ML20053C445

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Public Version of Revised Lzp Procedures,Including Procedures Lzp 1330-25 Re Sampling of Reactor Coolant at High Radiation Sample Sys & Lzp 1330-26 Re Sampling of Containment Air at High Radiation Sampling Sys.Index Encl
ML20053C445
Person / Time
Site: LaSalle  Constellation icon.png
Issue date: 03/19/1982
From:
COMMONWEALTH EDISON CO.
To:
Shared Package
ML20053C431 List:
References
PROC-820319-04, NUDOCS 8206020151
Download: ML20053C445 (66)


Text

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. I INDEX PAGE y  ;

f7 8/17/81 LZP i Wi REV. AEV OATE CISAETT{

PROC. No. TITLE

[

.. t

.u 03

  • i.ZP- 1330-24 DETERMINATION OF REACTOR COOLANT 00 to/8l i HYOROGEN C0t* CENTRATION AT THE HIGH (

s RADIATION SAMPLING SYSTEM h

Lu 03 V

LZP 1330-25 SAMPLING OF REACTOR COOLANT AT THE HIGH Qi ,

3/D l m

Pr; RADIATION SAMPLE SYSTEM 'f

$ 01 3/gd 03 f MZP 1330-26 SAMPLING OF CONTAINMENT AIR AT THE HIGH RADIATION SAMPLING SYSTEM 1330-27 SAMPLING OF REACTOR COOLANT OFF-GAS AT Of .3/g;) 03 f' QZP 5 b THE HIGH RADIATION SAMPLE SYSTEM h 01 3/ 85L 03 {

6.ZP 1330-28 SAMPLING OF PROCESS WATERS CONTATNIMt D_AnIn_

i

. 'r ACTIVITY AT THE HIGH RADIATION SA'iPLING SYSTDi 03 1330-29 SAMPLING AT THE HIGH RADIATION CO 0/00 }

~l 2 P &

SAMPLING SYSTEM (VALVE OPERATION AT T THE VALVE CONTROL PANEL)

D bR a /61 03  !

TR Ar.SFER OF W ASTE FROM THE HRSS WASTE 00 LZP 1330-30 >

TANK AND WASTE PUMP f:]

[j?.ZP 1330-31 & 50 See next pace '

IMPLEMENTING PROCEDURE FOR FIRE: Of 9/B/ 02  ;

LZP 1390-1 FIRE MARSHALL 0I 9/6/ 02

%.ZP 1340-2 IMPLEMENTING PROCEDURE FOR FIRE:

FIRE CHIEF (OESIGNATED Sr11FT FOREMAN) ,

F7?

b2P 1340-3 IMPLEMENTING PROCEDURE FOR FIRE: 01 9/6/ 02 [

FIRE OFFICER ::1 (COGNIZANT MAINTENANCE i-m FOREMAN)

% 0t 9/8/ 02

$2P 1340-4 IMPLEMENTING PROCEDURE FOR FIRE:

FIRE BRIGADE t

01 8/81 02  !

.i. Z P 1340-5 IMPLEMENTING PROCEDURE FOR FIRE:

FIRE COMPANY NO. 1 (MAINTENANCE PERSONNEL) h q t.

R 03 7/81 02 i~

" LIP 1360-1 PROTECTIVE MEASURES FOR ON-SITE PERSONNEL r  :

% USE OF POTASSIUM IODIDE (KI) AS A 00 7/61 03 t-RZP 1360-2 THYROID BLOCKING AGENT

$ZI' 1360-4 SEE NEXT PAGE RESCUE 00 10/80 02 h

@ZP 1370-1 t 01 11/80 02 g.Z P 1370-2 ' RSONNEL INJURIES ,

FIRST AID, OECONTAMINATION ANC 00 10/80 02 ZP 1370-3 EVACUATION Cc EXPOSED AND/OR t

er CONTAMINATEC CASUALTIES t k**

& on CONTROL OF OIL SPILLS CO 10/80 02 f LZP 1 8206020151 820525

[.

t-PDR ADOCK 05000373 F P_DR p #,

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b LZP-1330-25 [

Revisicn 1 Maren 18, 1982 j[

1 .! .'

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SAMPLING OF REACTOR CCOLANT AT THE HIGH RADIATION SAMPLE SYSTEM l p  ;-

li i A. PgSj ('

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d." The purpose of this procedure i s to celineate a metnoo of obtaining liquia samples at the High Raolation Sample f::

g System (HRSS) during normal anc post-accident operations, [

y incluaing grad, diluted (1000:1), and unciluteo (15 mi) samples. g e

s B. REFERENCES [

[}' t

1. Sentry Equipment Corporation, Post-Accicent Sample i b

System, volume 1. ,

r LT 93

2. LZP 1330-29, "Sampiing at the High Radiation Sampiing  ;

I System (Valve Operation at the HRSS Valve Control {i f

,_{ {..

Panel)." (

3. LZP 1330-31, "HRSS Sample Movement." .
4. AAIS-CCP-0031, "BWR Coolant Radionuciide Analysis." h' b

LCP 410-1, " Preparation of S4mples for Gamma Ray o 5.

Spectroireter Neasurements."

C. PREREQUISITES [

1. The Operator should be fami1iar with the cperation of the FRSS panels. t I-
2. Verify tnat nitrogen, approximately 100 psig, is
  • availaole at the Liquid Sampling Panel (LSP), OPL0dJ.

t.

3 Establish communications eith the Unit Nuclear [

(' Station Operator (NS0). lE 1 f

4. Equipmen**

y b-

a. Clean one liter polyetnylene octtles witn caps. [v.

4 m

O D. Paper towels. l' 4.

c. Plastic cr ruoner gloves.

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'b  % - -~.,. . ,

7 n__.

....m. , . _ , , _ __

,-, G ~. . . a _i. . u..a. . _ _ , _ . . _ _ . . . _ , . . . _ _ ,

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  • t LZP-1330-25 I; V

'k" Revisioni March 18, 1982 ij 2 L

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a. Sample tote tray. ((-

k

e. Survey instruments, as appropr i ate. 1 e

e

f. Shielded syringe assembly. -

b-N The sample must have been obtained in accordance I l'n' 5.

k

  • with Reference 2 prior to performing this procecure.

h g{T D. PR,ELAUTTOM f.

k,

1. A Regulatory Guide 1.3 or 1.4 release of fission i;
k. proaucts implies extremely high levels of #'

L radioactivity. Oose rates may be high encugh to prevent entry into many areas of the plant tnat are 6 normal 1y habitabie. Rad /Cnem Supervision shoulo De E p contacted prior to entry into any area unen such a f';

b release of fission products is suspected. F.

J

, e wear raciation dosimetry as reccmmenced Dy Rac/ Chem  !;

.t 2. K Supervision. '

3. wear protective clotning and respiratory protection F.#is as recommended by Rad / Chem Supervision. (f h

E

n. 4. Appropriate survey i nstr uments shoul d De available h, e for monitoring curing this procecure.

. . s., '.

5. The splash box door of the Liquid Sample Panel (LSP), f.

OPLD8J, must be closec during panel 1ine purge and j.

%, g En grao sample collection operations.

h

[

z E. LIMITATIONS AND ACTIONS b i #

l. Nctify Chemistry Supervision if any proclems are >

encountered at tne HRSS panel s.

'b

2. This procedure, though intended for use uncer post-accident conditions, can De usea for sampling at

{c T

T the HRSS panels during normal operaticns, ouring 6 which the precautions may' nave limiteo applications.

However, normal routine sampling precauticns snould ce ooserved. F.

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II LZP-1330-25 Revision 1

{ March 18, 1982 3

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b b.911 .

53 For noun names associated with the valves operatec bN in this procecure, refer to Attachment A.

l. Verify the following valve lineup at the LSP. OPLO8J' .

(('

ut

a. RC-V-1 1 (closed). {

n?

o. RC-V-1.2 (closed).

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c. RC-V-1.3 (closec).

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(d'n c. RC-V-1 4 (closec).

  • 7 e. RC-V-1 5 (closed).

6

f. RC-DV-1 (BYPASS).

I PI g. RC-V-19 (8YPASS).

2. Connect the flusn water nose to RC-C-1 at the LSP, y gp OPLD8Je and open the fl ush water valve. l L

p~b

3. To ootain a dilutec (1000:1) reactor coolant sample, proceed to step F.5. To ootain an uncilutea reactor s coolant sample (15 ml), proceed to step F.4. To l obtain a reactor coolant grac sample, proceec in i.

l accordance with the following at tne LSP, OPLO8J or i na as otherwise directed: r gi a. Verify the following valve lineup:

f l

1) RC-V-5.1 (closec). .

h(

as g

2) RC-V-5.2 (closec). r s.

59

(( 3) RC-V-17 (closed). f._

i

4) RC-V-17 (closec). y gy I

3-.

ch 5) RC-V-4 (closec). [.

r pf 6) RC-V-ll (closec). [h i

Ch  !

7) RC-V-9 (closec). i' i
19. ,

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.. _ . _ _ _ _ _ . . _ . . L .c. . ___1 __. .. 2 _

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... . _ - . _ - _ . _ _ _ . . _ _ . _ . . _ . . _ _ _ t ,

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' " LZP-1330-25

. t.

Revision 1 Marcn 18. 1982 4

C# ,

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8) RC-V-8.2 (closeo).

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9) RC-V-8.1 (closed). a

- 6/  ;

10) RC-V-16 (closed).

p.

~ h.. 11) RC-V-18 (6 o' clock).

12) RC-V-22 (TO WASTE). r

, 7, .

00tain the sample in accordance with the b LL b.

following: ,

j', .. t s 1) Open RC-V-3.

- 2) Open RC-V-2.

  • f U 3) Select one of the sample sources ano open its' corresponding valve, RC-V-1.1 (-1 2, ,

+

b -1 3, -1.4, -1.5).

,E , t Lu

4) Slowl y open RC-VREL-1 until RC-FI-l reaos  ;

35-40 inches of water. Allow tc purge

m. - -

b for a minimum of five (5) minutes. >

b L2:

5) Sl owl y close RC-VREL-1 until RC-FI-1 reacs 5 12-15 inches of water. Continue tne purge b

((

for a minimum of one (1) minute.  !

bd I.

pp 6) Cl ose RC-V-3. {,

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7) Open RC-V-7.
5. 8) Slowly open RC-VREL-2 until RC-FI-2 reaos ,

W 18-22 inches of water. Allow tc purge f-l for three (3) minutes. l-1 l !%

l

(( 9) Align RC-V-16 to the 3 o' clock position. [l

10) Open RC-V-17, acjust RC-VREL-2 until RC-  ;

fr A FI-2 reacs 18-22 incnes of water or RC-G- 1 f

EU 3 reads 20 PSIG. DO NOT exceed 20 PSIG f on RC-G-3. Allow tC purge for two (2)

~ minutes.  ;

'!_ 11) .Close RC-V-17 anc place a sample Dottle under the sample tap.

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r0 LZP-1330-25 4 Revision .I g;3 March 18, 1982  ;

5  :

ty F Ootain sufficient sample 5

12) Open RC-V-17.

to rinse the sample cottle.

b f

d, 13) Close RC-V-17 and empty the sample bottle {

into the tray.

II r-r: I

((:?. 14) Replace the sample bottle under the sample

'" tap and open RC-V-17. h L

Fill the sample cottle to overflow and i$

I 15) U I.id screw the cap on 1oosely.

W:

1 m 16) Gentl y squeeze tne bottle to ef fect U E

b over fl ow, then immeciately tighten tne D.

cap.

p

, (2:' NOH -

,:u The physical shape of the polyethylene bottle should .k

,{ be somewhat distorted after step F.3.b.16). {

b.

C:s p

17) Close RC-V-17.  ;.

M:

18) Wipe tne bottie ory with paper towels.

{ Label the bottie witn the fclIowing [

19) information: L:

Ef b$ "

a. Sample point. -

ry. Cate sampiea.

<- b.

ii+.i

c. Time sampled. g,

,q/

rig o. Initials of person sampling. >

nn $3  ;

M' Tnis labeling may De cone prior to taking the sample. [.

?:

20) Tag the sample cottle with tne appropriate

[~ sticker i f the sample contains racionucl ioes. {(

(;

fr $3 1

This tagging may De cone prior to taking tne sample.

21) Place the cottle in the tote tray for NY bL transport to tne chemica) 1accratory.

l-r  !

- J.

L4  :

9

% .% - . - = ,. . - , . . - - . , . .

_- . . _ . . _ . . . . . _ . _ . . . _ . __ ___.3.- __. a .

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,f 7m LZP-1330-25 te; GU Revision 1 [

Marcn 16, 1982 f:

6

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c. Flush ano secure the system in accordance witn (

tne f ollowing: g y i.

p*l

1) At the Valve Control Panel, OPLC9J, secure [ '

the sampling lineup in accordance with Reference 2, steps F.1.d.6) througn

[10 f' .c l.d.7).

2) Close the sample valve, RC-V-1.1 (-1.2. [..

p7 -1.3, -1.4, -1.5). p gg ..

L Open RC-V-4  ;'

3) n i-MJ 4) Open RC-V-17, adjust RC-VREL-2 until RC- [

FI-2 reads 18-22 inches of water. Flush [

T+ with demineralized water for a n.inimum of three (3) minutes. f i

E

5) Close RC-V--17. -

l

(( Al i gn RC-V-18 to the 6 o' clock position, Lc 6) adjust RC-VREL-2 until RC-FI-2 reads lo- [

"T 22 inches of water. Flush with cemineralizea [

hkl water for a minimum of three (3) minutes. {y.

, 7) Close RC-V-7. f'

.i i

  • 8) Open RC-V-3. ,

y 9) Adjust RC-VREL-1 until RC-FI-l reacs 35- fL 40 inches of water. Flush with demineralizec e

V water for a minimum of one (1) minute. I I

l -

10) Cl ose RC-V-3.

Open tne sample valve, RC-y-l.1 (-1.2, - [

11)  ;

1 3, -1.4, -1 5), flush with cerineralizea

-g [

4 water for five (5) minutes.

I i

Close the sample valve, RC-9-1.1 (-1.2, f m

12)

-1 3, -1.4, -1.5).

CJ I

13) Close RC-V-4. y C 1*) Close RC-VREL-1 and RC-VREL-2.

L.

I

15) Close the flusn water valve and disconnect  ;

the flusn water nose f rom RC-CV-1. i

[S'W:

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- LZP-1330-25 L Ni Revision I h

'Ul March 18, 1982 6 7 k:

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gg 16) Secure tne system in accordance with h Reference 2, steps F.1.d.8) through F.1.f.

{-

4. To oDtain an undiluted (15 ml) reactor coclant fa.I sample, proceed in accordance .#ith the following at f.'

g' the LSP, CPLD8J or as otherwise directeo: r Et-F');

g a. Verify the following valve lineup: 5

1) RC-V-5.1 (closed). A:

N.;. W G

2) RC-V-5.2 (closed).

[v De 3) RC-V-17 (closec). h g y

4) RC-V-4 (closed). {

e

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5) RC-V-7 (closed). D.

(

1:

6) RC-V-ll (closed). [

y g- p 4 7) RC-V-9 (closeo). E i-ps 8) RC-V-11 (closed). k W V

9) RC-V-8.1 (closed). h
10) RC-V-16 (c)osed).

'r.

