ML071730449

Final Status Survey (FSS) Final Report - Phase VII - Chapter 4 of 19 - Appendix A3, Survey Unit Release Record 9312-0001, Containment (Former Radiologically Controlled Area)

ML071730449
Person / Time
Site:	Haddam Neck File:Connecticut Yankee Atomic Power Co icon.png
Issue date:	04/27/2007
From:	Wojtkowiak D Connecticut Yankee Atomic Power Co
To:	NRC/FSME
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Download: ML071730449 (163)

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Final Status Survey Final Report Phase VII Appendix A3 Survey Unit Release Record 9312-0001, Containment (Former Radiologically Controlled Area)

May 2007 41

C*YAPCO FINAL STATUS SURVEY RELEASE RECORD CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 931.2-0001 Prepared By.

0M "l4tA F.s Engineer Reviewed By:

FSS Engineer Approved By:

___-1 Tecimical Support Mianager Date: -4 1g 10-7 Date:

/

?(7 Revision 0

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD TABLE OF CONTENTS

1.

SURVEY UNIT DESCRIPTION...........................................

3

2.

CLASSIFICATION BASIS.................................................

3

3.

DATA QUALITY OBJECTIVES (DQO).................................

6

4.

SURVEY DESIGN.........................................................

10

5.

SURVEY IMPLEMENTATION..........................................

13

6.

SURVEY RESULTS.......................................................

14

7.

QUALITY CONTROL.....................................................

18

8.

INVESTIGATIONS AND RESULTS....................................

19

9.

REMEDIATION AND RESULTS........................................

20

10. CHANGES FROM THE FINAL STATUS SURVEY PLAN.......... 20

11. DATA QUALITY ASSESSMENT (DQA)...............................

20

12. ANOMALIES...............................................................

21

13. CONCLUSION..............................................................

21

14. ATTACHMENTS...........................................................

22 14.1 - Figures (7 pages including cover) 14.2 Attachment 2 - Scan Results (5 pages including cover) 14.3 Attachment 3 - Laboratory Data (I111 pages including cover) 14.4 Attachment 4 - DQA Results (17 pages including covers)

TOTAL 162 Revision 0

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD SURVEY UNIT DESCRIPTION Survey Unit 9312-0001 (Containment) is designated as Final Status Survey (ESS)

Class 1 and consists of approximately one thousand nine hundred-seventy five (1,975) square meters of open land and is located approximately one thousand four hundred eighty feet (1,480 ft) to the southeast of the site benchmark (Northing:

237370.20, Easting: 667394.57) site reference coordinate system benchmark used at Haddam Neck Plant (HNP) (see Attachment 1).

The survey unit is bounded as follows: land Survey Unit 93 12-0005 and land Survey Unit 93 12-0006 to the north (called north as oriented with the north to south flow of the Connecticut River), land Survey Unit 9312-0003 to the west and south and land Survey Unit 9312-0002 to the east and south.

As a result of demolition and remediation activities, the area topography is mostly flat and de-vegetated.

The survey unit has a moderate slope running from east to west.

The reference coordinates associated with this survey unit are E009 through E0 12 by S067 through S069 (refer to "HNP License Termination Plan" (LTP) Section 5.4.4).

The reference coordinates provide the maximum dimensions of a rectangle containing this survey unit. Some areas contained in this rectangle may not be part of this survey unit. The boundary of the survey unit was defined using a Global Positioning System (GPS) based on the Connecticut State Plane System North American Datum (NAD) 1927.

2.

CLASSIFICATION BASIS The survey unit was classified in accordance with Procedure RPM 5. 1-10, "Survey Unit Classification. "

The "Classification Basis Summary" conducted for Survey Unit 93 12-0001 consisted of:

a) A review of the 10CFR5O.75 (g) (1) database, b) A review of the "Initial Characterization Report" and the "Historic Site Assessment Supplement, "

c) Historic and current survey records review, d) Visual inspections and a "walkdown."

A review of the "Initial and Supplemental Characterization Reports" as well as the previous "Classification Basis Summaries" was performed. The source documents, the "Connecticut Yankee Haddam Neck Characterization Report" and "Initial Classification for Survey Areas at Connecticut Yankee", were incorporated by reference in LTP, Revision 0.

Revision 03 3

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD During plant operation, Survey Unit 9312-0001 was the location of significant, radiologically contaminated structures and systems, namely the reactor, the reactor systems and the Containment structure.

The Containment Building housed the reactor, reactor primary systems and components as well as numerous other support systems.

With the exception of various service water, gas and air systems, the majority of the systems within the Containment were radiologically contaminated. Radioactive material concentrations in many of these components and systems were high enough to create high radiation areas in their vicinity.

The entire Containment Building interior was posted as a "Contaminated Area". Hi storical surveys of the building show that significant levels of fixed and loose contamination were present in this structure. Some components, equipment, structural steel and concrete became radioactive due to neutron activation.

A review of the Historical Site Assessment and Supplement, as well as, other historical documents (e.g., the I OCFR5O.75(g)(l) files) indicated a significant number of operational events have impacted Survey Unit 9312-0001. These events included significant spills and leakage from contaminated systems. These events would have had the most impact on the radiological condition of subsurface structures and footers; and the underlying soil and bedrock prior to system and structural decontamination and demolition.

Major demolition and remediation activities began in 2002.

All contaminated systems and components located inside the Containment Building, including the reactor vessel, were removed and appropriately packaged and shipped to an approved off-site disposal facility. Interior structural surfaces inside the Containment Building were decontaminated to ensure contamination levels were acceptable for controlled demolition, Interior walls and floors were then demolished and removed.

The Containment liner was removed with the exception of the Incore Sump, which was filled with grout to the basement floor elevation. The remaining interior surfaces inside the Containment shell were decontaminated.

Following decontamination, the Containment basement was filled with soil to the grade of the exterior open land.

The above grade portion of the Containment structure was then demolished and removed. Fill was then placed over the survey unit, raising the grade of the area by approximately four (4) feet. No above grade structures currently remain within Survey Unit 93 12-000 1.

Outside of the structures, considerable remediation was performed on the soils surrounding the Containment structure, particularly around the northeast, northwest and southeast quadrants of the survey unit. A large excavation was created to the north of the Containment that was designated as Excavation #1. This excavation included the area in the vicinity of the Refueling Waster Storage Tank and the Primary Auxiliary Building (PAB) corridor. A second large excavation, designated as Excavation #2 was located over the Primary Auxiliary Building (PAB) footprint.

A third excavation, designated as Excavation #3 was located in the area between the Containment Building and Spent Fuel Building (SFB).

Revision 04 4

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD As adjacent structures were demolished, soil was excavated and removed.

This process continued until bedrock was exposed. Subsurface structures and footings that remained following demolition and excavation include the Containment Mat, the Cable Vault wall, the Service Building east wall, a remnant of the PAB northwest wall, Waste Disposal Building (WDB) footing and miscellaneous fragments of footings and slabs on the bedrock. As with the Containment basement shell, all excavations were backfilled following the performance of radiological assessments.

In Survey Area 9312, post-remediation soil samples were taken from the as-left surface soils under two (2) Survey and Sampling Work Plans, SSWVP-06-08-000 and SSWPT-06-12-001.

Thirty-five (35) post remediation surface soil samples were collected from the various locations within Survey Area 9312.

All samples were collected and analyzed by gamma spectroscopy by an approved off-site laboratory.

Ten (10) of the thirty-five (35) post remediation samples collected were analyzed for the full suite of "Hard-to-Detect" (HTD) radionuclides specified in the LTP, Table 2-12, "Radionuclides Potentially Present at Haddam Neck Plant" and as provided in Table 3. Statistical quantities (mean, median and standard deviation) from the 2006 post-remediation survey conducted under SSWP-06-08-000 and SSWP-06-12-001 are provided in Table 1.

Minimum Value:

1.32E-02

-5.OOE-02 Maximum Value:

1.70E+00 1.43E+/-00 Mean:

2.3 8E-0lI 1.08E-01 Median:

1.65E-01 1.46E-02 Standard Deviation: T3.

1OE-0 I 2.76E-0lI A review of this sample data shows Cs-137 and Co-60 to be the primary radionuclides of concern, with both isotopes reported at fairly low concentrations.

The sample population as a whole was evaluated to assess the distribution of the detected radionuclides. The radionuclide distribution percentage for each sample in the population was calculated by dividing the concentration of each detected radionuclide by the total activity concentration in the sample, expressing the abundance of the specific nuclide in the sample compared against the total activity.

The mean radionuclide distribution was then calculated by taking the average of the individual sample distribution fractions. The results are provided in Table 2.

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CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD Cs-137 0.689 Co-60 0.3 11 No HTD radionuclides were positively identified in concentrations meeting the accepted criteria for detection (i.e., a result greater than two (2) standard deviations uncertainty). Radionuclide screening or de-selection is a process where an individual radionuclide or aggregates may be considered insignificant and eliminated from the FSS.

The criteria for de-selection are concentrations less than 5% for individual radionuclides and less than 10% for aggregates.

While Sr-90 was not identified in the soil characterization results, it was decided to include Sr-90 is a radionuclide of concern for this survey unit as Sr-90 was prevalent in the soils prior to remediation. Therefore, all volumetric soil samples taken as part of the survey design for this survey unit were subjected to direct analysis for Sr-90.

The FSS Engineer performed a visual inspection and walk-down during March 2007 to assess the physical condition of the survey unit, evaluate access points, travel paths and identify potentially hazardous conditions.

This survey area is affected by existing and future groundwater (reference CY memo ISC 06-024) which will be a source of dose from residual radioactivity, as discussed in Section 3 under the Data Quality Objectives.

Based upon the identification of radioactive material above the Derived Concentration Guideline Levels (DCGLs), and the need for radiological remediation, it was concluded that there was some probability for residual radioactivity in concentrations greater than the DCGLs, justifying a final survey unit classification of Class 1 (refer to Section 3).

3.

DATA QUALITY OBJECTIVES (DQO)

FSS design and planning used the Data Quality Objective (DQO) process as described by the LTP, Procedure RPM 5. 1-11, "Preparation of Final Status Survey Plan," and the "Multi-Agency Radiation Survey and Site Investigation Manual" (MARSSIM).

A summary of the main features of the DQO process are provided herein.

The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition.

The baseline condition is technically known as the null hypothesis.

Revision 06 6

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria.

The primary objective of the FSS plan was to demonstrate that the level of residual radioactivity in Survey Unit 9312-0001 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of DCGLs. The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations.

Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil (called Base Case Soil DCGL), existing groundwater radioactivity and future groundwater radioactivity that will be contributed by building basements and footings.

The DCGLs presented in Chapter 6 of the LTP were developed for exposures from three (3) components, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity.

Equation 1 shows the mathematical relationship between the three (3) components and the total dose.

Equation 1 Hiotai -H Soil +/-H ExistingGW +/-H FutureG W The total dose under the LTP criteria is twenty-five (25) mrem/yr Total Effective Dose Equivalent (TEDE) from all three (3) components. The allowable total dose under the Connecticut Department of Environmental Protection (CTDEP) radiological remediation standard for CY is nineteen (19) mrem/yr TEDE. To satisfy both the LTP and CY CTDEP criteria, the dose from soil must be reduced when using the existing and future groundwater dose values discussed above.

This survey area is affected by existing groundwater (reference CY memo ISC 06-024). Therefore, the dose contribution from existing groundwater is bounded by two (2) mrem/yr TEDE.

This survey unit is considered impacted by future groundwater radioactive contamination, as there are underground foundations containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024).

The dose contribution from future groundwater, the third dose component, is bounded by two (2) mremlyr TEDE.

Revision 07 7

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD Equation 2 19 mremlyrTotal, = 15 mremf/yrs,)j1 + 2 mrem/yrExisting ow+ 2 mrem/yrFutureGW The allowable dose for soil in this survey unit is fifteen (15) mrem/yr TEDE as shown by Equation 2 above. The concentration of residual radioactivity resulting in fifteen (15) mremlyr TEDE is designated as the Operational DCGL (DCGLop), and has been established for the radionuclides of concern as provided in Table 3.

Revision 08 8

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD H-3 4.12E+02 2.47E+02 1.65E+01 C-14 5.66E+00 3.40E+00 2.26E-01 Mn-54 1.74E+01I 1.04E+01 6.96E-01 Fe-55 2.74E+04 1.64E+04

1. 1 OE+03 Co-60 3.8 1 E+00 2.29E+00 1.52E-0 1 Ni-63 7.23E+02 4.34E+02 2.89E+0 1 Sr-90 1.55E+00 9.30E-0 1 6.20E-02 Nb-94 7.1 2E+00 4.27E+00 2.85E-0 1 Tc-99 1.26E+/-01 7.56E+00 5.04E-0OI Ag-i 08m 7.1 4E+00 4.28E+00 2.86E-0 1 Cs-134 4.67E+00 2.80E+00 1.87E-01 Cs-137 7.9 1E+00 4.75E+00 3.16E-01 Eu-152 l.O1E+01 6.06E+00 4.04E-0OI Eu-154 9.29E+00 5.57E+00 3.72E-01 Eu-155 3.92E+02 2.35E+02 1.57E+01 Pu-238 2.96E+0l Il.78E+01

1. 18E+00 Pu-239/240 2.67E+O1 Il.60E+01 1.07E+00 Am-241 (5) 2.5 8E+O1 Il.55E+01 1.03E+/-00 Pu-241 8.70E+02 5.22E+02 3.48E+O I Cm-2431244 2.90E+O 1 1.74E+0 1

1. 16E+00 (1)

Bold indicates those radionucidies considered Hard to Detect (HTD)

(2)

The Base Case Soil DCGL(s) are specified by the LTP in Chapter 6 and are equivalent to twenty-five (25) mrem/yr TEDE (3)

The Operational DCGL is equivalent to achieving fifteen (15) mremlyr TEDE (4)

The required MDC is equivalent to achieving one (1) mremlyr TEDE (5)

Americium-241 can be analyzed by gamma and alpha spectroscopy and is considered to be Easy to Detect (ETD). The preferred result is the alpha spectroscopy's when both analyses are performed Revision 09 9

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration variability. Soil samples were collected in 2006 to establish the radiological condition of Survey Unit 9312-0001 for FSS.

Cs-137 and Co-60 were the two (2) gamma emitting radionuclides reported in concentrations with the potential for exceeding the release criteria.

Sr-90 was included as a radionuclide of concern due to its prevalence in the soil prior to remediation.

The characterization data were used for the survey design and are provided in Table 1.

Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the DCGL. Survey instrument response checks were required prior to issue and after the instrument had been used. Control and accountability of survey instruments was required to assure the quality and prevent the loss of data.

As, part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results.

Results reported as less than Minimum Detectable Concentration (MDC) were not accepted for FSS. Sample report summaries included unique sample identification, analytical method, radionuclide, result, and uncertainty to two (2) standard deviations, laboratory data qualifiers, units, and the required and observed MDC.

4.

SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in Procedure RPM 5.1-11, "Preparation of Final Status Survey Plans". The FSS plan uses an integrated sample design that combines scanning surveys and sampling which can be either random or biased.

The DQO process determnined that Cs-137, Co-60 and Sr-90 would be the radionuclides of concern in Survey Unit 93 12-0001 (refer to Section 3).

The characterization survey did not include any other additional HTD radionuclides of concern for this survey unit.

As Sr-90 concentrations were determined by direct analysis, surrogate DCGLs were not required as part of the survey design for this survey unit via screening under LTP Section 5.4.7.2, "Gross Activity DCGLs". Other radionuclides that were positively identified in concentrations greater than the screening criteria during the performnance of this FSS would be evaluated to ensure adequate survey design.

As the survey unit is classified as a Class 1 surface soils area, and discrete, elevated areas of contamination was possible, the application of the Elevated Measurement Comparison (EMC) remained an option.

The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.

Revision 0 to

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD The number of soil samples for FSS was determined in accordance with Procedure RPM 5.1-12, "Determination of the Number of Surface Samples for Final Status Survey." The Lower Bound of the Gray Region (LBGR) was set in accordance with Procedure RPM 5. 1-11 ito 0.73 to achieve a relative shift (A/cy) in the range of 1 and 3.

The resulting adjusted relative shift was 2.0.

A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARS SIM in support of the decommissioning license termination rule (I OCFR2O, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design. The survey design specified. fifteen (15) surface soil samples for non-parametric statistical testing. Based upon a review of the historical information and Characterization Survey data, four (4) judgmental samples were taken in this survey area.

One (1) judgmental sample was taken at the northeast corner of the survey unit in the vicinity of the "Tank Farm" excavation; two (2) judgmental samples were taken in the southeast corner of the survey unit in the vicinity of the Fuel Transfer Tube excavation and the Spent Fuel Building foundation and one (1) judgmental sample was taken in the northwest quadrant in the vicinity of the Primary Auxiliary Building excavation.

The grid pattern and locations of the soil samples were determnined using Visual Sample Plan (VSP) in accordance with Procedure RPM 5.1-14, "Identifying, and Marking Surface Sample Locations for Final Status Survey." Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy. A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate for a Class 1 area.

Sample locations were identified using AutoCAD-LT, a commercially available plotting software package with coordinates consistent with the Connecticut State Plane System.

These coordinates were integrated with a GPS to locate sample locations in the field. Sample Measurement Locations for the design are listed with the GPS coordinates in Table 4.

9312-0001-OOIF 236653.27 668703.89 93 12-0001-002F 236653.27 668744.35 9312-0001-003F 236618.24 668683.67 9312-0001-004F 236618.24 668724.12 9312-0001-005F 236618.24 668764.58 9312-0001-006F 236618.24 668805.03 Revision 0 1I I

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD 93 12-0001-007F 236583.20 668663.44 93 12-0001-008F 236583.20 668703.89 9312-0001-009F 236583.20 668744.35 9312-0001-OlOF 236583.20 668784.80 93 12-0001-01 lF 236583.20 668825.26 9312-0001-012F 236548.17 668683.67 9312-0001-013F 236548.17 668724.12 9312-0001-014F 236548.17 668764.58 9312-0001-015F 236513.14 668744.35 93 12-0001-016B(')

236676.51 668734.75 9312-0001-017B~')

236622.41 668815.99 9312-0001-018B(')

236599.54 668836.44 9312-0001-019B~')

236594.08 668662.08 (1) B = biased - indicates judgmental sample location Procedure RPM 5.1-11 specifies that 5% of the samples are required to be selected for HTD analysis. Two (2) soil samples, or 13% of the number of samples that would be used for non-parametric statistical testing were randomly selected for HTD radionuclide analysis using the Microsoft Excel "RANDBETWEEN" function. Each sample was sent off-site for a full suite analysis of the HTD radionuclides specified in the LTP, Table 2-12, "Radionuclides Potentially Present at Haddam Neck Plant" and as provided in Table 3.

The LTP requires a minimum of 5% of the samples taken for non-parametric statistical testing be selected for QC evaluation.

The implementation of quality control measures as referenced by Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey," included the collection of one (1) soil sample for "split sample" analysis by the off-site laboratory.

This location was selected randomly using the Microsoft Excel "RANDBETWEEN" fuinction.

The LTP specifies a required scanning coverage of 100% for outdoor Class 1 areas.

For this Class 1 survey unit, the "Investigation Level" for area scanning and soil sample measurement results are those levels specified in LTP, Table 5-8.

Table 5 provides a synopsis of the survey design.

Revision 0 112

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UINIT 93 12-0001 RELEASE RECORD Survey Unit Land Area 1,975 M2 Based on AutoCAD-LT Type 1 and Type 2 errors were 19 0.05, sigma was 0. 14 pCilg, the Number of Measurements (15 systematic grid)

LBGR was set at 0.73 to achieve a (4 judgmental)

Relative Shift in the range of I and 3

Grid Spacing 12.29 mn Based on triangular grid 4.75 pCi/g Cs-137 Administratively set to achieve Operational DCGL 2.29 pCi/g Co-60 fifteen (15) mremlyr TEDE ~

0.93 pCi/g Sr-90 4.75 pCi/g Cs-137 The Operational DCGL meets the Soil Investigation Level 2.29 pCi/g Co-60 LTP criteria for a Class I survey 0.93 pCi/g Sr-90 unit Scan Survey Area Approximately The LTP requires 100% area Coverage 100% of the area coverage for Class 1 survey units An instrument response greater than the Scan Scan Investigation Level MDC(DCGLEMC)

Per BCY-HP-0239 Revision #0 of 2,000 cpm plus ambient background (1) The allowable dose for soil in this survey unit is fifteen (15) mrem/yr TEDE as the bounding dose from existing and future groundwater has been established based on field data (reference CY memo ISC 06-024)

5.

SURVEY IMPLEMENTATION Final status survey field activities were conducted under a Final Status Survey Plan (FSSP). The FSSP package included a detailed survey plan, job safety analysis, job planning checklist and related procedures for reference.

Daily briefings were conducted to discuss the expectations for job performance and the safety aspects of the survey. The "Daily Survey Journal" was used to document field activities and other inform-ation pertaining to the FSS.

A single scan area was established that constituted approximately 100% of the surface area of Survey Unit 9312-0001. Grid lines, one (1) meter wide, were painted on the ground of the scan area. A background survey was performed around the survey unit and it was determined that, using an Eberline E-600 with a SPA-3 sodium iodide detector, background ranged from 7,170 counts per minute (cpm) up to 13,200 cpm.

Revision 0 113

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 9312-0001 RELEASE RECORD The scan area was established and scanned for elevated readings (see Attachment 2 for all scan results). Scanning was performed with an Eberline E-600 using a SPA-3 sodium iodide detector. The E-600 was operated in the rate-meter mode and used with audio response. The probe was positioned as close to the ground as possible and was moved at a scan speed of about 0.5 meters per second. Approximately 100% of the survey unit was scanned.

Meastfr ement locations were identified* in North American Datum (NAD) 1927 coordinates using GPS coordinates; sample locations were identified and marked with a surveyor's flag or paint for identification. At each sample location, a one (1) meter radius circle was established around the sample flag or paint mark was scanned for elevated radiation levels.

Nineteen (19) surface soil samples were collected and packaged in accordance with Haddam Neck Plant (HNP) Procedure RPM 5.1-3, "Collection of Sample Media for Final Status Survey" and FSS design. Samples were controlled, transported, stored, and transferred to the off-site laboratory using Chain-of-Custody (COC) protocol in accordance with Procedure RPM 5.1-5, "Chain of Custody for Final Status Survey Samples."

Two (2) samples (93 12-0001-005F and 9312-0001-015F) were randomly selected for HTD radionuclide analysis.

The implementation of survey specific quality control measures included the collection of one (1) sample (9312-0001-003F) for "split sample" analysis.

6.

SURVEY RESULTS All field survey activities were conducted between March 24, 2007 and March 26, 2007.

The sample locations identified in the FSS plan were scanned over approximately a one (1) meter radius for elevated radiation levels. Table 6 provides an overview of the scan results for sample measurement locations.

Scan results are provided in.

