne total I-131 equivalent curie [
[d. content of the primary containment in accordance f[
I with the following:
L W I'
{' C = 0 L050S.55.1.
(lE06 uCi/Ci)
A w
j u
k,
- ~ L r
b b -
I-
- - - - - - ~ - - ~
l _ _
p t. '
, bi 7- Ri 1:
f
- o f[.
'{ !.ZP-1330-26 i
- Revision j g.
March 18, 1982 .-
rc , 14 tj
- khers: C = Total I-131 equivalent curie content in the primary containment.
fl
+- w >,
,- I a S= I-131 equivalent concentration uCi/cc, in the sample from Step {g r- F.7. or F.8. (p.
w .
O0 F 1.1E10 cc = Primary containment free air h volume. $.
f2 %
C o. Sum the particulate radionuclide ccncentrations. [L uti/cc, from the isotopic analysis in Step F.7.
L
- c. Calculate tne total particulate curie content f;
of the primary containtent in accordance with tne following: r pL t C=JMDdGBQ g (lE06 uCi/Ci) y o?- L
., Where C = Total particulate curie content f of the prircary containment. [
IS r)"g~1 S = Particulate racionuciice t, c orice nt ra t i on , uCi/cc, in b the. sampl e f rom Step F.10.D. [
1.lE10 cc = Pr! mary containment free air volume. .
Il
- c. Sum the noble gas radionuciice concentrations, '
uCi/cc, from the isotopic analysis in Step F.7.
- e. Calculate the total noole gas curie content of r.
i@t the primary containment in accoroance witn the }
following: [,
F f C=LMDdD%Q (lE06 uCi/Cs) :
f.f where: C
- Total nocle gas curie content L of tne pr ircar y ccnta i ntrent.
[
m S= Noble. gases racionuclice
{ concentration, uCi/cc, ir tne sample from Step F.1C.c, r v
a i i
(
. . . - - . - . - - - ~ ~ ~
p - -
.r-
-"~~ ' ~- '- e
(
- I.s fs 5
V [ r p LZP-1330-26 e
" Revision 1 :
^
March 18, 1982 15 1.1E10 cc = Primary containment free air voluse. 4
- y. 4- I-n ~
E.! 11. Report the sartple results to tne Rad / Chem Director for evaluation in accordance with Reference 9. ,
- 12. Route all output data and calculations to Rad / Chem Supervision for review. [t h[I 13. Dispose of the SF al r sampies fol1owing anal ysi s, i.
LC in accordance wita the following: [
te a. At the Valve Control Panel, O P L( ~3 J , proceed in [;
[, accordance with the following: {e F.
g 1) Place the UNIT 1(2) PCHER switch in the (
ON position. .
- 2) Open tne following valees and verify tne [
, F' indication snows OPEN: !
Ul ;f a) HRSS SYSTEM AIR RETURN TO SUPPRESSION POOL, 1(2)CM-088 and 1(2)CM-009. I{
U b) HRSS SYSTEM AIR RETURN TC SUPPRESSION f POOL, 1(2)CM-090. f d'rt D. Connect the cask / cart assemoly to an availaole O sampling station at the CASP, OPLD9J, ano note I rr the samplitig station number.
- c. Close the sample flasx oypass valve at the CASP, OPLD9J.
+
V d. Open the sample flask inlet and outlet valves ,
at the CASP, OPLO9J. '
- e. At the CCP, OPLE2J, place the FUNCTION SELECT ,
switch in the SF4 position.
y f. Press the EXERCISE STOP pusncutton on the CCP, S OPLE2J, if not already depressed. f.
I er g. Turn all air and solenoid operated valves on }
[i the CCP, OPLE2J. to tne CLOSED position. },
L
- n. Turn the following valves on the CCP, OPLE2J, 4 h.
m to tne OPEN pos i ti on:
{
l.
LS V
-- . ~ . . . --
- t. 1 I-
- a. -. .. '. - - - .- . - - -..... . . . . . - .
y' W.
u
- e.
- k:
r; '. ,
p
- - F LZP-1330-26 Ei
' Revision I h
'-~
March 18, 1982 I 16 h L
- 1) SV-10 to open the nitrogen supply. I L_
.v U
- 2) SV-1.2 and AV-1 for SF-1 flushing.
h"-. h.
- 3) SV-2.1 and SV-2.2 for SF-2 flushing. E b," b 6 4) SV-3.1 and SV-3.2 for SF-3 flushing. [
r
- 5) SV-4.1 and SV-4.2 for SF-4 flushing. [f p
gj
- i. Allow the sample flask to flush f or a minimum g_
g,, of three (3) minutes. 4 L
t',.
L j. At the CCP, OPLE2J, turn Sv-10 to the CLGSED !!:
position. Ir.
Turn the solenoid operated valves opened in [t C[
[ k.
Step F.13.h. to tne CLOSED position. t g
Press the SYSTEM RESET button cn the CCP, 4
" bo. 1.
b OPLE2J. to return the electroprograme.er to the ,
initial startup moce. {
g:
Turn the FUNCTION SELECT switch on the CCP, f' h m.
OPLE2J, to the OFF position.
- c f? Release the EXERCISE STOP pusnbutten on tne p; g' n.
CCP, OPLE2J. {j p
r M o. Close the sample flask inlet and outlet val ve s did on the CASP, OPLO9J. h c
- p. Unl ock the Quick disconnects fror the cask / cart b g f:.
?, assembly and remove the cask / cart. p L
- i. . c E i The cask / cart may De left coupled to the CASP, ',
b j.
OPLD9J, for future anal yses.
cg:- .:
- q. At the Valve Control Panel, OPLC9J, proceed in E accordance with tne f ol l ow i ng : {';
t.
em C1ose tne fol1 ow ing val ves and verify tne I:
b= 1)
O irdication conows CLOSED: [
f t,
a) HRSS SYSTEM AIR RETURN TO SUPPRESSION
[7~ POOL, 1(2)CM-088 and 1(2)CM-089.
ai .
e h'.
6
. . . . . . ~ . - . . . . . , .-
p.
C' *
.. . . . .. . . . . . . . . . - - . V b B b
- e. .
11 *
- 6
.n y p:'
I' ' LZP-1330-26 (B*
'- d' Revision 1 [',
'iarcn 18, 1982 4' I#
17
- 7. , .
As HRSS SYSTEM AIR RETURN TC SUPPRESSIDA {
. ivo o)
POOL, 1(2)CM-090. n{
v.
9V f
- 2) Place the UNIT 1(2) POWER switch in the ((
OFF position. }'.
((.
$ B 3d G. gg MLISTS 3: p qu 1. None. g y '"
H. Tgggj,g g g g G Q TIONJ g g G Q ), f' !
E:
m~
- 1. None. h
. 12 ".; .
L !!
) I" b
r
. e.
F'7) *
{. e R
8
- l;;
n-L.
f$
k l 4
k..
E E, b, '.
- y-h?
.- r.
Ml?
aa L
y.
i' E
U.
ki; h
(i.?r g)F l,
,mm~==*- -m~~ -'~m * .ws*
~ . . ~ .
. . . .~...- - . -
t t
D'
._ , -. _ j L.
i
,, 3 .,
LZP 1330-26 [
y .
Revision 1 i L..
- March 18, 1982 r 18 sI 7e
"" f ATTACHMENT A t VALVE LISTING g.
7, s.,
M k
'i Q AV-1 Sample Flask #1 Inlet' k.*, '
Sample Flask #1 Outlet
{(
r SV-1.2 i l
M~ Sample Flask #2 Inlet *
.g SV-2.1 u.s {L SV-2.2 Sample Flask #2 Outlet [
i w<
r, . p W SV-3 1 Sample Flask #3 Inlet j
.g SV-3.2 Sample Flask #3 Outlet {
. 3 4 SV-4.1 Sample Flask #4 Inlet E.
Sample Flask #4 Outlet l F SV-4.2 I.U -
SV-5 Sample Purge t
[
i '
' ", h. AV-2 CASP Outlet <
2 SV-10 Nitrogen Inlet {
'T. .- y
..2 s iM I
. i t
r-e.