11) RC-V-18 (6 o' clock). ['

Ks

12) RC-V-22 (TO nASTE). r.

D. Prepare tne sample Dottle in accercance witn tne following:

1) Place the cottle on the cart / cask assembly cavity piston.
2) Turn the di rection val ve for the hydraulic ofston in the DOWN position and 1ower the h Octtle into tne cask cavity. fr'
3) Close and open the cask tc verify that -

E, the cover is working prcper1y. [

ric "

4) Turn en the L5P undiluteo reactor coolant

$* sample fill station lignts.

h e r k ..

.. - + *

- ..:. ..-.  : a- - .- .-. = _ . - . . . . . . . . ... . . . ._ . _

---___-.~...-.

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b LZP-1330-25' h.

Revision 1 F Maren 18, 1982 b 8 O C; l k 4 5) Pcsition the casx/ cart under the LSP ff f undiluteo reactor ccolant sample fill )f

~

station needles and set tne brake. tf f

Turn tne direction valve for the hydraulic h

6) I piston in the UP positicn and raise the e-

~

bottle onto the needles.  :

h e

Obtain the sample in acccraance with the y

c. b following: e C
t. .

(b

1) Open RC-V-3. k

~~

y

' T:'

Open RC-V-2. J jc< 2)

3) Select one of the sample sources anc open [
r. ,

its' corresponding valve. RC-V-1.1 (-1.2, [..

p -1.3, -1.4, -1.5).  :~

h-r' ~ 4) Slowly open RC-VREL-1 ur.til RC-FI-l reads  ;,

35-40 inches of water. Allcw tc purge [

b:.__ for a minimum of five (5) minutes. P h

,,.7

- 5) Slowly close RC-VREL-1'until RC-FI-l reacs p; 12-15 inches of water. Continue tne purge i:

for.a minimum of cne (1) sinute. "ff;

~

ff n~ 6) Close RC-V-3. g

$k rA y 7) Open RC-V-7. 3:

n 5
8) Slowl y open RC-VREL-2 until RC-FI-2 reads 18-22 inches of water. AllCw tC purge for three (3) minutes. 4{

p g //-

r .-

9) Turn RC-V-19 to SAMPLE. V

[ -.

10) Adjust RC-VREL-2 until RC-FI-2 reads id- k l h~. 22 incnes of water or RC-G-3 reads 20 )

PSIG. DO NOT exceed 20 PSIG cn RC-G-3.

! f. ' '.

Allow to purge for two (2) minutes. (

E l

11) Cl ose RC-V-7. Let RC-G-3 return to O PSIG If tnen wait 30 seconds to allow the sample i

,y

' Octtle to cepressurize. 2 Y

i . . ,

F y

LS l.

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M .

LZP-1330-25 rr Revision 1 7 I Maren 18, 1982 7' 9 .

B

{', 12) Turn RC-V-19 to BYPASS.

. D

13) Turn the direction valve for the cart / cask g'- hydraul ic plunger to the 00hN pcs i tion.

Lower the sample cottle intc the cask and close tne cask. [ -

> r

' L, 14) At tne Valve Control Panel, OPLC9J, secure 6" the sampl i ng l ineup in accordance with y Reference 2. steps F.1.d.6) thrcugn

{

[",

F.1.d.7). ,

i:> f

d. Flush and secure the system in accorcance with [

tne following:

73

,u

1) Close the sampl e val ve, RC-y-1 1 (-1 2, ,

-1.3, -1.4, -1.5). j

c. '.r, t 2) Open RC-V-7.
3) Open RC-V-4.

, pl _

'+" - *

4) Adjust RC-VREL-2 until RC-FI-2 reads 18- '

22 inches of water. Flush with demineralized E" water for a minimum of three (3) minutes. E i L

5) Close RC-V-7. b

+

p$g Open RC-V-3. I:

[h 6)

I:.

7) Adjust RC-VREL-1 until RC-FI-l reads 35- 0 40 inches of water. Flush with demineralized k E7 b1 water for a minimum of one (1) minute. h L

er 8) Close RC-V-3. l W: h*

9) Open the sample valve, RC-V-1.1 (-1.2, - t 1.3, -1.4, . 5), and flusn fcr a minimum }

c' (c .

of five (5) minutes. [

t

10) Close the sample valve, RC-V-1.1 (-1.2, [

-1.3, -1.4, -1.5).

Pd i(-

i.

11) Release the Drake anc remcVe tne cart / cask .-

from tne sample station. [.

s,-..

1.

t

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i- b m

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- - . . . , . _ . , _ m- _A. .;_ ._ _ .: __

s_ _ _ . . . . . . _ _ .

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LIP-1330-25

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k. Revision 1 March 18, 1962 '

10 y p- k

. : ?.

k' Install and secure tne auxiliary sni el a. fj 12) t Install and secure tne needle flush tool . r 13)

"b~? f[

14) Open RC-V-8 1.

l'l

15) Open RC-y-8.2. #

[9?<2 ,

r <

16) Adjust RC-VREL-2 until RC-FI-2 reaas 18 t.

7 22 inches of water. Flush with demineralizeo  !

y{u<.y f.

a water for one (1) minute.  ;

P3 17) Turn RC-V-19 to SAMPLE.  :

(i '

~

18) Adjust RC-VREL-2 until RC-FI-2 reads 18- ,

22 inches of water or RC-G-3 reads 20 I hs.:. PSIG. DO NOT exceed 20 PSIG on RC-G-3. '

" Allow to flush with demineralizea water for two (2) m i nu te s. f, o em ,

h, 19) Close RC-V-2.

t

n 20) Allow RC-G-3 return to O PSIG then wait

{;: 30 seconds to allow the bottle to _

depressurize.

Turn RC-V-19 to BYPASS. j

}$ 21) c; f

22) Close RC-V-8.2.

[

h hy 23) Close RC-V-8.1.

y 9;

24) Close RC-V-4. r 53 25) Remove the needl e flush tool . }<

Turn off tne LSP unoiluted reatcr coolant rc 26)

([ sample fill station lights.

27) Close the flush water valvo and disconnect , 7' F

the flush water nose from RC-CV-1. '

[

I 28) Secure the system in accordance with t; Reference 2, steps F.1.d.8) thrcugn F.1.f.  !

{J '

I

5. To ootain a diluted (1000:1) reactor cociant sampl e, -  ;

r proceed in accordance with the following at tne LSP,  !

' k--

OPLOSJ or as otnermise directed: /

c e-t i I #

w. e, I . - . , e..

- -. 7,._ e . -

- . - . . . . .. w . a. ~ .. ......=:.-..u.s....-~..~ .

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LZP-1330-25 {t <

m Revision .1 i

'E '

Marcn 18, 1982 t-gg lx,

. F

a. Fill reservoir RC-R-1 with demineralized water. t

,' ic:.[s ,-

t o. Open RC-V-20 then cpen RC-V-21. Adjust reservcir

-g RC-R-1 until the water level in graduatec b_

d ',

i cylinder RC-C-1 1s:125 ml.  !

g.

c. Close RC-V-21. [y

{7 "

f

d. Close RC-V-20.

4

[

e.

e. Verify the following valwe 1ineup:

{.'

1) RL-V-5 1 (closed).  ?

re k I."

w 2) RC-V-5.2 (closed). '

I

};

m, 3) RC-V-17 (cicsed).

it Le 4) RC-V-4 (closed). [

5) RC-V-2 (closed). [

>p ..

Ee I

6) RC-V-7 (closed). f.
k. 7)* RC-V-11 (closed).

L

8) RC-V-9 (closed).

C g 9) RC-V-16 (closed).

a

10) RC-V-18 (6 o' clock). "

i E.d s

, 11) RC-V-19 (BYPASS).

s:

l oi 12) RC-V-22 (TO WASTE).

W- ,
f. Prepare the sample Dottle,in accordance with the foilowing:

7 ZT

1) Insert the needl e of the hand operated vacuum pump in c the septum of the dilutea .

5 reactcr coolant sample cottle. Evacuate

[i, s to the maximum vacuum achievable witn the j

- a hanc operated pump. . Tne vacuum MUST oe t at LEAST 15 incnes of Hg.  ;

t.

', 2) Keep the hana operated vacuum pump connected I

,. to ne evacuatec oottle for three (3) }-

g i A {

C# I.

D.,

'a d -

L - .- - ..

..s. . ~- .. _ . _ _ -

7 . , _ _ _ . _ _ _

i 1

w .

,w A W^ LZP-1330-25  ;

.g.

Revision 1 '

Parcn 18, 1982 I IF j N-minutes to assure that tne bottle retains ,

the vacuum. 7 f.

TP Remove the cottle from tne hand operatec i.

[i 3)  !

vacuum pump and place the octtle on tne cart / cask assemD1y Cavity piston. f "U 4) Turn tne cirection valve for tne nyaraulic piston to the DOWN position and lower the [-

Dottle into the cask cavity. [

fl m?

I-

5) Close and open tne cask tc verify that [

the cover is working properly. t

.- V
6) Turn on the LSP diluted reacter coolant I sample fill station lights. [

rr ..

pv Position the cask / cart unoer the LSP l uh 7) olluted reactor coolant sample fill station j

, 3; neeole and set the Drake.

w

"^ Turn the direction vaise for the hyoraulic 8) piston to the VP position and raise the f octtle onto the neeole. {

g. Sample in accordance with the following: I L

I 1) Open RC-V-8 1.

2) Open RC-V-8.2.

@ Open RC-V-3.

3)

4) Select orse of the sample sources ano open

{p gi its' correcponcing valve, RC-V-1.1 (-1.2, . _ _ ,

-1.3, -1 4, -1.5).

ll

5) Slowly open RC-VREL-1 until RC-F1-1 reaos 35-40 inches of water. Purge for a minimum of five (5) m i nute s.

$b 6) Slowly close RC-vREL-1 until RC-FI-1 reads j 12-15 incnes of water. Ccntinue the purge [

l .

7 for a minimum of cne (1) minute. j-

7) Cl ose RC-V-3. ,

V IL v-: *!

4 wu

m. _ _ _

. .. .. . .. - .. .m..

.. m w: 'e,-

'^

c,'

W

. k I

t i

LZP-1330-25 }

r. ' Revision 1  :

I" March 18, 1982  !

'^

13  :

,- 4

8) Open RC-V-2. [

u (

9) Slowly open RC-vREL-2 until RC-FI-2 reacs [

p' 18-22 inches of water. Purge for three -

[; (3) minutes.  !

s ,-. 10) Close RC-V-8.1. I 6

I 11) Turn RC-DV-1 to SAMPLE.

12) Close the sample source i sol aticn valve.  :

{'"

ti .

13) At the Valve Control Panel, OPLC9J, secure the sampling lineup in accordance witn  ;

p[y- Reference 2, steps F.1.c.6) througn F

~~

F.1.d.7).

f5 14) Close the sample valve, RC-V-1 1 (-1 2, i LL -1.3, -1.4, -1.5).

, g, r, n. F*,ush and secure the system in acccraance with l Q

the following: j

1) Open RC-V-7.

77

2) Open RC-V-4.

.- 3) Adjust RC-VREL-2 until RC-FI-2 reacs 18-

{3 b 22 inches of water. Flush with cemineralizeu ,

water for a minioum of three (3) minutes.

[&

4) Close RC-V-7.

I

5) Open RC-V-3. p T* [

13 6) Adjust RC-VREL-1 until RC-FI-1 reads 35- [

40 inches of water. Flush with demineralized i-gp water for a minimum of cne (1) minute. 5

'h$

7) Close RC-V-3. [

t EY 8) Open RC-V-21 [

bl 7

9) Crack open RC-y-21, and aca 24 el of water j

., y from RC-C-1 to tne sample octtle, then j gg close RC-V-21.

re i L; t

--~ -

. . . . . . . .-... - -,s-. .- . . , .

r,' '

e.

?- t1 i

- LZi'-1330-25 I I

I Revision 1 Marcn 18, 1982 14  !

(

$5 l

,~ The ollution volume may oe changea as assired oy l ~

it Rao/ Chem Supervision.

u.

  • , 10) Turn RC-DV-1 to BYPASS. .

V4 11) Open RC-V-8.1. l p- 12) Adjust RC-VREL-2 until RC-FI-2 reads 18-  ;

A 22 inches of water. Flush witn demineralizea water for one (1) minute.

Eb 13) Close RC-V-2.  ;

L: '

14) Open the sample valve, RC-V-1.1 (-1 2, -

F 1.3, -1.4, -1.5) anc flush with aemineralized

(; water f or a mi ni mum of five (5) minutes.

-. 15) Close the sample valve, RC-V-1 1 (-1.2, ,

' E' -1.3, -1.4, -1.5).

L i

16) Close RC-V-8.2.

f',

> (j 17) Close RC-V-8.1.

4 l ILq 18) Close RC-V-4 {

i. Remove the sample and casx/ cart assencly and f secure the system in accorcance with the ,

l r:5 following: t t $;- i l i) Place the direction valve for the nyaraulic f 7, plunger in tne 00hN position.

L.1' 2) Lower the Dottle into the cask. l i

l [,[ 3) Close the cask.  !

l- $.

4) Release tne Drake and remcVe the cart / Cask )

,.r from the sample station. [

i * ' 1 Install and secure tne auxiliary snielo.  !

5) l 6) Turn off the LSP dilutec reactor coolant

[h k sample fill station lights. -;

r

? 7) Close tne fluin mater valve and disconnect 8 l J, tne riusn water nose frc RC-cv-1. -

i b

t

[;

p'

Y LZP-1330-25 ,

I Revision 1 Marcn 18, 1982 1 15

8) Secure the system in accordance with ,

Reference 2, steps F.1.d.8) througn F.1.f. V IS 6. Transport the samples to the sample preparation area

  • k in accordance with Reference 3.
7. Prepare the sample frem Step F.4. or F.5. for anal ysis i 7'
k. in accordance witn the following:

h.

'  ?

a. Place a 47 mm fiber filter in a new petri oisn fc, and place behino a shielced are= witn the cover '

- off.

.' $U '

tu-If less than 500 ul (0.5 ml) of sample is usea, p- campen the fiber filter with celonizea water prior CN to placing the sample on the fil ter. ,

L2 4, D. Recove the small shield. plug from the top of p [i- the shielo cask. .

L '

c. Using the syringe assemoly, witncraw 20 ul of the sample and immediately replace the shielo ,

plug.

((?  ;

n. . $U  !

d Sample volume and geometry may be changed at the t discretion of Rad / Chem Supervision to f acili tate f

, 5". anal ysis of samples.

f' 1-L Discharge tne sample ontc the fiber filter in

d. '

p.

the petri cish in sucn a manner tnat the sample qi is evenly aepositeo over the entire ficer fil ter

surface.

e. Place the cover on the petri aish anc tape it i

^['

closed.

I m f. wrap the petri dish in plastic wrap ano seal it.

33

g. Label the sample in accorcance with tne following:

ar 1) System sampled and sample location.

(a .

NE.

r k.

[

. F

. I'

?.

?

G LZP-1330-25 Revision 1 [';

Marcn 18, 1982 16 r- ,

2) Time of sampling.
r. 3) Date of sampiing.
4) Sample volure, refer to Step F.8.

E' 5) Initials. i

6) Survey results. <

W "

y.

