Text

Submittal of 2014 Annual Radiological Environmental Operating Report (AREOR)
	ML15113A621
Person / Time
Site:	Grand Gulf
Issue date:	04/23/2015
From:	Nadeau J; Entergy Operations
To:	; Document Control Desk, Office of Nuclear Reactor Regulation
References
	GNRO-2015/00027
	Download: ML15113A621 (140)
	v • d • e

Q Entergy GNRO-2015/00027April23,2015 U.S.Nuclear Regulatory Commission Attn: Document Control Desk Washington,DC20555-0001 Entergy Operations, Inc.P.O.Box756PortGibson,MS39150 James Nadeau Manager, Regulatory AssuranceGrandGulf Nudear StationTel.(601)437-2103

SUBJECT:

DearSirorMadam:

Grand Gulf Nuclear Station2014Annual Radiological Environmental OperatingReport(AREOR)

Grand Gulf NuclearStation,Unit1 DocketNo.50-416LicenseNo.

NPF-29 In accordancewiththeGrand Gulf NuclearStationUnit1 Technical Specification 5.6.2, attachedistheAnnual Radiological Environmental OperatingReport(AREOR)forthetimeperiodof January1,2014 through December31,2014.Therearenonew commitments containedinthissubmittal.Ifyouhaveany questionsorrequireanyadditional information, please contact Richard Sumrall at 601-437-2115.

Sincerely,

Attachment:

Grand Gulf NuclearStation2014Annual Radiological Environmental Operating Report (AREOR)cc:(seenextpage)

GNRO-2015/00027Page2of2 cc: NRC Senior Resident InspectorGrandGulf Nuclear StationPortGibson,MS39150 U.S.Nuclear Regulatory CommissionATTN:Mr.MarcDapas(w/2)

Regional Administrator,RegionIV1600EastLamar BoulevardArlington,TX76011-4511 U.S.Nuclear Regulatory CommissionATTN:Mr.A.Wang, NRR/DORL (w/2)MailStopOWFN8B1 Washington,DC20555-0001Mr.B.J.SmithDirector,Divisionof Radiological HealthMississippiState DepartmentofHealthDivisionof Radiological HealthP.O.Box1700Jackson,MS39205Dr.MaryCurrier,M.D.,M.P.HStateHealth Officer Mississippi DepartmentofHealthP.O.Box1700 Jackson, MS 39205-1700 Attachment 1toGNRO-20 15/00027GrandGulf Nuclear Station 2014 Annual Radiological Environmental Operating Report (AREOR)

ENTERGY OPERA 11 NS, INCa GRAND GULF NUCLEAR STATION ANNUAL RADIOlO leAL ENVIR N ENTAL PERATINGREPRT January1,2014...December 31, 2014Reviewed By Approved By TABLEOFCONTENTS

SUMMARY

1.0INTRODUCTION

1.1 Radiological

Environmental Monitoring Program 1.2 Pathways Monitored1.3LandUse Census2.0INTERPRETATIONANDTRENDSOFRESULTS 2.1 Air Particulate and Radioiodine Sample Results 2.2 Thermoluminescent Dosimetry (TLD)Sample Results 2.3 Water Sample Results 2.4 Sediment Sample Results 2.5 Milk Sample Results2.6Fish Sample Results2.7Food Product Sample Results2.8LandUse Census Results 2.9 Interlaboratory Comparison Results 3.0 RADIOLOGICAL ENVIRONMENTALMONITORINGPROGRAM

SUMMARY

3.1 Program

Results Summary 2 6 9 9 9 9 22 22 22 23 24 24 24 24 24 31 32 32 TABLE 1.1 TABLE 1.2 TABLE 2.1 TABLE 3.1LISTOF TABLES AIR SAMPLINGDEVIATIONSIN2014 RADIOLOGICAL ENVIRONMENTALSAMPLINGPROGRAMLANDUSECENSUS RESULTS RADIOLOGICAL ENVIRONMENTAL MONITORINGPROGRAM

SUMMARY

3 8 11 26 33 FIGURE1-1FIGURE1-2FIGURE1-3FIGURE2-1LISTOFFIGURES EXPOSURE PATHWAYS SAMPLECOL.LECTIONSITES-NEARFIELD SAMPLECOL.LECTIONSITES-FARFIELD TLD READINGS 4 19 20 21 23 ATTACHMENT 1LISTOF ATTACHMENTS RADIOLOGICAL MONITORING REPORT

SUMMARY

OF MONITORING RESULTS 5 38 SummaryTheAnnual Radiological Environmental Operating Report presents data obtained through analyses of environmental samplescollected.forGrand Gulf Nuclear Station's (GGNS)Radiological EnvironmentalMonitoringProgram(REMP)fortheperiod January1,2014, through December 31,2014.Thisreport fulfills the requirementsofGGNSTechnical Specification 5.6.2.To supplementtheREMP,GGNS personnel installed duplicateTLDsandcollected duplicate samplesduringthereportingperiod.

Radiological Environmental Monitoring Program GGNS establishedtheREMPin1978priortothestation becoming operational(1985)toprovidedataon backgroundradiationand radioactivity normally presentinthearea.GGNS has continued to monitor the environmentbysamplingair,water, sediment,fishandfoodproducts,aswellas measuringradiationdirectly.GGNSalso samplesmilk,ifcommercialmilk productionoccurswithinfivemilesoftheplant.TheREMP includes sampling indicatorandcontrol locationswithinan18-mileradiusoftheplant.TheREMPutilizes indicator locations nearthesitetoshowany increasesorbuildupof radioactivitythatmightoccurduetostation operationandcontrol locations fartherawayfromthesitetoindicate naturally occurring background radioactivity.

GGNS personnel compare indicatorresultswithcontroland preoperationalresultstoassessanyimpactGGNS operationmighthaveonthe surrounding environment.In2014,GGNS personnel collected environmentalsamplesfor radiologicalanalysis.The monitoringresultsfor indicator locationswhencomparedtocontrol locations and previousstudiesshowthatGGNShasno significant effectonthelocal environment.Thereviewof 2014 monitoringdata,inmanycases,showed undetectableradiationlevelsinthe environmentandnear bac.kgroundlevelsin potential exposure pathways associatedwithGGNS.Harmful Effects or Irreversible.

Dama..9.!TheREMP monitoringdidnot detect any harmful effects or evidence of irreversible damage in the current year..Reporting levels When averaged over any calendarquarter,no environmental samples equaled or exceededreportinglevelsfor radioactivityasoutlinedin Offsite Dose CalculationManual(ODCM)

Specifications Table 6.12.1-2;the analyticalresultsdidnot trigger any Radiological MonitoringProgramSpecialReports.

Radioactivity Not AttributabletoGGNS Over previousyears,theGGNSREMP detected radioactivity attributable to other sources.These.sourcesincludedthe Chinese nucleartestin1980andthe accidentatthe Chernobyl Nuclear PowerPlantin1986.In2011,theGGNSREMP detected radioactivityreleasedfrom 6

the Fukushima Dai-ichi Nuclear Power Plant followingtheMarch11,2011, Tohoku earthquake.In2014,the GGNS REMP detected no radioactivity attributable to other sources.Comparison to Federal and State Programs GGNS personnel compareREMPdatato federalandstate monitoring programs.Historically, the programsusedfor comparison includedtheU.S.Nuclear Regulatory Commission (NRC)Thermoluminescent Dosimeter(TLD)Direct Radiation Monitoring Networkandthe Mississippi State DepartmentofHealth(MSDH),Divisionof Radiological Health monitoring program.AlthoughtheNRCTLD Network Program was discontinuedin1998, these results compared favorably to thosefromthe GGNS REMP.TheMSDHandthe GGNSREMPhave similar monitoring requirements.

These programs include co-located air samplingandsharing samplemediasuchaswater, sediment,fishand food products.Both programs have obtained similarresults.The2014resultsoftheMSDH monitoring program compared favorablywiththeGGNSREMPresults.

Sample Deviations

MilkTheGGNS aDCM requires collectionofmilk samples if thereisa commercially available sourcewithin5miles(8km)oftheplant.In2014,theREMPdidnot include milk sampling because no commercial milk production occurredwithin5milesofGGNS.GGNS personnel instead collected vegetation samples to monitor the ingestionpathway,as specified in aDCM Specifications Table 6.12.1-1.*Required Lower Limit of Detection (LLD)Values Analytical lowerlimitof detection (LLD)valuesrequiredbythe aDCM specifications were achievedin2014werewithinthelimitsforallsamples.

Thermoluminescent DosimetersTLDM-50was retrieved wetinthe2nd quarter.TLDM-98wasretrievedwetinthe4th quarter.Similarly locatedTLDdata werereviewedandfound consistent with previousdata,with readings near background.Forthefirst quarterof2014,a higher than averageresultforTLDM-33wasreported.TLDM-33is considered a control location.Follow up inspectionbythevendor, Stanford Dosimetry, determined thattheTLDhadbeen damaged,andtheinitiallyreportedresultwasnotreliable.The sampling field notes show no indication of damagetoTLDM-33 during collection.

The analyticalresultforM-33forthefirst quarterof2014arenotincludedintheTLDdata evaluationsinthisreport.*Air Samples The following air sample locations had reducedruntimesdueto weather-related power 7 outages or mechanicalproblems.As describedinODCM SpecificationTable6.12.1-1, footnote (a), deviationsfromtherequiredsampling schedulearepermitteddueto malfunctionofsampling equipment and other legitimate reasons.Table1.1 Air Sampling Deviations in 2014RunTime Out-of-ServiceSampleLocationDateIn<DateOut (Hours)(Hours)CommentsAS-1PG01/21/1401/29/14 190.76 61.4 Power outageAS-7UH.02/25/1403/04/14168.0432.6 Power outageAS-7UH03/25/1404/01/14 152.46 97QA Power outageAS-1PG03/25/1404/01/14165.55188.0 Power outageAS-7UH04/08/1404/15/14171.4330.2Poweroutage AS-361VA 04/15/1404/22/14168.1649.4PoweroutageAS-1PG06/03/1406/10/14165.89326.6Poweroutage AS-361VA06/03/1406/10/14174.42 326.8PoweroutageAS-7UH06/03/1406/10/14167.52 327.8Poweroutage

\...AS-1PG06/10/1406/17/14162.09 96.6PoweroutageAS-7UH09/30/1410/07/14158.64222.6PoweroutageBasedonthesamplecollectionperiodreductions,air sampleswerecollectedthefollowing percentagesofthe available time:*Missed SamplesAS-1PG E)1VAAS-7UH 99.9%99.9%99.7%Allrequired sampleswerecollectedin accordancewithREMPrequirements.

Therewerenomissedsamples.

Unavailable ResultsGGNSreceived analyticalresultsin adequatetimeforinclusioninthisreport.

Program ModificationsNoREMP modifications tookplaceduringthissamplingperiod.

Attachments Attachment 1 containsresultsofTLD,air,water,sediment,fish,food productsandspecialsamplescollectedinthereportingperiod.TLDswereanalyzedby StanfordDosimetryofSterling,MA.

Other sampleswereanalyzedbyGEL Laboratories,LLCof Charleston, SC.Attachment 1 includesresultsfrom Stanford Dosimetry's and GEL'sparticipationin interlaboratory comparison programs.8

1.0 Introduction

1.1 Radiological

Environmental Monitoring Program GGNS establishedtheREMPtoensurethatplantoperatingcontrolsproperlyfunctiontominimizeanyradiationthatcould endangerhumanhealthorthe environment.TheREMPisdesignedto:

Analyze important pathways for anticipatedtypesand quantities of radionuclidesreleasedintothe environment,*Considerthepossibilityofabuildupoflong-lived radionuclidesinthe environment and identifyanyphysicalandbiological accumulationsthatmay contributetohuman exposures,*Considerthepotentialradiation exposuretoplantandanimallifeinthe environment surrounding GGNS,*Correlatelevelsofradiationandradioactivityinthe environment with radioactivereleasesfromthe operationofGGNS.1.2 Pathways MonitoredTheairborne,directradiation, waterborneandingestionpathways,asseeninFigure1-1aremonitoredasrequiredbytheGGNSODCMTable6.12.1-1.AdescriptionoftheGGNSREMPutilizedto monitor the exposure pathways isprovidedinTable1.2andshowninFigures1-2and1-3.GGNSmay supplementthisprogramwith additionalsamplinginordertoprovidea comprehensive and well-balanced program.Section2.0ofthisreportprovidesa discussionofsamplingresults,withSection3.0providingasummaryofresultsforthemonitored exposure pathways.1.3LandUse CensusGGNSpersonnel conductabienniallandusecensus,asrequiredbyODCM Specification6.12.2.ThemostrecentlandusecensusdataareincludedinTable2.1.The purposeofthis censusistoidentifylandusechangeswithineachofthe16 meteorologicalsectorsandwithina5-mileradiusofGGNSthatwould require modificationstotheREMPortheODCM.Thepurposeofthecensusistoidentifythenearest:

1)2)3)Occupiedand unoccupied residences 2 2Gardenof greaterthan50squaremeters(m)[500squarefeet(ft)]producing broadleaf vegetationAnimalmilkedforhuman consumption 9

GGNSpersonnel conductthelandusecensusby:

Conductingfieldsurveysineach meteorologicalsectorouttofivemilesinordertoconfirm:

Nearestoccupiedresidence

Nearest unoccupied residence*Nearestgardenand approximate size*Nearestmilkinganimal

Identifyinglocationsonmapsandaerial photographs, measuring distancestoGGNSandrecordingresultson surveillancedatasheets*Comparingcurrentlandusecensusresultstopreviousresultsfromthe2012census*Contactingthe ClaiborneCountyAgentforverificationof nearest dairy animals\No significant differenceswereobservedbetweenthebienniallandusecensusesperformedin2012and2014.

10 Table 1.2 Radiological Environmental Sampling Program Exposure Sample Point Description, Sampling and Type and Frequency Pathway Requirement Distance and Direction Collection Frequency Of Analyses Radioiodine and Particulates 1 sampleclosetotheSITEAS-7UH (Sector H, Radius 0.5 BOUNDARYhavingthe highest Miles)-South-southeastofGGNScalculatedannual averageatthe IBEWUnionHall.groundlevel D/O.Radioiodine Canister-1-Continuous sampler131;7days Radioiodine and Particulates operation with sample Particulate Sampler-Airborne1samplefromthevicinityofaAS-1PG (Sector G, Radius 5.5 collectionper7daysor Gross beta radioactivity communityhavingthe highestMiles)-SoutheastofGGNSattheasrequiredbydust following filter change,calculatedannual averagePortGibsonCityBarn.

loading, whichever is composite (by location)groundlevel D/O.more frequentforgammaisotopic;92 days Radioiodine and ParticulatesAS-361VA (Sector 8,Radiu's181samplefromacontrollocation Miles)-North-northeastofGGNS15-30km(10-20miles)onHwy61,NorthoftheVicksburg distance.Airport.TLDs M-16 (Sector A, Radius 0.9 Miles)-MeteorologicalTower.Aninnerringofstationsinthe Direct generalareasoftheSITE M-19 (Sector E, Radius 0.5 Miles)92days Gammadose;92 days Radiation BOUNDARY.-EasternSITE BOUNDARYPropertyline, North-northeast of HWSA.11 Table 1.2 Radiological Environmental Sampling Program Exposure Sample Point Description, Sampling and Type and Frequency Pathway Requirement Distance and Direction Collection Frequency Of Analyses M-21 (Sector J, Radius 0.4 Miles)-Near Former Training Center BuildingonBaldHillRoad.

M-22 (Sector G, Radius 0.5 Miles)-Former RR EntranceCrossingOnBaldHillRoad.TLDs M-23 (Sector Q, Radius 0.5 Miles)-DirectAninnerringofstationsintheGinLakeRoad50YardsNorthof Radiation generalareasoftheSITEHeavyHaulRoadon Power Pole.92 days Gammadose;92 days BOUNDARY.M-25 (Sector N, Radius1.6Miles)-RadialWell Number 1.M-28 (Sector L, Radius0.9Miles)-BaldHillRoad.

M-94 (Sector R, Radius0.8Miles)-

Sector R Near Meteorological Tower.-, 12 Table 1.2 Radiological Environmental Sampling Program Sampling and Exposure Sample Point Description, Collection Type and Frequency Pathway Requirement Distance and Direction Frequency Of Analyses M-95 (Sector F, Radius0.5mi)-SpoilsArea,fenceofoldstoragearea,nearentrancegate M-96 (Sector B, Radius0.7mi.)-NorthGateFence TLOs M-97 (Sector 0, Radius0.8mi.)-Grand DirectAninnerringofstationsintheGulfRoadentrancegatetospoilsarea RadiationgeneralareasoftheSITE M-98 (Sector H, Radius0.5mi.)-Bald92daysGammadose;92days BOUNDARY.HillRoad,acrossfromUnionHall,in curve M-99 (Sector K, Radius0.4mi.)-NorthFenceofoldBallFieldnearutilitypole M-100 (Sector C, Radius 0.6 mi.)-GrandGulfRoad TLOs M-36 (Sector P, Radius 5.0 Miles)-Anouterringapproximately3toCurveonHW608,PointNearestGGNS5milesfromthesite.atPowerPole.

M-40 (Sector M, Radius 2.3 Miles)-HeadlyDrive,NearRiverPortEntrance.

13 Table 1.2 RadiologicalEnvironmentalSampling Program Exposure Sample Point Description, Sampling and Type and Frequency Pathway Requirement Distance and Direction Collection Frequency Of Analyses TLOs M-48 (Sector K, Radius 4.8 Miles)-Anouterringapproximately30.4MilesSouthonMontGomerRoadto5milesfrom'thesite.onWestSide.

M-49 (Sector H, Radius4.5Miles)-ForkinBessie Weathers Road/Shaifer Road.M-50 (Sector B, Radius 5.3 Miles)-PanolaHuntingClubEntrance.

M-55 (Sector 0, Radius 5.0 Miles)-NearIngelsideKarnacFerryRoad/AshlandRoadIntersection.

M-57 (Sector F, Radius 4.5 Miles)-DirectHwy61,BehindtheWelcometoPort RadiationGibsonSignatGlensdaleSubdivision.92daysGammadose;92days

.---TLOs M-01 (Sector E, Radius 3.5 Miles)-8stationsinspecialinterestAcrosstheroadfromLakeClaiborneareassuchaspopulationEntryGate.(SpecialInterest)centers,nearbyresidences, M-07 (Sector G, Radius5.5Miles)-schools,andin1or2areastoAS-1PG,PortGibsonCityBarn.serveascontrolstations.(SpecialInterest)

M-09 (Sector 0, Radius 3.5 Miles)-WarnerTullyV-Camp.(SpecialInterest)

M-10 (Sector A, Radius1.5Miles)-GrandGulfMilitaryPark.(Special Interest)14 Table 1.2 RadiologicalEnvironmentalSampling Program Exposure Sample Point Descrlptlon, Sampling and Type and Frequency Pathway Requirement Distance and Direction Collection Frequency Of Analyses M-14 (Sector B, Radius 18.0 Miles)-AS-3-61VA,Hwy61,NorthofVicksburgAirport.(Control)

TLDs M-33 (Sector P, Radius 12.5 Miles)-Newellton,Louisiana Water Tower.8stationsinspecialinterest(SpecialInterest)

Directareassuchaspopulation M-38 (Sector M, Radius 9.5 Miles)-92days Gammadose;92days Radiationcenters,nearbyresidences,LakeBruinStatePark,*Entranceschools,andin1or2areastoRoad.(SpecialInterest)serveascontrolstations M-39 (Sector M, Radius 13.0 Miles)-St.Joseph,Louisiana, Auxiliary WaterTank.(SpecialInterest) 15 Table 1.2 Radiological Environmental Sampling Program Sampling and Exposure Sample Point Description, Collection Type and Frequency Pathway Requirement Distance and Direction Frequency Of Analyses Surface Water MRUP (Sector R, Radius1.8Miles)-At92daysGammaisotopicand1sampleupstream.least4500ftupstreamoftheGGNStritiumanalyses;92dischargepointintotheMississippiRiverto days1sample downstream.allowadequatemixingoftheMississippiandBigBlackRivers.

MRDOWN (Sector N, Radius1.6Miles)-Atleast5000ftdownstreamoftheGGNSdischargepointintheMississippiRivernear Waterborne Radial VVell No.1.1sampledownstreamduringa MRDOWN (Sector P, Radius 1.3 Miles)-366daysGammaisotopicandLiquidRadwasteDischarge.DownstreamoftheGGNSdischargepointtritiumanalyses;366intheMississippiRivernearRadialWellNo.

days1samplefromOutfall007 5.31daysTritium;31days OUTFALL 007 (Sector N, Radius 0.2Miles)-StormDrainSystem 16 Table 1.2 Radiological Environmental Sampling Program Exposure Sample Point Description, Sampling and Type and Frequency Pathway Requirement Distance and Direction Collection Frequency Of Analyses PGWELL (Sector G, Radius 5.0Miles)-PortGibsonWells-Takenfromdistributionsystemoroneof Groundwaterthefivewells.

WaterborneSamplesfrom2sources.

CONSTWELL (Sector Q, Radius366daysGammaisotopicandtritiumanalyses;366days0.4Miles)-GGNSConstruction Water Well-Takenfromdistributionsystemorthewell.

SEDHAM (Sector N, Radius 1.6 Sediment From ShorelineMiles)-DownstreamoftheGGNS1samplefromdownstreamdischargepointintheMississippi area.RivernearHamiltonLakeoutlet.1samplefromupstreamarea.

SEDCONT (Minimum of 100 yds)-366daysGammaisotopic;366daysUpstreamoftheGGNSdischargepointintheMississippiRiver.

-, Milk1samplefrommilkingCurrently,noavailablemilkinganimalswithin8km(5miles)animalswithin8kmofGGNS.ifmilkisavailable Ingestion commercially.

ALCONT (Sector K, Radius 10.592dayswhenrequiredGammaisotopicand 1-1controlsample(onlyifMiles)-Located South-southwest of131;92daysindicatorexists)>8kmifmilkGGNSatAlcornStateUniversity.isavailable.

17 Table 1.2 Radiological Environmental Sampling Program Exposure Sample Point Description, Sampling and Type and Frequency Pathway Requirement Distance and Direction Collection Frequency Of AnalysesFISHDOWN-Downstreamofthe Fish GGNS dischargepointintothe1sampleinvicinityofGGNSMississippiRiver discharge point.FISHUP-UpstreamoftheGGNS366days Gamma isotopic on edible1sample uninfluenced by dischargepointintotheMississippiportion;366daysGGNSdischarge.

River uninfluencedbyplant operations.

Food Products Ingestion1sampleof broadleaf VEG-J (Sector J, Radius0.4Miles)vegetationgrowninoneoftwo-SouthofGGNSnear former different offsiteiocationswith Training CenteronBaldHillRoad.

highestanticipatedannual VEG-CONT (Sector K, Radius 10.5 Gamma isotopicandI-.averagegroundlevel DIQ if92dayswhen availablemilksamplingisnotperformed.Miles)-AlcornState University131;92 days south-southwestofGGNSwhen1sampleofsimilar vegetation available, otherwisealocation15-30grown15-30kmdistantifkmdistant.milksamplingisnotperformed.

18 Figure 1-1 Exposure Pathways 19 FIGURE1-2 SAMPLE COLLECTIONSITES-NEAR FIELD Gland GIS;U1lt 13.0-7RiMslort 88 ItI CoUectionSite Locadons MAA.--ENTERGY FIGURE 3.0-1 I.5 til ,j,'., SCAlt GRANO GULF NUClEAR.STATION 8anlJIinQ LOcatlon'Map...LEGEND ,.FISh o MSampler O*SurfaoeWater LS Groun(j W.ill O.5edm8nt OnD*'Ramey Wells*Milk 20 N LFIGURE1-3 SAMPLE COLLECTIONSITES-FARFIELD c (If)D E la GI h,, iii.21 FIGURE 3.0-2 Collection Site Locations, General Area Map 4-10 Mile Area Map LEGEND o 0&mat W,....Ground Wiltsr 8 BrowIellfVeg&talb1

SeclnwIt 0 TU:l*AaMey Wels*....Ik 16 MILES FROM GRAI'I)Gl.lF TO;.n;PQRI'SlIcD (B)-..,....-EHlERGY GRAND GULF MJClEAA STAllON 4-10 Mile Environmental SflTT1:llng L..ooa1Ion Map Grand Gul, Unit 13.0-8 RevIsion 35 0907 2.0, Interpretation and Trends of Results 2.1 Air Particulate and Radioiodine Sample ResultsGGNSdidnot detectanyplantrelatedgammaemitting radionuclidesinthe quarterly air particulate composites.TheREMPhad previously detected airborne radioactivity attributabletoothersourcesinthispathway.Thesesourcesincludethe Chinese nucleartestin1980andthe accidentatthe ChernobylNuclearPowerPlantin1986.TheGGNSREMPdetected radioactivityreleasedfromtheFukushimaDai-ichi Nuclear PowerPlantfollowingtheMarch11,2011, Tohoku earthquake.

No radioiodine was detectedin2014.Table3.1,whichalsoincludesgrossbetaactivity,providesa comparisonofthe indicatorandcontrolmeansandranges, further emphasizingthattheairbornepathwayremainsat background levels.lin the absence of plant-relatedgammaradionuclides,grossbetaactivityisattributedto naturallyoccurringradionuclides.Similartrendsarepresentforcontroland indicatorlocations,which support the presenceofnaturallyoccurringradioactivity.

2.2 Thermoluminescent

Dosimetry Sample Results GGNS calculatesdoseby subtractingshieldreadingsfromcontroland indicatorlocationreadingsandreports measureddoseasnetexposure,normalizedto92days.GGNSreliesonthe comparisonofthe indicator locationstothecontrollocationasanindicationofplantimpact.Gammaradiationdoseinthereportingperiodiscomparedtocontrollocationreadingsfor previousyearsasshowninFigure2-1.

The comparisonofthe indicatorresultstothecontrol,andto previousindicator results,asseeninFigure2-1and Table 3.1, indicatesthatplantoperationhashadno significantimpactonambientradiationlevelsduringthereportingperiod.

22 Figure 2-12014TLO Readings mR/qtr 20.0 2009-2013 Control Location Minimum (-2 Stdev)2009-2013 Control Location Maximum(+2Stdev)x x X X x a x X X A X X A C.X A A*X*0 aa*A X A 0 0 t1 g X X*t.i*B*A 0X A e 0 x 0 0 ii I)0 0 X A e 0 0 ft 0 X A X 0 A*X XA 8 0XX o o 0 8.0;..12.0X e X A A: X 016.04.0.1Q14 0.0***,***..******,******

..****r***********f***********!***********r**********!***********!***********"I***********!"**********T***********T"**********,.**********..r***..*****,*****..*..*,**..*..*r**..*******T**..***..*,., ,."f"._e_NMMee..e e 0____N N N N N M M M M@e2.3 Water Sample Results Surface water sampleswerecollectedfromthree indicator locations (Outfall 007,MRDOWN,and MRDOWN During Discharge)andonecontrollocation(MRUP)andanalyzedforgammaemitting radionuclidesandtritium.Plantrelatedgammaemitting radionuclidesandtritiumremained undetectableinthe upstream and downstreamMississippiRiver locations,whichis consistent with preoperational and previous operationalyears.Stormwaters contributetoOutfall 007andcan includetritiumasaresultof washout and entrainmentofnormal, previously monitored gaseous effluents.Asaresult,tritiumis occasionally observed.In February 2014,tritiumwasmeasuredat a concentration of1492+/-374pCi/LattheOutfall 007 (indicator)location.Tritiumwasnotobservedintheremaining Outfall 007 samplescollectedduring 2014.Basedonreviewofresultsand historicaldata,plant operationshadno significantimpactonthis pathwayduringthereportingperiod.

23 Groundwater samples were collectedfromtwolocations(indicatorandcontrol)andanalyzedforgammaemitting radionuclidesandtritium(TablesA4.2andA4.3).Inadditiontothe samplesrequiredbytheREMP,anextrasamplefromthelocationswasanalyzedforlodine-131(TableA4.3).GGNSdidnot detectanyplantrelatedgamma emitting radionuclidesortritiumin groundwater samplesduringthereportingperiod.Basedonreviewofresultsandhistoricaldata,plant operationshadno significantimpactonthispathwayduringthereportingperiod.