I 7.64 10.52 NO 2

9.73 10.94 NO 3

10.20

{

11.19 NO 4

10.30 10.89 NO Revision 0 114

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD 5

9.45 11.33 NO 6

8.64 10.66 NO 7

9.52 10.70 NO 8

9.92 12.00 NO 9

12.40 14.40 NO 10 12.10 14.20 NO 1 1 11.00 12.20 NO 12 10.80 11.44 NO 13 9.42 10.83 NO 14 10.50 12.10 NO 15 10.30 11.46 NO 16 (2) 7.79 9.62 NO 17 (2) 10.30 11.63 NO 18(2) 9.96 11.96 NO 19(2) 8.72 9.95 NO (1) The action level is based on a measurement in accordance with the FSS plan (MDC(DCGLEMC) of 2,000 cpm plus ambient background)

(2) Indicates judgmental sample locations (biased)

The scan area, that comprised approximately 100% of the total surface area for the survey unit, was scanned for elevated radiation levels. The area was scanned in accordance with the FSS plan on March 24, 2007 and March 26, 2007.

Fifty-one (51) scan strips were initially established in this survey unit. Seven (7) elevated measurement locations were identified during scanning. Table 7 provides an overview of the scan area survey. Scan results are provided in Attachment 2.

Revision 0 115

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD 1 thru 10 11.20 13.10 INone None IlIthru 20 10.20 12.20 None None 21lthru 30 13.40 15.20 None None 9312-01 -ER-00 1 9312-0001-020-1 9312-01 -ER-00 1 9312-0001-021-1 31lthru 40 15.40 14.30 9312-01-ER-00-35-1 9312-0001-022-1 93 12-01-ER-00-36-1 9312-0001-023-1 9312-01 -ER-00 1 9312-0001-024-1 41lthru 51 15.00 12.00 9312-01 -ER-00-4 1-1 9312-0001-025-1 9312-01 -ER-00 I 9312-0001-026-1 (1) The action level is based on a measurement in accordance with the FSS plan (MDC(DCGLEMC) Of 2,000 cpm plus ambient background)

The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories, LLC. The laboratory analyzed the fifteen (15) samples collected for non-parametric statistical testing, the associated field splits and the four (4) judgmental samples using gamma spectroscopy. Gamma spectroscopy analysis was performed to the required MDCs.

Gamma spectroscopy results identified some radionuclides meeting the accepted criteria for detection (i.e., a result greater than two (2) standard deviations uncertainty). However, Cs-137 was the only gamma-emitting radionuclide reported in any appreciable concentration.

Cs-137 was positively identified in six (6) of the fifteen (15) samples collected for non-parametric statistical testing. Co-60 was positively identified in one (1) sample from the statistical sample population.

The mean of the gamma spectroscopic analysis results for the sample population indicated that Cs-137 was present at levels at or below expected environmental levels for Cs-137 within the vicinity of the HNP as presented in the Health Physics TSD BCY-HP-0063.

The "sum-of-fractions" or "unity rule" is the mathematical test used to evaluate compliance with radiological criteria for license termnination when more than one radionuclide has been determined to be potentially present. The combination of the fractions of each detected radionuclide against their respective Operational DCGL must be less than or equal to one (1).

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CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD The unity rule is:

Equation 3 C,

C2 C,,

DCGL, DCGL 2 DCGL,,

Where:

C,,

concentration of radionuclide n and.

DCGL,, = DCGL of radionuclide n.

A summary of the fifteen (15) samples collected for non-parametric statistical testing results as well as the results of the unity rule calculation for the identified radionuclides are provided in Table 8.

93 12-000 1-OOIF 1

.28E-02 1.39E-02 9312-0001-002F 7.15E-02

-7.8 1E-04 0.015 9312-0001-003F 0.OOE+/-00 2.42E-02 9312-0001-004F 6.82E-02 4.22E-04 0.014 9312-0001 -005F 5.55E-02

2. 14E-03 0.0 12 9312-0001 -006F 4.1 2E-02 2.0 1E-03 0.009 93 12-0001-007F

-6.43E-03

-4.50E-03 9312-0001 -008F

-2.1 7E-03 2.3 7E-03 9312-0001-009F 4.70E-03

-4.23E-03 9312-0001 -01 OF 7.99E-02 3.97E-03 0.017 9312-0001-011 IF

-2.03E-02 2.57E-02 0.007 9312-0001-012F 1.20E-02 3.94E-03 0.003 9312-0001-013F 1.38E-02 2.02E-03 9312-0001-01 4F

-6.46E-03

-1.85E-03 9312-0001-015SF

-2.30OE-03 1.22E-02 (1) "-" indicate that the radionuclide was not positively detected in the sample (2) The Operational DCGL from Table 2 is 4.75 pCi/g for Cs-137 and 2.29 pCi/g for Co-60 to achieve fifteen (15) mrem/yr TEDE respectively.

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CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD In addition to the non-parametric statistical sample population, four (4) judgmental surface soil samples were taken at biased locations. These locations were selected by the FSS Engineer based upon a review of the historical site assessment for this area and previous survey results. These judgmental soil samples were analyzed for Cs-137, Co-60 and Sr-90 in accordance with the DQOs used during the survey design.

A summary of the four (4) judgmental samples collected as well as the results of the unity rule calculation for the identified radionuclides are provided in Table 9.

9312-0001-016B 1.7 1E-02

-4.65 E-04 9312-0001-017Bj 5.01 E-04 6.58E 9312-0001-018B

-4.40E-03

7. 1 OE-03 0.0 93200109l.71E-02 5.30E-03 0.0 (1) -- " indicate that the radionuclide was not positively detected in the sample (2) The Operational DCGL from Table 2 is 4.75 pCi/g for Cs-137 and 2.29 pCi/g for Co-60 to achieve fifteen (15) mrem/yr TEDE respectively.

(3) B = biased - indicates judgmental sample location In addition to Cs-137 and Co-60, Sr-90 was also identified during the DQO process as a radionuclide of concern. Subsequently, all samples were subjected to analysis by gas proportional counting for Sr-90. All analyses met the required minimum MDC.

Sr-90 was not positively identified (i.e., a result greater than two (2) standard deviations uncertainty) in any of the fifteen (15) samples collected for non-parametric statistical testing nor in any of the judgmental soil samples. In addition to Sr-90, the off-site laboratory also processed, as required by the sample plan, two (2) samples for the full suite of HTD radionuclides as specified in LTP, Table 2-12, "Radionuclides Potentially Present at Haddam Neck Plant" and as provided in Table 3. The requested analyses included alpha spectroscopy, gas proportional counting, and liquid scintillation depending on the radionuclide and the measurement method.

All analyses performed met the required minimum MDC. No other HTD radionuclides were positively identified.

7.

QUALITY CONTROL The off-site laboratory processed the split samples and performed gamma spectroscopy analysis. One sample location was selected for analysis, which exceeds the 5% minimum required by the LTP.

The data were evaluated using USNRC acceptance criteria specified in Inspection Procedure 84750 as detailed in HNP Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey ".

Revision 0 18

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD Cs-137 was not detected in sufficient quantity in the field split results at location 93 12-0001-003FS to evaluate in accordance with procedure. Evaluation using the reported results for naturally occurring K-40 resulted in acceptable agreement between the field-split results at this location.

The sample analysis vendor, General Engineering Laboratories, LLC, maintains quality control and quality assurance plans as part of normal operation. Refer to Attach ments 3 and 4 for data and data quality analysis results

8.

IN~VESTIGATIONS AND RESULTS Seven (7) investigative surface soil samples were collected from several scan areas exhibiting elevated scan readings.

These soil samples were analyzed for Cs-137, Co-60 and Sr-90 in accordance with the DQOs used during the survey design. The Investigative Sample designations are listed with the GPS coordinates in Table 10.

9312-0001-020-1 236596.22 668760.32 9312-0001-021-1 236591.06 668722.54 9312-0001-022-1 236588.64 668780.33 9312-0001-023-1 236591.73 668782.14 9312-0001-024-1 236593.28 668785.43 9312-0001-025-1 236598.60 668800.13 9312-0001-026-I 236600.66 668803.01 A summary of the seven (7) investigative samples collected as well as the results of the unity rule calculation for the identified radionuclides are provided in Table 11.

9312-0001-020-1 2.15E-03 2.76E-02 9312-0001-021-I

-4.99E-03

-2.38E-02 9312-0001-022-1 1.07E-02

-1I.59E-02 9312-0001-023-I

-2.3 1E-02 7.70E-03 Revision 0 119

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD 0111 AtAA1AY)AA I KIr ~T OA I KM; Al) 9312-0001-025-1 5.90E-03 1.47E-02 9312-0001-026-I

-1.45E-02 8.34E-03 (4) "-" indicate that the radionuclide was not positively detected in the sample (5) The Operational DCGL from Table 2 is 4.75 pCi/g for Cs-137 and 2.29 pCi/g for Co-60 to achieve fifteen (15) inrer/yr TEDE respectively.

(6) 1 = Investigation - indicates investigative sample location Cs-137, Co-60 and Sr-90 were not positively identified in any of the seven (7) samples collected for investigation.

Gamma spectroscopy results identified some radionuclides meeting the accepted criteria for detection (i.e., a result greater than two (2) standard deviations uncertainty). However, no gamma emitting radionuclide was reported in any concentration greater than its respective MDC.

9.

REMEDIATION AND RESULTS Radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to FSS. All excavations were characterized and backfilled prior to performing FSS. In the area where remediation occurred, the ground area is comprised of barren dirt with no vegetation, and the soils have been graded relatively flat to the corresponding elevation of the adjacent survey units.

The results for Cs-137 following remediation were well below the Operational DCGL provided in Table 3.

Health Physics TSD BCY-HP-0078, "ALARA Evaluation of Soil Remediation in Support of Final Status Survey, " determined that remediation beyond that required to meet the release criteria is unnecessary and that the remaining residual radioactivity in soil was ALARA.

10.

CHANGES FROM THE FINAL STATUS SURVEY PLAN No changes were made to the FSS plan.

11.

DATA QUALITY ASSESSMENT (DQA)

The DQO sample design and data were reviewed in accordance with Procedure RPM 5.1-23, "Data Quality Assessment, " for completeness and consistency. The sampling design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected.

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CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 9312-0001 RELEASE RECORD Documentation was complete and legible.

Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 1.

The preliminary data review consisted of calculating basic statistical quantities (e.g.,

mean, median, standard deviation). The mean and median values are well below the Operational DCGL.

Also, the retrospective power curve shows that a sufficient number of samples were cOllected to achieve the desired power.

Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs. The basic statistical quantities for the statistical sample population are provided below in Table 9.

DCGLoP:

4.75E+/-00 2.29E+/-00 9.30E-01 Minimum Value:

-2.03E-02

-4.50E-03

-3.49E-02 Maximum Value:

7.99E-02 2.57E-02 2.82E-02 Mean:

2.15E-02 5.43E-03

-3.5 1E-03 Median:

1.20E-02 2.14E-03

-7.40E-04 Standard Deviation:

3.28E-02 9.40E-03 1.44E-02 Cs-137 was positively detected in six (6) of the samples collected for non-parametric statistical testing. The range of the data is less than one (1) standard deviation and the data set exhibits a calculated positive skew of 0.74.

The Cs-137 results are represented graphically through posting plots, a frequency plot, and a quantile plot.

Co-60 and Sr-90, although included in the FSS plan for compliance purposes, was positively identified in only one (1) of the fifteen (15) samples collected for non-parametric statistical testing.

Assessment of the basic statistical quantities and graphical representation of Co-60 and Sr-90 was not considered useful given the non-existent number of actual data points to represent the distribution.

All data, assessments, and graphical representations are provided in Attachment 4.

12.

ANOMALIES No anomalies were noted.

13.

CONCLUSION Survey Unit 9312-0001 has met the final DQOs of the FSS plan.

The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved.

Elevated Measurement Comparison was not required.

Revision 0 21

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD All positively identified radionuclides of concern were used for statistical testing to determine the adequacy of the survey unit for FSS.

The sample data passed the Sign Test.

The null hypothesis was rejected.

The Retrospective Power Curve generated using COMPASS shows adequate power was achieved. The survey unit is properly designated as Class 1.

The dose contribution from soil is 0.10 mremlyr TEDE based on the average concentration of the samples used for non-parametric statistical sampling.

This survey area is affected by existing groundwater (reference CY memo ISC 06-024); therefore the dose contribution from existing groundwater is bounded at two (2) mrem/yr TEDE.

This survey unit is considered impacted by future groundwater radioactive contamination, as there are underground foundations containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component, is bounded by two (2) mremlyr TEDE.

The average total dose from residual radioactivity in this survey unit, including exposures from the three (3) components as described in Section 3, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity will not exceed 4.10 mremlyr TEDE. Therefore, Survey Unit 9312-0001 is acceptable for unrestricted release.

14.

ATTACHMENTS 14.1 Attachment 1 - Figures 14.2 Attachment 2 - Scan Results 14.3 Attachment 3 - Laboratory Results 14.4 Attachment 4 - DQA Results Revision 0 222

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD ATTACHMENT 1 (FIGURES)

Revision 0

= Wet Land Notes Notes Coordinates =etin NAD27Connwatscnt State PAme System, Connecticut Yankee A tomic Power Company Survey Unit 9312-0001

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Revision: 0

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9312-60005 9312-0002 I

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15 30E Noto Cmrdioato =o in NAD27C-oor ckt Swae Pl~e Systms II.

Figure 6 Connecticut Yankee Atomic Power Company 9312-0001 Investigative Soil Samples Posting Plot for Cs-137 I

Date:- Apri2007 I

Revision: 0

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD ATTACHMENT 2 (SCAN RESULTS)

Revision 0

Survey Unit 9312-0001 Scan Survey Results Sample Location Scans Survey Location Log Date Log Time Reading Alarm

>Alarm E-600 SIN Probe SIN Level Level 9312-01-BL-00-01-0 3/24/2007 10:04:00 8.52E+03 1117 1008 9312-01 -SL-00-01 -0 3/24/2007 10:04:00 7.64E+03 1.05E+04 1117 1008 9312-01 -BL-00-02-0 3/24/2007 10:07:00 8.94E+03 1117 1008 9312-01-SL-00-02-0 3/24/2007 10:07:00 9.73E+03 1.09E+04 1117 1008 9312-01 -BL-00-03-0 3/24/2007 10:08:00 9.1 9E+03 1117 1008 9312-01-SL-00-03-0 3/24/2007 10:09:00 1.02E+04 1.12E+04 1117 1008 9312-01 -BL-00-04-0 3/24/2007 10:10:00 8.89E+03 1117 1008 9312-01 -SL-00-04-0 3/24/2007 10:11:00 1.03E+04 1.09E+04 1117 1008 9312-01 -BL-00-05-0 3/24/2007 10:12:00 9.33E+03 1117 1008 9312-01-SL-00-05-0 3/24/2007 10:12:00 9.45E+03 1.13E+04 1117 1008 9312-01 -BL-00-06-0 3/24/2007 10:13:00 8.66E+03 1117 1008 9312-01-SL-00-06-0 3/24/2007 10:14:00 8.64E+03 1.07E+04 1117 1008 9312-01 -BL-00-07-0 3/24/2007 10:21:00 8.70E+03 1117 1008 9312-01 -SL-00-07-0 3/24/2007 10:22:00 9.52E+03 1.07E+04 1117 1008 9312-01 -BL-00-08-0 3/24/2007 10:20:00 1.OOE+04 1117 1008 9312-01 -SL-00-08-0 3/24/2007 10:20:00 9.92E+03 1.20E+04 1117 1008 9312-01 -BL-00-09-0 3/24/2007 10:19:00 1.24E+04 1117 1008 9312-01 -SL-00-09-0 3/24/2007 10:19:00 1.24E+04 1.44E+04 1117 1008 9312-01 -BL-00-1 0-0 3/24/2007 10:17:00 1.22E+04 1117 1008 9312-01 -SL-00-1 0-0 3/24/2007 10:18:00 1.21 E+04 1.42E+04 1117 1008 9312-01 -BL-00-1 1-0 3/24/2007 10:16:00 1.02E+04 1117 1008 9312-01 -SL-00-1 1-0 3/24/2007 10:17:00 1.10E+04 1.22E+04 1117 1008 9312-01 -BL-00-1 2-0 3/24/2007 10:24:00 9.44E+03 1117 1008 9312-01-SL-00-12-0 3/24/2007 10:24:00 1.08E+04 1.14E+04 1117 1008 9312-01 -BL-00-1 3-0 3/24/2007 10:25:00 8.83E+03 1117 1008 9312-01 -SL-00-1 3-0 3/24/2007 10:25:00 9.42E+03 1.08E+04 1117 1008 9312-01 -BL-00-14-0 3/24/2007 10:27:00 1.01 E+04 1117 1008 9312-01-SL-00-14-0 3/24/2007 10:27:00 1.05E+04 1.21 E+04 1117 1008 9312-01 -BL-00-1 5-0 3/24/2007 10:26:00 9.46E+03 1117 1008 9312-01-SL-00-15-0 3/24/2007 10:26:00 1.03E+04 1.15E+04 1117 1008 9312-01 -BL-00-1 6-0 3/24/2007 10:30:00 7.62E+03 1117 1008 9312-01-SL-00-16-0 3/24/2007 10:31:00 7.79E+03 9.62E+03 1117 1008 9312-01 -BL-00-1 7-0 3/24/2007 10:14:00 9.63E+03 1117 1008 9312-01 -SL-00-1 7-0 3/24/2007 10:15:00 1.03E+04 1.16E+04 1117 1008 9312-01 -BL-00-1 8-0 3/24/2007 10:28:00 9.96E+03 1117 1008 9312-01-SL-00-18-0 3/24/2007 10:29:00 9.96E+03 1.20E+04 1117 1008 9312-01-BL-00-19-0 3/24/2007 10.22.00 7.95E+03 1117 1008 9312-01-SL-00-19-0 3/24/2007 10:23:00 8.72E+03 9.95E+03 1117 1008 5/2/2007 1o 1 of 1

Survey Unit 9312-0001 Scan Survey Results Scan Strip Scans Survey Location Log Date Log Time Reading Alarm

>Alarm E-600 S/N Probe S/N Level Level 9312-01-BC-00-01-0 3/24/2007 13:41:00 9.85E+03 1107 1007 9312-01-SC-00-01-0 3/24/2007 13:47:00 8.44E+03 1.19E+04 1107 1007 9312-01 -BC-00-02-0 3/24/2007 13:48:00 8.89E+03 1107 1007 9312-01 -SC-00-02-0 3/24/2007 13:51:00 1.02E+04 1.09E+04 1107 1007 9312-01 -BC-00-03-0 3/24/2007 13:53:00

1. 11 E+04 1107 1007 9312-01 -SC-00-03-0 3/24/2007 13:58:00 1.03E+04 1.31 E+04 1107 1007 9312-01 -BC-00-04-0 3/24/2007 14:00:00 9.79E+03 1107 1007

.9312-01 -SC-00-04-0 3/24/2007 14:06:00

1. 12E+04

1. 18E+04 1107 1007 9312-01 -BC-00-05-0 3/24/2007 14:06:00 9.92E+03 1107 1007 9312-01-SC-00-05-0 3/24/2007 14:12:00 8.1 OE+03

1. 19E+04 1107 1007 9312-01 -BC-00-06-0 3/24/2007 14:14:00 8.32E+03 1107 1007 9312-01 -SC-00-06-0 3/24/2007 14:20:00 1.01E+04 1.03E+04 1107 1007 9312-01 -BC-00-07-0 3/24/2007 14:22:00 1.OOE+04 1107 1007 9312-01 -SC-00-07-0 3/24/2007 14:28:00 9.1 5E+03 1.20E+04 1107 1007 9312-01 -BC-00-08-0 3/24/2007 14:30:00 8.53E+03 1107 1007 9312-01 -SC-00-08-0 3/24/2007 14:33:00 1.02E+04 1.05E+04 1107 1007 931 2-01 -BC-00-09-0 3/24/2007 14:34:00 9.82E+03 1107 1007 9312-01 -SC-00-09-0 3/24/2007 14:37:00 8.33E+03 1.18E+04 1107 1007 9312-01-BC-00-10-0 3/24/2007 14:38:00 9.03E+03 1107 1007 9312-01-SC-00-10-0 3/24/2007 14:41:00 9.89E+03 1.10E+04 1107 1007 9312-01 -BC-00-1 1 -0 3/24/2007 14:42:00 9.68E+03 1107 1007 9312-01 -SC 11 -0 3/24/2007 14:45:00 9.42E+03

1. 17E+04 1107 1007 9312-01-BC-00-12-0 3/24/2007 14:46:00 9.19E+03 1107 1007 9312-01 -SC-00-1 2-0 3/24/2007 14:48:00 1.02E+04 1.12E+04 1107 1007 9312-01 -BC-00-1 3-0 3/24/2007 14:49:00 1.02E+04 1107 1007 9312-01-SC-00-13-0 3/24/2007 14:51:00 8.89E+03 1.22E+04 1107 1007 9312-01 -BC-00-1 4-0 3/24/2007 14:52:00 9.30E+03 1107 1007 9312-01 -SC-00-1 4-0 3/24/2007 14:54:00 1.OOE-'04 1.1 3E+04 1107 1007 9312-01 -BC-00-1 5-0 3/24/2007 14:56:00 9.54E+03 1107 1007 9312-01-SC-00-15-0 3/24/2007 14:58:00 8.50E+03

1. 15E+04 1107 1007 9312-01 -BC-00-1 6-0 3/24/2007 14:58:00 8.61 E+03 1107 1007 9312-01-SC-00-16-0 3/24/2007 15:01:00 8.35E+03 1.06E+04 1107 1007 9312-01-BC-00-17-0 3/24/2007 15:02:00 8.74E+03 1107 1007 9312-01-SC-00-17-0 3/24/2007 15:04:00 8.86E+03 1.07E+04 1107 1007 9312-01-BC-00-18-0 3/24/2007 15:05:00 8.92E+03 1107 1007 9312-01 -SC-00-1 8-0 3/24/2007 15:08:00 8.96E+03 1.09E+04 1107 1007 9312-01-BC-00-19-0 3/24/2007 15:09:00 9.31 E+03 1107 1007 9312-01-SC-00-19-0 3/24/2007 15:11:00 9.72E+03 1.13E+04 1107 1007 9312-01 -BC-00-20-0 3/24/2007 15:12:00 9.42E+03 1107 1007 9312-01-SC-00-20-0 3/24/2007 15:14:00 9.43E+03 1.14E+04 1107 1007 9312-01-BC-00-21-0 3/24/2007 15:15:00 9.59E+03 1107 1007 9312-01 -SC-00-21 -0 3/24/2007 15:17:00 1.08E+04 1.16E+04 1107 1007 9312-01 -BC-00-22-0 3/26/2007 8:01:00 8.88E+03 1107 1007 9312-01 -SC-00-22-0 3/26/2007 8:09:00 1.04E+04 1.09E+04 1107 1007 5/2/2007 1o 1 of 3