' ^ ~

8. The sample volume for undiluted samples is the same as the syringa volume oiscnarged. For a o8 luteo  !-

sample, calculate the actual volure of sample on ,

p the floer filter in accordance with the following:

%. m V = b2 # ,

r. , y b,k l-where: V = The actual volume of rcactor water f

_. to De analyzec on the filter paper in ml.

{ l.

S = The volume of the diluted sample in

$' the syringe in rl. t L:

A = The valve aliquot of sample collected

g. in the cask Dottle in ml. ,

'# T = The total volume in the cask oottle, .

the valve aliquot of the sarple plus [

the water added from the graduated cylinder p g in ml. -

g- 9. Anal yze the samples in accordance with Reference 4

Q Report the sample results to the Rao/ Chem Director t

10.

for evaluation.

-n n s.

f{$

d. 11. Route al1 output oata and calcuiatians to Rad / Chem -

Supervision for review. l p 1.

E G- Ctf21.1111 l

, 1. None.

L L H. TECHNICAL SPECIFIQ TION REFERQ g l  ;

m-c' i 4.- f i* k

~

,. _ . ...r. _ .-

wM

(

. e v

' t:

. s.

2 5

LZP-1330-25 Revision 1 i March 18, 1982 17

1. None.

k t

1. . -

i.

i 5

e.p.+

i .

ki .

rw

~

s IO 5

8 5

F3' I

-3 i.

L, 1: .

=

?

  • F

,, v

d. F' p.

a i

% S JE, .

id

  • L,,"

T F

ue t

X-5.

G I

s, M6 E,

e

.k .' .

+:+

f Li

I e

-. . a. . = = ~ ;- =. r- .-- - - = -. = : -- - -  :

_ ;= . .- _

=::= -  := : = = - .:

LZP 1330-25 RevIsl'on 1 L March 18, 1982 [

i8 1 ATTACHMENT A VALVE LISTING RC-V-1.1 Reactor Recire. Loop B Sample Cutout Valve l Y

+

I. .. RC-V-1.2 RT Domin. Inlet Sample Cutout Valve c-- RC-V-1.3 RHR Loop A Sample Cutout Valve l t

^'

RC-V-1.4 RHR Loop B Sample Cutout Valve  :

l RT Demin. Outlet Sample Cutout Valve  :

I' RC-V-1.5 '

c.

RC-V-2 Sample Source isolation Valve  :

re Sample Purge Cutout Valve RC-V-3

{

  • RC-V-4 81ushing Vater Isolation Valve P'

p.

6. RC-V-5.1 Pressurized Sample inlet isolation Valve Pressurized Sample Outlet isolation Valve  ;

,g, RC 'i 5.2 i: . L RC-V-7 Diluted Sample Bypass Valve \

7 RC-V-8.1 RC-SF-1.2 inlet Isolation Valve [

iC. '

RC-V-8.2 RC-SF-1.2 Outlet isolation Valve e

2 RC-V-9 RC-EV-1 Isolation Valve [

w RC-V-10 RC-EV-1 Evacuation Cutout Valve [6 M' I' LV. RC-V-11 Off-gas 4-way Valve Argon to Air Ejector Cutout Valve

,j RC-V-12 '

.x i Off gas Vial Evacuation Cutout Valve RC-V-13 i

RC-V-14 Argon Supply to Off-gas Vial Cutout Valve RC-V-15 Off gas Sample to Gas Chromatograph Isolation Valve ]

t' RC-V-16 RC-SF-1.2 Argon Purge Cutout Valve RC-V-17 Reactor Ccolant Grab Sample Cutout Valve

,w

[3 7 .,

-w

r f

y

' L _*_ _ .

t 6

LIP 1330-25 i

~

Revision :)  ;

e.

~- March 18,- 1982 ,

f.

19 (Final)

ATTACHMENT A l

[

(Continued) e  :

t:

k. .

Reactor Coolant Undiluted Sample Backflush Cutout Valve b RC-V-18 d

?l' Reactor Coolant Undiluted Sample injection Valve [

f~ RC-V- 19 t

RC-V-20 RC-C-1 Fill Valve -

r-y:

E-- RC-V-21 RC-C-1 Isolation Valve b

'a RC-V-22 Liquid Sample to CAP lsolation Valve .

f RC-DV-1 Reactor Coolant Olluted Sample injection Valve

.. w Of f gas Sample injection Valve 1J RC-DV-2 Cv RC-VREL-1 Reactor Coolant Purge Throttle Valve '.

y <

g RC-VREL-2 Reactor Coolant Sample Throttle Valve p TTc:  ?

c sr._.

?

I*

1 C4

.S m

>8._

O-CJ' t ,

CL 9 4

i

,3c =

1 p  :

EL V 4 l

t- ,

i e 6

' ~ ' ' -~ ' *~~:  :# * *~ :

a .. .

f1

e.  % 1 E

r LZP-1330-26 -

Revision 1 March 18, 1982 1 1

- SAMPLING CF CONTAINMEhT AIR AT THE HIGH p RADIATION SAMPLING SYSTEM w..

A. f,U,3P_91) c' O ,

U The purpose of this procedure i s to delineate a metnod {

of obtaining a containment air sample at the High Radiation y F Sampling System (HRSS) suppl ement i ng the containment [

[;

monitors during normal and post-accident concitions.

e YJ B. REEERENCES l

L1

1. Sentry Equipment Corporation, Post-Accicent Sample I System, Volume 1. -

{7" ..

2. LZP 1330-29, " Sampling at the High Radiation Sampling -

c ..

System (Valve Operation at tne HRSS Valve Control g Panel)."  ;

a- t.

i

3. LZP 1330-31, "HRSS Sampl e Movement."

IE*

AAIS-CCP-0002, " General Radionuclide Analysis of a  !

Li 4.

Gas Sample." [

p h, 5. AAIS-CCP-00C3, " Particulate Radionuclide Analysis."

t-!

6. AAIS-CCP-0004, " Iodine Radionuclide Analysis." I

! . 52 h

N

! $N 7. Action Item Record (AIR), 1-81-494.

8. Hewlett Packard Program Instructions, "I-131 Equivalent [

! gy l

gg. Concentration." {

9. GSEP Environmental Director Energency Plan Implementing Procedure EC-16, " Quick Estimate of Offsite Dose

)_k Wu From Unplannec Release: Liquid and Gaseous." .

10. Calculatiogj of Distance FdStprj for Powgg ggo Tgs3 '

((d L

Reactor Siter, Chemical Infcrmation Document, Division of Licensing anc Regulations, Washington, D.C., 23 TIC 14844, Taole III.

! rr March 62.

h0" C. PRgREQUISITES

1. Verify tnat nitrogen pressure, apprcximately 100

{I w; psig, is available at the Containment Air Control '

l Panel (CCP), OPLE2J.

u. .

6

. o .

[.

(

l s

b.

r p.

LIP-1330-26 h Revision 1 March 16, 1982 i 2

2. Verify that the CCP printer power is GN and the  ; ,

printer is set to the proper date and time.

i 9

6

3. Set the CCP FUNCTION SELECT to tne SF1-SF3/GGD

- position and cbserve the following at the CCP, CPLE2J: p L.'

a. The POWER CN 1ight turns on.
. Annunciator Windcws glow steady in:

' t. : o.

"; ROh COL ,'

+

1 2 -

r.

1. , 1 3

" 2 2

]

The flow monitor 20% and 100% ficw 1ights turn  ;'

C c.

b on for approximatel y 25 seconds af ter poner is  ;

first applieo.

-. \

$5 L

There is no flow at this time. '

~. ,

, di C. The 20 minute Gross Gamma Detector (GGD) timer g; b.

is energized. f-t*,

M [-

I Pt M

There is no GGD incluced in this system, nowever,

, M the steps were incluced to ciarify tne tir.er l b; sequencing. _

gm 4. Press the annunciator RESET pushoutton to turn off lg all lighted annunciator wincows.

' 5 Verify tne timers on the CCP. OPLE2J, are set as  ;

fh follows: ,

,u l

t

a. Pre-sample Dack flush - two minutes. ,

l tin lg( D. Sample capture / residual gas removal -

tnree ,

s minutes. r l a w

I l

(

l s .;

l l . , . . . . . _ - .. . . , . - , _ . _ . -

- - , - .n - -. - - ,

t e

g r

LZP-1330-26 Revision 1 Marcn 18, 1982 e 3 m

c. Sample flask line flush - tnree mir.utes.

i' d. Equilibrate flask pressure and post sample oack -

flush - fifteen seconds.

I e. Time between SF1 and SF2 - twenty minutes. {

!! L

f. Time between GGO exercises - twenty minutes. l 7'

(( g. Time between SF2 and SF3 - 120 minutes. E r 6. Verify all air and solenoid valve selector switenes [

!E on the CCP, OPLE2J, are positionec to AUTO. [

Lk z

7. Press the PILOT LIGHT TEST pushbutton on tne CCP, I" OPLE2J, and observe all pilot lights are functiona.l.
8. Press the annunciator TEST outton on the CCP', OPLE2J, and verify the following:

, 7r

" a. Horn sounds.

b. Annunciator winoows flash on and off in: '.

n.

ROW COL 1 1 i

~

1 2 {

1 3

c. Annunciator windcw in ROW 2, COL 1 lights up  ;

p:3 and remains l ighted. '

ki Annunciator windcw in R0h 2, COL 3 is off.

d.

Tnis position has no operator functicn. i i 9. Release the annunciator TEST pusnbutton. Verify that the annunciator windcw in R0h 2, COL 1 turns,

?. ? off and remains off. -

C.:

10. Press the annunciator ACKNOWLEDGE pushbutton en the
y- CCP, OPLE2J. Verify tne following

! fla. '"

l a. Horn turns off.

l 97 s

V W:

.._ .m. . - _ .

k t

f:

f LZP-1330-26 5-Revision 1 ,

Marcn 18, 1982 T

-.. 4 p

[
0. All flashing winoows change to a stedoy glow. 0(

t

.N,plj {

'l ' t If desired, push tne TEST pushoutton to retest ROW (

2 COL 1 lamps. ROW 2, COL 1 lamps remain 1ignteo ).

The I; as long as tne TEST pushcutton is presseo.

other windows vill maintain a steady gicw. [

[ j, 11. Press the annunciator RESET pushbutton en the CCP, fs Verify that all annunciator windcws return  !

OPLE2J.

e to the normal (off) condition. .

I "

12. At the Containment Air Sampiing Panel (CASP), CPLO9J, f;'

verify the following: f:

1 3a a. The green INACTIVE pilot light is on. .

t D. All four green SAMPLE FLASK INACTIVE pilot _t

,r 1Ights are on. )

I-Ls ,

c. Sarple flasks are properly coupled and lockeo I' to the CASP, OPLO9J.

E I

o. All sample flask inlet and outl et valves are
y. opened. [

6 L e. All sample flask bypass valves are closed. {

jn E' 13. Datain the sample in accordance with Reference 2 r t.

prior to performing this procedure.

I r

14. Equipment: p E. i C
a. Reach rods. }L g, .

p b b. Sample flask assemolles. .

c. Partioner sampling assembly.

{f L

15. The operator should be faciliar with tne cperation .

of the hRSS panel s.

g. '

g.

    • 17. Establisn communications with the Unit huclear Station Operator (NS0). j f-e' .
p. l, e 5

E 4 h.

.-a. .

l' n..._. .. . . _ _ _ _ . .. .._

V i, h b yrr N

u .- t LZP-1330-26

((

M Revision 1

[

March 18, 1982 I

TT' 5 7

?/

sa D. EBILA2119El .

m t 1. A Regulatory Guide 1 3 or 1 4 release of fission .

  • products implies extremely high levels of  ;

racioactivity. Oose rates may oe nigh enougn to

' G3 prevent entry into,many areas of the plant that are -

50 normall y habitable. Rac/Cnem Supervision shoulo be  ;.

t-contacted pricr to entry into any area wnen such a release of fission products is suspected.

[gy S 2. Wear radiation aosimetry as recommended by Rao/Cnem f Supervision.

Sb 3. Wear protective clothing and respiratcry protection as recommended by Rad / Chem Supervision.

m '

k,, 4 Appropriate survey instruments should De available ,

for monitoring during this procedure.

)

f 5. Under no circumstances snould the sample fl a s k Ei assemblies be uncoupled from the CASP, OPLD9J, t witnout either verifying tnat the "sasple flask flushing exercise complete" indicating lignts are i

[{

tg on or performing a manual flushing operation.

Reach roos should be used to cpen and close the i 6.

valves on the sample fl a sk assemblies for nign radiation level samples. e

7. A LOW NEGATIVE CABINET PRESSURE ALARM, at the  ;;

M{ Containment Air Control Panel, OPLE2J, implies a [

L' potential for airborne activity leaking into tne 'J y HRSS room. Investigate and correct the proolem [

pj immediately to precluoe contamination of the area.

E. LIMITATIONS AND AgTIONS kh l  !.

lT After the "SF3 exercise complete" indicatcr lights, I dA 1.

the START pushoutton becomes inocerative until tne v

& CCP SYSTEM RESET outton is pusneo. This resets the (c.

j[ automatic sample sequence program.

2. After the "SF4 exercisa complete" indicatcr liynts, re. the START pushoutton oecomes inoperative until the

{6 i CASP SF4 RESET button is pushed. This signifies that the operator has removed the filleo sample  ;

flask and replaced it with an empty one. p n[E

w. ,

i

n. t E

<c  :

.w p i'

. . ..~.

'f'

? ' .. L \

v.; t

[! ,

n h!

hE. '

r'

?

[

LZP-1330-26 f.

Revision 1 b Marcn 18, 19d2 [

OS 0 t'

,ix c.

3. The exercise stop pushoutton, when pusheo, will stop [,

automatic sequencing and disaole tne start pusnoutton. p

"? i

4. If any proolems are encountereo at the HRSS panels. (

contact Rad / Chem Supervision.  !

g.

9

  • This procedure, though intenced far use uncer post- t 5.

accident conditions, can be used for sampling at [_

f; the HRSS panels during normal operations, during j f[{ which the precautions l i sted may have limited C However, normal routine sampling [

applicatioits. P precautions should be observed.  !

'.i;

  • 6. S51 may be replaced with the post-accident sample [

partitioner. For purposes of this procedure. SF1 e

is equal to the post-accicent sample partitioner. [

E To obtain a sample in the sample partitioner, proceeo {s El in accordance with Step F.1. 1 L

F. PROCEDURE g 7{(r L US.I.5  !

m 0 4

& For noun names associated with the valves operated [

in this procedure, refer to Attachment A.

{.

rt h 1. Obtain iodine, particulate and noble gas samples in (

the post-accident sampie partitioner in accordance t E

with the following:

h i

- a. Install tne sampler unit in the sample {

partitioner.

b. Slide the positioner over tne top cf the sampler h unit.

~

[

c. Remove the neeole guard.

P

o. Place the noble gas vial with septum in its u protective housing and place the lid on the p' R

E vial housing. ,

i

e. Install the vial and nousing in the partitioner g l-v oevice.

G #

f. At the CCP, CPLE2J. adjust the nitrogen pressure [.

i b,, regulator PC-1 until the pressure gauge reads I G 100 psi.

I l-w 9-f io2:

I .-

~ . . .. ..

- . ,. ~ _ . . . . . . . .

+

p5. . - . . - - - ., - .m.

e '

c, i

iI f.A ,.