2.4 Sediment

Sample Results Sedimentsampleswerecollectedfromtwo locations (indicatorandcontrol)andanalyzedforgammaemittingradionuclides.Inthisreportingperiod,plantrelatedgammaemitting radionuclideswerebelow detectable concentrationsintheupstream(control)location.

Cesium-137 was detectedatan average concentrationof39.4+/-25pCi/kginthe downstream(indicator)location.AreviewofREMPdatacollectedatthe downstreamlocationfrom1983through2013 indicates the Cesium-137 concentrationhasrangedfromlessthan detectableto300 pCi/Kg.Cesium-137 has previously been detectedintheupstream(control)location.

The presence of Cesium-137 is attributed to atmospheric weapons testing.Basedonreviewofresultsandhistoricaldata,plant operationshadno significantimpactonthispathwayduringthereportingperiod.

2.5 Milk Sample ResultsMilksampleswerenotcollectedwithinfivemilesofthesiteinthereportingperiodduetothe absenceofmilkinganimals.SincetherearenodairieswithinfivemilesofGGNS,andbasedon non-detectable radioiodineandgamma radionuclidesinairand vegetationsamples,plant operationshadnoimpactonthispathwayduringthereportingperiod.

2.6 Fish Sample ResultsFishsampleswerecollectedfromtwo locations (indicatorandcontrol)andanalyzedforgammaemittingradionuclides.GGNSdidnot detectanyplantrelatedgammaemitting radionuclidesinfishsamples(edibleportions)duringthereportingperiod,ashasbeenthecasein preoperationalandprevious operationalyears.Theseresultsindicatethatthispathwayhasnotbeen affectedbyplantoperations.

2.7 Food Product (Vegetation)

Sample ResultsFoodproductsampleswerecollectedfromtwolocations(indicatorandcontrol)andanalyzedforlodine-131andgammaemittingradionuclides.GGNSdidnotdetectanyplantrelated.lodine-131orgammaemitting radionuclides in vegetationsamplesduringthereportingperiod.Theseresultsindicatethatthispathwayhasnotbeenaffectedbyplantoperations.Inadditiontothefood productsamplesrequiredbytheREMP,onespecialmeatsamplefrom deerharvestedonthesitepropertywasanalyzedforgammaemitting 24 radionuclides (TableA8.1),in accordancewithsite procedure 06-EN-SOOO-V-0001 section 5.8.This sampleisnot required by theREMP,andis included as supplemental data.Plant related gamma emitting radionuclides were undetectable in the meat sample.2.8LandUse Census Results Results fromtheLand Use Census performed in 2014 are included in this report.Methods utilized to perform the Land Use Census include: visual surveys, door to door surveys, telephone interviews, Global Positioning System (GPS), Aerial Photography, and consultation with the local county agent concerning dairy production in Claiborne County.During the survey the following information was obtained: 1)nearest location of occupied and unoccupied residences 2)nearest location of dairy production 3)nearest location of gardens Changes from the previousLandUse Census were evaluated in accordance with GGNS surveillance"Land Use Census", 06-EN-SOOO-O-0002.

The differences were compared to the locations and assumptions used in calculations for compliance with the ODCM Limiting Condition for Operation 6.11.6 and 6.12.2.The locations and assumptions currently used in ODCM were determined more conservative thananyof the changes.Determinations from the most recentLandUse Census results are:*Because of downwind location and/or distance from thesite,inno casewillthe occupancyofan existing unoccupied residence cause any existing ODCM critical receptor calculation resultstobeless conservative.*No additional sampling locations are required as the onsite vegetation sampling location (SectorJ,0.4 miles)is more conservative than changes identifiedinthelanduse census.*Cattleareraised for human consumption (most notably in SectorsF,H,J,and K).GGNS uses the Grass/Cow/Meat pathway.*The milk pathway does not needtobe activated because no commercial dairy production is occurring within5miles,as referenced by ODCM Table 6.12.1-1.*SectorsM,N,P,andQare remote areas in which the primary use is hunting.Areas were surveyed by vehicle, aerial photographs, and interviews.

Gardens, regardlessofsize, were included in the census data Based on evaluation of theLandUse Census data, no ODCM revision is required.25 Table2.1 2014 Land Use Census Parameter Sector A*Sector B Sector C*Sector 0*I.Nearest Occupied a.Distance (mile)1.76 1.51 0.70 2.60 Residence b.Degreesfromtruenorth 351.6 23.7 42.3 60.8 II.Nearest Unoccupied a.Distance (mile)0.94 0.83 None None Residence (closer b.Degreesfromtruenorth 8.0 15.1 than occupied residence)

III.Nearest Milk Animal a.Distance None None None None IV.Nearest Broadleaf a.Distance (mile)1.02 1.52 4.53 3.06 Garden b.Gardensize(ft2)400251200 c.Degreesfromtruenorth 355.4 21.9 49.1 58.8 V.Census Comparisona.Is nearest occupied No Yes Yes Yes residence in same locationaslast census?b.Is nearestmilkanimalin N/A N/A N/A N/A same locationaslast census?-c.Is nearest broadleaf No Yes'No No gardeninsame location as last census?-Retained previousgardenlocation.Locatedno other gardensinthesector.*Changefromlastcensus.SeetableofLandUseCensus Changes 26 Table 2.1 2014 Land Use Census, continued.

Parameter Sector E Sector F*Sector G*Sector H I.Nearest Occupieda.Distance(miles) 0.89 2.25 3.72 1.10 Residenceb.Degreesfromtruenorth 86.9 101.3 134.1 151.4 II.Nearest Unoccupieda.Distance(miles)

None None 3.71 1.07 Residence (closerb.Degreesfromtruenorth 131.8 151.0 than occupied residence)

III.Nearest Milk Animala.Distance None None None None IV.Nearest Broadleafa.Distance(miles) 0.89 4.50 4.20 4.39 Gardenb.Gardensize(ft2)10001600200c.Degreesfromtruenorth 86.9 110.0 130.1 155.0 V.Census Comparisona.IsnearestoccupiedYes'Yes No Yesresidenceinsamelocationaslastcensus?b.Isnearestmilkanimalin N/A N/A N/A N/Asamelocationaslast census?c.IsnearestbroadleafgardenYes No No Yesinsamelocationaslast census?1-Nearestoccupiedresidencelocationisthesameaslastcensus.Locationdatarevisedduetonew mapping method.*-Changefromlastcensus.SeetableofLandUseCensusChanges 27 Table 2.1 2014 Land Use Census, continued.

Parameter Sector J Sector K Sector L Sector M I.Nearest Occupied a.Distance (miles)3.14 2.20 0.89 None Residenceb.Degrees fromtruenorth174.2 197.0 219.7 II.Nearest Unoccupied a.Distance (miles)None 1.70 None None Residence (closer thanb.Degreesfromtruenorth 203.3 occupied residence)(Hunting Lodge-Info Only)III.Nearest Milk Animala.Distance(miles)

None NoneNoneNone IV.Nearest Broadleaf a.Distance (miles).3.16 2.18 0.89 None Gardenb.Gardensize(ft2)5002500c.Degreesfromtruenorth 174.0 196.3 219.5V.Census Comparisona.Is nearest occupied Yes Yes Yes N/Aresidenceinsamelocationaslastcensus?b.Is nearestmilkanimalin N/A N/A N/A N/Asamelocationaslast census?c.Is nearest broadleaf Yes Yes Yes N/Agardeninsamelocationaslastcensus?

28 Table 2.1 2014 Land Use Census, continued.

Parameter Sector N Sector P Sector Q Sector R I.Nearest Occupieda.Distance(miles)

None None None 1.11 Residenceb.Degreesfromtruenorth 346.1 II.Nearest Unoccupieda.Distance(miles)

None None None None Residence (closerb.Degreesfromtruenorth than occupied residence)

III.Nearest Milk Animala.Distance(miles)

None None None None IV.Nearest Broadleafa.Distance(miles)

None None None None Gardenb.Gardensize(ft2)c.Degreesfromtruenorth V.Census Comparisona.Isnearestoccupied N/A N/A N/A Yesresidenceinsamelocationaslastcensus?b.Isnearestmilkanimalin N/A N/A N/A N/Asamelocationaslast census?c.Isnearest broadleaf N/A N/A N/A N/Agardeninsamelocationaslastcensus?

29 2014LandUseCensusChanges SECTOR PARAMETERReasonfor Change A Nearest Occupied Residence Nearest occupied residence from 2012 census no longer occupied.New nearest occupied residence identified in 2014.A Nearest Broadleaf Garden No garden location identified in 2012 census.New garden location identified in 2014.C Nearest Broadleaf Garden Garden location identified in 2012 census no longer active.New nearest garden location identified in 2014.D Nearest Broadleaf Garden New nearest garden location identified in 2014.E Nearest Occupied Residence Nearest occupied residence is the same as previous census.Location data revised due to new mapping method.F Nearest Broadleaf Garden New nearest garden location identified in 2014.G Nearest Occupied Residence Nearest occupied residence from 2012 census no longer occupied.New nearest occupied residence identified in 2014.G Nearest Broadleaf Garden Nearest garden location from 2012 census no longer planted.New nearest garden location identified in 2014.30

2.9 Interlaboratory

Comparison ResultsStanfordDosimetryCompanyanalyzed interlaboratory comparison thermoluminescent dosimeterstofulfillthe requirements of aDCM Specification6.12.1.TheresultsareshowninTableA.9.1.

GEL Laboratories analyzed interlaboratory comparison samplestofulfillthe requirements of aDCM Specification6.12.1.TheresultsareshowninTableA.9.2.

31

3.0 Radiological

Environmental Monitoring Program Summary 3.1 Program Results SummaryTable3.1 summarizes the REMP results.Valuesreportedaslessthanthelowerlimitofdetection

<<LLD)werenotusedwhen determiningrangesandmeansfor indicatorandcontrollocations.

32 TABLE3.1RadiologicalEnvironmentalMonitoringProgramSummaryNameofFacility:GrandGulfNuclearStationDocketNo:50-416LocationofFacility:ClaiborneCounty,MississippiReportingPeriod:

January-December 2014SampleTypeType

&NumberLLDbIndicatorLocationsLocationwithHighestAnnual Control Number of (Units)ofAnalysesaMean(F)c Mean Locations Nonroutine

[Range]Mean(F)cResultse[Range]LocationdMean(F)c[Range]AirParticulatesGB1560.010.0310(104/104)AS-1PG0.0316(52/52)0.0292(52/52) 0 (pCi/m 3)[0.0097-0.0616](SectorG,5.5mi)[0.0102-0.0616][0.0086-0.0604]

GS 12 Cs-134 0.05<LLD N/A N/A<LLD 0 Cs-137 0.06<LLD N/A N/A<LLD 0AirborneIodine 1-1311560.07<LLD N/A N/A<LLD 0(pCi/m 3)InnerRingTLDs Gamma 56 f10.0(56/56)

M-99 13.3(4/4)N/A 0 (mRlQtr)[6.3-14.8](Sector J,0.4mi.)[12.7-14.8]OuterRingTLDs Gamma 28 f9.9(28/28)

M-57 11.9 (4/4)N/A 0 (mRlQtr)[5.2-13.7](SectorF,4.5mi.)[10.7

-13.7]SpecialInterest Gamma 28 f10.3(28/28)

M-0112.0(4/4)N/A 0 TLDs[7.4-20.1](SectorE,3.5mi.)[11.5-12.9]

(mRlQtr)ControlTLDs Gamma 4 f N/A N/A N/A11.0(4/4)0 (mRlQtr)[10.1-12.5]

33 TABLE 3.1 Radiological Environmental Monitoring Program Summary Name of Facility: Grand Gulf Nuclear Station DocketNo:50-416 Location of Facility: Claiborne County, Mississippi Reporting Period: January-December 2014 Sample Type Type&NumberLLDb Indicator Location Location with Highest Annual Mean Control Number of (Units)of Analyses aMean(F)c Locations Nonroutine

[Range]Mean(F)c Results e[Range]Location dMean(F)c[Range]Surface Water H-33030001817(1/14)Outfall0071817(1/14)

<LLD a (pCi/1)[1492](SectorN,Radius0.2mi.)

[1492]GS 16 1-131 15<LLD N/A N/A<LLD a Mn-54 15<LLD N/A N/A<LLD a Fe-59 30<LLD N/A N/A<LLD a Co-58 15<LLD N/A N/A<LLD 0 Co-60 15<LLD N/A N/A<LLD a Zn-65 30<LLD N/A N/A<LLD 0 Zr-95 30<LLD N/A N/A<LLD 0 Nb-95 15<LLD N/A N/A<LLD 0 Cs-134 15<LLD N/A N/A<LLD 0 Cs-137 18<LLD N/A N/A<LLDo.Ba-140 60<LLD N/A N/A<LLD 0 La-140 15<LLD N/A N/A<LLD a 34 TABLE 3.1 Radiological Environmental Monitoring Program Summary Name of Facility: Grand Gulf Nuclear Station DocketNo:50-416 Location of Facility: Claiborne County, Mississippi Reporting Period: January-December 2014 Sample Type Type&LLD b Indicator Locations Location with Highest Annual Mean Control Number of (Units)NumberMean(F)c Locations Nonroutine of Analyses a[Range]Mean(F)c Results e[Range]Location dMean(F)c[Range]Groundwater H-3 6 2000<LLD N/A N/A<LLD 0(pCi/1)1-131 3 1<LLD N/A N/A<LLD 0GS3 Mn-54 15<LLD N/A N/A<LLD 0 Fe-59 30<LLD N/A N/A<LLD 0 Co-58 15<LLD N/A N/A<LLD 0 Co-60 15<LLD N/A N/A<LLD 0 Zn-65 30<LLD N/A N/A<LLD 0 Zr-95 30<LLD N/A N/A<LLD 0 Nb-95 15<LLD N/A N/A<LLD 0 Cs-134 15<LLD N/A N/A<LLD 0 Cs-137 18<LLD N/A N/A<LLD 0 Ba-140 60<LLD N/A N/A<LLD 0 La-140 15<LLD N/A N/A<LLD 0 SedimentGS2 (pCi/kg)Cs-134 150<LLD N/A N/A<LLD 0 Cs-137 18039.39(1/1)

SEDHAM39.39(1/1)

<LLD 0[39.39](SectorN,1.6Miles)

[39.39]35 TABLE 3.1 Radiological Environmental Monitoring Program Summary..Name of Facility: Grand Gulf Nuclear Station DocketNo:50-416 location of Facility: Claiborne County, Mississippi Reporting Period: January-December 2014 Sample Type Type&LLDb Indicator Location Location with Highest Annual Control Number of (Units)NumberMean(F)c Mean Locations Nonroutine of Analyses a[Range]Mean(F)c Results e[Range]Location dMean(F)c[Range]Fish GS 4 (pCilkg)Mn-54 130<LLD N/A N/A<LLD 0 Fe-59 260<LLD NiA NiA....1I r""'\.n<, LLU.U Co-58 130<LLD N/A N/A<LLD 0 Co-60 130<LLD N/A N/A<LLD 0 Zn-65 260<LLD N/A N/A<LLD 0 Cs-134 130<LLD N/A N/A<LLD 0 Cs-137 150*<LLD N/A N/A<LLD 0 Food 1-131.10 60<LLD N/A N/A<LLD 0 ProductsNegetation (pCi/kg)GS 10 Cs-134 60<LLD N/A N/A<LLD 0 Cs-137 80<LLD N/A N/A<LLD 0 36 TABLE 3.1 Radiological Environmental Monitoring Program Summary Name of Facility: Grand Gulf Nuclear Station DocketNo:50-416 Location of Facility: Claiborne County, Mississippi Reporting Period: January-December 2014 Location with Highest Annual Mean Control Indicator Location Locations Number of Sample Type Type&NumberMean(F)cMean(F)cMean(F)c Nonroutine (Units)of Analyses a LLD b[Range]Location d[Range][Range]Results e Meat GS 1 (Special)Mn-54 15<LLD N/A N/A<LLD 0(pCi/1)Fe-59 30<LLD N/A N/A<LLD 0 Co-58 15<LLD N/A N/A<LLD 0 Co-60 15<LLD N/A N/A<LLD 0 Zn-65 30<LLD N/A N/A<LLD 0 Cs-134 15<LLD N/A N/A<LLD 0 Cs-137 18<LLD N/A N/A<LLD 0aGB=Grossbeta; 1-131=lodine-131;H-3

=Tritium;GS

=Gammascan.bLLD=Requiredlowerlimitofdetectionbasedon aDCMTable6.12.1-3.cMeanandrangebasedupondetectable measurementsonly.Fractionofdetectablemeasurementsatspecifiedlocationsisindicatedinparenthesis(F).dWhereapplicable,locationsarespecifiedbyname,distancefromreactorsiteandmeteorologicalsector.eNon-routineresultsarethosewhichexceedtentimesthecontrolstationvalue.Ifnocontrolstationvalueisavailable,theresultisconsiderednon-routineifitexceedstentimesthepreoperationalvalueforthelocation.fLLDisnotdefinedin aDCMTable6.12.1-3.

37 Attachment 1 Radiological'Monitoring Report Summary of Monitoring Results 38 T ABLEOFCONTENTS TABLE A1.1 AIR PARTICULATE FILTERGROSSBETAAND CHARCOAL CARTRIDGEAS-1PG 40 TABLEA1.2 AIR PARTICULATE FILTERGROSSBETAAND CHARCOALCARTRIDGEAS-361VA 42 TABLEA1.3 AIR PARTICULATE FILTER GROSS BETA AND CHARCOAL CARTRIDGEAS-7UH 44 TABLEA1.4 AIR PARTICULATE FILTER GAMMA 46 TABLEA2.1 THERMOLUMINESCENT DOSIMETERS 47 TABLEA2.2 THERMOLUMINESCENT DOSIMETERS 48 TABLEA2.3 THERMOLUMINESCENT DOSIMETERS 48 TABLEA3.1SURFACEWATERGAMMA 49 TABLEA3.2SURFACEWATERTRITIUM 50 TABLE A4.1 GROUNDWATER GAMMA 51 TABLEA4.2 GROUNDWATER TRITIUM 52 TABLEA4.3 GROUNDWATER IODINE-131 53 TABLEA5.1SEDIMENT 54 TABLEA6.1FISH 55 TABLEA7.1FOODPRODUCTS 56 TABLEA8.1 SPECIAL SAMPLES 57 TABLEA9.1 INTERLABORATORYPROGRAM-TLDS TABLEA9.2 INTERLABORATORYPROGRAMS-SAMPLES 39 TableA1.1SampleType:AirParticulateFilterand Radioiodine CartridgeAnalysis:GrossBetaand 1-131Units:pCilm3AIRSAMPLEAS-1PGLLD(pCi/m3) 0.07 0.01 LAB 10STARTDATEENDDATE 1-131GROSSBETA 34096100412/31/1301/07/14

<0.0134 0.04669+1-0.00554 341489004 01/07/14 01/14/14<0.0248 0.02244+1-0.00393 341839004 01/14/14 01/21/14<0.0223 0.01987+1-0.00372 342164004 01/21/14 01/29/14<0.0234 0.0390+1-0.00481 342457004 01/29/14 02/04/14<0.0337 0.02417+1-0.00434 34299900402/04/1402/11/14

<0.0195 0.02937+1-0.00444 34330300402/11/1402/18/14

<0.0171 0.03345+1-0.00476 343772004*02/18/1402/25/14

<0.0148 0.02173+1-0.00384 34406700402/25/1403/04/14

<0.0226 0.03161'.+1-0.00461 34461900403/04/1403/11/14

<0.0381 0.03895+1-0.00514 34494300403/11/1403/18/14

<0.022 0.02276+1-0.00387 34533100403/18/1403/25/14

<0.0301 0.0318+1-0.0047 34569300103/25/1404/01/14

<0.0326 0.02732+1-0.00432 34655300404/01/1404/08/14

<0.0312 0.02419+1-0.00407 34700600404/08/1404/15/14

<0.042 0.02067+1-0.00373 34747100404/15/1404/22/14

<0.0138 0.05222+1-0.0059 34785800404/22/1404/29/14

<0.0222 0.02786+1-0.00437 34833500404/29/1405/06/14

<0.022 0.03754+1-0.00509 34888300405/06/1405/13/14

<0.0395 0.02833+1-0.00435 349205004 05/13/14 05/20/14<0.013 0.02623+1-0.00428 349706004 05/20/14 05/27/14<0.0344 0.04886+1-0.00575 350161004 05/27/14 06/03/14<0.0363 0.01023+1-0.00279 350610004 06/03/14 06/10/14<0.0325 0.01035+1-0.00276 350879004 06/10/14 06/17/14<0.0248 0.02688+1-0.00435 35142400106/17/1406/24/14

<0.0164 0.02955+1-0.00438 35178300406/24/1407/01/14

<0.0461 0.02105+1-0.00389 35233000407/01/1407/08/14

<0.0159 0.03515+1-0.00487 352845004 07/08/14 07/15/14<0.0328 0.02597+1-0.00419 35337200407/15/1407/22/14

<0.0378 0.01949+1-0.00364 353766004 07/22/14 07/29/14<0.0294 0.03233+1-0.00468 35426900407/29/1408/05/14

<0.0288 0.03508+1-0.0048 354720004 08/05/14 08/12/14<0.0248 0.02372+1-0.00406 35521500408/12/1408/19/14

<0.0383 0.02807+1-0.00437 35561900408/19/1408/26/14

<0.0195 0.03025+1-0.00448 355880004 08/26/14 09/02/14<0.00976 0.01594+1-0.00337 40 TableA1.1SampleType:Air Particulate Filter and Radioiodine CartridgeAnalysis:GrossBetaand 1-131Units:pCi/m3AIRSAMPLEAS-1PG LLD (pCi/m3)0.07 0.01LAB10 STARTDATEENDDATE 1-131 GROSS BETA 35663800409/02/1409/09/14

<0.0213 0.02202+1-0.00387 356995004 09/09/14 09/16/14<0.0212 0.02922+1-0.00443 35750500409/16/1409/23/14

<0.0153 0.04019+1-0.00518 35841300409/23/1409/30/14

<0.0331 0.03333+1-0.00467 358535004 09/30/14 10107/14<0.0184 0.02965+1-0.00454 359166004 10107/14 10/14/14<0.0162 0.02888+1-0.00443 359683004 10/14/14 10/21/14<0.0305 0.06161+1-0.00783 360209004 10/21/14 10/28/14<0.034 0.05208+/-0.00716 360702004 10/28/14 11/04/14<0.0149 0.03394+1-0.00474 361199004 11/04/14 11/11/14<0.0282 0.04031+1-0.00521 361662004 11/11/14 11/18/14<0.0294 0.02785+1-0.00433 362062004 11/18/14 11/25/14<0.0361 0.03725+1-0.00498 362389004 11/25/14 12/02/14<0.0383 0.02751+1-0.0043 363028004 12/02/14 12/09/14<0.0245 0.06018+1-0.00626 36344500412/09/1412/16/14

<0.032 0.04673+1-0.00562 363792004 12/16/14 12/23/14<0.031 0.04481+1-0.00551 363939004 12/23/14 12/30/14<0.0527 0.02715+1-0.00428 L61599 12/30/14 01/06/15<0.0500 0.0196+1-0.00357 Average: Maximum: Minimum: 41 0.0313 0.0616 0.0102 Table A1.2 SampleType:Air Particulate Filter and Radioiodine CartridgeAnalysis:GrossBetaand 1-131Units:pCi/m3 AIR SAMPLEAS-361VA LLD (pCi/m3)0.07 0.01 LAB 10STARTDATE ENID DATE 1-131GROSSBETA 340961005 12/31/13 01/07/14<0.013 0.04805+/-0.00559

.34148900501/07/1401/14/14

<0.033 0.02221+/-0.00395 341839005 01/14/14.01/21/14<0.0165 0.02017+/-0.00372 342164005 01/21/14 01/29/14<0.017 0.03658+/-0.00464 342457005 01/29/14 02/04/14<0.034 0.01914+/-0.0039 34299900502/04/1402/11/14

<0.0264 0.02717+/-0.00429 34330300502/11/1402/18/14

<0.0111 0.03512+/-0.00486 34377200502/18/1402/25/14

<0.0226 0.02018+/-0.00371 344067005 02/25/14 03/04/14<0.026 0.0255+/-0.00414 34461900503/04/1403/11/14

<0.0222 0.03105+/-0.00459 344943005 03/11/14 03/18/14<0.0299 0.01579+/-0.00329 345331005 03/18/14 03/25/14<0.0251 0.0262+/-0.00425 345693005 03/25/14 04/01/14<0.02770.02253+/-0.00391 346553005 04/01/14 04/08/14<0.0366 0.01668+/-0.00339 34700600504/08/1404/15/14

<0.0306 0.02044+/-0.00369 347471002 04/15/14 04/22/14<0.0227 0.02717+/-0.00428 34785800504/22/1404/29/14

<0.0243 0.0230+/-0.00406 34833500504/29/1405/06/14

<0.0206 0.0289+/-0.00441 34888300505/06/1405/13/14

<0.0317 0.02191+/-0.00396 349205005\

05/13/14 OS/20/14<0.0249 0.01904+/-0.00365 349706005OS/20/14OS/27/14

<0.0363 0.04752+/-0.00564 350161005 OS/27/14 06/03/14<0.0398 0.01155+/-0.00293 350610005 06/03/14 06/10/14<0.0373 0.008584+/-0.00247 35087900506/10/1406/17/14

<0.0131 0.02368+/-0.00417 351424005 06/17/14 06/24/14<0.0178 0.02562+/-0.00416 35178300506/24/1407/01/14

<0.0378 0.02195+/-0.00389 35233000507/01/1407/08/14

<0.0143 0.02568+/':0.00419 352845005 07/08/14 07/15/14<0.033 0.02924+/-0.00444 35337200507/15/1407/22/14

<0.0277 0.01786+/-0.00349 353766005 07/22/14 07/29/14<0.0266 0.03909+/-0.00514 354269005 07/29/14 08/05/14<0.0331 0.03375+/-0.00478 35472000508/05/1408/12/14

<0.0321 0.02973+/-0.00446

.355215005 08/12/14 08/19/14<0.0445 0.02757+/-0.00433 355619005 08/19/14 08/26/14<0.0263 0.02844+/-0.00439 42 355880005 08/26/14 09/02/14*1<0.029 0.0210+/-0.00379 ITableA1.2SampleType:Air Particulate Filter and Radioiodine CartridgeAnalysis:GrossBetaand 1-131Units:pCi/m3AIRSAMPLEAS-361VALLD(pCi/m3) 0.07 0.01 LAB 10STARTDATEENDDATE 1-131GROSSBETA 356638005 09/02/14 09/09/14<0.03160.02677+/-0.00425 356995005 09/09/14 09/16/14<0.0290.02724+/-0.00431 35750500509/16/1409/23/14

<0.01990.03448+/-0.00482 35841300509/23/1409/30/14

<0.0276 0.02934+/-0.0043 358535005 09/30/14 10/07/14<0.0203 0.02406+/-0.00416 35916600510/07/1410/14/14

<0.0146 0.02594+/-0.00421 359683005 10/14/14 10/21/14<0.0271 0.05999+/-0.00773 360209005 10/21/14 10/28/14<0.033 0.05325+/-0.00724 360702005 10/28/14 11/04/14<0.0276 0.03138+/-0.0046 36119900511/04/1411/11/14

<0.02040.03424+/-0.00477 361662005 11/11/14 11/18/14<0.0205 0.03093+/-0.00455 362062005 11/18/14 11/25/14<0.03430.03936+/-0.00511 36238900511/25/1412/02/14

<0.0309 0.02247+/-0.0039 363028005 12/02/14 12/09/14<0.0414 0.06044+/-0.00626 363445002 12/09/14 12/16/14<0.0366 0.04554+/-0.0056 36379200512/16/1412/23/14