'l r
5
[,
L 4
'3
('
g u
i er m
s inA
, V La e
- .p I
- s I, s c.
I.
- e. l.
- .9
fil !
- 6. ,
~ *'
s... . -7m-- - + *-*u----*~
,-a.m.,--
-- . . - - , . , .--,y v -- , - - - - - , , _ . - - - . - -- -- .,- . _ _ - - - - - , - - - - -
- ! (
>/ 7
, f.. .. l, ,
,t
, .- 4 t.
i I
p .
ATTACH}fENT B LZP 1330-26 h Revision 1 e
~
19 i <
- tinai-
- ~
j, P Determination of I-131 equivalent concentration of the con ta intnent L,i t air grab sample in the event that ensputer analysis is not available. -.....
f h
n !.
- 1. Determine the I-135 concentracios in the containment [
air grab sample from Step 7.7 I
., F
- 2. Determine the I-135 concentration in the containment air N at T , the cima at which the release was made to the i
'j cont 31==ent, using the following equation: -
Q~ A k2- I-135 concentration (uci/ce) at T, = ,_3e t v
n ate: A = I-135 concentration (uci/ce) frem p procedure Step 7 7 .
[4.
e = 2.718 !
pr ~
d A= 1.724 E-03 min decay const. I 1 I t= Sample decay time (sin.) - -
F[ teactor shutdewn to sample time ( a T) i
$ I .
5 l
S 3. Determine the concentration of I-131, I-132, I-133 and I-134 using }
che following celationships:
.- e
~~"' < :
, y I-131 Concentration (uci/ce) = I-135 concentre.cion x 1.0E-01 .i
{
- ~4
't I-132 Concentration (uci/ce) = I-135 Concentration x 9.23E-01 l. ?
. i'
- y I-133 Concentration (uci/ce) = I-135 concentration x 6.85E-01 ,(t h i
/ ^' [
I-134 Concentration (uci/ce) = I-135 concentration x 1.846 p Deternine the I-13I equivalent concentratien of all iodine concentrati6ns.
4 in the contain=ent air using the following equation:
t k
Iotal I-131 Equivalent = I-131 concentration + (1-132 Concentration)(0.036)
[
Cencentration (uci/cc) t f
~
+ (1-133 Concentration)(0.027) + (1 ' S - wc - tration)(0.017) 0 0
F
"'"' + (1-135 Concentrati.on)(0.084) $i m ,
lh1 I
i 'Mi, i
b-(L ;
- e Q w
^ .
[ ,3c e,
~. . r, '
1 < .
.[s ,.
(
e- - f(-
s W
L LZP-1330-27 f~ Revision 1 g
. 4 Parch 19, 1982 p I f i pj k; S AMPLIf4G CF RE ACTOR CCOL AhT OFF-GAS AT THE HIGH RACIATION SAPPLIhG SYSTEP ,
c
[>
p't i.
t ,
, 4 y --
g,s d ' ,4- A. P,UR P C Sj
~
The purpose of this pr 'idure is tc celineate a metnod 6 of ootaining a reacter ,3alant of f gas sa.nple at the High [
[Gp L
Radiation Sampling Systs t (HRSS) during normal ano post- [C accident conditions. Tais procecure i ncluoes tne steps h to route gas to the Cheeical Analysis Panel (CAP) and g,
tne Chemical Monitcring Panel (CFP f er, nydrogen anal ysis. if tw a B- Ef.fE3f.yC_gi
.r -
b[ 1. Sentry Equipment Corporation, Pcst Accicent Sampie h System, Vclume 1.
- 2. LZP 1330-29, " Sampling at the'High Raciation $ampling [
' System (Valve Operation at the HRSS Valve Control {
s Panel)." b b L7P 133C'31, "HRSS Sample Mcvement."
- {
i 3. (
b N 4. AAIS,-CCP-0031., "BWR Coolant Radionuciide Analy5is."
^$ C. PREREQUISITES p
The operator should oe f amil iar with tne cperation h
'"'~
1.
of the HRSS panels.
t r
-% 2. Estaolisn ccmmunications witn the Unit Auclear [
y Station Operator (NS0).
i
- 3. Verify that argen, and nitrcgen, apprcximately 100 psig, is availacle at the Liquid Sampl ir:9 Panel (LSP), CPLD8J. i
- 4. Equipment:
- a. Reach rocs., [
l r
- c. Griotong. r 9: 1
- c. Re.3ctor coclant ctf-gas sample octtle witn e k
septum.
L !
2 -
, F~q *l l
(:,. f.'
)
C. . . . _ , . _ ,
rp ,
k
. . .- ~ a p.>--x--..--..--.-. . . . . - . . . . .
y:
p
+
. . p
~',
15 LZP-1330-27 4 J.
' Revision i Maren 19, 1982 fg, n
> :)
b
- 5. The sample must nave oeen obtainec in acccrdance k" with Reference 2 prior to performing this procecure. [
p " [
O.
P R,,3Q UT I O N S t I[, 1. A Regulatory Guide 1.3 or 1., release of fission ;
b- prooucts i mplies extremely high levels cf O l.
radioactivity. Dose rates may be nign encugh to
["
& prevent entry into many areas of the plant tnat are normally haDitable. Rad / Chem Supervisicn snould be h h contacted pricr to entry into any area when such a e
release.of fission products is suspectec.
., ((.
C N 2. wear radiation cosimetry as recomner.ded by Rac/ Chem f Supervision. '
rr b 3. Wear protective clothing and respiratcry protection ;,
as reconmencec cy Rad /Cher Supervision. ll p
Apprcpriate survey instruments shculd De availaole
' b
- 4. T for monitoring during this prececure.
0 I"l E. LI QTATIONS ANC AQ,I,,,gg ,L b 1. Notify Rad /C9em Supervision if any prcolens are ji:
encountered at the HRSS panels. {
eg r
- 2. This procedure, though i ntended for use under post-accident.conditons, can ce used fcr sampling at the I;-
HRSS panels during normal operaticns, during knicn [
- the precautions may nave 1inited applications.
However, normal routine sampling precauticns snoula ce coserved.
5 F. PRCCEDURE
[
i hE.5.5 b
For noun names associated aith tne valves operatec p In this procecure, refer to Attachment B. .
3 y I-
- 1. Prepare the system for sampling in accordance with the foilowing: ~
tT
- g. :
ts.: a. Install tne neeale fl usn tcol . k 99 m [!
E p:- (
c.
u
~ ~ " ~ " "
k
- t
- f: ;
L
. r:
~
a h
L e
U" LZP-1330-27 f
- h. . Revision 1 }
March 19, , 1982 l 3 L
{? ' ' '
- o. Verify the following valve lineup: b i
h'[ 1) RC-V-1.1 (closed).
w
- 2) RC-V-1.2 (closec). l 0
4 p- [
(h 3) RC-V-1 3 (closed).
,r -
j ex. 4) RC-V-1.4 (closec).
(O : [,
" 5) RC-V-1.5 (closed). )
- 6) verify RC-V-* i s cicsed. Ccnnect the {
{i" p,,
flusn water nose to RC-C-1 anc cpen the t.
flush water l i ne valve. [>
.e.
- 7) RC-V-5.1 ( cl os ed ) . '[
.{ f-
- 8) RC-V-5.2 (closec). p
, r _..
L Li 9) RC-V-4 (cl osed ) . I-t
- 10) RC-y-2 (closec). [.
cg l
- 11) RC-V-7 (closed). [
b
- 12) R C-V- 17 (closed).
- 13) RC-V-16 (closed).
j ]?
g} 14) RC-CV-1 (BYPASS). j t.
l 15) RC-V-19 (BYPASS).
1 4
I
- 16) RC-CV-2 (9 o' clock). [
i W 17) RC-V-15 (closca). [
~
i (J
- 18) RC-V-13 (closec).
- 19) R C-V - 12 (closed).
- 20) RC-V-l* (closed). [
I5' ).