Y I[E L Z P- 133 0-26

'{,' Revision 1 Marcn 18, 1982 '

sn 7 .

b Se

g. Press the SYSTEM RESET button to initialize .

the automatic sample fl a sk filling program. ~

f..*.) t' kJ n. Press the exercise RESET button and then exercise START button to initiate the automatic sample .

acquisition sequence. 4

{ The CCP, OPLE2J, will control the collection 3]

i.

of a sample automatically. Iil

%L J. Wnen the ISOLATE S AMPLE FLASK annu.; iator windcw h t

flashes, press the exercise STOP outton. This F5[ freezes the program in the PAUSE mode. {

sw h p

k. At the partitioner controller, set the counter to the number of aliquots of the sample to ce .

$5 taken as designated by Rad / Chem Supervision,  ;

LU

  • then start the sampling sequence oy depressing ,

y 70 the START button. v.

R

~

EE f r, .

  • d4

/j" The sample tire will be determined by the time of

'and sampl e injection valve turning and injecting t the sample into the partitioner. k FP-

1. At the completion of the sampling sequence, "h k(I the vial and housing will pop up. At the CCP, p OPLE2J, release the exercise STOP pusnbutton i and press the exercise START pushoutton. fy' Pressing the START button initiates a tnree t minute sample flask line flush. When the flush is complete, the programr.er returns to the home 3

'N

' position and turns on the TIME BETWEEN SF1 - I LE SF2 timer.

li li l$

Et If the sample lines are not flusned dur ing automatic I[

i fg sample acquisition, a manual line flusn must ce g 8

, E. performed before the sampler unit can ce removed F.: .

' from the CASP, OPLO9J. Proceed immediately to Step f-p F.4. for manual sample l ine flusn. t n

(;

m. When the TIME BETWEEN SF1 - SF2 tirer times out, (20 min.) tne programmer will repeat tne j $d sampl e acqui s i ti on sequence of Step F.1.h. for SF2. If a sample in SF2 is.casirec, proceea

[E r0 l

in accordance witn Step F.2. If nc furtner [

l

t F, . _ _ . . _ _ _ . _ _ _ _ _ _ . _ _ . _ _ _ . . _ _ . . _

I y .

L

,7-LZP-1330-26 Revision 1 Marcn 18, 1982

,. 8 c

1, samples are desired proceed in accoroance with Steps F.5.c. through F.5.f.

2. To obtain a continament air sample in sample flask (SF) 02, or 03, proceea in accordance with the following at the CCP, OPLE2J, or as otherwise

~

be directed:

7 a. When the ISOLATE SAMPLE FLASK annunciator windcw flashes, press the exercise STOP outton. This

{f( freezes the program in the PAUSE mode.

e.

c O. At the CASP, OPLD9J, close the inlet and outlet ,

[d

' valves for the sample flask, SF2, anc open the bypass valve.

m. um Reach rods should be used to open and close the y [rn valves on the sample fl ask assemolles for hign

- - - radiation level samples.

? c. At the CCP, OPLE2J, release the exercise STOP '

K2 pusncutton ano press the exercise START pusnbutton. Pressing the START butten initiates 3.

a three-minute sample fissK line flush.

gv -

(d~

t!95 f

If the SF lines are not fl ushed during automatic <

75

  • s4 sample acquisition, a manual line flusn must be performed later before the SF can be removed from the CASP, OPLD9J. Refer to Step F.4.

P: -

c. When the SF2 exercise has endec, the programmer returns to the home position and turns on tne f ol l ow i ng: {

TIME BETWEEN GGO EXERCISES timer (20 min.). b 1) ry

2) TIME BETWEEN SF2-SF3 timer (120 min.). b bl

,, e. Four GGD exercises will be accomplishea oefore 7i the TIME BETWEEN SF2-SF3 timer times out. At

" the completion of tne four GGO exercises, tne CCP, OPLE2J. will collect the SF3 sample. If tne TIME SETWEEN SF2 and SF3 timer times out F?.?C cefore completion of a GGD exercise tne GGD exercise will continue to compl etion ano tr.en i

F L. '

r

.; . . . - . . ..-~. u . .

rs ,

r L Z P- 133 0-26 i Revision 1 March 18, 1982 9

f~

\c .

the SF3 exercise will Degin. Perform Steps

. , F.2.a. through F.2.c.

i i

f. Observe that all SF EXERCISE COMPLETE incicators, for sample flasks SF1, SF2, and SF3 cn the CCP,

[~ OPLE2J, are l i ghted. If all inoicators are e lightea, proceed to Step F.5. for system shutcown ano cart / cask removal. If all exercise '

e ." complete indicators are not lightec, proceed immediately to Step F.4 for manual sample flask  !

I.

l ine flusning. CO NOT uncouple the sampling ,

flasks at th i s ti .ne .

r-I

3. To obtain a containment air sample in sample flask i
  1. 4, SF4, proceed in accordance with the following ,

i at the CCP, OPLE2J, or as otherwise directed-

". c  !

~

a. Adjust the nitrogen pressure regulater, PC-1, until the pressure gauge reads 100 psi. [

o 7. y l

k b. Place the CCP Function Select Switch to tne  !

SF4 position. [

W ,

[j c. Press the exercise RESET outton anc then exercise  !

START button to initiate sampling. i p_.

I

d. The CCP, OPLE2J, will control the collection [;

{~. of a sample automatically through tne following sequential operations: ,

in 1) Two-minute pre-sample Dackflush. [.

cy 2) Three-minute sample capture.  :

b ..

" Fifteen-secona equilibrate flask pressure.

3)

  • ) Three-minute resiaual gas removal. f-
5) Fifteen-seconc post-sample Dackflusn. ,

7-:

(( 6) Fifteen-second post-sample backflusn.

e. When the ISOLATE SAMPLE FLASK annunciator winaca  !

flashes, press the exercise STOP Dutton. Tnis j f_

5- freezes the program in the PAUSE mcoe.

l

% f. At the CASP, OPLC9J, close the inlet and outlet  !

valves for the sample flask, SF4, anc open the l

[L bypass valves.  !

-q _ , , , ,, . . _ , _ - - . - _ . -

s

.i

. _ . ~ . . . - _ _ . _ _

7. ,_ m_.____. t

('

L

< r-,.

o f' '

LZP-1330-26 Revision 1

-. March 18, 1982 10 e 13 '

g. At the CCP, OPLE2J, release the exercise STOP pushbu+, ton and press the exercise STAAT I3, pushbutton. The CCP, OPLEZJ+ will initiate a
r. - three-minute sample flask line flusn to complete the sampling sequence.

rv L@, NOH If the SF lines are not flushec during automatic f.", sample acquisition, a manual line flusn must be U" performed later Defore tne sample flask can De Refer to Step F.4.

removed from CASP, OPLD9J.

gn

[i h. Observe tnat the SF4 exercise complete incicator is lightea. If tne inoicator is lighted, w proceed to Step F.5 for system shutocwn ano k;, cart / cask removal. If the indicator is not

-' lighted, proceed to Step F.4 to perfcrm a manual flushing operation prior to further action.

DO NOT uncouple the sampling flasks at tnis

)f time.

6.

e 4. To perform a manual sample flask line flush, proceso in accordance with the following at the CCP, OPLE2J:

{.{

a. Turn all air operated and solenoid valves to I2 the CLOSED position. ,

YU I D. Turn the f ollowing valves to the 3 PEN position.

I 1) SV-10.

SV-1.2 and AV-1 for SF-1 flushing. r

2) ,

.Y?

SV-2.1 and SV-2.2 for SF-2 flushing.

G; 3) 1 rp 4) SV-3.1 and SV-3.2 for SF-3 flushing.

b 5) SV-4.1 anc SV-4.2 for SF-4 flushing.

m.

. " c. Flush the sampl e fl ask lines for a period of we three-minutes and close SV-lO anc the inlet and outlet sampling line valves previously F" openec in Step F.4 0.

\

N. c. Proceea to Step F.5. for system snutcown ana j gr.

cart / cask removal.

n we ,

t A .'

. ,,,.,,,w.,.,

  • ~
  • m~*

-..asm-,, mn. .

ff k'

E b ..

i u- '

i k- f' i g si ,

LZP-1330-26 f*

f. Revision 1 March 18, 1982

-e LL f

y y

5. To temove the partitioned sample proceec to Step g

'F.6. To remove the cart / cask and shut the system y, down, proceed in accordance with the following at f.

b the CASP, OPLC9J, or as otnerwise directed:

LC t

r't ' a. Unl ock the quick disconnects from the flusheo [

cask or casks. Remove the cart / cask assemoly y k3 to the laooratory area in accordance witn F Reference 3. [

g i

L# CAUTION a Reach rods should De used to unl ock the quick [

7[ disconnects on tne sample cask assemblies for nigh _

go level radiation samples. [

f s

Install the backup cart / cask assemoly.

f O.

c. Pusn the RESET outton at the CASP, OPLD9J. to L

)

"" clear sampling flusn indicator l ights f rom .

ACTIVE to INACTIVE status.  !

I-Push the SYSTEM RESET button at the CCP, OPLE2J.

pg d.

to return electro-programmer to initial startup I I"9' moce. f t-P

e. At the CCP, OPLE2J, turn FUNCTION SELECT to k
  1. OFF, and remove the tape output frcm the printer. h" The tape output snould acccmpany the samples '

to the chemical l acor ator y.

p; i i

( be Upon completion of the sampling operations, I

f.

secure the sampling lineup in accordance witn  !

Reference 2. Steps F.4 0 6) through F.4.c. ,

6. Tc remove the partioned sample, proceed in accorcance y..

with tne following:

a. Remove the vial ano nousing from the partitioner.

I

' Log tne following information (as appropriate) [

b

  • for entry into the A.A.I.S.: p I
1) System sampled ano unit. l.

F [

2) Sampl e l ocati on.

kb L T

t

, 7 t l T -

tv

--n.- .,-.....n w-

,, o . L r:

k . b

~

n

! h.

N g p- LZP-1330-26 i~ Revision 1 ,'

" Maren 18, 1982 P 12 I;l r e f 3) Sample time on. ,'

Yi p(,,;

4) Sample time off (this time will oe tne same as time on).

fg; g

b

5) Sample cate on. fp

.t.

I 6) Sample date off (this date will De tne r same as date on). '.

7) Reactor power, megawatts thermal. -

F

8) Reactor power, megawatts electric.

g ,

9) Initials. k.

I.

P.? o. Remove the protective housing from the noole E 3] gas vial and determi ne the radi aticn level of the sample. If radiation l evel s warrant, place [i

,p the vial in a lead shielo for transpcrting to i

y. the analytical area. y V
c. Remove the protective housing from the particulate r and iodine cartridges. l.

b l

d. Remove neeole from the sampier unit. ll
e. Remove the particulate and iodine cartridges.

f.

, fe Transport the samples to the sample preparation .

A area in accordance witn Reference 3. F Lis i

g. Separate the particulate filter anc iocine l; y, cartriage utilizing a knife to cut the ccnnectcrs. {

p Cut relatively close to the top anc Dottom of F the samples i n oraer to set tnem flat in secondary containers.

n. Place the silver Zeolite iodine cartriage inlet side down into its plastic sample holaer.
i. Place the particulate filter inlet side up in '

a plastic petri disn. .

w j' y

j. 'w r a p tne sample containers in plastic wrap or J.

seal in plastic bag. [

t

k. LaDel the samples i n acccrdance witn the

.1 following: p t-t-

A h-g.em q=w - esdery ey 9gae.g-O

  • e.m ey u ,a ,,,,y,ge

- 4.*.n.a

I

.~_

.  ?

L .e r,. ,

w.

LZP-1330-26 r-i~ Revision 1

" ~ ' March 18, 1982 ,

13 Q )

[2 t 1) System sampleo ant unit.

rf: 2) Sample location. p

3) Sample time.

t b 4) Sampie cate. b k y;

5) Sample volunte. [O R

O' 6) Survey results. $

'"'' ~

t fn.

$" 1. Prepare the post-acci dent sample partitioner [t for further sampling in accordance with Steps

" F.1.a. througn F.1.e. f

e. t;
7. Perform the racioactive anal ysis for each sample in y, accordance with Reference 4, 5, or 6, as apprcpriate. h.'

V w T C' 8. Determine the I-131 equi valent concentration using 3 th Hewlett Packard Calculator program in accordance f-with Reference 8.

7:

9. If the Hewlett Packaro calculator or calculatcr [

g program "I-131 Equivalent Concentration" is not I g available, calculate the I-131 equivalent concentration of the containment ai r sarr.ple in accordance with

[4 p

Attachment B.

10. Calculate the iodine, particulate, and nocle gases r

curie content in tne primary containment in accorcance with the following: p w

!!.9.I.E i-Calculations should De perforzeo on the isotopic I anal ysis hard copy printer output.  ;

2

a. Calculate tne total I-131 equivalent curie [

[d. content of the primary containment in accordance f[

I with the following:

L W I'

{' C = 0 L050S.55.1.

(lE06 uCi/Ci)

A w

j u

k,

  • ~ L r

b b -

I-

- - - - - - ~ - - ~

l _ _

p t. '

, bi 7- Ri 1:

f

o f[.

'{  !.ZP-1330-26 i

Revision j g.

March 18, 1982 .-

rc , 14 tj

fl

+- w >,

,- I a S= I-131 equivalent concentration uCi/cc, in the sample from Step {g r- F.7. or F.8. (p.

w .

O0 F 1.1E10 cc = Primary containment free air h volume. $.

f2  %

C o. Sum the particulate radionuclide ccncentrations. [L uti/cc, from the isotopic analysis in Step F.7.

L

c. Calculate tne total particulate curie content f;

of the primary containtent in accordance with tne following: r pL t C=JMDdGBQ g (lE06 uCi/Ci) y o?- L

., Where C = Total particulate curie content f of the prircary containment. [

IS r)"g~1 S = Particulate racionuciice t, c orice nt ra t i on , uCi/cc, in b the. sampl e f rom Step F.10.D. [

1.lE10 cc = Pr! mary containment free air volume. .

Il

c. Sum the noble gas radionuciice concentrations, '

uCi/cc, from the isotopic analysis in Step F.7.

e. Calculate the total noole gas curie content of r.

i@t the primary containment in accoroance witn the }

following: [,

F f C=LMDdD%Q (lE06 uCi/Cs)  :

f.f where: C

  • Total nocle gas curie content L of tne pr ircar y ccnta i ntrent.

[

m S= Noble. gases racionuclice

{ concentration, uCi/cc, ir tne sample from Step F.1C.c, r v

a i i

(

. . . - - . - . - - - ~ ~ ~

p - -

.r-

-"~~ ' ~- '- e

(

I.s fs 5

V [ r p LZP-1330-26 e

" Revision 1  :

^

March 18, 1982 15 1.1E10 cc = Primary containment free air voluse. 4

y. 4- I-n ~

E.! 11. Report the sartple results to tne Rad / Chem Director for evaluation in accordance with Reference 9. ,

12. Route all output data and calculations to Rad / Chem Supervision for review. [t h[I 13. Dispose of the SF al r sampies fol1owing anal ysi s, i.

LC in accordance wita the following: [

te a. At the Valve Control Panel, O P L( ~3 J , proceed in [;

[, accordance with the following: {e F.

g 1) Place the UNIT 1(2) PCHER switch in the (

ON position. .