<0.0263 0.04349+/-0.0054 363939005 12/23/14 12/30/14<0.03560.02976+/-0.00447 L61599 12/30/14 01/06/15<0.0501 0.02191+/-0.00355 Average: Maximum: Minimum: 43 0.0290 0.0604 0.0086 TableA1.3 ,SampleType:Air ParticulateFilterand Radioiodine CartridgeAnalysis:GrossBetaand 1-131'Units:pCi/m3AIRSAMPLEAS-7UHLLD(pCi/m3) 0.07 0.01 LASlOSTARTDATE END DATE 1-131GROSSBETA 340961006 12/31/13 01/07/14<0.0123 0.0406+/-0.00518 341489006 01/07/14 01/14/14<0.026" 0.02459+/-0.0041 341839006 01/14/14 01/21/14<0.0223 0.01952 r+/-0.00369 342164006"01/21/1401/29/14

<0.014 0.0395+/-0.00482 342457006 01/29/14 02/04/14<0.0133 0.0224+/-0.00421 342999006 02/04/14 02/11/14<0.0427 0.0314+/-0.00458 343303006 02/11/14 02/18/14<0.0127 0.03887+/-0.00513 343772006 02/18/14 02/25/14<0.0196 0.03099+/-0.00455 344067006 02/25/14 03/04/14<;0.0203 0.03193+/-0.00463 344619006 03/04/14 03/11/14'<0.0273 0.03997+/-0.00522 344943006 03/11/14 03/18/14<0.0233<:>>: 0.01706+/-0.00343 345331006 03/18/14 03/25/14<0.027 0.02673+/-0.00427 345693006 03/25/14 04/01/14<0.0305 0.02657+/-0.00445 346553006 04/01/14 04/08/14<0.0207'0.01704+/-0.00344 347006006 04/08/14 04/15/14<0.0315'0.02359+/-0.00397 347471006 04/15/14 04/22/14<0.0168 0.03742+/-0.005 347858006 04/22/14<0.0179 0.0274+/-0.00437 348335006 04/29/14 05/06/14<0.0238 0.0356+/-0.00491 348883006 05/06/14 05/13/14<0.036 0.02816+/-0.00434 349205006 05/13/14OS/20/14<0.0184 0.02296+/-0.00402 349706006OS/20/14OS/27/14<0.026 0.03632+/-0.00496 350161003 OS/27/14 06/03/14<0.0335 0.009739+/-0.00273 350610006 06/03/14 06/10/14<0.0387 , 0.01073+/-0.00279 350879006 06/10/14 06/17/14<0.0126 0.02813+/-0.00444 351424006 06/17/14 06/24/14<0.0203 0.02477+/-0.00402 351783003 06/24/14 07/01/14<0.03850.02243+/-0.00401 352330006 07/01/14 07/08/14<0.022 0.02569+/-0.00419 352845006 07/08/14 07/15/14<0.0342 0.02462+/-0.00409 353372006 07/15/14 ,07/22/14<0.0261 0.01473+/-0.0032 35376600607/22/1407/29/14<0.0251 0.03547'+/-0.0049 354269006 07/29/14 08/05/14<0.0217 0.03726+/-0.00495 354720006 08/05/14 08/12/14<0.0382 0.02016+/-0.00375 355215006 08/12/14 08/19/14<0.0328 0.02906+/-0.00445 355619006 08/19/14 08/26/14<0.0343 0.03258+/-0.00465 355880006 08/26/14 09/02/14<0.01720.01973+/-0.00371 44 TableA1.3SampleType:Air ParticulateFilterand Radioiodine CartridgeAnalysis:GrossBetaand 1-131Units:pCi/m3AIRSAMPLEAS-7UHLLD(pCi/m3) 0.07 0.01 LABIDSTARTDATEENDDATE 1-131GROSSBETA 356638006 09/02/14 09/09/14<0.0405 0.02348+/-0.00399 35699500609/09/1409/16/14

<0.02680.02991+/-0.0044835750500609/16/14 09/23/14<0.01950.04132+/-0.00525 358413006 09/23/14 09/30/14<0.0389 0.03195+/-0.00457 358535006 09/30/14 10/07/14<0.0141 0.02903+/-0.00455 359166006 10/07/14 10/14/14<0.0116 0.0223+/-0.00392 359683006 10/14/14 10/21/14<0.0310.05997+/-0.00773 360209006 10/21/14 10/28/14<0.0307 0.05034+/-0.00704 360702006 10/28/14 11/04/14<0.0381 0.03345+/-0.0047 361199006 11/04/14 11/11/14<0.01840.03627+/-0.00495 361662006 11/11/14 11/18/14<0.02980.03109+/-0.00457 362062006 11/18/14 11/25/14<0.0270.03354+/-0.00472 362389006 11/25/14 12/02/14<0.02450.03002+/-0.00448 363028006 12/02/14 12/09/14<0.03280.05834+/-0.00616 363445006 12/09/14 12/16/14<0.0419 0.0477+/-0.0057 363792006 12/16/14 12/23/14<0.0243 0.0407+/-0.00525 363939006 12/23/14 12/30/14<0.03350.02405+/-0.00404 L61599 12/30/14 01/06/15<0.0499 0.0228+/-0.00378 Average: Maximum: Minumum: 45 0.0302 0.0600 0.0097 TableA1.4 Sample Type: Air Particulate Filter Analysis: Gamma Isotopic Units: pCi/m3AIRPARTICULATEFILTERSAMPLES(GAMMA)LLD(pCi/m3) 0.05 0.06 LASlO LOCATION DATE CS-134 CS-137 347217002 AS-361VA 02/14/14 0.1267+/-0.0163<0.000662 347217001AS-1PG02/14/140.1324+/-0.0173

<0.00071 347217003AS-7UH02/14/140.1404+/-0.019

<0.000977 353670002 AS-361VA 05/16/140.1198+/-0.0212*

<0.000982353670001AS-1PG05/16/140.1566+/-0.0211

<0.000735353670003AS-7UH05/16/140.1519+/-0.0193

<0.000708360405001AS-1PG08/15/140.1168+/-0.0193

<0.000702360405003AS-7UH08/15/140.09427

+/-0.0211<0.000764 360405002 AS-361VA08/15/140.1286+/-0.0204

<0.000851365218001AS-1PG11/14/140.09448

+/-0.0139<0.000628365218003AS-7UH11/14/140.07944+/-0.0151

<0.00056 365218002 AS-361VA11/14/140.07654

+/-0.0135<0.000509 46 TableA2.1SampleType:

Thermoluminescent DosimetersAnalysis:GammaDose Units: mrem/Qtr Inner Ring.Within GeneralAreaofSite Boundary Station 1st Qtr 2nd Qtr3rdQtr4th Qtr.Annual Mean 11.0..:....9.7 11.9 8.4 8.6 9.1 11.1 10.5 7.2 8.1 ,.**".*.,,,,,.*.*..W......y.,*.......*.,....y."".....7.9 12.1 13.3 11.5 12.5 11.3 13.9........................................

',..,." 9.9 10.0 10.9 12.6 12.3 8.6 8.8 8.8 13.7 14.8 12.4 11.1 10.3 12.3 8.7 8.5 9.4 11.8 ,.*"""'v , 10.2 7.2 8.1 8.1 12.1 12.7 11.7 10.4 8.9..........................

.;.,.11.2 7.5 7.8 7.0 9.7 9.1............v*****6.3 6.6 , ,.'" ,*.y.".........;.**,*6.8 10.7 12.8 10.3 9.8...*****1--8.5 10.4 ,*w""".*..*..." , 7.6 8.1 8.9 10.2"""".....,...,....10.6 6.7 9.0...., , ,-".'

..,..,., 8.0 12.0 12.9 11.5 M-16 M-19 M-21'.-......*,....,."*.,."'...".y..,..",.... M-22 M-23 M-25 M-28................

" ,., M-94 M-95 M-96 M-97 M-98 M-99*M-I00*Locationwith highestannualmean OuterRing-Approximately Three(3)toFive(5)Miles fromtheSite Station 1st Qtr 2nd Qtr 3rd Qtr 4th Qtr Annual Mean M-36 7.9 7.9................................

,.,....._........,.....M-40 5.9 5.2M-489.3 8.5**************

<-.***.**M-4910.9 10.4M-509.4 9.0M-5510.6 10.5M-57*11.3 10.7 9.0 ,y....._.,*...**.-5.8 10.3 11.6.................

'.....,*********

- - - ,,'9.4 11.5 12.0 9.6 8.6 ,"".,...., 7.0 6.0 11.6 9.9 12.5 11.3 11.7 9.9 13.0 11.4 13.7 11.9"Location with highestannualmean 47 TableA2.2 Sample Type: Thermoluminescent DosimetersAnalysis:GammaDose Units: mrem/Qtr Special InterestAreas-Population Centers&Schools;.Station1stQtr2ndQtr

,../M-Ol*11.5 11.7....-,....,-.: ,..,.,..,M-0710.3 10.5M-09'9.8 9.1 M-I0 8.8 7.7M-3320.1 7.4M-389.5 7.9..M-398.2 7.93rdQtr 11.7 11.0 10.6 8.8 8.3 10.4 9.4 4th Qtr 12.9 12.2 11.3 10.3 9.7 12.1 10.5 j Annual Mean 12.0 11.0 10.2 8.910.0 9.0*Location with highestannualmeanTableA2.3SampleType:

Thermoluminescent Dosimeters Analysis: Gamma Dose Units: mrem/Qtr Special InterestAreas-Control Station M-14 1st Qtr 10.1 2nd Qtr 10.3 48 3rd Qtr 11.0 4th Qtr 12.5 Annual Mean 11.0 Table A3.1 Sample Type: Surface Water Analysis: Gamma Isotopic Units: pC ilLSURFACEWATER SAMPLES (GAMMA)LLD (pCi/L)1515 30 15301530151518 60 15 LAB 10 LOCATIONDATEMN-54CO-58FE-59CO-60ZN-65NB-95ZR-95 1-131CS-134CS-137 BA-140 LA-140 344610003 MRUP03/11/14<3.45<3.33<7.18<4.11<6.82<3.69<5.77<5.57<3.58<3.69<5.60<5.60 344610004MRUPDUP03/11/14<3.92<3.62<8.48<4.49<7.75<3.72<7.13<6.69<4.49

<4.29<7.18<7.18 344610001 MRDOWN03/11/14<3.14<3.31<6.81<4.60<6.80<3.56<5.89<5.82<3.72<3.57<4.85<4.85 344610002 MRDOWN DUP03/11/14<3.66<3.44<7.39<4.18<7.87<4.04<5.78<5.58<4.02<3.56<5.63<5.63 351013005 MRUP 06/12/14<2.69<2.76<5.68<2.84<5.76<3.20<5.21<9.27<2.86<2.95<6.61<6.61 351013006MRUPDUP06/12/14<3.29<3.32<7.73<3.68<6.77<3.32<5.90<10.2<3.45<3.13<8;58<8.58 351013003 MRDOWN06/12/14<2.46<2.63<6.04<2.95<5.22<2.57<4.85<8.76<2.83<2.63<6.92<6.92 351013004 MRDOWN DUP06/12/14<2.59<3.01<6.06<2.8<5.24<3.00<5.35<10.2<2.78<2.96<7.85<7.85 356999002 MRUP 09/10/14<2.56<2.64<5.20<2.67

<4.94<2.57<4.58<5.37<2.84<2.74

<4.39<4.39 356999004MRUPDUP 09/10/14<2.31<2.5<5.09<2.78<5.43<2.47<4.27<5.43<2.67<2.80<4.34<4.34 356999001 MRDOWN09/10/14<2.20<2.70<5.19<3.04<5.60<2.75<4.48<5.47<2.86<2.65<4.82<4.82 356999003 MRDOWN DUP 09/10/14<2.32<2.63<4.83<3.01<5.55<2.68<4.97<5.70<2.94<2.73<4.70

<4.70 362094003 MRDOWN11/20/14<4.95

<4.52<8.92<5.48<11.3<5.10<9.07<15.0<5.31<5.43<12.5<12.5 362094004 MRUP11/21/14<4.45

<4.58<9.46<5.47<10.4<5.29<11.0<13.7<5.26<5.50<11.0<11.0 362094001 MRDOWN*11/20/14<4.01<4.00<8.01<3.78<8.18<4.38<6.86<11.2<4.49<3.55<9.11<9.11 362094002 MRDOWN DUP11/20/14<4.11<4.23<9.29<4.55<9.68<4.84<7.97<12.0<4.59<5.85<8.95<8.95*"DUP"-indicates duplicate sample*AnnualSamplecollectedduringliquiddischarge 49 Table A3.2 Sample Type: Surface Water Analysis: Tritium Units: pCilL SURFACE WATER SAMPLES (TRITIUM)LLO (pCi/L)3000 LASlO LOCATION DATE H-3 341487001 Outfall 00"101/14/14<350 343003001 Outfall 00"102/06/141492

+/-374 344618001Outfall007 03/07/14<430 344608001Outfall007 03/10/14<433 344610003 MRUP03/11/14<431 344610004MRUPDUP 03/11/14<433 344610001 MRDOWN 03/11/14<439 344610002MRDOWNDUP03/11/14<438 346231001Outfall00704/03/14<484 348187001Outfall007 05/01/14<461 350286001Outfall007 06/05/14<434 351013005 MRUP 06/12/14<488 351013006MRUPDUP 06/12/14<486 351013003 MRDOWN 06/12/14<493 351013004MRDOWNDUP06/12/14

<487 352091001Outfall00707/03/14<362 354271001Outfall00708/04/14<389 356092001Outfall00709/03/14<562 356999002 MRUP09/10/14<534 356999004MRUPDUP09/10/14<527 356999001 MRDOWN09/10/14<538 356999003MRDOWNDUP09/10/14<533 358411001 Outfall 00'709/30/14<346 360251001 Outfall 00'710/29/14<545 362094003 MRDOWN11/20/14<217 362094004 MRUP 11/21/14<218 362094001 MRDOWN*11/20/14<218 362094002MRDOWNDUP*11/20/14<216 362064001Outfall00711/24/14<218 363680001Outfall00712/22/14<375

AnnualSamplecollectedduringliquiddischarge"DUP"-indicates duplicate sample.50 TableA4.1SampleType:GroundWaterAnalysis:GammaIsotopicUnits:pCi/L GROUND WATERSAMPLES(GAMMA)LLD(pCi/L)1515301530153015186015 LABIDLOCATIONDATEMN-54CO-58FE-59CO-60ZN-65NB-95ZR-95CS-134CS-137BA-140LA-140362696001PGWELL12/08/14<3.33<3.47<6.84<3.33(<6.53<3.34<5.57<3.68<3.23<7.18<7.18 362696003 CONSlWELL3 12/08/14<4.20<4.62<7.69<3.60<7.15<4.73<7.33

<4.44<4.12<7.29<7.29 362696005 CONSlWELL4 12/08/14<3.47<3.40<7.09<3.99<7.19<3.47

<6.22<3.44<3.28<6.86<6.86 51 Table A4.2 Sample Type: Ground Water Analysis: Tritium Units: pCi/L GROUND WATER SAMPLES (TRITIUM)LLD (pCi/L)2000 LASID LOCATION DATE H-3 362696001 PGWELL 12/08/14<528 362696001 362696002 PGWELL GG DUP 12/08/14.;: 565 362696002 362696003 CONSTWELL3 12/08/14<566362696003 362696004 CONSTWELL3GG DUP 12/08/14<549362696004 362696005 CONSTWELL4 12/08/14<557362696005 362696006 CONSTWELL4GG DUP 12/08/14<562362696006"DUP"-indicates duplicate sample.52 TableA4.3SampleType:GroundWaterAnalysis:lodine-131Units:pCi/L GROUND WATER SAMPLES (IODINE-131)LLD(pCi/L) 1 LASID LOCATION DATE 1-131362696001PGWELL 12/08/14<0.576 362696003 CONSlWELL3 12/08/14<0.559 362696005 CONSlWELL4 12/08/14<0.811 53 Table A5.1SampleType:

SedimentAnalysis:Gamma IsotopicUnits:pCi/kg SEDIMENTSAMPLES(GAMMA)LLD(pCi/kg) 150 180 LASlO LOCATIONDATECS-134CS-137 357217002 SEDCONT 9/10/2014<43<31.4 357217001 SEDHAM 9/10/2014<38.5 39.39"DUP"-indicates duplicate sample.54 Table A6.1 Sample Type: Fish Analysis: Gamma Isotopic Units: pCi/kg FISH SAMPLES (GAMMA)LLD (pCi/kg)130130260130260130 150 LASlO LOCATION DATEMN-54CO-58FE-59CO-60ZN-65CS-134 CS-137356996001FISHUP09/10/14<11.0<11.5<33.5<13.7<26.1<11.3<10.9356996003FISHUPGGDUP 09/10/14<6.12<6.85<20.6<8.72<17.8<7.01<7.85 356996002 FISHDOWN 09/10/14<8.99<9.12<22.5<9.94<22.1<10.9

<10.4 356996004 FISHDOWNGGDUP09/10/14<6.91<8.35<17.8<7.94<19.5<8.20<7.07 55 TableA7.1SampleType:VegetationAnalysis:GammaIsotopic Units;pCi/kg VEGETATIONSAMPLES(GAMMA)LLD(pCi/kg) 60 60 80 LASlOLOCATIONDATE 1-131 CS-134 CS-137 345719001 VEG-CONT 03/26/14<18.1<9.63<8.91 345719002 VEG-J 03/27/14<22.7<15.8<13.9 351418001 VEG-CONT 06/18/14<11.1<5.98<5.75 351418003 VEG-CONTGGDUP 06/18/14<18.8<9.04<7.15 351418002 VEG-J 06/19/14<17.4<10.3<10.3 351418004VEG-JGGDUP 06/19/14<20.9<12.1<11.7 356447001 VEG-CONT 09/08/14<8.79<7.30<.7.30 356447002 VEG-J 09/08/14<9.95<8.40<7.41 56 TableA8.1 Sample Type: Special SamplesAnalysis:GammaIsotopicUnits:pCi/L SPECIALDEERMEAT SAMPLES (GAMMA)LLD15153015 30 15 18 LASlO LOCATIONDATEMN-54 CO-58 FE-59CO-60ZN-65CS-134CS-137 359956001 DEER 10/24/14<7.82<9.33<17.3<9.35<14.3<7.5<10 57 TableA9.1SampleType:

Quality Assurance Report Analysis: Environmental Dosimeters STANFORD DOSIMETRY ENVIRONMENTAL DOSIMETRY COMPANY ANNUAL QUALITY ASSURANCE STATUS REPORT January-December 2014 Prepared By: Approved By:\r'"../y AfI(

../*l Date: Date: Environmental Dosimetry Company 10 Ashton Lane Sterling,MA01564 TABLEOF CONTENTS PageLISTOFTABLES iii EXECUTIVE SUMMARy iv I.INTRODUCTION

1A.QCProgram 1B.QAProgram

, 1 II.PERFORMANCE EVALUATION CRITERIA 1 A.AcceptanceCriteriaforInternal Evaluations

1B.QC InvestigationCriteriaandResultReporting 3C.Reportingof Environmental DosimetryResultstoEDC Customers 3III.DATA

SUMMARY

FOR ISSUANCE PERIOD JANUARY-DECEMBER 2014 3 A.General Discussion

3B.Result Trending 4 IV.STATUSOFEDC CONDITION REPORTS (CR);4 V.STATUS OF AUDITS/ASSESSMENTS 4A.Internal 4B.External

4 VI.PROCEDURESANDMANUAL.S REVISED DURING JANUARY-DECEMBER20144 VII.CONCLUSION AND RECOMMENDATIONS 4 VIII.REFERENCES 4 APPENDIX A DOSIMETRY QUALITY CONTROL TRENDING GRAPHS-ii-1.2.3.LIST OF TABLES Percentage of Individual Analyses Which Passed EDC Internal Criteria, January-December 2014 Mean Dosimeter Analyses (n=6), January-December 2014 Summary of Independent QC Results for 2014-iii-5 5 5 EXECUTIVE

SUMMARY

Routine quality control (QC)testing was performed for dosimeters issued by the Environmental Dosimetry Company (EDC).During this annual period, 100%(72/72)ofthe individual dosimeters, evaluated against the EDC internal performance acceptance criteria (high-energy photons only), met the criterion for accuracy and 100%(72/72)met the criterion for precision (Table1).In addition, 100%(12/12)of the dosimeter sets evaluated against the internal tolerance limits met EDC acceptance criteria (Table2)and100%(6/6)of independent testing passed the performance criteria (Table 3).Trending graphs, which evaluate performance statistic for high-energy photon irradiations and co-located stations are given in Appendix A.Two assessments were performedin2014, one internal and one external.There were no findings.\-iv-I.INTRODUCTION The TLD systems at the Environmental Dosimetry Company (EDC)are calibrated and operated to ensure consistent and accurate evaluation of TLDs.The qualityofthe dosimetricresultsreported to EDC clients is ensured by in-house performance testing and independent performance testingbyEDC clients,andboth internal and client directed program assessments.

The purpose of the dosimetry quality assurance programisto provide performance documentation of the routine processingofEDC dosimeters.

Performance testing provides a statistical measure of the bias and precision of dosimetry processing against a reliable standard, whichinturn pointsoutany trends or performance changes.Two programsareused:A.QC Program Dosimetry quality control tests are performed on EDC Panasonic 814 Environmental dosimeters.

These tests include: (1)the in-house testing program coordinated by theEDCQA Officerand(2)independent test performbyEDC clients.In-house test are performedusingsix pairsof814 dosimeters, a pair is reportedasan individual resultandsix pairs are reportedasthe mean result.Results of these tests are described in this report.Excluded from this report are instrumentation checks.Although instrumentation checks represent an important aspectofthe quality assurance program, they are not included as process checks in this report.Instrumentation checks represent between 5-10%of the TLDs processed.

B.QA Program An internal assessment of dosimetry activities is conducted annually by the Quality Assurance Officer (Reference 1).The purpose of the assessmentisto review procedures, results, materials or components to identify opportunities to improve or enhance processes and/or services.II.PERFORMANCE EVALUATION CRITERIA A.Acceptance Criteria for Internal Evaluations1.Bias For each dosimeter tested, the measure of bias is the percent deviation of the reported result relative to the delivered exposure.The percent deviation relative to the delivered exposure is calculated as follows: where: H;=the corresponding reported exposure for the ith dosimeter (i.e., the reported exposure)Hi=the exposure delivered to the ith irradiated dosimeter (i.e., the delivered exposure)1of6 2.MeanBiasForeach group of test dosimeters,themeanbiasisthe average percent deviationofthe reported result relativetothe delivered exposure.The mean percent deviation relativetothe delivered exposure is calculated as follows: where:=the corresponding reported exposurefortheith dosimeter(Le.,the reported exposure)Hi=the exposure deliveredtotheith irradiated test dosimeter,(Le., the delivered exposure)n=the number of dosimetersinthetest group 3.PrecisionFora groupoftest dosimeters irradiatedtoa given exposure, the measure of precisionisthe percent deviation of individual results relativetothemean reported exposure.Atleasttwo values are requiredforthe determination of precision.

The measure of precisionforthe l" dosimeter is:(H'-R J l;H100 where:=the reported exposurefortheith dosimeter(Le.,the reported exposure).-(1)H=themean reported exposure;Le., H=nn=the number of dosimetersinthe test group 4.EDC Internal Tolerance Limits All evaluation criteria are takenfromthe"EDC Quality System Manual," (Reference 2).These criteriaareonly applied to individual test dosimeters irradiated withhigh-energyphotons (Cs-137)andareas follows for Panasonic Environmental dosimeters:

+/-15%forbiasand+/-12.8%for precision.

20f6 B.QC Investigation Criteria and Result Reporting EDC Quality System Manual (Reference 2)specifies when an investigation is required duetoaQC analysis thathasfailed theEDCbias criteria.The criteriaareas follows:1.No investigation is necessary when an individual QC result falls outsidetheQC performance criteria for accuracy.2.Investigations are initiated when the meanofaQC processing batch is outside the performance criterion for bias.C.Reporting of Environmental Dosimetry ResultstoEDC Customers 1.All resultsaretobe reportedina timely fashion.2.IftheQA Officer determines that an investigation is requiredfora process, the resultsshallbe issued as normal.IftheQCresults, prompting the investigation, have a meanbiasfrom the known of greater than+/-20 0/o, the resultsshallbe issuedwithanote indicating that theymaybe updatedinthefuture, pending resolutionofaQAissue.

3.Environmental dosimetry resultsdonot require updatingifthe investigation has shown that the mean bias between the original resultsandthe corrected results, based on applicable correction factorsfromthe investigation, does not exceed+/-20 0/0.III.DATA

SUMMARY

FOR ISSUANCE PERIOD JANUARY-DECEMBER 2014 A.General Discussion Results of performance tests conducted are summarized and discussedinthe following sections.Summariesofthe performance tests for the reporting period are given in Tables 1 through3and Figures 1 through 4.Table 1 provides a summary of individual dosimeter results evaluated against the EDC internal acceptance criteria for high-energy photons only.Duringthisperiod, 100%(72/72)ofthe individual dosimeters, evaluated against these criteria met the tolerance limits for accuracyand100%(72/72)met the criterion for precision.

A graphical interpretation is provided in Figures1and2.Table 2 providestheBias+Standard deviation results for each group(N=6)of dosimeters evaluated against the internal tolerance criteria.Overall, 100%(12/12)ofthe dosimeter sets evaluated against the internal tolerance performance criteria met these criteria.A graphical interpretation is provided in Figures 3 Table 3 presents the independent blind spike results for dosimeters processed during this annual period.All results passed the performance acceptance criterion.

Figure 4isa graphical interpretation of Seabrook Stationblind located station results.30f6 B.ResultTrendingOneofthemainbenefitsofperformingqualitycontroltestsonaroutinebasisistoidentifytrendsor performancechanges.TheresultsofthePanasonic environmental dosimeter performancetestsarepresentedinAppendixA.TheresultsareevaluatedagainsteachoftheperformancecriterialistedinSectionII,namely:individual dosimeteraccuracy,individual dosimeterprecision,andmean bias.AlloftheresultspresentedinAppendixAareplottedsequentiallybyprocessing date..IV.STATUSOFEDCCONDITIONREPORTS(CR)Noconditionreportswereissuedduringthisannualperiod.V.STATUSOF AUDITS/ASSESSMENTSA.InternalEDCInternalQuality Assurance Assessmentwasconductedduringthefourthquarter2014.Therewerenofindingsidentified.B.External The FPUNextEraEnergyNuclearOversightAuditSBK-14-019wasconducted on September 24,2014.Therewerenofindingsidentified.VI.PROCEDURESANDMANUALSREVISEDDURINGJANUARY-DECEMBER2014Noproceduresormanualswererevisedin2014.VII.CONCLUSIONAND RECOMMENDATIONSThequalitycontrolevaluationscontinuetoindicatethedosimetryprocessingprogramsattheEDCsatisfythecriteriaspecifiedintheQualitySystemManual.TheEDCdemonstratedtheabilitytomeetallapplicable acceptance criteria.VIII.REFERENCES1.EDCQualityControlandAuditAssessmentSchedule,2014.2.EDCManual1,QualitySystemManual,Rev.3,August1,2012.

4of6 TABLE 1 PERCENTAGE OF INDIVIDUAL DOSIMETERS THAT PASSED EDC INTERNAL CRITERIA JANUARY-DECEMBER 2014(1), (2)(1)This table summarizesresultsoftests conductedbyEDC.(2)Environmental dosimeterresultsarefreeinair.

TABLE 2 MEAN DOSIMETER ANALYSES (N=6)JANUARY-DECEMBER 2014(1), (2)4/19/2014 4/22/2014 4/30/2014 7/22/2014 7/25/2014 8/04/2014 9/24/2014 10/21/2014 10/28/2014 1/2512015 1/28/2015 3/11/2015 2.7-0.1 0.1 1.7 2.8-3.6 2.5 0.7 3.9 4.1 2.1-8.2 1.6 0.9 1.9 1.5 1.2 1.0 0.6 0.5 1.5 1.1 1.6 1.0 Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass Pass (1)This table summarizesresultsoftests conductedbyEDCforTLDsissuedin2014.

(2)Environmental dosimeterresultsarefreeinair.

