ML071730456

Final Status Survey (FSS) Final Report - Phase Vii - Chapter 16 of 19 - Appendix A15, Survey Unit Release Record 9514-0001, East Primary Parking Lot

ML071730456
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Site:	Haddam Neck File:Connecticut Yankee Atomic Power Co icon.png
Issue date:	03/23/2007
From:	Massengill B Connecticut Yankee Atomic Power Co
To:	NRC/FSME
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Book 1 of 1 4 Final Status Survey Final Report Phase VII Appendix Al 5 Survey Unit Release Record 9514-0001, East Primary Parking Lot May 2007 CYAPCO FINAL STATUS SURVEY RELEASE RECORD EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 FSSEngeDate:r FSS Engineer Prepared By: Reviewed-,KWAW S ýngineer Approved By: _ _ _ _Telhnical Support Manager Date: 3 1 1q 107 Date:_____

Revision 0 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD TABLE OF CONTENTS 1. SURVEY UNIT DESCRIPTION

......................................................

3 2. CLASSIFICATION BASIS ................................................................

3 3. DATA QUALITY OBJECTIVES (DQO) ..........................................

6 4. SU RV EY D ESIGN .............................................................................

9 5. SURVEY IMPLEMENTATION

.......................................................

12 6. SURVEY RESULTS ........................................................................

14 7. QUALITY CONTROL ....................................................................

19 8. INVESTIGATIONS AND RESULTS .............................................

20 9. REMEDIATION AND RESULTS ..................................................

21 10. CHANGES FROM THE FINAL STATUS SURVEY PLAN ...... 21 11. DATA QUALITY ASSESSMENT (DQA) .....................................

21 12. A N O M A LIES ..................................................................................

22 13. CO N CLU SIO N ................................................................................

22 14. A TTA CH M EN TS .............................................................................

23 14.1 Attachment 1 -Figures (5 pages including cover)14.2 Attachment 2 -Scan Results (6 pages including cover)14.3 Attachment 3 -Laboratory Results (114 pages including cover)14.4 Attachment 4 -DQA Results (18 pages including covers)TOTAL 166 Revision 0 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD SURVEY UNIT DESCRIPTION Survey Unit 9514-0001 (East Primary Parking Lot) is designated as a Final Status Survey (FSS) Class 2 survey unit and consists of eight thousand seven hundred thirty-nine square meters (8,739 m 2) or 2.159 acres of uninhabited open land located approximately five hundred and eighty-four feet (584 ft) south of the reference coordinate system benchmark used at Haddam Neck Plant (HNP).This survey unit is bounded by Survey Units 9504-0000, 9506-0000 and 9508-0000 to the north (called north based on the general north to south flow of the Connecticut River), Survey Units 9527-0001 and 9527-0004 to the east, Survey Units 9313-0000 and 9527-0005 to the south and by Survey Unit 9514-0000 to the west.The survey unit is located outside of the former Radiological Controlled Area (RCA), outside the former Industrial Area but within the Owner Controlled Area.The survey unit is comprised of predominantly flat disturbed open land that gently slopes from east to west toward the Connecticut River. The eastern portion of the survey unit contains a small stream that collects water from the hillside to the south and east of the survey unit and flows from south to north through the survey unit until it discharges into the onsite retention pond (Survey Unit 9508-0000).

The reference coordinates associated with this survey unit are E004 through E012 by S050 through S058 (refer to LTP Section 5.4.4). The reference coordinates provide the maximum dimensions of a rectangle containing this survey unit. Some areas contained in this rectangle may not be part of this survey unit. The boundary of the survey unit was defined using a Global Positioning System (GPS) based on the Connecticut State Plane System North American Datum (NAD) 1927.2. CLASSIFICATION BASIS The survey unit was classified in accordance with Procedure RPM 5.1-10,"Survey Unit Classification. " The historical information, scoping analyses and characterization results provided sufficient data to designate Survey Unit 9514-0001 as Class 2 in February 2007.The "Classification Basis Summary" conducted for Survey Unit 9514-0001 consisted of: a) A review of the 1OCFR50.75 (g) (1) database, b) A review of the "Initial Characterization Report" and the "Historic Site Assessment Supplement, " c) Historic and current survey records review, d) Visual inspections and a "walk-down." of the area were performed.

Revision 0 3 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Survey Area 9514, which consists of the Primary Parking Lot, is a surface survey area (the corresponding sub-surface Survey Area is 9803) that has historically been used to stockpile soils, asphalt spoils, snow and other materials.

Containerized radioactive materials have also been stored here over the past few years. The historical assessment of the survey area indicated that the age of the paved area dates back to the earliest days of plant operation.

The scoping report in 1997 had little information on this area, but did note that Plant Incident Report (PIR) 80-37 reported the discovery of several sources of elevated activity in March 1980, along with other areas of the site. The investigation into the incident concluded that the elevated activity was most likely due to radioactive materials ejected from the Primary Vent Stack as a result of operational events in 1979. Isotopic analysis of the particles indicated that the short-lived fission products, Ce- 144 and Ru- 106, dominated the particulate radioactivity.

All elevated areas were removed upon detection according to supplemental reports.A review of the 10 CFR 50.75(g) files identified five (5) additional entries identifying Survey Area 9514 (Survey dated 6/11/79; Contract, drawings and Spec. work logs from 10/11/82; Email from GTS Duratek dated 1/26/99; memo HP 111; memo HP-99-113);

however, these sources did not provide a significant amount of additional information for characterization of Survey Area 9514. Additionally, Warehouse

1. 2 and the Office Building #3/Primary Access Point were constructed in 1989 and the primary parking lot was re-configured.

The primary parking lot was enlarged, re-paved and storm drains installed.

Scanning of the parking lot was conducted on September 17-25, 1997 using a floor monitor. No elevated areas of activity were identified.

Soil samples were taken of a proposed sanitary sewer sump location just west of the Security Building Primary Access Point (PAP). No plant related radioactivity was identified in these samples. Areas behind the Building Maintenance Equipment Warehouse and the Chemical Storage Warehouse were also used as storage areas for radioactive materials returned to site as a result of the Offsite Materials Recovery Program.A storm drain system was installed under the parking area. The storm drain system's purpose was to conduct runoff water from the parking lot, including the northern-most side of Survey Area 9313 (adjacent to the office building and warehouses), and the west hillside primarily to the retention pond. Outfalls from the storm drain system discharge to the southeast and southwest banks of the pond (Survey Area 9508). Overflow from the retention pond discharges to the west bank of the Connecticut River (Survey Area 9512).Recent decommissioning activities included the removal of asphalt, concrete and sub-surface commodities such as storm drain and sewer system piping.Two (2) potential pathways for residual contamination to exist within this survey area are from the mixing of surface soils with paving materials during demolition or from storm drain pipe leakage.Revision 0 4 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD After remediation was complete in Survey Area 9514, characterization samples were collected and analyzed in accordance with Survey and Sampling Work Plan (SSWP) 06-09-001.

Evaluation of soil samples collected for the SSWP provided the information with regard to the radionuclides of concern within Survey Area 9514. These results are summarized in Table 1.Table 1- Basic statistical quantities from SSWP 06-09-001 Radiological Assessment survey Parameter Cs-137 Co-60 Sr-90 (pci/g) (pC00) (pci/g)Operational DCGL: 5.38E+00 2.59E+00 1.05E+00 Minimum Value: -9.68E-03

-3.21E-02 5.67E-03 Maximum Value: 8.44E-01 9.36E-02 7.39E-02 Mean: 9.22E-02 4.87E-03 3.43E-02 Median: 3.06E-02 3.16E-03 2.95E-02 Standard Deviation:

2.06E-01 2.64E-02 2.18E-02 Characterization sample data indicated that several locations in the eastern portion of Survey Area 9514 contained elevated amounts of Sr-90 at levels up to seven percent (7%) of the Operational Derived Concentration Guideline Level (DCGL) for Sr-90.Based on the characterization results provided in Table 1, Survey Area 9514 was split into two (2) survey units. Survey Unit 9514-0001 (the survey unit covered by this Release Record) is a Class 2 survey unit which consists of open land and comprises the eastern portion of the former primary parking lot.The western portion of the former primary parking lot is covered by Survey Unit 9514-0000, a Class 3 survey unit.The characterization results for Survey Unit 9514-0001 indicate that Cs-137 and Co-60 are the primary radionuclides of concern for this survey unit.Additionally, HTD radionuclide analysis indicated that Sr-90 was present in several samples at levels up to seven percent (7%) of the Operational DCGL.Therefore, Sr-90 was selected as a radionuclide of concern. No other HTD radionuclides were present in concentrations above 5% of the Operational DCGL for soil individually or 10% of the Operational DCGL for soil as a composite.

The FSS Engineer performed a visual inspection and walk-down during February 2007 to assess the physical condition of the survey unit, evaluate access points and travel paths and identify potentially hazardous conditions.

Revision 0 5 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD This survey area is affected by existing groundwater (reference CY memo ISC 06-024) which will be a source of dose from residual radioactivity, as discussed in Section 3 under the Data Quality Objectives.

Based upon the historical information and the results of radiological surveys performed during characterization, it was concluded that there was a low probability for residual radioactivity to be present in this survey unit in concentrations greater than the Operational DCGLs justifying a final survey unit classification of Class 2 (refer to Section 3).3. DATA QUALITY OBJECTIVES (DQO)FSS design and planning used the Data Quality Objective (DQO) process as described by the LTP, Procedure RPM 5.1-11, "Preparation of Final Status Survey Plan, " and the "Multi-Agency Radiation Survey and Site Investigation Manual" (MARSSIM).

A summary of the main features of the DQO process are provided herein.The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis.

Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition.

The baseline condition is technically known as the null hypothesis.

Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection.

In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria.

Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria.

Therefore, the survey unit does satisfy the primary objective of the Final Status Survey Plan (FSSP). Probabilistic sampling is a preferred method to select a sample so that each item in the population being studied has a known likelihood of being included in the sample. Probabilistic sampling may include simple random sampling where every sample has the same chance of being included, or systematic random sampling where samples are arranged in some order and a random starting point is selected.The primary objective of the FSSP was to demonstrate that the level of residual radioactivity in Survey Unit 9514-0001 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity.

This is done through the development of DCGLs. The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations.

Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil (called Base Case Soil DCGL), existing groundwater radioactivity and future groundwater radioactivity that will be contributed by building basements and footings.Revision 0 6 Revision 0 6 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD The DCGLs presented in Chapter 6 of the LTP were developed for exposures from three (3) components, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity.

Equation 1 shows the mathematical relationship between the three (3) components and the total dose.Equation I HTotal =Hsoil +HExistingGW

+ HFutureGW The total dose under the LTP criteria is twenty-five (25) mrem/yr TEDE from all three (3) components.

The allowable total dose under the Connecticut Department of Environmental Protection (CTDEP) radiological remediation standard for CY is nineteen (19) mrem/yr TEDE. To satisfy both the LTP and CY CTDEP criteria, the dose from soil must be reduced when using the existing and future groundwater dose values discussed above.This survey area is affected by existing groundwater (reference CY memo ISC 06-024). Therefore, the dose contribution from existing groundwater is bounded by two (2) mrem/yr TEDE.This survey unit is not considered impacted by future groundwater radioactive contamination, as there are no buried concrete foundations or footings containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component is, therefore, zero (0) mrem/yr TEDE.Equation 2 19 mrem/yrTotal

= 17 mrem/yrsoil

+ 2 mrem/yrExisting GW+ 0 mrem/yrFuturcGW The allowable dose for soil in this survey unit is seventeen (17) mrem/yr TEDE as shown by Equation 2 above. The concentration of residual radioactivity resulting in seventeen (17) mrem/yr TEDE is designated as the Operational DCGL, and has been established for the radionuclides of concern as provided in Table 2.Revision 0 7 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Table 2 -Radionuclide Specific Base Case Soil DCGL, Operational DCGLs and Rpnauired Minimum Detectahle Radionuclide (1) Base Case Soil Operational DCGL Required MDC DCGL (pCi/g) (2) (pCi/g) (3) (pCi/g) (4)H-3 4.12E+02 2.81E+02 1.65E+01 C-14 5.66E+00 3.84E+00 2.26E-01 Mn-54 1.74E+01 1.18E+O1 6.96E-01 Fe-55 2.74E+04 1.87E+04 1.1OE+03 Co-60 3.81E+00 2.59E+00 1.52E-01 Ni-63 7.23E+02 4.91E+02 2.89E+01 Sr-90 1.55E+00 1.05E+00 6.20E-02 Nb-94 7.12E+00 4.85E+00 2.85E-01 Tc-99 1.26E+01 8.57E+00 5.04E-01 Ag-108m 7.14E+00 4.86E+00 2.86E-01 Cs- 134 4.67E+00 3.18E+00 1.87E-01 Cs-137 7.91E+00 5.38E+00 3.16E-01 Eu-152 1.01E+01 6.87E+00 4.04E-01 Eu-154 9.29E+00 6.32E+00 3.72E-01 Eu-155 3.92E+02 2.67E+02 1.57E+01 Pu-238 2.96E+01 2.01E+01 1.18E+00 Pu-239/240 2.67E+01 1.82E+01 1.07E+00 Pu-241 8.70E+02 5.92E+02 3.48E+01 Am-241(5) 2.58E+01 1.75E+01 1.03E+00 Cm-243/244 2.90E+01 1.97E+01 1.16E+00 k1) Bod inuicates mHose rauionucliues consiuereu to be ham LO ueeCLL.(2) The Base Case Soil DCGLs for soil are specified by the LTP in Chapter 6 and are equivalent to twenty-five (25) mrem/yr TEDE.(3) The Operational DCGL is equivalent to seventeen (17) mrem/yr TEDE.(4) The required MDC is equivalent to one (1) mrem/yr TEDE.(5) Americium-241 can be analyzed by gamma and alpha spectroscopy and is considered to be Easy to Detect (ETD). The preferred result is the alpha spectroscopy's when both analyses are performed.

Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration variability.

Fifteen (15) samples were collected and analyzed during characterization, as discussed in Section 2.The mean and variability of Cs-137, Co-60 and Sr-90 in soil in this survey unit was determined during characterization and are provided in Table 1.Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the DCGL. Survey instrument response checks were required prior to issue and after the instrument had been Revision 0 8 Revision 0 8 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD used. Control and accountability of survey instruments was required to assure the quality and prevent the loss of data.As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. Results reported as less than Minimum Detectable Concentration

(<MDC) were not accepted for FSS. Sample report summaries included unique sample identification, analytical method, radionuclide, result, and uncertainty to two (2) standard deviations, laboratory data qualifiers, units, and the required and observed MDC.4. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in Procedure RPM 5.1-11, "Preparation of Final Status Survey Plans".The FSSP uses an integrated sample design that combines scanning surveys and sampling which can be either random or biased.Characterization sampling was used to determine concentration variability.

The DQO process determined that Cs-137, Co-60 and Sr-90 would be the radionuclides of concern in survey unit 9514-0001 (refer to Section 3). The sum of fractions or unity rule was used with the individual Operational DCGLs because multiple radionuclides (Cs-137, Co-60 and Sr-90) are considered in the survey design. Other radionuclides identified during FSS were evaluated to ensure adequate survey design.Surrogate DCGLs were not required for this survey unit based on process knowledge from FSS of adjacent areas and via screening under LTP Section 5.4.7.2, "Gross Activity DCGLs". Radionuclide screening or de-selection is a process where an individual radionuclide or aggregates may be considered insignificant and eliminated from the FSS. The criteria for de-selection are concentrations less than 5% for individual radionuclides and less than 10% for aggregates.

The Elevated Measurement Comparison (EMC) did not apply to this survey unit since it is a Class 2 area and discrete, elevated areas of contamination were not expected.The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation.

This approach was conservative since it included background Cs-137 as part of the sample set.The number of soil samples for FSS was determined in accordance with Procedure RPM 5.1-12, "Determination of the Number of Surface Samples for Final Status Survey." The Lower Bound of the Gray Region (LBGR) was set in accordance with Procedure RPM 5.1-11 to 0.91 to maintain the relative shift (A/a) in the range of 1 and 3. The resulting Adjusted Relative Shift was 2.0. A Prospective Power Curve was generated using COMPASS, a software package Revision 0 9 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10 CFR 20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design.Survey design specified fifteen (15) surface soil samples for non-parametric statistical testing.The grid pattern and locations of the soil samples were determined using Visual Sample Plan (VSP) in accordance with Procedure RPM 5.1-14, "Identifying, and Marking Surface Sample Locations for Final Status Survey." Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy. A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate for a Class 2 area.Judgmental sampling was included as a feature of this survey design to investigate suspect areas and account for any anomalies identified in the field.Sample locations were identified using AutoCAD-LT, a commercially available plotting software package with coordinates consistent with the Connecticut State Plane System. These coordinates were integrated with a Global Positioning System (GPS) to locate sample points in the field. Sample Measurement Locations for the design are listed with the GPS coordinates in Table 3.Revision 0 10 Revision 0 10 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Table 3 -Sample Measurement Locations identified for Non-parametric Statistical Testin2 with their Associated GPS Coordinates Designation")

Northing Easting 9514-0001-OO1F 237249.28 668065.13 9514-0001-002F 237177.80 668023.86 9514-0001-003F 237177.80 668106.40 9514-0001-004F/FS 237177.80 668188.94 9514-0001-005F 237106.31 668065.13 9514-0001-006F 237106.31 668147.67 9514-0001-007F 237106.31 668230.21 9514-0001-008F" 2) 237106.31 668312.75 9514-0001-009F 237034.83 668188.94 9514-0001-010F/FS 237034.83 668271.48 9514-0001-01iF 237034.83 668354.02 9514-0001-012F 236963.35 668312.75 9514-0001-013F 236963.35 668395.29 9514-0001-014F 236963.35 668477.83 9514-0001-015F 236891.87 668354.02 9514-0001-016F13) 237086.27 668140.73 (1)"F" denotes Final Status Survey sample location and "FS" denotes Field-Split sample location.2),"Sample number 9514-0001-008F could not safely be collected so that sample location was abandoned and a new location was randomly selected.(3)Random sample number 9514-0001-016F was selected as a Non-parametric sample location because sample number 9514-0001-008F could not be collected.

Although Procedure RPM 5.1-11 only specified that 5% of the samples are required to be selected for HTD analysis, two (2) soil samples or 13% of the number of samples that would be used for non-parametric statistical testing were randomly selected for HTD radionuclide analysis using the Microsoft Excel "RANDBETWEEN" function.

Each sample was sent off-site for a full suite analysis of the HTD radionuclides specified in the LTP, Table 2-12,"Radionuclides Potentially Present at Haddam Neck Plant" and as provided in Table 2.The implementation of quality control measures as referenced by Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey," included the collection of two (2) soil samples for "split sample" analysis by the off-site laboratory.

These locations were selected randomly using the Microsoft Excel"RANDBETWEEN" function.

The number of quality control soil samples was determined to be 13% of fifteen (15) samples.The LTP specifies that scanning will be performed along with a combination of systematic and judgmental measurements (samples) for a Class 2 land area and should cover 10% to 100% of the area. The fraction of scanning coverage was determined during the DQO process with the total amount and location(s) based on the likelihood of finding elevated activity during FSS.Revision 0 I1I Revision 0 11 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Based on the historical site assessment and the characterization data available, it was determined that three (3) separate scan grids needed to be established.

The total surface area to be scanned was approximately 25% of the survey unit. A map of the scan grid locations is provided in Attachment 1.For this Class 2 survey unit, the "Investigation Level" for area scanning and soil sample measurement results are those levels specified in LTP, Table 5-8. Table 4 provides a synopsis of the survey design.Table 4 -Svnonsis of the Survev Design(1)Feature Design Criteria Basis Survey Unit Land 8,739 m 2 Based on AutoCAD-LT and Area Visual Sample Plan calculations Type 1 and Type 2 errors were Number of 0.05, sigma was 0.04 pCi/g, and Measurements 15 the LBGR was adjusted to 0.91 to maintain Relative Shift in the range of 1 and 3.Grid Spacing 25.9 m Based on triangular grid 5.38 pCi/g Cs-137 Administratively set to achieve Operational DCGL 2.59 pCi/g Co-60 seventeen (17) mrem/yr TEDE (2)1.05 pCi/g Sr-90 Soil Investigation 5.38 pCi/g Cs-137 The Operational DCGL meets the Lnvel 2.59 pCi/g Co-60 LTP criteria for a Class 2 survey 1.05 pCi/g Sr-90 unit Scan Survey Area Approximately 25% The LTP requires >10% area coverage for Class 2 Survey Coverage of the area Uis Units.Scan Investigation Detectable over Administratively set to achieve Level background seventeen (17) mrem/yr TEDE (2)k 1) i ne survey aesign used a mucn smatter value ior me Operational Ltl.AJL man proviueu by Table 2 to conservatively account for the contribution to the total dose from existing and future groundwater which had not been established at the time of planning this FSS.(2) The allowable dose for soil in this survey unit is seventeen (17) mrem/yr TEDE as the bounding dose from existing and future groundwater has been established based on field data (reference CY memo ISC 06-024.)5. SURVEY IMPLEMENTATION Final status survey field activities were conducted under a detailed FSSP 9514-0001 that included the implementation of a job safety analysis, job planning checklist and related procedures for reference.

Daily briefings were conducted to discuss the expectations for job performance and the safety aspects of the survey. The "Daily Survey Journal" was used to document field activities and other information pertaining to the FSS.Three (3) scan areas were established that constituted approximately 25% of the surface area of Survey Unit 9514-0001.

Grid lines, one (1) meter wide, were Revision 0 12 Revision 0 12 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD painted on the ground of each of the three (3) scan areas. A background survey was performed around the survey unit and it was determined that the range of background measurements, using a Eberline E-600 with a SPA-3 sodium iodide detector, was varied from 4,000 counts per minute (cpm) in the western part of the survey unit up to 9,000 cpm near the southeastern part of the survey unit toward the hillside.The scan areas were established and each area was scanned for elevated readings (see Attachment 2 for all scan results).

Scanning was performed with an Eberline E-600 using a SPA-3 sodium iodide detector.

The E-600 was operated in the rate-meter mode and used with audio response.

The probe was positioned as close to the ground as possible and was moved at a scan speed of about 0.5 meters per second. Approximately 25% of the survey unit was scanned.Measurement locations were identified in North American Datum (NAD) 1927 coordinates using GPS coordinates; sample fixed measurement locations were identified and marked with a surveyor's flag or paint for identification.

At each sample fixed measurement location, a one (1) meter radius around the sample flag or paint mark was scanned for elevated radiation levels.One (1) of the original fifteen (15) samples identified, 9514-0001-008F was not collected because the sample location was found to be inaccessible.

Additionally, the sample location could not be identified within 3 meters of the original location.

As part of the survey design, several additional alternate sample locations were selected randomly, as determined by using Visual Sample Plan (VSP), in accordance with Procedure RPM 5.1-14, "Identifying, and Marking Surface Sample Locations for Final Status Survey." One (1) of the random sample locations was selected and designated as 9514-0001-016F.

Fifteen (15) surface soil samples were collected for non-parametric statistical testing and packaged in accordance with Haddam Neck Plant (HNP) Procedure RPM 5.1-3, "Collection of Sample Media for Final Status Survey" and FSS design. Samples were controlled, transported, stored, and transferred to the off-site laboratory using Chain-of-Custody (COC) protocol in accordance with Procedure RPM 5.1-5, "Chain of Custody for Final Status Survey Samples." Two (2) samples (9514-0001-001F and 9514-0001-010F) were randomly selected for HTD radionuclide analysis.The implementation of survey specific quality control measures included the collection of two (2) samples (9514-0001-001F and 9514-0001-013F) for "split sample" analysis.Follow-up sampling was conducted at each of the elevated measurement locations.

Revision 0 13 Revision 0 13 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Five (5) judgmental sample locations in the creek bed that runs south to north along the eastern portion of the survey unit, were identified by the FSS Engineer.A map identifying all of the sample locations is provided in Attachment

1.6. SURVEY

RESULTS All field survey activities were conducted between February 22 and February 27, 2007.On February 22, 2007, three (3) scan areas, that comprised approximately 25%of the total surface area for the survey unit, were scanned for elevated radiation levels.Six (6) elevated measurement locations within scan area three (3) were identified during scanning.