Survey Unit 931 2-0001 Survey Location 9312-01 -BC-OO-23-O 9312-01 -SC-00-23-0 9312-01 -BC-00-24-0 9312-01 -SC-00-24-0 9312-01 -BC-00-25-0 9312-01 -SC-00-25-0 9312-01 -BC-00-26-0 9312-01 -SC-00-26-0 9312-01 -BC-00-27-0 9312-0 1-SC-00-27-0 9312-01 -BC-00-28-0 9312-01 -SC-00-28-0 9312-01 -BC-00-29-0 9312-01 -SC-00-29-0 9312-01 -BC-00-30-0 9312-01 -SC-00-30-0 9312-01 -BC-00-31-0 931 2-01-SC-00-31-0 931 2-01-BC-00-32-0 931 2-01-SC-00-32-0 9312-01 -ER-00-32-1 9312-01 -BC-00-33-0 9312-01 -SC-00-33-0 9312-01 -BC-00-34-0 9312-01 -SC-00-34-0 9312-01 -ER-00-34-1 9312-01 -BC-00-35-0 9312-01 -SC-00-35-0 9312-01 -ER-00-35-1 9312-01 -BC-00-36-0 9312-01 -SC-00-36-0 9312-01 -ER-00-36-1 9312-01 -BC-00-37-0 9312-01 -SC-00-37-0 9312-01 -ER-00-37-1 9312-01 -BC-00-38-0 9312-01 -SC-00-38-0 9312-01 -BC-00-39-0 9312-01 -SC-00-39-0 9312-01 -BC-00-40-0 9312-01 -SC-00-40-0 93 12-01 -BC-00-41-0 9312-01 -SC-00-4 1-0 9312-01-ER-00-41-1 Scan Survey Results Scan Strip Scans Log Date 3/26/2007 3/26/2007 Log Time 8:10:00 8:13:00 Reading 1.25E+04 1.13E+04 Alarm

>Alarm Level Level 1.45E+04 3/26/2007 8:18:00 1.20E+04 3/26/2007 8:22:00 1.26E+04 3/26/2007 8:23:00 7.17E+03 3/26/2007 8:25:00 8.41 E+03 3/26/2007 8:27:00 9.58E+03 3/26/2007 8:30:00 1.11E+04 3/26/2007 8:31:00 1.32E+04 3/26/2007 8:35:00 1.34E+04 3/26/2007 8:35:00 1.27E+04 3/26/2007 8:40:00

1. 19E+04 3/26/2007 8:42:00 8.98E+03 3/26/2007 8:42:00 9.74E+03 3/26/2007 9:51:00 1.08E+04 3/26/2007 9:53:00 1.16E+04 3/26/2007 9:54:00 1.29E+04 3/26/2007 9:57:00 1.30E+04 3/26/2007 3/26/2007 3/26/2007 9:58:00 10:05:00 13:49:00

1. 11E+04 1.17E+04 1.52E+04 3/26/2007 10:05:00 9.95E+03 3/26/2007 10:06:00 9.97E+03 1.40E+04 9.17E+03 1.16E+04 1.52E+04 1.47E+04 1.10E+04 1.28E+04 1.49E+04 1.31 E+04 1.31 E+04 1.20E+04 1.37E+04 1.37E+04 1.32E+04 1.32E+04 1.43E+04 1.43E+04 1.25E+04 1.25E+04 1.44E+04 1.23E+04 1.26E+04

1. 15E+04

1. 15E+04

+

E-600 SIN 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 1107 Probe SIN 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 1007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 3/26/2007 10:07:00 10:15:00 13:51 :00 10:17:00 10:22:00 13:51 :00 10:23:00 10:28:00 13:52:00 10:29:00 10:36:00 13:53:00 1.17E+04 1.22E+04 1.42E+04 1.12E+04 1.16E+04 1.49E+04 1.23E+04 1.10E+04 1.54E+04 1.05E+04 1.23E+04 1.54E+04

+

+

+

+

3/26/2007 10:38:00 1.24E+04 3/26/2007 10:42:00 1.18E+04 3/26/2007 10:43:00 1.03E+04 3/26/2007 10:47:00 1.13E+04 3/26/2007 10:49:00 1.06E+04 3/26/2007 10:54:00 1.02E+04 3/26/2007 3/26/2007 3/26/2007 10:55:00 11:00:00 13:54:00 9.45E+03 1.02E+04 1.41 E+04

+

5/2/2007 2o 2 of 3

Survey Unit 9312-0001 Scan Survey Results Scan Strip Scans Survey Location Log Date Log Time Reading Alarm

>Alarm E-600 SIN Probe SIN Level Level 9312-01 -BC-0O-42-0 3/26/2007 11:22:00 1.OOE+04 1107 1007 9312-01 -SC-00-42-0 3/26/2007 11:26:00 9.38E+03 1.20E+04 1107 1007 9312-01-ER-00-42-1 3/26/2007 13:55:00 1.50E+04 1.20E+04

+

1107 1007 9312-01 -BC-00-43-0 3/26/2007 11:26:00 9.02E+03 1107 1007 9312-01 -SC-00-43-0 3/26/2007 11:30:00 9.80E+03 1.10E+04 1107 1007 9312-01 -BC-00-44-0 3/26/2007 11:32:00

1. 11 E+04 1107 1007 9312-01 -SC-00-44-0 3/26/2007 11:35:00 9.47E+03 1.31E+04 1107 1007 9312-01-BC-00-45-0 3/26/2007 11:36:00 9.52E+03 1107 1007 9312-01-SC-00-45-0 3/26/2007 11:38:00 1.03E+04 1.15E+04 1107 1007 9312-01 -BC-00-46-0 3/26/2007 11:39:00 9.OOE+03 1107 1007 9312-01 -SC-00-46-0 3/26/2007 11:42:00 8.45E+03 1.10OE+04 1107 1007 9312-01 -BC-00-47-0 3/26/2007 11:43:00 8.82E+03 1107 1007 9312-01 -SC-00-47-0 3/26/2007 11:45:00 1.02E+04 1.08E+04 1107 1007 9312-01 -BC-00-48-0 3/26/2007 11:47:00 9.73E+03 1107 1007 9312-01 -SC-00-48-0 3/26/2007 11:50:00 8.26E+03 1.17E+04 1107 1007 9312-01-BC-00-49-0 3/26/2007 11:51:00 8.54E+03 1107 1007 9312-01 -SC-00-49-0 3/26/2007 11:54:00 1.02E+04 1.05E+04 1107 1007 9312-01 -BC-00-50-0 3/26/2007 11:56:00 1.01 E+04 1107 1007 9312-01 -SC-00-50-0 3/26/2007 11:58:00 8.94E+03 1.21 E+04 1107 1007 9312-01 -BC-00-51 -0 3/26/2007 12:00:00 9.07E+03 1107 1007 9312-01 -SC-00-51 -0 3/26/2007 12:02:00 1.05E+04

1. 11 E+04 1107 1007 5/2/2007 3o 3 of 3

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 9312-0001 RELEASE RECORD ATTACHMENT 3 (LABORATORY DATA)

Revision 0

General Narrative Page 1 of 10

General Narrative for Connecticut Yankee Atomic Power Co.

Work Order: 183245 SDG: MSR#07-0129 April 04,2007 Laborato~ry Identification:

GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary Sample receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on March 29, 2007 for analysis.

Shipping container temperatures were checked, documented, and within specifications. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage.

Sample Identification The laboratory received the following samples:

Laboratory Identification 183245001 183245002 183245003 183245004 183245005 183245006 183245007 183245008 183245009 183245010 183245011 183245012 183245013 183245014 183245015 183245016 183245017 183245018 183245019 183245020 183245021 183245022 183245023 183245024 183245025 Sample Description 9312-0001 -001F 9312-0001 -002F 9312-0001 -003F 9312-0001 -003FS 9312-0001-004F 9312-0001 -00SF 9312-0001 -006F 93 12-000 1-007F 9312-0001 -008F 9312-0001 -009F 9312-0001 -01OF 9312-0001 -01 IF 9312-0001-012F 9312-0001-013F 9312-0001-014F 9312-0001-015F 9312-0001-016B 9312-0001-017B 9312-0001-018B 9312-0001-019B 9312-0001-020-1 9312-0001-021-1 9312-0001-022-1 9312-0001-023-1 9312-0001-024-1 GEL Laboratories Pfige 2 P(9jBqxp~l 2 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 w glcm www.gol.com

183245026 9312-0001-025-1 183245027 9312-0001-026-1 Items of Note There are no items to note.

Case Narrative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package.

Analytical Requ~est Twenty-five soil samples were analyzed for FSSGAM and Strontium-90. Two soil samples were analyzed for FSSALL.

Data Package The enclosed data package contains the following sections: General Narrative, Chain of Custody and Supporting Documentation, Data Review Qualifier Definitions, and data from the following fractions: Radiochemistry.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

o~_'

Cheryl Jones Project Manager GEL Laboratories Kge 3 P(918fX1W1 2 Chafesof, SC 29417 2040 Savage Road Charlesmn. SC 29407 P 843.556.8171 F 843.766.1178 wwg~o www.gol.com

List of current GEL Certifications as of 29 March 2007 StateCertification Alaska UST-062 Arizona Arkansas AZ0668 88-065 1 42DO904046 CLIA California Colorado Connecticut i

01 151CA GenEngLabs Dept. of Navy EPA Florida/NELAP Georgia Hawaii PH-0169 NFESC 413 WG-15J E87 156 E871 56 (FL/NELAP)

N/A Idaho Illinois Indiana Kansas N/A 200029 C-SC-01 E-10332 90129 Kentucky Louisiana Maryland Massachusetts Michigan Nevada New Jersey New Mexico 03046 270 M-SCO1 2 9903 SC 12 SCO02 FL NELAP E87156 11501 233 New York North Carolina North Carolina Drinking W North Dakota-Oklahoma Pennsylvania South Carolina 45709 R-158 9904 68-00485 101 20001/10595001/10120002 Tennessee Texas Texas NELAP U.S. Dept. of Agriculture US Army Corps of Engineer Utah VTermont

_________Virginia_____.

-_____Washington__

02934 TX2I 3-2006A Ti104704235-06-TX S-52597 N/A 8037697376 GEL-VT87 156 00151 C 1641 Page 4 of 110

Chain of Custody and Supporting Documentation Page 5 of 110

ON 0

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Cl Page 6 of 110

Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2007-00092 362 Injun Hollow Road, East Hampton. CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Contact Name & Phone:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State):

General Engineering Laboratories 2040 Savage Road Charleston, SC 29407 ATT: Cheryl Jones ( 843-556-8171)

Priority:D[30OD. E 15 D. 07D.

Other:

Analyses Requested Lab Use Only F

7 7

I Comments:

Media Code Sample Type Code Container Size-

&Type Code C)

Sample Designation Date Time Comment, Preservation 9312-0001-OIIF 3/24/07 1100 TS G

BP X_________

9312-0001-012F 3/24/07 1103 TS G

BP X

9312-0001-013F 3/24/07 1105 TS G

BP X

9312-000,1-014F 3/24/07 1110 TS G

BP X_______________

9312-0001-015F 3/24/07 1112 TS G

BP X____________

931,2-0001-016B 3/24/07 1116 TS G

BP X_________

9312-0001-017B 3/24/07 1120 TS G

BP X

9312-0001-018B 3/24/07 1124 TS G

BP X

9312-0001-019B 3/24/07 1128 TS G

BP X_____

NOTES: P0 #: 002332 MSR #: 07-0129 Z LTP QA El Radwaste QA ElNon QA 1

)RD te/Time

2) Rneived By Date/Time

3) ~

~

~

~

~1 Reinuihe ByDteTme 4

/IAe B

3)

Relinquished By Date/Time

6) Reeived By Date/Time Samples Shipped Via:

SFed Ex ElUPS 7-1 Hand LIOther Bill of Lading #

Internal Container Temp.:.__ Deg. C Custody. Sealed?

Custody Seal Intact?

YC NO

5) Relinquished By Date/Time

6) Received By Date/Time

Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2007-00.099 362 Injun Hollow Road, East H-ampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested' SLab Use Only r

Contact Name & Phone:

Jack McCarthy 860-267-3924 Comments:

Media Code Sample Type Code Container Size-

&Type Code Analytical Lab (Name, City, State):

General Engineering Laboratories 2040 Savage Road Charleston, SC 29407 ATT: Cheryl Jones ( 843-556-8171)

Priority: 0 30 D. El 15 D. Z 7 D.

Other:_____

00 CI-

0 Sample Designation Date Time Comment, Preservation 9312-0001-020-1 3/26/07 1348 TS G

BP X-9312-0001-021-1 3/26/07 1350 TS G

BP X_____________

9312-0001-022-1 3/26/07 1351 TS G

BP X

9312-0001-023-1 3/26/07 1352 TS G

BP X________________

93 12-0001-024-1 3/26/07 1353 TS I

G BP X

93 12-0001-025-1 3/26/07 1354 TS G

BP X

9312-0001-026-1 3/26/07 1355 TS G

BP X

NOTES: PO 4!: 002332 MSR #- 07-0 129 Z LTP QA Eli Radwaste QA EL Non QA

1) Relinciy D t/Time 2)Rc e

yDate/Time

3) Relnquishd By at/ime

4) Recived By aeTm

5) Relinquished,By Date/Time

6) Recived By D ate/Time Samples Shipped Via:

0 'Fed Ex F1 UPS.

Hý Hand ELI Other Bill of Lading#

Internal. Container.

Temp.:.

D eg. C Custod'v Sealed?

Custody Seal Intact?

YJ0 N 0

5) Relinquished By Date/Time

6) Received By Date/Time

Connecticut Yankee Statement of Work for Analytical 'Lab Services

.CY-lsc-SOW-o0l Figure 1. :Sample Check-in List

• Date/Time Received:_=t

.. )12"/6L SDG#-

L~1 ZI

)~)O?

Work Order Number:

tj3 cV3Z5

,Shipping Cctntainer ID:-8 Se E

tZ Cano utdy#

5e cmtn-.

PV-I.

Custody Seals. oai shipping container intact?:..

Yes No [

2.

Custody Seals dated and. signed?

Yes WNo[

3.

Chain-of-Custody record present?

Yes I~No[IJ

4. Cooler temperature 5e e-, 6-EL. 6fk

.ericltepakigmaterials -is:

• Wet

[]Dry-6:'

Number of samples in shipping contain'r

_79

7.

Sample holding times exceeded?

Yes.(

No J~j'

.8. Samples have-'

j tape

-hazard labels

.jutody seals zipropriate sample labels

9. Samples are-.

.. 4ngood condition leaking broken

__have air bubbles

10.

Were any anomnalies iden~ti~fied in sample receipt?

Yes [1No II..

,Description of anomalies. (include samnple numbers):.

Sample. CustodiantLab~oratory:,

Telephoned to:______________

72 777.

'1

.FV

-J Page 9 of 110

w SAMPLE RECEIPT & REVIEW FORM PM use only fClient:

ýJ 3\\-SDG/ARCOC/Work Order:

1 %&2-43, I &3234$5, 193Z-'ý-

Date Received:

3:i 91.0-4i PM(A) Review (ensure non-con-formi sitems Ore resolved prior to signing);

Received By:

JTy Sample Receipt Criteria 0

Comments/Qualifiers. (Required for Non-Conforming Items)

Shipping c ainers received Circle Applicable: seals broken damaged container leaking container other (describe)

Iintact and s~eale Samples requiring icolý'

Circle Coolant #'

ice bags blue ice dry ice none other describei 2 preservation within (4 +1/- 2'

?

ReodPreservation method.

Chain of custody documents included with shipment?

Sample containers intact and Circle Applicable: seals broken damaged container leaking container other (describe) sealed?________________________________

5Smlsrqiigchemical Sample ID's. containers affected and observed pH:

__ reserv-ation at proper PH?

VOA vials free of headspace Ssrnp IDsand containers affected:

6 (defined as < 6mm bubble)?

Are Encore containers present?

7 (if yes, immediately deliver to

__VOA laboratory)

Samples received. within holding Id's and tests affected:

8_ time'?

SSample ID's-on COC match ID's Sample ID's and containers affect 9on bottles?

,10Date & time on COGC match date Sample ID's affected:

& timne on bottles?

Number of containers received Sample ID's affected.

match number indicated on COG?

12COC form is properly signed in 12relinquished/received sections?

Air Bill,Tracking #'s, &

7q 0

1Z-41

`i36

' 3-7'Z 5,&

S1 3Z 14Additional Comments 7"15 S376-(

'-4-Ou -7,ý 7'7

-8t

~3-7 71 7

55Y S

T ~RSO RAD Receipt # ___________

SuspctedHazad Inormaion 11

• If > x2 area background is observed on samples identified as "non-Susi~ctd HaardInfrmaton

~

Iregulated/non-radioactive", contact the Radiation Safety group for further A fRadiological Classitication?

IIMaxirnum Counts Observed*: ZZC'"

• PCB Regulated?

Shipped as DOT1 Hazardous C Material? If yes, contact Waste Manager or ESH Manager.Y 1? Regulated as a Foreign Soil lazard Class Shipped:

IN#i:ls QA (

ae bli~t1 PM (or PMA) review of Hazard classification:

Page 10 of 110

V

-JuJ C,

SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM

/

Client:

14 N V-Date.Received:

jT-V age

/of z-oo7-49ooo Ze,)o,7- 001 I o zeoo7- 00o'cil 2o1~oi P)

Page I11 of 10

Data Review Qualifier Definitions Page 12 of 110

Data Review Qualifier Definitions Qualifier Explanation A quality control analyte recovery is outside of specified acceptance criteria Analyte is a surrogate compound Result is less than value reported Result is greater than value reported RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL A

The TIC is a suspected aldol-condensation product Target analyte was detected in the associated blank B

Metals-Either presence of analyte detected in the associated blank, or MDL/IDL < sample value < PQL BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample d

5-day SOD-The 2:1 depletion requirement was not met for this sample E

Organics-Concentration of the target analyte exceeds the instrument calibration range E

Metals-%difference of sample and SD is >10%.

Sample concentration must meet flagging criteria H

Analytical holding time was exceeded h

Preparation or preservation holding time was exceeded J

Value is estimated N

Metals-The Matrix spike sample recovery is not within specified control limits N

Organics-Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC).

Quantitation is based on nearest internal standard response factor N/A Spike recovery limits do not apply.

Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the reporting limit UT Gamma Spectroscopy-Uncertain identification X

Consult Case Narrative, Date Summary package, or Project Manager concerning this qualifier Y

QC Samples were not spiked with this compound Z

Paint Filter Test-Particulates passed through the filter, however no free liquids were observed.

GEL Laboratories Ikrge 1 ý0ýPqU~?2 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.765.1178 www.gal.com

RADIOLOGICAL ANALYSis Page 14 of 110

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 183245 Method/Analysis Information Product:

Aiphaspec Am241, Cm, Solid ALL FSS Analytical Method:

DOE EML HASL-300, Am-05-RC Modified Prep Method:

Dry Soil Prep GL-RAD-A-021 Method:

Analytical Batch Number:

Prep Batch Number:

Dry Soil. Prep GL-RAD-A-021 Batch Number:

Ash Soil Prep Dry Soil Prep 621107 621096 621094 Sample ID 183245006 183245016 1201305240 1201305241 1201305242 1201305243 Client ID 9312-0001 -005F 9312-0001-015SF Method Blank (MB) 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 183245006(9312-0001 -00SF) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-0l I REV# IS.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Page 15 of 110

Oualitv Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (93 12-0001 -005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Gualifier information Manual qualifiers were not required.

Method/Analysis Information Page 16 of 110

Product:

Liquid Scint Pu241, Solid-ALL FSS DOE EML HASL-300, Pu-I I -RC Modified Analytical Method:

Prep Method:

Dry Soil Prep GL-RAD-A-021 Method:

Analytical Batch Number:

Prep Batch Number:

Dry Soil Prep GL-RAD-A-021 Batch Number:

Ash Soil Prep Dry Soil Prep 622105 621096 621094 Sample ID 183245006 183245016 1201307488 1201307489 1201307490 1201307491 Client ID 9312-0001 -00SF 9312-0001-015F Method Blank (MB) 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 183245006(9312-0001 -00SF) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 9.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Oualitv Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (9312-0001 -00SF).

QC Information All of the QC samples met the required acceptance limits.

Page 17 of 110

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 183245006 (9312-0001-005F) and 183245016 (9312-0001-015F) were reprepped due to low/high carrier/tracer yield.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Oualifier information Manual qualifiers were not required.

Method/Analysis Information Product:

Alphaspec Pu, Solid-ALL FSS Analytical Method:

DOE EML HASL-300, Pu-I I1-RC Modified Prep Method:

Ash Soil Prep Dry Soil] Prep GL-RAD-A-021 Method:

Dry Soil] Prep Analytical Batch Number:

622351 Prep Batch Number:

621096 Dry Soil Prep GL-RAD-A-021 Batch Number:

621094 Page 18 of 110

Sample ID 183245006 183245016 1201308034 1201308035 1201308036 1201308037 Client ID 9312-0001 -00SF 9312-0001 -015F Method Blank (MB) 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 183245006(9312-0001 -00SF) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 I REV# 15.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (93 12-0001-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples were reprepped due to low/high carrier/tracer yield.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from Page 19 of 110

referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product:

Analytical Method:

Prep Method:

Analytical Batch Number:

Prep Batch Number:

Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived EML HASL 300, 4.5.2.3 Dry Soil Prep 621148 621094 Page 20Oof 110

Sample ID 183245001 183245002 183245003 183245004 183245005 183245006 183245007 183245008 183245009 183245010 183245011 183245012 183245013 183245014 183245015 183245016 183245017 183245018 183245019 183245020 1201305340 1201305341 1201305342 Client ID 9312-0001 -001F 9312-0001-002F 9312-0001 -003F 9312-0001 -003FS 9312-0001 -004F 9312-0001 -00SF 9312-0001 -006F 9312-0001 -007F 9312-0001 -008F 9312-0001 -009F 9312-0001 -OlOF 93 12-0001 -01 IF 9312-0001-012F 9312-0001-013F 9312-0001 -014F 9312-0001-015F 9312-0001-016B 9312-0001 -017B 9312-0001-018B 9312-0001-019B Method Blank (MB) 183245001(9312-0001-001 F) Sample Duplicate (DUP)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 3 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245001 (9312-0001 -001F).

Page 21 of 110

QC Information Refer to Non-Conformance Report.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. The following NCR was generated for this SDG:

NCR 419166 was generated due to Failed RPD for DUP. 1. The sample (183245001) and the duplicate (1201305341) did not meet the relative percent difference or the relative error ratio requirements for Pb-2 12. All other isotopes met the rel ative percent difference requirement. 1. Reporting results.

Additional Comments Additional comments were not required for this sample set.

Oualifier information Page 22 of 110

Qualifier U'

U' Reason Analyte Data rejected due to high counting uncertainty.

Potassium-40 Data rejected due to high peak width.

Cesium-137 Manganese-54 Data rejected due to interference.

Europiumn-155 U'

U' Data rejected due to low abundance.

Data rejected due to no valid peak.

