ML16344A259

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Letter Report for Analytical Results for Six Soil Samples Associated with the Humboldt Bay Power Plant in Eureka, California
ML16344A259
Person / Time
Site: Humboldt Bay
Issue date: 10/27/2016
From: Ivey W
Oak Ridge Institute for Science & Education
To: John Hickman
Office of Nuclear Material Safety and Safeguards
References
DCN: 5201-LR-04-0, DE-SC0014664, RFTA 16-001, TAC J00338
Download: ML16344A259 (10)
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October 27, 2016 Mr. John Hickman ltr* OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION Managed by ORAU for DOE U.S. Nuclear Regulatory Commission 11545 Rockville Pike Mailstop T8FS Rockville,IvID 20852 ORISE CONTRACT NO. DE-SC0014664

SUBJECT:

LETTER REPORT FOR ANALYTICAL RESULTS FOR SIX SOIL SAMPLES ASSOCIATED WITH THE HUMBOLDT BAY POWER PLANT IN EUREKA, CALIFORNIA [TAC NO. J00338] [DOCKET NO. 50-133](RFTA NO.16-001) DCN: 5201-LR-04-0

Dear Mr. Hickman:

Oak Ridge Institute for Science and Education (ORISE) received SL'i: soil samples on September 14, 2016 from the Humboldt Bay Power Plant in Eureka, Califomia. ORISE is managed by Oak Ridge Associated Universities(ORAU) under DOE contract number DE-SC0014664. The samples were shipped to the laboratory from the licenssee's laboratory. The samples were received in good condition. Per the chain of custody, the samples were analyzed for gamma emitting isotopes by gamma spectrometry. In addition, per your request, the samples were analyzed for tritium by liquid scintillation counting. The analytical data, along with the procedure references, are presented in the attached reports. Quality Control (QC) requirements were met for these analyses. The QC files are available for your review upon request. Please feel free to contact me at 865.576.9184 or Forrest Smith at 865.574.9802 with any questions or comments. *Ir Ivey Laboratory Manager ORAU WPI:\'<!FS:km:lw Enclosures Electronic distribution: T. Carter, NRC S. Roberts, ORAU E. Bailey, ORAU D. Hagemeyer, ORAU File code: 5201; Lab code: 12372 P.O. Box 117 Oak Ridge, TN 37831

  • www.orau.org T. Vitkus, ORAU

j OAK RIDGE INSTITUTE FOR AND EDUCATION Managed by ORAU for DOE Project#: 201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 coc #: 1609-008 Analyst: smithw Client Sample ID: FSS-0757: OOL02-01-002-F Lab Sample ID: 1237280001 Detector ID: DET07 Count Date: 912812016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 105.31 K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (< MDC) TPU = Total Propagated Uncertainty -0.082 -0.001 -0.002 0.026 0.128 0.003 -0.07 0.033 11.9 0.025 -0.015 1.40 -0.150 MDC= Minimum Detectable Concentration Smp Qty.: 646.98 Live Time(s): 3,600 Receipt Date: 911412016 0.045 0.102 0.013 0.031 0.026 0.054 0.027 0.066 0.027 0.034 0.054 0.124 0.11 0.25 0.043 0.110 1.1 0.5 0.018 0.038 0.022 0.050 0.44 0.63 0.089 0.136 Units: grams Geometry: LM SOP (Rev.#): CP1 (20) Collection Date: 8130/2016 pCi/g u NIA pCilg u NIA pCilg u NIA pCilg u NIA pCilg 661.71 NIA pCilg u NIA pCi/g u NIA pCilg u NIA pCilg 1461.09 NIA pCilg 835.96 u NIA pCi/g u NIA pCilg 63.22 NIA pCilg u NIA NIA N/A NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 1of8 l1fj OAK RIDGE INSTITUTE FOR II SCIENCE AND EDUCATION I Managed by ORAU for DOE Project#: 201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 coc #: 1609-008 Analyst:' smithw Client Sample ID: FSS-0765: OOL02-01-010-F Lab Sample ID: 1237280002 Detector ID: DET08 Count Date: 912812016 SDG: 201212372-1 Am-241 59.54 -0.143 Co-57 122.06 -0.001 Co-60 1332.49 -0.015 Cs-134 795.86 0.049 Cs-137 661.66 0.056 Eu-152 344.28 -0.028 Eu-154 723.30 -0.129 Eu-155 105.31 0.007 K-40 1460.82 15.3 Mn-54 834.85 0.010 Se-75 264.66 -0.010 U-238 by Th-234. 63.29 2.80 Zn-65 1115.54 -0.079 Qualifier Flags: U = Analyte not detected(< MDC) TPU = Total Propagated Uncertainty MDC = Minimum Detectable Concentration Smp Qty.: 502.55 Live Time(s): 3,600 Receipt Date: 911412016 0.050 0.104 0.012 0.029 0.027 0.050 0.026 0.064 0.018 0.031 0.049 0.106 0.071 0.203 0.051 0.12Q 1.3 0.7 0.018 0.050 0.025 0.054 0.73 0.75 0.061 0.113 Units: grams Geometry: LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCilg u NIA pCilg u NIA pCilg u NIA pCilg u NIA pCi/g 661.65 NIA pCilg u NIA pCi/g u NIA pCilg u NIA pCilg 1461.05 NIA pCilg u NIA pCilg u NIA pCilg 63.25 NIA pCilg u NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 2 of 8 l1rj OAK RIDGE INSTITUTE FOR AND EDUCATION Managed by ORAU for DOE Project#: 201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 ---------------Gamma Spectrometry Summary Sheet Further: Toget11er Report Date: October24, 2016, coc #: 1609-008 Analyst: smithw .Client Sample ID: FSS-0779: OOL02-01-024-F Lab Sample ID: 1237250003 Detector ID: DET09 Count Date: 912812016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 . Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 .105.31 K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (< MDC)