Li 21) RC-V-8.1 (closec). f-f i
TW
. b kkk i':
a.
s ., . w-.,,s ,--.e.%~
-y..,w,,
. m -+% e , v e-t 5
L
. . . . - . . - t se4-.-__--__~.----.--....._---..--.- V V
u e
~
h ru t u 1 tb LZP-1330-27 y k
' b: Revisicn 1 [
Marcn 19, 1982 0 4 I-
- [3 !
Lh l
- 22) RC-V-ll (CLOSED).
rm RC-V-18 (6 o' clock).
23)
{.. j
- 24) RC-V-22 (YO WASTE). g
,a ,
dl 25) RC-V-9 (open).
p riyt 26) RC-V-8.2 (open).
I b) 27) RC-y-10 (open). [
F, RC-V-3 (open). i.
h$ 28) 5 LL '
- c. Dry the expansion vessel RC-EV-1 in accoraance 2 witn the following:
E7 Fi 1) Turn RC-V-Il clockwise to the 3 o'clocx
~
[
position.
,3 l 2*
- 2) Pull cpen RC-VREL-2. When tnere is a !
sharp increase in pressure incicatec on s RC-G-3, release RC-VREL-2.
{# b k
- 3) Acjust RC-VREL-2 until RC-G-3 incicates !
approximately 2C psig. Ory RC-EV-1 with argen for a minimum of cne (1) rinute.
{
l.
- 4) Turn RC-V-11 counterclockwise tc tne 9 o' clock position to permit RC-EV-1 to [-
t
vent, then close RC-V-9.
l k l Evacuate the expansion vessel ano sarple lines i c.
in accorcance witn the fcilowing: f; Install the ciluted gas sample cottle on !
- 1) i the front panel neecle.
Open RC-V-13 anc then open RC-V-12 anc 2) evacuate until RC-G-2.1 anc RC-G-2.2
'?
indicate a minimun cf 22 incnes of mercury.
- 3) Turn RC-DV-2 to the 6 o' clock pcsition [
$[ and continue tne evacuation urtil RC-G- [
Lw 2.2 inoicates tne same reaains as RC-G- r 2.1 or a mir.irun of 22 incnes of mercury. :
- ) Close in creer RC-V-13, RC-V-10, anc RC- l l
v-12. Recora tne vacuur en RC-G-2.1. on j:
rr i
- e
.m.w.
m,. . --
- -e.*,m, v w n ,
. .. . g.j p
ll.' ll P E ra F LLP-1330-27
.f Revision 1 C March 19, 1982 L
-5 i tt !
h** LRC Fcrm 1097A (Attachment A). nait for sE P
a minimum of twc (2) mirutes anc verify that tne vacuum is holding.
{
g ,.
f I
- 5) Turn RC-V-11 slscad g to tre CLOSEC
&~ position. y E.
[;
u
- 6) Turn RC-DV-2 to the 9 o' clock pcs i ti on . '
e.
[
h
- 7) Open RC-V-14 anc verify the pressure on RC-G-2 2 is approxinately 1 psig. [
t.
- e. Purge the sampie 1ines in accordance with tne {;;
f Oy f ol l owing:
I Open RC-V-8.1 t-m 1) is
- 2) Open tne sample source val ve RC-V-1.1 (- p 1.2, -1.3, -1.4, -1.5) for tne sample to a.
(.
De cDtained* r_
?f t.
G
- 3) Sl owl y open RC-VREL-1 unti1 RC-FI-1 (
p indicates 35-40 inches water. Purge for
((g a minimum of five (5) minutes.
v.
- 4) 51owly close RC-VREL-1 unti1 RC-FI-1 l'-
I, ty' indicates 12-15 inches water. Continue b the purge for a minimum of cne (1) minute. $
- 5) Close RC-V-3. ;
g 11 6
- 2. Sample in acccreance witn the fcilowing: 7
[ a. Cpen RC-V-2. j ~.
M[ (
D. Adjust RC-VREL-2 until RC-FI-2 inoicates 18-22 Y incnes of water. Purge for a minitur of tnree 3
t (3) minutes.
J.
- c. Close RC-V-8.2.
Close RC-V-8.1.
d.
r 7 e. Cicse RC-V-1.1 (- 1. 2, - 1. 3 , - 1. 4, -1 5). {
J: !
At the Valve Control Panel, CPLC9J, secure the m;
f.
sampling lineup in accercance witn Reference I steps F.1.c.e) enc P.1.c.2).
lg 2.
i I
I r k
k l-t (e e spe. ym
" -NuluW'**
WN1F*f4Y4i-
L 7-___....__._.._.____.._ r IX E
. p 2' .
.ki l
un LLP-1330-27 /
' *E f'~f Revision 1 Marcn 19, 1982 -
L rn- 6 k
,[j[
- g. Cpen RC-V-7 and tnen open RC-V-9. ts-
- n. Adjust RC-VR EL-2 unt i l RC-FI-2 indicates 18-22 h l
inches of water. Flush witn demineralizea I water for a minimum cf three (3) minutes. {a n.
s c:
kU i. Close RC-V-7. i.
- j. Open RC-V-3. g'n y
s.
f K. Adjust RC-VREL-1 until RC-FI-l indicates 35-40 inches of water. Flush with demineralized i EM water for a minimum cf one (1) minute. Close Is RC-V-3. f...
E
- 1. Cpen RC-V-1 1 (-1 2, -1 3, - 1 4, -1.5). Flusn
$gm/j witn demin water for a minimum of five (5) A minutes.
6
-1 5). S F7 m. Cicse RC-V-1.1 (- 1. 2, - 1.3, - 1. 4,
(:
N2
- n. Close RC-V-4.
gL o. Secure the system li neup in accordance witn (
Reference 2, steps F.1.d.8) through F.1.f. f i b I
- p. Open RC-V-9, wait approximately five (5) seconcs, j u J
and close RC-V-9. i l <
1.
p.
- q. Open RC-V-16. '
F1 r. Snap open RC-V-9 and wait for cne (1) minute. 0 t
y t
g y[m} s. Cicse RC-V-16 anc tnen close RC-V-9.
- t. Turn RC-V-ll .cou_n3, erg,1,cQ w113 to tre 9 o' clock F
Of positicn. The pressure reading cn RC-G-2.1 is '
ku normall y Detween 8 and LC psig. Reccra tne I reading cn LRC Fcrm 1097A (Attachment A). i p.
r f g[P $g u. Verify with the CMP, OPLE4J, operator that the {
' gas chromatograph as reacy tc receive tne ! ;
sample. l [
g.,, ! !
$u J4! v. Cpen RC-V-15.
[
I
(
pg w. Instruct the CFP, OPLc4J, cperatcr tc cegin L
,{
loading tne gas enronatograph sample Icops.
FF-
!\ ~
c_
-._.n,--,. . . _ _ - _ . . .
.~
c L
- i K L Eu [
I I^ LZP-1330-27 Revision 1 U(
b[. Parcn 19, 1982 fj 7 h F
[94
'" x. Upcn nctification frcm the CPP, CPLE4J, cperatcr h O
that all icops are fill ec, close RC-V-15.
m
(:f , (
mA y. The pressure indicated on RC-G-2.1 is normally 5 ana 7 psige record the reacing on LRC Form ft EN 1C97 A (Attachmert A).
EN h,
- 3. Octain tne cilutec gas sarple in accorcance with
, the following: [
n: l' '
U a. Turn RC-CV-2 to tne 6 c'cicck positicn. Wait ;
until tne pressure on RC-G-2.2 returns to 1 j
> f$ P5i9 Ek:
- b. Turn RC-CV-2 to tne 9 c' clock positicn. Close !c RC-V-14.
g- s V4 c. Remove the griptcng containing the diluted gas b sample and place meninc snielcing.
' VS CA 4. Flush the system in accorcance witn the fcllowing:
p? a. Verify RC-V-15 is cicsec. Turn RC-V-ll jj counterclockwise to tne 6 c'cicck positicn. p D. Open RC-V-9, RC-V-7 anc RC-V-8.1. k
, ?
^: I l
- c. Adjust RC-VREL-2 until RC-FI-2 indicates 18-22 I incnes of water. Flush with cemineralizea y water for a minimum cf one (1) minute. [
L I Open RC-V-8.2. E d.
h '
% e. Cl cse RC-V-9 anc RC-V-7.