Each of the locations was evaluated using the Exploranium, and were determined to be Naturally Occurring Radioactive Material (NORM) based on the presence of loose rock. Table 5 provides an overview of the scan area survey. Attachment 1 contains a map that identifies the locations of the three (3) scan grids. All scan results are provided in Attachment 2.Revision 0 14 Revision 0 14 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD... .... Table 5-Scan Area Results Scan Grid Rangeof Highest Range of > Elevated Investigation Aran Grd Rgedn Logged Action Action Reading sample Area #'s Reading Reading Levels Level Identification Sample (kcpm) (kcpm) (kcpm) () (2) (3)1 6.04 6.04 8.36 NO 2 6.00 6.00 7.66 NO 3 6.47 6.47 7.48 NO 1 4 6.09 6.09 7.75 NO 5 6.78 6.78 7.88 NO 6 7.19 7.19 7.48 NO 1 6.00 6.00 7.24 NO 2 5.98 5.98 6.48 NO 2 3 5.55 5.55 7.60 NO 4 5.53 5.3 6.77 NO 5 5.48 5.48 6.55 NO 1-5 6.05-7.19 7.19 7.46-8.34 NO 6-10 5.46-6.49 6.49 6.15-9.14 YES 9514-01-ER-03-09-01 9514-0001-024F 1 1-5 4.48-7.54 7.4 601- YES 9514-01-ER-03-13-01 9514-0001-025F 11-15 4.4 7.54 7.54 6.0 4 Y S 9514-01-ER-03-13-02 9514-0001-026F 16-20 4.79-6.22 6.22 6.19-7.07 NO 5.10- 9514-01 -ER-03-23-0 1 9514-0001-027F 13.82 9514-01-ER-03-25-01 9514-0001-028F 4.41-26-30 17.19 5.75-8.76 YES 9514-01-ER-03-26-01 9514-0001-029F 17.19 3 1-35 4.28-4.97 4.97 5.48-6.06 NO 36-40 4.71-5.87 5.87 5.90-6.69 NO (1) The action level is based on a measurement above ambient background.

(2) Elevated areas were determined to be Naturally Occurring Radioactive Material, refer to Section 8.(3) ER nomenclature is associated with the barcodes used in the field where ER stands for Elevated Reading.On February 23, 2007 the fifteen (15) samples identified for non-parametric statistical testing were collected.

One (1) of the original fifteen (15) samples established by VSP using a random start, systematic triangular grid pattern, was deemed not accessible and was therefore replaced by a random sample location that was also identified by VSP. Sample number 9514-0001-008F was replaced by sample number 9514-0001-016F.

Additionally, on February 26, 2007, six (6) investigative samples were collected at the elevated measurement locations identified by the scan surveys and were designated as 9514-0001-024F, 9514-0001-025F, 9514-0001-026F, 9514-0001-027F, 9514-0001-028F and 9514-0001-029F.

Revision 0 15 Revision 0 15 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Five (5) judgmental sample locations in the creek bed were collected on February 27, 2007 and were designated as sample numbers 9514-0001-019J, 9514-0001-020J, 9514-0001-021 J, 9514-0001-022J and 9514-0001-023J.

Material Service Requisition (MSR) number 07-00100 was generated to cover the analysis of the samples at the approved off-site laboratory.

The fifteen (15) sample locations identified for non-parametric statistical testing along with the five (5) judgmental samples and the six (6) investigative sample locations were scanned over approximately a one (1) meter radius for elevated radiation levels, in accordance with the FSSP. Table 6 provides an overview of the scan results for sample measurement locations.

A map identifying all of the sample locations is provided in Attachment 1.Revision 0 16 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Table 6- Scan Results for Sam le Measurement Locations Sample Measurement Highest Logged Action Level (1)Location (5) Reading (kcpm) > Action Level (2)(kcpm)9514-0001-001F 3.98 4.08 NO 9514-0001-002F 4.74 4.95 NO 9514-0001-003F 4.64 5.95 NO 9514-0001-004F 5.95 7.22 NO 9514-0001-005F 4.02 5.57 NO 6514-0001-006F 5.38 6.78 NO 9514-0001-007F 6.19 7.10 NO 9514-0001-008F SAMPLE LOCATION IS INACCESSIBLE 9514-0001-009F 6.23 6.32 NO 9514-0001-O0OF 4.47 5.92 NO 9514-0001-01IF 5.91 7.83 NO 9514-0001-012F 5.25 6.14 NO 9514-0001-013F13) 6.76 6.19 YES 9514-0001-014F 6.45 6.69 NO 9514-0001-015F 5.45 5.94 NO 9514-0001-016F 4.93 5.69 NO 9514-0001-019J 4.79 6.58 NO 9514-0001-020J 6.06 7.01 NO 9514-0001-021J 7.80 9.49 NO 9514-0001-022J 8.97 10.1 NO 9514-0001-023J 8.60 10.3 NO 9514-0001-024F(4) 6.24 6.15 YES 9514-0001-025F(4) 6.07 6.01 YES 9514-0001-026F(4) 7.53 6.01 YES 9514-0001-027F(4) 8.43 8.11 YES 9514-0001-028F(4) 13.82 8.21 YES 9514-0001-029F(4) 17.19 8.40 YES (1) The action level is based on a measurement above ambient background in accordance with the FSSP.(2) FSS sample plans require movement of the sample measurement location to the area within the one (1) meter radius yielding the response above the action level (3) During the one (1) meter radius scanning conducted around sample location 9514-0001-013F an elevated measurement was detected.

In accordance with the FSSP, the sample was moved to the location of the elevated measurement.

(4) Denotes the follow-up samples that were collected at elevated scan grid locations identified in Table 6.(5)"F" denotes Final Status Survey sample location and "J" denotes Judgmental or Biased sample location.Revision 0 17 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories, LLC, Charleston, South Carolina.

The laboratory analyzed the fifteen (15) samples collected for non-parametric statistical testing, the associated duplicates, the five (5) biased samples and the six (6) investigative samples using gamma spectroscopy.

Gamma spectroscopy analysis was performed to the required MDCs. Gamma spectroscopy results identified some radionuclides meeting the accepted criteria for detection (i.e., a result greater than two (2) standard deviations uncertainty).

Cs-137 was identified in thirteen (13) of the fifteen (15) samples collected for non-parametric statistical testing. Co-60 was not identified in any of the fifteen (15) samples collected for non-parametric statistical testing. Sr-90 was identified in five (5) of the fifteen (15) samples collected for non-parametric statistical testing. The mean of the gamma spectroscopic analysis results for the samples indicated that Cs-137 was present at levels that are similar to the concentrations of Cs-137 found in soil at off-site locations within the vicinity of the HNP as presented in the Health Physics TSD BCY-HP-0063.

The "sum-of-fractions" or "unity rule" is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present. The combination of the fractions of each detected radionuclide against their respective Operational DCGL must be less than or equal to one (1).The unity rule is: Equation 3 Ci C 2 C,-÷++ C2 -- <1 DCGLI DCGL 2 DCGL, Where: Cn = concentration of radionuclide n and DCGLn = DCGL of radionuclide n.The results of the unity rule calculation for the radionuclides of concern in the statistical sample population for Survey Unit 9514-0001 are provided in Table 7.Revision 0 18 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Table 7- Summarv of Soil SamDle Results Fraction of Sample Number Cs-137 Co-60 Sr-90 the pCi/g pCi/g pCi/g Operational DCGL (1)9514-0001-OOIF 2.71E-02 2.88E-03 -8.87E-04 0.005 9514-0001-002F 6.23E-02 7.82E-03 -2.05E-02

-0.005 9514-0001-003F 1.57E-02 7.03E-03 3.52E-03 0.009 9514-0001-004F 1.05E-01 2.06E-02 4.64E-02 0.072 9514-0001-005F 5.04E-02 2.47E-04 9.28E-03 0.018 9514-0001-006F 4.02E-02 7.60E-03 6.81E-01 0.657 9514-0001-007F 6.41 E-02 1.66E-03 1.58E-02 0.028 9514-0001-009F 2.49E-02 5.94E-03 2.58E-02 0.031 9514-0001-O0OF 3.59E-02 -3.76E-03 3.30E-02 0.037 9514-0001-011F 3.70E-01 1.69E-02 3.26E-02 0.106 9514-0001-012F 5.55E-02 5.27E-03 4.59E-02 0.056 9514-0001-013F

1. 19E-01 5.90E-03 1.65E-02 0.040 9514-0001-014F 8.44E-0 1 0.OOE+00 -3.44E-03 0.154 9514-0001-015F

-1.62E-03 1.50E-02 -2.01E-02

-0.014 9514-0001-016F 1.91E-02 0.OOE+00 6.55E-03 0.010 (1) The Operational DCGLs are 5.38 pCi/g for Cs-137, 2.59 pCilg for Co-60 and 1.05 pCi/g for Sr-90 from Table 2 and are used in conjunction with the unity rule The off-site laboratory also processed two (2) samples for HTD analysis (other than Sr-90 which was analyzed for in each sample) as required by the sample plan. The requested analyses included alpha spectroscopy, gas proportional counting, and liquid scintillation depending on the radionuclide and the measurement method. All analyses met the required MDC. No HTD radionuclides, other than Sr-90, met the accepted criteria for detection (i.e., a result greater than two (2) standard deviations uncertainty).

Additionally, all HTD radionuclide, other than Sr-90, met the criteria for de-selection of a radionuclide is a concentration that is less than 5% of the Operational DCGL for individual radionuclides and less than 10% of the Operational DCGLs for aggregates.

7. QUALITY CONTROL The off-site laboratory processed the split samples and performed gamma spectroscopy analysis.

Two (2) samples or thirteen percent (13%), of the fifteen (15) total samples collected for non-parametric statistical testing were selected for split sample analysis which exceeds the 5% minimum required by the LTP.The data were evaluated using USNRC acceptance criteria specified in Inspection Procedure 84750 as detailed in HNP Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey." Split samples 9514-0001-004F/FS were assessed and it was determined that there were low resolution ratios (<4) for both Cs-137 and Co-60. The agreement Revision 0 19 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD range could not be established because NRC Inspection Procedure 84750 does not address resolution ratios below 4. Therefore, a determination of the acceptability for such low rations cannot be made. However, Potassium-40 (K-40) was found to be present at an acceptable level of agreement.

Therefore, no further action was warranted.

Split samples 9514-0001-010F/FS were assessed and it was determined that there was an acceptable level of agreement for Cs-137. Therefore, no further action was warranted.

Due to the extremely low levels of Co-60 reported the same situation was exhibited as was observed for split sample numbers 9514-0001-004F/FS.

The sample analysis vendor, General Engineering Laboratories, LLC, Charleston, South Carolina, maintains quality control and quality assurance plans as part of normal operation.

Refer to Attachment 3 and Attachment 4 for data and data quality analysis results.8. INVESTIGATIONS AND RESULTS Five (5) biased samples were collected at locations along the creek bottom that runs south to north along the eastern edge of the survey unit.Six (6) investigative samples were collected at elevated scan locations throughout the survey unit.Gamma spectroscopy and Sr-90 analyses was performed by the off-site laboratory to the required MDC. None of the samples exceeded 19% of the Operational DCGL. No further action or investigations were required (see Table 8).Table 8- Judgmental and Investigative Sample Results Fraction of the Sample Number (2) Cs-137 Co-60 Sr-90 Oprtoa pCi/g pCi/g pCi/g Operational DCGL(" 9514-0001-024F

-7.30E-03

-1.11E-02

-1.78E-02

-0.023 9514-0001-025F

-8.96E-04

-6.86E-03

-4.16E-03

-0.007 9514-0001-026F 2.35E-02 -7.36E-03

-2.29E-03

-0.001 9514-0001-027F 1.07E-02 1.13E-02 6.32E-03 0.012 9514-0001-028F 1.96E-02 -2.77E-02 5.62E-03 -0.002 9514-0001-029F

-8.66E-03 1.39E-02 -2.46E-02

-0.020 9514-0001-019J 5.22E-01 5.25E-02 7.39E-02 0.188 9514-0001-020J 4.65E-0 1 2.32E-02 3.46E-02 0.128 9514-0001-021J 3.05E-01 9.23E-03 5.01E-02 0.108 9514-0001-022J 5.19E-01 1.53E-02 5.46E-02 0.154 9514-0001-023J 3.34E-01 3.06E-02 6.94E-02 0.140 (1) The Operational DCGLs from Table 2 are 5.38 pCi/g for Cs-137, 2.59 pCi/g for Co-60, 1.05 pCi/g for Sr-90 and are used in conjunction with the unity rule (2)"F" denotes Final Status Survey sample location and "J" denotes Judgmental or Biased sample location.Revision 0 20 Revision 0 20 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD 9. REMEDIATION AND RESULTS Historically, no radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to or as a result of the FSS. Health Physics TSD BCY-HP-0078, "ALARA Evaluation of Soil Remediation in Support of Final Status Survey, " determined that remediation beyond that required to meet the release criteria to be unnecessary and that the remaining residual radioactivity in soil was ALARA.10. CHANGES FROM THE FINAL STATUS SURVEY PLAN Sample location number 9514-0001-008F was deemed inaccessible and was replaced by sample location number 9514-0001-016F.

None other changes to the FSSP were made.11. DATA QUALITY ASSESSMENT (DQA)The DQO sample design and data were reviewed in accordance with Procedure RPM 5.1-23, "Data Quality Assessment," for completeness and consistency.

The sampling design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected.Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 2.The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation).

The standard deviation was slightly less than the value used for the survey design. This would indicate that the number of samples collected was sufficient to meet the Operational DCGL. The mean and median values are well below the Operational DCGL when used in conjunction with the unity rule. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power.Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs.For Cs-137, the range of the data, about four (4) standard deviations, was not a particularly large variation considering that the levels were essentially at existing environmental levels where such variation is to be expected.

The difference between the mean and median was 32% of the standard deviation which indicates some skewness in the data. The data was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot indicates a positive skewness as confirmed by the calculated skew of 3.02.Revision 0 21 Revision 0 21 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD Since Co-60 was not identified (i.e., a result greater than two (2) standard deviations uncertainty) in any of the fifteen (15) samples collected for non-parametric statistical testing, the data was not used to determine the adequacy of statistical testing for this survey unit.For Sr-90, the range of the data, about three (3) standard deviations, was not a particularly large variation considering that the levels were at extremely low levels where such variation is to be expected.

The difference between the mean and median was 36.7% of the standard deviation which indicates a small skewness in the data. The data was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot shows a slightly positive skew as confirmed by the calculated skew of 0.367.All data, assessments, and graphical representations are provided in Attachment 3 and Attachment 4.12. ANOMALIES The anomalies associated with the disagreement between the field splits was presented in Section 7. The source of the disagreement for Co-60 is likely due to extremely low levels of activity being reported and the statistical uncertainties associated with the comparison of very small numbers. Standard statistical tests, ratio comparisons and skew, may not provide the same information at extremely low numbers as compared to higher numbers.No other anomalies were noted.13. CONCLUSION Survey Unit 9514-0001 has met the final DQOs of the FSS plan. The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved.

Elevated Measurement Comparison and remediation was not required.Cs-137 and Sr-90 were used for statistical testing to determine the adequacy of the survey unit for FSS.The sample data passed the Sign Test. The null hypothesis was rejected.

The Retrospective Power Curve generated using COMPASS shows adequate power was achieved.

The survey unit is properly designated as Class 2.The dose contribution from soil is 1.43 mrem/yr TEDE based on the average concentration of the samples used for non-parametric statistical sampling.This survey area is affected by existing groundwater (reference CY memo ISC 06-024); therefore the dose contribution from existing groundwater is two (2)mrem/yr TEDE.This survey unit is not considered impacted by future groundwater radioactive contamination, as there are no buried concrete foundations and footings containing residual radioactive material within the groundwater saturated zone Revision 0 22 Revision 0 22 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD in the area (reference CY memo ISC 06-024); therefore, the dose contribution from future groundwater is zero (0) mrem/yr TEDE.The average total dose from residual radioactivity in this survey unit, including exposures from the three (3) components as described in Section 3, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity, will not exceed 3.43 mrem/yr Total Effective Dose Equivalent (TEDE). Therefore, Survey Unit 9514-0001 is acceptable for unrestricted release.14. ATTACHMENTS 14.1 Attachment 1 -Figures 14.2 Attachment 2 -Scan Results 14.3 Attachment 3 -Laboratory Results 14.4 Attachment 4 -DQA Results Revision 0 23 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 1 (FIGURES)

I 9527-0004 9514-0001 oo527-9504-0000

\2d 9514-0001 J 9514-0001-023J 514-0001-014F 9514-0001-019J 9514-0001-O1IF 99514-0001-OOIF 9514-0001-022J

'9514-0001-003F 9514-0001-007F 9514-0001-010F 9514-0001 13F 9514-0001-025F 514-0001 -0M2F 9514-0001-006F 9514-0001-026F

§9 51 4-0 0 0 1-0 2§ 9 5 14-0 0 0 1-01 2 F 9514-0001-0241' 9514-0001-009 f 9514-0001-0271' 9514-001-015F

• =Pond 0 = P.-d 0 =Sop Loc40io fork Lowlmon EknWodScanL-,M-o 4 s 4o NAD27 C ..ntt 5044 PIan Syntn 9514-0001-005F 9514-0001-016F 9514-0000 9313-0000-4. ________________

L ________________

Figure I Connecticut Yankee Atomic Power Company Sample Location Map for Survey Unit 9514-0001 March 2007 Created by: R- Massengill Revision:

0 9514-000 9527-0001 0.105 0.334 0.3115 0.370 0.522 0.519 0.016 0.064 0.119 0.036 0.062-0.001 0 0 0.050 -0.007 0.040 0.019 0.024 -0.009 0 0.011 0.056 0 9514-0000 I Figure 2 Cesium-137Posting Plot for Surface Soil Samples Survey Unit 9514-0001 "ELd O =Pod 9514-000 9527-0001 0 = N,,-Pr..fnS.,,pi RM~ffsinto pCylg 0.021 o j*MsP RooIt in P M~og 0.009 0.031 0.017 S~pk Res.J. p Ci'g 0.015 0.007 0.002-0.004 ,0.006-0.007 0.008-0.007 0.031 0©0.008 0 0.000 -0.011 0.000 0.011 : 0.005 0 0 40 6 F-9514-0000 NAD27Coý~do St060PY.asyýo~

Figure 3 Cobalt-60 Posting Plot for Surface Soil Samples Survey Unit 9514-0001 9514-000-0O ~N-.o-p S-PI.o J9.fSW R0.ko,, pin Gg 0.069 0.050 0.033 0 Bk,.d Sc..Looto Spic R-ub Mc p Q19 0.055 ,0.004 0.016 0.017 0.033-0.021-0.004 0.681 0 o 0.007-0.002 -0.025 0 o.o6 0.006 0.046 0 9514-0000 0 40 so N.W NAD27CO.c.-a-Ic SSOSPh- Sym~.~Figure 4 Strontium-90 Posting Plot for Surface Soil Samples Survey Unit 9514-0001 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 2 (SCAN RESULTS)

SURVEY UNIT 9514-0001 SAMPLE LOCATION SCAN RESULTS suryLocatonI Log I Log IReading MDCR Action L. >AL I 00 Probe Number Date Time (cpm) (cpm) (cpm) ("+"=Yes)

Serial # Serial #9514-01-BL-00-01-0 2/23/2007 8:47:00 3.26E+03 8.15E+02 4.08E+03 1110 1010 9514-01-SL-00-01-01 2/23/2007 1 8:48:00 [3"98E+031 1110 100 9514-01-BL-00-02-0 2/23/2007 8:45:00 4.04E+03 9.08E+02 4.95E+03 1110 1010 9514-01-SL-00-02-01 2/23/2007 1 8:46:00 4.74E+031 I 1110 j1010 9514-01-BL-00-03-0 2/23/2007 8:49:00 4.95E+03 1.00E+03 5.95E+03 1110 1010 9514-01-SL-00-03-01 2/23/2007 1 8:50:00 14.64E+031 I I I 1110 1010 9514-01-BL-00-04-0 2/23/2007 8:50:00 6.10E+03 1.12E+03 7.22E+03 1110 1010 9514-01-SL-00-04-01 2/23/2007 8:51:00595E+03 1110 I1010 9514-01-BL-00-05-0 2/23/2007 8:44:00 4.60E+03 9.69E+02 5.57E+03 1110 1010 9514-01-SL-00-05-01 2/23/2007 1 8:44:00 14.02E+03 1 110 1010 9514-01-BL-00-06-0 2/23/2007 8:42:00 5.70E+03 1.08E+03 6.78E+03 1110 1010 9514-01-SL-00-06-0 2/23/2007 1 8:43:00 15.38E+03[

1110 11010 9514-01-BL-00-07-0 2/23/2007 8:32:00 5.99E+03 1.11E+03 7.10E+03 1110 1010 9514-01-SL-00-07-01 2/23/2007 1 8:32:00 6.19E+031 I 1110 1010 9514-01-BL-00-09-0 2/23/2007 8:28:00 5.28E+03 1.04E+03 6.32E+03 1110 1010 9514-01-SL-00-09-01 2/23/2007 F 8:28:00 I 6.23E+031 I -1110 1O 010 9514-01-BL-00-10-0 2/23/2007 8:16:00 4.92E+03 1.OOE+03 5.92E+03 1110 1010 9514-01-SL-00-10-0I 2/23/2007 1 8:17:00 1 4.47E+031 I I 1110 o 11o0 9514-01-BL-00-11-0 2/23/2007 8:35:00 6.66E+03 1.17E+03 7.83E+03 1110 1010 9514-01-SL-00-11-0 2/23/2007 8:36:00I5.91E+03I 1 ý Ii 1110 1010 9514-01 -BL-00-1 2-0 2/23/2007 8:19:00 5.12E+03 1.02E+03 6.14E+03 1110 1010 9514-01-SL-00-12-01 2/23/2007 F -8:20:00 j5.25E+03 I I 111 1010 9514-01-BL-00-13-0 2/23/2007 8:23:00 5.16E+03 1.03E+03 6.19E+03 1110 1010 9514-01-SL-00-13-0 2/23/2007 8:24:00 6.76E+03 + 1110 1010 9514-01-BL-00-14-0 2/23/2007 8:25:00 5.62E+03 1.07E+03 6.69E+03 1110 1010 ,9514-01-SL-00-14-01 2/23/2007 1 8:26:00 6.45E+031 I 1110 1010 K:\Survey Area Records\9514\9514-0001

\SCAN DATA\SAMPLESCANRESULTS022807.xlw 1 3/28/2007 SURVEY UNIT 9514-0001 SAMPLE LOCATION SCAN RESULTS Survey Location Log Log Reading MDCR Action L. o>AL I E-600 Probe Number Date Time (cpm) (cpm) (cpm) ("+"=Yes)

Serial # Serial #9514-01-1BL-00-15-0 2/2312007 8:21:00 4.94E+03 1.OOE+03 5.94E+03 1110 1010 9514-01-SL-00-15-01 2/23/2007 18:22:00 5.45E+031 1110 1010 9514-01-BL-00-16-0 2/23/2007 8:40:00 4.71E+03 9.80E+02 5.69E+03 1110 1010 9514-01-SL-00-16-0l 2/23/2007 1 8:41:00 14.93E+031 J1110 1010 9514-01-BL-00-19-0 2/27/2007 10:00:00 5.52E+03 1.06E+03 6.58E+03 1107 1007 9514-01-SL-00-19-01 2/27/2007 1 0:01:0014.79E+031 II I 1107 1007 9514-01-BL-00-20-0 2/27/2007 10:01:00 5.91E+03 1.10E+03 7.01E+03 1107 1007 9514-01 -SL-00-20-0 J 2/27/2007 10:02:001 6.06E+03 111 1 107 1 1007 9514-01-BL-00-21-0 2/27/2007 10:03:00 8.20E+03 1.29E+03 9.49E+03 1107 1007 9514-01-SL-00-21-01 2/27/2007 10:04:00 780E*031_

_ IJ1107 I 1007 9514-01-BL-00-22-0 2/27/2007 10:15:00 8.77E+03 1.34E+03 1.01E+04 1107 1007 9514-01-SL-00-22-01 2/27/2007 10:16:00 18.97E+031

-11071= 1007 9514-01-BL-00-23-0 2/27/2007 10:18:00 8.97E+03 1.35E+03 1.03E+04 1107 1007 9514-01-SL-00-23-01 2/27/2007 110:19:0018.60E+03 1 1 1107 I 1007 K:\Survey Area Records\9514\9514-0001

\SCAN DATA\SAMPLESCANRESULTS022807.xlw 2 3/28/2007 SURVEY UNIT 9514-0001 SCAN AREA SURVEY RESULTS Surve Location Log Log Reading MDCR Action L. >AL E-600 Probe Number Date Time (cpm) (cpm) (cpm) ("+"=Yes)