Manganese-54 Actiniumn-228 Amnericiumn-24 1 Cesium-134 Potassium-40 Thallium-208 Bismuth-2 12 Sample 1201305340 183245003 183245005 183245012 183245014 183245018 183245020 183245020 183245005 183245012 183245002 183245006 183245007 183245009 183245010 183245011 183245012 183245013 183245015 183245016 183245017 183245018 183245019 183245005 1201305340 183245001 U'

Method/Analysis Information Page 23 of 110

Product:

Analytical Method:

Prep Method:

Analytical Batch Number:

Prep Batch Number:

Sample ID 183245021 183245022 183245023 183245024 183245025 183245026 183245027 1201305347 1201305348 1201305349 Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived EML HASL 300, 4.5.2.3 Dry Soil Prep 621149 621097 Client ID 9312-0001-020-1 9312-0001-021-1 9312-0001-022-1 9312-0001-023-1 9312-0001-024-1 9312-0001-025-I 9312-0001-026-1 Method Blank (MB) 183245021(9312-0001-020-1) Sample Duplicate (DUP)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-0 13 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (00 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245021 (93 12-0001-020-1).

QC Information All of the QC samples met the required acceptance limits.

Page 24 of 10

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Qualifier Reason Analyte U'

Data rejected due to low abundance.

Cesium-134 Sample 183245021 183245022 1201305348 Method/Analysis Information Product:

GFPC, Sr9O, solid-ALL FSS Analytical Method:

EPA 905.0 Modified Prep Method:

Dry Soil Prep GL-RAD-A-021 Method:

Analytical Batch Number:

Prep Batch Number:

Dry Soil Prep GL-RAD-A-021 Batch Number:

Ash Soil Prep Dry Soil Prep 621123 621096 621094 Page 25 of 110

Sample ID 183245001 183245002 183245003 183245004 183245005 183245006 183245007 183245008 183245009 183245010 183245011 183245012 183245013 183245014 183245015 183245016 183245017 183245018 183245019 183245020 1201305273 1201305274 1201305275 1201305276 Client ID 9312-0001 -001F 9312-0001 -002F 9312-0001 -003F 9312-0001 -003FS 9312-0001 -004F 9312-0001 -005F 9312-0001 -006F 9312-0001 -007F 9312-0001 -008F 9312-0001 -009F 9312-0001 -01IOF 9312-0001 -01 IF 9312-0001-01 2F 9312-0001-013F 9312-0001-014F 9312-0001-015F 9312-0001-016B 9312-0001-017B 9312-0001-01 8B 9312-0001-01 9B Method Blank (MB) 183245001(9312-0001-001 F) Sample Duplicate (DUP) 183245001(9312-0001 -GOlF) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 11.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Oualitv Control (0C0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Page 26 of 110

Designated QC The following sample was used for QC: 183245001 (93 12-0001 -001F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information AU preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 183245005 (93 12-0001-004F) was recounted due to a negative result greater than three times the error. Sample 1201305276 (LCS) was recounted due to low/high recovery.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

MiscelIlaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product:

GFPC, Sr9O, solid-ALL FSS Analytical Method:

EPA 905.0 Modified Prep Method:

Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method:

Dry Soil Prep Analytical Batch Number:

621125 Prep Batch Number:

621098 Dry Soil Prep GL-RAD-A-021 Batch Number:

621097 Page 27 of 10

Sample ID 183245021 183245022 183245023 183245024 183245025 183245026 183245027 1201305281 1201305282 1201305283 1201305284 Client ID 9312-0001-020-1 9312-0001-021-1 9312-0001-022-1 9312-0001-023-1 9312-0001-024-1 9312-0001-025-1 9312-0001-026-1 Method Blank (MB) 183245021(9312-0001-020-I) Sample Duplicate (DUP) 183245021(9312-0001-020-I) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 11.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245021 (9312-0001 -020-1).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Page 28 of 10

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product:

Liquid Scint Tc99, Solid-ALL FSS Analytical Method:

Analytical Batch Number:

Sample ID 183245006 183245016 1201305310 1201305311 1201305312 1201305313 DOE EML HASL-300, Tc-02-RC Modified 621139 Client ID 9312-0001 -00SF 9312-0001-015F Method Blank (MB) 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 183245006(9312-0001 -00SF) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Page 29 of 110

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:.

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (931 2-0Q001-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 183245016 (9312-0001-015F) was recounted due to a negative result greater than three times the error. Sample 1201305312 (9312-0001-005F) was recounted due to low/high recovery.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Oualifier information Manual qualifiers were not required.

Method/Analysis Information Page 3Oof 110

Product:

Product:Liquid Scint Fe55, Solid-ALL FSS Analytical Method:

DOE RESL Fe-I, Modified Ash Soil Prep Prep Method:

Dry Soil Prep GL-RAD-A-021 Method:

Analytical Batch Number:

Prep Batch Number:

Dry Soil Prep GL-RAD-A-021 Batch Number:

Dry Soil Prep 621136 621096 621094 Sample ID 183245006 183245016 1201305300 1201305301 1201305302 1201305303 Client ID 9312-0001 -00SF 9312-0001-015F Method Blank (MB) 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 183245006(9312-0001-005F) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 4.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (9312-0001 -00SF).

QC Information All of the QC samples met the required acceptance limits.

Page 31 of 110

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product:

Liquid Scint Ni63, Solid-ALL FSS Analytical Method:

DOE RESL Ni-I, Modified Prep Method:

Dry Soil Prep GL-RAD-A-021 Method:

Analytical Batch Number:

Prep Batch Number:

Dry Soil Prep GL-RAD-A-021 Batch Number:

Ash Soil Prep Dry Soil Prep 621137 621096 621094 Sample ID 183245006 183245016 1201305304 1201305305 1201305306 1201305307 Client ID 9312-0001 -00SF 9312-0001 -015F Method Blank (MB) 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 183245006(9312-0001 -00SF) Matrix Spike (MS)

Laboratory Control Sample (LCS)

Page 32 of 110

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (93 12-0001-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Page 33 of 10

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product:

LSC, Tritium Dist, Solid - 3 pCilg Analytical Method:

Analytical Batch Number:

Sample ID 183245006 183245016 1201305316 1201305317 1201305318.

1201305319 EPA 906.0 Modified 621141 Client ID 9312-0001 -00SF 9312-0001-015F Method Blank (MB) 183255002(931 2-0003-002F) Sample Duplicate (DUP) 183255002(931 2-0003-002F) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (00)

Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183255002 (9312-0003-002F).

QC Information All of the QC samples met the required acceptance limits.

Page 34of 110

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product:

Liquid Scint C14, Solid AII,FSS Analytical Method:

Analytical Batch Number:

Sample ID 183245006 183245016 1201305324 1201305325 1201305326 1201305327 EPA EERF C-01 Modified 621144 Client ID 9312-0001 -00SF 9312-0001-015SF Method Blank (MB) 183245006(9312-0001 -00SF) Sample Duplicate (DUP) 183245006(9312-0001-005F) Matrix Spike (MS)

Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 9.

Page 35 of 110

Calibration Information.

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:.

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 183245006 (93 12-0001-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 1201305324 (MB), 1201305325 (9312-0001-005F), 1201305326 (9312-0001-005F) and 1201305327 (LCS) were recounted due to detector error.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Page 36 of 110

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

/7 LtIl Reviewer/Date:

Page 37 of 110

GEL Laboratories LLC Form GEL-NCR Rev. 06/05 NCR Report No.:

419166 Revision No.: 1 COMPANY - WIDE NONCONFORMANCE REPORT Mo.Day Yr.

04-APR-07 Division:

Radiochemistry Quality Criteria:

Specifications Type:

Process Instrument Type:

Test / Method:

j Matrix Type:

Client Code:

GAMMA SPECTROMETER EML HASL 300, 4.5.2.3 Solid YANK Batch ID:

Sample Numbers:

621148 See Below Potentially affected work order(s)(SDG): 183245(MSR#07-01 29)

Application Issues:

Failed RPD for DUP Specification and Requirements Nonconformance

Description:

1. The sample (183245001) and the duplicate (1201305341) did not meet the relative percent difference or the relative error ratio requirements for Pb-21 2. All other isotopes met the relative percent difference requirement.

NRG Disposition:

i

1. Reporting results.

Originator's Name:

Shenise Euland Quality Review:

Data Validator/Group Leader:

Melanie Aycock 04-APR-07 04-APR-07 Director:

Page 1 Page 38 of 10

SAMPLE DATA

SUMMARY

Page 39 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOOlI Connecticut Yankee Atomric Power Co.

Client SDG: MSR#07-0129 GEL Work Order: 183245 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Prolect Manager, Cheryl Jones.

Reviewed by Page 40 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack-.McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

9312-0001-OOIF Project:

YANK01204 Sample ID:

183245001 Client ID:

YANKOOI Matrix:

TS Vol. Recv.:

Collect Date:

24-MAR-07 Receive Date:

29-MAR-07 Collector:

Client Moisture:

.178%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch D Rad Gamma Spec Analysis Gczrnma,Solid-FSS GAM & ALL ESS 226 In growth Waived Actinium-228 0.454

+/-0.150 0.0552

+/-0.150 0.110 pCi/g MJHI 04/02/07 1204 621148 Americium-241 U

0.0498

+/-0.066 0.0543

+/-0.066 0.109 pCi/g Bismuth-212 UI 0.00

+/-0.207 0.118

+/-0.207 0.236 pCi/g Bismuth-214 0.371

+/-0.0773 0.0298 +/-0.0773 0.0595 pCi/g Cesium-134 U

0.0207

+/-0.0199 0.018 +/-0.0199 0.036 pCi/g Cesium-137 U

0.0128

+/-0.0247 0.0163 +/-0.0247 0.0326 pCi/g Cobalt-60 U

0.0139

+/-0.0215 0.0173 +/-0.0215 0.0347 pCi/g Europium-152 U

-0.0239

+/-0.0558 0.0413 +/-0.0558 0.0826 pCi/g Europium-154 U

0.00648

+/-0.0619 0.053 +/-0.0619 0.106 pCi/g Europium-ISS U

0.0856

+/-0.0514 0.0483 +/-0.0514 0.0966 pCi/g Lead-2 12 0.534

+/-0.0676 0.0231 +/-0.0676 0.0463 pCi/g Lead-214 0.436

+/-0.0773 0.0307 +/-0.0773 0.0614 pCi/g Manganese-54 U

0.0173

+/-0.0166 0.0158 +/-0.0166 0.0315 pCi/g Niobium-94 U

0.00137

+/-0.0179 0.0152 +/-0.0179 0.0303 pCi/g Potassium-40 9.22

+/-0.883 0.142

+/-0.883 0.285 pCi/g Radium-226 0.371

+/-0.0773 0.0298 +/-0.0773 0.0595 pCi/g Silver-108m U

0.00822

+/-0.0162 0.0146 +/-0.0162 0.0291 pCi/g Thallium-208 0.159

+/-0.034 0.0156

+/-0.034.

0.03 11 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

-0.0117

+/-0.0206 0.0196 +/-0.0206 0.047 pCi/g KSDI 04/03/07 2021 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Page 41 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address :

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-OOIF Project:

YANK01204 Sample ID:

183245001 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 56 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UT Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 42 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company : Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-002F 183245002 TS 24-MAR-07 29-MAR-07 Client 9.2 1%

Project:

Client ID:

Vol. Recv.:

YANK01 204 YANKOO I Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Gamma Spec Analysis Gamma, Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.715

+/-0.180 0.0606

+/-0.180 0.121 pCi/g MIHI 04/02/07 1205 621148 Americium-241 U

0.0651

+/-0.0825 0.0722 +/-0.0825 0.144 pCi/g Bismuth-212 U

0.224

+/-0.279 0.138

+/-0.279 0.275 pCi/g Bismuth-214 0.562

+/-0.0875 0.0322 +/-0.0875 0.0643 pCi/g Cesium-] 34 UI 0.00

+/-0.037 0.021

+/-0.037 0.042 pCi/g Cesium-]137 0.0715

+/-0.0264 0.0185 +/-0.0264 0.037 pCi/g Cobalt-60 U-0.000781

+/-0.0197 0.0168 +/-0.0197 0.0337 pCi/g Europium-152 U -0.00608

+/-0.0657 0.0456 +/-0.0657 0.091 pCi/g Europium-154 U

-0.0382

+/-0.0656 0.0534 +1-0.0656 0.107 pCi/g Europium-155 U

0.0834

+/-0.0747 0.0503 +/-0.0747 0.101 pCi/g Lead-21 2 0.726

+/-0.0786 0.0261 +/-0.0786 0.0521 pCi/g Lead-214 0.580

+/-0.0866 0.0286 +/-0.0866 0.0572 pCi/g Manganese-54 U -0.00752

+/-0.0211 0.0175 +/-0.0211 0.035 pCi/g Niobium-94 U

0.00481

+/-0.0167 0.0148 +/-0.0167 0.0295 pCi/g Potassium-40 12.5

+/-1.18 0.161

+/-1.18 0.322 pCi/g Radium-226 0.562

+/-0.0875 0.0322 +/-0.0875 0.0643 pCi/g Silver-108m U

-0.0171

+/-0.0166 0.014 +/-0.0166 0.028 pCi/g Thallium-208 0.242

+/-0.0458 0.0155 +/-0.0458 0.031 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U

0.00183

+/-0.0212 0.0175 +/-0.0212 0.0421 pCi/g KSD1 04/03/072021 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 43 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-002F Project:

YANK01204 Sample ID:

183245002 Client ID:

YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Di Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 62 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 44 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel corn Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack;McCarthy Project:

Soils P04* 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-003F 183245003 TS 24-MAR-07 29-MAR-07 Client 5.54%

Project:

Client ID:

Vol. Recv.:

YANK01204 YANKOOI Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.07

+/-0.271 0.0834

+/-0.271 0.167 pCilg MJHI1 04/02/07 1208 621148 Americium-241 U

0.0192

+/-0.0424 0.0349 +/-0.0424 0.0698 pCi/g Bismuth-212 0.747

+/-0.406 0.184

+/-0.406 0.368 pCilg Bismuth-214 0.708

+/-0.139 0.0435

+/-0.139 0.087 pCilg Cesium-134 U

0.0307

+/-0.0423 0.0314 +/-0.0423 0.0627 pCilg Cesium-137 UI 0.00

+/-0.0451 0.0253 +1-0.0451 0.0505 pCilg Cobalt-60 U

0.0242

+/-0.0352 0.03 17 +/-0.0352 0.0634 pCilg Europium-152 U

-0.0266

+/-/-0.1 10 0.0544

+/-0.110 0.109 pCi/g Europium-154 U

0.0121

+/-/-0.102 0.0865

+/-0.102 0.173 pCi/g Europium-l55 U

0.0968

+/-0.0756 0.0523 +/-0.0756 0.104 pCi/g Lead-212 0.928

+1-0.106 0.0313

+/-0.106 0.0625 pCilg Lead-2 14 0.707

+/-0.118 0.0406

+/-0.118 0.0811 pCi/g Manganese-54 U -0.00186

+/-0.0293 0.0254 +/-0.0293 0.0509 pCi/g Niobium-94 U

0.021

+/-0.0289 0.0236 +/-0.0289 0.0472 pCi/g Potassium-40 15.7

+/-1.24 0.281

+/-1.24 0.562 pCi/g Radium-226 0.708

+/-0.139 0.0435

+/-0. 139 0.087 pCi/g Silver-1O8m U

-0.008

+/-0.0217 0.0185 +/-0.0217 0.037 pCi/g Thallium-208 0.303

+/-0.0614 0.0227 +/-0.0614 0.0454 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U

-0.0177

+/-0.022 0.0209

+/-0.022 0.0481 pCi/g KSDI 04/03/07 2021 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 45 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-003F Project:

YANK01204 Sample ID:

183245003 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 60 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol -condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 46 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address :

362 Injun Hollow Rd

Contact:

Project:

East Hampton, Connecticut 06424 Mr. Jack McCarthy Soils P04* 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-003FS 183245004 TS 24-MAR-07 29-MAR-07 Client 5.56%

Project:

Client ID:

Vol. Recv.:

YANKO01204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch D~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.967

+/-0.215 0.0724

+1-0.2 15 0.145 pCi/g MIHI 04/02/07 1426 621148 Americium-241 U

0.0464

+/-0.111 0.0945

+/-0.111 0.189 pCi/g Bismuth-212 0.603

+/-0.292 0.163

+/-0.292 0.326 pCi/g Bismuth-214 0.604

+/-0.108 0.0386

+/-0.108 0.0771 pCi/g Cesium-I 34 U

0.0247

+/-0.0303 0.0268 +/-0.0303 0.0535 pCi/g Cesium-I 37 0.0527

+/-0.0352 0.0201 +/-0.0352 0.0402 pCi/g Cobalt-60 U

0.0238

+/-0.0342 0.025 +/-0.0342 0.0499 pCi/g Europium-152 U

0.0209

+/-0.0733 0.0538 +/-0.0733 0.108 pCi/g Europium-154 U

-0.0372

+/-0.0814 0.0659 +/-0.0814 0.132 pCi/g Europium-155 U

0.0653

+/-0.1 10 0.0563

+/-0.110 0.113 pCi/g Lead-2 12 0.886

+/-0.096 0.0333

+/-0.096 0.0666 pCi/g Lead-214 0.764

+/-0.126 0.0401

+/-0.126 0.0802 pCi/g Manganese-54 U

0.0275

+/-0.0283 0.0231 +/-0.0283 0.0461 pCi/g Niobium-94 U

0.0131

+/-0.0297 0.0209 +/-0.0297 0.0418 pCi/g Potassium-40 15.7

+/-1.46 0.174

+/-1.46 0.348 pCi/g Radium-226 0.604

+/-0.108 0.0386

+/-0.108 0.0771 pCi/g Silver-108m U

0.00504

+/-0.0216 0.0188 +/-0.0216 0.0376 pCi/g Thallium-208 0.355

+/-0.0589 0.019 +/-0.0589 0.038 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

-0.016

+/-0.0211 0.0199 +/-0.0211 0.0455 pCi/g KSDI 04/03/07 2021 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Page 47 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

'Mr. Jack McCarthy Project:

Soils POS# 002332 Client Sample ID:

9312-0001-003FS Project:

YANK01204 Sample ID:

183245004 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 75 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 48 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

.. Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-004F 183245005 TS 24-MAR-07 29-MAR-07 Client 5.97%

Proiect:

Client ID:

Vol. Recv.:

YANKO 1204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Gamma Spec Analysis Gamnma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 UI 0.00

+1-0.144 0.128

+1-0.144 0.257 pCi/g MJHI 04/02/07 1409 621148 Americium-241 U

0.00396

+/-0.105 0.0871

+/-0.105 0.174 pCi/g Bismuth-212 0.431

+/-0.296 0.157

+/-0.296 0.315 pCi/g Bismuth-214 0.492

+/-0.100 0.0339

+/-0.100 0.0678 pCi/g Cesium-134 U

0.0403

+/-0.0384 0.023 +/-0.0384 0.0459 pCi/g Cesium-137 0.0682

+/-0.0348 0.0192 +/-0.0348 0.0383 pCi/g Cobalt-60 U 0.000422

+/-0.0197 0.0166 +/-0.0197 0.0331 pCi/g Europium-152 U -0.00217

+/-0.0652 0.0479 +/-0.0652 0.0957 pCi/g Europium-154 U

-0.077

+/-0.0831 0.054 +/-0.0831 0.108 pCi/g Europium-I155 U

0.0303

+/-0.0639 0.0593 +/-0.0639 0.119 pCi/g Lead-2 12 0.628

+/-0.0723 0.0269 +/-0.0723 0.0537 pCi/g Lead-214 0.599

+/-0.0888 0.033 +/-0.0888 0.066 pCi/g Maniganese-54 UI 0.00

+/-0.0353 0.0155 +/-0.0353 0.031 pCi/g Niobium-94 U

0.0166

+/-0.0202 0.0182 +/-0.0202 0,0364 pCi/g Potassium-40 UI 0.00

+/-0.958 0.871

+/-0.958 1.74 pCi/g Radium-226 0.492

+/-0.100 0.0339

+/-0.100 0.0678 pCi/g Silver-108m U

-0.0246

+/-0.0186 0.0149 +/-0.0186 0.0297 pCi/g Thallium-208 0.222

+/-0.0435 0.0175 +/-0.0435 0.035 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U -0.00371

+/-0.0222 0.0193 +/-0.0222 0.0462 pCi/g KSDI 04104/07 1038 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description 2

3 EML HASL 300, 4.5.2.3 EPA 905.0 Modified EPA 905.0 Modified Page 49 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-004F Project:

YANK01204 Sample ID:

183245005 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 56 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 5Oof 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Company : Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils P04* 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-005F 183245006 TS 24-MAR-07 29-MAR-07 Client 2.21%

Project:

Client ID:

Vol. Recv.:

YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1P Rad Alpha Spec Analysis Alphaspec Am24J, Cm, Solid ALL FSS Americium-241 U

Curium-242 U

Curium-243/244 U

Aiphaspec Pu, Solid-ALL FSS Plutonium-238 U

Plutonium-239/240 U

Liquid Scint Pu24J, Solid-ALL FSS Plutonium-241 U

Rad Gamma Spec Analysis

-0.0394 0.00 0.00

+/-0.0816

+/-0.083

+/-0.0794 0.0363 0.00 0.00

+/-0.0818

+/-0.083

+/-0.0794 0.182 0.115 0.110 0.195 0.151 18.1 0.0429

+/-0.0969 0.0522 +/-0.0971 0.059

+/-0.0943 0.0301

+/-0.0946

-3.12

+/-10.1 8.60

+/-10.1 Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 Americium-241 U

Bismuth-2 12 Bismuth-2 14 Cesium-134 UI Cesium-I 37 Cobalt-60 U

Europium-152 U

Europium-154 U

Europium-155 U-Lead-212 Lead-214 Manganese-54 U

Niobium-94 U

Potassium-40 Radium-226 Silver-108m U 0 Thallium-208 Rad Gas Flow Proportional Counting GFPC, 5r90, solid-ALL FSS Strontium-90 U

Rad Liquid Scintillation Analysis LSG, Tritiumn Dist, Solid -

3 pCi/g Tritium U

0.669 0.0462 0.431 0.5 15 0.00 0.0555 0.002 14

-0.0538

-0.0198 0.00446 0.579 0.561 0.00793 0.00603 10.5 0.515

.000976 0.204

+/-0. 133

+/-0.0606

+/-0.162

+/-0.0687

+/-0.0315

+/-0.0202

+/-0.0164

+/-0.0472

+/-0.0441

+/-0.0349

+/-0.0605

+/-0.071

+/-0.0145

+/-0.0133

+/-0.802

+/-0.0687

+/-0.012

+/-0.0313 0.0357 0.0489 0.0822 0.0209 0.0148 0.0115 0.0126 0.0287 0.0372 0.0325 0.0169 0.021 0.0112 0.0103 0.095 0.0209 0.01 03 0.011

+/-0. 133

+/-0.0606

+/-0.162

+/-0.0687

+/-0.0315

+/-0.0202

+/-0.0164

+/-0.0472

+/-0.0441

+/-0.0349

+/-0.0605

+/-0.071

+/-0.0145

+/-0.0133

+/-0.802

+/-0.0687

+/-0.012

+/-0.0313 0.07 14 0.0978 0.164 0.04 17 0.0295 0.0229 0.0252 0.0574 0.0743 0.0649 0.0339 0.04 19 0.0223 0.0205 0.190 0.0417 0.0207 0.022 0.0434 1.80 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MIHI 04/02/07 1511 621148 KSDI 04/03/07 2022 621123 AXD2 03/31/07 1247 621141 GXRI 04/03/07 0933 621107 GXRI 04/04/07 2258 622351 BXLI 04/05/07 1354 622105