2
- f. Adjust RC-VREL-2 until RC-FI-2 inoicates 18-22 c, inches of water. Flusn witn cemineralized
% water for a minimum of three (3) minutes.
t P
n g. Close RC-V-8.1. ~
5 l I;
- n. Turn RC-V-11 counterclockwise to the 3 o' clock position.
EmL i. Open RC-V-9. g
-r J. Pull open RC-VREL-2. when trere is a snarp
[$ increase in pressure inoicated on RC-G-3,
'" release RC-VREL-2. Acjust RC-VREL-2 until RC-c: i
/
<- 3.
t
- - - ~ - .- -- .
t W...-___....... .. . - - . - . --
}. -
4 a
,:. h l
j.
E y'
f, LZP-1330-27 i L' Revision 1 March 19, 1962 8
!?. '
?
G-3 incicates 20 psig. Flush with argen for
- a minirrun of three - (3 ) minutes.
p(q.
- k. Close RC-V-9.
[][ l. Open RC-V-10.
- e. . 1
- m. Turn RC-V-11 counter ci cckwise to the 9 o' clock p' position ano allo RC-EV-1 te vent.
- n. Clcse RC-V-10. _
ET. o. Turn RC-V-11 clockw i se tc CLCSED.
h.
uu
- p. Open RC-V-8.1.
P Adjust RC-VREL-2 until RC-FI-2 indicates 18-22 (f, c.
inches of water. Flush with water fcr a minimum rm of one (1) minute. v p.
Ei r. Terminate flushing oy cicsing the folicwing:
@ 1) RC-V-8.2. *
{bi ;
- 2) RC-V-8.1.
E h,.f 3) RC-V-2. ,!
- 4) RC-V-4,. Ib c Cicse the flush water valve anc ciscennect the id s.
flusn water from RC-C-1. i r
At the Valve Control Panel, CPLC9J, perform t.
M";n t.
h the folicwing:
- 1) Secure the sample ccoler water flow. i; S e s
- i. . ,
- 2) Close the remote ficsh isclation valve. {
?
- 5. Transport the sample to the sample preparation area ,
E[p ]
in accordance with Reference 3. ;.
l-
- 6. Prepare the sample for analysis in accordance with h the fol1owing:
{
- a. '
n rap the vial in plastic wrap cr seal it in a pl ast i c t:ag. 3
{}-
u.
p-i r
o
- r. 1
- r. .
- ;(
LZP-1330-27 Revision 1 ;
Marcn 19, 1982 v 9 -
i i C D. Lacel the sarple in accorcance with tne following: .
- 1) System samplea ano sample lccation. .
"~
- 2) Sample time. ,
e Sample cate. y
((. 3) k h;. r s
- 4) Sample volume.
., I.
- 5) Initials. r d ?
- 6) Survey results.
b 7. The sample volute in tne vial is estimatec in i!
accordance wi tn the fcilowing:
m 6" L1'4i
/ V =V, V, *(P, + 14.7) v g p1 + 14.<3 s.
m 7 = Sampl e vcl ume in ml. f.
where V
[. L V
g
= System vol ume (RC-EV-1 anc 1ines t
to RC-V-15). ,
Ca, V = Volure of RC-DV-2.
V3 = Total glass vial vclume. p P = Pressure read ing f rom Step F.2. t. [V r
q y l
6 P 2 = Pressure readins fror Step F.2.y.
.y 8. Analyze the sample in accordance with Reference 4. ..
[;i 1
MH e
~
.f.
ff The results will ce in uCi/r.1 of cff gas not reactor .
' water. .
fy 9. Report the sarple results to tne Rac/ Chem Di rector I LC f or eval uati on.
Route all output aata anc calculaticns to Rad /Chen v4 10. -
t; Supervisicn fcr review.
- 11. Tc cisocse et the reacter coolant off-gas sample.
c proceec in accoraance with the f olicwing:
A
!'~
_m . . _ , 3
[L y, t
- 2. f x
-b-
"D _
y L
t, m LZP-1330-27 h Revision 1 [
I March 19, 1982 [
10 !.
W t M
A a. Verify the following valve 1ineup: {
- 1) RC-V-1 1 (closed). i k ,
- 2) RC-V-1 2 ( cl osec ) . J '
ri-
] 3) RC-V-1 3 (closec).
- 4) RC-V-1.4 (closec). ::
'y LU 5) RC-V-1.5 (closed).
po 6) RC-V-1C (cicsed).
g 7) RC-V-ll (CLCSED). {;
- 8) RC-V-12 (closec). Fl-
- h. t
- 9) RC-V-13 (cicsed). {
,tm
$ 10) RC-V-14 (cicsed). [b RC-V-15 (closec). f' 11) b RC-CV-2 (9 o' clock). P
- 12) y.
I:.
i Install the ciluted gas sample octtle on the 7
ti b.
frcnt panel needle. 3 F
Cpen RC-V-13. b c.
b
- o. Open RC-V-12 and evacuate until RC-G-2.2 E indicates a minimum vacuum of 22 inches mercury. h.
@ Turn RC-CV-2 to tne 6 c'cicck positicn and h'I
$ e.
continue the evacuation until a rir.irum vacuum !
j of 22 incnes of mercury is indicated on RC-G- [-
2.2. [
h 5:
- f. Cicse in orcer RC,V-13 and RC-V-12. lJ E (
N g. Cpen RC-V-14 ano all ow the octtle to pressurize to approximatel y 1 psig as indicated on RC-G- [
2.2. {.
4 i U
- h. Clcse RC-V-14 7; i s p
}
r x
.~
- : .n c~ .. . . -
D
. . . .~ ~.
p
'd 5.
LE' y.
b.I r' .
y i.
LZP-1330-27 IN Revision 1 fj C March 19, 1982 y 11 pre {.
[7" i. Open RC-V-13 and RC-y-12 and evacuate until [-
RC-G-2.2 inoicates a minimum vacuur cf 22 inches f-if T mercury.
[.
b J. Close in orcer RC-V-13 and RC-V-12. [
P m
g k. Cpen RC-V-14 and allow the bottle to pressurize h to approximately 1 psig as inoicatea on RC-G- [F 2.2.
m t'
- 1. Cicse RC-V-14. I; rg 'n . Repeat Steps Fill.c tnrcugh F.11.1 trree times I
h; to remove all racioactive gases.
- n. Remove the sanipis cottle f rom the panel.
- o. Survey the sample bottle and dispose of as i directed by Rad /Cnem Supervision.
>C w.
s c. qs_ga u sis a
p
.- 1. None.
H. T((g lC( y g yFig TJONJ {fjRMC_jj, -
8 ';
- l. None.
h e(c l's E
E e t-E i-b.
i l
e
,a ?
t . -.
..._......._....a_.m.. -_.o
. ; : u _ a u.. sc a _. m - m _. __._ . . .__ _ .
._.u .~ . . .. . ,_
LZP 1330-2/
' Revision 1 1 ATTACllHENT A Hareh I'1,1982 1aSalle County Station 12 I IIRSS Analyses Date*
Conductivity LZP 1330-23 Dissolved Oxveen.LZP 1110-23 pH, LZp 1330-23 J ta nda rd iza t ion ,pH-41ni t / Time : Sample Init/ Time: Calibration luit/ Time:
Eccire. Water Temperature, C:
. Calibration Check init/ Time: 3,p , g .g.empe e r% "C:
tieasured Conductivity,umho/cm: Recirc. Water 0 Conc.,mg/l*
Heasured pil: (PH -7) 7 7* SamMc Init/ Time: ,
Correct the measured conductivity to Ituf fer pil Value: i Check SAT /llHEAT,1.1 0 pil units; 25" C using the following formula: Sample D.O., og/1: .,
l.
,'! Sample Init/ Time:
, Sample Temperature, "C: C , ,, C2-[0.018F(5.8E-5xTg)) _
1 + 0.018 (Tg - 25 C) Off-Cas LZp 1330-27 Hensured pil:
Vacuum, RC-C-2.1., Step F.I.d.h.