2) Open tne following valees and verify tne [

, F' indication snows OPEN:  !

Ul ;f a) HRSS SYSTEM AIR RETURN TO SUPPRESSION POOL, 1(2)CM-088 and 1(2)CM-009. I{

U b) HRSS SYSTEM AIR RETURN TC SUPPRESSION f POOL, 1(2)CM-090. f d'rt D. Connect the cask / cart assemoly to an availaole O sampling station at the CASP, OPLD9J, ano note I rr the samplitig station number.

c. Close the sample flasx oypass valve at the CASP, OPLD9J.

+

V d. Open the sample flask inlet and outlet valves ,

at the CASP, OPLO9J. '

e. At the CCP, OPLE2J, place the FUNCTION SELECT ,

switch in the SF4 position.

y f. Press the EXERCISE STOP pusncutton on the CCP, S OPLE2J, if not already depressed. f.

I er g. Turn all air and solenoid operated valves on }

[i the CCP, OPLE2J. to tne CLOSED position. },

L

n. Turn the following valves on the CCP, OPLE2J, 4 h.

m to tne OPEN pos i ti on:

{

l.

LS V

-- . ~ . . . --

t. 1 I-
a. -. .. '. - - - .- . - - -..... . . . . . - .

y' W.

u

e.
  • k:

r; '. ,

p

- F LZP-1330-26 Ei

' Revision I h

'-~

March 18, 1982 I 16 h L

EO

1) SV-10 to open the nitrogen supply. I L_

.v U

2) SV-1.2 and AV-1 for SF-1 flushing.

h"-. h.

3) SV-2.1 and SV-2.2 for SF-2 flushing. E b," b 6 4) SV-3.1 and SV-3.2 for SF-3 flushing. [

r

5) SV-4.1 and SV-4.2 for SF-4 flushing. [f p

gj

i. Allow the sample flask to flush f or a minimum g_

g,, of three (3) minutes. 4 L

t',.

L j. At the CCP, OPLE2J, turn Sv-10 to the CLGSED  !!:

position. Ir.

Turn the solenoid operated valves opened in [t C[

[ k.

Step F.13.h. to tne CLOSED position. t g

Press the SYSTEM RESET button cn the CCP, 4

" bo. 1.

b OPLE2J. to return the electroprograme.er to the ,

initial startup moce. {

g:

Turn the FUNCTION SELECT switch on the CCP, f' h m.

OPLE2J, to the OFF position.

  • c f? Release the EXERCISE STOP pusnbutten on tne p; g' n.

CCP, OPLE2J. {j p

r M o. Close the sample flask inlet and outlet val ve s did on the CASP, OPLO9J. h c

p. Unl ock the Quick disconnects fror the cask / cart b g f:.

?, assembly and remove the cask / cart. p L

i. . c E i The cask / cart may De left coupled to the CASP, ',

b j.

OPLD9J, for future anal yses.

cg:- .:

q. At the Valve Control Panel, OPLC9J, proceed in E accordance with tne f ol l ow i ng : {';

t.

em C1ose tne fol1 ow ing val ves and verify tne I:

b= 1)

O irdication conows CLOSED: [

f t,

a) HRSS SYSTEM AIR RETURN TO SUPPRESSION

[7~ POOL, 1(2)CM-088 and 1(2)CM-089.

ai .

e h'.

6

. . . . . . ~ . - . . . . . , .-

p.

C' *

.. . . . .. . . . . . . . . . - - . V b B b

e. .

11 *

  • 6

.n y p:'

I' ' LZP-1330-26 (B*

'- d' Revision 1 [',

'iarcn 18, 1982 4' I#

17

7. , .

As HRSS SYSTEM AIR RETURN TC SUPPRESSIDA {

. ivo o)

POOL, 1(2)CM-090. n{

v.

9V f

2) Place the UNIT 1(2) POWER switch in the ((

OFF position. }'.

((.

$ B 3d G. gg MLISTS 3: p qu 1. None. g y '"

H. Tgggj,g g g g G Q TIONJ g g G Q ), f' !

E:

m~

1. None. h

. 12 ".; .

L  !!

) I" b

r

. e.

F'7) *

{. e R

8

l;;

n-L.

f$

k l 4

k..

E E, b, '.

y-h?

.- r.

Ml?

aa L

y.

i' E

U.

ki; h

(i.?r g)F l,

,mm~==*- -m~~ -'~m * .ws*

~ . . ~ .

. . . .~...- - . -

t t

D'

._ , -. _ j L.

i

,, 3 .,

LZP 1330-26 [

y .

Revision 1 i L..

  • March 18, 1982 r 18 sI 7e

"" f ATTACHMENT A t VALVE LISTING g.

7, s.,

M k

'i Q AV-1 Sample Flask #1 Inlet' k.*, '

Sample Flask #1 Outlet

{(

r SV-1.2 i l

M~ Sample Flask #2 Inlet *

.g SV-2.1 u.s {L SV-2.2 Sample Flask #2 Outlet [

i w<

r, . p W SV-3 1 Sample Flask #3 Inlet j

.g SV-3.2 Sample Flask #3 Outlet {

. 3 4 SV-4.1 Sample Flask #4 Inlet E.

Sample Flask #4 Outlet l F SV-4.2 I.U -

SV-5 Sample Purge t

[

i '

' ", h. AV-2 CASP Outlet <

2 SV-10 Nitrogen Inlet {

'T. .- y

..2 s iM I

. i t

r-e.

'l r

5

[,

L 4

'3

('

g u

i er m

s inA

, V La e

.p I
s I, s c.

I.

e. l.
.9

fil  !

6. ,

~ *'

s... . -7m-- - + *-*u----*~

,-a.m.,--

-- . . - - , . , .--,y v -- , - - - - - , , _ . - - - . - -- -- .,- . _ _ - - - - - , - - - - -

-  ! (

>/ 7

, f.. .. l, ,

,t

, .- 4 t.

i I

p .

ATTACH}fENT B LZP 1330-26 h Revision 1 e

~

19 i <

  • tinai-
  • ~

j, P Determination of I-131 equivalent concentration of the con ta intnent L,i t air grab sample in the event that ensputer analysis is not available. -.....

f h

n  !.

1. Determine the I-135 concentracios in the containment [

air grab sample from Step 7.7 I

., F

2. Determine the I-135 concentration in the containment air N at T , the cima at which the release was made to the i

'j cont 31==ent, using the following equation: -

Q~ A k2- I-135 concentration (uci/ce) at T, = ,_3e t v

n ate: A = I-135 concentration (uci/ce) frem p procedure Step 7 7 .

[4.

e = 2.718  !

pr ~

d A= 1.724 E-03 min decay const. I 1 I t= Sample decay time (sin.) - -

F[ teactor shutdewn to sample time ( a T) i

$ I .

5 l

S 3. Determine the concentration of I-131, I-132, I-133 and I-134 using }

che following celationships:

.- e

~~"' <  :

, y I-131 Concentration (uci/ce) = I-135 concentre.cion x 1.0E-01 .i

{

  • ~4

't I-132 Concentration (uci/ce) = I-135 Concentration x 9.23E-01 l.  ?

. i'

- y I-133 Concentration (uci/ce) = I-135 concentration x 6.85E-01 ,(t h i

/ ^' [

I-134 Concentration (uci/ce) = I-135 concentration x 1.846 p Deternine the I-13I equivalent concentratien of all iodine concentrati6ns.

4 in the contain=ent air using the following equation:

t k

Iotal I-131 Equivalent = I-131 concentration + (1-132 Concentration)(0.036)

[

Cencentration (uci/cc) t f

~

+ (1-133 Concentration)(0.027) + (1 ' S - wc - tration)(0.017) 0 0

F

"'"' + (1-135 Concentrati.on)(0.084) $i m ,

lh1 I

i 'Mi, i

b-(L  ;

  • e Q w

^ .

[ ,3c e,

~. . r, '

1 < .

.[s ,.

(

e- - f(-

s W

L LZP-1330-27 f~ Revision 1 g

. 4 Parch 19, 1982 p I f i pj k; S AMPLIf4G CF RE ACTOR CCOL AhT OFF-GAS AT THE HIGH RACIATION SAPPLIhG SYSTEP ,

c

[>

p't i.

t ,

, 4 y --

g,s d ' ,4- A. P,UR P C Sj

~

The purpose of this pr 'idure is tc celineate a metnod 6 of ootaining a reacter ,3alant of f gas sa.nple at the High [

[Gp L

Radiation Sampling Systs t (HRSS) during normal ano post- [C accident conditions. Tais procecure i ncluoes tne steps h to route gas to the Cheeical Analysis Panel (CAP) and g,

tne Chemical Monitcring Panel (CFP f er, nydrogen anal ysis. if tw a B- Ef.fE3f.yC_gi

.r -

b[ 1. Sentry Equipment Corporation, Pcst Accicent Sampie h System, Vclume 1.

2. LZP 1330-29, " Sampling at the'High Raciation $ampling [

' System (Valve Operation at the HRSS Valve Control {

s Panel)." b b L7P 133C'31, "HRSS Sample Mcvement."

- {

i 3. (

b N 4. AAIS,-CCP-0031., "BWR Coolant Radionuciide Analy5is."

^$ C. PREREQUISITES p

The operator should oe f amil iar with tne cperation h

'"'~

1.

of the HRSS panels.

t r

-% 2. Estaolisn ccmmunications witn the Unit Auclear [

y Station Operator (NS0).

i

3. Verify that argen, and nitrcgen, apprcximately 100 psig, is availacle at the Liquid Sampl ir:9 Panel (LSP), CPLD8J. i
4. Equipment:
a. Reach rocs., [

l r

c. Griotong. r 9: 1
c. Re.3ctor coclant ctf-gas sample octtle witn e k

septum.

L  !

2 -

, F~q *l l

(:,. f.'

)

C. . . . _ , . _ ,

rp ,

k

. . .- ~ a p.>--x--..--..--.-. . . . . - . . . . .

y:

p

+

. . p

~',

15 LZP-1330-27 4 J.

' Revision i Maren 19, 1982 fg, n

> :)

b

5. The sample must nave oeen obtainec in acccrdance k" with Reference 2 prior to performing this procecure. [

p " [

O.

P R,,3Q UT I O N S t I[, 1. A Regulatory Guide 1.3 or 1., release of fission  ;

b- prooucts i mplies extremely high levels cf O l.

radioactivity. Dose rates may be nign encugh to

["

& prevent entry into many areas of the plant tnat are normally haDitable. Rad / Chem Supervisicn snould be h h contacted pricr to entry into any area when such a e

release.of fission products is suspectec.

., ((.

C N 2. wear radiation cosimetry as recomner.ded by Rac/ Chem f Supervision. '

rr b 3. Wear protective clothing and respiratcry protection  ;,

as reconmencec cy Rad /Cher Supervision. ll p

Apprcpriate survey instruments shculd De availaole

' b

4. T for monitoring during this prececure.

0 I"l E. LI QTATIONS ANC AQ,I,,,gg ,L b 1. Notify Rad /C9em Supervision if any prcolens are ji:

encountered at the HRSS panels. {

eg r

2. This procedure, though i ntended for use under post-accident.conditons, can ce used fcr sampling at the I;-

HRSS panels during normal operaticns, during knicn [

  • the precautions may nave 1inited applications.

However, normal routine sampling precauticns snoula ce coserved.

5 F. PRCCEDURE

[

i hE.5.5 b

For noun names associated aith tne valves operatec p In this procecure, refer to Attachment B. .

3 y I-

1. Prepare the system for sampling in accordance with the foilowing: ~

tT

g. :

ts.: a. Install tne neeale fl usn tcol . k 99 m [!

E p:- (

c.

u

~ ~ " ~ " "

k

- t

- f:  ;

L

. r:

~

a h

L e

U" LZP-1330-27 f

h. . Revision 1 }

March 19, , 1982 l 3 L

{? ' ' '

o. Verify the following valve lineup: b i

h'[ 1) RC-V-1.1 (closed).

w

2) RC-V-1.2 (closec). l 0

4 p- [

(h 3) RC-V-1 3 (closed).

,r -

j ex. 4) RC-V-1.4 (closec).

(O  : [,

" 5) RC-V-1.5 (closed). )

6) verify RC-V-* i s cicsed. Ccnnect the {

{i" p,,

flusn water nose to RC-C-1 anc cpen the t.

flush water l i ne valve. [>

.e.

7) RC-V-5.1 ( cl os ed ) . '[

.{ f-

8) RC-V-5.2 (closec). p

, r _..

L Li 9) RC-V-4 (cl osed ) . I-t

10) RC-y-2 (closec). [.

cg l

11) RC-V-7 (closed). [

b

12) R C-V- 17 (closed).
13) RC-V-16 (closed).

j ]?

g} 14) RC-CV-1 (BYPASS). j t.

l 15) RC-V-19 (BYPASS).

1 4

I

16) RC-CV-2 (9 o' clock). [

i W 17) RC-V-15 (closca). [

~

i (J

18) RC-V-13 (closec).
19) R C-V - 12 (closed).
20) RC-V-l* (closed). [

I5' ).

Li 21) RC-V-8.1 (closec). f-f i

TW

. b kkk i':

a.

s ., . w-.,,s ,--.e.%~

-y..,w,,

. m -+% e , v e-t 5

L

. . . . - . . - t se4-.-__--__~.----.--....._---..--.- V V

u e

~

h ru t u 1 tb LZP-1330-27 y k

' b: Revisicn 1 [

Marcn 19, 1982 0 4 I-

- [3  !

Lh l

22) RC-V-ll (CLOSED).

rm RC-V-18 (6 o' clock).

23)

{.. j

24) RC-V-22 (YO WASTE). g

,a ,

dl 25) RC-V-9 (open).

p riyt 26) RC-V-8.2 (open).

I b) 27) RC-y-10 (open). [

F, RC-V-3 (open). i.

h$ 28) 5 LL '

c. Dry the expansion vessel RC-EV-1 in accoraance 2 witn the following:

E7 Fi 1) Turn RC-V-Il clockwise to the 3 o'clocx

~

[

position.

,3 l 2*

2) Pull cpen RC-VREL-2. When tnere is a  !

sharp increase in pressure incicatec on s RC-G-3, release RC-VREL-2.

{# b k

3) Acjust RC-VREL-2 until RC-G-3 incicates  !

approximately 2C psig. Ory RC-EV-1 with argen for a minimum of cne (1) rinute.

{

l.

4) Turn RC-V-11 counterclockwise tc tne 9 o' clock position to permit RC-EV-1 to [-

t

vent, then close RC-V-9.

l k l Evacuate the expansion vessel ano sarple lines i c.

in accorcance witn the fcilowing: f; Install the ciluted gas sample cottle on  !

1) i the front panel neecle.

Open RC-V-13 anc then open RC-V-12 anc 2) evacuate until RC-G-2.1 anc RC-G-2.2

'?

indicate a minimun cf 22 incnes of mercury.