TABLE 3

SUMMARY

OF INDEPENDENT DOSIMETER TESTING JANUARY-DECEMBER 2014(1), (2)1 5 Qtr.2014 2" Qtr.2014 2" Qtr.2014 3 r Qtr.2014 4 Qtr.2014 4 t Qtr.2014 Millstone Millstone Seabrook Millstone Millstone Seabrook 2.8-6.0 0.3-10.2-6.5 5.5 Pass Pass Pass Pass Pass Pass(1)Performancecriteriaare+/-30%.

(2)Slind spike irradiations using Cs-137 50f6 APPENDIX A DOSIMETRY QUALITY CONTROL TRENDING GRAPHSISSUEPERIOD JANAURY-DECEMBER 2014 6of6 16-10-, 8--16-;1I',..,,[""1 M"'"*'r""'"..., , ,'".I'I"'....1""\'lo.\'lo.\'lo.\'lo."" to-'"'k:V...,'<:ic)'I'l}"'V....."'V PROCESSING DATE-10-

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TableA.9.2SampleType:Quality Assurance ReportMatrix:Milk,Soil,Liquid, Vegetation,AirCharcoal,AirParticulate, Water GEL LABORATORIES LLC Laboratories LLC 2014 ANNUAL QUALITY ASSURANCE REPORTFORTHE RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM (REMP)GEL LLCP.O.Box30712,Charleston,SC29417 843.556.8171 Laboratories LLCP.O.Box30712, Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage2of64 2014 ANNUAL QUALITY ASSURANCE REPORTFORTHE RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM (REMP)Approved By: Robert L.Pullano Director, Quality Systems February15,2015Rev.1 Date Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORT TABLE OF CONTENTSPage3of64 1.INTRODUCTION 5 2.QUALITY ASSURANCE PROGRAMS FOR INTER-LABORATORY, INTRA-LABORATORY AND THIRD PARTY CROSS-CHECK 6 3.QUALITY ASSURANCE PROGRAM FOR INTERNAL AND EXTERNAL AUDITS 7 4.PERFORMANCE EVALUATION ACCEPTANCE CRITERIA FOR ENVIRONMENTAL SAMPLE ANALySiS:*8 5.PERFORMANCE EVALUATION SAMPLES 8 6.QUALITY CONTROL PROGRAM FOR ENVIRONMENTAL SAMPLE ANALYSIS 8 7.

SUMMARY

OF DATA RESULTS 9 8.

SUMMARY

OF PARTICIPATIONINTHE ECKERT&ZIEGLER ANAL YTICS ENVIRONMENTAL CROSS-CHECK PROGRAM ,..9 9.

SUMMARY

OF PARTICIPATION IN THE MAPEP MONITORING PROGRAM 10 10.

SUMMARY

OF PARTICIPATION IN THE ERA MRAD PT PROGRAM 10 11.

SUMMARY

OF PARTICIPATION IN THEERAPT PROGRAM 10 12.CORRECTIVE ACTION REQUEST AND REPORT (CARR)10 13.REFERENCES 12 Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORT TABLE OF CONTENTS (CONTINUED)

TABLESPage4of64Table12014 Radiological ProficiencyTestingResultsand Acceptance Criteria 13Table22014Eckert

&Ziegler Analytics Performance Evaluation Results 29Table32014 DepartmentofEnergyMixed Analyte Performance EvaluationProgram(MAPEP)

Results 31Table42014ERAProgram Performance Evaluation Results 36Table52014ERAProgram(MRAD)

Performance Evaluation Results 38Table6REMP Intra-Laboratory Data Summary:BiasandPrecisionByMatrix 53Table7All Radiological Intra-LaboratoryDataSummary:BiasandPrecisionByMatrix'",'",'"55Table82014 CorrectiveActionReport Summary 62 FIGURESFigure1 Cobalt-60 Performance EvaluationResultsand

%Bias 44Figure2 Cesium-137 Performance EvaluationResultsand

%Bias 45Figure3Tritium Performance EvaluationResultsand

%Bias 46Figure4 Strontium-90 Performance EvaluationResultsand

%Bias 47Figure5GrossAlpha Performance EvaluationResultsand

%Bias 48Figure6GrossBeta Performance EvaluationResultsand

%Bias 49Figure7lodine-131 Performance EvaluationResultsand

%Bias 50Figure8Americium-241 Performance EvaluationResultsand

%Bias 51Figure9 Plutonium-238 Performance EvaluationResultsand

%Bias 52 Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage5of64 2014 ANNUAL QUALITY ASSURANCE REPORTFORTHE RADIOLOGICAL ENVIRONMENTAL MONITORING PROGRAM (REMP)1.Introduction GEL Laboratories, LLC (GEL)isa privately owned environmental laboratory dedicated to providing personalized client servicesofthe highest quality.GEL was establishedasan analytical testing laboratoryin1981.Nowafull servicelab,our analytical divisionsusestateoftheart equipment and methods to provide a comprehensive array of organic, inorganic, and radiochemical analyses to meet the needs of our-clients,AtGEL, quality is emphasized at everylevelof personnel throughout the company.Management's ongoing commitmenttogood professional practiceandtothe qualityofour testing servicestoour customers is demonstrated by their dedication of personnel and resources to develop, implement, assess, and improve our technical and management operations.

The purpose of GEL's quality assurance programisto establish policies, procedures, and processes to meet or exceed the expectationsofourclients.To achievethis"all personnel that support these servicestoour clients are introducedtothe program and policies during their initial orientation, and annually thereafter during company-wide training sessions.GEL's primary goalsareto ensure that all measurement data generated are scientifically and legally defensible,ofknownand acceptable qualityperthedata quality objectives (DQOs), and thoroughly documented to provide sound support for environmental decisions.

In addition, GEL continues to ensure compliancewithall contractual requirements, environmental standards, and regulations establishedbylocal,stateand federal authorities.

GEL administerstheQA program in accordancewiththe Quality Assurance Plan, GL-QS-B-001.

Our Quality Systems include a.1I quality assurance (QA)policies and qualitycontrol(QC) procedures necessarytoplan, implement, and assess the work we perform.GEL's QA Program establishes a quality management system (QMS)that governsallofthe activitiesofour organization.

This report entails the quality assurance programforthe proficiency testing and environmental monitoring aspects of GEL fot 2014.GEL's QA Program is designed to monitor the quality of analytical processing associated with environmental, radiobioassay, effluent (10 CFRPart50),and waste (10CFRPart61) sample analysis.This report covers the category of Radiological Environmental Monitoring Program (REMP)and includes:*intra-laboratory QC results analyzed during 2014.*Inter-laboratoryQCresults analyzed during 2014 where known values were available.

Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage6of64 2.Quality Assurance Programs for Inter-laboratory, Intra-laboratory and Third PartyCheckInadditiontointernalandclientaudits,ourlaboratoryparticipatesinannualperformanceevaluationstudiesconductedbyindependentproviders.Weroutinelyparticipateinthefollowingtypesofperformanceaudits:*Proficiencytestingandotherinter-laboratorycomparisons*PerformancerequirementsnecessarytoretainCertifications*Evaluationofrecoveriesofcertifiedreferenceandin-housesecondaryreferencematerialsusingstatisticalprocesscontroldata.*Evaluationofrelativepercentdifferencebetweenmeasurementsthrough SPCdata.Wealsoparticipateinanumberofproficiencyprogramsforfederalandstateagenciesandasrequiredbycontracts.Itisourpolicythatnoproficiencyevaluationsamplesbeanalyzedinanyspecialmanner.Ourannualperformanceevaluationparticipationgenerallyincludesacombinationofstudiesthatsupportthefollowing:*USEnvironmentalProtectionAgencyDischargeMonitoringReport,QualityAssuranceProgram(DMR-QA).AnnualnationalprogramsponsoredbyEPAforlaboratoriesengagedintheanalysisofsamplesassociatedwiththeNPDESmonitoringprogram.ParticipationismandatoryforallholdersofNPDESpermits.Thepermitholdermustanalyzeforalloftheparameterslistedonthedischargepermit.Parametersincludegeneralchemistry,metals,BOD/COD,oilandgrease,ammonia,nitrates,etc.*DepartmentofEnergyMixedAnalytePerformanceEvaluationProgram(MAPEP).AsemiannualprogramdevelopedbyDOEinsupportofDOEcontractorsperformingwasteanalyses.Participationisrequiredforalllaboratoriesthatperformenvironmentalanalyticalmeasurementsinsupportofenvironmentalmanagementactivities.Thisprogramincludesradioactiveisotopesinwater,soil,vegetationandairfilters.

ERA'sMRAD-MultimediaRadiochemistryProficiencytestprogram.Thisprogramisforlabsseekingcertificationforradionuclidesin wastewaterandsolidwaste.TheprogramisconductedinstrictcompliancewithUSEPANationalStandardsforWaterProficiencystudy.*ERA'sInterLaBRadCheMProficiencyTestingProgramforradiologicalanalyses.ThisprogramcompletestheprocessofreplacingtheUSEPAEMSL-LVNuclearRadiationAssessmentDivisionprogramdiscontinuedin1998.Laboratoriesseekingcertificationforradionuclideanalysisindrinkingwateralsousethestudy.ThisprogramisconductedinstrictcompliancewiththeUSEPANationalStandardsforWaterProficiencyTestingStudies.ThisprogramencompassesUraniumbyEPAmethod200.8(fordrinkingwatercertificationinUtah/PrimaryNELAP),gammaemitters,GrossAlpha/Beta,lodine-131,naturallyoccurringradioactiveisotopes,Strontium-89/90,andTritium.*ERA'sWaterPollution(WP)biannualprogramforwastemethodologiesincludesparametersforbothorganicandinorganicanalytes.

Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage7of64*ERA's Water Supply (WS)biannual program for drinking water methodologies includes parameters for organic and in9rganic analytes.*Environmental Cross-Check Program administered by Eckert&Ziegler Analytics,Inc.This program encompasses radionuclidesinwater,soil,milk, naturally occurring radioactive isotopesinsoilandairfilters.

GEL procures single-blind performance evaluation samples from Eckert&Ziegler Analytics to verify the analysis of sample matrices processedatGEL.Samples are receivedona quarterly basis.GEL's Third-Party Cross-Check Program provides environmental matrices encounteredina typical nuclear utility REMP.The Third-Party Cross-Check Program is intended to meet or exceed the inter-laboratory comparison program requirements discussedinNRC Regulatory Guide 4.15.Once performance evaluation samples have been prepared in accordancewiththe instructions providedbythePT provider, samples are managed and analyzedinthe same manner as environmental samples from GEL's clients.3.Quality Assurance Program for Internal and External Audits During each annual reporting period, at least one internal assessmentofeachareaofthe laboratory is conducted in accordancewiththe pre-established schedule from Standard Operating Procedureforthe Conduct of Quality Audits, GL-QS-E-001.

The annual internal auditplanis reviewed for adequacy and includes the scheduled frequency and scope of quality control actions necessary to GEL's QA program.Internal audits are conducted at least annually in accordancewitha schedule approvedbythe Quality Systems Director.Supplieraudits'are contingentuponthe categorizationofthe supplier, and mayormaynotbe conducted priortotheuseofa supplier or subcontractor.

Type I suppliers and subcontractors, regardlessofhow they were initially qualified, are re-evaluated at least once every three years.In addition, prospectivecustomersaudit GEL during pre-contract audits.GEL hosts several external audits each yearforbothour clients and other programs.These programs include environmental monitoring, waste characterization, and radiobioassay.

The followinglistof programs may audit GEL at least annuallyorupto every three years dependingonthe program.*NELAC, National Environmental Laboratory Accreditation Program*DOECAP, U.S.Department of Energy Consolidated Audit Program*DOELAP, U.S.Department of Energy Laboratory Accreditation Program*DOEQSAS,U.S.

Department of Energy, Quality Systems for Analytical Services.'ISOIIEC 17025:2005

A2LA, American Association for Laboratory Accreditation*DODELAP,US Department of Defense Environmental Accreditation Program*NUPIC, Nuclear Procurement Issues Committee*South Carolina Department of Heath and Environmental Control (SC DHEC)The annual radiochemistry laboratory internal audit (13-RAD-001) was conductedinJuly,2014.

One (1)finding, four (4)observations, and eight (8)recommendations resultedfromthis assessment.

By September,2014,the finding was closed and appropriate laboratory staff addressed each observation and recommendation.

Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage8of64 4.Performance Evaluation Acceptance Criteria for Environmental Sample AnalysisGELutilizedanacceptanceprotocolbasedupontwoperformancemodels.Forthoseinter-laboratoryprogramsthatalreadyhaveestablishedperformancecriteriaforbias(i.e.,MAPEP,andERAIELAP),GELwillutilizethecriteriaforthespecificprogram.Forintra-laboratoryorthirdpartyqualitycontrolprogramsthatdonothaveaspecificacceptancecriteria(i.e.theEckert-ZieglerAnalyticsEnvironmentalCross-checkProgram),resultswillbeevaluatedinaccordancewithGEL'sinternalacceptancecriteria.

5.Performance Evaluation SamplesPerformanceEvaluation(PE)resultsandinternalqualitycontrolsampleresultsareevaluatedinaccordancewithGELacceptancecriteria.Thefirstcriterionconcernsbias,whichisdefinedasthedeviationof anyoneresultfromtheknownvalue.Thesecondcriterionconcernsprecision,whichdealswiththeabilityofthemeasurementtobereplicatedbycomparisonofanindividualresultwiththemeanofallresultsforagivensampleset.AtGEL,wealsoevaluateouranalyticalperformanceonaregularbasisthroughstatisticalprocesscontrol(SPC)acceptancecriteria.Wherefeasible,thiscriterionisappliedtobothmeasuresofprecisionandaccuracyandisspecifictosamplematrix.Weestablishenvironmentalprocesscontrollimitsatleastannually.ForRadiochemistryanalysis,qualitycontrolevaluationisbasedonstaticlimitsratherthanthosethatarestatisticallyderived.OurcurrentprocesscontrollimitsaremaintainedinGEL'sAlphaLlMS.Wealsomeasureprecisionwithmatrixduplicatesand/ormatrixspikeduplicates.Theupperandlowercontrollimits(UCLandLCLrespectively)forprecisionareplusorminusthreetimesthestandarddeviationfromthemeanofaseriesofrelativepercentdifferences.Thestaticprecisioncriteriaforradiochemicalanalysesare0-20%,foractivitylevelsexceedingthecontractrequireddetectionlimit(CRDL).

6.Quality Control Program for Environmental Sample AnalysisGEL'sinternalQAProgramisdesignedtoincludeQCfunctionssuchasinstrumentationcalibrationchecks(toinsureproperinstrumentresponse),blanksamples,instrumentationbackgrounds,duplicates,aswellasoverallstaffqualificationanalysesandstatisticalprocesscontrols.Bothqualitycontrolandqualificationanalysessamplesareusedtobeassimilarasthematrixtypeofthosesamplessubmittedforanalysisbythevariouslaboratoryclients.Theseperformancetestsamples(orperformanceevaluationsamples)areeitheractualsamplesubmittedinduplicateinordertoevaluatetheprecisionoflaboratorymeasurements,orfortifiedblanksamples,whichhavebeengivenaknownquantityofaradioisotopethatisintheinteresttoGEL'sclients.Accuracy(orBias)ismeasuredthroughlaboratorycontrolsamplesand/ormatrixspikes,aswellassurrogatesandinternalstandards.TheUCLsandLCLsforaccuracyareplusorminusthreetimesthestandarddeviationfromthemeanofaseriesofrecoveries.Thestaticlimitforradiochemicalanalysesis75-125%.Specificinstructionsforout-of-controlsituations'areprovidedintheapplicableanalytical SOP.GEL'sLaboratoryControlStandard(LCS)isanaliquotofreagentwaterorotherblankmatrixtowhichknownquantitiesofthemethodanalytesareaddedinthelaboratory.TheLCSisanalyzedexactlylikeasample,anditspurposeistodeterminewhetherthemethodologyisincontrol,andwhetherthelaboratoryiscapableofmakingaccurateandprecisemeasurements.Somemethodsmayrefertothese Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage9of64 samples as Laboratory Fortified Blanks(LFB).The requirement for recovery is between75and 125%for radiological analyses excluding drinking water matrix.Bias(%)=(observed concentration)*100%(known concentration)

Precisionisadata quality indicatorofthe agreement between measurementsofthesameproperty, obtained under similar conditions,andhowwellthey conform to themselves.

Precision is usually expressed as standard deviation, varianceorrangein either absoluteorrelative (percentage) terms.GEL's laboratory duplicate(OUPorLCSO)isan aliquotofa sampletakenfromthesame container and processedinthesame manner under identical laboratory conditions.

The aliquotisanalyzed independentlyfromthe parent sampleandtheresultsare compared to measure precision and accuracy.Ifasampleduplicate is analyzed,itwillbereportedas Relative Percent Difference(RPO).TheRPOmustbe20 percentorless,ifboth samples are greaterthan5 timestheMOC.Ifbothresultsarelessthan5timesMOC,thentheRPO mustbeequaltoorlessthan100

%.IfoneresultisabovetheMOCandthe otherisbelowtheMOC,thentheRPOcanbe calculatedusingtheMOCfortheresultofthe one belowtheMOC.TheRPOmustbe100

%orless.Inthe situation where both results are above theMOCbutoneresultis greaterthan5 timestheMOCandthe otherislessthan5 timestheMOC,theRPOmustbelessthanorequalto 20%:Ifbothresultsare belowMOC,thenthelimitson%RPOare not applicable.

Difference

(%)=(high duplicate result-low duplicate result)*100%(averageofresults) 7.Summary of Data ResultsDuring2013, forty-four (44)radioisotopes associatedwithseven(7) matrix types were analyzed under GEL's Performance Evaluation program in participationwithERA,MAPEP,and Eckert&Ziegler Analytics.Matrixtypeswere representativeofclient analyses performedduring2014.

Ofthefour hundred forty-five(445)totalresults reported, 98.6%(439of445)werefoundtobe acceptable.Thelist below containsthetypeof matrix evaluatedbyGEL.*AirFilter

Cartridge*Water*Milk*Soil*Liquid*Vegetation Graphs are provided in Figures1-9ofthis report to allowforthe evaluation of trendsorbiases.These graphs include radioisotopes Cobalt-60, Cesium-137, Tritium, Strontium-90, Gross Alpha, Gross Beta, lodine-131, Americium-241, and Plutonium-238.

8.Summary of Participation in the Eckert&Zie'gler Analytics Environmental Cross-Check Program Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage10of64 Eckert&ZieglerAnalyticsprovidedsamplesforsixty-nine(69)individualenvironmentalanalyses.TheaccuracyofeachresultreportedtoEckert

&ZieglerAnalytics,Inc.ismeasuredbytheratioofGEL'sresulttotheknownvalue.AllresultsfellwithinGEL'sacceptancecriteria(100

%).9.Summary of Participation in the MAPEP Monitoring ProgramMAPEPSeries30and31wereanalyzedbythelaboratory.Oftheonehundredthirty-eight(138) analyses, 97.80/0(135outof138)ofallresultsfellwithinthePTprovider'sacceptancecriteria.Threeanalyticalfailuresoccurred:Uranium-234/233andUranium-238inSoilandUranium-238invegetation.ForthecorrectiveactionsassociatedwithMAPEPSeries30,refertoCARR140605-879whichisdetailedinTable8.

10.Summary of ParticipationintheERAMRaDPT ProgramTheERAMRadprogramprovidedsamples(MRAD-20andMRAD-21)foronehundredeighty-eight(188)individualenvironmentalanalyses.Onehundredeighty-seven(187)ofthe188analysesfellwithinthePTprovider'sacceptancecriteria(99.4%).Oneanalyticalfailureoccurred:Americium-241inwater.ForthecorrectiveactionsassociatedwithMRAD-20,refertoCARR140520-874whicharedetailedinTable8.11.Summary of ParticipationintheERAPT ProgramTheERAprogramprovidedsamples(RAD-96,RAD-98,and011014L)forfifty(50)individualenvironmentalanalyses.Ofthe50analyses, 96.0%(48outof50)ofallresultsfellwithinthePTprovider'sacceptancecriteria.Oneisotopefailureoccurred:Strontium-89inwater.ForthecorrectiveactionsassociatedwithRAD-98refertocorrectiveactionsCARR140825-902(Table 8).12.Corrective Action Request and Report (CARR)TherearetwocategoriesofcorrectiveactionatGEL.OneiscorrectiveactionimplementedattheanalyticalanddatareviewlevelinaccordancewiththeanalyticalSOP.TheotherisformalcorrectiveactiondocumentedbytheQualitySystemsTeaminaccordancewithGL-QS-E-002.Aformalcorrectiveactionisinitiatedwhenanonconformancereoccursorissosignificantthatpermanenteliminationorpreventionoftheproblemisrequired.Formalcorrectiveactioninvestigationsincluderootcause analysis.GELincludesqualityrequirementsinmostanalyticalstandardoperatingprocedurestoensurethatdataarereportedonlyifthequalitycontrolcriteriaaremetorthequalitycontrolmeasuresthatdidnotmeettheacceptancecriteriaaredocumented.AformalcorrectiveactionisimplementedaccordingtoE-002forConductingCorrective/PreventiveActionandIdentifyingOpportunitiesforImprovement.RecordinganddocumentationisperformedfollowingguidelinesstatedinGL-QS-E-012forClientNCRDatabaseOperation.

Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage11of64AnyemployeeatGELcanidentifyandreportanonconformanceandrequestthatcorrectiveactionbetaken.AnyGELemployeecanparticipateonacorrectiveactionteamasrequestedbytheQSteamorGroupLeaders.ThestepsforconductingcorrectiveactionaredetailedinGL-QS-E-002.Intheeventthatcorrectnessorvalidityofthelaboratory'stestresultsindoubt,thelaboratorywilltakecorrectiveaction.Ifinvestigationsshowthattheresultshavebeenimpacted,affectedclientswillbeinformedof the issueinwritingwithinfive(5)calendardaysofthediscovery.Table8providesthestatusofCARRsforradiologicalperformancetestingduring2014.Ithasbeen determined that causes of the failures did not impactanydata reported to our clients.

Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORT 13.ReferencesPage12of641.GELQuality AssurancePlan,GL-QS-B-0012.GELStandardOperatingProcedureforthe ConductofQualityAudits,GL-QS-E-0013.GELStandardOperatingProcedurefor Conducting Corrective/PreventiveActionandIdentifyingOpportunitiesforImprovement, GL-QS-E-0024.GELStandardOperatingProcedurefor AlphaLiMS Documentation of Nonconformance ReportingandDispositioningandControlof Nonconforming Items, GL-QS-E-0045.GELStandardOperatingProcedureforHandling ProficiencyEvaluationSamples, GL-QS-E-0136.GELStandardOperating ProcedureforQuality Assurance Measurement Calculations and Processes, GL-QS-E-0147.40CFRPart136 GuidelinesEstablishingTest ProceduresfortheAnalysisofPollutants8.ISO/IEC17025-2005,General Requirementsforthe CompetenceofTestingandCalibration Laboratories9.ANSI/ASQCE4-1994, Specifications and GuidelinesforQualitySystemsfor Environmental DataCollectionand Environmental TechnologyPrograms,AmericanNationalStandard10.2003NELACStandard,National Environmental Laboratory Accreditation Program11.2009TNIStandard,TheNELACInstitute,National Environmental Accreditation Program12.MARLAP, Multi-Agency Radiological LaboratoryAnalyticalProtocols13.10CFRPart21,ReportingofDefectsand Noncompliance14.10CFRPart50 AppendixB,Quality AssuranceCriteriafor NuclearPowerPlantsandFuelReprocessingPlants 15.10CFRPart61,Licensing RequirementsforLandDisposaland Radioactive Waste16.NRCREGGuide4.15andNRCREGGuide4.8 Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage13of64 TABLE 1 2014 RADIOLOGICAL PROFICIENCY TESTINGRESULTSAND ACCEPTANCE CRITERIA1st I RAD-ERA 2014 02/24/14 96 Water Gill Barium-133 80.676.263.8-83.8Accetable1st I RAD-ERA2014 02/24/14 96 Water GillGesium-13464.766.854.4-73.5Accetable1st I RAD-ERA 2014 02/24/1496Water GillGesium-137112.010998.1-122Accetable1st I RAD-ERA2014 02/24/14 96 Water GillGobalt-6095.088.779.8-99.9Accetable1st I RAD-ERA 2014 02/24/1496Water GillZinc-65200185166-218Accetable1st I RAD-ERA 2014 02/24/14 96 Water GillGrossAIha34.836.118.6-46.4Accetable1st I RAD-ERA2014 02/24/14 96 Water GillGrossBeta19.622.313.5-30.4Accetable1st I RAD-ERA 2014 02/24/1496Water GillGrossAIha34.636.118.6-46.4Accetable1st I RAD-ERA2014 02/24/14 96 Water Gill Radium-226

.16.216.812.5-19.2Accetable1st I RAD-ERA 2014 02/24/1496Water Gill4.625.043.01-6.67Accetable1st I RAD-ERA2014 02/24/14 96 Water7.397.235.51-8.53Accetable1st I RAD-ERA 2014 02/24/1496Water 11.00 10.68.07-12.5Accetable 1st I RAD-ERA2014 02/24/14 96 Water GillRadium-22615.1016.812.5-19.2Accetable1st I RAD-ERA2014 02/24/14 96 Water Gill4.665.043.01-6.67Accetable1st I RAD-ERA2014 02/24/14 96 Water7.477.235.51-8.53Accetable 1st I RAD-ERA2014 02/24/14 96 Water 11.4 10.68.07-12.5Accetable1st I RAD-ERA2014 02/24/1496Water Gill Tritium 3320 35803030-3950Accetable1st I RAD-Strontium-ERA2014 02/24/14 96 Water Gill8944.144.434.4-51.6Accetable 1st I RAD-Strontium-ERA2014 02/24/14 96 Water Gill 90 34.230.322.1-35.2Accetable1st I RAD-Strontium-ERA2014 02/24/14 96 Water Gill8938.944.434.4-51.6Accetable1st I RAD-Strontium-ERA2014 02/24/1496Water Gill 90 27.130.322.1-35.2Accetable1st I Strontium-ERA2014 02/06/14 011014l Water Gill8942.338.729.3-45.7Accetable1st I Strontium-ERA2014 02/06/14 011014l Water Gill 89 42.238.729.3-45.7Accetable1st I RAD-ERA 2014 02/24/1496Water Gill lodine-13125.224.420.2-28.9Accetable1st I RAD-ERA2014 02/24/14 96 lodine-13122.424.420.2-28.9Accetable EZA 1sU2014 05/16/14 E10846 lodine-1317.83E+017.50E+031.04Accetable Strontium-EZA 1sU2014 05/16/14 E10847 Milk Gill899.14E+019.17E+01Accetable Strontium-EZA 1sU2014 05/16/14E10847Milk Gill901.27E+011.51E+010.84Accetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage14of64