Serial # Serial #9514-01-BC-01-01-0 2/22/2001 9:51M00 7f15E+03 1.21E+03 8.36E+03 1107 1007 9514-01-SC-01

-01 __2/22/2007 9:55:001 6.04E+03_

1107 1007 5227%66 9-56T00 6.51E03 E1-5E0 766E03 1-107---107-9514-01-SC-01-02-0 2/22/2007 10:00:00 6.OOE+03 I1107 1I 1007 9514-01-BC-01-03-0 2/22/2007 10:01:00 6.34E+03 1.14E+03 7.48E+03 1107 1007 9514-01-SC-01-03-0 2/22/2007 10:06:00 6.47E+03 I 1 1 1107 L 1007 9514-01-BC-01-04-0 2/22/2007 10:07:00 6.59E+03 1.16E+03 7.75E+03 1107 1007 9514-01-SC-01-04-0 I /22/2007 110:09:001 I6"09E+03

-1 1 11607 1007 9514-01-BC-01-05-0 2/22/2007 10:11:00 6.71E+03 1.17E+03 7.88E+03 1107 1007 9514-01-SC-01-05-0 2/22/2007

[10:14:00 1 678E+03 I 1107 1007 9514-01-BC-01-06-0 2/22/2007 10:16:00 6.34E+03 1.14E+03 7.48E+03 1107 1007 9514-01-SC-01-06-0 2/22/2007 10:22:00 1 7.19E+03 I I I 1107 1007 9514-01-BC-02-01-0 2/22/2007 9:49:00 6.12E+03 1.12E+03 7.24E+03 1110 1010 9514-01-SC-02-01-0 2/22/2007 9:53:00 I 6.OOE+03 I I 1110-I 1010 9514-01 -BC-02-02-0 2/22/2007 9:53:00 5.43E+03 1.05E+03 6.48E+03 1110 1010 9514-01-SC-02-02-0 2/22/2007 9:57:00 I 5.98E+03 I I I 1110 I 1010 9514-01-BC-02-03-0 2/22/2007 9:58:00 6.45E+03 1.15E+03 7.60E+03 1110 1010 9514-01 -SC-02-03-0 2/22/2007 10:01:00 5'55E+03 1110 1010 9514-01 -BC-02-04-0 2/22/2007 10:02:00 5.69E+03 1.08E+03 6.77E+03 1110 1010 9514-01-SC-02-04-0 2/22/2007 10:04:001 5"53E+03 I I1110 1010 9514-01-BC-02-05-0 2/22/2007 10:07:00 5.49E+03 1.06E+03 6.55E+03 1110 1010 9514-01-SC-02-05-0 2/22/2007 I10:10:00 5"48E+03 I I 1110 1010 9514-01-BC-03-01-0 2/22/2007 13:14:00 6.32E+03 1.14E+03 7.46E+03 1107 1007 9514-01-SC-03-01-0 2/22/2007 13:29:00 6'85E+03 I I 1107 1007 9514-01-BC-03-02-0 2/22/2007 13:40:00 6.70E+03 1.17E+03 7.87E+03 1107 1007 9514-01-SC-03-02-0 2/22(2007 13:45:00 6"48E+03 1107 1007 9514-01 -BC-03-03-0 2/22/2007 13:48:00 6.71 E+03 1.17E+03 7.88E+03 1107 1007 9514-01-SC-03-03-0 2/22/2007

[13:56:00 6.05E+03 1107 1007 9514-01-BC-03-04-0 2/22/2007 13:57:00 7.13E+03 1.21E+03 8.34E+03 1107 1007 9514-01-SC-03-04-0 2/22/2007 14:00:001 6.41E+03 I 1107 I 1007 K:\Survey Area Records\9514\9514-0001

\SCAN DATA\

SUMMARY

TABLE 022607.xls 1 3/28/2007 SURVEY UNIT 9514-0001 SCAN AREA SURVEY RESULTS Survey Location Log Log Reading MDCR Action L. >AL E-600 Probe Number Date Time (cpm) (cpm) (cpm) ("+"=Yes)

Serial # Serial #9514-01-BC-03-05-0---

2/2212007 14:02:00 6.39E+03 -1.14E+03 7.53E+03 1107 1007 9514-01-s0-03-05-0 2/22/2007 14:05:00 7.19E+03 1107 1007 9514-01-BC-03-06-0 2/22/2007 14:06:00 7.37E+03 1.23E+03 8.60E+03 1107 1007 9514-01-SC-03-06-0 2/22/2007 14:10:001 6.09E+03 1107 L1007 9514-01-BC-03-07-0 2/22/2007 14:14:00 6.02E+03 1.11E+03 7.13E+03 1107 1007 9514-01 -SC-03-07-0 2/22/2007 14:17:00 6.49E+03 1107 1007 9514-01 -BC-03-08-0 2/22/2007 14:18:00 7.87E+03 1.27E+03 9.14E+03 1107 1007 9514-01-SC-03-08-0 2/22/2007 14:21:00 6"24E+03 I II1107 1007 9514-01-BC-03-09-0 2/22/2007 13:15:00 5.13E+03 1.02E+03 6.15E+03 1110 1010 9514-01-SC-03-09-0 2/22/2007 13:31:00 1 4.61E+03 I I I 1110 I 1010 9514-01-ER-03-09-1 2/23/2007 8:10:00 6.24E+03 + 1110 1010 9514-01-BC-03-10-0 2/22/2007 13:35:00 5.42E+03 1.05E+03 6.47E+03 1110 1010 9514-01-SC-03-10-0 2/22/2007 13:42:001 5.46E+03 1I 1110 1010 9514-01-BC-03-11-0 2/22/2007 13:43:00 5.17E+03 1.03E+03 6.20E+03 1110 1010 9514-01-SC-03-11-0 2/22/2007 13:52:00I 5.75E+03I I 1110 1010 9514-01-BC-03-12-0 2/22/2007 13:53:00 5.71 E+03 1.08E+03 6.79E+03 1110 1010 9514-01-SC-03-12-0 I 2/22/2007 13:56:00 I 4.95E+03 I I 1110 1 1010 9514-01 -BC-03-13-0 2/22/2007 13:59:00 5.OOE+03 1.01 E+03 6.01E+03 1110 1010 9514-01-SC-03-13-0 2/22/2007 14:04:001 5.77E+03 I I 1110 1010 9514-01-ER-03-13-1 2/23/2007 8:12:00 6.08E+03 + 1110 1010 9514-01-ER-03-13-2 2/23/2007 8:13:00 7.54E+03 + 1110 1010 9514-01 -BC-03-14-0 2/22/2007 14:06:00 5.74E+03 1.08E+03 6.82E+03 1110 1010 9514-01-S0-03-14-0 2/22/2007 14:09:001 4"86E+03 1 1110 1 10 9514-01-BC-03-15-0 2/23/2007 12:51:00 6.31E+03 1.13E+03 7.44E+03 1110 1010 9514-01-SC-03-15-0 2/23/2007 13:00:001 4.48E+03 1 1110 1010 9514-01-BC-03-16-0 2/23/2007 13:01:00 5.97E+03 1.10E+03 7.07E+03 1110 1010 9514-01-SC-03-16-0

/223/2007 13:05:00 I 6.22E+03 __II_1110 lOlO 9514-01-BC-03-17-0 2/23/2007 13:07:00 5.71E+03 1.08E+03 6.79E+03 1110 1010 9514-01-SC-03-17-0 2/23/2007 13:10:00 1 4.79E+03 I1-i 110 [ 1010 9514-01-BC-03-18-0 2/23/2007 13:12:00 5.16E+03 1.03E+03 6.19E+03 1110 1010 9514-01-sc-03-18-0 2/23/2007 13:15:00 5.84E+03 I I I 1110 1010 9514-01-BC-03-19-0 2/23/2007 13:16:00 5.60E+03 1.07E+03 6.67E+03 1110 1010 9514-01-SC-03-19-0 2/23/2007 13:20:00 5.1 8E+033 I _ I_ 1110 1010 9514-01-BC-03-20-0 2/23/2007 13:21:00 5.72E+03 1.08E+03 6.80E+03 1110 1010 9514-01-SC-03-20-0 2/23/2007 13:25:00 5.42E+03 I } I 1110 I 101 9514-01-BC-03-21-0 2/23/2007 13:26:00 5.73E+03 1.08E+03 6.81 E+03 1110 1010 9514-01-SC-03-21-0 2/23/2007 I 13:29:00 5"35E+03 I 1110 1010 9514-01-BC-03-22-0 2/23/2007 13:31:00 6.66E+03 1.17E+03 7.83E+03 1110 1010 9514-01-SC-03-22-0 2/23/2007 13:34:00 1 5.10E+03 I I 1110 I 1010 K:\Survey Area Records\9514\9514-0001\SCAN DATA\

SUMMARY

TABLE 022607.xls 2 3/28/2007 SURVEY UNIT 9514-0001 SCAN AREA SURVEY RESULTS Surve Location Lo Log Readin MDCR Action L. >AL E-600 Probe Number Date Time (cpm) (cpm) (cpm) ("+"=Yes)

Serial # Serial #9514-01-BC-03-23-0 212312007 12:50:00 6.92E+03 1.19E+03 8.11E+03 -1107 '1007 9514-01-SC-03-23-0 2/23/2007 13:00:00 6.67E+03 I 1107 I 1007 9514-01-ER-03-23-1 2/26/2007 10:09:00 8.43E+03 + 1107 1007 9514-01-BC-03-24-0 2/23/2007 13:00:00 7.40E+03 1.23E+03 8.63E+03 1107 1007 9514-01-SC-03-24-0 2/23/2007 13:04:00 6,83E+03 I I 1107 I 1007 9514-01-BC-03-25-0 2/23/2007 13:06:00 7.01 E+03 1.20E+03 8.21 E+03 1107 1007 9514-01-SC-03-25-0 2/23/2007 13:12:001 6.80E+031 I I I 1107 1 1007 9514-01-ER-03-25-1 2/26/2007 10:12:00 1.38E+04 + 1107 1007 9514-01-BC-03-26-0 2/23/2007 13:12:00 7.19E+03 1.21E+03 8.40E+03 1107 1007 9514-01-SC-03-26-0 2/23/2007 13:18:00l7.215E+03 1 I 1107 1007 9514-01 -ER-03-26-1 2/26/2007 10:16:00 1.72E+04 + 1107 1007 9514-01-BC-03-27-0 2/23/2007 13:19:00 7.52E+03 1.24E+03 8.76E+03 1107 1007 9514-01-SC-03-27-0 2/23/2007 13:23:00 6.71E+03 I 1107 1007 9514-01-BC-03-28-0 2/23/2007 13:26:00 4.76E+03 9.85E+02 5.75E+03 1107 1007 9514-01-SC-03-28-0 2/23/2007 1 13:27:00 1 5.47E+031 I 1107 1007 9514-01-BC-03-29-0 2/23/2007 13:28:00 4.70E+03 9.79E+02 5.68E+03 1107 1007 9514-01 -SC-03-29-0 2/23/2007 13:29:001 5.22E+03 III 1107 1007 9514-01-BC-03-30-0 2/23/2007 13:29:00 4.76E+03 9.85E+02 5.75E+03 1107 1007 9514-01-SC-03-30-0 2/23/2007 13:31:00 4.41E+03 I 1107 1007 9514-01-BC-03-31-0 2/23/2007 13:31:00 4.92E+03 1.00E+03 5.92E+03 1107 1007 9514-01-SC-03-31-0 2/23/2007 13:32:00 4.28E+03 I Ii l 1107 1007 9514-01-BC-03-32-0 2/23/2007 13:32:00 4.91 E+03 1.OOE+03 5.91 E+03 1107 1007 9514-01-SC-03-32-0 2/23/2007 J13:33:00 1 4.57E+03 1 1 I 1107 1007 9514-01-BC-03-33-0 2/23/2007 13:34:00 4.52E+03 9.60E+02 5.48E+03 1107 1007 9514-01-SC-03-33-0 2/23/2007 13:35:00 I-4.97E+03 I I 1107 I 1007 9514-01-BC-03-34-0 2/23/2007 13:35:00 4.77E+03 9.86E+02 5.76E+03 1107 1007 9514-01-SC-03-34-0 12/23/2007 13:36:00 4.77E+03I I 1107 1007 9514-01-BC-03-35-0 2/23/2007 13:37:00 5.05E+03 1.01E+03 6.06E+03 1107 1007 9514-01-SC-03-35-0 2/23/2007 13:38:00 I 4.64E+03 I I I 1107 I 1007 9514-01-BC-03-36-0 2/23/2007 13:39:00 4.90E+03 1.OOE+03 5.90E+03 1107 1007 9514-01-SC-03-36-0 I 2/23/2007 13:39:00]

5.52E+03 1107 1007 9514-01-BC-03-37-0 2/23/2007 13:41:00 5.62E+03 1.07E+03 6.69E+03 1107 1007 9514-01-SC-03-37-0 2/23/2007 I 13:42:00 I 5.35E+03 I j 1107 I 1007 9514-01-BC-03-38-0 2/23/2007 13:42:00 5.21E+03 1.03E+03 6.24E+03 1107 1007 9514-01-SC-03-38-0 2/23/2007 13:43:001 4.71E+03 I I 117 I 1007 9514-01-BC-03-39-0 2/23/2007 13:44:00 5.27E+03 1.04E+03 6.31 E+03 1107 1007 9514-01-SC-03-39-0 2/23/2007 13:45:00 5.87E+03 I I 1107 1007 9514-01-BC-03-40-0 2/23/2007 13:46:00 5.82E+03 1.09E+03 6.91 E+03 1107 1007 9514-01-SC-03-40-0 2/23/2007 113:47:00 5.07E+03 I 1107 1007 K:\Survey Area Records\9514\9514-0001\SCAN DATA\

SUMMARY

TABLE 022607.xls 3 3/28/2007 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 3 (LABORATORY DATA)

Laboratories LLC a member of The GEL Group INC PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com Connecticut Yankee Atomic Power Co.Soils PO# 002332 Work Order: 181554 SDG: MSR#07-00100 Laboratory ID 181554001 181554002 181554003 181554004 181554005 181554006 181554007 181554008 181554009 181554010 181554011 181554012 181554013 181554014 181554015 181554016 181554017 181554018 181554019 181554020 181554021 181554022 181554023 181554024 181554025 181554026 181554027 181554028 Client ID 9514-0001-OO1F 9514-0001-002F 9514-0001-003F 9514-0001-004F 9514-0001-004FS 9514-0001-005F 9514-0001-006F 9514-0001-007F 9514-0001-009F 9514-0001-O0OF 9514-0001-01OFS 9514-0001-O0IF 9514-0001-012F 9514-0001-013F 9514-0001-014F 9514-0001-015F 9514-0001-016F 9514-0001-024F 9514-0001-025F 9514-0001-026F 9514-0001-027F 9514-0001-028F 9514-0001-029F 9514-0001-019J 9514-0001-020J 9514-0001-02IJ 9514-0001-022J 9514-0001-023J nrnhilm cnhivori Table of Contents General Narrative

..................................................................

1 Chain of Custody and Supporting Documentation

...........

5 Data Review Qualifier Definitions

.......................................

12 Radiological Analysis ...........................................................

14 Sample Data Summary ......................................................

38 Q uality C ontrol D ata ...........................................................

98 General Narrative 1 General Narrative for Connecticut Yankee Atomic Power Co.Work Order: 181554 SDG: MSR#07-00100 March 06, 2007 Laboratory Identification:

GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary Sample receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on March 01, 2007 for analysis.Shipping container temperatures were checked, documented, and within specifications.

The samples were delivered with proper chain of custody documentation and signatures.

All sample containers arrived without any visible signs of tampering or breakage.Sample Identification The laboratory received the following samples: Laboratory Identification 181554001 181554002 181554003 181554004 181554005 181554006 181554007 181554008 181554009 181554010 181554011 181554012 181554013 181554014 181554015 181554016 181554017 181554018 181554019 181554020 181554021 181554022 181554023 181554024 181554025 Sample Description 9514-0001-OO1F 9514-0001-002F 9514-0001-003F 9514-0001-004F 9514-0001-004FS 9514-0001-005F 9514-0001-006F 9514-0001-007F 9514-0001-009F 9514-0001-O0OF 9514-0001-OIOFS 9514-0001-01iF 9514-0001-012F 9514-0001-013F 9514-0001-014F 9514-0001-015F 9514-0001-016F 9514-0001-024F 9514-0001-025F 9514-0001-026F 9514-0001-027F 9514-0001-028F 9514-0001-029F 9514-0001-019J 9514-0001-020J GEL Laboratories u.c PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.765.1178 2 www.gol.com 181554026 181554027 181554028 9514-0001-021J 9514-0001-022J 9514-0001-023J Items of Note There are no items to note.Case Narrative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures.

Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package.Analytical Request Twenty-six soil samples were analyzed for FSSGAM and Strontium-90.

Two soil samples were analyzed for FSSALL.Data Package The enclosed data package contains the following sections:

General Narrative, Chain of Custody and Supporting Documentation, Data Review Qualifier Definitions, and data from the following fractions:

Radiochemistry.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl Jones Project Manager GEL Laboratories LLC PO Box 30712 Chadeston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 3 www.gol.com List of current GEL Certifications as of 06 March 2007 State Certification Alaska UST-062 Arizona AZ0668 Arkansas 88-0651 CLIA 42D0904046 California 01 151CA Colorado GenEngLabs Connecticut PH-0169 Dept. of Navy NFESC 413 EPA WG-15J Florida/NELAP E87156 Georgia E87156 (FL/NELAP)

Hawaii N/A Idaho N/A Illinois 200029 Indiana C-SC-01 Kansas E-10332 Kentucky 90129 Louisiana 03046 Maryland 270 Massachusetts M-SCO12 Michigan 9903 Nevada SC12 New Jersey SCO02 New Mexico FL NELAP E87156 New York 11501 North Carolina 233 North Carolina Drinking W 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania 68-00485 South Carolina 10120001/10585001/10120002 Tennessee 02934 Texas TX213-2006A Texas NELAP TI 04704235-06-TX U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah 8037697376 GEL Vermont VT87156 Virginia 00151 Washington C1641 4 Chain of Custody and Supporting Documentation 5

Connecticut Yankee Atomic Power Company Chain of Custody Form 362 Injun Hollow Road, East Hampton, CT 06424 No. 2007-00039 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments: Jack McCarthy 860-267-3924 Media Sample Container Code Type Size-Analytical Lab (Name, City, State): Code &Type General Engineering Laboratories Code 2040 Savage Road Charleston, SC 29407 ATT: Cheryl Jones (843-556-8171)

Priority:

nI 30 D. [-115 D. 0 7 D.Other: _ __l____Sample Designation Date Time 4 Comment, Preservation Lab Sample ID 9514-0001-001F 2/23/07 0930 TS G BP X 9514-0001-002F 2/23/07 0903 TS G BP X 9514-0001-003F 2/23/07 0912 TS G BP X 9514-0001-004F 2/23/07 0905 TS G BP X 9514-0001-004FS 2/23/07 0905 TS G BP X 9514-0001-005F 2/23/07 0903 TS G BP X 9514-0001-006F 2/23/07 0905 TS G BP X 9514-0001-007F 2/23/07 0910 TS G BP X 9514-0001-009F 2/23/07 0911 TS G BP X 9514-0001-01 OF 2/23/07 0917 TS G BP X 9514-0001-010FS 2/23/07 0917 TS G BP X NOTES: PO #: 002332 MSR #: 07-00100 0 LTP QA LI Radwaste QA Li Non QA Samples Shipped Via: Internal Container[ Fed Ex Temp.: 13 Deg. C Li UPS[ Hand Sealed?C5N 1) Relinquished

., Date/Time

2) R ceived Date/Time Custody Seal Intact?.Z'a8Iol, 3.3 BA,,(, ElOte 3) Relinquished By Date/Time 4), ecefived By batefOime N Bill of Lading #5) Relinquished By Date/Time

6) Received By Date/Time Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2007-00040 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments: Jack McCarthy 860-267-3924 Media Sample Container Code Type Size-Analytical Lab (Name, City, State): Code &Type General Engineering Laboratories Code 2040 Savage Road 0 Charleston, SC 29407 ATT: Cheryl Jones (843-556-8171)

Priority:

[1 30 D. E] 15 D. M 7 D. /_"_Sample Designation Date Time I ý -4 Comment, Preservation Lab Sample ID 9514-0001-01 IF 2/23/07 0911 TS G BP X 9514-0001-012F 2/23/07 0920 TS G BP X 9514-0001-013F 2/23/07 0922 TS G BP X 9514-0001-014F 2/23/07 0925 TS G BP X 9514-0001-015F 2/23/07 0920 TS G BP X 9514-0001-016F 2/23/07 0906 TS G BP X 9514-0001-024F 2/23/07 0900 TS G BP X 9514-0001-025F 2/23/07 0901 TS G BP X 9514-0001-026F 2/23/07 0902 TS G BP X NOTES: PO #: 002332 MSR #: 07-00100 [ LTP QA [] Radwaste QA [I Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.: 1_ Deg. C El uPs El Hand Cudy Sealed?(Vy., N 1) Relinquished By C ,, Date/Time

2) Re eived B Date/Time Custody Seal Intact?'Q oo 4.~j'7 1,qo 3/1o-7"7 ,co El Other 3) Relinquished By Date/Time

4) feceived By Date/Time B L N Bill of Lading #5) Relinquished By Date/Time

6) Received By Date/Time Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2007-00041 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments: Jack McCarthy 860-267-3924 Media Sample Container Code Type Size-Analytical Lab (Name, City, State): Code &Type General Engineering Laboratories Code 2040 Savage Road Charleston, SC 29407 1.ATT: Cheryl Jones (843-556-8171)

Priority:

] 30 D. [] 15 D. M 7 D.Other: __Sample Designation Date Time 1 4 L Comment, Preservation Lab Sample ID 9514-0001-027F 2/26/07 1009 TS G BP X 9514-0001-028F 2/26/07 1012 TS G BP X 9514-0001-029F 2/26/07 1016 TS G BP X NOTES: PO #: 002332 MSR #: 07-00100 Z LTP QA LI Radwaste QA El Non QA Samples Shipped Via: Internal Container[ Fed Ex Temp.: _+/- Deg. C Ej ups F- Hand Custody Sealed?T) N 1) Relinquis Date/Time

2) Re ived By Date/Time Custody Seal Intact?3) Relinquished By Date/Time

4) eived By Date/Time Bill other 5) Relinquished By Date/Time

6) Received By Date/Time Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2007-00042 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments: Jack McCarthy 860-267.3924 Media Sample Container Code Type Size-Analytical Lab (Name, City, State): Code &Type General Engineering Laboratories Code 2040 Savage Road Charleston, SC 29407 ATT: Cheryl Jones (843-556-8171)

Priority:["30 D. L] 15 D. 0 7 D.O th e r : _ _ _ _ _ q Sample Designation Date Time L L Comment, Preservation Lab Sample ID 9514-0001-019J 2/27/07 0959 TS G BP X 9514-0001-020J 2/27/07 1002 TS G BP X 9514-0001-021J 2/27/07 1005 TS G BP X 9514-0001-022J 2/27/07 1020 TS G BP X 9514-0001-023J 2/27/07 1023 TS G BP X NOTES: PO #: 002332 MSR #: 07-00100 0 LTP QA LI Radwaste QA E] Non QA Samples Shipped Via: Internal Container 0 Fed Ex Temp.: 1 Deg. C fluPs fi Hand Custody Sealed?N 1) Reli By. Date/Time

2) Rece i.ved By Date/Time Custody Seal Intact?Da-te,`T"m0 q3 [:1 Other 3) Relinquished By Date/Time

4) Rec#ved By "Date/Time Bill _of _Lading_#)Bill of Lading #5) Relinquished By Date/Time

6) Received By Date/Time

-Connecticut Yankee Statement of Work for Analytical Lab Services-cy-ISC-SOW-001 Figure 1. Sample Check-in List.Datefrime'ecived:

3/e/'U L;tf .SDG#: /L (-7 Work Order Number __ *ShippingCcntainerID:

See c-4,-/-'L Chain of Custody# "See -.1" .Custody Seals ouishipping container intact?..

Yes (4No []2. Custody Seals dated and signed? Yes 1J4. No [ ]3. Chain-of-Custody record present? " Yes No [ J* 4. Cooler e c .-, .5. Vermiculitetpacking materials is: Wet [ Dry E 6. " Number of samples in shipping container.