3) Turn RC-DV-2 to the 6 o' clock pcsition [

$[ and continue tne evacuation urtil RC-G- [

Lw 2.2 inoicates tne same reaains as RC-G- r 2.1 or a mir.irun of 22 incnes of mercury.  :

  • ) Close in creer RC-V-13, RC-V-10, anc RC- l l

v-12. Recora tne vacuur en RC-G-2.1. on j:

rr i

e

.m.w.

m,. . --

  • -e.*,m, v w n ,

. .. . g.j p

ll.' ll P E ra F LLP-1330-27

.f Revision 1 C March 19, 1982 L

-5 i tt  !

h** LRC Fcrm 1097A (Attachment A). nait for sE P

a minimum of twc (2) mirutes anc verify that tne vacuum is holding.

{

g ,.

f I

5) Turn RC-V-11 slscad g to tre CLOSEC

&~ position. y E.

[;

u

6) Turn RC-DV-2 to the 9 o' clock pcs i ti on . '

e.

[

h

7) Open RC-V-14 anc verify the pressure on RC-G-2 2 is approxinately 1 psig. [

t.

e. Purge the sampie 1ines in accordance with tne {;;

f Oy f ol l owing:

I Open RC-V-8.1 t-m 1) is

2) Open tne sample source val ve RC-V-1.1 (- p 1.2, -1.3, -1.4, -1.5) for tne sample to a.

(.

De cDtained* r_

?f t.

G

3) Sl owl y open RC-VREL-1 unti1 RC-FI-1 (

p indicates 35-40 inches water. Purge for

((g a minimum of five (5) minutes.

v.

4) 51owly close RC-VREL-1 unti1 RC-FI-1 l'-

I, ty' indicates 12-15 inches water. Continue b the purge for a minimum of cne (1) minute. $

5) Close RC-V-3.  ;

g 11 6

2. Sample in acccreance witn the fcilowing: 7

[ a. Cpen RC-V-2. j ~.

M[ (

D. Adjust RC-VREL-2 until RC-FI-2 inoicates 18-22 Y incnes of water. Purge for a minitur of tnree 3

t (3) minutes.

J.

c. Close RC-V-8.2.

Close RC-V-8.1.

d.

r 7 e. Cicse RC-V-1.1 (- 1. 2, - 1. 3 , - 1. 4, -1 5). {

J:  !

At the Valve Control Panel, CPLC9J, secure the m;

f.

sampling lineup in accercance witn Reference I steps F.1.c.e) enc P.1.c.2).

lg 2.

i I

I r k

k l-t (e e spe. ym

" -NuluW'**

WN1F*f4Y4i-

L 7-___....__._.._.____.._ r IX E

. p 2' .

.ki l

un LLP-1330-27 /

' *E f'~f Revision 1 Marcn 19, 1982 -

L rn- 6 k

,[j[

g. Cpen RC-V-7 and tnen open RC-V-9. ts-
n. Adjust RC-VR EL-2 unt i l RC-FI-2 indicates 18-22 h l

inches of water. Flush witn demineralizea I water for a minimum cf three (3) minutes. {a n.

s c:

kU i. Close RC-V-7. i.

j. Open RC-V-3. g'n y

s.

f K. Adjust RC-VREL-1 until RC-FI-l indicates 35-40 inches of water. Flush with demineralized i EM water for a minimum cf one (1) minute. Close Is RC-V-3. f...

E

1. Cpen RC-V-1 1 (-1 2, -1 3, - 1 4, -1.5). Flusn

$gm/j witn demin water for a minimum of five (5) A minutes.

6

-1 5). S F7 m. Cicse RC-V-1.1 (- 1. 2, - 1.3, - 1. 4,

(:

N2

n. Close RC-V-4.

gL o. Secure the system li neup in accordance witn (

Reference 2, steps F.1.d.8) through F.1.f. f i b I

p. Open RC-V-9, wait approximately five (5) seconcs, j u J

and close RC-V-9. i l <

1.

p.

q. Open RC-V-16. '

F1 r. Snap open RC-V-9 and wait for cne (1) minute. 0 t

y t

g y[m} s. Cicse RC-V-16 anc tnen close RC-V-9.

t. Turn RC-V-ll .cou_n3, erg,1,cQ w113 to tre 9 o' clock F

Of positicn. The pressure reading cn RC-G-2.1 is '

ku normall y Detween 8 and LC psig. Reccra tne I reading cn LRC Fcrm 1097A (Attachment A). i p.

r f g[P $g u. Verify with the CMP, OPLE4J, operator that the {

' gas chromatograph as reacy tc receive tne  !  ;

sample. l [

g.,,  !  !

$u J4! v. Cpen RC-V-15.

[

I

(

pg w. Instruct the CFP, OPLc4J, cperatcr tc cegin L

,{

loading tne gas enronatograph sample Icops.

FF-

!\ ~

c_

-._.n,--,. . . _ _ - _ . . .

.~

c L

- i K L Eu [

I I^ LZP-1330-27 Revision 1 U(

b[. Parcn 19, 1982 fj 7 h F

[94

'" x. Upcn nctification frcm the CPP, CPLE4J, cperatcr h O

that all icops are fill ec, close RC-V-15.

m

(:f , (

mA y. The pressure indicated on RC-G-2.1 is normally 5 ana 7 psige record the reacing on LRC Form ft EN 1C97 A (Attachmert A).

EN h,

3. Octain tne cilutec gas sarple in accorcance with

, the following: [

n: l' '

U a. Turn RC-CV-2 to tne 6 c'cicck positicn. Wait  ;

until tne pressure on RC-G-2.2 returns to 1 j

> f$ P5i9 Ek:

b. Turn RC-CV-2 to tne 9 c' clock positicn. Close !c RC-V-14.

g- s V4 c. Remove the griptcng containing the diluted gas b sample and place meninc snielcing.

' VS CA 4. Flush the system in accorcance witn the fcllowing:

p? a. Verify RC-V-15 is cicsec. Turn RC-V-ll jj counterclockwise to tne 6 c'cicck positicn. p D. Open RC-V-9, RC-V-7 anc RC-V-8.1. k

,  ?

^: I l

  1. c. Adjust RC-VREL-2 until RC-FI-2 indicates 18-22 I incnes of water. Flush with cemineralizea y water for a minimum cf one (1) minute. [

L I Open RC-V-8.2. E d.

h '

% e. Cl cse RC-V-9 anc RC-V-7.

2

f. Adjust RC-VREL-2 until RC-FI-2 inoicates 18-22 c, inches of water. Flusn witn cemineralized

% water for a minimum of three (3) minutes.

t P

n g. Close RC-V-8.1. ~

5 l I;

n. Turn RC-V-11 counterclockwise to the 3 o' clock position.

EmL i. Open RC-V-9. g

-r J. Pull open RC-VREL-2. when trere is a snarp

[$ increase in pressure inoicated on RC-G-3,

'" release RC-VREL-2. Acjust RC-VREL-2 until RC-c: i

/

<- 3.

t

- - - ~ - .- -- .

t W...-___....... .. . - - . - . --

}. -

4 a

,:. h l

j.

E y'

f, LZP-1330-27 i L' Revision 1 March 19, 1962 8

!?. '

?

G-3 incicates 20 psig. Flush with argen for

  • a minirrun of three - (3 ) minutes.

p(q.

k. Close RC-V-9.

[][ l. Open RC-V-10.

- e. . 1

m. Turn RC-V-11 counter ci cckwise to the 9 o' clock p' position ano allo RC-EV-1 te vent.
n. Clcse RC-V-10. _

ET. o. Turn RC-V-11 clockw i se tc CLCSED.

h.

uu

p. Open RC-V-8.1.

P Adjust RC-VREL-2 until RC-FI-2 indicates 18-22 (f, c.

inches of water. Flush with water fcr a minimum rm of one (1) minute. v p.

Ei r. Terminate flushing oy cicsing the folicwing:

@ 1) RC-V-8.2. *

{bi  ;

2) RC-V-8.1.

E h,.f 3) RC-V-2. ,!

4) RC-V-4,. Ib c Cicse the flush water valve anc ciscennect the id s.

flusn water from RC-C-1. i r

At the Valve Control Panel, CPLC9J, perform t.

M";n t.

h the folicwing:

1) Secure the sample ccoler water flow. i; S e s
i. . ,
2) Close the remote ficsh isclation valve. {

?

5. Transport the sample to the sample preparation area ,

E[p ]

in accordance with Reference 3.  ;.

l-

6. Prepare the sample for analysis in accordance with h the fol1owing:

{

a. '

n rap the vial in plastic wrap cr seal it in a pl ast i c t:ag. 3

{}-

u.

p-i r

o

r. 1
r. .
  • ;(

LZP-1330-27 Revision 1  ;

Marcn 19, 1982 v 9 -

i i C D. Lacel the sarple in accorcance with tne following: .

1) System samplea ano sample lccation. .

"~

2) Sample time. ,

e Sample cate. y

((. 3) k h;. r s

4) Sample volume.

., I.

5) Initials. r d  ?
6) Survey results.

b 7. The sample volute in tne vial is estimatec in i!

accordance wi tn the fcilowing:

m 6" L1'4i

/ V =V, V, *(P, + 14.7) v g p1 + 14.<3 s.

m 7 = Sampl e vcl ume in ml. f.

where V

[. L V

g

= System vol ume (RC-EV-1 anc 1ines t

to RC-V-15). ,

Ca, V = Volure of RC-DV-2.

V3 = Total glass vial vclume. p P = Pressure read ing f rom Step F.2. t. [V r

q y l

6 P 2 = Pressure readins fror Step F.2.y.

.y 8. Analyze the sample in accordance with Reference 4. ..

[;i 1

MH e

~

.f.

ff The results will ce in uCi/r.1 of cff gas not reactor .

' water. .

fy 9. Report the sarple results to tne Rac/ Chem Di rector I LC f or eval uati on.

Route all output aata anc calculaticns to Rad /Chen v4 10. -

t; Supervisicn fcr review.

11. Tc cisocse et the reacter coolant off-gas sample.

c proceec in accoraance with the f olicwing:

A

!'~

_m . . _ , 3

[L y, t

2. f x

-b-

"D _

y L

t, m LZP-1330-27 h Revision 1 [

I March 19, 1982 [

10  !.

W t M

A a. Verify the following valve 1ineup: {

1) RC-V-1 1 (closed). i k ,
2) RC-V-1 2 ( cl osec ) . J '

ri-

] 3) RC-V-1 3 (closec).

4) RC-V-1.4 (closec).  ::

'y LU 5) RC-V-1.5 (closed).

po 6) RC-V-1C (cicsed).

g 7) RC-V-ll (CLCSED). {;

8) RC-V-12 (closec). Fl-
h. t
9) RC-V-13 (cicsed). {

,tm

$ 10) RC-V-14 (cicsed). [b RC-V-15 (closec). f' 11) b RC-CV-2 (9 o' clock). P

12) y.

I:.

i Install the ciluted gas sample octtle on the 7

ti b.

frcnt panel needle. 3 F

Cpen RC-V-13. b c.

b

o. Open RC-V-12 and evacuate until RC-G-2.2 E indicates a minimum vacuum of 22 inches mercury. h.

@ Turn RC-CV-2 to tne 6 c'cicck positicn and h'I

$ e.

continue the evacuation until a rir.irum vacuum  !

j of 22 incnes of mercury is indicated on RC-G- [-

2.2. [

h 5:

f. Cicse in orcer RC,V-13 and RC-V-12. lJ E (

N g. Cpen RC-V-14 ano all ow the octtle to pressurize to approximatel y 1 psig as indicated on RC-G- [

2.2. {.

4 i U

h. Clcse RC-V-14 7; i s p

}

r x

.~

-  : .n c~ .. . . -

D

. . . .~ ~.

p

'd 5.

LE' y.

b.I r' .

y i.

LZP-1330-27 IN Revision 1 fj C March 19, 1982 y 11 pre {.

[7" i. Open RC-V-13 and RC-y-12 and evacuate until [-

RC-G-2.2 inoicates a minimum vacuur cf 22 inches f-if T mercury.

[.

b J. Close in orcer RC-V-13 and RC-V-12. [

P m

g k. Cpen RC-V-14 and allow the bottle to pressurize h to approximately 1 psig as inoicatea on RC-G- [F 2.2.

m t'

1. Cicse RC-V-14. I; rg 'n . Repeat Steps Fill.c tnrcugh F.11.1 trree times I

h; to remove all racioactive gases.

n. Remove the sanipis cottle f rom the panel.
o. Survey the sample bottle and dispose of as i directed by Rad /Cnem Supervision.

>C w.

s c. qs_ga u sis a

p

.- 1. None.

H. T((g lC( y g yFig TJONJ {fjRMC_jj, -

8 ';

l. None.

h e(c l's E

E e t-E i-b.

i l

e

,a  ?

t . -.

..._......._....a_.m.. -_.o

.  ; : u _ a u.. sc a _. m - m _. __._ . . .__ _ .

._.u .~ . . .. . ,_

LZP 1330-2/

' Revision 1 1 ATTACllHENT A Hareh I'1,1982 1aSalle County Station 12 I IIRSS Analyses Date*

Conductivity LZP 1330-23 Dissolved Oxveen.LZP 1110-23 pH, LZp 1330-23 J ta nda rd iza t ion ,pH-41ni t / Time : Sample Init/ Time: Calibration luit/ Time:

Eccire. Water Temperature, C:

. Calibration Check init/ Time: 3,p , g .g.empe e r% "C:

tieasured Conductivity,umho/cm: Recirc. Water 0 Conc.,mg/l*

Heasured pil: (PH -7) 7 7* SamMc Init/ Time: ,

Correct the measured conductivity to Ituf fer pil Value: i Check SAT /llHEAT,1.1 0 pil units; 25" C using the following formula: Sample D.O., og/1: .,

l.

,'! Sample Init/ Time:

, Sample Temperature, "C: C , ,, C2-[0.018F(5.8E-5xTg)) _

1 + 0.018 (Tg - 25 C) Off-Cas LZp 1330-27 Hensured pil:

Vacuum, RC-C-2.1., Step F.I.d.h.

' II the sample pil > l.5, correct the pil to Where: Cg = Conductivity corrected to Pressure, RC-G-2.1. , S tep F. 2.t , t 25,C in accordance with the following 25 C - Pressure, RC-C-2.1. ,St ep F.2 y. l formula C2 - Hessured Conductivity T

ll pilt = pilg + 0.03 (Tg - 25)

Tg = Sample Temperature, C Sample Inlt/ Time: '

'i

'l Where: plir a pil corrected to 25 C Comments:

pilg = measured pII Tg s Sample Temperature, C t

h r-i D t e

I

' Reviewed:

ph at 25"C: Conductivity at 250C, umho/cm:

' I,R'f: FORH 1097A

!.u  : $.3 $ S:$) f$UI k'$$ hb b bbkl $ BIN h b b b hhd b

- _ .._w... -

3 . p .. ..