-0.0135

+/-0.0195 0.0186 +/-0.0195 0.761

+/-1.06 0.859

+/-1.06 Page 51 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Certificate ofAnaksis Company : Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

931 2-0001-005F 183245006 Proiect:

Client ID:

Vol. Reev.:

YANK01204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Rad Liquid Scintillation Analysis Liquid Scint C04, Solid AIIFSS Carbon-14 U

0.0236

+/-0.090 0.075

+/-0.090 0.154 pCi/g AXD2 03/30/07 1847 621144 Liquid Scint Fe5S, Solid-ALL FSS Iron-55 U

-26.4

+/-34.3 25.3

+/-34.3 53.1 pCi/g MXPI 04/02/07 2041 621136 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U

-11.2

+/-9.41 8.39

+/-9.41 17.6 pCi/g MXP1 04/02/07 1548 621137 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U

-0.155

+/-0.229 0.196

+/-0.229 0.401 pCi/g MXPI 04/03/07 1246 621139 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

DOE EML HASL-300, Am-05-RC Modified 2

DOE EML HASL-300, Pu-lI 1-RC Modified 3

DOE EML HASL-300, Pu-lI l-RC Modified 4

DOE EML HASL-300, Pu-I I1-RC Modified 5

DOE EML HASL-300, Pu-lIl-RC Modified 6

EML HASL 300, 4.5.2.3 7

EPA 905.0 Modified 8

EPA 906.0 Modified 9

EPA EERF C-01 Modified 10 DOE RESL Fe-I, Modified I1I DOE RESL Ni-I, Modified 12 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Americium-243 Tracer Plutonium-242 Tracer Plutonium-242 Tracer Strontium Carrier lror-59 Tracer Nickel Carrier Alphaspec Am24l, Cm, Solid ALL Alphaspec Pu, Solid-ALL FSS Liquid Scint Pu241, Solid-ALL Fý GFPC, Sr90, solid-ALL ESS Liquid Scint Fe55, Solid-ALL ES Liquid Scint Ni63, Solid-ALL FS 74 81 70 72 64 78 (15%-125%)

(15%-125%)

(25%-I125%)

(25%-125%)

(15%-125%)

(25%-I 25%)

Page 52 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-005F Proiect:

YANK01204 Sample ID:

183245006 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch D~

Technetium-99m Tracer Liquid Scint Tc99, Solid-ALL FS 85 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD1 Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +f-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 53 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-006F 183245007 TS 24-MAR-07 29-MAR-07 Client 3.5 1%

Proiect:

Client ID:

Vol. Recv.:

YANK01204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch 1D Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.817

+/-0.136 0.0405

+/-0.136 0.081 pCi/g MIHI 04/02/07 1512 621148 Americium-241 U

0.00132

+/-0.0861 0.0703 +/-0.0861 0.141 pCi/g Bismuth-212 0.528

+/-0.171 0.0918

+/-0.171 0.184 pCi/g Bismuth-214 0.664

+/-0.0809 0.0209 +/-0.0809 0.0417 pCi/g Cesium-134 UI 0.00

+/-0.0211 0.0147 +/-0.0211 0.0294 pCi/g Cesium-137 0.0412

+/-0.0173 0.0108 +/-0.0173 0.0215 pCi/g Cobalt-60 U

0.00201

+/-0.0137 0.0116 +/-0.0137 0.0232 pCi/g Europium-152 U -0.0156

+1-0.044 0.0303

+/-0.044 0.0605 pCi/g Europium-154 U -0.0493

+/-0.0477 0.0376 +/-0.0477 0.0751 pCi/g Europium-ISS U

0.0379

+/-0.0504 0.0363 +/-0.0504 0.0725 pCi/g Lead-212 0.853

+/-0.101 0.0178

+/-0.101 0.0356 pCi/g Lead-214 0.714

+/-0.0865 0.0227 +/-0.0865 0.0453 pCi/g Manganese-54 U

0.0154

+/-0.0185 0.0103 +/-0.0185 0.0206 pCi/g Niobium-94 U

0.00406

+/-0.0 126 0.011

+/-0.0126 0.0219 pCi/g Potassium-40 14.3

+/-1.09 0.116

+/-1.09 0.233 pCi/g Radium-226 0.664

+/-0.0809 0.0209 +/-0.0809 0.0417 pCi/g Silver-lO8m U

0.0022

+/-0.0129 0.0101

+/-0.0129 0.0203 pCi/g Thallium-208 0.249

+/-0.033 0.0117

+/-0.033 0.0233 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.000837

+/-0.0244 0.0203 +/-0.0244 0.0475 pCi/g KSDI 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Surrogate/T racer recovery Test Recovery%

Acceptable Limits Page 54 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

.:Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-006F Project:

YANKOI1204 Sample ID:

183245007 Client ID:

YANKOQ I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, SrOO, solid-ALL FSS 71 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD1 Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 55 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address; 362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001 -007F 183245008 TS 24-MAR-07 29-MAR-07 Client 7.81%

Proiect:

Client ID:

Vol. Recv.:

YANK01204 YANK0OI Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.910

+/-0.160 0.0409

+/-0.160 0.0817 pCi/g MJHI 04/02/07 1513 621148 Americium-241 U

0.0826

+/-0.0682 0.0566 +/-0.0682 0.113 pCilg Bismuth-212 0.588

+/-0.182 0.0882

+/-0.182 0.176 pCilg Bismuth-214 0.661

+/-0.084 0.0227

+/-0.084 0.0453 pCilg Cesium-134 U

0.0268

+/-0.019 0.0151

+/-0.019 0.0302 pCilg Cesium-137 U -0.00643

+/-0.0161 0.0114 +/-0.0161 0.0227 pCilg Cobalt-60 U -0.0045

+/-0.0 146 0.0119 +/-0.0146 0.0239 pCilg Europium-152 U

-0.0708

+/-0.0434 0.0308 +/-0.0434 0.0616 pCi/g Europium-154 U

-0.0425

+/-0.0436 0.0341

+/-0.0436 0.0682 pCi/g Europium-ISS U

0.0503

+/-0.0496 0.0357 +/-0.0496 0.0715 pCi/g Lead-212 0.847

+/-0.0765 0.0181

+/-0.0765 0.0363 pCi/g Lead-214 0.737

+/-0.0804 0.023 +/-0.0804 0.046 pCi/g Manganese-54 U

0.00748

+/-0.0161 0.0124 +/-0.0161 0.0248 pCi/g Niobium-94 U

0.00969

+/-0.0129 0.0108 +/-0.0129 0.0215 pCi/g Potassium-40 15.3

+/-1.19 0.108

+1-1.19 0.216 pCi/g Radium-226 0.661

+/-0.084 0.0227

+/-0.084 0.0453 pCi/g Silver-108m U -0.00395

+/-0.0122 0.0105 +/-0.0122 0.0209 pCi/g Thallium-208 0.309

+/-0.0426 0.0115 +/-0.0426 0.023 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.00423

+/-0.0231 0.0201

+/-0.0231 0.0471 pCi/g KSDI 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Page 56 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel~com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-007F Project:

YANK01204 Sample ID:

183245008 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty

[C TPU MDA Units DF Analyst Date Time Batch b Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-1 25%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by CC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 57 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Anallsis Company:

Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

931 2-0001-008F 183245009 TS 24-MAR-07 29-MAR-07 Client 3.29%

Project:

Client ID:

Vol. Recv.:

YANKO 1204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch D~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.934

+/-0.150 0.0379

+/-0.150 0.0758 pCi/g MIHI 04/02/07 1515 621148 Americium-241 U

0.0407

+/-0.0474 0.0368 +/-0.0474 0.0735 pCi/g Bismuth-212 0.510

+/-0.172 0.0814

+/-0.172 0.163 pCi/g Bismuth-214 0.602

+/-0.076 0.0195

+/-0.076 0.039 pCi/g Cesium-134 UI 0.00

+/-0.0202 0.0135 +/-0.0202 0.027 pCi/g Cesium-]137 U -0.00217

+/-0.0143 0.0104 +/-0.0143 0.0209 pCi/g Cobalt-60 U

0.00237

+1-0.0134 0.0113 +/-0.0134 0.0227 pCi/g Europium-152 U

0.0119

+/-0.0413 0.0286 +/-0.0413 0.0571 pCi/g Europium-154 U -0.00741

+/-0.0446 0.0343 +/-0.0446 0.0685 pCi/g Europium-155 U

0.0514

+/-0.0407 0.0301 +/-0.0407 0.0601 pCi/g Lead-212 0.875

+1-0.0764 0.0161 +/-0.0764 0.0321 pCi/g Lead-214 0.689

+/-0.0776 0.0201 +/-0.0776 0.0402 pCi/g Manganese-54 U

0.00835

+/-0.0124 0.0112 +/-0.0124 0.0223 pCi/g Niobium-94 U

0.00908

+/-0.0122 0.0104 +/-0.0122 0.0207 pCi/g Potassium-40 15.7

+/-1.06 0.0963

+/-1.06 0.193 pCi/g Radium-226 0.602

+/-0.076 0.0195

+/-0.076 0.039 pCi/g Silver-108m U

-0.0051

+/-0.0108 0.00934 +/-0.0108 0.0187 pCi/g Thallium-208 0.285

+/-0.0348 0.0102 +/-0.0348 0.0203 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U

0.0282

+/-0.0288 0.0202 +/-0.0288 0.0472 pCi/g KSDI 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 58 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-008F Project:

YANK01204 Sample ID:

183245009 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 70 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GCIMS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 59 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address :

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-009F 183245010 TS 24-MAR-07 29-MAR-07 Client 4.49%

Proiect:

Client ID:

Vol. Recv.:

YANK0 1204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date.Time Batch P' Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.41

+/-0.215 0.0478

+/-0.215 0.0956 pCilg MJHI1 04/02/07 1516 621148 Americium-241 U

0.05 15

+/-0.0732 0.0586 +/-0.0732 0.117 pCi/g Bismuth-212 0.972

+/-0.231 0.095

+/-0.231 0.190 pCi/g Bismuth-2 14 1.11

+/-0.127 0.0252

+/-0.127 0.0504 pCi/g Cesium-] 34 UI 0.00

+1-0.0268 0.0187 +/-0.0268 0.0374 pCi/g Cesium-] 37 U

0.0047

+/-0.0203 0.0143 +/-0.0203 0.0285 pCi/g Cobalt-60 U -0.00423

+/-0.0173 0.0145 +/-0.0173 0.0289 pCi/g Europium-152 U

-0.0 192

+/-0.0461 0.034 +1-0.0461 0.0679 pCi/g Europium-]54 U

-0.0363

+/-0.0567 0.0431 +/-0.0567 0.0861 pCi/g Europium-ISS U

0.0672

+/-0.0606 0.0412 +/-0.0606 0.0824 pCi/g Lead-212 1.24

+/-0.104 0.0202

+1-0.104 0.0403 pCi/g Lead-214 1.22

+/-0.121 0.0253

+/-0.121 0.0506 pCi/g Manganese-54 U

0.0203

+/-0.0219 0.0127 +/-0.0219 0.0255 pCi/g Niobium-94 U

0.00836

+/-0.0147 0.0129 +/-0.0147 0.0257 pCi/g Potassium-40 20.4

+/-1.47 0.114

+/-1.47 0.229 pCi/g Radium-226 1.11I

+/-0.127 0.0252

+/-0.127 0.0504 pCi/g Silver-108m U

0.00904

+/-0.0142 0.0122 +/-0.0142 0.0244 pCi/g Thallium-208 0.395

+/-0.0481 0.0128 +/-0.0481 0.0256 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

0.00266

+/-0.0262 0.02 17 +/-0.0262 0.0485 pCi/g KSDI 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 60 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-009F Project:

YANK01204 Sample ID:

183245010 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 63 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain ]Identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 61 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils P04* 002332 Report Date:

April 5, 2007 Client Sample ID:

9312-0001-OlOF Project:

YANK01204 Sample ID:

183245011 Client ID:

YANKO0l Matrix:

TS Vol. Recv.:

Collect Date:

24-MAR-07 Receive Date:

29-MAR-07 Collector:

Client Moisture:

4.22%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Gamma Spec Analysis Gainma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.686

+/-0.127 0.0363

+1-0.127 0.0725 pCi/g MIHI 04/02/07 1517 621148 Americium-241 U

0.0377

+/-0.0472 0.0364 +/-0.0472 0.0729 pCi/g Bismuth-212 0.537

+/-0.175 0.0747

+/-0.175 0.149 pCi/g Bismuth-214 0.561

+/-0.0724 0.0208 +/-0.0724 0.0416 pCilg Cesium-134 UI 0.00

+/-0.0173 0.0126 +/-0.0173 0.0253 pCi/g Cesium-137 0.0799

+/-0.0234 0.0112 +/-0.0234 0.0223 pCi/g Cobalt-60 U

0.00397

+/-0.0137 0.0118 +/-0.0137 0.0235 pCi/g Europium-152 U

0.0167

+/-0.0467 0.0286 +/-0.0467 0.0571 pCi/g Europium-154 U

-0.0381

+/-0.0403 0.0318 +/-0.0403 0.0635 pCi/g Europium-ISS U

0.0325

+/-0.0365 0.0302 +/-0.0365 0.0604 pCi/g Lead-212 0.683

+/-0.063 0.016

+/-0.063 0.032 pCi/g Lead-214 0.666

+/-0.0806 0.0203 +/-0.0806 0.0405 pCi/g Manganese-54 U -0.00141

+/-0.0123 0.0106 +/-0.0123 0.0211 pCi/g Niobium-94 U

0.00888

+/-0.0119 0.0103 +/-0.0119 0.0206 pCi/g Potassium-40 11.8

+/-0.856 0.0912

+/-0.856 0.182 pCi/g Radium-226 0.561

+/-0.0724 0.0208 +/-0,0724 0.0416 pCi/g Silver-I 08m U -0.00434

+/-0.0111 0.00946 +/-0.0111 0.0189 pCi/g Thallium-208 0.218

+/-0.0338 0.0102 +/-0.0338 0.0203 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

0.0079

+/-0.0261 0.0211 +/-0.0261 0.0472 pCi/g KSDI 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Page 62of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Ce rtificate of Analysis Company Connecticut Yankee Atomic Power Address:

362 lnjun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-01 OF Project:

YANK0 1204 Sample ID:

193245011 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 64 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

131 Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 63 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-01 IF 183245012 TS 24-MAR-07 29-MAR-07 Client 9.94%

Proiect:

Client ID:

Vol. Recv.:

YANK01 204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.21

+/-0.181 0.0449

+/-0.181 0.0897 pCilg MIHI 04/02/07 1518 621148 Americium-241 UI 0.00

+/-0.0237 0.020 +/-0.0237 0.040 pCi/g Bismuth-212 0.705

+/-0.196 0.0996

+/-0.196 0.199 pCilg Bismuth-214 1.01

+/-0.114 0.0236

+1-0.114 0.0472 pCilg Cesium-134 UI 0.00

+/-0.0285 0.0175 +/-0.0285 0.0351 pCi/g Cesium-137 U

-0.0203

+1-0.0193 0.0125 +1-0.0193 0.025 pCi/g Cobalt-60 U

0.0257

+/-0.0234 0.0131 +/-0.0234 0.0261 pCi/g Europium-152 U

-0.0467

+/-0.0394 0.0304 +/-0.0394 0.0608 pCi/g Europium-154 U

-0.0628

+/-0.0492 0.0381 +/-0.0492 0.0762 pCi/g Europium-iSS UI 0.00

+/-0.0511 0.0307 +/-0.0511 0.0613 pCilg Lead-212 1.24

+/-0.135 0.0177

+/-0.135 0.0353 pCilg Lead-214 1.14

+/-0.119 0.0225

+/-0.119 0.0449 pCi/g Manganese-54 U

0.0105

+/-0.0155 0.0134 +/-0.0155 0.0268 pCi/g Niobium-94 U

0.00351

+/-0.0142 0.0121

+/-0.0142 0.0241 pCi/g Potassium-40 18.4

+1-1.30 0.0912

+/-1.30 0.182 pCilg Radium-226 1.01

+/-0.114 0.0236

+/-0.114 0.0472 pCilg Silver-108m U

-0.0143

+/-0.0124 0.0105 +/-0.0124 0.0209 pCilg Thallium-208 0.421

+/-0.0498 0.0122 +/-0.0498 0.0244 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U

-0.0162

+/-0.022 0.021

+/-0.022 0.049 pCi/g KSDI 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 64 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-01 IF Project:

YANK01204 Sample ID:

183245012 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 61 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

131 Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y

QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 65 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Certificate ofA alvsis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-012F 183245013 TS 24-MAR-07 29-MAR-07 Client 6.43%

Project:

Client ID:

Vol. Recv.:

YANK0 1204 YANKO0l Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.816

+/-0.137 0.0309

+/-0.137 0.0618 pCi/g MJHI 04/02/07 1528 621148 Americium-241 U

0.0449

+/-0.0409 0.0352 +/-0.0409 0.0704 pCi/g Bismuth-212 0.654

+/-0.171 0.0706

+/-0.171 0.141 pCi/g Bismuth-214 0.511

+/-0.0697 0.0184 +/-0.0697 0.0368 pCi/g Cesium-] 34 UI 0.00

+/-0.0183 0.0131 +/-0.0183 0.0262 pCi/g Cesium-]137 U

0.012

+/-0.0117 0.00988 +/-0.0117 0.0197 pCilg Cobalt-60 U

0.00394

+/-0.0114 0.00983 +/-0.0114 0.0196 pCilg Europium-152 U

-0.036

+/-0.0318 0.0249 +/-0.0318 0.0498 pCi/g Europium-154 U

-0.0316

+/-0.0361 0.0288 +/-0.0361 0.0575 pCi/g Europium-155 U

0.0238

+/-0.0393 0.0295 +/-0.0393 0.059 pCi/g Lead-212 0.778

+/-0.0661 0.015 +/-0.0661 0.030 pCi/g Lead-214 0.604

+/-0.0645 0.0184 +/-0.0645 0.0368 pCi/g Manganese-54 U

0.00303

+/-0.0113 0.0101 +/-0.0113 0.0201 pCi/g Niobium-94 U

0.00658

+/-0.0104 0.00914 +/-0.0104 0.0183 pCi/g Potassium-40 13.1

+/-0.940 0.0838

+/-0.940 0.168 pCi/g Radium-226 0.511

+/-0.0697 0.0184 +/-0.0697 0.0368 pCi/g Silver-108m U

-0.0129

+/-0.00974 0.00819 +/-0.00974 0.0164 pCi/g Thallium-208 0.233

+/-0.0309 0.0102 +/-0.0309 0.0204 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

0.0084

+/-0.0214 0.0164 +/-0.0214 0.0399 pCi/g KSDI 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Page 66 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-012F Project:

YANK01204 Sample ID:

183245013 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 64 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected al dol -condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD1 Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy---Uncertain identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 67 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-013F 183245014 TS 24-MAR-07 29-MAR-07 Client

.163%

Project:

Client ID:

Vol. Recv.:

YANKO01204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pt Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.691

+1-0.136 0.0462

+/-0.136 0.0923 pCi/g MJHI 04/02/07 1535 621148 Americium-241 U

0.00635

+/-0.0224 0.0182 +/-0.0224 0.0363 pCi/g Bismuth-212 0.496

+/-0.189 0.101

+/-0.189 0.202 pCi/g Bismuth-214 0.580

+/-0.0828 0.0228 +/-0.0828 0.0456 pCi/g Cesium-134 U

0.0327

+/-0.023 0.017

+/-0.023 0.0339 pCi/g Cesium-] 37 U

0.01 38

+/-0.0207 0.0118 +/-0.0207 0.0236 pCi/g Cobalt-60 U

0.00202

+/-0.017 0.0142

+/-0.017 0.0284 pCi/g Europium-152 U

0.00641

+/-0.0349 0.0295 +/-0.0349 0.059 pCi/g Europium-154 U

0.01 84

+/-0.0474 0.0405 +/-0.0474 0.081 pCi/g Europium-155 UI 0.00

+/-0.0489 0.0298 +/-0.0489 0.0595 pCi/g Lead-21 2 0.737

+/-0.0758 0.0158 +/-0.0758 0.0315 pCi/g Lead-214 0.560

+/-0.0713 0.0218 +/-0.0713 0.0436 pCi/g Manganese-54 U

0.0022

+/-0.0195 0.0134 +/-0.0195 0.0267 pCi/g Niobium-94 U -0.00857

+/-0.0139 0.0113 +/-0.0139 0.0226 pCi/g Potassium-40 13.2

+/-0.970 0.118

+/-0.970 0.235 pCi/g Radium-226 0.580

+/-0.0828 0.0228 +/-0.0828 0.0456 pCi/g Silver-108m U

0.00976

+/-0.0118 0.0108 +/-0.0118 0.0215 pCi/g Thallium-208 0.258

+/-0.0382 0.0119 +/-0.0382 0.0237 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, so/id-ALL FSS Strontium-90 U -0.00074

+/-0.0218 0.0184 +/-0.0218 0.0445 pCi/g KSDI 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Moditied Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 68 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-013F Project:

YANK01204 Sample ID:

183245014 Client ID:

YANKOO I Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Dt Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 63 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• • Analyte is a surrogate compound Result is less than value reported

Ž> Result is greater than value reported A

The TIC is a suspected aldol-condensation product 13 For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by CC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL hi Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 69of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils P04* 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-014F 183245015 TS 24-MAR-07 29-MAR-07 Client 4.35%

Project:

Client ID:

Vol. Recv.:

YANKO 1204 YANK00l Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch PI Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.868

+1-0.146 0.0359

+/-0.146 0.0717 pCi/g MJH 1 04/02/07 1524 621148 Americium-241 U

0.0525

+1-0.0539 0.0464 +/-0.0539 0.0927 pCi/g Bismuth-212 0.716

+/-0.203 0.0789

+/-0.203 0.158 pCi/g Bismuth-214 0.597

+/-0.0771 0.0193 +/-0.0771 0.0386 pCilg Cesium-134 UI 0.00

+/-0.0176 0.0135 +/-0.0176 0.0269 pCilg Cesium-137 U -0.00646

+/-0.014 0.0102

+/-0.014 0.0204 pCi/g Cobalt-60 U -0.00185

+/-0.0127 0.0108 +/-0.0127 0.0215 pCi/g Europium-152 U

-0.0392

+/-0.0407 0.0268 +/-0.0407 0.0536 pCi/g Europium-154 U -0.00108

+/-0.0451 0.0333 +/-0.0451 0.0666 pCi/g Europium-ISS U

0.051

+/-0.043 0.0322

+/-0.043 0.0644 pCi/g Lead-212 0.908

+/-0.078 0.0164

+/-0.078 0.0329 pCi/g Lead-214 0.704

+/-0.0794 0.020 +/-0.0794 0.0399 pCi/g Manganese-54 U

0.00355

+/-0.0141 0.00984 +/-0.0141 0.0197 pCi/g Niobium-94 U

0.00125

+/-0.0114 0.00992 +/-0.0114 0.01 98 pCi/g Potassium-40 15.7

+/-1.15 0.0835

+/-1.15 0.167 pCi/g Radium-226 0.597

+/-0.0771 0.0193 +/-0.0771 0.0386 pCi/g Silver-108m U -0.00155

+/-0.0109 0.00972 +/-0.0109 0.0194 pCi/g Thallium-208 0.264

+/-0.0323 0.0106 +/-0.0323 0.0211 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL ESS Strontium-90 U

-0.0349

+/-0.0253 0.023 +/-0.0253 0.0483 pCi/g KSD1 04/03/07 2022 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 70 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-014F Proiect:

YANK01204 Sample ID:

183245015 Client ID:

YANKOO I Vol. Recv.:

Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GCI/vS analysis D

Results are reported from a diluted aliquot of the sample 1-1 Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit Sample results are rejected

• J Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 71 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-015F 183245016 TS 24-MAR-07 29-MAR-07 Client 6.8 1%

Proiect:

Client ID:

Vol. Recv.:

YANK0 1204 YANKO0l Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P' Rad Alpha Spec Analysis Alphaspec Am24l, Cm, Solid ALL FSS Americium-241 U

Curium-242 U

Curium-243/244 U

Aiphaspec Pu, Solid-ALL FSS Plutonium-238 U

Plutonium-239/240 U

Liquid Scint Pu24J, Solid-ALL FSS Plutonium-241 U

Rad Gamma Spec Analysis 0.0157 0.00

-0.0742

+/-0.105

+/-0.0693

+/-0.171 0.080 0.00 0.166

+/-0. 105

+/-0.0693

+/-0.172 0.251 0.0958 0.423 0.393 0.245 13.5

-0.042

+1-0.152 0.144

+/-0.152

-0.0373

+1-0.0845 0.0698 +/-0.0845

-6.64

+/-7.32 6.45

+/-7.32 Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228I Americium-241 U

0.