_ _ _- __"__ _""_ _7. Sample holding times exceeded?

Ye [JNof[Ye .f ]N W .A. rpeihave:*

I -~k~~ap@ _--hazard labels 9. Samnples are--good condition leaking-broken -.. have air bubbles 10. Were any anomalies identified in sample receipt?1ii..: Description of anomalies(include sample numbers): ample CustodianLabor

.-..Telephoned to:____ ___ __I 10, 10 /

• ._oFAT 0 oI,/ SAMPLE RECEIPT & REVIEW FORM., .j A ..W. CONTINUATION FORM -0Lo Client: Y4M9K Date Received:

3N0k7 Page g -of .

Zo.7 -Qoo'ý 2 e-7,-11 Data Review Qualifier Definitions 12 Data Review Qualifier Definitions Qualifier Explanation

• A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank 2 Metals-Either presence of analyte detected in the associated blank, or MDL/IDL < sample value < PQL BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample d 5-day BOD-The 2:1 depletion requirement was not met for this sample E Organics-Concentration of the target analyte exceeds the instrument calibration range E Metals-%difference of sample and SD is >10%. Sample concentration must meet flagging criteria H Analytical holding time was exceeded h Preparation or preservation holding time was exceeded J Value is estimated N Metals-The Matrix spike sample recovery is not within specified control limits N Organics-Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest internal standard response factor N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the reporting limit UI Gamma Spectroscopy-Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound z Paint Filter Test-Particulates passed through the filter, however no free liquids were observed.GEL Laboratories LLC P0Box30712 Chafeston, SC 29417 2040 Savae Road Chaflestn, SC29407 P843.555.8171 F843.765.1178 www.gel.com 13 RADIOLOGICAL ANALYSIS 14 Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)Work Order 181554 Method/Analysis Information Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Dry Soil Prep GL-RAD-A-021 Method: Analytical Batch Number: Prep Batch Number: Dry Soil Prep GL-RAD-A-021 Batch Number: Ash Soil Prep Dry Soil Prep 613994 613800 613798 Sample ID 181554001 181554014 1201287982 1201287983 1201287984 1201287985 Client ID 9514-0001-001F 9514-0001-013F Method Blank (MB)181554001(9514-0001-001 F) Sample Duplicate (DUP)181554001(9514-0001-OOIF)

Matrix Spike (MS)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 I REV# 14.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

15 Quality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554001 (9514-0001-001F).

QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis Sample 181554014 (9514-0001-013F) was recounted due to a suspected false positive.Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Manual Integration No manual integrations were performed on data in this batch.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Method/Analysis Information 16 Product: Alphaspec Pu, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- 11-RC Modified Prep Method: Dry Soil Prep GL-RAD-A-021 Method: Analytical Batch Number: Prep Batch Number: Dry Soil Prep GL-RAD-A-021 Batch Number: Ash Soil Prep Dry Soil Prep 613995 613800 613798 Sample ID 181554001 181554014 1201287986 1201287987 1201287988 1201287989 Client ID 9514-0001-001 F 9514-0001-013F Method Blank (MB)181554001(9514-0001-001 F) Sample Duplicate (DUP)181554001(9514-0001-001 F) Matrix Spike (MS)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554001 (9514-0001-001F).

QC Information All of the QC samples met the required acceptance limits.17 Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis Sample 181554001 (9514-0001-001F) was recounted due to a suspected false positive.Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Manual Integration No manual integrations were performed on data in this batch.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Method/Analysis Information Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- 11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 613997 Prep Batch Number: 613800 Dry Soil Prep GL-RAD-A-021 Batch Number: 613798 18 Sample ID Client ID 181554001 9514-0001-001F 181554014 9514-0001-013F 1201287994 Method Blank (MB)1201287995 181554001(9514-0001-OO1F)

Sample Duplicate (DUP)1201287996 181554001(9514-0001-001F)

Matrix Spike (MS)1201287997 Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 9.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554001 (9514-0001-001F).

QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from 19 referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Manual Integration No manual integrations were performed on data in this batch.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Method/Analysis Information Product: Analytical Method: Prep Method: Analytical Batch Number: Prep Batch Number: Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived EML HASL 300, 4.5.2.3 Dry Soil Prep 614269 613798 20 Sample ID 181554001 181554002 181554003 181554004 181554005 181554006 181554007 181554008 181554009 181554010 181554011 181554012 181554013 181554014 181554015 181554016 181554017 181554018 181554019 181554020 1201288621 1201288622 1201288623 Client ID 9514-0001-001F 9514-0001-002F 9514-0001-003F 9514-0001-004F 9514-0001-004FS 9514-0001-005F 9514-0001-006F 9514-0001-007F 9514-0001-009F 9514-0001-O0OF 9514-0001-01OFS 9514-0001-01 IF 9514-0001-012F 9514-0001-013F 9514-0001-014F 9514-0001-015F 9514-0001-016F 9514-0001-024F 9514-0001-025F 9514-0001-026F Method Blank (MB)181554011(9514-0001-01OFS)

Sample Duplicate (DUP)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-0 13 REV# 13.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554011 (9514-0001-01OFS).

21 QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments Additional comments were not required for this sample set.Oualifier information 22 Qualifier UI Reason Data rejected due to interference.

UI Data rejected due to low abundance.

Analyte Cesium-134 Europium-155 Americium-241 Cesium- 134 Cobalt-60 Manganese-54 Silver- 108m Sample 181554014 181554010 181554014 181554011 181554012 181554006 181554007 181554008 181554009 181554010 181554011 181554012 181554013 181554015 181554015 181554017 181554009 181554011 181554011 Method/Analysis Information Product: Analytical Method: Prep Method: Analytical Batch Number: Prep Batch Number: Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived EML HASL 300, 4.5.2.3 Dry Soil Prep 614271 613799 23 Sample ID 181554021 181554022 181554023 181554024 181554025 181554026 181554027 181554028 1201288624 1201288625 1201288627 Client ID 9514-0001-027F 9514-0001-028F 9514-0001-029F 9514-0001-019J 9514-0001-020J 9514-0001-021J 9514-0001-022J 9514-0001-023J Method Blank (MB)181545014(07-LE24-0047)

Sample Duplicate (DUP)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 13.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181545014 (07-LE24-0047).

QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

24 Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments The sample and the duplicate,1201288625 (07-LE24-0047), for TI-208 did not meet the relative percent difference requirement, however they do meet the relative error ratio requirement with value of 2.333.Qualifier information Qualifier Reason Analyte Sample UI UI UI Data rejected due to high peak-width.

Data rejected due to interference.

Data rejected due to low abundance.

Bismuth-212 Cobalt-57 Beryllium-7 Cerium-141 Cesium-134 181554026 1201288624 1201288625 1201288625 181554023 181554025 181554027 1201288625 1201288624 1201288625 Lead-214 Niobium-95 Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Dry Soil Prep GL-RAD-A-021 Method: Analytical Batch Number: Prep Batch Number: Dry Soil Prep GL-RAD-A-021 Batch Number: Ash Soil Prep Dry Soil Prep 613959 613800 613798 25 Sample ID 181554001 181554002 181554003 181554004 181554005 181554006 181554007 181554008 181554009 181554010 181554011 181554012 181554013 181554014 181554015 181554016 181554017 181554018 181554019 181554020 1201287892 1201287893 1201287894 1201287895 Client ID 9514-0001-OO1F 9514-0001-002F 9514-0001-003F 9514-0001-004F 9514-0001-004FS 9514-0001-005F 9514-0001-006F 9514-0001-007F 9514-0001-009F 9514-0001--OOF 9514-0001-O1OFS 9514-0001-O11F 9514-0001-012F 9514-0001-013F 9514-0001-014F 9514-0001-015F 9514-0001-016F 9514-0001-024F 9514-0001-025F 9514-0001-026F Method Blank (MB)181554003(9514-0001-003F)

Sample Duplicate (DUP)181554003(9514-0001-003F)

Matrix Spike (MS)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 11.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (00 Information:

Blank Information The blank volume is representative of the sample volume in this batch.26 Designated QC The following sample was used for QC: 181554003 (9514-0001-003F).

QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Dry Soil Prep GL-RAD-A-021 Method: Analytical Batch Number: Prep Batch Number: Dry Soil Prep GL-RAD-A-021 Batch Number: Ash Soil Prep Dry Soil Prep 613960 613843 613799 27 Sample ED 181554021 181554022 181554023 181554024 181554025 181554026 181554027 181554028 1201287896 1201287897 1201287898 1201287899 Client ID 9514-0001-027F 9514-0001-028F 9514-0001-029F 9514-0001-019J 9514-0001-020J 9514-0001-021J 9514-0001-022J 9514-0001-023J Method Blank (MB)181554022(9514-0001-028F)

Sample Duplicate (DUP)181554022(9514-0001-028F)

Matrix Spike (MS)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 11.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554022 (9514-0001-028F).

QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information 28 All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Method/Analysis Information Product: Liquid Scint Tc99, Solid-ALL FSS Analytical Method: Analytical Batch Number: Sample ID 181554001 181554014 1201288002 1201288003 1201288004 1201288005 DOE EML HASL-300, Tc-02-RC Modified 614001 Client ID 9514-0001-OO1F 9514-0001-013F Method Blank (MB)181554001(9514-0001-001 F) Sample Duplicate (DUP)181554001(9514-0001-OO1F)

Matrix Spike (MS)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 13.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.29 Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volumes in this batch.Designated QC The following sample was used for QC: 181554001 (9514-0001-001F).

QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis Samples 1201288002 (MB), 1201288003 (9514-0001-001F), 181554001 (9514-0001-001F) and 181554014 (9514-0001-013F) were recounted to verify sample results. Second counts being reported..

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Method/Analysis Information 30 Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-1, Modified Prep Method: Dry Soil Prep GL-RAD-A-021 Method: Analytical Batch Number: Prep Batch Number: Dry Soil Prep GL-RAD-A-021 Batch Number: Ash Soil Prep Dry Soil Prep 613996 613800 613798 Sample ID 181554001 181554014 1201287990 1201287991 1201287992 1201287993 Client ID 9514-0001-OO1F 9514-0001-013F Method Blank (MB)181554001(9514-0001-001 F) Sample Duplicate (DUP)181554001(9514-0001-00iF)

Matrix Spike (MS)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554001 (9514-0001-001F).

QC Information All of the QC samples met the required acceptance limits.31 Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Method/Analysis Information Product: Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-1, Modified Prep Method: Dry Soil Prep GL-RAD-A-021 Method: Analytical Batch Number: Prep Batch Number: Dry Soil Prep GL-RAD-A-021 Batch Number: Ash Soil Prep Dry Soil Prep 613999 613800 613798 Sample ID 181554001 181554014 1201287998 1201287999 1201288000 1201288001 Client ID 9514-0001-001F 9514-0001-013F Method Blank (MB)181554001(9514-0001-001 F) Sample Duplicate (DUP)181554001(9514-0001-001 F) Matrix Spike (MS)Laboratory Control Sample (LCS)32 SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554001 (9514-0001-001F).

QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments Additional comments were not required for this sample set.33 Oualifier information Manual qualifiers were not required.Method/Analysis Information Product: LSC, Tritium Dist, Solid -3 pCi/g Analytical Method: Analytical Batch Number: Sample ID 181554001 181554014 1201288006 1201288007 1201288008 1201288009 EPA 906.0 Modified 614003 Client ID 9514-0001-001F 9514-0001-013F Method Blank (MB)181554014(9514-0001-013F)

Sample Duplicate (DUP)181554014(9514-0001-013F)

Matrix Spike (MS)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 13.Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554014 (9514-0001-013F).

QC Information All of the QC samples met the required acceptance limits.34 Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Method/Analysis Information Product: Liquid Scint C14, Solid AII,FSS Analytical Method: Analytical Batch Number: Sample ID 181554001 181554014 1201288010 1201288011 1201288012 1201288013 EPA EERF C-01 Modified 614005 Client ID 9514-0001-OO1F 9514-0001-013F Method Blank (MB)181554014(9514-0001-013F)

Sample Duplicate (DUP)181554014(9514-0001-013F)

Matrix Spike (MS)Laboratory Control Sample (LCS)SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 8.35 Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.Designated QC The following sample was used for QC: 181554014 (9514-0001-013F).

QC Information All of the QC samples met the required acceptance limits.Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.Preparation Information All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysis Samples 1201288011 (9514-0001-013F), 181554001 (9514-0001-001F) and 181554014 (9514-0001-013F) were recounted due to a negative result greater than three times the error.Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents.

A nonconformance report (NCR) was not generated for this SDG.Additional Comments Additional comments were not required for this sample set.Qualifier information Manual qualifiers were not required.Certification Statement 36 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator.

In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.The following data validator verified the information presented in this case narrative:

Reviewer/Date:

C-, 4CL J Ca #ocX 31 3, o-7 37 SAMPLE DATA

SUMMARY

38 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report for YANK001 Connecticut Yankee Atomic Power Co.Client SDG: MSR#07-00100 GEL Work Order: 181554 The Qualifiers in this report are defined as follows:* A quality control analyte recovery is outside of specified acceptance criteria** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the detection limit.The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures.

Please direct any questions to your Project Manager, Cheryl Jones.Reviewed by 39 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Report Date: March 8, 2007 Project: Soils PO# 002332 Client Sample ID: 9514-0001-OOIF Project: YANK01204 Sample ID: 181554001 Client ID: YANK001 Matrix: TS Vol. Recv.: Collect Date: 23-FEB-07 Receive Date: 01-MAR-07 Collector:

Client Moisture:

5.6%Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U Curium-242 U Curium-243/244 U Alphaspec Pu, Solid-ALL FSS Plutonium-238 U Plutonium-239/240 U Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 0.027 +/-0.101 0.0714 +/-0.101 0.0292 +/-0.0572 0.00 +/-0.0573 0.0563 +/-0.119 0.0757 +/-0.119-0.0213 +/-0.106 0.099 +/-0.106 0.0612 +/-0.138 0.0895 +/-0.139 1.13 +/-7.38 6.14 +/-7.38 0.219 0.0791 0.228 0.288 0.269 13.0 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MXA 03/03/07 1706 613994 1 MXA M MXA I 03/08/07 0958 613995 03/05/07 2211 613997 Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.229 +/-0.111 Americium-241 U -0.00525 +/-0.0639 Bismuth-212 U 0.147 +/-0.140 Bismuth-214 0.227 +/-0.0551 Cesium-134 U 0.0203 +/-0.0176 Cesium-137 U 0.0271 +/-0.0199 Cobalt-60 U 0.00288 +/-0.0172 Europium-152 0.344 +/-0.0676 Europium-154 U 0.0102 +/-0.0518 Europium-155 U 0.0211 +/-0.0463 Lead-212 0.257 +/-0.0424 Lead-214 0.268 +/-0.0569 Manganese-54 U -0.0141 +/-0.0164 Niobium-94 U 0.00364 +/-0.0146 Potassium-40 4.88 +/-0.604 Radium-226 0.227 +/-0.0551 Silver-108m U -0.00662 +/-0.0129 Thallium-208 0.0699 +/-0.0243 Rad Gas Flow Proportional Counting 0.0511 0.0631 0.130 0.0268 0.0171 0.0145 0.015 0.0342 0.0452 0.0451 0.0201 0.0252 0.0136 0.013 0.130 0.0268 0.0113 0.0149+/-0.111+/-0.0639+/-0.140+/-0.0551+/-0.0176+/-0.0199+/-0.0172+/-0.0676+/-0.0518+/-0.0463+/-0.0424+/-0.0569+/-0.0164+/-0.0146+/-0.604+/-0.0551+/-0.0129+/-0.0243 0.102 0.126 0.260 0.0535 0.0342 0.029 0.0299 0.0683 0.0904 0.0902 0.0402 0.0504 0.0271 0.0259 0.259 0.0535 0.0225 0.0297 0.0414 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MJHI 03/05/07 1020 614269 KSD1 03/06/07 1616 613959 GFPC, Sr90, solid-ALL FSS Strontium-90 U-0.000887

+/-0.0206 0.0174 +/-0.0206 40 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: 9514-0001-OOIF 181554001 Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid -3 pCi/g Tritium U 0.330 Liquid Scint C14, Solid AII,FSS Carbon- 14 U -0.0471 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 30.3 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -7.41 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.221 Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%+/-1.23 1.02 +/-1.23 2.12 0.154+/-0.0885 0.0753 +/-0.0885+/-45.6 29.4 +/-45.6 62.0+/-7.32 6.50 +/-7.32 13.7+/-0.245 0.200 +/-0.245 0.411 pCi/g pCi/g pCi/g pCi/g pCi/g AXD2 03/03/07 0040 614003 AXD2 03/05/07 1153 614005 MXPI 03/07/07 1010 613996 MXP1 03/06/07 1446 613999 MXP1 03/03/07 2013 614001 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EML HASL 300, 4.5.2.3 5 EPA 905.0 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 EPA EERF C-01 Modified 9 DOE RESL Fe-1, Modified 10 DOE RESL Ni-1, Modified 11 DOE EML HASL-300, Tc-02-RC Modified 12 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Americium-243 Tracer Americium-243 Tracer Plutonium-242 Tracer Alphaspec Am241, Cm, Solid ALL Alphaspec Am241, Cm, Solid ALL Alphaspec Pu, Solid-ALL FSS 88 88 80 (15%-125%)

(15%-125%)

(15%-125%)

41 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: 9514-0001-OOIF 181554001 Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch N Plutonium-242 Tracer Plutonium-241 Plutonium-242 Tracer Plutonium-242 Tracer Strontium Carrier Strontium Carrier Iron-59 Tracer Iron-59 Tracer Nickel Carrier Nickel Carrier Technetium-99 Technetium-99m Tracer Technetium-99m Tracer Alphaspec Pu, Solid-ALL FSS Liquid Scint Pu241, Solid-ALL F5 Liquid Scint Pu241, Solid-ALL FS Liquid Scint Pu241, Solid-ALL FS GFPC, Sr90, solid-ALL FSS GFPC, Sr90, solid-ALL FSS Liquid Scint Fe55, Solid-ALL FS Liquid Scint Fe55, Solid-ALL FS Liquid Scint Ni63, Solid-ALL FS Liquid Scint Ni63, Solid-ALL FS Liquid Scint Tc99, Solid-ALL FS Liquid Scint Tc99, Solid-ALL FS Liquid Scint Tc99, Solid-ALL FS 80 89 89 89 71 71 66 66 100 100 76 76 76 (15%-125%)

(25%-125%)

(25%-125%)

(25%-125%)

(25%-125%)

(25%-125%)

(15%-125%)

(15%-125%)

(25%-125%)

(25%-125%)

(15%-125%)

(15%-125%)

(15%-125%)

Notes: The Qualifiers in this report are defined as follows** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.42 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-002F 181554002 TS 23-FEB-07 01-MAR-07 Client 11.9%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.583 +/-0.139 0.0551 +/-0.139 0.110 pCi/g MJHI 03/05/07 1021 614269 Americium-241 U -0.00801 +/-0.0643 0.0521 +/-0.0643 0.104 pCi/g Bismuth-212 0.361 +/-0.237 0.118 +/-0.237 0.237 pCi/g Bismuth-214 0.362 +/-0.0914 0.0295 +/-0.0914 0.059 pCi/g Cesium-134 U 0.0308 +/-0.0266 0.0202 +/-0.0266 0.0403 pCi/g Cesium-137 0.0623 +/-0.0288 0.0153 +/-0.0288 0.0306 pCi/g Cobalt-60 U 0.00782 +/-0.0224 0.0195 +/-0.0224 0.0389 pCi/g Europium-152 U 0.038 +/-0.0429 0.0439 +/-0.0429 0.0877 pCi/g Europium-154 U -0.0436 +/-0.0638 0.0492 +/-0.0638 0.0984 pCi/g Europium-155 U 0.0292 +/-0.0523 0.048 +/-0.0523 0.0959 pCi/g Lead-212 0.537 +/-0.0633 0.0233 +/-0.0633 0.0465 pCi/g Lead-214 0.427 +/-0.0805 0.0291 +/-0.0805 0.0583 pCi/g Manganese-54 U -0.00035 +/-0.0195 0.0169 +/-0.0195 0.0338 pCi/g Niobium-94 U -0.013 +/-0.0193 0.0153 +/-0.0193 0.0307 pCi/g Potassium-40 9.93 +/-0.935 0.131 +/-0.935 0.262 pCi/g Radium-226 0.362 +/-0.0914 0.0295 +/-0.0914 0.059 pCi/g Silver-108m U -0.00619 +/-0.0177 0.0151 +/-0.0177 0.0302 pCi/g Thallium-208 0.136 +/-0.0439 0.0159 +/-0.0439 0.0317 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, solid-ALL FSS Strontium-90 U -0.0205 +/-0.0201 0.0202 +/-0.0201 0.0471 pCi/g KSD1 03/06/07 1616 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 43 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 -www.gel.com UPrtifie2ti~

nf Analvsi FPXtjfJ*Lr1q1R_(ALAn Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: 9514-0001-002F 181554002 Project: Client ID: Vol. Recv.: YANKO 1204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1A Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier Strontium Carrier GFPC, Sr9O, solid-ALL FSS GFPC, Sr9O, solid-ALL FSS 57 57 (25%-125%)

(25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.13D Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.44 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-003F 181554003 TS 23-FEB-07 01-MAR-07 Client.419%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1A Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.473 +/-0.118 0.0398 +/-0.118 0.0796 pCi/g MJH1 03/05/07 1022 614269 Americium-241 U 0.0213 +/-0.0847 0.0734 +/-0.0847 0.147 pCi/g Bismuth-212 0.441 +/-0.347 0.0923 +/-0.347 0.185 pCi/g Bismuth-214 0.348 +/-0.0644 0.024 +/-0.0644 0.0479 pCi/g Cesium-134 U 0.0159 +/-0.0207 0.0153 +/-0.0207 0.0306 pCi/g Cesium-137 U 0.0157 +/-0.0152 0.014 +/-0.0152 0.0279 pCi/g Cobalt-60 U 0.00703 +/-0.0144 0.013 +/-0.0144 0.026 pCi/g Europium-152 U -0.0203 +/-0.0466 0.0318 +/-0.0466 0.0636 pCi/g Europium-154 U-0.000222

+/-0.0447 0.0381 +/-0.0447 0.0761 pCi/g Europium-155 U 0.0382 +/-0.0453 0.0427 +/-0.0453 0.0853 pCi/g Lead-212 0.431 +/-0.0516 0.0201 +/-0.0516 0.0403 pCi/g Lead-214 0.422 +/-0.0666 0.0232 +/-0.0666 0.0464 pCi/g Manganese-54 U 0.00505 +/-0.0138 0.0125 +/-0.0138 0.0249 pCi/g Niobium-94 U 0.0132 +/-0.0139 0.0126 +/-0.0139 0.0251 pCi/g Potassium-40 9.99 +/-0.843 0.0956 +/-0.843 0.191 pCi/g Radium-226 0.348 +/-0.0644 0.024 +/-0.0644 0.0479 pCi/g Silver-108m U -0.00707 +/-0.0129 0.0111 +/-0.0129 0.0222 pCi/g Thallium-208 0.137 +/-0.0391 0.0116 +/-0.0391 0.0231 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.00352 +/-0.0252 0.0207 +/-0.0252 0.0475 pCi/g KSD1 03/06/07 1616 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1037 613798 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 45 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-003F Project: YANK01204 Sample ID: 181554003 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 70 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 70 (25%-125%)

Notes: The Qualifiers in this report are defined as follows** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.46 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-004F 181554004 TS 23-FEB-07 01-MAR-07 Client 9.7%Proiect: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.541 +/-0.158 0.0561 +/-0.158 0.112 pCi/g MJHI 03/05/07 1023 614269 Americium-241 U 0.0601 +/-0.062 0.0523 +/-0.062 0.105 pCi/g Bismuth-212 U 0.331 +/-0.315 0.172 +/-0.315 0.344 pCi/g'Bismuth-214 0.352 +/-0.0847 0.0345 +/-0.0847 0.0689 pCi/g Cesium-134 U 0.0373 +/-0.026 0.0245 +/-0.026 0.049 pCi/g Cesium-137 0.105 +/-0.050 0.0196 +1-0.050 0.0392 pCi/g Cobalt-60 U 0.0206 +/-0.0226 0.0208 +/-0.0226 0.0415 pCi/g Europium-152 U -0.0273 +/-0.0671 0.0469 +/-0.0671 0.0937 pCi/g Europium-154 U -0.0201 +/-0.0656 0.0531 +/-0.0656 0.106 pCi/g Europium-155 U 0.0766 +/-0.0694 0.0512 +/-0.0694 0.102 pCi/g Lead-212 0.492 +/-0.0696 0.027 +/-0.0696 0.0539 pCi/g Lead-214 0.426 +/-0.0893 0.0357 +/-0.0893 0.0714 pCi/g Manganese-54 U 0.0039 +/-0.0228 0.020 +/-0.0228 0.040 pCi/g Niobium-94 U -0.015 +/-0.0192 0.015 +/-0.0192 0.030 pCi/g Potassium-40 10.4 +/-0.992 0.158 +/-0.992 0.315 pCi/g Radium-226 0.352 +/-0.0847 0.0345 +/-0.0847 0.0689 pCi/g Silver-108m U -0.00146 +/-0.0229 0.0183 +/-0.0229 0.0366 pCi/g Thallium-208 0.169 +/-0.0342 0.0167 +/-0.0342 0.0334 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 0.0464 +/-0.0297 0.0182 +/-0.0298 0.0433 pCi/g KSDI 03/06/07 1616 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 47 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-004F Proiect: YANK01204 Sample ID: 181554004 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 77 (25%-125%)