' II the sample pil > l.5, correct the pil to Where: Cg = Conductivity corrected to Pressure, RC-G-2.1. , S tep F. 2.t , t 25,C in accordance with the following 25 C - Pressure, RC-C-2.1. ,St ep F.2 y. l formula C2 - Hessured Conductivity T
ll pilt = pilg + 0.03 (Tg - 25)
Tg = Sample Temperature, C Sample Inlt/ Time: '
'i
'l Where: plir a pil corrected to 25 C Comments:
pilg = measured pII Tg s Sample Temperature, C t
h r-i D t e
I
' Reviewed:
ph at 25"C: Conductivity at 250C, umho/cm:
' I,R'f: FORH 1097A
!.u : $.3 $ S:$) f$UI k'$$ hb b bbkl $ BIN h b b b hhd b
- _ .._w... -
3 . p .. ..
'y LIP 1330-27
- Rsvision 1 March t9', 1932 e 13 I~ ATTACHMENT B
~
VALVE LISTING RC-V-1.1 Reactor Recirc Loop B Sample Cutout Valve r-- - RC-V-l.2 RT Demin inlet Sample Cutour Valve n;
"* RHR Loop A Sample Cutout Valve RC-V-1.3 RC-V-1.4 RHR Loop B Sample Cutout Valve .
h'
- 1. > '
RC-V-1.5 RT Demin Outlet Sample Cutout Valve RC-V-2 Sample Source isolation Valve
_ RC-V-3 Sample Purge Cutout Valve ;
(~ Flushing Water Isolation Valve a RC-V-4
- ~ RC-V-5.1 Pressurized Sample inlet isolation Valve .
- p. '
RC-V-5.2 Pressurized Sample Outlet Isolation Valve I,
I.' RC-V-7 Diluted Sample Bypass Valve
[ 5 RC-V-8.1 RC-SF-1.2 Inlet isolation Valve l
,r-RC-SF-1.2 Outlet Isolation Valve
~
RC-V-8.2 I. _L RC-EV-1 Isolation Valve i RC-V-9 i
n f El: RC-V-10 RC-EV-1 Evacuation Cutout Valve y RC-V-11 Off gas 4-way Valve h i
e2 RC-V-12 Argon to Air Ejector Cutout Valve f G, RC-V-13 Off-gas Vial Evacuation Cutout Valve :
Et RC-V-14 Argon Supply to Off gas Vial Cutout Valve .
Ly$ RC-V-15 Off-gas Sample to Gas Chromatograph Isolation Valve i
RC-V-16 RC-SF-1.2 Argon Purge Cutout Valve [
RC-V-17 Reactor Coolant Grab Sample Cutout Valve RC-V-18 Reactor Coolant Undiluted Sample Backflush Cutout Valve. +
pp ri
" Reactor Coolant Undiluted Sample injection Valve j RC-V-19
+
F RC-V -20 RC-C-1 Fi?1 Valve b.
RC-V-21 RC-C-1 Isolation Valve RC-V-22 Liquid Sample to CAP isc,lation Valve
. = -
--s- _ _ , _ -. --- , -.. .,.-,. - . - - _ _ , _ ---
. ~. -_ _
h y_ . ,
p
, t..!
b.. .- LZP 1330-27 [
,- - s Revision 1 fg
- March 19, 1982 E-ATTACHMENT 8 (Cont'd) 14. (Final)' E Q ,
l' F
e m 7 b '
RC-DV-1 Reactor Coolant Diluted Sample Injection Valve ' I.
E.
RC-DV-2 Off gas Sample injection Valve
}
U- Reactor Coolant Purge Throttle Valve (
RC-VREL-1 RC-VREL-2 Reactor Coolant Sample Throttle Valve W. .
l f .
'%fA i
g, .
?*
F.
T en g
s
- .?
b".
gw 4.:
g t
t i' .'
ky. i.g.
- r. 11 L
3
- f.e.
V E f PP, W+
bls b\
i 1 'V-
[' ,'
b g
I.
[
7 r 2 i e.
T I ,
u gg l l-e i
n a t.
~- - - - - . . . . , - . -
t h,.
- n. .
T.
-t
_g .
l
[
, UI.
f LZP-1330-26 L
.;g Revision 1 [
. Lt Parcn 19, 1932 [
1 l pp i
,,3 di SAMPLING OF PROCESS WATERS CONTAINIhG RADIOACTIVITY [
E AT THE HIGE RACIATION SAMPLING SYSTEP l-e.r..,
z..
i A. PURES_{
[L
,m g.g The purpose cf this procedure i s tc delineate a method {
Lw of obtaining samples of the crywell sumps anc FRSS waste t
[
tank at the High Radiation Sampling System (HRSS) curing normal and post-accident conditions. s
-]
sa B. REFERENCES L[
y n~ 1. Sentry Equipment Corporation, Post-Accicent Sample
{ System. Volume 1. }
t-t
- 2. LZP 1330-29, "Sampiing at tne High Radiation Sarr.pling i:
System (Valve Operations at the HRSS Valve Control [
Q'd Panel)." {
s W 3. LZP 1330-31, "HRSS Sample Movement." 7 g !; ,
AAIS-CCP-0001, " General Radionuclide Analysis of a f 4.
Liquic Sample". [
Q ,-
12 LCP 410-1, " Preparation of Samples for Garma Ray [
5.
Spectror.eter M.easurements." {
g f N C. PREREQUISEfj f, -
- 1. The operator s.icula be familiar .vith tne cperation [
t
=
}'
of the HRSS panels. [.
I-
- 2. Establish ccmmunications witn the Unit huclear [.
9 g Station Operator (NSO). {.
l l 3. Equipment: 7 i
- a. Reach rocs. f g.
i
- o. Sarple cart / cask assemoly. ;
l d[U c. Sample bcttle witn septur, 15 r.l. L Q* d. Needle flusn tool with cemineralizec =ater [
- filled sample bottle and Septur. [
t 7,
n ,,5 h
a g ~
. . ~ .
< - , . - ~ . . . _ _ . . _ _ _ _
I O
> f.V' s h O"E l
I!
- r. '
e
- p LLP-1330-28 E Revision 1 March 19, 1982 fn 2 I' p./
p b} e. Shi el ded Syringe assembly. I L
L The sample rust nave been obtainec in accorcance te PP Eg, 4.
with Ref erence 2 prior to pe rf ormi ng tni s procecure. [
E
- 5. Ensure nitrogen pressure, approximately ICO PSIG, (L 3-- is available at the Liquid Sampling Panel (LSP),
t
- OPLOBJ. h p"
q h.
- ~ D. PRECAUTIONS
\; ,
- 1. A Regulatory Guide 1.3 or 14 release of fission gy procucts implies extremel y high levels cf h
((
radioactivity. Dose rates may De high encugn to [
p prevent entry into mar.y areas of tne plant tnat are ncrmall y hab itabl e. Rad / Chem Supervisicn should De {
,VZ contacted pricr to entry into any area when such a Le release of fission products is suspectec. y E
wear raciation dosimetry as reccmzended oy Rac/Cnem t.
77 2.
Supervisicn. (
3 h$ kL ry 3. Wear protective clotning and respiratcry prctection as recommended by Raa/ Chem Supervision.
{p
- 4. Appropriate survey instr uments shcul d De available . . ,
for monitoring curing this prccedure. f
((
tiW
- 5. The splash box coor of the Liquia Sample Panel (LSP), I OPLC8J, must be closeo curing panel line purge and pg.
gg-grab sarple cellection operations. (
f 5
E. LIFITATIONS AND ACTIONS P
.J L W l. Notify Rad / Chem Supervision if any prcblers are F encountered at tne HRSS panels.
l
- 2. This procedure, though intended fcr use unoer post-accident conditions, can be usec for sampling at L the HRSS panel curing normal cperations, curing which the precautions listed may have limited F
((n E applications. However, no rmal routine sanpling 1
precautions thould be ooservec. b r F. f ECQ DSR,j
- 6 .
r.
ry bb e
ki E
)
A '
-., .- _ . ,, --~ .
s 7
5
, , . - . .. . , ~ . . . ,
"z. .
i w
V;O N ,- ;
- u. ',
Ri' LZP-1330-28 Revisicn 1
' @3 Marcn 19, 1982 ;
3 5, r,c ,
i r !'
wd. - g For the neun nar.es associatec with tne valves operatec FJ
[AU in this procacure, refer to Attachment A. [
37 1. Perform the fc11owing valve lineup at tne LSP, '
OPLD8J*
'.6 }_. (
- a. RW-V-1.1 (closed). !