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" y EZA 1sU2014 05/16/14E10848Milk Ci/llodine-1319.84E+019.85E+01Accetable EZA1sU201405/16/14E10848Milk Ci/l Cerium-1411.21E+021.19E+02Accetable EZA 1sU2014 05/16/14E10848Milk Ci/l Cr-515.19E+024.91E+02Accetable EZA1sU201405/16/14E10848Milk Ci/lCesium-1341.79E+02 2.10E+02Accetable EZA1sU201405/16/14E10848Milk Ci/lCesium-1372.55E+02 2.53E+02Accetable EZA1sU201405/16/14E10848Milk Ci/lCobalt-582.58E+02 2.68E+02Accetable EZA1sU201405/16/14E10848Milk CillMn-543.01E+022.97E+02Accetable EZA1sU201405/16/14E10848Milk CillIron-592.24E+022.19E+02Accetable EZA1sU201405/16/14E10848Milk Ci/lZinc-653.45E+023.23E+02Accetable EZA1sU201405/16/14E10848Milk Ci/lCobalt-603.39E+023.37E+02Accetable EZA1sU201405/16/14E10849Water Ci/l lodine-1319.24E+018.99E+01Accetable EZA1sU201405/16/14 E10849 Water Ci/lCerium-1418.19E+017.71E+01Accetable EZA1sU201405/16/14E10849Water Ci/lCr-513.32E+023.19E+02Accetable EZA1sU201405/16/14E10849Water Ci/lCesium-1341.27E+021.36E+02Accetable EZA1sU201405/16/14E10849Water 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580 643444-824Accetable MAPEP-14-Manganese-MAPEP2nd/2014 06/05/14 MaS30SoilB Ik54147014301001-1859Accetable MAPEP-14-FalsePas MAPEP 2nd/2014 06/05/14 MaS30SoilB IkNickel-636.950 TestAccetable MAPEP-14-Plutonium-MAPEP2nd/2014 06/05/14MaS30SoilB Ik23889.796.067-125Accetable MAPEP-14-Plutonium-MAPEP2nd/2014 06/05/14MaS30SoilB Ik 239/240 69.8076.853.8-99.8Accetable MAPEP-14-Potassium-MAPEP 2nd/2014 06/05/14 MaS30SoilB Ik 40703622 435-809Accetable MAPEP-Strontium-FalsePasMAPEP2nd/2014 06/05/14 14-SoilB Ik901.480TestAccetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUALQUALITY ASSURANCE REPORTPage15of64 ,mp MaS30 MAPEP-14-Technetium-FalsePas MAPEP2nd/201406/05/14MaS30SoilB/k 9937.10 TestAccetable MAPEP-14-NotMAPEP2nd/2014 06/05/14 MaS30 SoilB/kU-234/23330.581.057-105Acce t.MAPEP-14-Uranium-NotMAPEP2nd/201406/05/14MaS30SoilB/k 238358358-108Acce t.MAPEP-14-MAPEP2nd/201406/05/14MaS30SoilB/kZinc-65766695487-904Accetable 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MAPEP-14-Strontium-MAPEP2nd/201406/05/14MaW30WaterB/L908.328.515.96-11.06Accetable MAPEP-14-Technetium-MAPEP 2nd/201406/05/14MaW30WaterB/L 999.510.37.2-13.4Accetable MAPEP-14-MAP,EP2nd/201406/05/14MaW30WaterB/LU-234/2330.2100.2250.158-0.293Accetable MAPEP-14-Uranium-MAPEP2nd/201406/05/14MaW30WaterB/L2381.411.451.02-1.89Accetable MAPEP-FalsePasMAPEP2nd/201406/05/1414-WaterB/LZinc-65-0.1260.0TestAccetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUALQUALITY ASSURANCE REPORTPage16of64 MaW30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 Water B ILGrossAIha0.960.850.255-1.443Accetable MAPEP-14-MAPEP 2nd/2014 06/05/14MaW30WaterB ILGrossBeta 4.7 4.22.10-6.29Accetable MAPEP-14-FalsePas MAPEP2nd/201406/05/14MaW30WaterB IL lodine-129 0.0227 0.00TestAccetable MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14RdF30Filter u IsamIe2350.0180.0200.014-0.026Accetable MAPEP-14-Uranium-MAPEP2nd/201406/05/14 RdF30 Filter u IsamIe2388.7710.47.3-13.5Accetable MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14 RdF30 Filter u IsamIeTotal8.8010.47.3-13.5Accetable MAPEP-14-Americium-MAPEP 2nd/2014 06/05/14 RdF30 Filter u IsamIe2410.0860.0900.063-0.117Accetable MAPEP-14-MAPEP2nd/201406/05/14 RdF30 Filter B Isam Ie Cesium-134 1.85 1.911.34-2.48Accetable MAPEP-14-MAPEP 2nd/2014 06/05/14 RdF30 Filter B Isam Ie Cesium-137 1.81 1.761.23-2.29Accetable MAPEP-14-FalsePas MAPEP 2nd/2014 06/05/14RdF30FilterB IsamIeCobalt-570.07570.00TestAccetable MAPEP-14-MAPEP2nd/201406/05/14 RdF30FilterB IsamIeCobalt-601.490 1.390.97-1.81Accetable MAPEP-14-Manganese-FalsePas MAPEP2nd/201406/05/14 RdF30 Filter B IsamIe540.0138

0.0 0TestAccetable

MAPEP-14-Plutonium-MAPEP2nd/201406/05/14 RdF30 Filter B IsamIe2380.0008190.00090Sens.Eva!.Accetable MAPEP-14-0.054-MAPEP2nd/201406/05/14 RdF30FilterB Isam Ie Pu-239/240 0.0710.77200.1004Accetable MAPEP-14-Strontium-MAPEP2nd/201406/05/14 RdF30FilterB IsamIe90 1.191.180.83-1.53Accetable MAPEP-14-0.0137-MAPEP 2nd/2014 06/05/14RdF30FilterB Isam Ie U-234/233 0.0159 0.0195 0.0254Accetable MAPEP-14-Uranium-MAPEP2nd/201406/05/14 RdF30FilterB IsamIe2380.1180.1290.090-0.168Accetable MAPEP-14-FalsePas MAPEP 2nd/2014 06/05/14 RdF30FilterB Isam Ie Zinc-65 0.2460.00TestAccetable MAPEP-14-MAPEP 2nd/2014 06/05/14RdF30Filter 0.6561.200.36-2.04Accetable MAPEP-14-MAPEP2nd/201406/05/14 RdF30FilterB Isam IeGrossBeta0.950.850.43-1.28Accetable MAPEP-Americium-MAPEP2nd/201406/05/14 14-FilterB Isam Ie 241 0.1060.1040.073-0.135Accetable Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage17of64

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MAPEP-14-Uranium-MAPEP2nd/201406/05/14 RdV30 23812.713.39.3-17.3Aeeetable MAPEP-14-Uranium-MAPEP2nd/201406/05/14RdV30Total12.713.39.3-17.3Aeeetable MAPEP-14-Amerieium-

.MAPEP2nd/201406/05/14RdV30.2410.11000.1080.076-0.140Aeeetable MAPEP-14-MAPEP2nd/201406/05/14RdV30 Cesium-1345.656.044.23-7.85Aeeetable MAPEP-14-MAPEP2nd/201406/05/14RdV30.Cesium-1374.984.743.32-6.16Aeeetable MAPEP-14-MAPEP2nd/201406/05/14 RdV30 Cobalt-5711.110.17.1-13.1Aeeetable MAPEP-14-MAPEP2nd/201406/05/14RdV30 Cobalt-607.216.934.85-9.01Aeeetable MAPEP-14-Manganese-MAPEP2nd/201406/05/14RdV30 549.248.626.03-11.21Aeeetable MAPEP-14-Plutonium-MAPEP2nd/201406/05/14 RdV302380.1160.1210.085-0.157Aeeetable MAPEP-14-0.108-MAPEP2nd/2014 06/05/14 RdV30 Pu-239/240

.0.1340.1540.0200Aeeetable MAPEP-14-Strontium--r:**MAPEP2nd/201406/05/14RdV30 901.5801.461.02-1.90Aeeetable MAPEP-14-0.0177-MAPEP2nd/201406/05/14RdV30U-234/2330.26400.25300.0329Aeeetable MAPEP-14-Uranium-MAPEP2nd/201406/05/14RdV302380.1740.1650.116-0.215Aeeetable MAPEP-14-MAPEP2nd/201406/05/14RdV30Zine-658.877.004.38-8.13Aeeetable MRAD-Aetinium-ERA2nd/201405/16/14 20SoilCi/k22811401240795-1720Aeeetable MRAD-Amerieium-ERA2nd/201405/16/14 20SoilCi/k 241 418 399 233-518Aeeetable MRAD-Bismuth-ERA2nd/201405/16/1420SoilCi/k 2129761240330-1820Aeeetable MRAD-Bismuth-ERA2nd/201405/16/14 20 Soil Ci/k214229019601180-2820Aeeetable MRAD-ERA2nd/201405/16/14 20SoilCilk Cesium-134 3080 33902220-4070Aeeetable MRAD-ERA 2nd/20M05/16/1420SoilCi/kCesium-137 8310 8490 6510-10900Aeeetable MRAD-ERA2nd/201405/16/14 20SoilCi/kCobalt-60 657068304620-9400Aeeetable MRAD-ERA2nd/201405/16/1420SoilCi/kLead-212 13301240812-1730AeeetableERA2nd/2014 05/16/14 MRAD-SoilCi/k Lead-214280020701210-3090Aeeetable Laboratories LLC P.O.Box 30712, Charleston, SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage18of64 ERA2nd/201405/16/1420SoilCilk54<44.3<10000-1000Accetable ERA2nd/201405/16/1420SoilCi/k238579578348-797Accetable ERA2nd/201405/16/1420 Soil Ci/k239488471.00308-651Accetable ERA2nd/201405/16/1420 Soil Ci/k 4010500105007660-14100Accetable ERA2nd/201405/16/1420SoilCi/k 90250027801060-4390Accetable ERA2nd/201405/16/1420SoilCi/k234 3420 33601060-6320Accetable ERA2nd/201405/16/1420SoilCi/kZinc-65570054004300-7180Accetable ERA 2nd/2014 05/16/1420SoilCi/k 90 6730 85303250-13500Accetable ERA2nd/201405/16/1420SoilCi/k234260233902070-4350Accetable ERA 2nd/2014 05/16/1420SoilCi/k2382425 33602080-4260AccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetable 911-1980 1470-342044800 253-804 2300-5150 415-839 3750-9120 2070-4350 3750-9120 1260-2890 2080-4260 0.00-300 638-1220 639-1290 3750-9120 2070-4350 2080-4260 5570-12700 5570-12700 5570-12700 5570-12700 6910 3390 3390<300 1490 3740 2580 3360 2110 3360 646 6910 880 516 926 6910 31900 10100 10100 10100 10100 514 3780 2230 7310 3680 3810 7683 997 2330 1670 7110 5027 861 3440 3740 657<62.2 30800 11200 11300 11000 238 Strontium-Total Cobalt-60 239 40 Curium-244 Cesium-137 Cesium-134 54 Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil2020202020202020202020202020202020 MRAD-202020 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage19of64.W***M*****\t..",,,w 20 90 MRAD-Uranium-ERA2nd/201405/16/1420234192017601160-2260Accetable MRAD-Uranium-ERA2nd/201405/16/1420238197017501170-2220Accetable MRAD-Uranium-ERA2nd/201405/16/1420Total4025 3580 2430-4460Accetable MRAD-ERA2nd/2014*05/16/14 20592052403510-6650Accetable MRAD-ERA2nd/201405/16/1420 Zinc-651030919663-1290Accetable MRAD-Uranium-ERA2nd/201405/16/1420 234173017601160-2260Accetable MRAD-Uranium-ERA2nd/201405/16/1420238200017501170-2220Accetable MRAD-Uranium-ERA2nd/2014 05/16/14 20Total3817 35802430-4460Accetable MRAD-ERA2nd/201405/16/1420 599052403510-6650Accetable MRAD-ERA2nd/201405/16/1420562052403510-6650Accetable MRAD-ERA2nd/201405/16/1420 Filter60.259.736.8-80.8Accetable MRAD-ERA2nd/201405/16/1420 Filter Cesium-1349201010643-1250Accetable MRAD-ERA2nd/201405/16/1420 Filter Cesium-137816828622-1090Accetable MRAD-ERA2nd/201405/16/14 20 FilterCobalt-6011301120867-1400Accetable MRAD-ERA2nd/201405/16/14 20 FilterIron-5525424074.4-469Accetable MRAD-Manganese-ERA2nd/201405/16/14 20 Filter54<6.64<50.00-50.0Accetable MRAD-Plutonium-ERA2nd/201405/16/1420 Filter 23851.356.338.6-74.0Accetable MRAD-Plutonium-ERA2nd/201405/16/14 20 Filter 23947.548.635.2-63.5Accetable MRAD-Strontium-ERA2nd/201405/16/1420 Filter 90 76.778.938.6-118Accetable MRAD-Uranium-ERA2nd/201405/16/14 20 Filter 23433.836.422.6-54Accetable MRAD-Uranium-ERA2nd/201405/16/14 20 Filter23834.536.123.3-49.9Accetable MRAD-Uranium-ERA2nd/201405/16/1420 FilterTotal70.374.341.1-113Accetable MRAD-Uraniuni-ERA2nd/201405/16/1420 FilterTotalmass10410869.1-152Accetable MRAD-ERA2nd/201405/16/14 20 FilterZinc-65737667478-921Accetable MRAD-Uranium--, ERA2nd/201405/16/1420 Filter 234 35.536.422.6-54Accetable MRAD-Uranium-ERA2nd/201405/16/14 20 Filter 23835.336.123.3-49.9Accetable MRAD-Uranium-ERA2nd/201405/16/1420 Filter Total72.474.341.1-113Accetable MRAD-Uranium-I.ERA2nd/201405/16/1420 FilterTotalmass10510869.1-152Accetable.MRAD-Uranium-ERA2nd/201405/16/14 20 FilterTotalmass10010869.1-152Accetable MRAD-ERA2nd/201405/16/1420 FilterGrossAIha60.94615.4-71.4AccetableERA2nd/201405/16/14MRAD-FilterGrossBeta58.953.834.0-78.4Accetable Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage20of64 ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/14 05/16/142020202020202020202020202020202020202020202020202020202020 Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill Gill 241 Gesium-134 Gesium-137 Gobalt-60 Iron-55 54 238 239 90234238Total Zinc-65234238TotalGrossAIhaGrossBeta 186 1540 2760 1320 1230<7.54 37 124 95 77.8 50.8 156 233 2030 82.1 84.6 170 253 80.5 90.0 175 269 77.8 78.3 156 233 232 141.0 172 114 1660 2690 1270 1200<100 44 160 890 82.4 48.4 168 245 1800 82.4 48.4 168 245 82.4 48.4 168 245 82.4 48.4 168 245 245 133 174.0 76.8-153 1220-1910 2280-3220 1100-1490 716-1630 0.00-100 32.6-54.9 124-202 580-1180 61.9-106 36.9-59.4 123-217 195-296 1500-2270 61.9-106 36.9-59.4 123-217 195-296 61.9-106 36.9-59.4 123-217 195-296 61.9-106 36.9-59.4 123-217 195-296 195-296 47.2-206 99.6-258 NotAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetable AccetableAccetableAccetableAccetableAccetableAccetable AccetableAccetableAccetableAccetableAccetableAccetableAccetableAccetable AccetableAccetable ERA EZA 2nd/2014 2nd/2014 05/16/14 08/08/1420 E10897 Tritium lodine-131 5280 8.73E+01 5580 8.54E+01 3740-7960 1.02AccetableAccetable Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage21of64

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.<:(Strontium-EZA2nd/201408/08/14 E10898 Milk Ci/l 899.84E+019.13E+011.08Accetable Strontium-EZA2nd/201408/08/14E10898Milk Ci/l 901.44E+011.45E+010.99Accetable EZA 2nd/2014 08/08/14 E10899 Milk Ci/llodine-1319.89E+019.09E+011.09Accetable EZA2nd/201408/08/14 E10899 Milk Ci/lCerium-1411.38E+021.24E+021.12Accetable Chromium-EZA2nd/201408/08/14E10899Milk Ci/l 512.68E+022.53E+02 1.06Accetable EZA2nd/201408/08/14 E10899 Milk Ci/lCesium-1341.58E+021.62E+020.97Accetable EZA2nd/201408/08/14E10899Milk Ci/lCesium-1371.27E+021.20E+021.06Accetable EZA2nd/201408/08/14E10899Milk Ci/lCobalt-581.20E+021.12E+021.07Accetable Manganese-EZA 2nd/2014 08/08/14E10899Milk Ci/l541.67E+021.56E+021.07Accetable EZA2nd/201408/08/14E10899Milk Ci/lIron-591.02E+021.02E+021.00Accetable EZA2nd/201408/08/14E10899Milk Ci/l Zinc-652.68E+022.52E+021.06Accetable EZA2nd/201408/08/14E10899Milk Ci/lCobalt-602.42E+022.24E+021.08Accetable EZA2nd/201408/08/14E10900Water Ci/llodine-1311.13E+029.83E+011.15Accetable EZA2nd/201408/08/14E10900Water Ci/lCerium-1411.52E+021.43E+021.06Accetable Chromium-EZA2nd/201408/08/14E10900Water Ci/l513.62E+022.94E+021.23Accetable EZA 2nd/2014 08/08/14E10900Water Ci/lCesium-1341.69E+021.88E+020.90Accetable EZA2nd/201408/08/14E10900Water Ci/l Cesium-1371.48E+021.39E+021.06Accetable EZA 2nd/2014 08/08/14 E10900 Water" Ci/l/Cobalt-581.34E+021.30E+02 1.03Accetable Manganese-EZA2nd/201408/08/14 E10900 Water541.88E+021.80E+021.04Accetable EZA2nd/201408/08/14 E10900 WaterIron-591.29E+021.19E+02 1.09Accetable EZA2nd/201408/08/14E10900Water Zinc-653.29E+022.93E+021.12Accetable EZA2nd/201408/08/14E10900WaterCobalt-602.74E+022.60E+02 1.05Accetable 3rd IRAD-ERA2013 08/25/14 98 Water Ci/lBarium-13367.868.757.3-75.6Accetable 3rd I RAD-ERA 2013 08/25/14 98 Water Ci/l71.72.359.0-79.5Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/l Cesium-137161163147-181Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/l Cobalt-6076.775.568.0-85.5Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/l Zinc-65928273.8-98.5Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/lGrossAIha45.345.423.6-57.4Accetable 3rd IRAD-ERA 2013 08/25/14 98 Water Ci/lGrossBeta32.3 33.421.7-41.1Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/lGrossAIha48.645.423.6-57.4Accetable 3rd I RAD-ERA 2013 08/25/14 98 Water Ci/l Radium-2268.269.066.80-10.6Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/lRadium-2268.549.066.80-10.6Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/l Radium-226 9.79.066.80-10.6Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/l Radium-2285.075.073.03-6.79Accetable 3rd I RAD-ERA2013 08/25/14 98 Water Ci/l5.745.07 3.03-6.79Accetable 3rd I RAD-ERA 2013 08/25/14 98 Water 13.913.510.7-15.4Accetable 3rd I RAD-ERA 2013 08/25/14 98 Water22.2519.815.6-22.6Accetable 3rd I RAD-ERA2013 08/25/14 98 Water 1313.510.7-15.4Accetable ERA 3rdI08/25/14 RAD-Water20.719.815.6-22.6Accetable Laboratories LLCP.O.Box30712, Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage22of64aer 2013 3rd IERA2013 08/25/14 Water Ci/l Tritium10200112009750-12300Accetable 3rd I ERA 2013 08/25/14 Water Ci/lTritium10400112009750-12300Accetable 3rd I Strontium-NotERA2013 08/25/14 Water Ci/l8956.3 42.732.9-49.8Accetable 3rd I Strontium-ERA 2013 08/25/14 Water Ci/l 9028.231.723.1-36.7Accetable 3rd I Strontium-NotERA2013 08/25/14 Water Ci/l8956.542.732.9-49.8Accetable 3rd I Strontium-ERA2013 08/25/14 Water Ci/l 902631.723.1-36.7Accetable 3rd IERA2013 08/25/14 Water Ci/l lodine-13128.626.121.7-30.8Accetable 3rd IERA2013 08/25/14lodine-13122.326.121.7-30.8Accetable EZA3rd/201411/22/14lodine-1319.47E+018.99E+011.05Accetable Strontium-EZA3rd/201411/22/14E10994Milk Cill 899.73E+019.69E+011.00Accetable Strontium-EZA 3rd/2014 11/22/14E10994Milk Ci/l901.31E+011.64E+000.80Accetable EZA3rd/201411/22/14E10995Milk Ci/llodine-1311.04E+029.76E+01 1.07Accetable EZA3rd/201411/22/14E10995Milk Ci/lCerium-1411.28E+021.26E+021.01Accetable Chromium-EZA3rd/201411/22/14E10995Milk Ci/l513.12E+022.88E+021.08Accetable EZA3rd/201411/22/14E10995Milk Ci/lCesium-1341.51E+021.58E+02 0.96Accetable EZA3rd/201411/22/14E10995Milk Ci/lCesium-1372.03E+021.93E+021.05Accetable EZA3rd/201411/22/14E10995Milk CillCobalt-581.44E+021.43E+021.01Accetable Manganese-EZA3rd/201411/22/14E10995Milk Ci/l541.49E+021.42E+021.05Accetable EZA 3rd/2014 11/22/14E10995Milk Ci/lIron-591.82E+021.58E+021.15Accetable EZA3rd/201411/22/14E10995Milk Ci/lZinc-657.41E+017.30E+011.01Accetable EZA 3rd/2014 11/22/14 E10995 Milk Ci/lCobalt-603.14E+022.94E+021.06Accetable EZA3rd/201411/22/14 E10996 Water Ci/llodine-1311.02E+029.88E+01103Accetable EZA3rd/201411/22/14E10996Water Ci/lCerium-1411.30E+021.25E+02104Accetable Chromium-EZA3rd/201411/22/14E10996Water Ci/l512.75E+022.86E+020.96Accetable EZA3rd/201411/22/14 E10996 Water Ci/lCesium-1341.45E+021.56E+020.93Accetable EZA3rd/201411/22/14E10996Water Ci/lCesium-1371.94E+021.92E+021.01Accetable EZA 3rd/2014 11/22/14E10996Water Ci/lCobalt-581.43E+021.42E+021.01Accetable Manganese-EZA 3rd/2014 11/22/14E10996Water Ci/l 541.46E+021.41E+021.04Accetable EZA3rd/201411/22/14E10996Water Ci/lIron-591.66E+021.57E+021.06Accetable EZA3rd/201411/22/14 E10996 Water Ci/lZinc-657.55E+017.24E+011.04Accetable EZA3rd/201411/22/14 E10996 Water Ci/lCobalt-603.09E+022.95E+021.05Accetable MAPEP-14-MAPEP 4th1201401/09/15GrF31Filter0.4330.5300.16-0.09Accetable MAPEP-14-MAPEP 4th1201401/09/15GrF31FilterBIsamIeGrossBeta1.0601.0600.53-1.59Accetable MAPEP-14-Americium-MAPEP4th 12014 01/09/15MaS31Soil B IK 24188.485.559.9-111.2Accetable MAPEP-14-MAPEP 4th1201401/09/15MaS31SoilB IKCesium-134588622435-809Accetable MAPEP-14-FalsePosMAPEP4th 12014 01/09/15 MaS31 Soil B IKCesium-1371.67 TestAccetable Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage23of64 14-MAPEP4th/201401/09/15MaS31SoilB/KCobalt-5711601116781-1451 Acce table MAPEP-14-MAPEP 4th/2014 01/09/15MaS31SoilB/KCobalt-60821779545-1013Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31SoilB/KIron-55796 680476-884Accetable MAPEP-14-Manganese-MAPEP 4th/2014 01/09/15 MaS31 SoilB/K5410601009706-1312Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31SoilB/KNickel-63924 980686-1274Accetable MAPEP-14-Plutonium-MAPEP4th/201401/09/15MaS31SoilB/K 238 0.92 0:48 Sens.Eval.Accetable MAPEP-14-Plutonium-MAPEP4th/201401/09/15MaS31 SoilB/K239/24061.558.641.0-76.2Accetable MAPEP-14-Potassium-MAPEP4th/201401/09/15MaS31SoilB/K 40879824577-1071Accetable MAPEP-14-Strontium-MAPEP4th/201401/09/15MaS31 SoilB/K 90 891858601-1115Accetable MAPEP-14-Technetium-MAPEP 4th/201401/09/15MaS31 SoilB/K 99 466 589412-766Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31SoilB/K U-234/2339058962-116Accetable MAPEP-14-Uranium-MAPEP4th/201401/09/15MaS31SoilB/K238257259181-337Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31SoilB/K Zinc-65605.0541379-703Accetable MAPEP-14-Americium-MAPEP4th/201401/09/15MaW31 WaterB/L 2410.9150.8800.62-1.14Accetable MAPEP-14-FalsePasMAPEP4th/201401/09/15MaW31WaterB/LCesium-134-0.06TestAccetable MAPEP-14-MAPEP4th/201401/09/15MaW31WaterB/L Cesium-13718.418.412.9-23.9Accetable MAPEP-14-MAPEP4th/201401/09/15MaW31WaterB/L Cobalt-572524.717.3-32.1Accetable MAPEP-14-MAPEP4th/201401/09/15 Ma'W31 WaterB/LCobalt-6012.512.48.7-16.1Accetable MAPEP-14-MAPEP4th/201401/09/15MaW31 Water216208146-270Accetable MAPEP-14-MAPEP 4th 12014 01/09/15 MaW31 WaterB/L Iron-5534.031.522.1-41.0Accetable MAPEP-14-Manganese-MAPEP4th/201401/09/15MaW31 WaterB/L 54 14.214.09.8-18.2Accetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage24of64 MAPEP-14-MAPEP 4th1201401/09/15 MaW31 Water B IL Nickel-6323.624.6 17.2-32.0Accetable MAPEP-14-Plutonium-MAPEP4th1201401/09/15MaW31Water B IL 2380.5470.618 0.433-0.803Accetable MAPEP-14-Plutonium-MAPEP4th1201401/09/15 MaW31 Water B IL 239/2400.0150.005Sens.Eva!.Accetable MAPEP-14-Potassium-MAPEP4th1201401/09/15 MaW31 Water B IL 40174161113-209Accetable MAPEP-14-Strontium-FalsePos MAPEP 4th1201401/09/15 MaW31 Water B IL 90 0.03TestAccetable MAPEP-14-Technetium-MAPEP 4th 12014 01/09/15 MaW31 Water B IL996.92 6.994.89-9.09Accetable MAPEP-14-Uranium-MAPEP4th1201401/09/15 MaW31 Water B IL 234/2330.2060.205 0.144-0.267Accetable MAPEP-14-Uranium-MAPEP 4th 12014 01/09/15 MaW31 Water B IL2381.2801.4200.99-1.85Accetable MAPEP-14-MAPEP4th1201401/09/15 MaW31 Water B ILZinc-6511.90010.907.6-14.2Accetable MAPEP-14-MAPEP 4th 12014 01/09/15 MaW31 Water B ILGrossAIha0.7930.701 0.201-1.192Accetable MAPEP-14-MAPEP 4th 12014 01/09/15 MaW31 Water B ILGrossBeta6.220 5.942.97-8.91Accetable MAPEP-14-Uranium-0.0278-MAPEP4th1201401/09/15 RdF31 Filter u IsamIe2350.0400.0400.0516Accetable MAPEP-14-Uranium-MAPEP 4th 12014 01/09/15 RdF31 Filter u IsamIe23819.320.314.2-26.4Accetable MAPEP-14-Uranium-MAPEP 4th 12014 01/09/15 RdF31 Filter u Isam Ie Total19.0020.414.3-26.5Accetable MAPEP-14-Americium-0.0472-MAPEP 4th1201401/09/15 RdF31 Filter u Isam Ie 241 0.0561 0.0670.0876Accetable MAPEP-14-MAPEP4th1201401/09/15RdF31FilterB Isam Ie Cesium-1340.86400.960.67-1.25Accetable MAPEP-14-MAPEP4th1201401/09/15RdF31FilterB Isam Ie Cesium-137 1.190 1.200.84-1.56Accetable MAPEP-14-MAPEP4th1201401/09/15RdF31Filter B Isam Ie Cobalt-57 1.5401.431.00-1.86Accetable MAPEP-14-MAPEP4th 12014 01/09/15 RdF31FilterB IsamIeCobalt-601.200 1.10 0.77-1.43Accetable MAPEP-14-Manganese-MAPEP4th1201401/09/15 RdF31FilterB Isam Ie540.8080.750.53-0.98Accetable MAPEP-14-Plutonium-MAPEP4th 12014 01109/15 RdF31 Filter B Isam Ie 238 0.155 0.107 0.075-0.139Accetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUALQUALITY ASSURANCE REPORTPage25of64 MAPEP-14-Plutonium-0.0328-MAPEP4th1201401/09/15 RdF31FilterB Isam Ie 239/2400.0480.04680.0608Accetable MAPEP-14-Strontium-MAPEP4th1201401/09/15 RdF31FilterB Isam Ie 900.7620.700.492-0.914Accetable MAPEP-14-Uranium-0.0251-MAPEP4th 12014 01/09/15RdF31FilterB Isam Ie 234/2330.0370.03580.0465Accetable MAPEP-14-Uranium-MAPEP4th1201401/09/15 RdF31FilterB IsamIe2380.2270.2530.177-0.329Accetable MAPEP-14-MAPEP4th1201401/09/15 RdF'31FilterB Isam Ie Zinc-650.7790.760.53-0.99Accetable MAPEP-14-Americium-MAPEP4th 12014 01/09/15 RdV31 241 0.226 0.190.135-0.251Accetable MAPEP-14-MAPEP 4th1201401/09/15 RdV31 Cesium-1344.7505.203.64-6.67Accetable MAPEP-14-MAPEP4th1201401/09/15 RdV31Cesium-1376.910 6.604.62-8.58Accetable MAPEP-14-FalsePosMAPEP4th1201401/09/15 RdV31Cobalt-57-0.0020.00TestAccetable MAPEP-14-FalsePosMAPEP4th1201401/09/15 RdV31Cobalt-600.0080.00TestAccetable MAPEP-14-Manganese-MAPEP4th1201401/09/15 RdV31547.9807.885.52-10.24Accetable MAPEP-14-Plutonium-MAPEP4th1201401/09/15 RdV312380.0010.001Sens.Eva!.Accetable MAPEP-14-Plutonium-MAPEP4th 12014 01/09/15 RdV31 239/2400.15100.1710.120-0.222Accetable MAPEP-14-Strontium-MAPEP4th 12014 01/09/15 RdV31 90 2.3302.321.62-3.02Accetable MAPEP-14-Uranium-0.0326-MAPEP4th1201401/09/15 RdV31 234/233 0.0460.0470.0606Accetable MAPEP-14-Uranium-MAPEP4th1201401/09/15 RdV312380.3320.3240.227-0.421Accetable MAPEP-14-MAPEP4th1201401/09/15 RdV31Zinc-652.8502.631.84-3.42Accetable MAPEP-14-SrF-Strontium-MAPEP 4th1201401/09/15 31FilterB Isam Ie893.623.792.65-4.93Accetable MAPEP-14-SrF-Strontium-MAPEP4th1201401/09/15 31 Filter B Isam Ie903.623.792.65-4.93Accetable MAPEP-14-MAPEP4th 12014 01/09/15XaW-31Water B IL lodine-1294.564.553.19-5.92Accetable 3rd I MRAD-Actinium-ERA2014 11/25/14 21SoilCi/k 228 12801240795-1720AccetableERA3rd I 11/25/14 MRAD-SoilCi/k Americium-825763431-956Accetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage26of64 a mp.Ef.*2014 21 241 3rd 1 MRAD-Bismuth-ERA2014 11/25/14 21SoilCi/k21216201240330-1820Accetable 3rd 1 MRAD-Bismuth-ERA2014 11/25/14 21SoilCi/k 214290028101690-4040Accetable 3rd 1 MRAD-ERA2014 11/25/14 21SoilCi/kCesium-134196021401400-2570Accetable 3rd 1 MRAD-ERA2014 11/25/14 21SoilCi/kCesium-1376760 65505020-8430Accetable 3rd 1 MRAD-ERA2014 11/25/14 21SoilCi/kCobalt-60448042602880-5860Accetable 3rd 1 MRAD-ERA2014 11/25/14 21SoilCi/kLead-21212601240812-1730Accetable 3rd 1 MRAD-ERA2014 11/25/14 21SoilCilkLead-2143480 27501610-4100Accetable 3rd 1 MRAD-Manganese-ERA2014 11/25/14 21SoilCi/k54<30.0<10000-1000Accetable 3rd 1 MRAD-Plutonium-ERA 2014 11/25/14 21 Soil Ci/k 238732739444-1020Accetable 3rd 1 MRAD-Plutonium-ERA 2014 11/25/14 21SoilCi/k239281 309202-427Accetable 3rd 1 MRAD-Potassium-ERA 2014 11/25/14 21SoilCi/k4011500107007810-14400Accetable 3rd 1 MRAD-Strontium-ERA2014 11/25/14 21 Soil Cilk 90879084203210-13300Accetable 3rd 1 MRAD-Thorium-ERA 2014 11/25/14 21SoilCi/k 23420002350743-4420Accetable 3rd 1 MRAD-ERA2014 11/25/14 21 Soil Ci/k391032702600-4350Accetable 3rd 1 MRAD-ERA2014 11/25/14 21SoilCi/k228023701450-3040Accetable 3rd 1 MRAD-ERA 2014 11/25/14 21SoilCi/k234023501450-2980Accetable 3rd 1 MRAD-ERA2014 11/25/14 21SoilCi/k476245402360-6390Accetable 3rd 1 MRAD-ERA 2014 11/25/14 21 Soil702070503890-8870Accetable 3rd 1 MRAD-ERA 2014 11/25/14 21226022901400-3505Accetable 3rd 1 MRAD-ERA2014 11/25/14 21 Cesium-134837849545-1100Accetable 3rd 1 MRAD-ERA 2014 11/25/14 21Cesium-137729644467-896Accetable 3rd 1 MRAD-ERA 2014 11/25/14 21Cobalt-60818784541-1100Accetable 3rd 1 MRAD-ERA 2014 11/25/14 21 Curium-244361367180-572Accetable 3rd 1 MRAD-Manganese-ERA 2014 11/25/14 21 54<25.3<3000-300Accetable 3rd 1 MRAD-Plutonium-ERA 2014 11/25/14 21238886 862514-1180Accetable 3rd 1 MRAD-Plutonium-ERA2014 11/25/14 21239675701430-965Accetable 3rd 1 MRAD-Potassium-22300-ERA 2014 11/25/14 21403530030900 43400Accetable 3rd 1 MRAD-Strontium-ERA 2014 11/25/14 21 9012301710975-2270Accetable 3rd 1 MRAD-Uranium-ERA2014 11/25/14 21234198017801170-2290Accetable 3rd 1 MRAD-Uranium-ERA 2014 11/25/14 21 238 197017601170-2240Accetable ERA 3rd 1 11/25/14 MRAD-Uranium-40383620 2450-4510Accetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage27of64 ffiP.,vmPQ 2014 21 Total3rd/MRAD-ERA201411/25/1421591052803540-6710Accetable3rd/MRAD-ERA201411/25/1421167017801170-2290Accetable3rd/MRAD-ERA201411/25/1421180017601170-2240Accetable3rd/MRAD-ERA201411/25/1421355636202450-4510Accetable3rd/MRAD-ERA201411/25/1421539052803540-6710Accetable3rd/MRAD-ERA 2014 11/25/14 21 586052803540-6710Accetable3rd/MRAD-ERA201411/25/1421Zinc-65193015701130-2200Accetable3rd/MRAD-Americium-ERA2014 11/25/14 21 Filter24141.438.623.8-52.2Accetable3rd/MRAD-ERA201411/25/1421 FilterCesium-134742765.0487-949Accetable3rd/MRAD-ERA 201411/25/1421 FilterCesium-137677647486-850Accetable3rd/MRAD-ERA201411/25/1421 Filter Cobalt-60543523405-653Accetable3rd/MRAD-ERA201411/25/1421 FilterIron-55117120.037.2-234Accetable3rd/MRAD-Manganese-ERA 201411/25/1421 Filter54<5.87<500.00-50.0Accetable3rd/MRAD-Plutonium-ERA201411/25/14 21 Filter 238 32.9'35.724.5-46.9Accetable3rd/MRAD-Plutonium-ERA201411/25/1421 Filter23926'.829.121.1-38.0Accetable3rd/MRAD-Strontium-ERA 2014 11/25/14 21 Filter 90 187 168 82,1-252Accetable3rd/MRAD-Uranium-ERA'201411/25/14 21 Filter 234 26 2827.8-41.9Accetable3rd/MRAD-Uranium-ERA 201411/25/1421 Filter 2382827.6017.8-38.2Accetable3rd/MRAD-Uranium-ERA201411/25/1421 Filter Total565731.4-86.3Accetable3rd/MRAD-Uranium-ERA201411/25/14 21 FilterTotalmass82.682.752.9-116Accetable3rd/MRAD-ERA201411/25/1421 FilterZinc-65629547392-755Accetable3rd/MRAD-Uranium-ERA201411/25/1421 Filter 234 282827.8-41.9Accetable3rd/