Strontium Carrier GFPC, Sr9O, solid-ALL FSS 77 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.48 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-004FS 181554005 TS 23-FEB-07 01-MAR-07 Client 9%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1A Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.432 +/-0.225 0.0848 +/-0.225 0.170 pCi/g MJHI 03/05/07 1024 614269 Americium-241 U 0.0472 +/-0.0358 0.0296 +/-0.0358 0.0591 pCi/g Bismuth-212 0.535 +/-0.276 0.122 +/-0.276 0.244 pCi/g Bismuth-214 0.402 +/-0.110 0.0417 +/-0.110 0.0833 pCi/g Cesium-134 U 0.0167 +/-0.0315 0.0284 +/-0.0315 0.0568 pCi/g Cesium-137 0.151 +/-0.0497 0.0245 +/-0.0497 0.0489 pCi/g Cobalt-60 U 0.0265 +/-0.0334 0.0307 +/-0.0334 0.0613 pCi/g Europium-152 U -0.0531 +/-0.0749 0.0486 +/-0.0749 0.0972 pCi/g Europium-154 U -0.00853 +/-0.0985 0.0811 +/-0.0985 0.162 pCi/g Europium-155 U 0.0316 +/-0.0576 0.0472 +/-0.0576 0.0944 pCi/g Lead-212 0.358 +/-0.0822 0.0335 +/-0.0822 0.067 pCi/g Lead-214 0.354 +/-0.0886 0.0388 +/-0.0886 0.0775 pCi/g Manganese-54 U -0.0119 +/-0.0284 0.0234 +/-0.0284 0.0467 pCi/g Niobium-94 U -0.0108 +/-0.0242 0.0201 +/-0.0242 0.0402 pCi/g Potassium-40 11.1 +/-1.09 0.169 +/-1.09 0.338 pCi/g Radium-226 0.402 +/-0.110 0.0417 +/-0.110 0.0833 pCi/g Silver-108m U -0.0152 +/-0.0227 0.0183 +/-0.0227 0.0366 pCi/g Thallium-208 0.171 +/-0.0599 0.022 +/-0.0599 0.044 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 0.0776 +/-0.0346 0.0204 +/-0.0347 0.047 pCi/g KSDI 03/06/07 1616 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 49 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-004FS Project: YANK01204 Sample ID: 181554005 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 74 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 74 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.50 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-005F 181554006 TS 23-FEB-07 01-MAR-07 Client 4.63%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.549 Americium-241 U 0.0391 Bismuth-212 0.420 Bismuth-214 0.421 Cesium-134 UI 0.00 Cesium-137 0.0504 Cobalt-60 U 0.000247 Europium-152 U 0.0306 Europium-154 U 0.000487 Europium-155 U 0.042 Lead-212 0.525 Lead-214 0.466 Manganese-54 U 0.00475 Niobium-94 U 0.00256 Potassium-40 9.47 Radium-226 0.421 Silver-108m U 0.00359 +Thallium-208 0.153 Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.00928+/-0.106+/-0.0596+/-0.141+/-0.0588+/-0.0163+/-0.0182+/-0.0104+/-0.0498+/-0.0348+/-0.0389+/-0.0503+/-0.057+/-0.014+/-0.0116+/-0.766+/-0.0588/-0.00922+/-0.0248 0.0294 0.0496 0.0651 0.0165 0.0109 0.00886 0.00868 0.0249 0.0293 0.0284 0.0139 0.0171 0.00916 0.00859 0.0826 0.0165+/-0.106+/-0.0596+/-0.141+/-0.0588+/-0.0163+/-0.0182+/-0.0104+/-0.0498+/-0.0348+/-0.0389+/-0.0503+/-0.057+/-0.014+/-0.0116+/-0.766+/-0.0588 0.0588 0.0991 0.130 0.033 0.0217 0.0177 0.0174 0.0498 0.0585 0.0567 0.0279 0.0343 0.0183 0.0172 0.165 0.033 0.0164 0.0172 0.0431 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MJH1 03/05/07 1333 614269 KSD1 03/06/07 1616 613959 0.00818 +/-0.00922 0.00858 +/-0.0248+/-0.0234 0.0181 +/-0.0234 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 51 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-005F Project: YANK01204 Sample ID: 181554006 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 75 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 75 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.52 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-006F 181554007 TS 23-FEB-07 01-MAR-07 Client 5.72%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1A Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.564 +/-0.103 0.0312 +/-0.103 0.0624 pCi/g MJHI 03/05/07 1333 614269 Americium-241 U 0.0469 +/-0.0515 0.0434 +/-0.0515 0.0868 pCi/g Bismuth-212 0.405 +/-0.134 0.0654 +/-0.134 0.131 pCi/g Bismuth-214 0.482 +/-0.0647 0.0166 +/-0.0647 0.0332 pCi/g Cesium-1 34 UI 0.00 +/-0.0141 0.0106 +/-0.0141 0.0211 pCi/g Cesium-137 0.0402 +/-0.0193 0.0084 +/-0.0193 0.0168 pCi/g Cobalt-60 U 0.0076 +/-0.0108 0.00888 +/-0.0108 0.0178 pCi/g Europium-152 U -0.038 +/-0.0306 0.0225 +/-0.0306 0.045 pCi/g Europium-154 U -0.0238 +/-0.034 0.0275 +/-0.034 0.0549 pCi/g Europium-155 U 0.0285 +/-0.0326 0.0271 +/-0.0326 0.0543 pCi/g Lead-212 0.534 +/-0.0486 0.0126 +/-0.0486 0.0252 pCi/g Lead-214 0.492 +/-0.0584 0.0163 +/-0.0584 0.0325 pCi/g Manganese-54 U 0.00553 +/-0.0103 0.00919 +/-0.0103 0.0184 pCi/g Niobium-94 U 0.0119 +/-0.0097 0.00858 +/-0.0097 0.0172 pCi/g Potassium-40 9.45 +/-0.715 0.0736 +/-0.715 0.147 pCi/g Radium-226 0.482 +/-0.0647 0.0166 +/-0.0647 0.0332 pCi/g Silver-108m U 0.00167 +/-0.00949 0.00765 +/-0.00949 0.0153 pCi/g Thallium-208 0.169 +/-0.026 0.00867 +/-0.026 0.0173 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 0.681 +/-0.0845 0.0195 +/-0.0864 0.0465 pCi/g KSD1 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 53 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-006F Project: YANK01204 Sample ID: 181554007 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 66 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 66 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.54 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-007F 181554008 TS 23-FEB-07 01-MAR-07 Client 9.67%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.808 +/-0.126 0.0324 +/-0.126 0.0647 pCi/g MJHI 03/05/07 1334 614269 Americium-241 U 0.0505 +/-0.0579 0.0443 +/-0.0579 0.0885 pCi/g Bismuth-212 0.486 +/-0.139 0.071 +/-0.139 0.142 pCi/g Bismuth-214 0.571 +/-0.0689 0.0179 +/-0.0689 0.0358 pCi/g Cesium-134 UI 0.00 +/-0.0183 0.0125 +/-0.0183 0.025 pCi/g Cesium-137 0.0641 +/-0.023 0.00988 +/-0.023 0.0198 pCi/g Cobalt-60 U 0.00166 +/-0.0113 0.00954 +/-0.0113 0.0191 pCi/g Europium-152 U 0.00825 +/-0.041 0.025 +/-0.041 0.050 pCi/g Europium-154 U -0.018 +/-0.0391 0.0269 +/-0.0391 0.0537 pCi/g Europium-155 U 0.0291 +/-0.0402 0.0289 +/-0.0402 0.0577 pCi/g Lead-212 0.782 +/-0.0675 0.0147 +/-0.0675 0.0293 pCi/g Lead-214 0.593 +/-0.069 0.0175 +/-0.069 0.035 pCi/g Manganese-54 U -0.00894 +/-0.0135 0.010 +/-0.0135 0.020 pCi/g Niobium-94 U 0.0128 +/-0.0116 0.00907 +/-0.0116 0.0181 pCi/g Potassium-40 11.0 +/-0.869 0.0803 +/-0.869 0.161 pCi/g Radium-226 0.571 +/-0.0689 0.0179 +/-0.0689 0.0358 pCi/g Silver-108m U -0.00979 +/-0.0102 0.00855 +/-0.0102 0.0171 pCi/g Thallium-208 0.257 +/-0.034 0.00912 +/-0.034 0.0182 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0158 +/-0.0266 0.0201 +/-0.0267 0.0469 pCi/g KSDI 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1037 613798 The following Analytical Methods were performed Method Description 1 EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 55 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-007F Proiect: YANK01204 Sample ID: 181554008 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Notes: The Qualifiers in this report are defined as follows** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.56 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-009F 181554009 TS 23-FEB-07 01-MAR-07 Client 2.92%Project: Client ID: Vol. Recv.: YANKO 1204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.521 +/-0.0902 0.0278 +/-0.0902 0.0555 pCi/g MJHI 03/05/07 1335 614269 Americium-241 U 0.034 +/-0.0315 0.0264 +/-0.0315 0.0528 pCi/g Bismuth-212 0.401 +/-0.123 0.0613 +/-0.123 0.123 pCi/g Bismuth-214 0.479 +/-0.0593 0.0154 +/-0.0593 0.0308 pCi/g Cesium-134 UI 0.00 +/-0.0171 0.0102 +/-0.0171 0.0205 pCi/g Cesium-137 0.0249 +/-0.0124 0.0079 +/-0.0124 0.0158 pCi/g Cobalt-60 U 0.00594 +/-0.00965 0.0084 +/-0.00965 0.0168 pCi/g Europium-152 U 0.0114 +/-0.0304 0.0226 +/-0.0304 0.0452 pCi/g Europium-154 U -0.0236 +/-0.0315 0.0253 +/-0.0315 0.0506 pCi/g Europium-155 U 0.0329 +/-0.0334 0.0224 +/-0.0334 0.0447 pCi/g Lead-212 0.552 +/-0.0503 0.0123 +/-0.0503 0.0247 pCi/g Lead-214 0.573 +/-0.0604 0.0147 +/-0.0604 0.0294 pCi/g Manganese-54 UI 0.00 +/-0.0153 0.00864 +/-0.0153 0.0173 pCi/g Niobium-94 U 0.00631 +/-0.00909 0.00787 +/-0.00909 0.0157 pCi/g Potassium-40 9.48 +/-0.668 0.0706 +/-0.668 0.141 pCi/g Radium-226 0.479 +/-0.0593 0.0154 +/-0.0593 0.0308 pCi/g Silver-108m U 0.000548 +/-0.00844 0.00742 +/-0.00844 0.0148 pCi/g Thallium-208 0.165 +/-0.0248 0.0081 +/-0.0248 0.0162 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0258 +/-0.0283 0.0199 +/-0.0283 0.047 pCi/g KSD1 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1037 613798 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 57 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-009F Proiect: YANK01204 Sample ID: 181554009 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.58 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-O0OF 181554010 TS 23-FEB-07 01-MAR-07 Client 5.13%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch IN Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.613 +/-0.0924 0.0227 +/-0.0924 0.0454 pCi/g MJH1 03/05/07 1335 614269 Americium-241 U 0.0505 +/-0.0501 0.0427 +/-0.0501 0.0852 pCi/g Bismuth-212 0.348 +/-0.147 0.051 +/-0.147 0.102 pCi/g Bismuth-214 0.544 +/-0.0657 0.0135 +/-0.0657 0.027 pCi/g Cesium-134 UI 0.00 +/-0.0136 0.00833 +/-0.0136 0.0167 pCi/g Cesium-137 0.0359 +/-0.0112 0.00669 +/-0.0112 0.0134 pCi/g Cobalt-60 U -0.00376 +/-0.00824 0.00692 +/-0.00824 0.0138 pCi/g Europium-152 U -0.015 +/-0.0246 0.0181 +/-0.0246 0.0362 pCi/g Europium-154 U -0.00414 +/-0.0258 0.0222 +/-0.0258 0.0443 pCi/g Europium-155 UI 0.00 +/-0.0347 0.0227 +/-0.0347 0.0453 pCi/g Lead-212 0.622 +/-0.0551 0.011 +/-0.0551 0.022 pCi/g Lead-214 0.583 +/-0.0604 0.0133 +/-0.0604 0.0265 pCi/g Manganese-54 U 0.0123 +/-0.0123 0.00635 +/-0.0123 0.0127 pCi/g Niobium-94 U 0.00134 +/-0.00776 0.00663 +/-0.00776 0.0132 pCi/g Potassium-40 10.6 +/-0.698 0.059 +/-0.698 0.118 pCi/g Radium-226 0.544 +/-0.0657 0.0135 +/-0.0657 0.027 pCi/g Silver-108m U -0.00882 +/-0.00811 0.00615 +/-0.00811 0.0123 pCi/g Thallium-208 0.180 +/-0.024 0.00665 +/-0.024 0.0133 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.033 +/-0.0292 0.0202 +/-0.0292 0.0468 pCi/g KSDI 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 59 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-01OF Project: YANK01204 Sample ID: 181554010 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 62 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 62 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.60 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis L Certficae of alvIs Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: 9514-0001-OIOFS Project: YANK01204 Sample ID: 181554011 Client ID: YANKOO Matrix: TS Vol. Recv.: Collect Date: 23-FEB-07 Receive Date: 01-MAR-07 Collector:

Client Moisture:

5.07%Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.663 +/-0.105 0.0327 +/-0.105 0.0653 pCi/g MJH1 03/05/07 1336 614269 Americium-241 UI 0.00 +/-0.0338 0.0283 +/-0.0338 0.0567 pCi/g Bismuth-212 0.358 +/-0.133 0.0706 +/-0.133 0.141 pCi/g Bismuth-214 0.584 +/-0.066 0.0177 +/-0.066 0.0354 pCi/g Cesium-134 UI 0.00 +/-0.0198 0.0119 +/-0.0198 0.0237 pCi/g Cesium-137 0.0286 +/-0.0158 0.00957 +/-0.0158 0.0191 pCi/g Cobalt-60 U 0.0087 +/-0.0112 0.00977 +/-0.0112 0.0195 pCi/g Europium-152 U -0.00597 +/-0.0342 0.0262 +/-0.0342 0.0525 pCi/g Europium-154 U -0.0172 +/-0.0317 0.0257 +/-0.0317 0.0515 pCi/g Europium-155 U 0.0355 +/-0.0322 0.0267 +/-0.0322 0.0533 pCi/g Lead-212 0.601 +/-0.057 0.0145 +/-0.057 0.029 pCi/g Lead-214 0.688 +/-0.0705 0.0186 +/-0.0705 0.0372 pCi/g Manganese-54 UI 0.00 +/-0.0192 0.0102 +/-0.0192 0.0204 pCi/g Niobium-94 U -0.00829 +/-0.0107 0.00875 +/-0.0107 0.0175 pCi/g Potassium-40 9.85 +/-0.733 0.0742 +/-0.733 0.148 pCi/g Radium-226 0.584 +/-0.066 0.0177 +/-0.066 0.0354 pCi/g Silver-108m UI 0.00 +/-0.0186 0.00914 +/-0.0186 0.0183 pCi/g Thallium-208 0.222 +/-0.0307 0.00868 +/-0.0307 0.0174 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, solid-ALL FSS Strontium-90 U -0.0146 +/-0.0212 0.020 +/-0.0212 0.0463 pCi/g KSDI 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified 61 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-OIOFS Project: YANK01204 Sample ID: 181554011 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 63 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 63 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.62 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Certificateof Analvsis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-01 IF 181554012 TS 23-FEB-07 01-MAR-07 Client 2.19%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1A Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.753 +/-0.125 0.0409 +/-0.125 0.0818 pCi/g MJH1 03/05/07 1337 614269 Americium-241 UI 0.00 +/-0.0206 0.0168 +/-0.0206 0.0336 pCi/g Bismuth-212 0.424 +/-0.169 0.0888 +/-0.169 0.178 pCi/g Bismuth-214 0.702 +/-0.092 0.0226 +/-0.092 0.0452 pCi/g Cesium-] 34 UI 0.00 +/-0.0307 0.0159 +/-0.0307 0.0317 pCi/g Cesium-137 0.370 +/-0.0468 0.0121 +/-0.0468 0.0241 pCi/g Cobalt-60 U 0.0169 +/-0.0182 0.016 +/-0.0182 0.0319 pCi/g Europium-152 U -0.0111 +/-0.0488 0.0286 +/-0.0488 0.0572 pCi/g Europium-154 U -0.0414 +/-0.0502 0.0398 +/-0.0502 0.0795 pCi/g Europium-155 U 0.0236 +/-0.0342 0.0257 +/-0.0342 0.0513 pCi/g Lead-212 0.749 +/-0.0734 0.0155 +/-0.0734 0.0309 pCi/g Lead-214 0.714 +/-0.0823 0.0208 +/-0.0823 0.0415 pCi/g Manganese-54 U -0.00128 +/-0.0145 0.0125 +/-0.0145 0.0249 pCi/g Niobium-94 U -0.0117 +/-0.013 0.011 +/-0.013 0.0219 pCi/g Potassium-40 10.4 +/-0.588 0.123 +/-0.588 0.246 pCi/g Radium-226 0.702 +/-0.092 0.0226 +/-0.092 0.0452 pCi/g Silver-108m U 0.00224 +/-0.012 0.0104 +/-0.012 0.0208 pCi/g Thallium-208 0.264 +/-0.0397 0.0108 +/-0.0397 0.0216 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0326 +/-0.0291 0.0201 +/-0.0292 0.0468 pCi/g KSD1 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1037 613798 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 63 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-01 IF Project: YANK01204 Sample ID: 181554012 Client ID: YANKOO Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 82 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 82 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.64 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-012F 181554013 TS 23-FEB-07 01-MAR-07 Client 5.34%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.545 +/-0.102 0.0292 +/-0.102 0.0584 pCi/g MJHI 03/05/07 1422 614269 Americium-241 U 0.0447 +/-0.0499 0.0411 +/-0.0499 0.0821 pCi/g Bismuth-212 0.392 +/-0.184 0.0672 +/-0.184 0.134 pCi/g Bismuth-214 0.581 +/-0.0677 0.0166 +/-0.0677 0.0332 pCi/g Cesium-134 UI 0.00 +/-0.0185 0.0107 +/-0.0185 0.0215 pCi/g Cesium-137 0.0555 +/-0.0241 0.00878 +/-0.0241 0.0176 pCi/g Cobalt-60 U 0.00527 +/-0.0111 0.00958 +/-0.0111 0.0192 pCi/g Europium-152 U -0.0175 +/-0.0362 0.0237 +/-0.0362 0.0475 pCi/g Europium-154 U -0.00245 +/-0.0341 0.0284 +/-0.0341 0.0568 pCi/g Europium-155 U 0.0206 +/-0.0348 0.0278 +/-0.0348 0.0555 pCi/g Lead-212 0.555 +/-0.0539 0.014 +/-0.0539 0.028 pCi/g Lead-214 0.632 +/-0.0716 0.0168 +/-0.0716 0.0335 pCi/g Manganese-54 U 0.00136 +/-0.0119 0.00895 +/-0.0119 0.0179 pCi/g Niobium-94 U 0.00516 +/-0.0104 0.00889 +/-0.0104 0.0178 pCi/g Potassium-40 9.34 +/-0.717 0.0757 +/-0.717 0.151 pCi/g Radium-226 0.581 +/-0.0677 0.0166 +/-0.0677 0.0332 pCi/g Silver-108m U -0.00363 +/-0.00933 0.00801 +/-0.00933 0.016 pCi/g Thallium-208 0.181 +/-0.028 0.00841 +/-0.028 0.0168 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U 0.0459 +/-0.0311 0.0196 +/-0.0311 0.0464 pCi/g KSDI 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1037 613798 The following Analytical Methods were performed Method Description 1 EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 65 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-012F Project: YANK01204 Sample ID: 181554013 Client ID: YANKOO Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 72 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.66 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-013F 181554014 TS 23-FEB-07 01-MAR-07 Client 6.8%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0153+/-0.0466 0.0223 +/-0.0466 Curium-242 U Curium-243/244 U Alphaspec Pu, Solid-ALL FSS Plutonium-238 U Plutonium-239/240 U Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U-0.00625 +/-0.0525 0.0234 +/-0.0526-0.0658 +/-0.0389 0.0741 +/-0.0397 0.0302 +/-0.0933 0.0606 +/-0.0934 0.121 +/-0.123 0.0271 +/-0.123-7.24 +/-7.27 6.48 +/-7.27 0.112 0.117 0.216 0.203 0.136 13.7 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MXA 03/05/07 1619 613994 1 MXA 03/03/07 1706 613995 1 MXA 03/05/07 2227 613997 1 Rad Gamma Spec Analysis Gamma, Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.806 Americium-241 U 0.0059 Bismuth-212 0.325 Bismuth-214 0.824 Cesium- 134 UI 0.00 Cesium-137 0.119 Cobalt-60 U 0.0059 Europium-152 U -0.00908 Europium-154 U -0.00201 Europium-155 UI 0.00 Lead-212 0.890 Lead-214 0.891 Manganese-54 U 0.0133 Niobium-94 U 0.0023 Potassium-40 10.4 Radium-226 0.824 Silver-108m U -0.00585 Thallium-208 0.294 Rad Gas Flow Proportional Counting+/-0.141+/-0.0542+/-0.148+/-0.0912+/-0.0178+/-0.0194+/-0.0113+/-0.034+/-0.0394+/-0.0471+/-0.0747+/-0.0894+/-0.015+/-0.0103+/-0.793+/-0.0912+/-0.0101+/-0.0358 0.0329 0.043 0.072 0.0159 0.0102 0.0095 0.00992 0.0254 0.0289 0.0295 0.0152 0.0188 0.00927 0.00894 0.0807 0.0159 0.00839 0.00938+/-0.141+/-0.0542+/-0.148+/-0.0912+/-0.0178+/-0.0194+/-0.0113+/-0.034+/-0.0394+/-0.0471+/-0.0747+/-0.0894+/-0.015+/-0.0103+/-0.793+/-0.0912+/-0.0101+/-0.0358 0.0657 0.086 0.144 0.0319 0.0204 0.019 0.0198 0.0507 0.0577 0.059 0.0304 0.0376 0.0185 0.0179 0.161 0.0319 0.0168 0.0187 0.0399 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MJH1 03/05/07 1610 614269 GFPC, Sr90, solid-ALL FSS Strontium-90 Rad Liquid Scintillation Analysis U 0.0165 +/-0.0231 0.0165 +/-0.0231 KSDI 03/06/07 1617 613959 67 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: 9514-0001-013F 181554014 Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid -3 pCilg Tritium U -0.0488 +/-1.61 1.35 +/-1.61 2.82 pCi/g AXD2 03/03/07 0143 614003 Liquid Scint C14, Solid All, FSS Carbon-14 U 0.0483 +/-0.0978 0.081 +/-0.0978 0.166 pCi/g AXD2 03/05/07 1255 614005 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 12.7 +/-46.0 30.0 +/-46.0 63.1 pCi/g MXP1 03/07/07 1026 613996 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -3.79 +/-8.02 6.91 +/-8.02 14.5 pCi/g MXP1 03/06/07 1502 613999 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.0425 +/-0.223 0.186 +/-0.223 0.384 pCi/g MXP1 03/03/07 2045 614001 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1037 613798 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-i I-RC Modified 4 DOE EML HASL-300, Pu-I I-RC Modified 5 EML HASL 300, 4.5.2.3 6 EPA 905.0 Modified 7 EPA 906.0 Modified 8 EPA EERF C-01 Modified 9 EPA EERF C-01 Modified 10 DOE RESL Fe-1, Modified 11 DOE RESL Ni-i, Modified 12 DOE EML HASL-300, Tc-02-RC Modified 13 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Americium-243 Tracer Americium-243 Tracer Alphaspec Am241, Cm, Solid ALL Alphaspec Am241, Cm, Solid ALL 90 90 (15%-125%)