Bismuth-212 2 Bismuth-2 14 Cesium-I 34 UI Cesium-] 37 U

-0.

Cobalt-60 U

0.

Europium-152 U -0.C Europium-154 U

-0.

Europium-155 U

0.

Lead-212 Lead-214 Manganese-54 U

0, Niobium-94 U

0.C Potassium-40 Radium-226 Silver-108m U

0.C Thallium-208 Rad Gas Flow Proportional Counting GFPC, SOO0, solid-ALL ESS Strontium-90 U 0.OC Rad Liquid Scintillation Analysis LSC', Tritium Dist, Solid -

3 pCi/g Tritium U

+/-0.134

+/-0.0402

+/-0.168

+/-0.0733

+/-0.025

+/-0.0135

+/-0.0127

+/-0.0385

+/-0.0398

+/-0.0357

+/-0.0801

+/-0.0729

+/-0.0149

+/-0.0122

+/-1.18

+/-0.0733

+/-0.0156

+/-0.0364 0.0399 0.0344 0.0894 0.0204 0.0147 0.0115 0.0113 0.0301 0.0324 0.033 0.01 74 0.02 18 0.0111 0.01 06 0.0793 0.0204 0.01 07 0.0107

+/-0. 134

+/-0.0402

+/-0. 168

+/-0.0733

+/-0.025

+/-0.0135

+/-0.0127

+/-0.0385

+/-0.0398

+/-0.0357

+/-0.0801

+/-0.0729

+/-0.0149

+/-0.0122

+/-1.18

+/-0.0733

+/-0.0156

+/-0.0364 0.0797 0.0688 0.179 0.0407 0.0294 0.023 0.0225 0.0602 0.0648 0.066 0.0347 0.043 6 0.0221 0.02 12 0.158 0.0407 0.02 15 0.0213 0.0386 1.94 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MIHI 04/02/07 1526 621148 KSDI 04/03/07 2022 621123 AXD2 03/31/07 1349 621141 GXR1 04/04/07 0820 621107 GXR1 04/04/07 2258 622351 BXLI 04/05/07 1410 622105

+/-0.0194 0.0162 +/-0.0194 0.00

+/-1.10 0.926

+/1-l0 Page 72 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

9312-0001-015F 183245016 Proiect:

Client ID:

Vol. Recv.:

YANK01204 "YANKOO I Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Liquid Scintillation Analysis Liquid Scint 014, Solid AIIFSS Carbon-14 U -0.00223

+/-0.0902 0.0758 +/-0.0902 0.155 pCi/g AXD2 03/30/07 1950 621144 Liquid Scint Fe5S, Solid-ALL FSS Iron-55 U

-2.52

+/-31.0 22.1

+/-31.0 46.6 pCi/g MXPI 04/02/07 2057 621136 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U

2.19

+/-10.5 8.70

+/-10.5 18.2 pCi/g MXP1 04/02/07 1605 621137 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U

-0.214

+/-0.216 0.186

+/-0.216 0.382 pCi/g MXPI 04/04/07 2357 621139 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

DOE EML HASL-300, Am-05-RC Modified 2

DOE EML HASL-300, Am-05-RC Modified 3

DOE EML HASL-300, Pu-I Il-RC Modified 4

DOE EML HASL-300, Pu-]Il-RC Modified 5

DOE EML HASL-300, Pu-Il-RC Modified 6

DOE EML HASL-300, Pu-Il-RC Modified 7

EML HASL 300, 4.5.2.3 8

EPA 905.0 Modified 9

EPA 906.0 Modified 10 EPA EERF C-01 Modified I I DOE RESL Fe-I, Modified 12 DOE RESL Ni-I, Modified 13 DOE EML HASL-300, Tc-02-RC Modified 14 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Americium-243 Tracer Plutonium-242 Tracer Plutonium-242 Tracer Aiphaspec Am24i, Cm, Solid ALL Aiphaspec Pu, Solid-ALL FSS Liquid Scint Pu24 1. Solid-ALL Fý 89 83 91 (15%-125%)

(15%-125%)

(25%-125%)

Page 73 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007

Contact:

Mr. Jaok McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-015F Project:

YANK01204 Sample ID:

183245016 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU M~DA Units DF Analyst Date Time Batch P Strontium Carrier GFPC, Sr90, solid-ALL FSS 76 (25%-125%)

Iron-59 Tracer Liquid Scint Fe55, Solid-ALL FS 64 (15%-125%)

Nickel Carrier Liquid Scint Ni63, Solid-ALL FS 75 (25%-125%)

Technetium-99m Tracer Liquid Scint Tc99, Solid-ALL FS 85 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

131 Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GCIMS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 74 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address:

362 lnjun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

93 12-000 1-0 16B 183245017 TS 24-MAR-07 29-MAR-07 Client 4.59%

Project:

Client ID:

Vol. Remv:

YANK0 1204 YANK0OI Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pt Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.947

+/-0.176 0.0419

+1-0.176 0.0837 pCi/g MJHI 04/02/07 1538 621148 Americium-241 U

0.067

+/-0.0671 0.0572 +/-0.0671 0.114 pCi/g Bismuth-212 0.727

+/-0.232 0.102

+/-0.232 0.205 pCi/g Bismuth-214 0.757

+/-0.0878 0.0242 +/-0.0878 0.0483 pCi/g Cesium-]134 UI 0.00

+/-0.0199 0.0161

+1-0.0199 0.0322 pCi/g Cesium-] 37 U

0.0171

+1-0.018 0.0138

+/-0.018 0.0276 pCilg Cobalt-60 U-0.000465

+/-0.0161 0.0136 +/-0.0161 0.0271 pCilg Europium-152 U

0.0532

+/-0.0642 0.0342 +/-0.0642 0.0683 pCi/g Europium-154 U

-0.0763

+/-0.0545 0.0428 +/-0.0545 0.0856 pCi/g Europium-ISS U

0.0574

+/-0.0527 0.0376 +/-0.0527 0.0752 pCi/g Lead-212 0.984

+/-0.087 0.0199

+/-0.087 0.0398 pCi/g Lead-214 0.890

+/-0.104 0.0242

+/-0.104 0.0485 pCi/g Manganese-54 U

0.0137

+/-0.0157 0.014 +/-0.0157 0.028 pCi/g Niobium-94 U

0.00465

+/-0.0143 0.0127 +/-0.0143 0.0254 pCi/g Potassium-40 16.3

+/-1.18 0.120

+/-1.18 0.240 pCi/g Radium-226 0.757

+/-0.0878 0.0242 +/-0.0878 0.0483 pCi/g Silver-108m U -0.00239

+/-0.0131 0.0116 +/-0.0131 0.0232 pCi/g Thallium-208 0.317

+/-0.0415 0.0127 +/-0.0415 0.0254 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

-0.0351

+/-0.0247 0.023 +/-0.0247 0.049 pCi/g KSDI 04/03/07 2023 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery.

Test Recovery%

Acceptable Limits Page 75 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-000-016B Project:

YANK01204 Sample ID:

183245017 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch D' Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 47 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GCIMS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y

QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 76 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-017B 183245018 TS 24-MAR-07 29-MAR-07 Client 6.44%

Proiect:

Client ID:

Vol. Recv.:

YANKO 1204 YANKOO I Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Gamma Spec Analysis Gamma,Solid-FSS GAM &ALL ESS 226 In growth Waived Actinium-228 0.977

+1-0.201 0.0637

+/-0.201 0.127 pCi/g MJHI 04/02/07 1540 621148 Americium-241 U

0.036

+/-0.0285 0.0228 +/-0.0285 0.0455 pCi/g Bismuth-212 0.998

+/-0.257 0.122

+/-0.257 0.243 pCi/g Bismuth-214 0.822

+/-0.119 0.0293

+/-0.119 0.0585 pCi/g Cesium-134 UI 0.00

+/-0.0304 0.0219 +/-0.0304 0.0439 pCi/g Cesium-137 U 0.000501

+/-0.0196 0.0172 +/-0.0196 0.0343 pCi/g Cobalt-60 U

0.00658

+/-0.0213 0.0181 +/-0.0213 0.0363 pCi/g Europium-152 U-0.000124

+/-0.0526 0.0373 +/-0.0526 0.0745 pCi/g Europium-I 54 U -0.00655

+/-0.0721 0.0598 +/-0.0721 0.120 pCi/g Europium-ISS UI 0.00

+/-0.0643 0.0342 +/-0.0643 0.0683 pCi/g Lead-212 1.03

+/-0.101 0.0206

+/-0.101 0.0411 pCi/g Lead-214 0.870

+/-0.104 0.0261

+/-0.104 0.0522 pCi/g Manganese-54 U

-0.0133

+/-0.0204 0.0169 +/-0.0204 0.0339 pCi/g Niobium-94 U

0.00641

+/-0.0177 0.0156 +/-0.0177 0.0312 pCi/g Potassium-40 16.9

+/-0.930 0.174

+/-0.930 0.348 pCi/g Radium-226 0.822

+/-0.119 0.0293

+/-0.119 0.0585 pCi/g Silver-108m U -0.00299

+/-0.0187 0.0138 +/-0.0187 0.0275 pCi/g Thallium-208 0.330

+/-0.0547 0.0156 +/-0.0547 0.03 13 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL ESS Strontium-90 U

0.0091

+/-0.0166 0.0127 +/-0.0166 0.0293 pCi/g KSDI 04/03/07 2231 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Page 77 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address :

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-017B Proiect:

YANK01204 Sample ID:

183245018 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch D~

Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 64 (25%-i125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 78 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-018B 183245019 TS 24-MAR-07 29-MAR-07 Client 2.18%

Project:

Client ID:

Vol. Recv.:

YANK0 1204 YANK001 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.901

+/-0.143 0.034

+/-0.143 0.0679 pCi/g MJHI 04/02/07 1546 621148 Americium-241 U

0.041

+/-0.0726 0.0632 +/-0.0726 0.126 pCi/g Bismuth-212 0.542

+/-0.166 0.0755

+/-0.166 0.151 pCi/g Bismuth-214 0.596

+/-0.0738 0.0186 +/-0.0738 0.0372 pCi/g Cesium-] 34 UI 0.00

+/-0.0162 0.0136 +/-0.0162 0.0271 pCi/g Cesium-137 U

-0.0044

+/-0.0125 0.0107 +/-0.0125 0.0213 pCi/g Cobalt-60 U

0.0071

+/-0.0138 0.012 +/-0.0138 0.0241 pCi/g Europium-152 U

-0.0338

+/-0.0478 0.0286 +/-0.0478 0.0572 pCi/g Europium-154 U

-0.029

+/-0.043 0.0351

+/-0.043 0.0701 pCi/g Europium-155 U

0.046

+/-0.0461 0.0364 +/-0.0461 0.0727 pCi/g Lead-212 0.802

+/-0.072 0.0174

+/-0.072 0.0348 pCi/g Lead-214 0.689

+/-0.0753 0.0195 +/-0.0753 0.0389 pCi/g Manganese-54 U

0.0222

+/-0.0158 0.012 +/-0.0158 0.0239 pCi/g Niobium-94 U

0.0049

+/-0.0118 0.0103 +/-0.0118 0.0206 pCi/g Potassium-40 14.8

+/-1.12 0.0746

+/-1.12 0.149 pCi/g Radium-226 0.596

+/-0.0738 0.0186 +/-0.0738 0.0372 pCi/g Silver-108m U -0.00189

+/-0.01 1 0.00983

+/-0.011 0.01 97 pCi/g Thallium-208 0.253

+/-0.0356 0.0104 +/-0.0356 0.0208 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.00185

+/-0.0146 0.0125 +/-0.0146 0.0285 pCi/g KSDI 04/03/07 2232 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 79 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-018B Project:

YANK01204 Sample ID:

183245019 Client ID:

YANKOQI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 84 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GCJMS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 80 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analy:sis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

93 12-0001-0 19B 183245020 TS 24-MAR-07 29-MAR-07 Client 6.55%

Proiect:

Client ID:

Vol. Recv.:

YANK0 1204 YANKOO I Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL ESS 226 In growth Waived Actinium-228 0.822

+1-0.125 0.0287

+/-0.125 0.0574 pCi/g MJHI 04/02/07 1547 621148 Americium-241 U

0.00221

+/-0.0599 0.0501 +/-0.0599 0.100 pCi/g Bismuth-212 0.452

+/-0.131 0.0607

+/-0.131 0.121 pCi/g Bismuth-214 0.514

+/-0.0663 0.0162 +/-0.0663 0.0323 pCi/g Cesium-]134 U

0.0189

+/-0.0163 0.0106 +/-0.0163 0.0211 pCi/g Cesium-] 37 U

0.0171

+/-0.0155 0.00872 +/-0.0155 0.0174 pCi/g Cobalt-60 U

0.0053

+/-0.0104 0.00919 +/-0.0104 0.0184 pCi/g Europium-152 U

-0.0192

+/-0.0294 0.0229 +/-0.0294 0.0457 pCi/g Europium-154 U -0.0102

+/-0.037 0.0268

+/-0.037 0.0536 pCi/g Europium-155 ul 0.00

+/-0.044 0.0291

+/-0.044 0.0581 pCi/g Lead-21 2 0.728

+/-0.0649 0.0134 +/-0.0649 0.0268 pCi/g Lead-214 0.563

+/-0.0637 0.0157 +/-0.0637 0.0314 pCi/g Manganese-54 UI 0.00

+/-0.0137 0.00784 +/-0.0137 0.0157 pCi/g Niobium-94 U -0.00827

+/-0.00935 0.00764 +/-0.00935 0.0153 pCi/g Potassium-40 12.2

+/-0.835 0.0805

+/-0.835 0.161 pCi/g Radium-226 0.514

+/-0.0663 0.0162 +/-0.0663 0.0323 pCi/g Silver-108m U

0.00612

+/-0.0083 0.00758 +/-0.0083 0.0152 pCi/g Thallium-208 0.210

+/-0.0276 0.00783 +/-0.0276 0.0157 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

0.0173

+/-0.0275 0.0213 +/-0.0275 0.0477 pCi/g KSDI 04/03/07 2232 621123 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1138 621094 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 81 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-019B Project:

YANK01204 Sample ID:

183245020 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch D' Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr9O, solid-ALL FSS 56 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GCIMS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 82 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

93 12-0001-020-1 Project:

YANKO 1204 Sample ID:

183245021 Client ID:

YANKO0l Matrix:

TS Vol. Recv.:

Collect Date:

26-MAR-07 Receive Date:

29-MAR-07 Collector:

Client Moisture:

1.52%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.53

+/-0.273 0.0781

+/-0.273 0.156 pCi/g MJHI1 04/03/07 0958 621149 Americium-241 U

-0.0412

+/-0.127 0.102

+/-0.127 0.203 pCi/g Bismuth-212 1.24

+/-0.343 0.177

+/-0.343 0.354 pCi/g Bismuth-214 1.72

+/-0.201 0.0417

+/-0.201 0.0834 pCi/g Cesium-134 UI 0.00

+/-0.0391 0.0319 +/-0.0391 0.0638 pCi/g Cesium-137 U

0.00215

+/-0.0314 0.0234 +/-0.0314 0.0468 pCi/g Cobalt-60 U

0.0276

+/-0.0282 0.0259 +/-0.0282 0.0518 pCi/g Europium-152 U -0.0264

+/-0.094 0.0628

+/-0.094 0.126 pCi/g Europium-154 U

0.0221

+/-0.100 0.0752

+/-0.100 0.150 pCi/g Europium-ISS U

0.119

+1-0.1 14 0.0745

+/-0.114 0.149 pCi/g Lead-212 1.71

+/-0.159 0.0382

+/-0.159 0.0763 pCi/g Lead-2 14 1.68

+/-0.189 0.0487

+/-0.189 0.0974 pCi/g Manganese-54 U

0.0119

+/-0.0307 0.0232 +/-0.0307 0.0463 pCi/g Niobium-94 U

0.01 26

+/-0.026 0.0228

+/-0.026 0.0455 pCi/g Potassium-40 25.6

+/-2.07 0.186

+/-2.07 0.373 pCi/g Radium-226 1.72

+/-0.201 0.0417

+/-0.201 0.0834 pCi/g Silver-108m U -0.00652

+/-0.0249 0.02 17 +/-0.0249 0.0434 pCi/g Thallium-208 0.564

+/-0.0846 0.0224 +/-0.0846 0.0448 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U

-0.0124

+/-0.0237 0.0214 +/-0.0237 0.0485 pCi/g NXL3 04/03/07 1641 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-02 I LXM2 03/29/07 1137 621097 The following Analytical Methods were performed Method Description 2

EML HASL 300,4.5.2.3 EPA 905.0 Modified Page 83 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-020-1 Project:

YANK01204 Sample ID:

183245021 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch PI Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, SrOO, solid-ALL FSS 55 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 84of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-021-1 183245022 TS 26-MAR-07 29-MAR-07 Client 1.24%

Proiect:

Client ID:

Vol. Recv.:

YANK01 204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.33

+/-0.272 0.0666

+/-0.272 0.133 pCi/g MJHI1 04/03/07 0959 621149 Americium-241 U

0.110

+/-0.0799 0.0691 +/-0.0799 0.138 pCi/g Bismuth-212 0.738

+/-0.284 0.174

+/-0.284 0.347 pCilg Bismuth-214 1.16

+/-/-0.153 0.0386

+/-0.153 0.0772 pCilg Cesium-134 UI 0.00

+/-0.0527 0.0288 +/-0.0527 0.0575 pCi/g Cesium-137 U -0.00499

+/-0.0287 0.0208 +/-0.0287 0.0415 pCilg Cobalt-60 U

-0.0238

+/-0.0258 0.0197 +/-0.0258 0.0395 pCilg Europium-152 U

-0.0743

+/-0.0781 0.0576 +/-0.0781 0.115 pCilg Europium-154 U

0.015

+/-0.080 0.0592

+/-0.080 0.118 pCi/g Europium-ISS U

0.0994

+/-0.0844 0.0657 +/-0.0844 0.131 pCi/g Lead-21 2 1.35

+/-0.128 0.03 5

+/-0.128 0.0699 pCilg Lead-214 1.26

+/-0.141 0.0441

+/-0.141 0.0881 pCi/g Manganese-54 U

0.0208

+/-0.0326 0.0229 +/-0.0326 0.0457 pCi/g Niobium-94 U

0.00391

+/-0.0231 0.0198 +/-0.0231 0.0397 pCi/g Potassium-40 20.2

+/-1.63 0.201

+/-1.63 0.401 pCi/g Radium-226 1.16

+/-0.153 0.0386

+/-0.153 0.0772 pCi/g Silver-108m U

-0.0348

+/-0.0237 0.0185 +/-0.0237 0.0371 pCi/g Thallium-208 0.448

+/-0,0582 0.0208 +/-0.0582 0.0416 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U

0.00941

+/-0.0269 0.0214 +/-0.0269 0.0488 pCi/g NXL3 04/03/07 1703 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1137 621097 The following Analytical Methods were performed Method Description I

~~EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 85 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-021-1 Project:

YANK01204 Sample ID:

183245022 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Di Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 54 (25%-I 25%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD1 Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 86 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

93 12-0001-022-1 183245023 TS 26-MAR-07 29-MAR-07 Client 6.25%

Project:

Client ID:

Vol. Recv.:

YANKO01204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch D~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.65

+/-0.377 0.142

+/-0.377 0.283 pCi/g MJHI 04/03/07 1005 621149 Americium-241 U

0.0858

+/-0.0729 0.0589 +/-0.0729 0.118 pCi/g Bismuth-212 1.43

+/-0.586 0.279

+/-0.586 0.558 pCi/g Bismuth-214 1.64

+/-0.258 0.071

+/-0.258 0.142 pCi/g Cesium-134 U

0.0887

+/-0.0734 0.0596 +/-0.0734 0.119 pCi/g Cesium-] 37 U

0.0107

+/-0.051 0.0451

+/-0.051 0.0901 pCi/g Cobalt-60 U

-0.0159

+/-0.0563 0.045 +/-0.0563 0.090 pCi/g Europium-152 U

0.0703

+/-0.176 0.0939

+/-0.176 0.188 pCi/g Europium-154 U

-0.0491

+/-0.190 0.129

+/-0.190 0.258 pCi/g Europium-ISS U

0.148

+/-0.123 0.0926

+/-0.123 0.185 pCi/g Lead-212 1.83

+/-0.198 0.0525

+/-0.198 0.105 pCi/g Lead-214 1.90

+/-0.257 0.0697

+/-0.257 0.139 pCi/g Manganese-54 U

-0.0188

+/-0.0496 0.0412 +/-0.0496 0.0823 pCi/g Niobium-94 U

0.0504

+/-0.0465 0.0432 +/-0.0465 0.0863 pCi/g Potassium-40 26.7

+/-2.06 0.286

+/-2.06 0.572 pCi/g Radium-226 1.64

+/-0.258 0.071

+/-0.258 0.142 pCi/g Silver-1O8m U

0.0229

+/-0.0396 0.031

+/-0.0396 0.062 pCi/g Thallium-208 0.578

+/-0.140 0.0372

+/-0.140 0.0744 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

0.00 135

+/-0.0261 0.02 17 +/-0.0261 0.0485 pCi/g NXL3 04/03/07 1704 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1137 621097 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Page 87 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