Uranium-ERA201411/25/14 21 Filter 2382527.6017.8-38.2Accetable3rd/MRAD-Uranium-ERA201411/25/14 21 Filter Total555731.4-86.3Accetable3rd/MRAD-Uranium-ERA201411/25/14 21 FilterTotalmass75.182.752.9-116Accetable3rd/MRAD-Uranium-ERA201411/25/1421 Filter'Totalmass 90.782.752.9-116Accetable3rd/MRAD-ERA201411/25/1421 FilterGrossAIha47.436.912.4-57.3Accetable3rd/MRAD-ERA201411/25/14 21 FilterGrossBeta27.221.113.3-30.8Accetable3rd/MRAD-Americium-ERA201411/25/14 21 Water Ci/l 24172.468.646.2-92.0Accetable3rd/MRAD-ERA201411/25/14 21 Water Ci/lCesium-134816.0850624-977Accetable ERA3rd/11/25/14 MRAD-Water Ci/lCesium-137131012401060-1490Accetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage28of64

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2014 21 3rd I MRAD-ERA2014 11/25/14 21 Water GillGobalt-6011301070930-1250Accetable 3rd I MRAD-ERA2014 11/25/14 21 Water GillIron-5513013479.9-182Accetable 3rd I MRAD-Manganese-ERA2014-11/25/14 21 Water Gill54<6.34<1000.00-100Accetable 3rd I MRAD-Plutonium-ERA 2014 11/25/14 21 Water Gill 238353324.6-41.4Accetable 3rd I MRAD-Plutonium-ERA2014 11/25/14 21 Water Gill 23946.45139.7-64.4Accetable 3rd I MRAD-Strontium-ERA 2014 11/25/14 21 Water Gill 90 300254165-336Accetable 3rd I MRAD-Uranium-ERA2014 11/25/14 21 Water Gill 234424432.9-56.5Accetable 3rd I MRAD-Uranium-ERA2014 11/25/14 21 Water Gill 238 5043.5033.2-53.4Accetable 3rd I MRAD-Uranium-ERA 2014 11/25/14 21 Water Gill Total928965.5-115Accetable 3rd I MRAD-ERA2014 11/25/14 21 Water137130104-157Accetable 3rd I MRAD-ERA 2014 11/25/14 21 Water GillZinc-651070921768-1160Accetable 3rd I MRAD-Uranium-ERA2014 11/25/14 21 Water Gill 234434432.9-56.5Accetable 3rd I MRAD-Uranium-ERA 2014 11/25/14 21 Water Gill 2384543.5033.2-53.4Accetable 3rd I MRAD-Uranium-ERA 2014 11/25/14 21 Water Gill Total9089 65.5-115Accetable 3rd I MRAD-ERA 2014 11/25/14 21 Water134130104-157Accetable 3rd I MRAD-ERA 2014 11/25/14 21 Water Gill494432.9-56.5Accetable 3rd I MRAD-ERA 2014 11/25/14 21 Water Gill4243.5033.2-53.4Accetable 3rd I MRAD-ERA 2014 11/25/14 21 Water Gill9389 65.5-115Accetable 3rd I MRAD-ERA2014 11/25/14 21 Water126130104-157Accetable 3rd I MRAD-ERA2014 11/25/14 21 Water 144130104-157Accetable 3rd I MRAD-ERA2014 11/25/14 21 Water GillGrossAIha96.298 34.8-152Accetable 3rd I MRAD-ERA2014 11/25/14 21 Water GillGrossBeta86.177.5 44.4-115Accetable 3rd I MRAD-ERA2014 11/25/14 21 Water GillTritium54905500 3680-7840 Acce table Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage29of64TABLE2 2014 ECKERT&ZIEGLER ANALYTICS PERFORMANCE EVALUATION RESULTS Acceptable 9.17E+01 9.14E+01pCilL Milk E10847 05/16/14 1sU2014 EZA EZA1sU201405/16/14 E10846 CartridgepCilodine-1317.83E+017.52E+011.04 Acceptable 89 EZA1sU201405/16/14 E10847MilkpCi/L901.27E+011.51E+010.84 Acceptable EZA1sU201405/16/14E10848Milk pCilLlodine-1319.84E+019.85E+01 Acceptable EZA1sU201405/16/14 E10848 MilkpCi/LCerium-1411.21E+02 1.19E+02 1.02 Acceptable EZA1sU201405/16/14E10848Milk pCi/L Cr-51 5.19E+02 4.91E+02 1.06 Acceptable EZA1sU201405/16/14E10848Milk pCi/L Cesium-134 1.79E+02 2.10E+02 0.85 Acceptable EZA1sU201405/16/14 E10848 Milk pCi/L Cesium-137 2.55E+02 2.53E+02 1.01 Acceptable EZA1sU201405/16/14E10848MilkpCi/LCObait-582.58E+022.68E+02 0.96 Acceptable EZA1sU201405/16/14E10848MilkpCi/LMn-54 3.01E+02 2.97E+02 1.01 Acceptable EZA1sU201405/16/14E10848MilkpCi/L Iron-59 2.24E+02 2.19E+02 1.02 Acceptable EZA1sU201405/16/14 E10848 Milk pCi/LZinc-653.45E+023.23E+02 1.07 Acceptable EZA1sU201405/16/14 E10848 Milk ec ilL Cobalt-603.39E+023.37E+02 1.00 Acceptable EZA1sU201405/16/14 E10849 Water pCi/Llodine-1319.24E+018.99E+011.03 Acceptable EZA 1sU2014 05/16/14E10849WaterpCilL Cerium-1418.19E+017.71E+011.06 Acceptable EZA1sU201405/16/14 E10849 WaterpCilLCr-51 3.32E+02 3.19E+02 1.04 Acceptable EZA1sU201405/16/14 E10849 Water ecn.Cesium-134 1.27E+02 1.36E+02 0.93 Acceptable EZA1sU201405/16/14 E10849 Water pCi/L Cesium..:137 1.69E+02 1.64E+02 1.03 Acceptable EZA1sU201405/16/14 E10849 Water pCi/L Cobalt-58 1.i5E+02 1.74E+02 1.01 Acceptable EZA1sU201405/16/14 E10849 Water pCi/L Mn-54 2.08E+02 1.93E+02 1.08 Acceptable EZA 1sU2014 05/16/14 E10849 WaterpCilL.Iron-59 1.68E+02 1.42E+02 1.18 Acceptable EZA 1sU2014 05/16/14 E10849 WaterpCilL Zinc-65 2.25E+02 2.10E+02 1.07 Acceptable EZA1sU201405/16/14 E10849 Water pCilL Cobalt-602.31E+022.19E+02 1.02 Acceptable EZA EZA 2nd/2014 2nd/2014 08/08/14 08/08/14 E10897 E10898 Cartridue Milk pCipCilL lodine-131 89 8.73E+01 9.84E+01 8.54E+01 9.13E+01 1.02 1.08 Acceptable

Acceptable EZA2nd/201408/08/14 E10898 MilkpCilL901.44E+011.45E+010.99 Acceptable EZA 2nd/2014 08/08/14 E10899 Milk ccu,lodine-1319.89E+019.09E+01 1.09 Acceptable EZA EZA 2nd/2014 2nd/2014 08/08/14 08/08/14 E10899 E10899 Milk Milk.pCi/L ccu.Cerium-14151 1.38E+02 2.68E+02 1.24E+02 2.53E+02 1.12 1.06 Acceptable Acceptable EZA2nd/201408/08/14 E10899 Milk ocu, Cesium-1341.58E+021.62E+02 0.97 Acceptable EZA 2nd/2014 08/08/14 E10899 Milk pCi/L Cesium-1371.27E+021.20E+02 1.06 Acceptable EZA 2nd/2014 08/08/14 E10899 Milk pCi/L Cobalt-58 1.20E+02 1.12E+02 1.07 Acceptable EZA2nd/201408/08/14 E10899MilkpCi/L 54 1.67E+02 1.56E+02 1.07 Acceptable EZA2nd/201408/08/14E10899MilkpCi/L Iron-591.02E+021.02E+02 1.00 Acceptable EZA 2nd/2014 08/08/14 E10899MilkpCi/L Zinc-65 2.68E+02 2.52E+02 1.06 Acceptable EZA 2nd/2014 08/08/14 E10899 Milk ecu.Cobalt-602.42E+022.24E+02 1.08 Acceptable EZA2nd/201408/08/14 E10900 Water pCi/L lodine-131 1.13E+029.83E+011.15 Acceptable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage30of64 EZA2nd/201408/08/14E10900Water3.62E+022.94E+021.23AccetableEZA2nd/201408/08/14E10900Water Cesium-1341.69E+021.88E+020.90Accetable EZA 2nd/201408/08/14E10900Water Cesium-1371.48E+021.39E+021.06AccetableEZA2nd/201408/08/14E10900WaterCobalt-581.34E+021.30E+021.03Accetable Manganese-EZA2nd/201408/08/14E10900Water541.88E+021.80E+021.04AccetableEZA2nd/201408/08/14E10900Iron-591.29E+021.19E+021.09AccetableEZA2nd/201408/08/14E10900Zinc-653.29E+02 2.93E+021.12Accetable EZA2nd/201408/08/14 E10900Cobalt-602.74E+022.60E+021.05AccetableEZA3rd/201411/22/14E10993lodine-1319.47E+018.99E+011.05Accetable Strontium-EZA3rd/2014 11/22/14 E10994 Milk 899.73E+019.69E+011.00Accetable Strontium-EZA3rd/201411/22/14E10994Milk901.31E+011.64E+010.80Accetable EZA3rd/201411/22/14E10995Milklodine-1311.04E+029.76E+011.07Accetable EZA3rd/201411/22/14E10995MilkCerium-1411.28E+021.26E+021.01Accetable Chromium-EZA3rd/201411/22/14E10995Milk513.12E+022.88E+021.08AccetableEZA3rd/2014 11/22/14 E10995 Milk Cesium-1341.51E+021.58E+020.96Accetable EZA3rd/201411/22/14E10995Milk Cesium-1372.03E+021.93E+021.05Accetable EZA3rd/201411/22/14E10995Milk Cobalt-581.44E+021.43E+021.01Accetable Manganese-EZA3rd/201411/22/14E10995 Milk541.49E+021.42E+021.05Accetable EZA3rd/201411/22/14E10995 MilkIron-591.82E+021.58E+021.15Accetable EZA3rd/201411/22/14E10995MilkZinc-657.41E+017.30E+011.01Accetable EZA3rd/201411/22/14E10995 MilkCobalt-603.14E+022.94E+021.06Accetable EZA3rd/201411/22/14E10996Waterlodine-1311.02E+02 9.88E+01 10'3Accetable EZA3rd/201411/22/14E10996 WaterCerium-1411.30E+021.25E+02 104Accetable Chromium-EZA3rd/201411/22/14E10996Water 512.75E+022.86E+020.96Accetable EZA3rd/201411/22/14E10996Water Cesium-1341.45E+021.56E+020.93Accetable EZA 3rd/201411/22/14E10996Water Cesium-1371.94E+021.92E+02 1.01Accetable EZA3rd/201411/22/14E10996WaterCobalt-581.43E+021.42E+021.01Accetable Manganese-EZA3rd/201411/22/14E10996Water541.46E+021.41E+021.04Accetable EZA3rd/201411/22/14E10996WaterIron-591.66E+021.57E+021.06Accetable EZA3rd/201411/22/14E10996 WaterZinc-657.55E+017.24E+011.04Accetable EZA 3rd/201411/22/14E10996WaterCobalt-603.09E+022.95E+021.05Accetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage31of64 TABLE 3 2014 DEPARTMENTOFENERGYMIXED ANALYTE PERFORMANCE EVALUATION PROGRAM (MAPEP)RESULTS MAPEP-14-MAPEP2nd/201406/05/14 GrF30 MAPEP-14-MAPEP2nd/201406/05/14 GrF30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaS30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 i MAPEP-14-MAPEP2nd/201406/05/14 MaW30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 MAPEP-14-MAPEP'2nd/201406/05/14 MaW30 MAPEP-14-MAPEP2nd/201406/05/14 MaW30 Filter Filter Soil Soil Soil Soil Soil Soil Soil Soil Soil.sen'Soil Soil Soil Soil Soil Soil Water Water Water Water Water Water Water Water Water Water B Isam Ie B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B Ik B IL B IL B IL B IL B IL B IL B IL B IL B ILGrossBeta 241 Cesium-134 Cesium-137 Cobalt-57 Cobalt-60 Iron-55 54 Niekel-63 238 239/240 40 90 99 U-234/233238 Zine-65 Am-241 Cesium-134 Cesium-137 Cobalt-57 Cobalt-60 Iron-55 54 Niekel-63 238 1.980 0.823 65 5.44 1270 947 0.581 580 1470 6.95 89.7 69.80 703 1.48 37.1 30.5 35 766 0.759 21.4 29.70 28.0 16.6 308 0.3 14.4 31.4 0.764 1.770.77'68.o 1238 966 1.220)643 1430 o 96.0 76.8 622 o o 81.0 83 695 0.720 23.1 28.9 27.5 16.0 321 0.0 13.9 34.0 0.828 0.53-3.01 0.39-1.16 47.6-88.4FalsePas Test 867-1609 676-1256Sens.Eva!.

444-824 1001-1859FalsePas Test 67-125 53.8-99.8 435-809FalsePas.TestFalsePas Test 57-105 58-108 487-904 0.504-0.936 16.2-30.0 20.2-37.6 19.3-35.8 11.2-20.8 225-417FalsePas Test 9.7-18.1 23.8-44.2 0.580-1.076AeeetableAeeetableAeeetableAeeetableAeeetableAeeetableAeeetableAeeetable Aeeetable AeeetableAeeetableAeeetableAeeetable AeeetableAeeetable Not Aeee 1.Not Aeee 1.AeeetableAeeetableAeeetableAeeetableAeeetable Aeee tableAeeetableAeeetableAeeetableAeeetableAeeetable Laboratories LLCP.O.Box30712,Charleston,SC29417 2014ANNUALQUALITY ASSURANCE REPORTPage32of64

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<um k?'uMeijla, ucllil<<RoU<<'vaua on MAPEP-14-MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L Pu-239/2400.65900.6760 0.473-0.879 Acceptable MAPEP-14-Potassium-FalsePos MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L 40 0.460 0 Test Acceptable MAPEP-14-Strontium-MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L 90 8.32 8.51 5.96-11.06 Acceptable MAPEP-14-Technetium-MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L 999.510.3 7.2-13.4 Acceptable MAPEP-14-MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L U-234/2330.2100.225 0.158-0.293 Acceptable MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L2381.411.45 1.02-1.89 Acceptable MAPEP-14-FalsePos MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L Zinc-65-0.1260.0Test Acceptable MAPEP-14-MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L GrossAlpha0.96 0.85 0.255-1.443 Acceptable MAPEP-14-MAPEP 2nd/2014 06/05/14 MaW30 Water Bo/L Gross Beta4.74.22.10-6.29Acceptable MAPEP-14-FalsePos MAPEP 2nd/2014 06/05/14 MaW30 Water Bq/L lodine-129 0.02270.00Test Acceptable MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14 RdF30 Filter uc/sarnole 235 0.018 0.020 0.014-0.026 Acceptable MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14 RdF30 Filter ug/sample 2388.7710.4 7.3-13.5 Acceptable MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14 RdF30 Filter uo/sarnoleTotal8.80 10.4 7.3-13.5 Acceptable MAPEP-14-Americium-MAPEP 2nd/2014 06/05/14 RdF30 Filter ug/sample2410.0860.090 0.063-0.117 Acceptable MAPEP-14-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sarnole Cesium-134 1.85 1.91 1.34-2.48 Acceptable MAPEP-14-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sample Cesium-1371.811.76 1.23-2.29 Acceptable MAPEP-14-FalsePos MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sample Cobalt-57 0.07570.00Test Acceptable MAPEP-14-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sampte Cobalt-60 1.4901.390.97-1.81 Acceptable MAPEP-14-Manganese-FalsePos MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sample 54 0.01380.00Test Acceptable MAPEP-14-Plutonium-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sample 238 0.000819 0.00090Sens.Eva!.

Acceptable MAPEP-14-0.054-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bu/sarnole Pu-239/240 0.071 0.7720 0.1004 Acceptable MAPEP-14-Strontium-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sarnple 90 1.19 1.18 0.83-1.53 Acceptable MAPEP-14-0.0137-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sample U-234/233 0.0159 0.0195 0.0254 Acceptable MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sample 2380.1180.129 0.090-0.168 Acceptable MAPEP-14-FalsePos MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sarnple Zinc-650.2460.00 Test Acceptable MAPEP-14-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sample Gross Alpha 1.9801.770.53-3.01 Acceptable MAPEP-14-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sarnple GrossBeta0.83 0.77 0.39-1.16 Acceptable MAPEP-14-Americium-MAPEP 2nd/2014 06/05/14 RdF30 Filter Bq/sample 241 0.106 0.104 0.073-0.135 Acceptable MAPEP-14-Uranium-0.0188-Not MAPEP 2nd/2014 06/05/14 RdV30 Vecetatlon uo/sample 235 0.261 0.0268 0.0348 Accept.MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14 RdV30 Vegetation uo/sarnole 23812.713.3 9.3-17.3 Acceptable MAPEP-14-Uranium-MAPEP 2nd/2014 06/05/14 RdV30 Veqetafion ug/sample Total 12.7 13.3 9.3-17.3 Acceptable MAPEP-14-Americium-MAPEP 2nd/2014 06/05/14 RdV30 veoetanon uo/samole 241 0.1100 0.108 0.076-0.140 Acceptable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUALQUALITY ASSURANCE REPORTPage33of641.461.02-1.90Accetable6.934.85-9.01Accetable7.004.38-8.13Accetable4.743.32-6.16Accetable10.17.1-13.1Accetable8.626.03-11.21Accetable6.044.23-7.85Accetable1.0600.53-1.59Accetable0.5300.16-0.09Accetable0.1650.116-0.215Accetable0.1210.085-0.157Accetable 0.108-0.1540.0200Accetable 0.0177-0.25300.0329Accetable 0.433Zinc-658.87 Uranium-2380.174Cobalt-5711.1Cobalt-607.21 Strontium-901.580U-234/2330.2640 Plutonium-2380.116Pu-239/2400.134Cesium-1374.98Cesium-1345.65 Manganese-549.24B/samIeGrossBeta1.060 Filter Filter MAPEP-14-MAPEP4th/201401/09/15GrF31 MAPEP-14-MAPEP4th/201401/09/15GrF31 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/2014 06/05/14 RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP2nd/201406/05/14RdV30 MAPEP-14-MAPEP4th/201401/09/15MaS31 Soil Americium-B/K24188.485.559.9-111.2Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31SoilB/KCesium-134588622435-809Accetable MAPEP-14-MAPEP4th/201401/09/15 MaS31'SoilB/K Cesium-137.