(15%-125%)

68 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: 9514-0001-013F 181554014 Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Plutonium-242 Tracer Plutonium-242 Tracer Plutonium-241 Plutonium-242 Tracer Plutonium-242 Tracer Strontium Carrier Strontium Carrier Iron-59 Tracer Iron-59 Tracer Nickel Carrier Nickel Carrier Technetium-99 Technetium-99m Tracer Technetium-99m Tracer Alphaspec Pu, Solid-ALL FSS Alphaspec Pu, Solid-ALL FSS Liquid Scint Pu241, Solid-ALL F5 Liquid Scint Pu241, Solid-ALL FýLiquid Scint Pu241, Solid-ALL FS GFPC, Sr90, solid-ALL FSS GFPC, Sr90, solid-ALL FSS Liquid Scint Fe55, Solid-ALL FS Liquid Scint Fe55, Solid-ALL FS Liquid Scint Ni63, Solid-ALL FS Liquid Scint Ni63, Solid-ALL FS Liquid Scint Tc99, Solid-ALL FS Liquid Scint Tc99, Solid-ALL FS Liquid Scint Tc99, Solid-ALL FS 77 77 82 82 82 76 76 75 75 96 96 82 82 82 (15%-125%)

(15%-125%)

(25%-125%)

(25%-125%)

(25%-125%)

(25%-125%)

(25%-125%)

(15%-125%)

(15%-125%)

(25%-125%)

(25%-125%)

(15%-125%)

(15%-125%)

(15%-125%)

Notes: The Qualifiers in this report are defined as follows** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.69 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-014F 181554015 TS 23-FEB-07 01-MAR-07 Client 6.07%Proiect: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1A Rad Gamma Spec Analysis Gamma, Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.654 +/-0.147 0.045 +/-0.147 0.090 pCi/g MJHI 03/05/07 1612 614269 Americium-241 U 0.0292 +/-0.0258 0.0209 +/-0.0258 0.0417 pCi/g Bismuth-212 0.292 +/-0.236 0.102 +/-0.236 0.204 pCi/g Bismuth-214 0.701 +/-0.0931 0.0247 +/-0.0931 0.0494 pCi/g Cesium-] 34 UI 0.00 +/-0.0234 0.0158 +/-0.0234 0.0315 pCi/g Cesium-137 0.844 +/-0.0843 0.0143 +/-0.0843 0.0285 pCi/g Cobalt-60 UI 0.00 +/-0.0245 0.0144 +/-0.0245 0.0288 pCi/g Europium-152 U -0.0107 +/-0.0511 0.0341 +/-0.0511 0.0682 pCi/g Europium-154 U -0.0145 +/-0.0477 0.0394 +/-0.0477 0.0788 pCi/g Europium-155 U 0.0406 +/-0.0401 0.032 +/-0.0401 0.064 pCi/g Lead-212 0.628 +/-0.0679 0.0186 +/-0.0679 0.0373 pCi/g Lead-214 0.746 +/-0.0878 0.0245 +/-0.0878 0.0489 pCi/g Manganese-54 U 0.00896 +/-0.0178 0.0134 +/-0.0178 0.0269 pCi/g Niobium-94 U 0.00112 +/-0.015 0.0126 +/-0.015 0.0252 pCi/g Potassium-40 9.09 +/-0.720 0.119 +/-0.720 0.238 pCi/g Radium-226 0.701 +/-0.0931 0.0247 +/-0.0931 0.0494 pCi/g Silver-108m U -0.00378 +/-0.0142 0.0123 +/-0.0142 0.0246 pCi/g Thallium-208 0.191 +/-0.0443 0.0129 +/-0.0443 0.0257 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.00344 +/-0.0216 0.0186 +/-0.0216 0.0435 pCi/g KSDI 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1037 613798 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 70 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-014F Proiect: YANK01204 Sample ID: 181554015 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.71 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-015F 181554016 TS 23-FEB-07 01-MAR-07 Client 5.62%Proiect: Client ID: Vol. Recv.: YANKO 1204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.578 +/-0.174 0.0508 +/-0.174 0.102 pCi/g MJH1 03/06/07 0917 614269 Americium-241 U 0.00594 +/-0.098 0.0825 +/-0.098 0.165 pCi/g Bismuth-212 0.270 +/-0.233 0.135 +/-0.233 0.269 pCi/g Bismuth-214 0.411 +/-0.102 0.0338 +/-0.102 0.0676 pCi/g Cesium-134 U 0.0222 +/-0.0297 0.0215 +/-0.0297 0.043 pCi/g Cesium-137 U -0.00162 +/-0.0194 0.0165 +/-0.0194 0.033 pCi/g Cobalt-60 U 0.015 +/-0.0219 0.0199 +/-0.0219 0.0397 pCi/g Europium-152 U 0.0211 +/-0.0549 0.0445 +/-0.0549 0.0889 pCi/g Europium-154 U -0.0136 +/-0.0688 0.057 +/-0.0688 0.114 pCi/g Europium-155 U 0.0268 +/-0.0573 0.0538 +/-0.0573 0.108 pCi/g Lead-212 0.542 +/-0.0656 0.0258 +/-0.0656 0.0516 pCi/g Lead-214 0.459 +/-0.0763 0.0309 +/-0.0763 0.0618 pCi/g Manganese-54 U -0.00761 +/-0.0234 0.017 +/-0.0234 0.034 pCi/g Niobium-94 U 0.0192 +/-0.0175 0.0162 +/-0.0175 0.0324 pCi/g Potassium-40 9.57 +/-0.945 0.125 +/-0.945 0.250 pCi/g Radium-226 0.411 +/-0.102 0.0338 +/-0.102 0.0676 pCi/g Silver-108m U 0.00409 +/-0.0176 0.0139 +/-0.0176 0.0278 pCi/g Thallium-208 0.210 +/-0.0407 0.0159 +/-0.0407 0.0318 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.0201 +/-0.0214 0.0207 +/-0.0214 0.047 pCi/g KSDI 03/06/07 1617 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%Acceptable Limits 72 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: 9514-0001-015F 181554016 Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1N Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier Strontium Carrier GFPC, Sr90, solid-ALL FSS GFPC, Sr90, solid-ALL FSS 61 61 (25%-125%)

(25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.73 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-016F 181554017 TS 23-FEB-07 01-MAR-07 Client 5.65%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.600 +1-0.151 0.0604 +/-0.151 0.121 pCi/g MJHI 03/06/07 0917 614269 Americium-241 U 0.0188 +/-0.066 0.0551 +/-0.066 0.110 pCi/g Bismuth-212 0.636 +/-0.228 0.130 +/-0.228 0.259 pCi/g Bismuth-214 0.551 +/-0.0932 0.0362 +/-0.0932 0.0723 pCi/g Cesium-] 34 U 0.042 +/-0.0228 0.0222 +/-0.0228 0.0444 pCi/g Cesium-137 U 0.0191 +/-0.0217 0.017 +/-0.0217 0.034 pCi/g Cobalt-60 UI 0.00 +/-0.0379 0.0236 +/-0.0379 0.0472 pCi/g Europium-152 U -0.0446 +/-0.0617 0.0423 +/-0.0617 0.0845 pCi/g Europium-154 U 0.0245 +/-0.0623 0.0546 +/-0.0623 0.109 pCi/g Europium-155 U 0.0672 +/-0.0518 0.049 +/-0.0518 0.098 pCi/g Lead-212 0.662 +/-0.072 0.0251 +/-0.072 0.0501 pCi/g Lead-214 0.562 +/-0.0884 0.0319 +/-0.0884 0.0638 pCi/g Manganese-54 U 0.0213 +/-0.0223 0.0171 +/-0.0223 0.0342 pCi/g Niobium-94 U 0.00191 +/-0.0175 0.015 +/-0.0175 0.0299 pCi/g Potassium-40 10.7 +/-1.01 0.142 +/-1.01 0.283 pCi/g Radium-226 0.551 +/-0.0932 0.0362 +/-0.0932 0.0723 pCi/g Silver-108m U -0.00779 +/-0.0172 0.0147 +/-0.0172 0.0293 pCi/g Thallium-208 0.217 +/-0.0405 0.016 +/-0.0405 0.0319 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, solid-ALL FSS Strontium-90 U 0.00655 +/-0.0245 0.0195 +/-0.0245 0.0466 pCi/g KSDI 03/06/07 1618 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%Acceptable Limits 74 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-016F Project: YANK01204 Sample ID: 181554017 Client ID: YANKOOl Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.75 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com CPrtifie2tP of Analys~is CPrfir1r.q1P_(&A Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-024F 181554018 TS 23-FEB-07 01-MAR-07 Client 3.3%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.635 +/-0.190 0.0789 +/-0.190 0.158 pCi/g MJHI 03/06/07 0918 614269 Americium-241 U 0.0097 +/-0.0307 0.0365 +/-0.0307 0.0729 pCi/g Bismuth-212 0.579 +/-0.433 0.174 +/-0.433 0.347 pCi/g Bismuth-214 0.435 +/-0.123 0.0452 +/-0.123 0.0903 pCi/g Cesium-] 34 U 0.0353 +/-0.0225 0.0258 +/-0.0225 0.0515 pCi/g Cesium-137 U -0.0073 +/-0.0316 0.0245 +/-0.0316 0.049 pCi/g Cobalt-60 U -0.0111 +/-0.0286 0.0231 +/-0.0286 0.0461 pCi/g Europium-152 U -0.0529 +/-0.0737 0.0576 +/-0.0737 0.115 pCi/g Europium-154 U -0.0334 +/-0.0826 0.067 +/-0.0826 0.134 pCi/g Europium-155 U 0.0777 +/-0.0859 0.0554 +/-0.0859 0.111 pCi/g Lead-212 0.657 +/-0.0843 0.0317 +/-0.0843 0.0633 pCi/g Lead-214 0.544 +/-0.0999 0.0399 +/-0.0999 0.0798 pCi/g Manganese-54 U -0.00686 +/-0.0262 0.0225 +/-0.0262 0.045 pCi/g Niobium-94 U 0.00362 +/-0.0281 0.0241 +/-0.0281 0.0481 pCi/g Potassium-40 9.49 +/-1.04 0.202 +/-1.04 0.403 pCi/g Radium-226 0.435 +/-0.123 0.0452 +/-0.123 0.0903 pCi/g Silver-108m U -0.0083 +/-0.0229 0.0198 +/-0.0229 0.0395 pCi/g Thallium-208 0.187 +/-0.0635 0.0244 +/-0.0635 0.0488 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.0178 +/-0.0207 0.0205 +/-0.0207 0.0482 pCi/g KSDI 03/06/07 1618 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description 1 EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 76 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-024F Project: YANK01204 Sample ID: 181554018 Client ID: YANKOO Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch IN Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.77 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-025F 181554019 TS 23-FEB-07 01 -MAR-07 Client 5.48%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter (Rad Gamma Spec Analysis Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 Americium-241 U Bismuth-212 U Bismuth-214 Cesium- 134 U Cesium-I 37 U-c Cobalt-60 U -Europium-152 U Europium-154 U Europium-155 U Lead-212 Lead-214 Manganese-54 U Niobium-94 U -Potassium-40 Radium-226 Silver-108m U -Thallium-208 Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.647 0.0147 0.221 0.519 0.0332.000896 0.00686 0.041-0.0228 0.0173 0.580 0.562-0.0148-0.00565 8.92 0.519 0.00539 0.203+/-0.176+/-0.0297+/-0.244+/-0.0983+/-0.0277+/-0.0251+/-0.0223+/-0.0612+/-0.0638+/-0.048+/-0.0734+/-0.0804+/-0.0261+/-0.0209+/-0.978+/-0.0983+/-0.0174+/-0.0432 0.0635 0.027 0.140 0.0358 0.0223 0.0214 0.0178 0.044 0.0509 0.0439 0.0236 0.0279 0.0186 0.0174 0.159 0.0358 0.0153 0.0172+/-0.176+/-0.0297+/-0.244+/-0.0983+/-0.0277+/-0.0251+/-0.0223+/-0.0612+/-0.0638+/-0.048+/-0.0734+/-0.0804+/-0.0261+/-0.0209+/-0.978+/-0.0983+/-0.0174+/-0.0432 0.127 0.054 0.281 0.0716 0.0446 0.0428 0.0356 0.088 0.102 0.0878 0.0471 0.0558 0.0372 0.0347 0.319 0.0716 0.0305 0.0343 0.0455 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MJHI 03/06/07 0919 614269 KSD1 03/06/07 1618 613959 0.00416 +/-0.0217 0.019 +/-0.0217 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 78 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-025F Project: YANK01204 Sample ID: 181554019 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.79 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-026F 181554020 TS 23-FEB-07 01-MAR-07 Client 5.6%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1r Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.624 +/-0.148 0.0644 +/-0.148 0.129 pCi/g MJHI 03/06/07 0919 614269 Americium-241 U 0.103 +/-0.0655 0.0575 +/-0.0655 0.115 pCi/g Bismuth-212 U 0.277 +/-0.257 0.141 +/-0.257 0.281 pCi/g Bismuth-214 0.897 +/-0.118 0.0323 +/-0.118 0.0645 pCi/g Cesium-134 U 0.0204 +/-0.0293 0.0219 +/-0.0293 0.0437 pCi/g Cesium-] 37 U 0.0235 +/-0.0219 0.0191 +/-0.0219 0.0382 pCi/g Cobalt-60 U -0.00736 +/-0.0234 0.0179 +/-0.0234 0.0359 pCi/g Europium-152 U 0.0216 +/-0.0635 0.0507 +/-0.0635 0.101 pCi/g Europium-154 U -0.00936 +/-0.067 0.0558 +/-0.067 0.112 pCi/g Europium-155 U 0.0575 +/-0.062 0.0537 +/-0.062 0.107 pCi/g Lead-212 0.554 +/-0.0704 0.0302 +/-0.0704 0.0605 pCi/g Lead-214 0.977 +/-0.116 0.0356 +/-0.116 0.0712 pCi/g Manganese-54 U 0.00664 +/-0.0212 0.019 +/-0.0212 0.0379 pCi/g Niobium-94 U 0.0119 +/-0.0184 0.0163 +/-0.0184 0.0326 pCi/g Potassium-40 10.9 +/-0.997 0.125 +/-0.997 0.249 pCi/g Radium-226 0.897 +/-0.118 0.0323 +/-0.118 0.0645 pCi/g Silver-108m U 0.0178 +/-0.0221 0.019 +/-0.0221 0.0379 pCi/g Thallium-208 0.195 +/-0.0434 0.0187 +/-0.0434 0.0373 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.00229 +/-0.0236 0.0201 +/-0.0236 0.0463 pCi/g KSD1 03/06/07 1618 613959 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 80 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-026F Project: YANK01204 Sample ID: 181554020 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 68 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 68 (25%-125%)

Notes: The Qualifiers in this report are defined as follows** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.81 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: 9514-0001-027F Project: YANK01204 Sample ID: 181554021 Client ID: YANKOOl Matrix: TS Vol. Recv.: Collect Date: 26-FEB-07 Receive Date: 01-MAR-07 Collector:

Client Moisture:

9.31%Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.629 +/-0.137 0.0461 +/-0.137 0.0921 pCi/g MJHI 03/06/07 1034 614271 Americium-241 U 0.0522 +/-0.0917 0.0812 +/-0.0917 0.162 pCi/g Bismuth-212 0.424 +/-0.206 0.0959 +/-0.206 0.192 pCi/g Bismuth-214 0.648 +/-0.0872 0.0234 +/-0.0872 0.0468 pCi/g Cesium-134 U 0.0244 +/-0.0229 0.0168 +/-0.0229 0.0335 pCi/g Cesium-137 U 0.0107 +/-0.0315 0.0122 +/-0.0315 0.0243 pCi/g Cobalt-60 U 0.0113 +/-0.0155 0.0142 +1-0.0155 0.0284 pCi/g Europium-152 U -0.0123 +/-0.0447 0.0358 +/-0.0447 0.0715 pCi/g Europium-154 U -0.00794 +/-0.0725 0.0369 +/-0.0725 0.0738 pCi/g Europium-155 U 0.021 +/-0.0514 0.048 +/-0.0514 0.0959 pCi/g Lead-212 0.670 +/-0.070 0.0216 +/-0.070 0.0432 pCi/g Lead-214 0.636 +/-0.0843 0.0252 +/-0.0843 0.0503 pCi/g Manganese-54 U -0.0172 +/-0.0153 0.0125 +/-0.0153 0.025 pCi/g Niobium-94 U 0.00807 +/-0.0131 0.0117 +/-0.0131 0.0234 pCi/g Potassium-40 10.7 +/-0.880 0.122 +/-0.880 0.243 pCi/g Radium-226 0.648 +/-0.0872 0.0234 +/-0.0872 0.0468 pCi/g Silver-108m U -0.008 +/-0.0136 0.0118 +/-0.0136 0.0235 pCi/g Thallium-208 0.225 +/-0.0357 0.0112 +/-0.0357 0.0224 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.00632 +/-0.0268 0.0222 +/-0.0268 0.0467 pCi/g KSDI 03/06/07 1734 613960 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified 82 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-027F Proiect: YANKO 1204 Sample ID: 181554021 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1A Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 55 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 55 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound* Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.IBD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.83 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-028F 181554022 TS 26-FEB-07 01-MAR-07 Client 5.22%Proiect: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.609 +/-0.178 0.061 +/-0.178 0.122 pCi/g MJH1 03/06/07 1035 614271 Americium-241 U 0.0228 +/-0.102 0.0816 +/-0.102 0.163 pCi/g B3ismuth-212 0.434 +/-0.300 0.143 +/-0.300 0.286 pCi/g 13ismuth-214 0.812 +/-0.127 0.0348 +/-0.127 0.0695 pCi/g Cesium-134 U 0.042 +/-0.0308 0.0229 +/-0.0308 0.0458 pCi/g Cesium-137 U 0.0196 +/-0.0225 0.0206 +/-0.0225 0.0413 pCi/g Cobalt-60 U -0.0277 +/-0.0222 0.0159 +/-0.0222 0.0317 pCi/g Europium-152 U -0.0664 +/-0.0733 0.0467 +/-0.0733 0.0934 pCi/g Europium-154 U -0.00276 +/-0.075 0.0549 +/-0.075 0.110 pCi/g Europium-155 U 0.0314 +/-0.0605 0.0572 +/-0.0605 0.114 pCi/g Lead-212 0.676 +/-0.076 0.0281 +/-0.076 0.0561 pCi/g Lead-214 0.950 +/-0.125 0.0343 +/-0.125 0.0686 pCi/g Manganese-54 U 0.0112 +/-0.023 0.0202 +/-0.023 0.0405 pCi/g Niobium-94 U 0.00356 +/-0.0197 0.0172 +/-0.0197 0.0344 pCi/g Potassium-40 9.85 +/-0.997 0.178 +/-0.997 0.357 pCi/g Radium-226 0.812 +/-0.127 0.0348 +/-0.127 0.0695 pCi/g Silver-108m U -0.00239 +/-0.0186 0.0156 +/-0.0186 0.0311 pCi/g Thallium-208 0.233 +/-0.0432 0.017 +/-0.0432 0.034 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, solid-ALL FSS Strontium-90 U 0.00562 +/-0.0278 0.0231 +/-0.0278 0.0487 pCi/g KSDI 03/06/07 1734 613960 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 84 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-028F Project: YANK01204 Sample ID: 181554022 Client ID: YANKOO Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 53 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 53 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.85 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-029F 181554023 TS 26-FEB-07 01-MAR-07 Client 5.92%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma, Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.770 +/-0.168 0.0563 +/-0.168 0.113 pCi/g MJHI 03/06/07 1036 614271 Americium-241 U 0.0742 +/-0.0692 0.0592 +/-0.0692 0.118 pCi/g Bismuth-212 0.302 +/-0.244 0.134 +/-0.244 0.268 pCi/g Bismuth-214 0.603 +/-0.102 0.0311 +/-0.102 0.0621 pCi/g Cesium-134 UI 0.00 +/-0.0332 0.0218 +/-0.0332 0.0436 pCi/g Cesium-137 U -0.00866 +/-0.022 0.0171 +/-0.022 0.0343 pCi/g Cobalt-60 U 0.0139 +/-0.0218 0.0195 +/-0.0218 0.0389 pCi/g Europium-152 U -0.0125 +/-0.0579 0.0427 +/-0.0579 0.0854 pCi/g Europium-154 U -0.0176 +/-0.0587 0.0476 +/-0.0587 0.0951 pCi/g Europium-155 U 0.058 +/-0.0745 0.0502 +/-0.0745 0.100 pCi/g Lead-212 0.562 +/-0.0683 0.0247 +/-0.0683 0.0493 pCi/g Lead-214 0.663 +/-0.0967 0.0317 +/-0.0967 0.0634 pCi/g Manganese-54 U 0.00708 +/-0.0189 0.0169 +/-0.0189 0.0338 pCi/g Niobium-94 U -0.00962 +/-0.0184 0.0148 +/-0.0184 0.0296 pCi/g Potassium-40 10.2 +/-0.976 0.135 +/-0.976 0.270 pCi/g Radium-226 0.603 +/-0.102 0.0311 +/-0.102 0.0621 pCi/g Silver-108m U 0.00154 +/-0.0163 0.0143 +/-0.0163 0.0286 pCi/g Thallium-208 0.218 +/-0.0408 0.0156 +/-0.0408 0.0312 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, solid-ALL FSS Strontium-90 U -0.0246 +/-0.0207 0.0186 +/-0.0207 0.0391 pCi/g KSDI 03/06/07 1734 613960 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 86 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-029F Proiect: YANK01204 Sample ID: 181554023 Client ID: YANKOO Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1l Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 63 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 63 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.87 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-019J 181554024 TS 27-FEB-07 01-MAR-07 Client 30.9%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.549 +/-0.226 0.0775 +/-0.226 0.155 pCi/g MJHI 03/06/07 1152 614271 Americium-241 U 0.0829 +/-0.123 0.0973 +/-0.123 0.195 pCi/g Bismuth-212 0.414 +/-0.341 0.150 +/-0.341 0.300 pCi/g Bismuth-214 0.549 +/-0.118 0.0402 +/-0.118 0.0804 pCi/g Cesium-134 U 0.0428 +/-0.033 0.0263 +/-0.033 0.0526 pCi/g Cesium-137 0.522 +/-0.0792 0.020 +/-0.0792 0.040 pCi/g Cobalt-60 U 0.0525 +/-0.0336 0.032 +/-0.0336 0.0641 pCi/g Europium-152 U -0.0543 +/-0.101 0.0624 +/-0.101 0.125 pCi/g Europium-154 U -0.0852 +/-0.0802 0.0567 +/-0.0802 0.113 pCi/g Europium-155 U 0.00883 +/-0.0778 0.0669 +/-0.0778 0.134 pCi/g Lead-212 0.717 +/-0.0939 0.0345 +/-0.0939 0.069 pCi/g Lead-214 0.690 +/-0.123 0.043 +/-0.123 0.0859 pCi/g Manganese-54 U -0.00585 +/-0.0261 0.0219 +/-0.0261 0.0437 pCi/g Niobium-94 U -0.00188 +/-0.0259 0.0212 +/-0.0259 0.0424 pCi/g Potassium-40 9.96 +/-1.22 0.221 +/-1.22 0.443 pCi/g Radium-226 0.549 +/-0.118 0.0402 +/-0.118 0.0804 pCi/g Silver-108m U -0.0134 +/-0.0288 0.0203 +/-0.0288 0.0405 pCi/g Thallium-208 0.231 +/-0.058 0.0197 +/-0.058 0.0394 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 0.0739 +/-0.0323 0.0225 +/-0.0326 0.0484 pCi/g KSD1 03/06/07 1733 613960 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 88 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-019J Project: YANK01204 Sample ID: 181554024 Client ID: YANKOO Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 76 (25%-125%)

Strontium Carrier GFPC, Sr9O, solid-ALL FSS 76 (25%-125%)