  • TPU = Total Propagated Uncertainty -0.080 0.001 -0.003 -0.006 0.464 -0.024 -0.15 0.054 13.4 0.002 -0.008 2.06 -0.091 MDC = Minimum Detectable Concentration Smp Qty.: 523.29 Live Time(s): 3,600 Receipt Date: 911412016 0.043 0.097 0.013 0.031 0.025 0.049 0.014 0.063 0.055 0.034 0.044 0.100 0.11 0.22 0.032 0.069 1.2 0.5 0.024 0.053 0.024 0.057 0.58 0.69 0.078 0.139 Units: grams Geometry: LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCilg u NIA NIA pCilg u NIA NIA pCilg u NIA N/A pCilg u NIA NIA pCilg 661.74 NIA NIA pCi/g u NIA N/A pCi/g u NIA NIA pCilg 104.93 u NIA NIA pCilg 1461.14 NIA NIA pCi/g u NIA NIA pCi/g u NIA NIA pCi/g 63.19 NIA NIA pCi/g u NIA NIA Page 3 of 8

,fj OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION Managed by ORAU for DOE Project#: 201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 coc # : 1609-008 Analyst: smithw Client Sample ID: FSS-0782: OOL02-01-027-F Lab Sample ID: 1237280004 Detector ID: DET10 *count Date: 912812016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154

  • 723.30 Eu-155 105.31 K-40 1460.82 Mn-54 834.85" Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (< MDC) TPU = Total Propagated Uncertainty -0.025 0.0084 -0.013 0.039 0.044 0.023 -0.133 0.037 11.1 -0.016 -0.004 0.99 -0.095 MDC = Minimum Detectable Concentration Smp Qty.: 745.59 Live Time(s): 3,600 Receipt Date: 911412016 0.087 0.212 0.0100 0.0234 0.021 0.039 0.022 0.055 0.017 0.035 0.042 0.102 0.095 0.175 0.052 0.133 1.0 0.6 0.020 0.038 0.021 0.049 0.58 1.21 0.060 0.101 Units: grams Geometry: LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCilg u NIA pCilg 121.30 u NIA pCilg u NIA pCilg u NIA pCilg 661.97 NIA pCilg u NIA pCilg u NIA pCilg u NIA pCilg 1460.60 NIA pCilg u NIA pCi/g u NIA pCi/g 63.55 u NIA pCilg u NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 4 of 8 l1fj OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION E I Managed by ORAU for DOE Project#: 201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 coc # : 1609-008 Analyst: smithw Client Sample ID: FSS-0783: OOL02-01-028-F Lab Sample ID: 1237250005 Detector ID: DET07 Count Date: 913012016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 105.31 K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (< MDC) TPU = Total Propagated Uncertainty 0.009 0.009 -0.014 0.025 0.218 -0.045 -0.23 0.059 15.2 -0.002 -0.006 0.66 -0.170 MDC = Minimum Detectable Concentration Smp Qty.: 628.05 Live Time(s): 3,600 Receipt Date: 911412016 0.036 0.112 0.014 0.034 0.031 0.060 0.031 0.074 0.036 0.041 0.064 0.136 0.15 0.25 0.047 0.122 1.4 0.6 0.027 0.058 0.026 0.062 0.36 0.73 0.089 0.153 Units: grams Geometry: LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCi/g u NIA pCilg u NIA pCilg u NIA pCilg u NIA pCilg 661.74 NIA pCi/g u NIA pCilg u NIA pCilg