1.67FalsePasTestAccetable MAPEP-14-MAPEP4th/201401/09/15MaS31 SoilB/KCobalt-5711601116781-1451Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31SoilB/KCobalt-60821779545-1013Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31SoilB/KIron-55796680476-884Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31 Soil Manganese-B/K5410601009706-1312Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31SoilB/KNickel-63924980686-1274Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31 Soil Plutonium-B/K2380.920.48Sens.Eva!.Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31 Soil Plutonium-B/K239/24061.558.641.0-76.2Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31 Soil Potassium-B/K40879824577-1071Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31 Soil Strontium-B/K90891858601-1115Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31 Soil Technetium-B/K99466589412-766Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31 SoilB/KU-234/2339058962-116

.Accetable MAPEP-14-.MAPEP4th/201401/09/15MaS31 Soil Uranium-.B/K238257259181-337Accetable MAPEP-14-MAPEP4th/201401/09/15MaS31 SoilB/KZinc-65605.0541379-703Accetable MAPEP-14-MAPEP4th/201401/09/15MaW31 Water Americium-B/L2410.9150.8800.62-1.14Accetable MAPEP-14-MAPEP4th/201401/09/15MaW31WaterB/L.Cesium-134-0.06FalsePasTestAccetable MAPEP-14-MAPEP4th/2014'01/09/15MaW31WaterB/LCesium-13718.418.412.9-23.9Accetable Laboratories LLCP.O.Box30712, Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage34of64 fRiiiJII

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/'/.*.****..**8Y:ea Dat N uri!l:i$r,<Media...ell CRatlo:.,."" uat MAPEP-14-MAPEP 4th1201401/09/15 MaW31 Water Sq/L Cobalt-572524.7 17.3-32.1 Acceptable MAPEP-14-MAPEP 4th1201401/09/15 MaW31 Water Sq/L Cobalt-6012.512.4 8.7-16.1 Acceptable MAPEP-14-MAPEP 4th1201401/09/15 MaW31 Water Sq/L Hvdroaen-3216208 146-270 Acceptable MAPEP-14-MAPEP 4th1201401/09/15 MaW31 Water Sq/L Iron-55 34.0 31.5 22.1-41.0 Acceptable MAPEP-14-Manganese-MAPEP 4th1201401/09/15 MaW31 Water Sq/L 54 14.2 14.0 9.8-18.2 Acceptable MAPEP-14-MAPEP 4th1201401/09/15 MaW31 Water Sq/L Nickel-63 23.6 24.6 17.2-32.0 Acceptable MAPEP-14-Plutonium-MAPEP 4th1201401/09/15 MaW31 Water Sq/L 2380.5470.618 0.433-0.803 Acceptable MAPEP-14-Plutonium-MAPEP 4th1201401/09/15 MaW31 Water Sq/L 239/2400.0150.005Sens.Eva!.

Acceptable MAPEP-14-Potassium-MAPEP 4th1201401/09/15 MaW31 Water Sq/L 40174161 113-209 Acceptable MAPEP-14-Strontium-FalsePas MAPEP 4th 12014 01/09/15 MaW31 Water Sq/L 90 0.03 Test Acceptable MAPEP-14-Technetium-MAPEP 4th 12014 01/09/15 MaW31 Water Sq/L 996.926.99 4.89-9.09 Acceptable MAPEP-14-Uranium-MAPEP 4th1201401/09/15 MaW31 Water Sq/L 234/2330.2060.205 0.144-0.267 Acceptable MAPEP-14-Uranium-MAPEP 4th1201401/09/15 MaW31 Water Sq/L 238 1.280 1.4200.99-1.85Acceptable MAPEP-14-MAPEP 4th1201401/09/15 MaW31 Water Sq/L Zinc-65 11.900 10.90 7.6-14.2 Acceptable MAPEP-14-MAPEP 4th 12014 01/09/15 MaW31 Water Sq/L Gross Alpha 0.793 0.701 0.201-1.192 Acceptable MAPEP-14-MAPEP 4th1201401/09/15 MaW31 Water Sq/L Gross Seta 6.220 5.94 2.97-8.91 Acceptable MAPEP-14-Uranium-0.0278-MAPEP 4th1201401/09/15 RdF31 Filter ug/sample 235 0.040 0.040 0.0516 Acceptable MAPEP-14-Uranium-MAPEP 4th1201401/09/15 RdF31 Filter uq/sample 23819.320.3 14.2-26.4 Acceptable MAPEP-14-Uranium-MAPEP 4th1201401/09/15 RdF31 Filter ug/sample Total 19.00 20.4 14.3-26.5 Acceptable MAPEP-14-Americium-0.0472-MAPEP 4th1201401/09/15 RdF31Filteruq/sarnple 2410.05610.067 0.0876 Acceptable MAPEP-14-MAPEP 4th1201401/09/15 RdF31 Filter Bc/sarnole Cesium-134 0.8640 0.960.67-1.25Acceptable MAPEP-14-MAPEP 4th1201401/09/15 RdF31 Filter Bo/sample Cesium-137 1.190 1.20 0.84-1.56 Acceptable MAPEP-14-MAPEP 4th1201401/09/15 RdF31 Filter Sq/sample Cobalt-57 1.540 1.43 1.00-1.86 Acceptable MAPEP-14-MAPEP 4th1201401/09/15 RdF31 Filter Sq/sample Cobalt-60 1.200 1.10 0.77-1.43 Acceptable MAPEP-14-Manganese-MAPEP 4th 12014 01/09/15 RdF31 Filter Bq/sarnole 54 0.808 0.75 0.53-0.98 Acceptable MAPEP-14-Plutonium-MAPEP 4th1201401/09/15 RdF31 Filter Bq/sarnple 238 0.115 0.107 0.075-0.139 Acceptable MAPEP-14-Plutonium-0.0328-MAPEP 4th1201401/09/15 RdF31 Filter Sq/sample 239/240 0.0480.04680.0608 Acceptable MAPEP-14-Strontium-MAPEP 4th 12014 01/09/15 RdF31 Filter Bq/sarnple 90 0.762 0.70 0.492-0.914 Acceptable MAPEP-14-Uranium-0.0251-MAPEP 4th1201401/09/15 RdF31 Filter Bo/sarnole 234/233 0.037 0.0358 0.0465 Acceptable MAPEP-14-Uranium-MAPEP 4th 12014 01/09/15 RdF31 Filter Sq/sample 238 0.227 0.253 0.177-0.329 Acceptable MAPEP-14-MAPEP 4th 12014 01/09/15 RdF31 Filter Sq/sample Zinc-65 0.779 0.76 0.53-0.99 Acceptable MAPEP-14-Americium-MAPEP 4th1201401/09/15 RdV31 Veoetatlon Bq/sarnole 241 0.226 0.19 0.135-0.251 Acceptable Laboratories LLC P.O.Box 30712, Charleston, SC 294172014ANNUAL QUALITY ASSURANCE REPORT Page 35 of 64 m mer'MAPEP-14-MAPEP4th/201401/09/15 RdV31 Cesium-134 4.750 5.203.64-6.67Accetable MAPEP-14-MAPEP4th/201401/09/15 RdV31 Cesium-137 6.910 6.604.62-8.58Accetable MAPEP-14-FalsePos MAPEP4th/201401/09/15RdV31Cobalt-57-0.0020.00TestAccetable MAPEP-14-FalsePosMAPEP4th/201401/09/15 RdV31 Cobalt-60.0.008 0.00TestAccetable MAPEP-14-Manganese-MAPEP 4th/2014, 01/09/15 RdV31 547.9807.885.52-10.24Accetable MAPEP-14-Plutonium-MAPEP4th/2014 01/09/15 RdV312380.0010.001Sens.Eva!.Accetable MAPEP-14-Plutonium-

.MAPEP4th/201401/09/15 RdV31239/2400.15100.171

0.120-0.222Accetable MAPEP-14-Strontium-MAPEP4th/201401/09/15RdV31902.3302.321.62-3.02Accetable MAPEP-14-Uranium-0.0326-MAPEP4th/201401/09/15 RdV31 234/2330.0460.0470.0606Accetable MAPEP-14-Uranium-MAPEP4th/201401/09/15 RdV312380.3320.3240.227-0.421Accetable MAPEP-14-MAPEP 4th/2014 01109/15 RdV31 Zinc-652.8502.63 1.84-3.42Accetable MAPEP-14-Strontium-MAPEP4th/201401/09/15SrF-31 Filter B/samIe893.623.792.65-4.93Accetable Strontium-MAPEP4th/201401/09/15 SrF-31 Filter B/samIe903.623.792.65-4.93Accetable MAPEP-14-MAPEP4th/201401/09/15XaW-31

.WaterB/L lodine-1294.564.55 3.19-5.92Accetable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage36of64TABLE42014ERAPROGRAM PERFORMANCEEVALUATIONRESULTS tlll1tiJli1iJlltJ l1li*../.1'\..............

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"/.,'."'i*'.....'u,/'.a ,.",Ratio1st 1 RAD-ERA2014 02/24/14 96 WaterpCilL Barium-13380.676.2 63.8-83.8 Acceptable1st 1 RAD-ERA2014 02/24/14 96 Water pCi/L Cesium-13464.766.854.4-73.5Acceptable1st 1 RAD-ERA2014 02/24/14 96 Water pCi/L Cesium-137112.010998.1-122Acceptable1st 1 RAD-ERA2014 02/24/14 96 Water pCi/L Cobalt-6095.088.779.8-99.9 Acceptable1st 1 RAD-ERA2014 02/24/14 96 Water pCi/L Zinc-65200185166-218Acceptable1st 1 RAD-ERA 2014 02/24/14 96 Water pCi/LGrossAlpha34.836.118.6-46.4 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 Water pCi/LGrossBeta19.622.313.5-30.4Acceptable1st 1 RAD-ERA2014 02/24/14 96 Water pCi/LGrossAlpha34.636.118.6-46.4 Acceptable1st 1 RAD-ERA2014 02/24/14 96 WaterpCilL Radium-22616.216.8 12.5-19.2 Acceptable1st 1 RAD-ERA2014 02/24/14 96 Water pCi/L Radium-2284.625.043.01-6.67 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 WaterpCi/LUranium(Nat) 7.397.235.51-8.53 Acceptable1st 1 RAD-Uranium (Nat)ERA 2014 02/24/14 96 Water uq/l, mass11.0010.68.07-12.5 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 WaterpCilL Radium-22615.1016.812.5-19.2 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 Water pCi/L Radium-2284.665.043.01-6.67 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 WaterpCi/LUranium(Nat)7.477.23 5.51-8.53 Acceptable1st 1 RAD-Uranium(Nat)ERA2014 02/24/14 96 Water uq/l, mass11.410.6 8.07-12.5 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 Water ecn,Tritium33203580 3030-3950 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 WaterpCilL Strontium-89 44.144.434.4-51.6 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 Water pCi/L Strontium-9034.230.3 22.1-35.2 Acceptable1st 1 RAD-ERA2014 02/24/14 96 Water pCi/L Strontium-89 38.9 44.4 34.4-51.6 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 Water pCi/L Strontium-9027.130.3 22.1-35.2 Acceptable1st 1 ERA 2014 02/06/14 011014L Water ccu.Strontium-8942.338.7 29.3-45.7 Acceptable1st 1ERA2014 02/06/14 011014L WaterpCilL Strontium-8942.238.7 29.3-45.7 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 WaterpCi/Llodine-13125.2 24.4 20.2-28.9 Acceptable1st 1 RAD-ERA 2014 02/24/14 96 WaterpCi/Llodine-13122.424.420.2-28.9 Acceptable 3rd 1 RAD-ERA 2014 08/25/14 98 Water pCi/L Barium-13367.868.7 57.3-75.6 Acceptable 3rd 1 RAD-ERA 2014 08/25/14 98 WaterpCilL Cesium-1347172.3 59.0-79.5 Acceptable 3rd 1 RAD-ERA 2014 08/25/14 98 Water pCi/L Cesium-137161163 147-181 Acceptable 3rd 1 RAD-ERA 2014 08/25/14 98 Water ocu.Cobalt-60 76.7 75.5 68.0-85.5 Acceptable Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage37of64

..f!1......RAD-ERA2014 08/25/14 98 Water Zine-65928273.8-98.5Aeeetable 3rd 1 RAD-ERA2014 08/25/14 98 WaterGrossAIha45.345.423.6-57.4Aeeetable 3rd 1 RAD-ERA 2014 08/25/14 98 WaterGrossBeta32.333.421.7-41.1Aeeetable 3rd 1 RAD-ERA2014 08/25/14 98 WaterGrossAIha48.645.423.6-57.4Aeeetable 3rd 1 RAD-ERA 2014 08/25/14 98 Water Radium-226 8.26 9.066.80-10.6Aeeetable 3rd 1 RAD-ERA 2014 08/25/1498WaterRadium-2268.549.066.80-10.6Aeeetable 3rd 1 RAD-ERA2014 08/25/14 98 WaterRadium-2269.79.06 6.80-10.6'Aeeetable 3rd 1 RAD-ERA 2014 08/25/1498WaterRadium-2285.075.073.03-6.79Aeeetable 3rd 1 RAD-ERA2014 08/25/1498WaterRadium-2285.745.073.03-6.79Aeeetable 3rd 1 RAD-ERA 2014 08/25/1498WaterUraniumNat13.913.510.7-15.4Aeeetable 3rd 1 RAD-Uranium(Nat)ERA2014 08/25/14 98 Watermass22.2519.815.6-22.6Aeeetable 3rd 1 RAD-ERA 2014 08/25/14 98 WaterUraniumNat1313.510.7-15.4Aeeetable 3rd 1 RAD-Uranium(Nat)

ERA 2014 08/25/14 98 Water mass20.719.815.6-22.6Aeeetable 3rd 1 RAD-ERA 2014 08/25/14 98 WaterTritium1020011200 9750-12300Aeeetable 3rd 1 RAD-ERA 2014 08/25/1498WaterTritium10400112009750-12300Aeeetable 3rd 1 RAD-NotERA2014 08/25/1498WaterStrontium-8956.3 42.732.9-49.8Aeeetable 3rd 1 RAD-ERA 2014 08/25/1498WaterStrontium-9014.331.723.1-36.7Aeeetable 3rd 1 RAD-Not ERA 2014 08/25/1498WaterStrontium-8956.542.732.9-49.8Aeeetable 3rd 1 RAD-ERA 2014 08/25/14 98/WaterStrontium-902631.723.1-36.7Aeeetable 3rd 1 RAD-ERA2014 08/25/1498Water lodine-13128.626.121.7-30.8Aeeetable 3rd 1 RAD-ERA2014 08/25/14 98 Water lodine-13122.326.121.7-30.8Aeeetable Laboratories LLCP.O.Box30712, Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage38of64TABLE52014ERA PROGRAM (MRAD)PERFORMANCE EVALUATION RESULTS ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Ci/k Ci/k Ci/k Ci/k Cilk Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k u/k Ci/k Ci/k Ci/k u/k Ci/k Ci/k Ci/k u/k Actinium-228 Americium-241 Bismuth-212 Bismuth-214 Cesium-134 Cesium-137 Cobalt-60 Lead-212 Lead-214 Plutonium-238 Plutonium-239 Potassium-40 Strontium-90 Thorium-234 Zinc-65 Strontium-90 Uranium-234

Uranium-238Uranium-Total Uranium-Total mass Uranium-234 Uranium-238Uranium-Total Uranium-Total mass Uranium-234 Uranium-238Uranium-Total Uranium-Total mass11401240795-1720Accetable418399233-518Accetable9761240330-1820Accetable229019601180-2820Accetable308033902220-4070Accetable 6510-8310849010900Accetable657068304620-9400Accetable13301240812-1730Accetable280020701210-3090Accetable<44.3<10000-1000Accetable579578348-797Accetable488471.00308-651Accetable 7660-105001050014100Accetable250027801060-4390Accetable342033601060-6320Accetable570054004300-7180Accetable 3250-6730853013500Accetable260233902070-4350Accetable242533602080-4260Accetable502769103750-9120Accetable 5570-71101010012700Accetable344033902070-4350Accetable368033602080-4260Accetable731069103750-9120Accetable 5570-110001010012700Accetable374033902070-4350Accetable 378033602080-4260Accetable768369103750-9120Accetable 5570-113001010012700Accetable Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage39of64Aeeetable23.3-49.9Aeeetable0.00-300Aeeetable35.2-63.5Aeeetable663-1290Aeeetable 23000-44800Aeeetable22.6-54Aeeetable911-1980Aeeetable253-804Aeeetable639-1290Aeeetable643-1250Aeeetable36.8-80.8Aeeetable38.6-118Aeeetable867-1400Aeeetable415-839Aeeetable38.6-74.0Aeeetable638-1220Aeeetable0-50.0Aeee table74.4-469Aeeetable622-1090Aeeetable3510-6650Aeeetable3510-6650Aeeetable1160-2260Aeeetable2430-4460Aeeetable1170-2220Aeeetable3510-6650Aeeetable1170-2220Aeeetable2430-4460Aeeetable1160-2260Aeeetable1470-3420Aeeetable2300-5150Aeeetable1260-2890Aeeetable51.356.347.548.634.536.176.778.933.836.425424059905240861880381735809979269201010113011205145165620524081682860.259.76576461030919592052401730176020001750192017602330258019701750402535803810374022302110<6.64<50.016701490<62.2<30030800319001120010100 Cesium-134 Cesium-137 Cesium-134 Am-241 Iron-55 Uranium-234 Strontium-90 Potassium-40 Uranium-238 Cesium-137 Cobalt-60 Uranium-234 Strontium-90 Zine-65 Uranium-238 Uranium-234 Cobalt-60 Uranium-238Uranium-Total Plutonium-239 Plutonium-238Uranium-Total Plutonium-239 Plutonium-238Mananese-54 Amerieium-241 Uranium-Total mass Uranium-Total mass Uranium-Total mass Uranium-Total mass u/k Soil Filter Filter Filter Filter Filter Filter Filter Filter Filter Filter Filter MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 MRAD-2nd/201405/16/1420 am'Ufub2nd/201405/16/1420 ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA Laboratories LLCP.O.Box30712, Charleston,SC294172014ANNUALQUALITYASSURANCE REPORTPage40of64 1.***

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ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA e: ir 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 MRAD-05/16/1420Filteruq/Filter Uranium-Total(mass\

MRAD-05/16/1420FilterpCi/FilterZinc-65 MRAD-05/16/1420FilterpCi/FilterUranium-234 MRAD-05/16/1420FilterpCi/FilterUranium-238 MRAD-05/16/1420FilterpCi/FilterUranium-Total MRAD-05/16/1420FilteruQ/Filter Uranlum-Totattmass)

MRAD-05/16/1420Filterug/Filter Uranium-Total(mass)

MRAD-05/16/1420FilterpCi/FilterGrossAlpha MRAD-05/16/1420FilterpCi/FilterGrossBeta MRAD-05/16/1420WaterpCi/LAmericium-241 MRAD-05/16/1420 Water ecu.Cesium-134 MRAD-05/16/1420WaterpCi/LCesium-137 MRAD-05/16/1420WaterpCi/LCobalt-60 MRAD-05/16/1420WaterpCi/L Iron-55 MRAD-05/16/1420WaterpCilLManQanese-54 MRAD-05/16/1420WaterpCi/LPlutonium-238 MRAD-05/16/1420WaterpCi/LPlutonium-239 MRAD-05/16/1420WaterpCi/LStrontium-90 MRAD-05/16/1420WaterpCi/LUranium-234 MRAD-05/16/1420WaterpCi/LUranium-238 MRAD-05/16/1420WaterpCilLUranium-Total MRAD-05/16/1420WateruQ/L Uranium-Total(mass)

MRAD-05/16/1420WaterpCi/L Zinc-65 MRAD-05/16/1420WaterpCi/LUranium-234 MRAD-05/16/1420WaterpCi/LUranium-238 MRAD-05/16/1420WaterpCi/LUranium-Total MRAD-05/16/1420Waterug/L Uranium-Totaumass)

MRAD-05/16/1420WaterpCi/LUranium-234 MRAD-05/16/1420WaterpCi/LUranium-238 MRAD-05/16/1420WaterpCi/LUranium-Total MRAD-05/16/1420WateruQ/L Uranium-Total(mass) 70.3 104 737 35.5 35.3 72.4 105 100 60.9 58.9 186 1540 2760 1320 1230<7.54 37 124 95 77.8 50.8 156 233 2030 82.1 84.6 170 253 80.5 90.0 175 269.i...74.3 108 667 36.4 36.1 74.3 108 108 46 53.8 114 1660 2690 1270 1200<100 44 160 890 82.4 48.4 168 245 1800 82.4 48.4 168 245 82.4 48.4 168 24569.1-152Acceptable478-921Acceptable22.6-54Acceptable23.3-49.9Acceptable41.1-113Acceptable69.1-152Acceptable69.1-152Acceptable15.4-71.4Acceptable34.0-78.4Acceptable Not76.8-153Acceptable1220-1910Acceptable2280-3220Acceptable1100-1490Acceptable716-1630Acceptable0.00-100Acceptable32.6-54.9Acceptable124-202Acceptable580-1180Acceptable61.9-106Acceptable36.9-59.4Acceptable123-217Acceptable195-296Acceptable1500-2270Acceptable61.9-106Acceptable36.9-59.4Acceptable123-217Acceptable195-296Acceptable61.9-106Acceptable36.9-59.4Acceptable123-217Acceptable195-296Acceptable Laboratories Ll_C P.O.Box 30712, Charleston, SC 294172014ANNUAL QUALITY ASSURANCE REPORT Page 41 of 64 ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA ERA 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 2nd/2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 m N4,OO""Q MRAD-05/16/1420 MRAD-05/16/1420 MRAD-05/16/1420 MRAD-05/16/1420 MRAD-05/16/1420 MRAD-'05/16/1420 MRAD-05/16/1420 MRAD-05/16/1420 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRADJ11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 Water Water Water'Water Water Water Water Water Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Ci/l Ci/l Ci/l u Il u Il Ci/l Cill Ci/l Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Cilk Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k Ci/k u IkUranium-23477.882.461.9-106AeeetableUranium-23878.348.436.9-59.4AeeetableUranium-Total156168123-217AeeetableUranium-Totalmass233245195-296AeeetableUranium-Totalmass232245195-296AeeetableGrossAIha141.013347.2-206AeeetableGrossBeta172174.099.6-258AeeetableTritium528055803740-7960AeeetableAetinium-22812801240795-1720AeeetableAmerieium-241825763431-956AeeetableBismuth-21216201240330-1820AeeetableBismuth-214290028101690-4040AeeetableCesium-13419602140.1400-2570AeeetableCesium-137676065505020-8430AeeetableCobalt-60448042602880-5860Aeeetable lead-21212601240812-1730Aeeetable lead-214348027501610-4100Aeeetable<30.0<10000-1000AeeetablePlutonium-238732739444-1020AeeetablePlutonium-239281309202-427Aeeetable 7810-Potassium-40115001070014400Aeeetable 3210-Strontium-908790842013300AeeetableThorium-23420002350743-4420AeeetableZine-65391032702600-4350AeeetableUranium-234228023701450-3040AeeetableUranium-238234023501450-2980AeeetableUranium-Total476245402360-6390AeeetableUranium-Totalmass702070503890-8870Aeeetable ERA ERA ERA ERA 3rd I 2014 3rd I 2014 3rd I 2014 3rd I 2014 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421 MRAD-11/25/1421Am-241226022901400-3505AeeetableCesium-134837849545-1100AeeetableCesium-137729644467-896AeeetableCobalt-60818784541-1100Aeeetable Laboratories LLCP.O.Box30712, Charleston,SC294172014ANNUALQUALITY ASSURANCE REPORTPage42of64..liliilill",.."'i'<,........".......,......MRAD-ERA2014 11/25/14 21 Vegetation pCi/kg Curium-244 361 367 180-572 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Veqetation pCi/kq Manqanese-54<25.3<300 0-300 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Veqetation pCi/kg Plutonium-238886862 514-1180 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Veqetatlon pCi/kg Plutonium-239675701 430-965 Acceptable 3rd 1 MRAD-22300-ERA2014 11/25/14 21 Vegetation pCi/kq Potassium-403530030900 43400 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Veqetation pCi/kg Strontium-90 1230 1710 975-2270 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Veqetation pCi/kq Uranium-23419801780 1170-2290 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Veaetatlon pCi/kg Uranium-238 1970 1760 1170-2240 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Veqetation pCi/kq Uranium-Total40383620 2450-4510 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Veaetation ug/kgUranium-Total(mass)59105280 3540-6710 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Veqetation pCi/kq Uranium-23416701780 1170-2290 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Vegetation pCi/kg Uranium-23818001760 1170-2240 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Vegetation pCi/kg Uranium-Total35563620 2450-4510 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Veoetation ug/kg Uranium-Total/mass)53905280 3540-6710 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Vegetation uq/kqUranium-Total(mass) 5860 5280 3540-6710 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Venetatlon pCi/kq Zinc-6519301570 1130-2200 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Filter pCi/Filter Americium-24141.438.6 23.8-52.2 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Cesium-134 742 765.0 487-949 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Cesium-137677647 486-850 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Cobalt-60543523 405-653 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Iron-55117120.037.2-234 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Filter pCi/Filter Manganese-54<5.87<50 0.00-50.0 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter uq/Filter Plutonium-238 32.9 35.7 24.5-46.9 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Filter pCi/Filter Plutonium-23926.829.1 21.1-38.0 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Strontium-90187168 82.1-252 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Uranium-234 26 28 27.8-41.9 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Filter pCi/Filter Uranium-2382827.60 17.8-38.2 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Uranium-Total 56 57 31.4-86.3 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter uq/Filter Uranium-Total/mass) 82.6 82.7 52.9-116 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Zinc-65629547 392-755 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Uranium-2342828 27.8-41.9 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/Filter Uranium-238 25 27.60 17.8-38.2 Acceptable Laboratories LLCP.O;Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORT Page43of64 1:81'."'<

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" ,;.;.': "",'I':,',".>:.'.'."'.'.1 IRAD-.:')':,":)"".,)/),..,..ERA2014 11/25/14 21 Filter pCi/Filter Uranium-Total 55 57 31.4-86.3 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter uq/Filter Uraniurn-Totaltrnass)75.182.7 52.9-116 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21FilteruQ/Filter Uranium-Tolal(mass)90.782.7 52.9-116 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Filter pCi/FilterGrossAlpha47.436.9 12.4-57.3 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Filter pCi/FilterGrossBeta27.2 21.1 13.3-30.8 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Water pCi/L Americium-24172.468.646.2-92.0Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water cc ilL Cesium-134816.0850 624-977 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water"pCilL Cesium-13713101240 1060-1490 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCi/L Cobalt-6011301070 930-1250 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCi/L Iron-55130134 79.9-182 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Water ec ilL Manqanese-se<6.34<100 0.00-100 Acceptable 3rd 1 11/25/14 MRAD-ERA 2014 21 WaterpCilL PILitonium-2383533 24.6-41.4 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCi/L Plutonium-23946.451 39.7-64.4 Acceptable 3rd 1 MRAD-ERA*2014 11/25/14 21 WaterpCilL Strontium-90 300 254 165-336 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water ec ilL Uranium-2344244 32.9-56.5 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 WaterpCilL Uranium-238 50 43.50 33.2-53.4 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCi/L Uraniurn-Total 92 89 65.5-115 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water ug/L Uranium-Tolal(mass)137130 104-157 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Water pCi/L Zinc-65 1070 921 768-1160 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water ec ilL Uranium-2344344 32.9-56.5 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCi/L Uranium-238 45 43.50 33.2-53.4 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCi/L Uranium-Total 90 89 65.5-115 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Water ug/L Uranium-Tolal(mass) 134 130 104-157 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 WaterpCilL Uranium-234 49 44 32.9-56.5 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 WaterpCilL Uranium-2384243.50 33.2-53.4 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCi/L Uranium-Total9389 65.5-115 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Water ug/L Uranium-Tolal(mass) 126 130 104-157 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Water uQ/L Uraniurn-Totaurnass) 144 130 104-157 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCi/LGrossAlpha 96.2 98 34.8-152 Acceptable 3rd 1 MRAD-ERA2014 11/25/14 21 Water pCilLGrossBeta86.177.5 44.4-115 Acceptable 3rd 1 MRAD-ERA 2014 11/25/14 21 Water pCilL Tritium 5490 5500 Acceptable Laboratories LLCP.O.Box30712, Charleston,SC294172014ANNUALQUALITYASSURANCEREPORTFIGURE1Page44of64 COBAlT-60 PERFORMANCE EVALUATION RESULTS AND%BIAS 2014 Cobalt-60 Perfonnance Evaluation Results and%Bias 100.0 75.0 50.0 25.0 U)ns iii 0.00-25.0-50.0-75.0-100.0----Co-60----LowerControl Limit----UpperControl Limit January 2014*December 2014 Laboratories LLCP.O.Box30712, Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTFIGURE2Page45of64 CESIUM-137 PERFORMANCE EVALUATIONRESULTSAND

%BIAS 2014 Cesium-137 Performance Evaluation Results and%Bias 100.0 75.0 50.0 25.0 t/)ns in 0.0-25.0-50.0-75.0-100.0----Cs-137----LowerControl Limit----UpperControl Limit January 2014-December 2014 Laboratories LLCP.O.Box30712, Charleston,SC294172014ANNUALQUALITYASSURANCEREPORTFIGURE3Page46of64 TRITIUM PERFORMANCE EVALUATIONRESULTSAND

%BIAS 2014 Tritium Performance' Evaluation Results and%Bias 100.0 75.0 50.0 25.0 t/)cu iii 0.00-25.0-50.0-75.0-100.0--H-3----LowerControl Limit----UpperControl Limit January 2014-December 2014 Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTFIGURE4Page47of64 STRONTIUM-gO PERFORMANCE EVALUATION RESULTS AND%BIAS 2014 Strontium-gO Performance Evaluation Results and%Bias 100.0 50.0 II)ns iii 0.0-50.0-100.0 January 2014-December 2014--Stronuurn-sn----Lower Control Limit----Upper Control Limit Laboratories LLCP.O.Box30712, Charleston,SC294172014ANNUALQUALITYASSURANCEREPORTFIGURE5Page48of64 GROSS ALPHA PERFORMANCE EVALUATIONRESULTSAND

%BIAS 2014 Gross Alpha Performance Evaluation Results and%Bias 100.0-==========

50.0 UJ cu iii 0.0-50.0-100.0-=======January 2014-December 2014-----GrossAlpha----Lower Control Limit----UpperControl Limit Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUALQUALITYASSURANCEREPORT FIGURE 6Page49of64 GROSS BETA PERFORMANCE EVALUATION RESULTS AND%BIAS2014GrossBeta Performance EvaluationResultsand%Bias 100.0 50.0 tnIJl 0.0'*'-50.0 January 2014-December 2014-----GrossBeta:..----Lower Control Limit----Upper Control Limit Laboratories LLCP.O.Box30712, Charleston,SC294172014ANNUALQUALITYASSURANCEREPORT FIGURE 7Page50of64 IODINE-131 PERFORMANCE EVALUATION RESULTS AND%BIAS 20141odine-131 Performance EvaluationResultsand

%Bias 100.0 75.0 50.0 25.0 en co iii 0.00-25.0-50.0-75.0-100.0--lodine-131----LowerControl Limit----Upper Control Limit January 2014-December 2014

/Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUALQUALITYASSURANCEREPORT FIGURE 8Page51of64 AMERICIUM-241 PERFORMANCE EVALUATION RESULTS AND%BIAS 2014 Americium-241 Performance Evaluation Resultsand%Bias 100.0 75.0 50.0 25.0 fn ns iii 0.00*-25.0-50.0-75.0-100.0--Am-241----LowerControl Limit----Upper Control Limit January 2014-December 2014 Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTFIGURE9Page52of64 PLUTONIUM-238 PERFORMANCE EVALUATIONRESULTSAND

%BIAS 2014 Plutonium-238 Performance Evaluation Results and%Bias 100.0 75.0 50.0 25.0 III nl iii 0.0-25.0-50.0-75.0-100.0----Plutonium-238----Lower Control Limit----Upper Control Limit January 2014-December 2014 Laboratories LLC P.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage53of64 TABLE 6 REMP INTRA-LABORATORY DATA

SUMMARY

BIASAND PRECISION BY MATRIX o o o o o o o 5 7 5 3 3 8 43 5 2 6 5 3 3 30 1 0 2 0 206 0 205 0 1 0 1 0 12 0 12 0 13 0 13 0 4 0 4 0 6 0 6 0 28 0 28 0 10 0 10 0 15 0 15 0 8 0 8 0 30 0 31 0 45 0 45 0 84 0 159 0GrossA&B GammaSec FilterLSCNickel63,AIhaSec UraniumGasFlow Sr-90 PlutoniumAIhaSec Am243 GammaSec LiuidRAD A-013 withBaLa LSC Iron-55 Gamma Iodine-131 GammaSec Li uid'RAD A-013GasFlow Total StrontiumAIhaSec PlutoniumGrossAIhaNonVolBetaGasFlowSr2nd countAIhaSec Am241 Curium Tritium REMP 2014GasFlowSr2nd countLSCNickel63GasFlow Total Strontium GammaSec Solid RAD A-013'withBaLa GammaSecSolidRAD A-Ot3GasFlow Total Strontium GammaSec Li LSC Iron-55GasFlowSr2nd count GammaSecSolidRAD A-013 with IodineGasFlowSr2nd Count Gamma S TISSQE:;;:;:!