Notes: The Qualifiers in this report are defined as follows** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.89 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-020J 181554025 TS 27-FEB-07 01-MAR-07 Client 31.9%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.746 +/-0.172 0.0634 +/-0.172 0.127 pCi/g MJH1 03/06/07 1153 614271 Americium-241 U 0.0491 +/-0.105 0.0831 +/-0.105 0.166 pCi/g Bismuth-212 0.368 +/-0.295 0.137 +/-0.295 0.274 pCi/g Bismuth-214 0.622 +/-0.102 0.0318 +/-0.102 0.0636 pCi/g Cesium-134 UI 0.00 +/-0.0266 0.0239 +/-0.0266 0.0477 pCi/g Cesium-137 0.465 +/-0.0551 0.0169 +/-0.0551 0.0338 pCi/g Cobalt-60 U 0.0232 +/-0.0247 0.0223 +/-0.0247 0.0446 pCi/g Europium-152 U -0.0155 +/-0.0642 0.0474 +/-0.0642 0.0948 pCi/g Europium-154 U 0.0523 +/-0.0729 0.0643 +/-0.0729 0.129 pCi/g Europium-155 U 0.0239 +/-0.0627 0.0549 +/-0.0627 0.110 pCi/g Lead-212 0.748 +/-0.087 0.028 +/-0.087 0.056 pCi/g Lead-214 0.626 +/-0.113 0.0348 +/-0.113 0.0696 pCi/g Manganese-54 U -0.0143 +/-0.0226 0.0177 +/-0.0226 0.0353 pCi/g Niobium-94 U -0.00322 +/-0.0209 0.0171 +/-0.0209 0.0342 pCi/g Potassium-40 9.54 +/-1.04 0.178 +/-1.04 0.356 pCi/g Radium-226 0.622 +/-0.102 0.0318 +/-0.102 0.0636 pCi/g Silver-108m U 0.0015 +/-0.0192 0.0165 +/-0.0192 0.0329 pCi/g Thallium-208 0.256 +/-0.0521 0.0173 +/-0.0521 0.0347 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0346 +/-0.0282 0.0211 +/-0.0282 0.0459 pCi/g KSDI 03/06/07 1733 613960 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 90 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-020J Project: YANK01204 Sample ID: 181554025 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 67 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 67 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.91 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-021J 181554026 TS 27-FEB-07 01-MAR-07 Client 24%Project: Client ID: Vol. Recv.: YANK01204 YANKOO I Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.844 +/-0.178 0.0546 +/-0.178 0.109 pCi/g MJHI 03/06/07 1223 614271 Americium-241 U -0.015 +/-0.116 0.0902 +/-0.116 0.180 pCi/g Bismuth-212 UI 0.00 +/-0.382 0.139 +/-0.382 0.278 pCi/g Bismuth-214 0.682 +/-0.120 0.0349 +/-0.120 0.0697 pCi/g Cesium-134 U 0.0431 +/-0.0339 0.0241 +/-0.0339 0.0481 pCi/g Cesium-137 0.305 +/-0.0523 0.0192 +/-0.0523 0.0384 pCi/g Cobalt-60 U 0.00923 +/-0.0247 0.0212 +/-0.0247 0.0425 pCi/g Europium-152 U 0.0373 +/-0.0675 0.0502 +/-0.0675 0.100 pCi/g Europium-154 U -0.0666 +/-0.0697 0.0516 +/-0.0697 0.103 pCi/g Europium-155 U -0.0191 +/-0.0655 0.0563 +/-0.0655 0.113 pCi/g Lead-212 0.750 +/-0.0825 0.0281 +/-0.0825 0.0562 pCi/g Lead-214 0.724 +/-0.110 0.0355 +/-0.110 0.071 pCi/g Manganese-54 U 0.00743 +/-0.0237 0.0207 +/-0.0237 0.0414 pCi/g Niobium-94 U 0.00346 +/-0.021 0.0176 +/-0.021 0.0352 pCi/g Potassium-40 8.64 +/-0.945 0.180 +/-0.945 0.360 pCi/g Radium-226 0.682 +/-0.120 0.0349 +/-0.120 0.0697 pCi/g Silver-108m U 0.00859 +/-0.0209 0.0182 +/-0.0209 0.0364 pCi/g Thallium-208 0.249 +/-0.0569 0.0189 +/-0.0569 0.0377 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 0.0501 +/-0.0312 0.0228 +/-0.0314 0.0493 pCi/g KSDl 03/06/07 1733 613960 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 92 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-021J Project: YANK01204 Sample ID: 181554026 Client ID: YANKOOl Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 62 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 62 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded I Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.93 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-022J 181554027 TS 27-FEB-07 01-MAR-07 Client 22.2%Project: Client ID: Vol. Recv.: YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.829 +/-0.201 0.0764 +/-0.201 0.153 pCi/g MJH1 03/06/07 1224 614271 Americium-241 U 0.00365 +/-0.0933 0.0723 +/-0.0933 0.145 pCi/g Bismuth-212 0.557 +/-0.322 0.172 +/-0.322 0.344 pCi/g Bismuth-214 0.892 +/-0.144 0.0408 +/-0.144 0.0815 pCi/g Cesium-I 34 UI 0.00 +/-0.0477 0.028 +/-0.0477 0.0559 pCi/g Cesium-137 0.519 +/-0.0692 0.0231 +/-0.0692 0.0461 pCi/g Cobalt-60 U 0.0153 +/-0.0249 0.0222 +/-0.0249 0.0444 pCi/g Europium-152 U 0.0264 +/-0.087 0.063 +/-0.087 0.126 pCi/g Europium-154 U -0.0534 +/-0.0874 0.0676 +/-0.0874 0.135 pCi/g Europium-155 U 0.0453 +/-0.104 0.0572 +/-0.104 0.114 pCi/g Lead-212 0.897 +/-0.100 0.035 +/-0.100 0.070 pCi/g Lead-214 1.10 +/-0.141 0.0458 +/-0.141 0.0916 pCi/g Manganese-54 U -0.0149 +/-0.0252 0.0204 +/-0.0252 0.0408 pCi/g Niobium-94 U -0.00852 +/-0.0256 0.0206 +/-0.0256 0.0412 pCi/g Potassium-40 12.3 +/-1.21 0.216 +/-1.21 0.432 pCi/g Radium-226 0.892 +/-0.144 0.0408 +/-0.144 0.0815 pCi/g Silver-108m U 0.0133 +/-0.0378 0.0233 +/-0.0378 0.0465 pCi/g Thallium-208 0.322 +/-0.0581 0.0214 +/-0.0581 0.0429 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 0.0546 +/-0.0281 0.0198 +/-0.0283 0.0429 pCi/g KSD1 03/06/07 1733 613960 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMBI 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 94 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-022J Project: YANK01204 Sample ID: 181554027 Client ID: YANK00I Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1A Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, S90, solid-ALL FSS 70 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 70 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.13D Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.95 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Report Date: March 8, 2007 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector:

Moisture: 9514-0001-023J 181554028 TS 27-FEB-07 01-MAR-07 Client 9.88%Project: Client ID: Vol. Recv.: YANKO01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1%Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.559 +/-0.314 0.117 +/-0.314 0.233 pCi/g MJH1 03/06/07 1224 614271 Americium-241 U 0.0165 +/-0.0641 0.0497 +/-0.0641 0.0992 pCi/g Bismuth-212 0.592 +/-0.465 0.262 +/-0.465 0.523 pCi/g Bismuth-214 0.978 +/-0.185 0.0621 +/-0.185 0.124 pCi/g Cesium-] 34 U 0.0153 +/-0.0477 0.0415 +/-0.0477 0.0829 pCi/g Cesium-137 0.334 +/-0.0797 0.0403 +/-0.0797 0.0806 pCi/g Cobalt-60 U 0.0306 +/-0.0508 0.0388 +/-0.0508 0.0775 pCi/g Europium-152 U -0.0077 +/-0.118 0.0878 +/-0.118 0.175 pCi/g Europium-154 U 0.0828 +/-0.137 0.0912 +/-0.137 0.182 pCi/g Europium-155 U 0.104 +/-0.122 0.0758 +/-0.122 0.152 pCi/g Lead-212 0.760 +/-0.110 0.046 +/-0.110 0.092 pCi/g Lead-214 1.00 +/-0.161 0.0581 +/-0.161 0.116 pCi/g Manganese-54 U 0.0091 +/-0.0434 0.0326 +/-0.0434 0.0651 pCi/g Niobium-94 U 0.00391 +/-0.037 0.0306 +/-0.037 0.0612 pCi/g Potassium-40 11.6 +/-1.33 0.274 +/-1.33 0.548 pCi/g Radium-226 0.978 +/-0.185 0.0621 +/-0.185 0.124 pCi/g Silver-108m U -0.0207 +/-0.0358 0.0293 +/-0.0358 0.0586 pCi/g Thallium-208 0.201 +/-0.0857 0.0315 +/-0.0857 0.0629 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 0.0694 +/-0.033 0.0233 +/-0.0333 0.0503 pCi/g KSDI 03/06/07 1733 613960 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 TMB1 03/01/07 1047 613799 The following Analytical Methods were performed Method Description I EML HASL 300,4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits 96 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: March 8, 2007 Contact: Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9514-0001-023J Proiect: YANK01204 Sample ID: 181554028 Client ID: YANK001 Vol. Recv.: Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch A Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 63 (25%-125%)

Strontium Carrier GFPC, Sr90, solid-ALL FSS 63 (25%-125%)

Notes: The Qualifiers in this report are defined as follows:** Analyte is a surrogate compound< Result is less than value reported> Result is greater than value reported A The TIC is a suspected aldol-condensation product B For General Chemistry and Organic analysis the target analyte was detected in the associated blank.BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.97 QUALITY CONTROL DATA 98 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com OC Summary Client : Connecticut Yankee Atomic Power 362 Injun Hollow Rd Report Date: March 8, 2007 Page 1 of 13 East Hampton, Connecticut Contact: Mr. Jack McCarthy Workorder:

181554 Parmname Rad Alpha Spec Batch 613994 NOM Sample Qual QC Units RPD%REC% Range Anlst Date Time QC 1201287983 Americium-241 Curium-242 Curium-243/244 QC1201287985 Americium-241 Curium-242 Curium-243/244 QC1201287982 Americium-241 181554001 DUP U 0.027 Uncert: +/-0.101 TPU: +/-0.101 U 0.0292 Uncert: +/-0.0572 TPU: +/-0.0573 U 0.0563 Uncert: +/-0.119 TPU: +/-0.119 LCS MB 13.1 Uncert: TPU: Uncert: TPU: 15.7 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: U -0.0285+/-0.0632+/-0.0632 U 0.00+/-0.0323+/-0.0323 U -0.0756+/-0.0778+/-0.0785 12.0+/-1.08+/-1.87 U 0.0507+/-0.080+/-0.0803 14.3+/-1.18+/-2.16 U 0.00304+/-0.0192+/-0.0192 U 0.0318+/-0.0623+/-0.0625 U -0.0227+/-0.0257+/-0.0259 pCi/g 7400 pCi/g 200 pCi/g 1370 Curium-242 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g 92 (75%-125%)

(0% -100%) AXA1 (0%- 100%)(0%- 100%)91 (75%-125%)

03/03/07 17:06 03/03/07 17:07 03/03/07 17:06 Curium-243/244 QCI 201287984 Americium-241 181554001 MS Curium-242 13.5 Uncert: TPU: Uncert: TPU: 16.2 Uncert: TPU: U 0.027+/-0.101+/-0.101 U 0.0292+/-0.0572+/-0.0573 U 0.0563+/-0.119+/-0.119 U 15.0+/-1.33+/-2.38 0.0319+/-0.0625+/-0.0626 17.2+/-1.43+/-2.67 111 (75%-125%)

03/03/07 17:06 Curium-243/244 106 (75%-125%)

Batch 613995 QC1201287987 181554001 DUP Plutonium-238 U -0.0213 U 0.0781 pCi/g 350 (0% -100%) VIXA1 03/03/07 17:06 99 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Page 2of 13 Units RPD% REC% Range Anlst Date Time Parmname Rad Alpha Spec Batch 613995 Plutonium-239/240 QC1201287989 LCS Plutonium-238 Plutonium-239/240 QC1201287986 MB Plutonium-238 Plutonium-239/240 NOM Sample Qual QC Uncert: +/-0.106 TPU: +/-0.106 U 0.0612 Uncert: +/-0.138 TPU: +/-0.139 Uncert: TPU: 13.0 Uncert: TPU: Uncert: TPU: Uncert: TPU:+/-0.104+/-0.105 U 0.026+/-0.0581+/-0.0582 0.117+/-0.114+/-0.115 12.3+/-1.18+/-1.84 U -0.0103+/-0.0202+/-0.0203 U -0.0413+/-0.0405+/-0.0408 U 0.00+/-0.100+/-0.100 13.8+/-1.21+/-1.99 U -8.93+/-7.37+/-7.37 pCi/g 81 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g (0%- 100%)(75%-1 25%)95 (75%-125%)

03/03/07 17:06 03/03/07 17:06 QC1201287988 181554001 MS Plutonium-238 Plutonium-239/240 U -0.0213 Uncert: +/-0.106 TPU: +/-0.106 13.4 U 0.0612 Uncert: +/-0.138 TPU: +/-0.139 U 1.13 Uncert: +/-7.38 TPU: +/-7.38 (75%-125%)

03/03/07 17:06 103 (75%-125%)

Batch 613997 QC1201287995 181554001 DUP Plutonium-241 QC1201287997 LCS Plutonium-241 QC1201287994 MB Plutonium-241 QC1201287996 181554001 MS Plutonium-241 Rad Gamma Spec Batch 614269 QC1201288622 181554011 DUP Actinium-228 pCi/g 0 139 Uncert: TPU: Uncert: TPU: 140 U Uncert: TPU: 114+/-13.6+/-18.5 U -10.2+/-7.27+/-7.27 pCi/g pCi/g pCi/g (0% -100%) vIXA1 82 (75%-125%)

93 (75%-125%)

03/05/07 22:59 03/05/07 23:31 03/05/07 22:43 03/05/07 23:15 1.13+/-7.38+/-7.38 131+/-14.3+/-19.4 0.663+/-0.105 Uncert: 0.580+/-0.165+/-0.165 pCi/g 13 (0%- 100%) MJHI 03/06/07 09:20 100 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Page 3 of 13 REC% Ranee Anist Date Time Parmname~NOM Samnle Oual OC Units RPD%Parin ame NO Samnle Ouall Rad Gamma Spec Batch 614269 Americium-241 Bismuth-212 Bismuth-214 Cesium-134 Cesium-137 Cobalt-60 Europium-152 Europium-154 Europium-155 TPU: +/-0.105 UI 0.00 Uncert: +/-0.0338 TPU: +/-0.0338 0.358 Uncert: +/-0.133 TPU: +/-0.133 0.584 Uncert: +/-0.066 TPU: +/-0.066 UI 0.00 Uncert: +/-0.0198 TPU: +/-0.0198 0.0286 Uncert: +/-0.0158 TPU: +/-0.0158 U 0.0087 Uncert: +/-0.0112 TPU: +/-0.0112 U -0.00597 Uncert: +/-0.0342 TPU: +/-0.0342 U -0.0172 Uncert: +/-0.0317 TPU: +/-0.0317 U 0.0355 Uncert: +/-0.0322 TPU: +/-0.0322 0.601 Uncert: +/-0.057 TPU: +/-0.057 0.688 Uncert: +/-0.0705 TPU: +/-0.0705 UI 0.00 Uncert: +/-0.0192 TPU: +/-0.0192 U -0.00829 Uncert: +/-0.0107 TPU: +/-0.0107 9.85 Uncert: +/-0.733 TPU: +/-0.733 0.584 Uncert: +/-0.066 TPU: +/-0.066 UI 0.00 Uncert: +/-0.0186 U 0.0426+/-0.0313+/-0.0313 0.426+/-0.250+/-0.250 0.574+/-0.104+/-0.104 U 0.0285+/-0.0417+/-0.0417 0.0524+/-0.0329+/-0.0329 U -0.00623+/-0.0226+/-0.0226 U 0.0301+/-0.0575+/-0.0575 U 0.0353+/-0.0762+/-0.0762 U 0.00712+/-0.0682+/-0.0682 0.561+/-0.0761+/-0.0761 0.636+/-0.0949+/-0.0949 U 0.0172+/-0.0213+/-0.0213 U 0.00806+/-0.0207+/-0.0207 10.5+/-1.05+/-1.05 0.574+/-0.104+/-0.104 U -0.00294+/-0.0184 pCi/g 32 pCi/g 17 pCi/g 2 Lead-212 Lead-214 pCi/g 38 pCi/g 59 pCi/g 1210 pCi/g 299 pCi/g 579 pCi/g 133 pCi/g 7 pCi/g 8 pCi/g 29 pCi/g 14200 pCi/g 6 pCi/g 2 pCi/g 269 (0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)(0% -20%)(0% -20%)(0%- 100%)(0%- 100%)(0% -20%)(0%- 100%)(0%- 100%)Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver- 108m 101 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Parname Rad Gamma Spec Batch 614269 Page 4 of 13 REC% Range Anist Date Time NOM Sample Qual QC Units RPD%Thallium-208 QC1201288623 Actinium-228 Americium-241 Bismuth-212 Bismuth-214 Cesium-134 Cesium-137 Cobalt-60 Europium-152 Europium-154 Europium-155 TPU: +/-0.0186 0.222 Uncert: +/-0.0307 TPU: +/-0.0307+/-0.0184 0.206+/-0.0422+/-0.0422 pCi/g 8 (0%- 100%)LCS Uncert: TPU: 23.4 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: 9.47 Uncert: TPU: 13.6 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: U -0.131+/-0.424+/-0.424 24.8+/-2.79+/-2.79 U -0.185+/-0.725+/-0.725 U -0.0169+/-0.157+/-0.157 U 0.0492+/-0.104+/-0.104 10.5+/-0.974+/-0.974 14.3+/-0.902+/-0.902 U 0.334+/-0.226+/-0.226 U 0.119+/-0.194+/-0.194 U -0.242+/-0.250+/-0.250 U 0.0261+/-0.119+/-0.119 U 0.234+/-0.199+/-0.199 U 0.0316+/-0.0961+/-0.0961 U -0.00244+/-0.0784+/-0.0784 U 0.382 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g 03/06/07 09:21 106 (75%-125%)

111 (75%-125%)

105 (75%-125%)

Lead-212 Lead-214 Manganese-54 Niobium-94 Potassium-40 102 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Parnmame Rad Gamma Spec Batch 614269 Page 5 of 13 QC Units RPD% REC% Range AnIst Date Time NOM Sample Qual Radium-226 Silver- 108m Thallium-208 QC1201288621 Actinium-228 Americium-241 MB Bismuth-212 Bismuth-214 Cesium-134 Cesium-137 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU:+/-0.684+/-0.684 U -0.0169+/-0.157+/-0.157 U -0.0103+/-0.0823+/-0.0823 U -0.0347+/-0.0835+/-0.0835 U -0.0652+/-0.0589+/-0.0589 U 0.00251+/-0.0115+/-0.0115 U 0.00644+/-0.102+/-0.102 U 0.0459+/-0.0496+/-0.0496 U 0.0112+/-0.0149+/-0.0149 U -0.00466+/-0.0129+/-0.0129 U -0.00808+/-0.0183+/-0.0183 U 0.00549+/-0.0299+/-0.0299 U 0.015+/-0.0479+/-0.0479 U -0.00213+/-0.0211+/-0.0211 U 0.0126+/-0.0264+/-0.0264 U 0.0268+/-0.0225+/-0.0225 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g 03/06/07 09:20 (75%-125%)

Cobalt-60 Europium-152 Europium-154 Europium-155 Lead-212 Lead-214 103 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Parmname Rad Gamma Spec Batch 614269 Page 6 of 13 Range Anist NOM Sample Qual QC Units RPD% REC%Date Time Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver- 108m Thallium-208 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: U -0.000197+/-0.0136+/-0.0136 U 0.00221+/-0.0126+/-0.0126 U -0.025+/-0.200+/-0.200 U 0.0459+/-0.0496+/-0.0496 U -0.00878+/-0.00978

+/-0.00978 U 0.00629+/-0.0153+/-0.0153 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Batch 614271 QC1201288625 Actinium-228 Americium-241 181545014 DUP Bismuth-212 Bismuth-214 Cesium- 134 Cesium- 137 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: 0.904 0.957+/-0.254 +/-0.154+/-0.154 u -0.0532 U 0.0447+/-0.172 +/-0.0681+/-0.0681 0.851 0.735+/-0.336 +/-0.185+/-0.185 0.684 0.699+/-0.135 +/-0.0882+/-0.0882 UI 0.00 UI 0.00+/-0.0361

+/-0.020+/-0.020 0.180 0.159+/-0.0492

+/-0.0226+/-0.0226 UI 0.00 U 0.00959+/-0.0429

+/-0.0115+/-0.0115 U 0.0188 U -0.0235+/-0.084 +/-0.0315+/-0.0315 U -0.00496 U -0.0267+/-0.0988

+/-0.0354+/-0.0354 U -0.0215 U 0.0334 pCi/g 6 pCi/g 2320 pCi/g 15 pCi/g 2 pCi/g 16 pCi/g 12 (0% -100%) MJH1 03/06/07 15:09 (0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)Cobalt-60 pCilg pCilg 115 1810 Europium-152 Europium-154 Europium-155 (0%- 100%)(0%- 100%)(0%- 100%)(0%- 100%)pCi/g 137 pCi/g 926 104 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Page 7 of 13 QC Units RPD% REC% Range AnIst Date Time Parmname NOM Sample Qual Rad Gamma Spec Batch 614271 Lead-212 Lead-214 Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver- 108m Thallium-208 QC1201288627 Actinium-228 Americium-241 Bismuth-212 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU Uncert: TPU Uncert: TPU+/-0.0932 1.15+/-0.123 0.694+/-0.120 U 0.00553+/-0.0327 Ul 0.00+/-0.0476 15.6+/-1.57 0.684+/-0.135 u 0.0169+/-0.0272 0.431+/-0.078+/-0.0444+/-0.0444 1.11+/-0.0951+/-0.0951 0.747+/-0.0797+/-0.0797 U 0.0078+/-0.0146+/-0.0146 U -0.0046+/-0.0105+/-0.0105 16.7+/-1.08+/-1.08 0.699+/-0.0882+/-0.0882 U -0.015+/-0.0118+/-0.0118 0.328+/-0.0375+/-0.0375 U 0.569+/-0.765+/-0.765 26.5+/-3.15+/-3.15 U -0.0201+/-1.00+/-1.00 U -0.0978+/-0.230+/-0.230 U 0.0117+/-0.142+/-0.142 10.1+/-0.899+/-0.899 13.8+/-1.09+/-1.09 pCi/g 3 pCi/g 7 pCi/g 34 pCi/g 277 pCi/g 7 (0% -20%)(0% -20%)(0%- 100%)(0%- 100%)(0%- 20%)(0%- 20%)(0%-20%)(0%-20%)pCi/g 2 pCi/g 3400*pCi/g 27*LCS Bismuth-214 Cesium-134 Cesium- 137 Uncert: TPU: 23.4 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: 9.47 Uncert: TPU: 13.6 Uncert: TPU: pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g 113 (75%-125%)

03/06/07 10:34 107 (75%-125%)

102 (75%-125%)

Cobalt-60 105 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Parmname Rad Gamma Spec Batch 614271 Europium-152 Page 8 of 13 REC% Range AnIst Date Time NOM Sample Qual QC Units RPD%Europium-154 Europium-155 Lead-212 Lead-214 Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver-108m Thallium-208 QC1201288624 Actinium-228 Americium-241 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: U 0.278+/-0.344+/-0.344 U 0.243+/-0.300+/-0.300 U -0.279+/-0.297+/-0.297 U 0.0605+/-0.165+/-0.165 U -0.0593+/-0.222+/-0.222 U -0.00776+/-0.140+/-0.140 U -0.0288+/-0.114+/-0.114 U 0.170+/-0.533+/-0.533 U -0.0978+/-0.230+/-0.230 U 0.0732+/-0.129+/-0.129 U -0.0278+/-0.125+/-0.125 U 0.0458+/-0.0547+/-0.0547 U -0.00491+/-0.0131+/-0.0131 U 0.0485+/-0.115+/-0.115 U 0.0501+/-0.0327+/-0.0327 U 0.00236+/-0.0146 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pci/g pCi/g pCi/g pCi/g (75%-125%)