> c:: i F
64, o. Rw-V-1 2 (closed). e p%
p.
r c. Rw-V-1 3 (closod).
LI't
- d. Rw-V-1.4 (closeo). 3 C) e. Rn-V-1.5 ( cl osec ) .
BR '
- f. RW-V-1.6 (ciosec). ;
I .
b [g~3 g. RW-V-1.7 (closed). l l
- h. RW-V-1.8 (closed). -
,,[_
U L2 i. RW-V-1.9 (closeo). !.
pj j. RW-V-1.10 (closeo).
C k. RW-V-2.1 (closed).
rr -
- 1. RW-V-2.2 ( cl ose d ) . -
g] I
- m. RW-V-2.3 (closed). i.
l I,I, i RW-V-2.4 (closed). I' Lm-
" n.
pn o. RW-V-2.5 (closed).
[
" d'
'l
- p. RW-v-2.6 (closec).
m kf q. RW-V-2.7 (closec). ,
Lt t'
- r. RW-V-2.8 (closed).
me 3 r
N; s. Ra-V-2.9 (closec). s
- u. .
r!' l LL i e
i-
[- t:
? I 02
. _ _ - - . - - - . . ~ . . . .
p2- !
c.
7,. .'
L.
p.
LZP-1330-28 ,
Revision 1
{" i*arcn 19, 1982 ,
4 kb :
00 t. RW-V-2.lC (closed). i I
e u. Rw-V-3 (closed).
"" v. RW-V-4 (closed). .
{3 w. RN-V-9 (cicsed).
ils l
- x. RW-V-10 (closec). t s
~
- ,j y. RW-V-6 (closed). ,
yy z. RW-V-5 (6 o'ciccx). s E- aa. RW-V-7 (BYPASS).
PP ao. RN-V-8 (BYPASS). i N: '
c-
- 2. Connect the flush water nose to Rh-C-1 cn the LSP, y ,s OPLC8J, and open tne flush mater line valve. ,
- 3. To ootain a diluted (1000:1) racicactive waste i I
sample, Lioceed to Step F.6. Tc cotain an uncilutec 75 (15 mi) radioactive waste sample, proceso to Step $
, b5 F.5. If neither, proceed to Step F.4. 1 t
i
- 4. To cDtain an cpen grab sarple, prcceec in accorcance L with the following at the LSP, CPLD8J or as otnerwise ;
l directcc: t CAUTION ,
ff.
The splash box coor of tne Licuid Sample Panel (LJP), f OPLC8J, must be closec curing panel line purge anc j i:s
($, grao sarple ccliection operations. t I
- a. Cpen Rh-V-1.1 (-1.2, -1.3) depencing on tne {g n sarple scurce, anc recirc for a ririnur cf six i
'd minutes, then cicse Rw-V-1 1 (-1 2, -1 3). [
l l
j.
D. Cpen Rh-V-2.1 (-2.2, -2 3) depencing on the j r
Cy sarple scurce. ;
j bC r
- c. Sicwly opcn Rd-V-4 until RW-FI-l indicates 4- ,
p, Purge to waste fcr a minimum i'
- e 8 inches of. water.
of one (1) minute.
Open Ra-V-e, purge a minimum of 50 ml of liquic f l {" L.
c.
to waste, then close Rh-v-c. i t
?
It.: A
..e-..m.-., w .
t vs - .
l.S *
. .f-6u
, 'e ni .
k?'
+>
E k
m LZP-1330-28 fr hIi
"# Revisicn 1 [
Marcn 19, 1962 g c,. v.
5 j,
un
- e. Cpen the splash cox cocr and place tre sample g bottl e under Rw-V-6. Then close Pe splasn r;
[4 box coor. ie LO f.
pp f. Open Rh-V-6, collect the cesired sampl e , and I cicse RW-V-6. y gg $
- g. Cl o se RW-V-2.1 ' (-2. 2. -2. 3 ) cepenaing on tne ,;
FE sample scurce. ,
L N$
- n. Cicse Rw-V-4. Open tne splasn ocx dcor. :(
y U2 Dry the sample bottle, remcve anc place in a i
(( i.
tote tray for transpcrting tc tne laboratory. E v.
Cicse tne spl asn oox acor. ;
V 0,;; '
i-
%f J.
At tne Valve Contrcl Panel, CPLC9J, secure tne sampling lineup in accercance witn Reference f T 2. Steps F.2.c.15) tnrougn F.2.c.17) OR Steps [
g }gg F.3.f tnrough F.3.g cepending cn tre sample {<
source sampled.
- k. Fully cpen Rw-V-4.
- 1. Sicwly open RW-V-3 until Rw-FI-l incicates *-
8 incnes of water. Flush with cemineralized ,
Eg gb water for a minimum cf two (2) minutes. [:
[
- m. Cicse RW-V-4.
Ei n. Coen Rh-V-1.1 (-1.2, -1.3) cepenair.g on tne sample scurce samplec.
cc kh o. Fully cpen RW-V-3 anc flush witn cemineralizec "
water for a minimum cf six (6) minutes.
bh p. C1cse Rw-V-1.1 (-1 2, - 1.3 ) . p" La
- o. Cpen Rh-V-2.1 (-2.2, -2.3) cepencing on tne sample scurce samplea.
E5 i bi r. Sicwl y open Rn-V-4 antil Rh-FI-l reacs 4-6 rn incnes of water. Parge to waste fcr a minimum 3_
[
of two (2) minutes.
hh i
- s. Caen Rh-V-6 purge a minin.um of 50 mi cf liquic to .aste, tnen close Rw-V-6.
i t
EI !
b.' l
't I~,
- I I,
m I 1 L
.- r
?
- f' LLP-1330-28 f L
- 4 Revisicn 1 p March 19, 1982 t i
6 in l G f' i
- t. Close Rw-V-2.1 (-2.2, -2.3) anc RW-V-4. f, e.
c' w At the Valve Control Panel, CPLC9J, align tne r B6 u.
d- LICUID SAMPLE BACAFLUSH switch, for rac aste i side, to the oackflusn line associated with
.p7 tne sarple source sarpl ea. Flust witn (h
' by - cemineralizea water for a mirinun et six (e) minutes. ,
hk v. Align the LIQUID SAMPLE BACKFLUSH switen to f
'* tne CFF position. (
h o
.. Close RW-V-3. L
&[9 x. Cicse the flush water valve anc cisccnnect the f flush water line from RW-Dv-1. {
?
N y. If nc further samples are to os cotained from !
this sample source, secure tre sampling lineup I .-
I in acccrcance witn Reference 2, Steps F.2.c.19) t QE througn F.2.c CR Step F.3.i cepending on tne I bd [
sample scurce sampleo.
11
-5 f
$n 5 To ootain an u'ncilutec (15 al) racicactive waste
"" sample, proceed in accoronace with the following at h the LSP, OPLD8J or as otnerwise directec
[l-'
L+# a. Place the tottle on tne cart / cask assemoly
I cavity piston.
Turn the direction valve for the nydraulic '.
o.
pisten in the DOWN posi tion anc lower tne cottle [
in the cask cavity. r la u c. Cicse anc cpen tne cask to verify tnat the cover is acrking properly.
- d. Positicn the cask / cart under tre LSP undiluted radwaste fill station needles anc set tne craxe. 4 E
l' -,
k Turn tre direction valve for the hyaraulic i.f k"
e.
pisten tc tne UP position anc raise the Dottle ento tre neeales.
Mb t. Cpen Rn-V-1.1 (-1.2. -1.3) cepencirg on tne f i
saaple scurce, anc reci rcul ate f cr a minimum [
l gp cf six (6) minutes.
U2 1 E5 r V
l ~ _;.; - _ _
_.m _ . . __ m .m _, - _ .