'y LIP 1330-27

- Rsvision 1 March t9', 1932 e 13 I~ ATTACHMENT B

~

VALVE LISTING RC-V-1.1 Reactor Recirc Loop B Sample Cutout Valve r-- - RC-V-l.2 RT Demin inlet Sample Cutour Valve n;

"* RHR Loop A Sample Cutout Valve RC-V-1.3 RC-V-1.4 RHR Loop B Sample Cutout Valve .

h'

1. > '

RC-V-1.5 RT Demin Outlet Sample Cutout Valve RC-V-2 Sample Source isolation Valve

_ RC-V-3 Sample Purge Cutout Valve  ;

(~ Flushing Water Isolation Valve a RC-V-4

~ RC-V-5.1 Pressurized Sample inlet isolation Valve .
p. '

RC-V-5.2 Pressurized Sample Outlet Isolation Valve I,

I.' RC-V-7 Diluted Sample Bypass Valve

[ 5 RC-V-8.1 RC-SF-1.2 Inlet isolation Valve l

,r-RC-SF-1.2 Outlet Isolation Valve

~

RC-V-8.2 I. _L RC-EV-1 Isolation Valve i RC-V-9 i

n f El: RC-V-10 RC-EV-1 Evacuation Cutout Valve y RC-V-11 Off gas 4-way Valve h i

e2 RC-V-12 Argon to Air Ejector Cutout Valve f G, RC-V-13 Off-gas Vial Evacuation Cutout Valve  :

Et RC-V-14 Argon Supply to Off gas Vial Cutout Valve .

Ly$ RC-V-15 Off-gas Sample to Gas Chromatograph Isolation Valve i

RC-V-16 RC-SF-1.2 Argon Purge Cutout Valve [

RC-V-17 Reactor Coolant Grab Sample Cutout Valve RC-V-18 Reactor Coolant Undiluted Sample Backflush Cutout Valve. +

pp ri

" Reactor Coolant Undiluted Sample injection Valve j RC-V-19

+

F RC-V -20 RC-C-1 Fi?1 Valve b.

RC-V-21 RC-C-1 Isolation Valve RC-V-22 Liquid Sample to CAP isc,lation Valve

. = -

--s- _ _ , _ -. --- , -.. .,.-,. - . - - _ _ , _ ---

. ~. -_ _

h y_ . ,

p

, t..!

b.. .- LZP 1330-27 [

,- - s Revision 1 fg

  • March 19, 1982 E-ATTACHMENT 8 (Cont'd) 14. (Final)' E Q ,

l' F

e m 7 b '

RC-DV-1 Reactor Coolant Diluted Sample Injection Valve ' I.

E.

RC-DV-2 Off gas Sample injection Valve

}

U- Reactor Coolant Purge Throttle Valve (

RC-VREL-1 RC-VREL-2 Reactor Coolant Sample Throttle Valve W. .

l f .

'%fA i

g, .

?*

F.

T en g

s

- .?

b".

gw 4.:

g t

t i' .'

ky. i.g.

r. 11 L

3

  • f.e.

V E f PP, W+

bls b\

i 1 'V-

[' ,'

b g

I.

[

7 r 2 i e.

T I ,

u gg l l-e i

n a t.

~- - - - - . . . . , - . -

t h,.

n. .

T.

-t

_g .

l

[

, UI.

f LZP-1330-26 L

.;g Revision 1 [

. Lt Parcn 19, 1932 [

1 l pp i

,,3 di SAMPLING OF PROCESS WATERS CONTAINIhG RADIOACTIVITY [

E AT THE HIGE RACIATION SAMPLING SYSTEP l-e.r..,

z..

i A. PURES_{

[L

,m g.g The purpose cf this procedure i s tc delineate a method {

Lw of obtaining samples of the crywell sumps anc FRSS waste t

[

tank at the High Radiation Sampling System (HRSS) curing normal and post-accident conditions. s

-]

sa B. REFERENCES L[

y n~ 1. Sentry Equipment Corporation, Post-Accicent Sample

{ System. Volume 1. }

t-t

2. LZP 1330-29, "Sampiing at tne High Radiation Sarr.pling i:

System (Valve Operations at the HRSS Valve Control [

Q'd Panel)." {

s W 3. LZP 1330-31, "HRSS Sample Movement." 7 g  !; ,

AAIS-CCP-0001, " General Radionuclide Analysis of a f 4.

Liquic Sample". [

Q ,-

12 LCP 410-1, " Preparation of Samples for Garma Ray [

5.

Spectror.eter M.easurements." {

g f N C. PREREQUISEfj f, -

1. The operator s.icula be familiar .vith tne cperation [

t

=

}'

of the HRSS panels. [.

I-

2. Establish ccmmunications witn the Unit huclear [.

9 g Station Operator (NSO). {.

l l 3. Equipment: 7 i

a. Reach rocs. f g.

i

o. Sarple cart / cask assemoly.  ;

l d[U c. Sample bcttle witn septur, 15 r.l. L Q* d. Needle flusn tool with cemineralizec =ater [

  • filled sample bottle and Septur. [

t 7,

n ,,5 h

a g ~

. . ~ .

< - , . - ~ . . . _ _ . . _ _ _ _

I O

> f.V' s h O"E l

I!

r. '

e

  1. p LLP-1330-28 E Revision 1 March 19, 1982 fn 2 I' p./

p b} e. Shi el ded Syringe assembly. I L

L The sample rust nave been obtainec in accorcance te PP Eg, 4.

with Ref erence 2 prior to pe rf ormi ng tni s procecure. [

E

5. Ensure nitrogen pressure, approximately ICO PSIG, (L 3-- is available at the Liquid Sampling Panel (LSP),

t

  1. OPLOBJ. h p"

q h.

~ D. PRECAUTIONS

\; ,

1. A Regulatory Guide 1.3 or 14 release of fission gy procucts implies extremel y high levels cf h

((

radioactivity. Dose rates may De high encugn to [

p prevent entry into mar.y areas of tne plant tnat are ncrmall y hab itabl e. Rad / Chem Supervisicn should De {

,VZ contacted pricr to entry into any area when such a Le release of fission products is suspectec. y E

wear raciation dosimetry as reccmzended oy Rac/Cnem t.

77 2.

Supervisicn. (

3 h$ kL ry 3. Wear protective clotning and respiratcry prctection as recommended by Raa/ Chem Supervision.

{p

4. Appropriate survey instr uments shcul d De available . . ,

for monitoring curing this prccedure. f

((

tiW

5. The splash box coor of the Liquia Sample Panel (LSP), I OPLC8J, must be closeo curing panel line purge and pg.

gg-grab sarple cellection operations. (

f 5

E. LIFITATIONS AND ACTIONS P

.J L W l. Notify Rad / Chem Supervision if any prcblers are F encountered at tne HRSS panels.

l

2. This procedure, though intended fcr use unoer post-accident conditions, can be usec for sampling at L the HRSS panel curing normal cperations, curing which the precautions listed may have limited F

((n E applications. However, no rmal routine sanpling 1

precautions thould be ooservec. b r F. f ECQ DSR,j

6 .

r.

ry bb e

ki E

)

A '

-., .- _ . ,, --~ .

s 7

5

, , . - . .. . , ~ . . . ,

"z. .

i w

V;O N ,-  ;

u. ',

Ri' LZP-1330-28 Revisicn 1

' @3 Marcn 19, 1982  ;

3 5, r,c ,

i r !'

wd. - g For the neun nar.es associatec with tne valves operatec FJ

[AU in this procacure, refer to Attachment A. [

37 1. Perform the fc11owing valve lineup at tne LSP, '

OPLD8J*

'.6 }_. (

a. RW-V-1.1 (closed).  !

> c:: i F

64, o. Rw-V-1 2 (closed). e p%

p.

r c. Rw-V-1 3 (closod).

LI't

d. Rw-V-1.4 (closeo). 3 C) e. Rn-V-1.5 ( cl osec ) .

BR '

f. RW-V-1.6 (ciosec).  ;

I .

b [g~3 g. RW-V-1.7 (closed). l l

h. RW-V-1.8 (closed). -

,,[_

U L2 i. RW-V-1.9 (closeo).  !.

pj j. RW-V-1.10 (closeo).

C k. RW-V-2.1 (closed).

rr -

1. RW-V-2.2 ( cl ose d ) . -

g] I

m. RW-V-2.3 (closed). i.

l I,I, i RW-V-2.4 (closed). I' Lm-

" n.

pn o. RW-V-2.5 (closed).

[

" d'

'l

p. RW-v-2.6 (closec).

m kf q. RW-V-2.7 (closec). ,

Lt t'

r. RW-V-2.8 (closed).

me 3 r

N; s. Ra-V-2.9 (closec). s

u. .

r!' l LL i e

i-

[- t:

? I 02

. _ _ - - . - - - . . ~ . . . .

p2-  !

c.

7,. .'

L.

p.

LZP-1330-28 ,

Revision 1

{" i*arcn 19, 1982 ,

4 kb  :

00 t. RW-V-2.lC (closed). i I

e u. Rw-V-3 (closed).

"" v. RW-V-4 (closed). .

{3 w. RN-V-9 (cicsed).

ils l

x. RW-V-10 (closec). t s

~

,j y. RW-V-6 (closed). ,

yy z. RW-V-5 (6 o'ciccx). s E- aa. RW-V-7 (BYPASS).

PP ao. RN-V-8 (BYPASS). i N: '

c-

2. Connect the flush water nose to Rh-C-1 cn the LSP, y ,s OPLC8J, and open tne flush mater line valve. ,
3. To ootain a diluted (1000:1) racicactive waste i I

sample, Lioceed to Step F.6. Tc cotain an uncilutec 75 (15 mi) radioactive waste sample, proceso to Step $

, b5 F.5. If neither, proceed to Step F.4. 1 t

i

4. To cDtain an cpen grab sarple, prcceec in accorcance L with the following at the LSP, CPLD8J or as otnerwise  ;

l directcc: t CAUTION ,

ff.

The splash box coor of tne Licuid Sample Panel (LJP), f OPLC8J, must be closec curing panel line purge anc j i:s

($, grao sarple ccliection operations. t I

a. Cpen Rh-V-1.1 (-1.2, -1.3) depencing on tne {g n sarple scurce, anc recirc for a ririnur cf six i

'd minutes, then cicse Rw-V-1 1 (-1 2, -1 3). [

l l

j.

D. Cpen Rh-V-2.1 (-2.2, -2 3) depencing on the j r

Cy sarple scurce.  ;

j bC r

c. Sicwly opcn Rd-V-4 until RW-FI-l indicates 4- ,

p, Purge to waste fcr a minimum i'

e 8 inches of. water.

of one (1) minute.

Open Ra-V-e, purge a minimum of 50 ml of liquic f l {" L.

c.

to waste, then close Rh-v-c. i t

?

It.: A

..e-..m.-., w .

t vs - .

l.S *

. .f-6u

, 'e ni .

k?'

+>

E k

m LZP-1330-28 fr hIi

"# Revisicn 1 [

Marcn 19, 1962 g c,. v.

5 j,

un

e. Cpen the splash cox cocr and place tre sample g bottl e under Rw-V-6. Then close Pe splasn r;

[4 box coor. ie LO f.

pp f. Open Rh-V-6, collect the cesired sampl e , and I cicse RW-V-6. y gg $

g. Cl o se RW-V-2.1 ' (-2. 2. -2. 3 ) cepenaing on tne ,;

FE sample scurce. ,

L N$

n. Cicse Rw-V-4. Open tne splasn ocx dcor.  :(

y U2 Dry the sample bottle, remcve anc place in a i

(( i.

tote tray for transpcrting tc tne laboratory. E v.

Cicse tne spl asn oox acor.  ;

V 0,;; '

i-

%f J.

At tne Valve Contrcl Panel, CPLC9J, secure tne sampling lineup in accercance witn Reference f T 2. Steps F.2.c.15) tnrougn F.2.c.17) OR Steps [

g }gg F.3.f tnrough F.3.g cepending cn tre sample {<

source sampled.

k. Fully cpen Rw-V-4.
1. Sicwly open RW-V-3 until Rw-FI-l incicates *-

8 incnes of water. Flush with cemineralized ,

Eg gb water for a minimum cf two (2) minutes. [:

[

m. Cicse RW-V-4.

Ei n. Coen Rh-V-1.1 (-1.2, -1.3) cepenair.g on tne sample scurce samplec.

cc kh o. Fully cpen RW-V-3 anc flush witn cemineralizec "

water for a minimum cf six (6) minutes.

bh p. C1cse Rw-V-1.1 (-1 2, - 1.3 ) . p" La

o. Cpen Rh-V-2.1 (-2.2, -2.3) cepencing on tne sample scurce samplea.

E5 i bi r. Sicwl y open Rn-V-4 antil Rh-FI-l reacs 4-6 rn incnes of water. Parge to waste fcr a minimum 3_

[

of two (2) minutes.

hh i

s. Caen Rh-V-6 purge a minin.um of 50 mi cf liquic to .aste, tnen close Rw-V-6.

i t

EI  !

b.' l

't I~,

  • I I,

m I 1 L

.- r

?

f' LLP-1330-28 f L
4 Revisicn 1 p March 19, 1982 t i

6 in l G f' i

t. Close Rw-V-2.1 (-2.2, -2.3) anc RW-V-4. f, e.

c' w At the Valve Control Panel, CPLC9J, align tne r B6 u.

d- LICUID SAMPLE BACAFLUSH switch, for rac aste i side, to the oackflusn line associated with

.p7 tne sarple source sarpl ea. Flust witn (h

' by - cemineralizea water for a mirinun et six (e) minutes. ,

hk v. Align the LIQUID SAMPLE BACKFLUSH switen to f

'* tne CFF position. (

h o

.. Close RW-V-3. L

&[9 x. Cicse the flush water valve anc cisccnnect the f flush water line from RW-Dv-1. {

?

N y. If nc further samples are to os cotained from  !

this sample source, secure tre sampling lineup I .-

I in acccrcance witn Reference 2, Steps F.2.c.19) t QE througn F.2.c CR Step F.3.i cepending on tne I bd [

sample scurce sampleo.

11

-5 f

$n 5 To ootain an u'ncilutec (15 al) racicactive waste

"" sample, proceed in accoronace with the following at h the LSP, OPLD8J or as otnerwise directec

[l-'

L+# a. Place the tottle on tne cart / cask assemoly

I cavity piston.

Turn the direction valve for the nydraulic '.

o.

pisten in the DOWN posi tion anc lower tne cottle [

in the cask cavity. r la u c. Cicse anc cpen tne cask to verify tnat the cover is acrking properly.

d. Positicn the cask / cart under tre LSP undiluted radwaste fill station needles anc set tne craxe. 4 E

l' -,

k Turn tre direction valve for the hyaraulic i.f k"

e.

pisten tc tne UP position anc raise the Dottle ento tre neeales.

Mb t. Cpen Rn-V-1.1 (-1.2. -1.3) cepencirg on tne f i

saaple scurce, anc reci rcul ate f cr a minimum [

l gp cf six (6) minutes.

U2 1 E5 r V

l ~ _;.; - _ _

_.m _ . . __ m .m _, - _ .

. rT : e k[-

h i-r t n-t t:

P i

r LZP-1330-26 "b Revisic7 1 b Marcn 19, 1962 b F- 7 O

g. Cicse RW-V-1.1 (-1 2, -1.3 ) anc cpen Rw-V-2.1 pp (-2.2, -2 3) depencing on tne sanple scurce. [

e, u Sicwly open Rw-V-4 until Rh-FI-l inoicates *- E

n. '

r, 8 incnes of water. Purge to waste fcr a minimum of one (1) minute. (

bu

i. Turn Rh-V-7 to SAMPLE. CD NCT exceec 20 psig [

on RW-G-1 in this step. Adjust Rw-V-4 until f (P

[t Rw-G-1 indicates 20 psig or Rw-FI-1 incicates [

10-14 inches of water. Purge for a nininum cf er one (1) minute.

p g.