MB 03/06/07 12:25 Bismuth-212 Bismuth-214 Cesium-134 106 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Parmname Rad Gamma Spec Batch 614271 Page 9 of 13 Range AnIst Date Time NOM Sample Qual QC Units RPD% REC%TPU: Cesium- 137 Cobalt-60 Europium-152 Europium-154 Europium-155 Lead-212 Lead-214 Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU: Uncert: TPU:+/-0.0146 U 0.00471+/-0.0145+/-0.0145 U 0.00496+/-0.0196+/-0.0196 U 0.0178+/-0.0365+/-0.0365 U -0.00467+/-0.0456+/-0.0456 U 0.00865+/-0.0249+/-0.0249 U -0.0173+/-0.0241+/-0.0241 UI 0.00+/-0.0465+/-0.0465 U 0.0133+/-0.0158+/-0.0158 U 0.00628+/-0.0139+/-0.0139 U 0.0693+/-0.199+/-0.199 U 0.0501+/-0.0327+/-0.0327 U 0.00102+/-0.0122+/-0.0122 U 0.00736+/-0.0204+/-0.0204 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver- 108m Thallium-208 Rad Gas Flow Batch 613959 QC1201287893 181554003 DUP Strontium-90 QC1201287895 LCS Strontium-90 U 0.00352 Uncert: +/-0.0252 TPU: +/-0.0252 U 0.00451+/-0.0231+/-0.0231 pCi/g 0 (0% -100%) KSD1 03/06/07 16:15 1.47 1.44 pCi/g 98 (75%-125%)

03/06/07 16:16 107 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Page 10 of 13 REC% Range AnIst Date Time Parmname Rad Gas Flow Batch NOM Sample Qual QC Units RPD %613959 QC1201287892 MB Strontium-90 QC1201287894 181554003 MS Strontium-90 Uncert: TPU: Uncert: TPU:+/-0.102+/-0.111 U 0.0158+/-0.0212+/-0.0212 pCilg pCilg 03/06/07 16:15 03/06/07 16:16 4.21 U Uncert: TPU: 0.00352+/-0.0252+/-0.0252 Batch 613960 QC1201287897 181554022 DUP Strontium-90 QC1201287899 LCS Strontium-90 QC1201287896 MB Strontium-90 QC1201287898 181554022 MS Strontium-90 U 0.00562 Uncert: +/-0.0278 TPU: +/-0.0278 U 4.00+/-0.302+/-0.325 0.00794+/-0.0273+/-0.0273 1.52+/-0.118+/-0.150 95 (75%-125%)

pCi/g 0 (0% -100%) KSDI 1.46 Uncert: TPU: Uncert: TPU: 4.74 U Uncert: TPU: U 0.0103+/-0.0208+/-0.0208 pCilg pCi/g pCi/g 104 (75%-125%)

03/06/07 17:33 03/06/07 16:32 03/06/07 17:33 03/06/07 16:32 0.00562+/-0.0278+/-0.0278 4.50+/-0.387+/-0.457 95 (75%-125%)

Rad Liquid Scintillation Batch 613996 QC1201287991 181554001 DUP Iron-55 U 30.3 Uncert: +/-45.6 TPU: +/-45.6 U -21.8+/-43.5+/-43.5 pCi/g 0 (0% -100%) %IXP1 QC1201287993 LCS Iron-55 QC1201287990 MB Iron-55 1190 Uncert: TPU: Uncert: TPU: 1220 U Uncert: TPU: 1030+/-74.0+/-97.9 U 24.8+/-38.0+/-38.1 pCi/g pCi/g pCi/g 87 (75%-125%)

03/07/07 10:58 03/07/07 11:31 03/07/07 10:42 03/07/07 11:15 03/06/07 15:35 QC1201287992 181554001 MS Iron-55 30.3+/-45.6+/-45.6 1060+/-80.1+/-104 86 (75%-125%)

(0% -100%) \IXP1 Batch 613999 QC1201287999 181554001 DUP Nickel-63 U -7.41 U -5.76 pCi/g 0 108 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Page 11 of 13 Parnname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 613999 QC1201288001 LCS Nickel-63 QC1201287998 MB Nickel-63 Uncert: TPU: 567 Uncert: TPU: Uncert: TPU: 592 U Uncert: TPU:+/-7.32+/-7.32+/-7.95+/-7.95 451+/-21.4+/-26.9 U -1.36+/-7.77+/-7.77 pCi/g pCi/g pCi/g 80 (75%-125%)

03/06/07 16:07 03/06/07 15:19 03/06/07 15:51 QC1201288000 181554001 MS Nickel-63-7.41+/-7.32+/-7.32 466+/-22.4+/-28.2 79 (75%-125%)

Batch 614001 QC1201288003 181554001 DUP Technetium-99 QC1201288005 LCS Technetium-99 QC1201288002 MB Technetium-99 QC1201288004 181554001 MS Technetium-99 Uncert: TPU: U 0.221+/-0.245+/-0.245 U 0.249+/-0.241+/-0.241 pCi/g 0 (0% -100%) VIXPi 19.7 Uncert: TPU: Uncert: TPU: 19.7+/-0.445+/-0.659 U -0.0689+/-0.188+/-0.188 pCi/g pCi/g pCi/g 100 (75%-125%)

03/03/07 21:48 03/02/07 19:22 03/03/07 21:17 03/02/07 18:35 19.7 Uncert: TPU: U 0.221+/-0.245+/-0.245 19.4+/-0.493+/-0.690 99 (75%-125%)

Batch 614003 QC1201288007 181554014 DUP Tritium QC1201288009 LCS Tritium QC1201288006 MB Tritium QC1201288008 181554014 MS Tritium U -0.0488 Uncert: +/-1.61 TPU: +/-1.61 U 0.559+/-1.26+/-1.26 pCi/g 0 (0% -100%) '\XD2 03/03/07 03:48 11.2 Uncert: TPU: Uncert: TPU: 11.5 U Uncert: TPU: 12.5+/-1.71+/-1.72 U -0.309+/-1.19+/-1.19 pCi/g pCi/g pCi/g 111 (75%-125%)

03/03/07 05:52 03/03/07 02:45 03/03/07 04:50-0.0488+/-1.61+/-1.61 12.0+/-1.71+/-1.73 105 (75%-125%)

Batch 614005 109 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Parmname Rad Liquid Scintillation Batch 614005 Page 12 of 13 REC% Range AnIst Date Time NOM Sample Qual QC Units RPD%QC1201288011 181554014 DUP Carbon-14 QC1201288013 LCS Carbon-14 QC1201288010 MB Carbon- 14 QC1201288012 181554014 MS Carbon- 14 U 0.0483 Uncert: +/-0.0978 TPU: +/-0.0978 U 0.0496+/-0.0988+/-0.0988 6.78+/-0.203+/-0.229 pCi/g 0 (0% -100%) ALXD2 03/05/07 13:58 6.93 Uncert: TPU: Uncert: TPU: 7.05 U Uncert: TPU: U -0.0452+/-0.0947+/-0.0947 pCi/g pCi/g pCi/g 98 (75%-125%)

03/03/07 14:25 03/03/07 11:16 03/03/07 13:23 0.0483+/-0.0978+/-0.0978 6.87+/-0.205+/-0.231 97 (75%-125%)

Notes: The Qualifiers in this report are defined as follows: A B BD C D H J N/A ND R U UI X Y A h Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product For General Chemistry and Organic analysis the target analyte was detected in the associated blank.Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Analytical holding time was exceeded Value is estimated Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more Analyte concentration is not detected above the detection limit Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL Preparation or preservation holding time was exceeded 110 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder:

181554 Page 13of 13 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.** Indicates analyte is a surrogate compound.A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.ill EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 4 (DQA RESULTS)

EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 4A (PRELIMINARY DATA REVIEW)

I lealth 11tv, sics I1roCCdUre GIIIIARK iR-R512 1 -001 Attachment B. Iýc\. CY-00 I IMAJOIýI Ieahh Phx sies Procedure

(,PP-(.( ~( iR-R5 121 -001 Attaehmern IL Rex. CY-flO I MAJOR Preliminary Data Review Form -Samples for the Sign Test SUrx cy I nit: Surxe'N I(nit Name: ('lassification:

SurxeN Media: I pe o0 Surve: I'\ pe of Measurement:

Number ot Measurements:

Operational I)(iiL: 9514 0o001 Fast Primary Parking Lot Soil linal Status Surxc)(iross Measurement 15 BASI(C STA I IS] ICAI. QUAN] I l1IIS Cs- 137 Co-60 Sr-90 Minimum Value: -1.62E-03

-3.76E-03

-2.05E-02 Maxinurm Value: 8.44E-01 2.06E-02 6.81E-0I Mean: 1.22E-01 6.2 1 E-03 6.18E-02 Median: 5.04E-02 5.90E-03 1.62E-02 Standard I)eviation:

2.25E-01 6.81 E-03 1.80E-0 I Skew: 3.02E+00 8.05E-01 3.65E+00 RýAIDION UCLIIDE, Co-60 CONCENTRATION (pCi/g)Sr-90 Cs Identified?

NUMBIER Cs-137 Co Identified'!

Sr Ided 9514-0001-OOIF 2.71E-02 2.88E-03 -8.87E-04 YES NO NO 9514-0001-002F 6.23E-02 7.82E-03 -2.05E-02 YES NO NO 9514-0001-003F 1.57E-02 7.03E-03 3.52E-03 YES NO NO 9514-0001-004F 1.05E-01 2.06E-02 4.64E-02 YES NO YES 9514-0001-005F 5.04E-02 2.47E-04 9.28E-03 YES NO NO 9514-000!-006F 4.02E-02 7.60E-03 6.81E-01 YES NO YES 9514-0001-007F 6.41E-02 1.66E-03 1.58E-02 YES NO NO 9514-0001-009F 2.49E-02 5.94E-03 2.58E-02 YES NO NO 9514-0001-0 1 OF 3.59E-02 -3.76E-03 3.30E-02 YES NO YES 9514-0001-01 IF 3.70E-01 1.69E-02 3.26E-02 YES NO YES 9514-000I-012F 5.55E-02 5,27E-03 4.59E.02 YES NO YES 9514-0001-013F 1.19E-O1 5.90E-03 1.65E-02 YES NO NO 9514-0001-014F 8.44E-01 0.OOE+00 -3.44E-03 YES NO NO 9514-0001-015F

-1.62E-03 1.50E-02 -2.01E-02 NO NO NO 9514-0001-016F 1.91E-02 O.OOE+00 6.55E-03 NO NO NO J, 7 Perlornicd B1: f<, ~)1/4~ C D~ate: D~ate:_ _ _ __ _ _ _Independent Reve ('i Ilfalth Physics Procfdurf 24265-000-(i['P-(i(;(jR-R5123-000-Rev.('Y-00(lithith Physics Procfdurf 24265-000-GPP-(iGGR-R5 I 23-000-Rev.CY-00(Preliminary Data Review Form -.Judgemental Samples Survey Unit: Survey Unit Name: Classification:

Survey Media: Type oe Survey: Type oe Measurement:

Number of Measurements:

Operational DCGI: 9514- 0001 Ilast Primary Parking Lot 2 Soil Final Status Survey Gross Measurement 4 1 BASIC STATISTICAl.

QUANTITIES Cs-137 Co-60 Sr-90 Minimum Value: -8.66E'.-03 2.19F-02 -2.46F.-02 Maximum Value: 5.22E-01 7.97F-02 7.39E-02 Mean: 1.98E-01 4.46F-02 2.23F-02 Median: 2.35E-02 3.16E-02 6.32E-03 Standard Deviation:

2.30E-0 1 2.33E-02 3.53E-02 RADIONUCIIDE CONCENTRATION (pCi/g)NUMBER Cs-137 Cs ID'ed? Co-60 Co ID'ed Sr-90 Sr ID'ed > DCGL 9514-0001-024F

-7.30E-03 NO 3.16E-02 NO -1.78E-02 NO NO 9514-0001-025F

-8.96E-04 NO 2.51E-02 NO -4.16E-03 NO NO 9514-0001-026F 2.35E-02 YES 2.19E-02 NO -2.29E-03 NO NO 9514-0001-027F 1.07E-02 NO 3.15E-02 NO 6.32E-03 NO NO 9514-0001-028F 1.96E-02 NO 2.25E-02 NO 5.62E-03 NO NO 9514-0001-029F

-8.66E-03 NO 2.20E-02 NO -2.46E-02 NO NO 9514-0001-019J 5&22E-01 YES 7.92E-02 YES 7.39E-02 YES NO 9514-0001-020J 4.65E-01 YES 5.51 E-02 NO 3.46E-02 YES NO 9514-0001-021J 3.05E-01 YE. 5.23E-02 NO 5.01E-02 YES NO 9514-0001-022J 5.19E-01 YES 6,92E-02 NO 5.46E-02 YES NO 9514-0001-023J 3.34E-01 YES 7.97E-02 NO 6.94E-02 YES NO In e rfor ied By: Independent Re... .w:......Y_ 2 ý-Zoo :ýD~ate: D~ate: 3)/2--7 10 7 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 4B (GRAPHICAL REPRESENTATION OF DATA)

I lealth Mysics Procedure (;(;(;R-R5 123-Rev.CY-00 I Attachment C Quantile Plot For Cesium -137 Survey IUnit: 9514-0001 Survey ('nit Narne: t-ast Primary Parking ILot Mean: 1.221-01 p('i/g 0L C 0 L).9.OOE-01 8.OOE-01 7.O0E-01 6.OOE-01 5.O0E-01 4.OOE-01 3.OOE-01 2.OOE-01 1 .0E-01 0.OOE+00-1.O0E-01 140* * *.*.-20----..+~* * *-60~* 9-80 I Percentage Cs-1 37-1.62E-03 1.57E-02 1.91 E-02 2.49E-02 2.71 E-02 3.59E-02 4.02E-02 5.04E-02 5.55E-02 6.23E-02 6.41 E-02 1.05E-01 1.19E-01 3.70E-01 8.44E-01 Rank 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Percentage 3%10 %17 %23 %30 %37 %43 %50 %57 %63 %70 %77 %83 %90 %97 %Prepared By: / j, /7 Reviewe Y: Date: V Date: ,3 ]0"&

I lealth Physics ProccdUrc (;(;(;[Z-R5 I 23-Rev.(Y-00 I Attachment C Quantile Plot For Cobalt -60 Survey Unit: 9514-0001 Survey Unit Name: Fast Primary Parking Lot Mean: 6.211F-03 p('i/g 0)0 0.0 4-(U I-4-(U U 0 0 2OOE-02 1.80E-02 1.60E-02 1.40E-02 1.20E-02 1.OOE-02 8.OOE-03 6.OOE-03 4.OOE-03 20O0E-03 o.O0E+00-2.OOE-03-4.00E-034' 4 -., .4 I 20 40 60 S80 1)0Percentage CO-60-3.76E-03 O.OOE+OO O.OOE+OO 2.47E-04 1.66E-03 2.88E-03 5.27E-03 5.90E-03 5.94E-03 7.03E-03 7.60E-03 7.82E-03 1.50E-02 1 .69E-02 2.06E-02 Rank 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Percentage 3%10%17 %23 %30 %37 %43 %50 %57 %63 %70 %77 %83 %90 %97 %Prepared By: ,, , C Reviewed 4: Date: Date: 3 jo7 Health Physics Procedure GGGR-R5 I 23-Rev.CY-00 I Attachment C Quantile Plot For Strontium-90 Survey Unit: 9514-0001 Survey Unit Niame: East Primary Parking Lot Mean: 6.181-02 pCi/g 5. 70E-01 0.4 20E-01 0* 2.70E-01 C Uo 1.20E-01-3.OOE-02L 0.--- --- -... .. ....... .20 40 60 Percentage Rank Percentage

., 100 80-2.05E-02-2.01 E-02-3.44E-03-8.87E-04 3.52E-03 6.55E-03 9.28E-03 1.58E-02 1.65E-02 2.58E-02 3.26E-02 3.30E-02 4.59E-02 4.64E-02 6.81 E-01 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 30%10%17%23 %30 %37 %43 %50 %57 %63 %70 %77 %83 %90 %97 %Z(Prepared By: 4 1 Reviewed Date: Date: 93 01-)

I lealth Physics ProcedUrc Pr(i( R-R5123-Rcv.(CY-00 I Attachment C Frequency Plot For Cesium-137 Survey Unit: Survey UInit Name: Mean: 9514-0001 last Primary Parking Lot 0.122 pCi/g C LL 7 6 5 4 3 2 1 0 0.000 0.050 0.100 0.150 0.200 0.250 Upper End Value (pCi/g)Upper End Value 0.000 0.050 0.100 0.150 0.200 0.250 Total Observation Frequency* 1 6 4 2 0 2 15 Observation

%Frequency 7%40%27%13%0%13%100%'7.1 ~ --I.Prepared fly: I~. / ~ ) V Date: -/D~ate: 3/iS /07 Reviewed Bly.

Health Physics llroccdurc GGGR-R5123-Rev.CY-001 Attachment (C Frequency Plot For Cobalt-60 Survey Unit: 9514-0001 Survey Unit Name: Fast Primary Parking Lot Mean: 0.006 pCi/g 10 CU 0 8 6 4 2 0 I-0.030 -0.020 -0.010 0.000 0.010 0.020 0.030 Upper End Value (pCilg)Upper End Observation Observation

%Value Frequency Frequency-0.030 1 7%-0.020 0 0%-0.010 0 0%0.000 2 13%0.010 9 60%0.020 2 13%0.030 1 7%Total 15 , 100%(/ .<Prepared By: J I/ , ,I I1/4 , , Px D)ate: Reviewed P, :-a:-9 I)atc: 3ý 19)67 I lealth Physics Procedure (iG(iR-R5 123-Rev.CY-001 Attachment C Frequency Plot For Sr -90 Survey Unit: 9514-0001 1 Survey Unit Name: I:last Primary Parking Lot Mean: 0.062 pC i/g 10 8 6 0r U_2 0 0.01 0.03 0.05 0.09 0.18 0.35 0.70 Upper End Value (pCi/g)Upper End Observation Observation

%Value Frequency Frequency 0.01 7 44%003 3 19%0.05 5 31%0.09 0 0%0.18 0 0%0.35 0 0%0.70 1 6%S16 0Y Prepared By: 1/D)atc: cd k-Review D~ate: 3/z-)/7 K j EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 4C (SIGN TEST)

ItIcalth Physics Procedure (jI'I'-GGGR-R5121-000 A ttachnient A. Rex. CY-001 %,I AJOR Sign Test Calculation Sheet For Multiple Radionuclisdes Survey I nit Numbekr: 9514-0001 Surve, Unit Name: Fast Primar, Parking I.ot WVP&IR#: NA Classification

2 I YPIl I (u error):0.05 IYPE I (11 error):0.05 Rad ionunl ides: Cs- 137 Co-60 ( pcrational I)('(I. ( p(i/g): 2.59 Results ('s- 137 2.71 E-02 6.23E-02 1.57E-02 1.05E-01 5.04E-02 4.02E-02 6.41E-02 2.49E-02 3.59E-02 3.70E-01 5.55E-02 1.19E-01 8.44E-01-1.62E-03 1.91E-02 Results (o-60 2.88E-03 7.82E-03 7.03E-03 2.06E-02 2.47E-04 7.60E-03 1.66E-03 5.94F-03-3.76E-03 1.69E-02 5.27E-03 5.90E-03 O.00E+00 1.50E-02 0.00E+00 Results Sr-90 Weighted Sum (W,)-8.87E-04-2.05E-02 3.52E-03 4.64E-02 9.28E-03 6.81E-01 1.58E-02 2.58F-02 3.30E-02 3.26E-02 4.59E-02 1.65E-02-3.44E-03-2.01E-02 6.55E-03 5.30E-03-4.92E-03 8,98E-03 7.17E-02 1.83E-02 6.59E-01 2.76E-02 3.15E-02 3.66E-02 1.06E-01 5.61E-02 4.01E-02 1.54E-01-1.37E-02 9.79E-03 l)CGI .-Result 9.95E-01 1,00E+00 9.91E-01 9.28E-01 9.82E-01 3.41E-01 9.72E-01 9.69E-01 9.63E-01 8.94E-01 9.44E-01 9.60E-0 I 8.46E-001 1.01E+00 9.90E-01 Sr-90 1.05 Sign Number of Positive I)ifferences (S+ ): 15 (ritical Value: 13 Pertbrmed I :-Survc, (!nit Meets Acceptance Criterion z /Date: Independent i-D ate 3)1 J92c 1 EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 4D (QC SPLIT RESULTS)

Connecticut Yankee Decommissioning Project Health Physics Procedure 24265-000-GPR-GGGR-R5124-000 Attachment A Split Sample Assessment Form Survey.. Suve Survey Unit Survey 9514 SurvyyU00ni East Primary Parking Lot Area#: Unit #: Name: Sample Plan or WPIR#: NA SML #: 0 Sample

Description:

Comparison of split samples collected from sample measurement location #04 and analyzed using gamma spectroscopy by an off-site vendor laboratory.

The standard sample was 9514-0001-004F the comparison sample was 9514-0001-004FS.

STANDARD COMPARISON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable (Y/N)Value Error Range Value Error Ratio Cs-137 1.05E-.0i

.5.0OE-02 2 NONE- 1.51E-01.

4.97E-02 1.44 NA Co-60 2.06E-02 .2.26E-02 I NONE- 2.65E-02 3.34E-02 1.29 NA K-40 1.04E+01 9.92E-01 10 0.6- .1.66 1.II E+01 1.09E+00 1.07 Y Comments/Corrective Actions: With regard to the Cs-137 and Co-60 results, guidance for agreement ranges, obtained from USNRC Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of acceptability for such rations cannot be made. _-However, K-40 was found to be present at an acceptable level of agreement.

Therefore, no further action is warranted.

Table is provided to show acceptance criteria used to assess split samples.Resolution

[ Agreement Range 4 7 8 15 16 50 51 200> 200 0.50 0.60 0.75 0.80 0.85 2.00 1.66 1.33 1.25 1.18 WPIR -Work Plan and Inspection Record SML -Sample Measurement Location designation Page I of I Connecticut Yankee Decommissioning ProjSect Health Physics Procedure 24265-000-GPR-GGGR-R5124-000 Attachment A Split Sample Assessment Form Survey 9514 Survey 0001 Survey Unit Es Pm a g Area#: Unit #: Name: Sample Plan or WPIR#: NA, SML #: 0 Sample

Description:

Comparison of split samples collected from sample measurement location #10 and analyzed using gamma spectroscopy by an off-site vendor laboratory.

The standard sample was 9514-0001-01OF, the comparison sample was 9514-0001-01OFS.

STANDARD COMPARISON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable (Y/N)Value Error Range Value Error Ratio Cs-137 3.59E-02.

' 5.60E-03 6 0.5-2 2.86E-02 :7.90E-03 0.80 Y Co-60 -3.76E-03

-1.88E-'03 2 INONE -8.70E-03 5.60E-03 r-2.31 NA K-40 1.06E+01 5.30E+00 2 NONE -9.85E+00 3.67E-01 0.93 NA Comments/Corrective Actions: Cs-137 was found to be present at an acceptable level of agreement.

Therefore, no further action is warranted.

With regard to the Co-60 and K-40 results, guidance for agreement ranges, obtained from USNRC Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of acceptability for such rations cannot be made.Table is provided to show acceptance criteria used to assess split samples.Resolution I Agreement Range 4 8 16 51 7 15 50 200> 200 0.50 0.60 0.75 0.80 0.85 2.00 1.66 1.33 1.25 1.18 V : WPIR -Work Plan and Inspection Record SML- Sample Measurement Location designation Page I of I EAST PRIMARY PARKING LOT SURVEY UNIT 9514-0001 RELEASE RECORD ATTACHMENT 4E (COMPASS DQA WITH POWER CURVE)

DQA Surface Soil Report Assessment Summary Site: Planner(s):

Survey Unit Name: Report Number: Survey Unit Samples: Reference Area Samples: Test Performed:

Judgmental Samples: Assessment

==

Conclusion:==

9514-0001 rwm open land area 1 15 0 Sign Test Result: Not Performed 0 EMC Result: Not Performed Reject Null Hypothesis (Survey Unit PASSES)Retrospective Power Curve 1 0.9 m 0.8 ,0.7.0.6* 0.5 E- 0.4 i 0.3 96 0.2 0.1 O- 0-Iz__+/-1-__A_ _ _ __-r _i1~z __ ~_I f -_ _ _Ii __ _ "I__ __ i'-I!_ -.-l _!_ _ _- ._I _ _ _ !it-_ _ -.__0.0 0.2 0.4 0.6 0.8 1.0 Unity Rule Sum4f-Ratie, ielullug backgriud--Prospective Power E 1-beta .Actual Power-LBGR Power DCGL Retrospective Power 1.2 COMPASS v1.0.0 3/14/2007 Page I