. rT : e k[-
h i-r t n-t t:
P i
r LZP-1330-26 "b Revisic7 1 b Marcn 19, 1962 b F- 7 O
- g. Cicse RW-V-1.1 (-1 2, -1.3 ) anc cpen Rw-V-2.1 pp (-2.2, -2 3) depencing on tne sanple scurce. [
e, u Sicwly open Rw-V-4 until Rh-FI-l inoicates *- E
- n. '
r, 8 incnes of water. Purge to waste fcr a minimum of one (1) minute. (
bu
- i. Turn Rh-V-7 to SAMPLE. CD NCT exceec 20 psig [
on RW-G-1 in this step. Adjust Rw-V-4 until f (P
[t Rw-G-1 indicates 20 psig or Rw-FI-1 incicates [
10-14 inches of water. Purge for a nininum cf er one (1) minute.
p g.
$".m J. Clcse Rw-V-2.1 (-2. 2, - 2. 3 ) . f Let Rw-G-1 return to O psig anc wait 3C seconos fh k.
to allow the cottle to cepressurize. [
es t
5 r,g
- 1. Turn Rin-y-7 to BYPASS. f L
$5 m. Turn the direction valve for a cask / cart g ,,
hycraulic plunger to the DCnN positicn and lower the cottle inte tne cask.
g
- n. Close the cask. Release the Drake ard remove ;
the cart / cask frcm the sample station.
pg kt Install ano secure tre auxiliary srielo en ene o.
l cart / cask assemoly. ;,
- n
~
- p. Install ano secure tne neecle flust toci on tne LSP, OPLO8J. 2 o
n I d? At the Valve Control Panel, OPLC9J, secure the q.
J sample lineup in accercance witn Reference 2, f Steps F.2.c.15) tnrougn F.2.c.17) CR Steps f p,
g}
F.3.f tnrough F.3.g cepending cn tre sample '
source sampled.
- r. Fully cpen RW-V-4.
- s. Si cwl y open Rw-V-3 until Ra-FI-l ir.dicates 4-pa 8 incnes of water. Flush witn cemineralizeo b f: water for a minimum cf two (2) minutes.
At
- t. C1cse Rw-V-4.
pr.
I/S u. Cpen Rw-V-1.1 (-1.2. -1.3) cepencir.g on :ne sample scurce.
,yG.
_t-f; p ..
r f?
I>
V F
e L
r
~
' Aevisicn 1 ,'
Paren 19, 19c2 ,
- 8 'r s .
,o
- v. Fully open RW-V-3 anc flush witn cemineralized ..
e water for a minimum cf six (c) minutes.
r:
- w. Cicse RW-V-1.1 (- 1. 2, - 1. 3 ) .
[ '. x. Cpen Rh-y-2 1 (-2.2, -2.3) cepencing on tne '
D. sample scurce.
Si cwl y open Ra-V-4 until Rw-FI-1 reacs 4-8 e y.
incnes of water. Purge to waste fcr a minimum 7-p '-
of two (2) minutes. '
t
- z. Close Rw-V-2 1 (-2.2, -2.3) anc Rw-V-4. {
aa. At the Valve Centrol Panel, CPLC9J, align tne !
r" LICUID S AMPLE B ACAF LUSH switch, for tne racwaste sice, to the oackflusn line associated with L the sarple source samplec. Flush witn fp cerineralizec water for a rir.imum cf six (e) ,
e minutes. 3 J
L-aD. Align tne LICUID SAMPLE BACKFLUSE switen to (
tne GFF position. F C* '
S CO NCT exceec 20 psig ac. Turn Rh-V-7 to SAMPLE. g e
en RW-G-1 in this step. Slowly cpen Rw-V-4 no until Rw-G-1 incicates 2C psig or Rw-FI-1 [
-(( incicates 10-14 incnes of water. Purge for a 1" mir.imum cf one (1) minute. %
r
nu Q. ac. Cicse RW-V-* anc let RW-G-1 return tc C psig. {f se.
wait 3C seconos to allow the octtle to ,r. .
- cepressurize.
ae. Turn Rh-V-7 to BYPASS. E at. Secure flusning cy closirg Rh-V-3 f:f.
L k ag. Cicse the flush water valve anc cisccnnect the f lush water line from Rw-DV-1. k pf -
t
~
Yf an. Remove the neeole flusn coci fror tne LSP, p I
CPLD8J.
r- i A ai. If nc turther sarples are to os cotainec froe "
tnis sample source, secure ene sampling lineuo h in accercance itn Reference 2, Steps F.2.c.19) [
!L tnrougr F.2.c CR Jtep F.3.a cepercing on :ne i sample scurce samplec. [
r L_ ,1
- -.i.
o4 ,-- - - - - - . - - ., - , .
?
- l. ~
e k
LZP-1330-28 !.
Revision 1
.Maren 19, 1982 ((
F#
5 h
i
- 6. To ootain a diluted (1000:1) radicactive waste p sample, proceso in accorcance witn the folicwing at i.
e the LSP, CPLD8J or as otherwise directec:
- b.5
- a. Verify Rh-CV-1 is turnec to BYPASS. Fill I reservcir Rw-R-1 witn cemineralizec water.
Open RW-V-10 and tnen RW-V-9. Acjust reservoir
[y
((p -
RW-R-1 until the water level in graduatec [
cylinder Rh-C-1 is 125 ml. Cicse RW-V-lO anc g O' Rw-V-9. 3 f
$N. 8 D. Align Rw-V-8 to the BYPASS (9 c'cicck) pcs i ti on.
p*' ,
Q; c. Align RW-DV-1 to tne BYPASS positicn. .
- c. Insert the neecle of the nano cperatec vacuur i
,y *
{De pump inte the septum of the cilutec racwaste L" sample Octtle. g-I
- e. Evacuate to tne maxieur vacuum acnievaole witn
>.;,i{} tne nand operated pump. The vacuur PUST oe at LEAST 15 inches of Hg. ,
- f. Keep the hanc operated vacuur purp ccnnectec [
3 '
to the evacuateo cottle for tnree rirutes to
- ssure that the cottle retains the vacuur. ;
e
,v.I? t.
La g. Remove the Dottle from the hanc cperated vacuum pump and place the octtle on the cart /casx {g assemoly cavity piston.
gy {.
LM
- h. Turn the direction valve fcr the nydraulic f i
pistc. to the DOWN posi tion anc lower the cottle {
g into the cask cavity. Close ana open tne cask
- k. to verify tnat the cover is working properly. f[
p
- i. Position the cask / art under the LSP dilute 0 f F}J} racwaste fill station neecle and set the oraxe. (
O
- cy j. Turn the cirect on valve (cr the nyaraulic l pisten tc the UP posi ti on anc r ai se tne cottle {
bk*?p onto tne neecle. S
"? x. Cpen Rh-V-1.1 (-1.2, -1.3) depencing on tne
[e sample scurce anc racirc fcr six (6) minutes.
Cicse RW-V-1.1 (- 1 2, - 1. 3 ) .
l rv 1. Caen Rh-V-2.1 (-2.2, -2 3) cepencir.g on tne fe '
L" sanple scurce.
7:
i' b2
5.
. "S o -
L t t f'.
.- I ge ;
ki
[
t (e- I M LZP-1330-28 u Revision 1 ,
Marcn 19, 1922 ?;
yg E3 Il
- m. Sl owl y open Rw-V-* until Rh-FI-L incicates 45- 6
?
50 inches of water. Purge tc waste for a e 7t U) minimum of one (1) minute. 1 O'
s
- n. Turn Rh-V-8 to BYPASS. r I
i
- o. C1cse RW-V-2.1 (-2.2, -2.3). g V
D. At the Valve Control Panel, CPLC9J, secure the r(
ax sample lineup in acccreance with Reference 2, !
Steps F.2.c.15) tnrough F.2.c.17) CR 5teps ;
F.3.f through F.3.g cepending on the sample ;
9 '
i" source samplea.