GammaSec Solid RAD A-013GasFlowSr2nd countGasFlow Total Strontium Gamma S ecSolidRAD A-013 withBaLa Laboratories LLCP.o.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage54of64 a 22 LSC Iron-55 5 a 6 a LSC Nickel 63 5 a 6 aGasFlow Total Strontium 6 a 6 a GrossAIhaNonVolBeta 6 a 6 a aGasFlowSr2nd count GammaSec Solid RAO A-013 with Iodine Gamma Iodine 131 RAO A-013 560 0 Carbon-14 (AscaritejSoda Lime Filter per Liter Tritium 39 0 40 a LSC Iron-55 17 0 16 0 LSC Nickel 63 16 a 15 0 Gamma Iodine-131 27 0 26 0GasFlowSr2nd count 12 0 12 0GasFlow Total Strontium 19 0 18 0GrossAIhaNonVolBeta 72 0 73 0 0 GammaSecLiuidRAO A-013 withBaLa35 0 75 Total 2200 2456Note1:TheRPOmustbe20percentorless,ifbothsamplesaregreaterthan5timestheMOC.Ifbothresultsarelessthan5timesMOC,thentheRPOmustbeequaltoorlessthan100%.IfoneresultisabovetheMOCandtheotherisbelowtheMOC,thentheRPOcanbecalculatedusingtheMOCfortheresultoftheonebelowtheMOC.TheRPOmustbe100%orless.InthesituationwherebothresultsareabovetheMOCbutoneresultisgreaterthan5timestheMOCandtheotherislessthan5timestheMOC,theRPOmustbelessthanorequalto20%.IfbothresultsarebelowMOC,thenthelimitson%RPOarenotalicable.

Laboratories LLC P.O.Box 30712,Charleston,SC 294172014ANNUAL QUALITY ASSURANCE REPORTPage55 of 64TABLE7 ALL RADIOLOGICAL INTRA-lABORATORYDATA

SUMMARY

BIASAND PRECISIONBYMATRIX: , MXt.Gamma Iodine-129 Gamma Iodine-131GasFlowSr2nd countGasFlow Strontium 90GasFlow Total'Strontium GammaSec LiuidRAD A-013 withBaLa o 36 36 5 23 48 o o o o o o 1 110 36 5 23 109 o o o o o o GammaSec LiuidRAD A-013 with Iodine**SQL:IP Gamma Percent LeachGasFlow Radium 228 3 5 16 o o o 4 o 20 o o o Tritium Tritium b Combustion Carbon-14 211 1 130 o o o 247 1 181 o o o LSC Iron-55AIhaSec Polonium Solid Gamma Nickel59RAD A-022 LSC Chlorine-Se in Solids GammaSecRa226RAD A-013 103 52 99 4 21 o o o o o 121 54 117 4 24 o o o o o GammaSecSolidRAD A-013 649 o 812 o LSC Nickel 63 LSC Plutonium Technetium-99 GammaSec LiuidRAD A-013 ICP-MS Technetium-99inSoil LSC Selenium 79 Total Activit TritiumAIhaSec Am243 Gamma Iodine-129 141 181 224 2 61 11 4 16 23 100 o o o o o o o o o o 154 202 250 2 60 11 4 17 37 120 o o o o o o o o o o o o o o o o o o o o o o 6 10 13 2 47 61 61 206 237 240 196 309 o o o o o o o o o o o o 7 2 6 9 42 62 49 213 214 231 158 152 ICP-MS Technetium-99PreinSoilAIhaSecNe tuniumLSCRaid Strontium89and90 LSC Promethium 147AIhaSec UraniumGasFlowLead210AIhaSec Plutonium ICP-MS Uranium-233 234inSolidAIhaSec PlutoniumAIhaSec Thorium GammaSecSolid withRa226Ra228 Total Uranium KPA Laboratories LLCP.O.Box30712,Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORT Page 56 of 64GasFlowSr2nd count 21 0 25 0GasFlow Strontium 90 195 0 201 0GasFlow Total Radium 2 0 3 0LucasCell Radium 226 38 0 47 0 Total Activity Screen 9 0 10 0AlphaSpec Am241 Curium 304 0 339 0AlphaSpec Total Uranium 4 0 8 0GasFlow Total Strontium 43 0 46 0GrossAlphaNonVolBeta 1 0 1 0 ICP-MS Uranium-233, 234PrepinSolid 49 0 48 0 ICP-MS Uranium-235, 236, 238inSolid 60 0 81 0 GammaSpecSolidRAD A-013 withBaLa 2 0 8 0 GammaSpecSolidRAD A-013 with Iodine 6 0 7 0 GFC Chlorine-36 in Solids 3 0 3 0 GammaSpecSolidRAD A-013 (pCi/Sample) 2 0 2 0 Tritium 8 0 8 0AlphaSpec Am241 (pCi/Sample) 2 0 2 0 ICP-MS Uranium-234235,236, 238inSolid 148 0 132 0 ICP-MS Uranium-235 236,238PrepinSolid 50 0 49 0AlphaSpec Thorium 1 0 1 0AlphaSpec Uranium 1 0 1 0 Gross Alpha/Beta 235 0 316 3AlphaSpec Neptunium 1 0 1 0GasFlowSr2nd count 2 0 1 0 Gross Alpha/Beta (Americium Calibration)

Solid 2 0 3 0 ICP-MS Uranium-234 235 236, 238PrepinSolid 69 0 65 0".*',.,,,,,,,.,.,,.,,*.**,*,,,',i::..::..?,'*,.i*e::..*"<ii,":*:i"".',i:*."',",."""",,<,",., i"""iiiAlphaSpec Uranium 14 0 18 0AlphaSpec Polonium 1 0 5 0 Gamma 1-131 filter 4 0 4 0 LSC Plutonium Filter 84 0 102 0 Tritium 76 0 112 0 Carbon-14 35 0 66 0 Nickel-63 0 0 8 0 LSC Iron-55 69 0 84 0 Gamma Nickel59RAD A-022 55 0 68 0LSCNickel63 60 0 78 0 Technetium-99 51 0 75 0 Gamma Spec Filter RAD A-013 143 0 174 6 Alohaspec Np Filter per Liter 8 0 13 0 Alphaspec Pu Filter per Liter 11 0 22 0 Gamma lodine-125 5 0 0 0 Gamma lodine-129 46 0 60 0 Gross Alpha/Beta 5 0 5 0AlphaSpec Am243 10 0 28 0GasFlowLead210 0 0 4 0 LSC Plutonium Filter per Liter 9 0 15 0 Total Uranium KPA 9 0 14 0 Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage57 of 64*AlphaSpec Uranium 55 a 96 a LSC Promethium 147 1 a 2 aLSC,Rapid Strontium89and9a 72 a 94 aAlphaSpec Thorium 42 a 66 aGasFlowRadium228 1 a 1 aAlphaSpec Plutonium 81 a 98 a ICP-MS Uranium-233,234in Filter a a 3 aAlphaSpec Neptunium 62 a 83 aAlphaSpec Plutonium 66'a 96 aAlphaSpec Polonium,(Filter/Liter) a a 14 aAlphaSpecRadium226 a a 2 a GasFlowSr2nd Count 72 a 81 1GasFlow Strontium so 61 a 68 aLucasCell Radium-226 1 a 1 aAlphaSpec Am241Curium 95 a 117 aGasFlow Total Strontium 5 a 5 a ICP-MS Uranium-233, 234Prepin Filter a a 3 a ICP-MS Uranium-235, 236,238in Filter a a 6 a Total Activity in Filter 1 a la a Alphaspec Am241 Curium Filter per Liter 15 a.2a a Tritium 86 a 89 a Gamma Spec Filter RAD A-a13 Direct Count 6 a 6 a Carbon-14 12 a 12 a GFC Chlorine-36 in Filters PL 1 a 1 a Direct Count-Gross Alpha/Beta 48 a 1 a Gross Alpha/Beta 48 a 6a a ICP-MS Uranium-234235236,238in Filter 4 a 6 a ICP-MS Uranium-235236238Prepin Filter a a 3 aAlphaSpecU 13 a 35 aGrossA&B 497 a 473 a LSC Iron-55 8 a 19 a Technetium-99 7 a 13 aGasFlow s--so 6 a 13 aLSCNickel63 14 a 19 aGasFlow Pb-21a 8 a 22 aGasFlow Ra-228 5 a la a Gamma Iodine 129 8 a 8 a ICP-MS Uranium-234 235,236238Prepin Filter 2 a 3 a Gamma Spec Filter 97 a 117 aLucasCell Ra-226 8 a 23 aAlphaSpec Thorium 7 a 22 a:8:0IJio.;::.;AlphaSpec Uranium 39a a 553 aAlphaSpec Polonium 4 a 7 a Electrolytic Tritium 14 a 25 a Tritium 1125 a 1177 a Carbon-14 149 a 161 a Laboratories LLC P.O.Box30712,Charleston,SC294172014ANNUALQUALITYASSURANCE REPORTPage58of64 Plutonium 43 0 63 0 Iodine-131 3 0 4 0 LSC Iron-55 192 0 233 0 GammaNickel59RAD A-022 18 0 21 0 Gamma Iodine131RAD A-013 2 0 2 0 Gamma Radium 228 RAD A-013 3 0 3 0LSCNickel63 209 0 236 0LSCRadon222 18 0 21 0 Technetium-99 377 0 425 0 Gamma Spec Liquid RAD A-013 702 0 732 0AlphaSpec TotalURAD A-Oll 31 0 56 0 LSC Selenium 79 2 0 2 0AlphaSpec Am243 17 0 18 0 Gamma Iodine-129 80 0 92 0 Gamma Iodine-131 28 0 28 0 ICP-MS Technetium-99 in Water 8 0 31 0GasFlowLead210 19 0 19 0 Total Uranium KPA 101 0 203 0 LSC Promethium 147 4 0 4 0LSCRapid Strontium89and90 7 0 8 0AlphaSpec Thorium 145 0 186 0GasFlow Radium 228 171 0 206 0GasFlow Radium 228 40 0 37 0GasFlow Radium 228 1 0 1 0AlphaSpec Plutonium 288 0 387 0 LSC Sulfur 35 1 0 1 0AlphaSpec Neptunium 90 0 141 0AlphaSpec Plutonium 21 0 49 0AlphaSpec Radium 226 7 0 7 0GasFlowSr2nd count 191 0 199 0GasFlow Strontium 90 365 0 422 0GasFlow Strontium 90 1 0 1 0GasFlow Total Radium 78 0 103 0 ICP-MS Technetium-99Prepin Water 8 0 32 0 ICP-MS Uranium-233 234 in Liquid 6 0 11 0 LSC Calcuim 45 1 0 1 0LucasCell Radium 226 310 0 366 0LucasCell Radium-226 10 0 10 0 Total Activity Screen 7 0 7 0 Chlorine-36 in Liquids 13 0 14 0AlphaSpec Am241 Curium 217 0 333 0GasFlow Total Strontium 112 0 116 0GrossAlphaNonVolBeta 980 0 1167 0 LSC Phosphorus-32 2 0 3 0LucasCell Radium226by Method Ra-04 2 0 2 0 ICP-MS Uranium-233, 234Prepin Liquid 6 0 11 0 Tritium in Drinking WaterbyEPA 906.0 9 0 12 0 Gamma Spec Liquid RAD A-013 withBa,La 84 0 159 0 Gamma Spec Liquid RAD A-013 with Iodine 162 0 189 0 Laboratories LLC P.O.Box 30712,Charleston,SC 294172014ANNUAL QUALITY ASSURANCE REPORTPage59of64GasFlow Strontium 89&90 5 0 3 0 ICP-MS Uranium-235, 236, 238 in Liquid 10 0 18 0GasFlow Total Alpha Radium 6 0 7 0 Gross Alpha Co-precipitation 3 0 13 0 ICP-MS Uranium-235 236, 238Prepin Liquid 6 0 11 0 ICP-MS Uranium-234, 235, 236, 238 in Liquid 31 0 74 0GrossAlphaBeta (Americium Calibration)

Liquid 32 0 46 0 ICP-MS Uranium-234, 235, 236, 238Prepin Liquid 15 0 38 0 Alpha/Beta Americium Calibration Drinkin Water 23 0 18 O.*******;:ltissUe;:i; Carbon-14 3 0 3 0 GammaSpecSolidRAD A-013 76 0 78 0 Technetium-99 4 0 4 0 Tritium 1 0 1 0 Alpha Spec Uranium 5 0 8 0 Alpha Spec Plutonium 5 0 10 0GasFlowSr2nd count 8 0 8 0GasFlow Strontium 90 11 0 12 0 Alpha Spec Am241 Curium 2 0 2 0GasFlow Total Strontium 17 0 17 0 GammaSpecSolidRAD A-013 withBa,La 10 0 10 0 GammaSpecSolidRAD A-013 with Iodine 23 0 22 0 Gross Alpha/Beta 2 0 2 0..........................

-.....-".LSC Iron-55 5 0 6 0 LSC Nickel 63 5 0 6 0GasFlow Total Strontium 6 0 6 0GrossAlphaNonVolBeta 6 0 6 0 GammaSpecLiquidRAD A-013 with Iodine7 0 11 0'VEG'EtAUON://"........:..........

LSC Iron-55 2 0 2 0 Gamma Nickel59RAD A-022 1 0 0 0 GammaSpecSolidRAD A-013 26 0 25 0 LSC Nickel 63 2 0 1 0 LSC Plutonium 1 0 1 0 Technetium-99 4 0 3 0 Tritium 11 0 11 0 Gamma Iodine-129 1 0 0 0GasFlowLead210 2 0 3 0 Total Uranium KPA 4 0 4 0 Alpha Spec Uranium 22 0 22 0 Alpha Spec Thorium 5 0 5 0AlphaSpec Plutonium 13 0 11 0AlphaSpec Neptunium 1 0 1 0 Alpha Spec Plutonium 1 0 1 0GasFlowSr2nd count 10 0 10 0 Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage60of64GasFlow Strontium 90 12 0 11 0GasFlow Total Radium 2 0 2 0AlphaSpec Am241 Curium 6 0 6 0 GammaSpecSolidRAD A-013 with Iodine 86 0 96 0 GammaSpecSolidRAD A-013 (pCi/Sample) 2 0 2 0AlphaSpec Am241 (pCi/Sample) 1 0 2 0 ICP-MS Uranium-234235,236, 238inSolid 12 0 7 0AlphaSpec Uranium 0 0 2 0 Gross Alpha/Beta 7 0 9 0AlphaSpec Plutonium 0 0 2 0GasFlow Strontium 90 4 0 2 0 ICP-MS Uranium-234235,236, 238PrepinSolid 7 0 4>.,: ii','*"":"1"**0;:.Gamma Iodine131RAD A-013 560 0 606 0 Gamma Iodine-129 7 0 6 0 Carbon-14 7 0 7 0 Carbon-14 (Ascarite/Soda Lime Filter per Liter)28 0 28 0 Gamma Iodine 129 7 0 7 0 Gamma Spec Filter 7 0 7 0AlphaSpec Uranium 4 0 5 0AlphaSpec Polonium 1 0 25 0 Tritium 39 0 40 0 Carbon-14 3 0 2 0 Iodine-131 2 0 2 0 LSC Iron-55 17 0 16 0LSCNickel63 16 0 15 0LSCRadon222 13 0 13 0 Technetium-99 2 0 1 0 Gamma Spec Liquid RAD A-013 17 0 18 0 Gamma Iodine-129 2 0 4 0 Gamma Iodine-131 27 0 26 0GasFlowLead210 4 0 3 0 Total Uranium KPA 17 0 34 0AlphaSpec Thorium 1 0 1 0GasFlow Radium 228 22 0 26 0AlphaSpec Plutonium 3 0 3.0GasFlowSr2nd count 12 0 12 0GasFlow Strontium 90 20 0 22 0 LSC Calcuim 45 2 0 2 0LucasCell Radium-226 23 0 49 0AlphaSpec Am241 Curium 2 0 2 0GasFlow Total Strontium 19 0 18 0GrossAlphaNonVolBeta 247 0 214 0 Tritium in Drinking WaterbyEPA 906.0 28 0 26 0 Gamma Spec Liquid RAD A-013 withBa,La 35 0 75 0GasFlow Strontium 89&90 17 0 11 0GasFlow Total Alpha Radium 1 0 1 0 Laboratories LLCP.O.Box30712,Charleston,SC294172014ANNUAL QUALITY ASSURANCE REPORTPage61of64 Gross Alpha Co-precipitation 99 0 91 0 Alpha/Beta (Americium Calibration)

Orinkinq Water 16 0 16 0 0 ECLS-R-GANJ48 Hr Rapid Gross Alpha 7 0 7 Total 16535 19734Note1:TheRPOmustbe20percentorless,ifbothsamplesaregreaterthan5timestheMOC.Ifbothresultsarelessthan5timesMOC,thentheRPOmustbeequaltoorlessthan100%.IfoneresultisabovetheMOCandtheotherisbelowtheMOC,thentheRPOcanbecalculatedusingtheMOCfortheresultoftheonebelowtheMOC.TheRPOmustbe100%orless.In thesituationwherebothresultsareabovetheMOCbutoneresultisgreaterthan5timestheMOCandtheotherislessthan5timestheMOC,theRPOmustbelessthanorequalto20%.IfbothresultsarebelowMOC,thenthelimitson%RPOarenot applicable.

I Laboratories LLCP.O.Box30712, Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage62of64 TABLE 8 2014 CORRECTIVE ACTION REPORT

SUMMARY

CORRECTIVEACTION 10#&DISPOSITION PE FAILURECARR140605-879 Root Cause Analysis of MAPEP-14-RdV28 in vegetation for Uranium-235byICP/MS ISO DocumentationofPT Failures in MAPEP-14-RdV30forUranium235inTherootcauseofthisfailurewashumanerrorandinattentionVegetationbyICP/MSand 14-MaS30todetail.TheQAO inadvertentlyenteredthe incorrect activity Uranium-233/234 and Uranium238byforthis parameterwhenshewasenteringtheresultsontheAlphaSpec.MAPEPwebsite.0.261 ug/sampleinsteadof0.0261 ug/samplewasentered.ThedataentryerrorwasnotcaughtduringtheGLreviewprocess.MAPEPresultsonlyarepeerreviewedbytheGLofthe applicableareatoensurethatthedatawasenteredcorrectly.

A secondPTwas successfully analyzed for this matrix.Uranium-234/233, and Uranium-238 in soil by Alpha Spec: Followingreviewsofourprocessanddataand conversations with personnelfromtheaffected laboratories,itwas determinedthatallfailureswereduetoan incomplete sample digestion.Atotaldigestion technique using Hydrofluoric Acid was performedonthesample.However,this digestion was not vigorousenoughto extractalltheU-234andU-238fromthesoil becausetheanalyteswerefusedintothesoilatan extremely high.temperature.Duetothehigh numberoflabsthatreceivedaNot Acceptableratingforthisanalysis,MAPEPhaspostedan explanationonthepreparationofthe UraniumSoilstandardon their website.Permanent Corrective/Preventive Actions or Improvements:

Upon notificationofthefailure,thesamplewasre-digestedusinga Sodium Hydroxidefusionmethodpriortoion-exchange separationchemistry.TheresultsforboththeU-234andU-238fallwithin acceptablerange.Inthefuture,all MAPEP soil sampleswillbeanalyzedwithaNaOHfusion dissolution technique.

Our analytical proceduresprovidethe flexibilitytoperform different extraction techniques (leaching, Laboratories LLC P.o.Box30712, Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTPage63of64 CARR140520-874 ISO DocumentationofPTFailuresin-MRAD-20forAmericium-241in water.HF dissolution)basedonclientrequests.ForourDOE, clients, complete dissolutionusingHFhasbeentheapproved methodforUranium.SomeclientsalsoaskfortheUranium analysisusingaleachprocedure.Inallcases,GELperformstherequiredcontractual procedurefortheanalysis.

A secondPTwas successfully analyzed for this matrix.Root Cause AnalysisAfterathoroughreviewofalldata,adefinitereasonforthefailurecouldnotbe determined.Thefollowingstepsweretakentoprovethatthiselevatedbiaswasanisolated occurrenceandthatouroverallprocessiswithincontrol.1.Thebatchqualitycontrolsampleswerereviewedandfoundtobecompliant.TherecoveriesintheLaboratoryControlSample(LCS)recoveredat98.2%.Twosample duplicateswerealsopreparedinthebatch.TheRPDswere4.8and8.6.2.Thesamplewasre-analyzedin duplicateafterthereportwasreceived.OnewithournormalAm-243tracer,andanotherwithCm-244tracer.Bothofthereanalysisconfirmtheoriginalreportedresult(whichisoutsidetherangeof acceptable results).ControlchartsforallAm tracerrecoverieswerealsoreviewed to determineiftheremaybeanissuewiththetracers.WhilethereisaslightbiasintheaverageLCSrecovery,itwasnot significantenoughto considerabnormal,anddidnotcomeclosetoaccountingforthehighresultonthisanalysis.

Additionally,sincethesamplewasreanalyzedusingtwo differenttracersandachievedthesameresult,atracerissuewasruledoutasthepotentialculprit Permanent Corrective/Preventive Actions or Improvements:Thelaboratorymustassume unidentifiedrandomerrorcausedtheelevatedbiasbecauseallqualitycontrolcriteriaweremetforthebatch.

Additionally,awell characterized performance evaluationsamplefromanothervendorwaspreppedandanalyzedafewweeksafterthissample.TheAm-241recoveredat105

%forthissampleandfellwellwithin its acceptance range.A secondPTwas successfully analyzed for this matrix.

Laboratories LLCP.O.Box30712, Charleston,SC29417 2014 ANNUAL QUALITY ASSURANCE REPORTCARR140825-902Page64of64ForFailuresofRAD-98for Strontium-Root Cause Analysis of Strontium-89 (Sr-89)89inWaterAfterareviewofthedata,anapparentreasonforthis discrepancycouldnotbe determined.Thefollowingstepsweretakentoprovethatthishighbiaswasanisolated occurrenceandthatouroverallprocessiswithincontrol.1.Thebatchqualitycontrolsampleswerereviewedandfoundtobecompliant.TheLCSrecoveredat 103%*2.Laboratorycontroldatawerealsoreviewedfortrends.Nonewasnoted.3.The instrumentcalibrationswerereviewedforpositivebiasesthatcouldhaveattributedtothisfailure.Nonewerenoted.4.Sample duplicateswerealsopreparedandcountedalongwiththereportedresult.Allresultsfellwithin the method's acceptancerangeforduplicates.

Permanent Corrective/Preventive Actions or Improvements The laboratorymustassumeanunidentifiedrandomerrorcausedthehighbiasforthisbatch.WhiletheLCSrecoveredoutsidetoits acceptancerange,thematrixspike(MS)recoveryfellwithinboththe acceptancerangefortheMS (80%-120%)andthe acceptancerangefortheLCS 1100/0).TheresultwasalsoconfirmedusingMethodLAB PBMS-A-004.Thelabwillcontinuetomonitortherecoveriesofthis radionuclidetoensurethattherearenoissues.

A secondPTwas successfully analyzed for this matrix.

ML15113A621

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SUBJECT:

DearSirorMadam:

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SUMMARY

1.0INTRODUCTION

1.1 Radiological

SUMMARY

3.1 Program

SUMMARY

SUMMARY

1.0 Introduction

1.1 Radiological

2.2 Thermoluminescent

2.4 Sediment

2.9 Interlaboratory

3.0 Radiological

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0.0 0TestAccetable

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ML15113A621

Text

SUBJECT:

DearSirorMadam:

Attachment:

SUMMARY

1.0INTRODUCTION

1.1 Radiological

SUMMARY

3.1 Program

SUMMARY

SUMMARY

1.0 Introduction

1.1 Radiological

2.2 Thermoluminescent

2.4 Sediment

2.9 Interlaboratory

3.0 Radiological

SUMMARY

SUMMARY

SUMMARY

SUMMARY

SUMMARY

SUMMARY

SUMMARY

SUMMARY

SUMMARY

0.0 0TestAccetable

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SUMMARY

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