,Jj OAK RIDGE INSTITUTE FOR 11 SCIENCE AND EDUCATION Managed by ORAU for DOE Project#: 201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Furt11e1: Together Report Date: October 24, 2016 coc # : 1609-008 Analyst: smithw Client Sample ID: FSS-0787: OOL02-01-032-F Lab Sample ID: 1237280006 Detector ID: DET07 Count Date: 912812016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 '795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 105.31 K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (<MDC) TPU = Total Propagated Uncertainty -0.045 0.0085 0.017 0.002 0.478 0.024 -0.18 -0.018 12.3 0.006 -0.009 0.70 -0.133 MDC= Minimum Detectable Concentration Smp Qty.: 655.82 Live Time(s): 3,600 Receipt Date: 911412016 0.046 0.107 0.0097 0.0227 0.027 0.063 0.031 0.065 0.054 0.040 0.054 0.134 0.13 0.25 0.043 0.106 1.2 0.6 0.027 0.059 0.025 0.057 0.35 0.69 0.085 0.148 Units: grams Geometry: LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCilg u NIA pCilg 123.06 u NIA pCilg u NIA pCilg u NIA pCilg 661.88 NIA pCilg u NIA pCilg u NIA pCilg u NIA pCilg 1461.00 NIA pCilg u NIA pCilg u NIA pCilg 63.26 NIA pCilg u NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 6 of 8 l1fj OAK RIDGE INSTITUTE FOR AND EDUCATION Managed by ORAU for DOE Project#: Project Name: Batch Number: GS0351 Client Sample ID: Lab Sample ID: BLK0351S Detector ID: DET09 Count Date: 912812016 SDG: Am-241 59.54 -1.7 Co-57 122.06 -0.9 Co-60 1332.49 -1.8 Cs-134 795.86 -1.7 Cs-137 661.66 5.1 Eu-152 344.28 3 Eu-154 723.30 . -14 Eu-155 105.31 12 K-40 1460.82 -11 Mn-54 834.85 -2.5 Se-75 264.66 -2.4 U-238 by Th-234 63.29 -27 Zn-65 1115.54 -8 Qualifier Flags: U = Analyte not detected (< MDC) TPU = Total Propagated Une;ertainty MDC= Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: October 24, 2016 COC#: Analyst: smithw Smp Qty.: 1.00 Live Time(s): 3,600 Receipt Date: 911412016 7.7 19.6 3.3 7.9 6.9 14.8 6.2 14.1 6.4 17.0 14 35 30 66 11 30 84 226 6.3 12.5 6.1 14.1 59 158 15 28 Units:* sample SOP (Rev.#): CP1 (20) Collection Date: pCilsample pCilsample pCi/sample pCilsample pCi/sample pCilsample pCilsample pCilsample pCilsample 1461.09 pCilsample pCilsample pCi/sample 63.48 pCilsample Further. Together Geometry: LM u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u .NIA NIA u NIA NIA u NIA NIA Page 7 of 8 l1fj OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION I Managed by ORAU for DOE Project#: Project Name: Batch Number: GS0351 Client Sample ID: Lab Sample ID: LCS0351S Detector ID: DET08 Count Date: 912812016 SDG: Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 105.31 .K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Electronically Validated By: Roxanne Nagle-10/512016 09:23 Electronically Approved By: Yr Wade Ivey 10/2412016 13:01 Qualifier Flags: U = Analyte not detected(< MDC) TPU = Total Propagated Uncertainty 9.04 2.96 5.62 0.07 3.73 ' 0.051 -0.13 0.122 0.14 -0.57 35 -14.6 -0.1 MDC= Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: October24, 2016 COC#: Analyst: smithw Smp Qty.: 514.39 Live Time(s): 3,600 Receipt Date: 911412016 0.27 0.12 0.35 0.59 0.25 0.12 0.14 *0.29 0.25 0.07 0.089 0.202 0.20 0.40 0.097 0.234 0.20 0.47 0.66 1.26 35 81 3.5 1.0 3.1 7.1 Units: grams SOP (Rev.#): CP1 (20) Collection Date: pCilg 59.45 pCilg 121.95 pCilg 1332.69 pCilg* pCilg 661.67 pCilg pCilg pCilg pCilg 1461.21 pCilg pCi/g. 263.79 pCi/g pCilg Further. Togetl1er Geometry: 250LM NIA 0.96 NIA N/A NIA NIA u NIA NIA NIA 0.95 u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA N/A u NIA N/A u NIA N/A u N/A N/A Page 8 of 8 Liquid Scintillation Analysis Summary Results by Analyte \1rl. OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION Managed by ORAU for DOE Analyte: H-3 Project Name:: Humboldt Bay PP 09-2016 Project#: 201212372 SOP (Rev.#): AP6 (21) SDG #: 201212372-1 *ro_.-:1c.*//*u.::-r Report Date: 10/11/2016 *----*_, .,-. :; * ' * *, * * * -** ... ... FSS-0757:00L02-01-002-F FS5-0765:00L02-01-010-F . F55-0765:00L02-01-010-F F55-0779:00L02-01-024-F FS5-0782:00L02-01-027-F F55-0783:00L02-01-028-F F55-0787:00L02-01-032-F 1237250001 1237250002 12372S0002Dup 1237250003 1237250004 1237250005 1237250006 Validated By: Date: Approved By: tr/ l/i.#W j? J.10L Date: I 0 / J 'I J) b I / Qualifier Flags: U= Analyte not detected (<MDC) TPU= Total Propagated Uncertainty MDC= Minimum Detectable Concentration 0.6 -0.9 0.2 -1.4 -0.9 0.2 -0.5 3.4 5.9 pCi/g u HB0362 2.9 5.2 pCi/g u HB0362 2.8 4.9 pCi/g u HB0362 2.1 3.8 pCi/g u HB0362 2.7 4.8 pCi/g u HB0362 2.9 5.0 pCi/g u HB0362 2.6 4.6 pCi/g u HB0362 Page 1 of 1

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