$".m J. Clcse Rw-V-2.1 (-2. 2, - 2. 3 ) . f Let Rw-G-1 return to O psig anc wait 3C seconos fh k.

to allow the cottle to cepressurize. [

es t

5 r,g

1. Turn Rin-y-7 to BYPASS. f L

$5 m. Turn the direction valve for a cask / cart g ,,

hycraulic plunger to the DCnN positicn and lower the cottle inte tne cask.

g

n. Close the cask. Release the Drake ard remove  ;

the cart / cask frcm the sample station.

pg kt Install ano secure tre auxiliary srielo en ene o.

l cart / cask assemoly.  ;,

n

~

p. Install ano secure tne neecle flust toci on tne LSP, OPLO8J. 2 o

n I d? At the Valve Control Panel, OPLC9J, secure the q.

J sample lineup in accercance witn Reference 2, f Steps F.2.c.15) tnrougn F.2.c.17) CR Steps f p,

g}

F.3.f tnrough F.3.g cepending cn tre sample '

source sampled.

r. Fully cpen RW-V-4.
s. Si cwl y open Rw-V-3 until Ra-FI-l ir.dicates 4-pa 8 incnes of water. Flush witn cemineralizeo b f: water for a minimum cf two (2) minutes.

At

t. C1cse Rw-V-4.

pr.

I/S u. Cpen Rw-V-1.1 (-1.2. -1.3) cepencir.g on :ne sample scurce.

,yG.

_t-f; p ..

r f?

I>

V F

e L

r

~

L2P-1330-2s g

' Aevisicn 1 ,'

Paren 19, 19c2 ,

8 'r s .

,o

v. Fully open RW-V-3 anc flush witn cemineralized ..

e water for a minimum cf six (c) minutes.

r:

w. Cicse RW-V-1.1 (- 1. 2, - 1. 3 ) .

[ '. x. Cpen Rh-y-2 1 (-2.2, -2.3) cepencing on tne '

D. sample scurce.

Si cwl y open Ra-V-4 until Rw-FI-1 reacs 4-8 e y.

incnes of water. Purge to waste fcr a minimum 7-p '-

of two (2) minutes. '

t

z. Close Rw-V-2 1 (-2.2, -2.3) anc Rw-V-4. {

aa. At the Valve Centrol Panel, CPLC9J, align tne  !

r" LICUID S AMPLE B ACAF LUSH switch, for tne racwaste sice, to the oackflusn line associated with L the sarple source samplec. Flush witn fp cerineralizec water for a rir.imum cf six (e) ,

e minutes. 3 J

L-aD. Align tne LICUID SAMPLE BACKFLUSE switen to (

tne GFF position. F C* '

S CO NCT exceec 20 psig ac. Turn Rh-V-7 to SAMPLE. g e

en RW-G-1 in this step. Slowly cpen Rw-V-4 no until Rw-G-1 incicates 2C psig or Rw-FI-1 [

-(( incicates 10-14 incnes of water. Purge for a 1" mir.imum cf one (1) minute.  %

r

nu Q. ac. Cicse RW-V-* anc let RW-G-1 return tc C psig. {f se.

wait 3C seconos to allow the octtle to ,r. .

- cepressurize.

ae. Turn Rh-V-7 to BYPASS. E at. Secure flusning cy closirg Rh-V-3 f:f.

L k ag. Cicse the flush water valve anc cisccnnect the f lush water line from Rw-DV-1. k pf -

t

~

Yf an. Remove the neeole flusn coci fror tne LSP, p I

CPLD8J.

r- i A ai. If nc turther sarples are to os cotainec froe "

tnis sample source, secure ene sampling lineuo h in accercance itn Reference 2, Steps F.2.c.19) [

!L tnrougr F.2.c CR Jtep F.3.a cepercing on :ne i sample scurce samplec. [

r L_ ,1

- -.i.

o4 ,-- - - - - - . - - ., - , .

?

l. ~

e k

LZP-1330-28  !.

Revision 1

.Maren 19, 1982 ((

F#

5 h

i

6. To ootain a diluted (1000:1) radicactive waste p sample, proceso in accorcance witn the folicwing at i.

e the LSP, CPLD8J or as otherwise directec:

  • b.5
a. Verify Rh-CV-1 is turnec to BYPASS. Fill I reservcir Rw-R-1 witn cemineralizec water.

Open RW-V-10 and tnen RW-V-9. Acjust reservoir

[y

((p -

RW-R-1 until the water level in graduatec [

cylinder Rh-C-1 is 125 ml. Cicse RW-V-lO anc g O' Rw-V-9. 3 f

$N. 8 D. Align Rw-V-8 to the BYPASS (9 c'cicck) pcs i ti on.

p*' ,

Q; c. Align RW-DV-1 to tne BYPASS positicn. .

c. Insert the neecle of the nano cperatec vacuur i

,y *

{De pump inte the septum of the cilutec racwaste L" sample Octtle. g-I

e. Evacuate to tne maxieur vacuum acnievaole witn

>.;,i{} tne nand operated pump. The vacuur PUST oe at LEAST 15 inches of Hg. ,

f. Keep the hanc operated vacuur purp ccnnectec [

3 '

to the evacuateo cottle for tnree rirutes to

ssure that the cottle retains the vacuur.  ;

e

,v.I? t.

La g. Remove the Dottle from the hanc cperated vacuum pump and place the octtle on the cart /casx {g assemoly cavity piston.

gy {.

LM

h. Turn the direction valve fcr the nydraulic f i

pistc. to the DOWN posi tion anc lower the cottle {

g into the cask cavity. Close ana open tne cask

k. to verify tnat the cover is working properly. f[

p

i. Position the cask / art under the LSP dilute 0 f F}J} racwaste fill station neecle and set the oraxe. (

O

cy j. Turn the cirect on valve (cr the nyaraulic l pisten tc the UP posi ti on anc r ai se tne cottle {

bk*?p onto tne neecle. S

"? x. Cpen Rh-V-1.1 (-1.2, -1.3) depencing on tne

[e sample scurce anc racirc fcr six (6) minutes.

Cicse RW-V-1.1 (- 1 2, - 1. 3 ) .

l rv 1. Caen Rh-V-2.1 (-2.2, -2 3) cepencir.g on tne fe '

L" sanple scurce.

7:

i' b2

5.

. "S o -

L t t f'.

.- I ge  ;

ki

[

t (e- I M LZP-1330-28 u Revision 1 ,

Marcn 19, 1922 ?;

yg E3 Il

m. Sl owl y open Rw-V-* until Rh-FI-L incicates 45- 6

?

50 inches of water. Purge tc waste for a e 7t U) minimum of one (1) minute. 1 O'

s

n. Turn Rh-V-8 to BYPASS. r I

i

o. C1cse RW-V-2.1 (-2.2, -2.3). g V

D. At the Valve Control Panel, CPLC9J, secure the r(

ax sample lineup in acccreance with Reference 2,  !

Steps F.2.c.15) tnrough F.2.c.17) CR 5teps  ;

F.3.f through F.3.g cepending on the sample  ;

9 '

i" source samplea.

E

q. Fully open Rw-V-4. t j

S r. Sl owl y open R w-V-3 unti l Rw-FI-l indicates 4- l' 8 inches of water. Flush witn demineralized y Fr ~

water for a minimum cf two (2) minutes. [

YC LN

5. Cicse RW-V-4.

b

t. Cpen RW-V-1 1 (-1 2, -1 3) cepencing on tne j

]'[ sample scurce sampled. Fully cpen Rh-v-3 and {

flush with cemi ne ral i zed water fcr a minimum  ;

7! of six (c) minutes.

61 (

u. Cicse Rw-V-1.1 (-1 2, - 1. 3 ) . *<

g.

! v. Cpen Rh-V-2.1 (-2.2, -2.3) depencing on tne sample scurce samplec.

{

w. Slowly open RW-V-* until RW-FI-l reacs 6-8 k

?? Flush witn demineralizec f.

$2 inches of water.

l water for a minimum cf two (2) mi nu te s . j' L 0 Close in orcer RW-V-2 anc Rw-v-4. f f x.

At the Valve Centrol Panel, CPLC9J, align tne i.

y. {

LICUID SAMPLE BACKFLUSE switen, for tne racwaste i

-3 i I

sice, to the backflusn line associatec .itn ,

the sample source samplec. Flusn witn  ;

ceniceralizec water for a mininum cf six (6) 8 mirutes.

?.)  :

i i z. Ali 9n the LICUID SAMPLE EACKFLUSP saiten to i - or 08 the CFF position.

j i as ,

l FU  !

! bb l

r p

r* *1 _o_ . _ _ . . . _ _ _ _ _ _ . . . . _ - _ . _ _ . _ _ _ _ _ . _ . _ _ . _ . _ _ _ .

.n g

V

. V

,g . .

7 s-. ~

b 3

p? LZP-1330-28 .

O, Revision 1 March 19, 1982 f

e ra b 11

.D7

.sc r

aa. Turn Rh-CV-1 to SAMPLE.

.ea r-cs an. Crack open Rw-V-9, ano aco 24 el of water trem l' Rw-C-1 tc the sampl e Octtle, then cicse Rw-V- n.

9* F t

[ ass pV L2e U.9.T,,) e nn: The dilution volume may De changea as directec oy [

[y ld Rad / Chem Supervision. h E

p ac. Turn Rw-CV-1 to SYPASS. {

t ld Place the airection valve for tne hycraulic 6 ac.

plunger in tne DOWN position and Icwer the [

m Dottle intc tne casx. j T

Lu/

o ae. Close the cask. b, p[ af. Turn Rh-V-8 to the 9 o' clock pcsition. {.

{~

ag. Sicwly open RW-V-* until RW-FI-1 indicates 45-r3 50 inches of water. Flush with cerireralizec gDi! t water for two (*2) m i r.ut e s .

b

" ah. Turn Rh-V-8 to SYPASS.

[N <

us al. Secute flushing by closing RW-V-4 anc RW-V-3* ry aj. Release the Drake and remove the cart / cask from h-l the sample station. {

ak. Install and secure the auxiliary shielo en the ,(

e cart / cask assemoly.

al . C1cse the flush water valve anc cisccnnect the h m flush water hose for Rh-CV-1.

~

l{ -:

P l

am. If nc f urther samples are to os cDtained from this sample source, secure the sampiing 1ineup [.

> h'* in accercance witn Reference 2, Steps F.2.c.19) [

through F.2.c CR Step F.3.i cepencing en the 'p t

, GF sample scurce sanplac.

l kb i 7. Transoort the samples to tns sample preparaticn area ,

itn Reference 3. f.

~

,.y in accoraance

, t. c

! " Prepare tne sample from Step F . e: for analysis in }

8.

accorcance witn the f c11 ow i n g : (l'.

[# t i

~. . . ~ . - - .

e.

f ~r O o . _ _ . . _ . . ._ .-

n e:

til f

. E,

}f O

r.

t.

L m

LZP-1330-28 l-

.< Revision 1 Marcn 19, 1982 {(

y r-12 >

\t G2 y

a. Place a 47 mm fiber filter in a new petri-cisn ana place Denind a shielced area with tne cover P[

'Qg4 off.

f. ,

m MH f If less than 500 ul (C.5 mi) cf sample is usec, h campen tne fiber filter with ceionizac mater prior d.

to placing the sample on the filter. f;;-

i.J

b. Remove the small shielo plug from tne top cr @

the shield cask. [

9 '.

3] ~

c. Using tne syringe assemoly, withcraw 2C ut of 7 the Sample and imneci atel y replace tre shiel e e plug.  ;

Tj7 7

r

$3 9 kv-

>N Sample volume anc geometry may De changed at the t g ciscretion cf Rad / Chem Supervision to facilitate j analysis of samples.

g.

g@

    • a. Discharge the sample onte tne fiber filter in .

fl tne petri cisn in sucn a manner that the sample [p is eveniy depositec cver the entire ficer fiiter

.g;l surface. g.

's

e. Place the cover en the petri dish anc tape it i clcsed.
f. wrap the petri aish in plastic wrap ano seal I" E

D 9

Lacel the sample in accordance with sne following: T

1) System samplea and sample lccation. -
2) Time of sampling.
3) Date of sampling.

' l'.

fi.ll~

5) Initials.

k i

4

- a w. jew e - ag -e , -6

, = - - - - - -

t

0. s . . e_ - . . _ _ _ . _ - . _ _ _ . _ . _ _ . _ _ . _ _ . _ _ __ .- .

{b ,

fC, . ,

1.,. o L2P-1330-28 Revision 1 ,

Marcn 19. 1982  ;

ct L 13 p,_st ,

6) Survey results. .

W The sample volume for undiluted samples is tne same [.'

-D$

9. s as the syringe volute dischargaa. For a cilutec eg, sample, calculate the actual volume of sample on i ip the fi1ter paper in accorcance with tne fc11o ing: f

ue V = 52# ,

T

@' 1<

CA:

where: V = The actual volor.e of tne rad-waste  ?

sample to oe analyzed on the fiber [

g)

,N filter in ml . p w.

5 = The vol ume o f the dil uted sample  ;"

cm in tne syringe in ml.

p.

a y

A = The val ve al icuot of sample ccliecteo

[I 7

rv: in the casx bcttle in ml.  ;

a.

  1. " T = The total vclume in the cask k Dottle, the valve aliquct of [

samp,le plus the . vater acced from k h['$

0 the graduateo cylinder in ml. [t y 10. Analyze the sampies in acCorCance with Reference 4+. t

'h w

11. Report the sample resul ts tc the Rad / Chem Di rector (i for evaluation. ['

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12. Route all output data and calculaticns to Rad /Cnem [
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Revision 1.

March 19, 1982" ATTACHMENT A Ifr (Final)  ;

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i VALVE LISTING RW-V - 1.1 Spare '

RW-V -1. 2 Spare t f_'

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RW-V -1. 3 RW-V-1. 4 Spare Spare i

RW-V-1. 5 Spare m RW-V-1.6 Spara j,

, ": 6 RW-V -1. 7 Spare t RW-V-1. 8 HRSS Weste Tank Sample Rect re Valve [

RW-V -1. 9 U-1:Drywell Equip. Drain Sample Recire Valve }*

h,, RW-V- 1.10 U-2 Drywell Equip. Drain Sample Recirc Valve ,

Le; RW-V-2.1 Spare g RW-V -2. 2 Spare g.

( r- RW-V-2.3 Spare Spare t

- (.'" RW-V-2.A RW-V-2.5 Spare [

RW-V-2. 6 Soare F. RW-V-2.7 Spare [

h RW-V-2.8 HRSS Waste Tank Sample Cuteut Valve -

RW-V -2. 9 U-l Drywll Equip. Drain Sample Cutout Valve f

,e RW-V-2.10 U-2 Drywll Equip. Drain Senple* Cutout Valve L RW-V -3 Flushing Water isolatit:rt Valve it RW-V -4 Rad-Weste Sample Throttle Valve

. RW-V-5 Backflush Cutout Valve {-

RW-V-6 Radwasta Grab Sample Valve .

1 RW-V -7 Radwaste Undiluted Sample injection Valve  ?

RW-V-8 Rad-Watte Diluted Sample Cutout Valve E RW-C-1 Fill Valve S 7 RW-V-9 '

A RW-V -10 RW-C-1 Isolation Valve '

l RW-DV-l Rad-Westr Dituted Sample injection Valve s

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