E
- q. Fully open Rw-V-4. t j
S r. Sl owl y open R w-V-3 unti l Rw-FI-l indicates 4- l' 8 inches of water. Flush witn demineralized y Fr ~
water for a minimum cf two (2) minutes. [
YC LN
- 5. Cicse RW-V-4.
b
- t. Cpen RW-V-1 1 (-1 2, -1 3) cepencing on tne j
]'[ sample scurce sampled. Fully cpen Rh-v-3 and {
flush with cemi ne ral i zed water fcr a minimum ;
7! of six (c) minutes.
61 (
- u. Cicse Rw-V-1.1 (-1 2, - 1. 3 ) . *<
g.
! v. Cpen Rh-V-2.1 (-2.2, -2.3) depencing on tne sample scurce samplec.
{
- w. Slowly open RW-V-* until RW-FI-l reacs 6-8 k
?? Flush witn demineralizec f.
$2 inches of water.
l water for a minimum cf two (2) mi nu te s . j' L 0 Close in orcer RW-V-2 anc Rw-v-4. f f x.
At the Valve Centrol Panel, CPLC9J, align tne i.
- y. {
LICUID SAMPLE BACKFLUSE switen, for tne racwaste i
-3 i I
sice, to the backflusn line associatec .itn ,
the sample source samplec. Flusn witn ;
ceniceralizec water for a mininum cf six (6) 8 mirutes.
?.) :
i i z. Ali 9n the LICUID SAMPLE EACKFLUSP saiten to i - or 08 the CFF position.
j i as ,
l FU !
! bb l
r p
r* *1 _o_ . _ _ . . . _ _ _ _ _ _ . . . . _ - _ . _ _ . _ _ _ _ _ . _ . _ _ . _ . _ _ _ .
.n g
V
. V
,g . .
7 s-. ~
b 3
- p? LZP-1330-28 .
O, Revision 1 March 19, 1982 f
e ra b 11
.D7
.sc r
aa. Turn Rh-CV-1 to SAMPLE.
.ea r-cs an. Crack open Rw-V-9, ano aco 24 el of water trem l' Rw-C-1 tc the sampl e Octtle, then cicse Rw-V- n.
9* F t
[ ass pV L2e U.9.T,,) e nn: The dilution volume may De changea as directec oy [
[y ld Rad / Chem Supervision. h E
p ac. Turn Rw-CV-1 to SYPASS. {
t ld Place the airection valve for tne hycraulic 6 ac.
plunger in tne DOWN position and Icwer the [
m Dottle intc tne casx. j T
Lu/
o ae. Close the cask. b, p[ af. Turn Rh-V-8 to the 9 o' clock pcsition. {.
{~
ag. Sicwly open RW-V-* until RW-FI-1 indicates 45-r3 50 inches of water. Flush with cerireralizec gDi! t water for two (*2) m i r.ut e s .
b
" ah. Turn Rh-V-8 to SYPASS.
[N <
us al. Secute flushing by closing RW-V-4 anc RW-V-3* ry aj. Release the Drake and remove the cart / cask from h-l the sample station. {
ak. Install and secure the auxiliary shielo en the ,(
e cart / cask assemoly.
al . C1cse the flush water valve anc cisccnnect the h m flush water hose for Rh-CV-1.
~
l{ -:
P l
am. If nc f urther samples are to os cDtained from this sample source, secure the sampiing 1ineup [.
> h'* in accercance witn Reference 2, Steps F.2.c.19) [
through F.2.c CR Step F.3.i cepencing en the 'p t
, GF sample scurce sanplac.
l kb i 7. Transoort the samples to tns sample preparaticn area ,
itn Reference 3. f.
~
,.y in accoraance
, t. c
! " Prepare tne sample from Step F . e: for analysis in }
8.
accorcance witn the f c11 ow i n g : (l'.
[# t i
~. . . ~ . - - .
e.
f ~r O o . _ _ . . _ . . ._ .-
n e:
til f
. E,
}f O
r.
t.
L m
LZP-1330-28 l-
.< Revision 1 Marcn 19, 1982 {(
y r-12 >
\t G2 y
- a. Place a 47 mm fiber filter in a new petri-cisn ana place Denind a shielced area with tne cover P[
'Qg4 off.
- f. ,
m MH f If less than 500 ul (C.5 mi) cf sample is usec, h campen tne fiber filter with ceionizac mater prior d.
to placing the sample on the filter. f;;-
i.J
- b. Remove the small shielo plug from tne top cr @
the shield cask. [
9 '.
3] ~
- c. Using tne syringe assemoly, withcraw 2C ut of 7 the Sample and imneci atel y replace tre shiel e e plug. ;
Tj7 7
r
$3 9 kv-
>N Sample volume anc geometry may De changed at the t g ciscretion cf Rad / Chem Supervision to facilitate j analysis of samples.
g.
g@
- a. Discharge the sample onte tne fiber filter in .
fl tne petri cisn in sucn a manner that the sample [p is eveniy depositec cver the entire ficer fiiter
.g;l surface. g.
's
- e. Place the cover en the petri dish anc tape it i clcsed.
- f. wrap the petri aish in plastic wrap ano seal I" E
D 9
Lacel the sample in accordance with sne following: T
- 1) System samplea and sample lccation. -
- 2) Time of sampling.
- 3) Date of sampling.
' l'.
fi.ll~
- 5) Initials.
k i
4
- a w. jew e - ag -e , -6
, = - - - - - -
t
- 0. s . . e_ - . . _ _ _ . _ - . _ _ _ . _ . _ _ . _ _ . _ _ . _ _ __ .- .
{b ,
fC, . ,
1.,. o L2P-1330-28 Revision 1 ,
Marcn 19. 1982 ;
ct L 13 p,_st ,
- 6) Survey results. .
W The sample volume for undiluted samples is tne same [.'
-D$
- 9. s as the syringe volute dischargaa. For a cilutec eg, sample, calculate the actual volume of sample on i ip the fi1ter paper in accorcance with tne fc11o ing: f
ue V = 52# ,
T
@' 1<
CA:
where: V = The actual volor.e of tne rad-waste ?
sample to oe analyzed on the fiber [
g)
,N filter in ml . p w.
5 = The vol ume o f the dil uted sample ;"
cm in tne syringe in ml.
p.
a y
A = The val ve al icuot of sample ccliecteo
[I 7
rv: in the casx bcttle in ml. ;
a.
- " T = The total vclume in the cask k Dottle, the valve aliquct of [
samp,le plus the . vater acced from k h['$
0 the graduateo cylinder in ml. [t y 10. Analyze the sampies in acCorCance with Reference 4+. t
'h w
- 11. Report the sample resul ts tc the Rad / Chem Di rector (i for evaluation. ['
w t
@ ~
- 12. Route all output data and calculaticns to Rad /Cnem [
- f. '
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Revision 1.
March 19, 1982" ATTACHMENT A Ifr (Final) ;
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i VALVE LISTING RW-V - 1.1 Spare '
RW-V -1. 2 Spare t f_'
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RW-V-1. 5 Spare m RW-V-1.6 Spara j,
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RW-V -1. 9 U-1:Drywell Equip. Drain Sample Recire Valve }*
h,, RW-V- 1.10 U-2 Drywell Equip. Drain Sample Recirc Valve ,
Le; RW-V-2.1 Spare g RW-V -2. 2 Spare g.
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- (.'" RW-V-2.A RW-V-2.5 Spare [
RW-V-2. 6 Soare F. RW-V-2.7 Spare [
h RW-V-2.8 HRSS Waste Tank Sample Cuteut Valve -
RW-V -2. 9 U-l Drywll Equip. Drain Sample Cutout Valve f
,e RW-V-2.10 U-2 Drywll Equip. Drain Senple* Cutout Valve L RW-V -3 Flushing Water isolatit:rt Valve it RW-V -4 Rad-Weste Sample Throttle Valve
. RW-V-5 Backflush Cutout Valve {-
RW-V-6 Radwasta Grab Sample Valve .
1 RW-V -7 Radwaste Undiluted Sample injection Valve ?
RW-V-8 Rad-Watte Diluted Sample Cutout Valve E RW-C-1 Fill Valve S 7 RW-V-9 '
A RW-V -10 RW-C-1 Isolation Valve '
l RW-DV-l Rad-Westr Dituted Sample injection Valve s
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