93 12-0001-022-1 Project:

YANKOI2O4 Sample ID:

183245023 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Di Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 64 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 88 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address :362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO#~ 002332 Report Date: April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-023-1 183245024 TS 26-MAR-07 29-MAR-07 Client 2.79%

Project:

Client ID:

Vol. Recv.:

YANKO 1204 YANKO0l Parameter Qualifier Result Uncertainty ILC TPU MDA Units DF Analyst Date Time Batch P~

Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 2.16

+/-0.390 0.140

+/-0.390 0.280 pCi/g MIHI 04/03/07 1207 621149 Americium-241 U

0.0788

+/-0.0736 0.0574 +/-0.0736 0.115 pCi/g Bismuth-212 1.14

+/-0.457 0.265

+/-0.457 0.530 pCi/g Bismuth-214 1.72

+/-0.268 0.068

+/-0.268 0.136 pCi/g Cesium-134 U

0.0729

+/-0.0624 0.0461 +/-0.0624 0.0921 pCilg Cesium-137 U

-0.0231

+/-0.0446 0.036 +/-0.0446 0.072 pCi/g Cobalt-60 U

0.0077

+/-0.0416 0.0355 +/-0.0416 0.0709 pCilg Europium-152 U -0.0148

+/-0.121 0.0918

+/-0.121 0.183 pCilg Europium-154 U

-0.0416

+/-0.146 0.119

+1-0.146 0.237 pCi/g Europium-155 U -0.00664

+/-0.102 0.0907

+/-0.102 0.181 pCilg Lead-212 2.12

+/-0.264 0.10511

+/-0.264 0.102 pCi/g Lead-214 1.88

+/-0.255 0.0699

+/-0.255 0.140 pCi/g Manganese-54 U

0.0215

+/-0.0474 0.0384 +/-0.0474 0.0767 pCi/g Niobium-94 U -0.0356

+/-0.0441 0.0347 +/-0.0441 0.0694 pCi/g Potassium-40 25.8

+/-2.29 0.282

+/-2.29 0.563 pCi/g Radium-226 1.72

+/-0.268 0.068

+/-0.268 0.136 pCi/g Silver-108m U

0.0278

+/-0.0384 0.0346 +/-0.0384 0.0692 pCi/g Thallium-208 0.597

+/-0.0964 0.0366 +/-0.0964 0.0732 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

-0.0172

+/-0.0249 0.0224 +/-0.0249 0.0489 pCi/g NXL3 04/03/07 1704 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1137 621097 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Page 89 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wvww.gei.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-023-1 Project:

YANK01204 Sample ID:

183245024 Client ID:

YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 49 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 90 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certific2tI~ of A n~i 1V~i5~

Certificate ofAnalvsis Company Connecticut Yankee Atomic Power Address :362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-024-I 183245025 TS 26-MAR-07 29-MAR-07 Client 8.93%

Project:

Client ID:

Vol. Recv.:

YANK01204 YANKOO 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 1.89

+1-0.405 0.129

+/-0.405 0.258 pCi/g MJHI 04/03/07 1208 621149 Americium-241 Ui 0.0723

+/-0.0792 0.0658 +/-0.0792 0.132 pCi/g Bismuth-212 1.59

+/-0.724 0.276

+/-0.724 0.551 pCi/g Bismuth-214 1.76

+/-0.251 0.0675

+/-0.251 0.135 pCi/g Cesium-134 U

0.0981

+/-0.0836 0.0511 +/-0.0836 0.102 pCi/g Cesium-137 U 0.000663

+/-0.0563 0.041 +/-0.0563 0.082 pCi/g Cobalt-60 U

0.01 67

+/-0.0472 0.0408 +/-0.0472 0.0816 pCi/g Europium-152 U -0.00532

+/-0.124 0.0993

+/-0.124 0.198 pCi/g Europium-154 U -0.0596

+/-0.146 0.118

+/-0.146 0.235 pCi/g Europium-155 U

0.100

+/-0.112 0.103

+/-0.112 0.205 pCi/g Lead-212 1.76

+/-0.196 0.0562

+/-0.196 0.112 pCi/g Lead-214 1.82

+/-0.231 0.0691

+/-0.231 0.138 pCi/g Manganese-54 U

0.00262

+/-0.0475 0.0413 +/-0.0475 0.0826 pCi/g Niobium-94 U

0.0433

+/-0.0446 0.0396 +/-0.0446 0.0792 pCi/g Potassium-40 24.1

+/-2.18 0.420

+/-2.18 0.839 pCi/g Radium-226 1.76

+/-0.251 0.0675

+/-0.251 0.135 pCi/g Silver-I 08m U -0.00324

+/-0.0392 0.0339 +/-0.0392 0.0677 pCi/g Thallium-208 0.571

+/-0.110 0.0383

+/-0.1 10 0.0765 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U

-0.0 174

+/-0.0253 0.0225 +/-0.0253 0.0487 pCi/g NXL3 04/03/07 1704 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1137 621097 The following Analytical Methods were performed Method Description I

EML HASL 300,4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery %

Acceptable Limits Page 91 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

93 12-0001-024-1 Project:

YANK01204 Sample ID:

183245025 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date TimneBatch P' Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS -55 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 92 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-025-I 183245026 TS 26-MAR-07 29-MAR-07 Client 8.18%

Proiect:

Client ID:

Vol. Recv.:

YANKO 1204 YANKOG 1 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 Americium-241 Bismuth-21 2 Bismuth-214 Cesium-I 34 Cesium-I 37 Cobalt-60 Europium-152 Europium-I 54 Europium-155 Lead-21 2 Lead-214 1.35 U -0.00336 1.67 1.37 U

0.0854 U

0.0059 U

0.0147 U

0.012 U -0.00904 U

0.0646 1.19 1.37

+/-0.289

+/-0.0551

+/-0.660

+/-0.2 17

+/-0.0698

+/-0.0451

+/-0.0339

+/-0.0883

+/-0.128

+/-0.0827

+/-0.153

+/-0. 187

+/-0.0368

+/-0.0344

+1-1.89

+/-0.2 17

+/-0.0294

+/-0.096 0.109 0.0463 0.232 0.0521 0.0454 0.0334 0.0299 0.077 0.105 0.0774 0.0503 0.0448 0.0307 0.028 0.250 0.0521 0.0244 0.030

+/-0.289

+/-0.0551

+/-0.660

+/-0.217

+/-0.0698

+/-0.0451

+/-0.0339

+/-0.0883

+/-0.128

+/-0.0827

+/-0.153

+/-0.187

+/-0.0368

+/-0.0344

+1-1.89

+/-0.2 17

+/-0.0294

+/-0.096 0.218 0.0925 0.464 0.104 0.0908 0.0668 0.0598 0.154 0.210 0.155 0.101 0.0896 0.0614 0.056 0.500 0.104

0. 0488 0.0599

0. 0495 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g MJHI 04/03/07 1209 621149 NXL3 04/03/07 1710 621125 Manganese-54 U -

Niobium-94 U -

Potassium-40 Radium-226 Silver-108m U

Thallium-208 Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U

.0.00848

.0.00882 20.4 1.37

-0.0191 0.427

-0.0131

+/-0.0239 0.0217 +/-0.0239 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1137 621097 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 93 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:

Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date:

April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

9312-0001-025-I Project:

YANK01204 Sample ID:

183245026 Client ID:

YANKOOI Vol. Recv.:

Parameter Quallifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 46 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

131 Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 94 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com (i~rtific2te of A n2Iv~i~

Certificate ofA alvsis Company :Connecticut Yankee Atomic Power Address:

362 Injun Hollow Rd East Hampton, Connecticut 06424

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Report Date:

April 5, 2007 Client Sample ID:

Sample ID:

Matrix:

Collect Date:

Receive Date:

Collector:

Moisture:

9312-0001-026-I 183245027 TS 26-MAR-07 29-MAR-07 Client 7.87%

Proiect:

Client ID:

Vol. Recv.:

YANK01 204 YANKOO I Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch P Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 In growth Waived Actinium-228 0.884

+/-0.479 0.146

+/-0.479 0.291 pCi/g MJHI1 04/03/07 1210 621149 Americium-241 U

0.0568

+/-0.078 0.0549

+/-0.078 0.110 pCi/g Bismuth-212 U

0.575

+/-0.449 0.308

+/-0.449 0.616 pCi/g Bismuth-2 14 1.56

+/-0.244 0.0589

+/-0.244 0.118 pCi/g Cesium-134 U

0.0979

+/-0.0723 0.0519 +/-0.0723 0.104 pCi/g Cesium-137 U

-0.0145

+/-0.0448 0.0382 +/-0.0448 0.0764 pCi/g Cobalt-60 U

0.00834

+/-0.0505 0.043 +/-0.0505 0.0859 pCi/g Europium-152 U

0.0373

+/-0.112 0.0911

+/-0.112 0.182 pCi/g Europium-154 U

0.0667

+/-0.172 0.131

+/-0.172 0.263 pCi/g Europium-155 U

0.0269

+1-0.105 0.0816

+1-0.105 0.163 pCi/g Lead-212 1.36

+/-0.160 0.048

+/-0.160 0.0959 pCi/g Lead-214 1.42

+/-0.202 0.0637

+/-0.202 0.127 pCi/g Manganese-54 U

0.057

+/-0.0454 0.043 +/-0.0454 0.0859 pCi/g Niobium-94 U

0.0453

+/-0.0681 0.0352 +/-0.0681 0.0704 pCi/g Potassium-40 23.1

+/-1.92 0.282

+/-1.92 0.563 pCi/g Radium-226 1.56

+/-0.244 0.0589

+/-0.244 0.118 pCi/g Silver-108m U -0.00173

+/-0.0378 0.0324 +/-0.0378 0.0648 pCi/g Thallium-208 0.469

+/-0.108 0.0386

+/-0.108 0.0771 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U -0.00858

+/-0.0193 0.0179 +/-0.0193 0.0434 pCi/g NXL3 04/03/07 1710 621125 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 03/29/07 1137 621097 The following Analytical Methods were performed Method Description I

EML HASL 300, 4.5.2.3 2

EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Page 95 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company :Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: April 5, 2007

Contact:

Mr. Jack McCarthy Project:

Soils PO# 002332 Client Sample ID:

93 12-0001-026-I Project:

YANK01204 Sample ID:

183245027 Client ID:

YANKO0l Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Pi Surrogate/Tracer recovery Test Recovery%

Acceptable Limits Strontium Carrier GFPC, Sr90, solid-ALL FSS 64 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GCIMS analysis D

Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 96 of 110

I QUALITY CONTROL DATA I I Page 97 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Client :

Connecticut Yankee Atomic Power 362 Injun Hollow Rd Renort Date: April 5, 2007 Page 1 of 13 East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder:

183245 Parmname Rad Alpha Spec Batch 621107 QC1201305241 183245006 DUP Americium-24 1 Curium-242 Curium-243/244 NOM Sample QuqJ OC Unit-RPD%

REC%

Ranue Anist Date Time u

-0.0394 Uncert:

+/-0.08 16 TPU:

+/-0.0818 U

0.00 Uncert:

+/-0.083 TPU:

+/-0.083 U

0.00 Uncert:

+1-0.0794 TPU:

+/-0.0794 QC1201305243 Americium-24 I Curium-242 Curium-243/244 QCI 201305240 Americium-24 I LCS MB 12.4 Uncert:

TPU:

Uncert:

TPU:

14.8 Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

U

-0.0452

+1-0.0683

+/-0.0684 U

0.00

+/-0.0676

+/-0.0676 U

-0.0555

+/-0.0411

+/-0.0418 11.2

+/-1.06

+/-1.79 U

0.00

+/-0.0518

+/-0.0518 14.2

+/-1.19

+/-2.18 U

-0.0487

+/-0.0641

+/-0.0641 U

0.00

+/-0.0603

+/-0.0603 U

0.0459

+/-0.0861

+/-0.0863 pCi/g 14 pCi/g 0

pCi/g 200 pCi/g Curium-242 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g (0% -100%) GXRI 04/03/07 09:33 (0%- 100%)

(0% - 100%)

90 (75%-125%)

96 (75%-125%)

Curium-243/244 QCI 201305242 Americium-24 I Curium-242 Curium-243/244 183245006 MS 3.5 U

-0.0394 Uncert:

+/-0.08 16 TPU:

+/-0.0818 U

0.00 Uncert:

+/-0.083 TPU:

+/-0.083 16.1 U

0.00 Uncert:

+/-0.0794 TPU:

+/-0.0794 U

12.0

+/-1.16

+/-1.94 0.0303

+/-0.0594

+/-0.0595 14.9

+/-1.29

+/-2.33 89 (75%-125%)

93 (75%-125%)

Batch 622105 QC1201307489 183245006 DUP Plutonium-24 I U

-3.12 U

-8.22 pCi/g 0

(0% -100%) BXLI 04/05/07 15:31 Page 98 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Parmname Rad Alpha Spec Batch 622105 Page 2 of 13 NOM Sample Qual QC Units RPD%

REC%

Range Anist Date Time QC1201307491 LCS Plutonium-24 I QC1201307488 MB Plutonium-24 1 QC1201307490 183245006 MIS Plutonium-241 Uncert:

TPU:

138 Uncen:

TPU:

Uncert:

TPU:

140 U

Uncert:

TPU:

+/-10.1

+1-10.1

+/-9.75

+/-9.75 113

+/-14.9

+/-19.1 U

-1.9 pCi/g pCi/g pCi/g 82 (75%-125%)

04/05/07 16:04 04/05/07 15:15 04/05/07 15:48

-3.12 Batch 622351 120

+/-13.1

+/-17.4

-0.0 147

+/-0.0204 86 (75%-125%)

QC1201308035 183245006 DUP Plutonium-238 Plutonium-239/240 QC1201308037 LCS Plutonium-238 Plutonium-239/240 QC 1201308034 MB Plutonium-238 Plutonium-239/240 QC1201308036 183245006 MIS Plutonium-238 u

0.0429 Uncert:

+/-0.0969 TPU:

+/-0.0971 u

0.059 Uncert:

+/-0.0943 TPU:

+/-0.0946 Uncert:

TPU:

12.7 Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

U 0.0429 Uncert:

+/-0.0969 TPU:

+/-0.0971 13.7 U

0.059 Uncert:

+/-0.0943 TPU:

+/-0.0946 u

+/-0.0204 U

0.0306

+/-0.060

+/-0.0601 U

0.0151

+/-0.0602

+/-0.0603 12.9

+/-1.20

+1-1.91 U

-0.00689

+1-0.0135

+/-0.0135 U

-0.0138

+/-0.0 191

+/-0.0192 pCilg 409 pCi/g 63 pCi/g pCi/g (0% - 100%) GXR I (0% -100%)

(75%-125%)

102 (75%-125%)

04/04/07 22:5 8 pCi/g pCi/g pCi/g pCi/g u

0.0767

+/-0.105

+/-0.106 14.9

+/- 1.32

+/-2.15 (75%-1 25%)

Plutonitim-239/240 109 (75%-125%)

Rad Gamnma Spec Batch 621148 QC1201305341 183245001 DUP Actinium-228 0.454

+/-0.150O Uncert:

0.539

+/-0. 112

+/-0.112 pCi/g 17 (0% - 100%) MJHI1 04/02/07 18:03 Page 99 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 3 of 13 Parmname NOM Sample Qual QC Units RPD%

REC%

Range Anist Date Time Rad Gamma Spec Batch 621148 Americium-241 Bismuth-2 12 Bismuth-214 Cesium-134 Cesium-137 Cobalt-60 Europium-I 52 Europium-154 Europium-155 TPU:

+1-0.150 u

0.0498 Uncert:

+/-0.066 TPU:

+/-0.066 Ul 0.00 Uncert:

+/-0.207 TPU:

+/-0.207 0.371 Uncert:

+/-0.0773 TPU:

+/-0.0773 U

0.0207 Uncert:

+/-0.0 199 TPU:

+/-0.0199 U

0.0128 Uncert:

+/-0.0247 TPU:

+/-0.0247 U

0.0139 Uncert:

+/-0.02 15 TPU:

+/-0.0215 U

-0.0239 Uncert:

+/-0.0558 TPU:

+/-0.0558 U

0.00648 Uncert:

+/-0.0619 TPU:

+/-0.06 19 U

0.0856 Uncert:

+/-0.05 14 TPU:

+/-0.05 14 0.534 Uncert:

+/-0.0676 TPU:

+/-0.0676 0.436 Uncert:

+/-0.0773 TPU:

+/-0.0773 U

0,0173 Uncert:

+/-0.0166 TPU:

+/-0.0 166 U

0.00137 Uncert:

+/-0.0 179 TPU:

+/-0.0 179 9.22 Uncert:

+/-0.883 TPU:

+/-0.883 0.371 Uncert:

+/-0.0773 TPU:

+/-0.0773 U

0.00822 Uncert:

+/-0.0 162 U

0.0345

+/-0.0596

+/-0.0596 0.34 1

+/-0.160

+/-0.160 0.379

+/-0.0602

+/-0.0602 U

0.000141

+/-0.0267

+/-0.0267 U

0.00416

+/-0.0193

+/-0.0193 U

0.00394

+/-0.0151

+/-0.0151 U

-0.000835

+/-0.0358

+/-0.0358 U

-0.00786

+/-0.0404

+/-0.0404 U

0.00483

+/-0.0343

+/-0.0343 0.423

+/-0.044

+/-0.044 0.415S

+/-0.057

+/-0.057 U

0.0164

+/-0.0143

+/-0.0143 U

-0.00269

+/-0.0117

+/-0.0117 9.84

+/-0.783

+/-0.783 0.379

+/-0.0602

+/-0.0602 U

-0.00827

+/-0.00995 pCi/g 36 pCi/g 14 pCi/g 2

pCi/g 197 pCi/g 102 pCi/g 112 pCi/g 187 pCi/g 2080 pCi/g 179 pCi/g 23*

pCi/g 5

pCi/g 5

pCi/g 614 pCi/g 7

pCi/g 2

pCi/g 66000 (0% - 100%)

(0% - 100%)

(0% - 100%)

(0% - 100%)

(0% -100%)

(0% - 100%)

(0% - 100%)

(0% - 100%)

(0% - 100%)

(0%-20%)

(0% - 100%)

(0% - 100%)

(0%- 100%)

(0% -20%)

(0%- 100%)

(0%- 100%)

Lead-212 Lead-214 Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver-I 08m Page 100 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Workorder:

183245 Parmname Rad Gamma Spec Batch 621148 Thallium-208 QC1201305342 LCS Actinium-228 Americium-24 I Bismuth-2 12 Bismuth-2 14 Cesium-134 Cesium-137 Cobalt-60 Europium-152 Europium-154 Europium-155 Lead-212 Lead-214 Manganese-54 Niobium-94 Potassium-40 QC Summary Page 4 of 13 NOM Sample Qua]

QC Units RPD%

REC%

Range Anist Date Tim e TPU:

Uncert:

TPU:

Uncert:

TPU:

16.0 Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

6.20 Uncert:

TPU:

9.32 Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

+1-0.0162 0.159

+/-0.034

+/-0.034

+/-0.00995 0.133

+/-0.0272

+/-0.0272 U

0.455

+/-0.477

+/-0.477 13.7

+/-2.15

+/-2.15 U

0.848

+/-0.760

+/-0.760 0.641

+/-0.309

+/-0.309 U

0.014

+/-0.115

+/-0.115 5.84

+/-0.487

+/-0.487 8.92

+/-0.678

+/-0.678 U

-0.26

+/-0.261

+/-0.261 U

0.023

+/-0.243

+/-0.243 U

-0.202

+/-0.290

+/-0.290 0.995

+/-0.293

+/-0.293 0.864

+/-0.307

+/-0.307 U

-0.0401

+/-0.107

+/-0.107 U

-0.0423

+/-0.0934

+/-0.0934 U

0.265 pCi/g 18 (0%- 100%)

pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g 04/02/07 13:59 86 (75%-125%)

94 (75%-125%)

96 (75%-125%)

Page 101 of 110

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 5 of 13 Parmname NOM SaMDie Oual OC IJnit' RPD%

REC%

Ranee Anist Date Time Rad Gamma Spec Batch 621148 Radium-226 Silver-i 08m Thallium-208 QC1201305340 Actinium-228 Americium-24 1 Bismuth-2 12 Bismuth-214 Cesium-134 Cesium-137 Cobalt-60 Europium-152 Europium-154 Europium-] 55 MB Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:-

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

+/-1.40

+/-1.40 0.641

+/-0.309

+/-0.309 U

0.0309

+/-0.0841

+/-0.0841 0.357

+/-0.178

+/-0.178 U

0.0219

+/-0.0568

+/-0.0568 U

0.0142

+/-0.0309

+/-0.0309 U

0.0481

+/-0.0585

+/-0.0585 U

-0.00992

+/-0.0231

+/-0.0231 U

0.00219

+/-0.0102

+/-0.0102 U

-0.00319

+/-0.00774

+/-0.00774 U

-0.00692

+/-0.00883

+/-0.00883 U

0.00367

+/-0.022

+/-0.022 U

0.0228

+/-0.022

+/-0.022 U

-0.0278

+/-0.0253

+/-0.0253 U

0.00794

+/-0.0205

+/-0.0205 U

-0.022

+/-0.0274

+/-0.0274 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g (75%-125%)

04/02/07 18:01 Lead-21 2 Lead-214 Page 102 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 6 of 13 Parmname NOM Sample Oual OC Units RPD%

REC %

Range AnIst Date Time Rad Gamma Spec Batch 621148 Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver-I 08m Thallium-208 Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Batch 621149 QC1 201305348 Actinium-228 Americium-24 I Bismuth-2 12 Bismuth-214 Cesium-I 34 Cesium-137 Cobalt-60 Europium-I 52 Europium-154 Europium-I 55 183245021 DUP 1.53 Uncert:

+/-0.273 TPU:

+/-0.273 U

-0.0412 Uncert:

+/-0.127 TPU:

+/-0.127 1.24 Uncert:

+/-0.343 TPU:

+/-0.343 1.72 Uncert:

+/-0.201 TPU:

+/-0.201 UI 0.00 Uncert:

+/-0.0391 TPU:

+/-0.0391 U

0.00215 Uncert:

+/-0.0314 TPU:

+/-0.03 14 U

0.0276 Uncer:

+/-0.0282 TPU:

+/-0.0282 U

-0.0264 Uncert:

+/-0.094 TPU:

+/-0.094 U

0.0221 Uncert:

+/-0.100 TPU:

+/-0.100 U

0.119 U

0.000811

+/-0.00741

+/-0.00741 U

-0.00166

+/-0.00749

+/-0.00749 UI1 0.00

+/-0.139

+/-0.139 U

-0.00992

+/-0.0231

+/-0.0231 U

-0.00426

+/-0.00719

+/-0.00719 UI1 0.00

+/-0.0123

+/-0.0123 1.59

+/-0.286

+/-0.286 U

0.0296

+/-0.0983

+/-0.0983 1.09

+/-0.394

+/-0.394 1.65

+/-0.195

+/-0.195 U 1 0.00

+/-0.0442

+/-0.0442 U

-0.00812

+/-0.0328

+/-0.0328 U

0.00443

+/-0.0349

+/-0.0349 U

0.0111

+/-0.0925

+/-0.0925 U

-0.0225

+/-0.0951

+/-0.0951 U

0.123 pCi/g pCi/g pCi/g pCi/g pCi/g pci/g pCi/g 4

pCi/g 1220 pCi/g 13 pCi/g 4

pCi/g 9

pCi/g 344 pCi/g 145 pCi/g 492 pCi/g 22900 pCi/g 31 (0% -100%)

MJH1 04/03/07 12:58 (0% - 100%)

(0% -100%)

(0% -20%)

(0%- 100%)

(0% - 100%)

(0% - 100%)

(0% - 100%)

(0% - 100%)

(0%- 100%)

Page 103 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 7 of 13 Parmname NOM Sample Qual QC Units RPD%

REC%

Range Anist Date Time Rad Gamma Spec Batch 621149 Lead-212 Lead-214 Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver-I 08m Thallium-208 QCI 201305349 Actinium-228 Americium-24 I Uncert:

+/-0.114 TPU:

+/-0.114 1.71 Uncert:

+/-0.159 TPU:

+/-0.159 1.68 Uncert:

+/-0.189 TPU:

+/-0.189 U

0.0119 Uncert:

+/-0.0307 TPU:

+/-0.0307 U

0.0126 Uncert:

+/-0.026 TPU:

+/-0.026 25.6 Uncert:

+/-2.07 TPU:

+/-2.07 1.72 Uncert:

+/-0.201 TPU:

+/-0.201 U

-0.00652 Uncert:

+/-0.0249 TPU:

+/-0.0249 0.564 Uncert:

+/-0.0846 TPU:

+/-0.0846

+/-0.120

+/-0.120 1.72

+1-0.155

+/-0.155 1.94

+/-0.205

+/-0.205 U

-0.00151

+/-0.0268

+/-0.0268 U

0.0123

+/-0.0256

+/-0.0256 24.1

+/- 1.82

+/-1.82 1.65

+/-0. 195

+/-0. 195 U

-0.0062

+/-0.0235

+/-0.0235 0.506

+/-0.0705

+/-0.0705 1.50

+/-0.705

+/-0.705 14.2

+/-1.49

+/- 1.49 U

0.645

+/-0.763

+/-0.763 0.697

+/-0.253

+/-0.253 U

0.0839

+/-0.105

+/-0. 105 5.80

+/-0.571

+/-0.571I 9.36

+/-0.701

+/-0.701I pCi/g 1

pCi/g 15 pCi/g 258 pCi/g 3

pCi/g 6

pCi/g 4

pCi/g 5

pCi/g 11I (0% -20%)

(0% -20%)

(0% -100%)

(0% - 100%)

(0% -20%)

(0%- 100%)

(0%- 100%)

(0% -20%)

LCS Bismuth-2 12 Bismuth-2 14 Cesium-134 Cesium-137 Cobalt-60 Uncert:

TPU:

16.0 Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

6.20 Uncert:

TPU:

9.32 Uncert:

TPU:

pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g 89 (75%-125%)

04/03/07 13:00 94 (75%-125%)

100 (75%-125%)

Page 104 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 8 of 13 Parnmanae Rad Gamma Spec Batch 621149 NOM Sample Qua]

OC Units RPD%

REC%

Range Anist Date Time Europium-I 52 Europium-154 Europium-1I55 Lead-212 Lead-214 M anganese-54 Niobium-94 Potassium-40 Radium-226 Silver-lO8m Thallium-208 QCI 201305347 Actinium-228 Americium-24 I Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncent:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

U ncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

U

-0.176

+/-0.243

+/-0.243 U

0.00147

+/-0.242

+/-0.242 U

0.0771

+/-0.250

+/-0.250 0.907

+/-0. 176

+/-0.176 0.454

+/-0.238

+/-0.238 U

0.0229

+/-0.0932

+/-0.0932 U

-0.0465

+/-0.084

+/-/-0.084 U

0.383

+/-0.835

+/-0.835 0.697

+/-0.253

+/-0.253 U

-0.0512

+/-0.0813

+/-0.0813 0.328

+/-0.152

+/-0.152 U

-0.00165

+/-0.0486

+/-0.0486 U

0.0179

+/-0.0243

+/-0.0243 U

-0.0577

+/-0.110

+/-0.110 U

0.0128

+/-0.0306

+/-0.0306 U

0.00507

+/-0.0126 pCilg pCilg pCi/g pCi/g pCilg pCilg pCilg pCilg pCi/g pCilg pCi/g pCi/g pCilg pCi/g pCilg pCilg (75%-1 25%)

MB 04/03/07 12:57 Bismuth-2 12 Bismuth-2 14 Cesium-I 34 Page 105 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 9 of 13 Parmname NOM Sample Qual QC Units RPD%

REC%

Range Anist Date Time Rad Gamma Spec Batch 621149 TPU:

Cesium-137 Cobalt-60 Europium-152 Europium-154 Europium-155 Lead-21 2 Lead-214 Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

Uncert:

TPU:

+/-0.0126 U

0.00189

+/-0.012

+/-0.012 U

0.00173

+/-0.0135

+/-0.0135 U

0.00881

+/-0.0314

+/-0.0314 U

-0.0162

+/-0.040

+/-0.040 U

0.0195

+/-0.032

+/-0.032 U

-0.0286

+/-0.0274

+/-0.0274 U

-0.0156

+/-0.0217

+/-0.0217 U

0.00042

+/-0.0108

+/-0.0108 U

-0.00626

+/-0.012

+/-0.012 U

0.200

+/-0.186

+/-0.186 U

0.0128

+/-0.0306

+/-0.0306 U

-0.000226

+/-0.0111

+/-0.0111 U

-0.000331

+/-0.0177

+/-0.0177 pCi/g pCi/g pCi/g pCi/g pCilg pCi/g pCi/g pCi/g pCi/g pCilg pCi/g PCi/g pCi/g Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver-108m Thallium-208 Rad Gas Flow Batch 621123 QC1201305274 183245001 DUP Strontium-90 QC120I 305276 LCS Strontium-90 u

-0.01 17 Uncert:

+/-0.0206 TPU:

+/-0.0206 U

-0.00416

+/-0.0137

+/-0.0137 pCi/g 0

(0% -100%)

KSDI 04/03/07 22:32 1.41 1.70 pCi/g 121 (75%-125%)

04/04/07 10:38 Page 106 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 10 of 13 Parmname NOM Sample Qua]

QC Units RPD%

REC%

Range Anist Date Time Rad Gas Flow Batch 621123 QC1201305273 MB Strontium-90 QC1201 305275 183245001 MS Strontium-90 Uncert:

TPU:

Uncert:

TPU:

+/-0. 106

+/-0. 113 U

0.0151

+/-0.0141

+/-0.0141 pCi/g pCilg 04/03/07 22:32 04/03/07 22:31 1.53 U

Uncert:

TPU:

-0.0 117

+/-0.0206

+/-0.0206 1.24

+/-0.103

+/-0.108 81 (75%-125%)

Batch 621125 QC1201305282 183245021 DUP Strontium-90 QCI2OI 305284 LCS Strontium-90 QC1201305281 MB Strontium-90 QC1201305283 183245021 MIS Strontium-90 Rad Liquid Scintillation Batch 621136 QC1201305301 183245006 DUP Iron-S55 u

-0.0124 Uncert:

+/-0.0237 TPU:

+/-0.0237 1.40 Uncert:

TPU:

Uncert:

TPU:

1.41 U

-0.0124 Uncert:

+/-0.0237 TPU:

+/-0.0237 U

0.013

+/-0.0268

+/-0.0268 1.38

+/-0.0937

+/-0.103 U

-0.00552

+/-0.0133

+/-0.0133 1.17

+/-0.127

+/-0.132 pCj/g 0

(0% - 100%) NXL3 pCi/g pCi/g pCi/g 99 (75%-125%)

04/03/07 17:11 04/03/07 17:53 04/03/07 17:11 04/03/07 17:11 83 (75%-125%)

U

-26.4 Uncert:

+/-34.3 TPU:

+/-34.3 U

2.65

+/-34.0

+/-34.0 pCi/g 0

(0% - 100%) VIXPl QC1201305303 LCS Iron-55 QC1201305300 MB Iron-55 1180 Uncert:

TPU:

Uncert:

TPU:

1230 U

Uncert:

TPU:

1130

+/-61.3

+/-98.0 pCi/g 96 (75%-125%)

04/02/07 22:19 04/02/07 22:51 04/02/07 22:02 04/02/07 22:35 U

-26.4 pCi/g

+/-28.2

+/-2 8.2 QC1201305302 183245006 MIS Iron-55

-26.4

+/-34.3

+/-34.3 1180

+/-69.4

+/-110 pCi/g 96 (75%-125%)

Batch 621137 QC1201305305 183245006 DUP Nickel-63 U

-11.2 U

-8.44 pCi/g 0

(0% - 100%) NIXPI 04/02/07 17:27 Page 107 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel~com QC Summary Workorder:

183245 Page 11 of 13 Parmname NOM Sanmle Oual OC Units RPD%

REC%

Range Anist Date Time Rad Liquid Scintillation Batch 621137 QC1201 305307 LCS Nickel-63 QC1201305304 MB Nickel-63 QC1201305306 183245006 MS Nickel-63 Uncert:

TPU:

556 Uncert:

TPU:

Uncert:

TPU:

591 U

Uncert:

TPU:

+/-9.41

+/-9.41 477

+/-25.4

+/-30.6 U

2.75 pCi/g pCi/g pCi/g 86 (75%-125%)

04/02/07 17:59 04/02/07 17:10 04/02/07 17:43

-11.2

+/-9.41

+/-9.41 Batch 621139 QC1201305311 183245006 DUP Technetium-99 QC1201305313 LCS Technetium-99 QC1201305310 MB Technetium-99 QC1201305312 183245006 MIS Technetium-99 u

-0.155 Uncert:

+/-0.229 TPU:

+/-0.229 U

505

+/-27.3

+/-33.0

-0.139

+/-0.236

+/-0.236 16.4

+/-0.466

+/-0.623 85 (75%-125%)

pCi/g 0

(0% - 100%) m4PI 19.6 Uncert:

TPU:

Uncert:

TPU:

20.0 U

Uncert:

TPU:

U

-0.281

+/-0.210

+/-0.210 pCi/g pCi/g pCi/g 84 (75%-125%)

04/03/07 15:56 04/03/07 17:00 04/03/07 15:25 04/05/07 09:59

-0.155

+/-0.229

+/-0.229 15.0

+/-0.676

+/-0.776 75 (75%-125%)

Batch 621141 QC1201305317 183255002 DUP Tritium U

-0.106 Uncert:

+/-1.06 TPU:

+/-1.06 U

0.451

+/-1.03

+/-1.03 pCi/g 0

(0% - 100%) 'XXD2 03/31/07 18:55 QC1201305319 LCS Tritium QC1201305316 MB Tritium 11.7 Uncert:

TPU:

Uncert:

TPU:

11.9 U

Uncert:

TPU:

12.0

+/-1.54

+/-1.55 U

-0.232

+/-0.991

+/-0.991 pCi/g pCi/g pCi/g 102 (75%-125%)

03/31/07 20:57 03/31/07 17:53 03/31/07 19:56 Q01201305318 183255002 MIS Tritium

-0.106

+1-1.06

+/-1.06 13.2

+/- 1.63

+/-1.65 111 (75%-125%)

Batch 621144 Page 108 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 12 of 13 Range Anist Date Time Parmname Rad Liquid Scintillation Batch 621144 NOM

_Sample ua OC Units RPD%

REC%

QC]201305325 183245006 DUP Carbon-14 QC1201305327 LCS Carbon-14 QC1201305324 MB Carbon-14 QC1201305326 183245006 MS Carbon-14 U

0.0236 Uncert:

+/-0.090 TPU:

+/-0.090 U

-0.0 162

+/-0.0934

+/-0.0934 7.02

+/-0.203

+/-0.231 pCi/g 0

(0% - 100%) %\\XD2 04/02/07 15:22 7.09 Uncert:

TPU:

Uncert:

TPU:

U

-0.0233

+/-0.0925

+/-0.0925 pCilg pCilg pCi/g 99 (75%-125%)

04/02/07 17:28 04/02/07 14:19 04/02/07 16:25 7.16 Uncert:

TPU:

U 0.0236

+/-0.090

+/-0.090 6.92

+/-0.202

+/-0.229 97 (75%-125%)

Notes:

The Qualifiers in this report are defined as follows:

Analyte is a surrogate compound Result is less than value reported Result is greater than value reported A

The TIC is a suspected aldol-condensation product B

For General Chemistry and Organic analysis the target analyte was detected in the associated blank.

BD Results are either below the MDC or tracer recovery is low C

Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample H

Analytical holding time was exceeded J

Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the detection limit R

Sample results are rejected U

Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy~-Uncertain identification X

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y

QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h

Preparation or preservation holding time was exceeded Page 109 of 10

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:

183245 Page 13 of 13 Parmname NOM Sample Qual

~QC Units RPD%

REC%

Range Anlst Date Time N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 110 of 110

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD ATTACHMENT 4 (DQA RESULTS)

Revision 0

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD ATTACHMENT 4A (PRELIMINARY DATA REVIEW)

Revision 0

CONTArNMENT SURVEY UNIT 93 12-0001 RELEASE RECORD Survey Unit:

931 2-0001 Area Description RCA Containment Classification 1

Survey Media Surface Soils Type of Survey Final Status Survey Number of Measurements 15 Static, 4 Judgmental, 7 Investigative STATISTICS on TOTAL POPULATION STATISTICS on NON-PARAMETRIC POPULATION Cs-i 37 DCGLOp (pCilg): 4.75E+00 Minimum Value: -2.31 E-02 Maximum Value:

7.99E-02 Mean:

1.41 E-02 Median:

4.70E-03 Standard Deviation: 2.83E-02 Co-60 2.29E+00

-2,38E-02 2.76E-02 5.90E-03 3.97E-03 1.18E-02 Sr-SO 9.30E-01

-3.51 E-02 2.82E-02

-5.08E-03

-3.71 E-03 1.43E-02 DCGLOp (pCilg):

Minimum Value:

Maximum Value:

Mean:

Median:

Standard Deviation:

Cs-i 37 4.75E+00

-2.03E-02 7.99E-02 2.15E-02 1.20E-02 3.28E-02 Co-60 Sr-SO 2.292+00 9.302-01

-4.50E-03 2.57E-02 5.43E-03 2.14E-03 9.40E-03

-3.49E-02 2.82E-02

-3.51 E-03

-7.40E-04 1.44E-02 0.29 7.36E-01 0.10 Cs-i 37 Co-60 Sr-SO GPS Coordinates 11FF 1

Sample ID Result MIDA Result IMDAT Result MDA 2r

[Identified j 2a IIdentified

[ 2ar Identified North East (pcl/g)

______j(PCll)(cl)

(pcl/g)

(pcllg)

(pcllg) 9312-0001 -OO1F 236653.27 668703.89 1.28E-02,0.025 3.26E-02 1.39E-02 0.022 3.47E-02

-1.17E-02 0.021 4.70E-02 931 2-0001-002F 236653.27 668744.35 7.15E-02 0.026 3.70E-02

+

-7.81 E-04 0.020 3.37E-02 1.83E-03 0.021 4.21 E-02 9312-0001-003F 236618.24 668683.67 0 OOE+00 0.045 5.05E-02 2.42E-02 0.035 6.34E-02

-1.77E-02 0.022 4.81 E-02 931 2-0001-004F 236618.24 668724.12 6.82E-02 0.035 3.83E-02

+

4.22E-04 0.020 3.31 E-02

-3.71 E-03 0.022 4.62E-02 931 2-0001-005F 236618.24 668764,58 5.55E-02 0.020 2.29E-02

+

2.14E-03 0.016 2.52E-02

-1.35E-02 0.020 4.34E-02 9312-0001-006F 236618.24 668805.03 4.12E-02 0.017 2.15E-02

+

2.01E-03 0.014 2.32E-02 8.37E-04 0.024 4.75E-02 9312-0001-007F 236583.20 668663.44

-6.43E-03 0.016 2.27E-02

-4.50E-03 0.015 2.39E-02

-4.23E-03 0.023 4.71 E-02 9312-0001-008F 236583.20 668703.89

-2.17E-03 0.014 2.09E-02 2.37E-03 0.013 2.27E-02 2.82E-02 0.029 4.72E-021 931 2-0001-009F 236583.20 668744.35 4.706 03 0.020 2.856 02

-4.23E-03 0.017 2.896 02 2.66E-03 0.026 4.85E-02 931 2-0001-01OF 236583.20 668784.80 7.99E-02 i0.023 2.23E-02

+

3.97E-03 0.014 2.35E-02 7.90E-03 0.026 4.72E-02 :

9312-0001 -O11 F 236583.20 668825.26 12.03E-02 0.019 2.506 02 2.57E-02 0.023 2.616 E02

+

-1.62E-02 0.022 4.906 02 Fraction of DCGL

-0.004 0.017

-0.008 0.011

-0.002 0.0 10

-0.008 0.031 0.002 0.027

-0.010 REVISION 0 Pg f

Page I of`4

CONTAINMENT SURVEY UNIT 93 12-0001 RELEASE RECORD Cs-i 37 Co-60 Sr-90 Sample ID GSCodnts Result 2a MDA Idniid Result 2a MDA Idniid Result 2a MDA Ietfe North East (pCi/g)

(pCi~g)

(pCi/g)

(pCtlg)

(pCtlg)

(pCtig) 9312-0001-012F 236548.17 668683.67 1,202 02 0,012 1.972 02

+

3.94E-03 0.011 1 6 28.402 03 0.021 3.99E-02 9312-0001-013F 236548.17 668724.12 1.38E-02 0.021 2.362 02 2.022-03 0.017 2.84E-02

-7.40E-04 0.022 4.452 02 931 2-0001-014F 236548.17 668764.58

-6.46E-03 0.014 2.04E-02

-1.85E-03 0.013 2.152 02

-3.49E-02 0.025 4.83E-02 9312-0001-015F 236513.14 668744.35

-2.302 03 0.014 2.302 02 1.22E-02 0.013 2.25E-02 i1.67E-04 0.019 3.86E-02 9312-0001-OO3FS 236618.24 668683.67 5.27E-02 0.035 4.02E-02

+

2.382-02 0.034 4.99E-02

-1.60E-02 0.021 4.552 02 9312-0001-016-B 236676.51 668734.75 1.71iE-02 0.018 2.76E-02

-4.65E-04 0.016 2.712 E02

-3.512 E02 0.025 4.902 02 9312-0001-017-B 236622.41 668815.99 5.0lE-04 0.020 3.43E-02 6.58E-03 0.021 3.63E-02 9.10E-03 0.017 2.932 02 9312-0001-018-B 236599.54 668836.44

-4.402 03 0.013 2.132-02 7.10E-03 0.014 2.412 E02

-1.85E-03 0.015 2.85E-02 9312-0001-019-B 236594.08 668662.08

1. 71iE02 0.016 1.74E-02

+

5.30E-03 0.010 1.842-02 1.732-02 0.028 4.77E-02 9312-0001-020-I 236596.22: 668760.32 2,152-03 0.031 4.68E-02 2.762-02 0.028 5.182 02

-1.242-02 0.024 4.852 02 9312-0001-021-I 236591.06: 668772.54 -4.992 03 0.029 4.152 02

-2.38E-02 0.026 3.95E-02 9.412 E03 0.027 4.882 02 9312-0001-022-I 236588.64 668780.33 1.072 02 0.051 9.012-02

-1.59E-02 0.056 9.002 02 1.35E-03 0.026 4.85E-02 9312-0001-023-I 236591.73: 668782.14 -2.312 E02 10.045 7.202 02 7.702-03 0.042 7.092 02

-1.722-02 0.025 4.89E-02 9312-0001-024-I 236593.28 668785.43 6.632-04 0.056 8.202-02 1.672-02 0.047 8.162 02

-1.74E202 0.025 4.87E-02 9312-0001-025-I 236598.60! 668800.13 5.902 03 0.045 6.682-02 1,47E-02 0.034 5.982 02

-1.312-02 0.024 4.952 02 9312-0001-026-I 236600,66: 668803.01

-1.452 02 0.045 7.642 02 8.342-03 0.051 8902-8.582 03 0.019 4320 Fraction of DCGL 0.013 0.003

-0.040 0.005 0.004

-0.034 0.013 0.000 0.025

-0.00 1

-0.001

-0.003

-0.020

-0.011

-0.006

-0.009 REVISION 0 Pg f

Page 2 of4

CONTAINMENT SURVEY UNIT 93 12-0001 RELEASE RECORD OTHER RADIONUCLIDES Sample ID Isotope Reul 2a M

Identified ICLP Fato J(pCI/g) J

_____[(PCi/g)

J_____

(PCi/g) of DCGL 9312-0001 -001F Cs-134 2.07E-02 0.020 3.60E-02

+

2.8E+00 0.007 9312-0001 -001F Eu-155 8,56E-02 0.051 9.66E-02

+

2.4E+02 0.000 9312-0001 -001F Mn-54 1.73E-02 0.017 3.15E-02

+

1.OE+0i 0.002 E u......-......................................

0...07

5.

E........

2.......................0 0 0 0.......

9312-0001-002F Eu-155 8.34E-02 0.076 1.01E-01

+

2.4E+02 0.000 9312-0001-003F Eu-155 9.68E-02 0.0506 1.0E-01

+

2.4E+02 0.000 931 2-0001-004F Eu-i3 55

.603E-02 0,0618 4.5E-02

+

2.8E+00 0.000 9312-0001-007F Am-241 4

8.2E-02 0.041 7.13E-01

+

1.6E+01 0.003 9312-0001-007F Cs-i 34 32.6E-02 0.023 3.02E-02

+

2.8E+00 0.012 9312-0001-007F Eu 155 5.03E-02 0.043 7.15E-02

+

2.4E+02 0.000 9312-0001-008F Eu15 i

5.14.E-02 10.036 6.01E-02

+

2.4E+02 0.000 9312-0001-016-B Eu 155 6.72E-02 0.053 78.24E-02

+

2.4E+02 0.000 9312-0001-017-B Am-241 4.49E-02 0.029 4.04E-02

+

1.6E+01 0.002 9312-0001-018-B Mn 54 3.27E-02 0.016 2.39E-02

+

1O+i 00 931-001-09-BCs 34

.8E-0 006

.2.1E-0

+

2.8E+00 0.007 9312-0001-014-I Eu 155 5.10E-02 01143 1

644E-02

+

24+2 00 9312-0001-0215I Eu 155 4.89E-02 0.084 1.60E-02

+

2.4E+02 0.000 9312-0001-0125I Am241 1.67E-02 0.073 2.1 E-02

+

16+i 00 9312-001 Cs134 8 8E 0 003 119E01

.2 E+01 0.032 9312-0001-016-I Eu 155 1.748E01 0.1532 7.852E01

+

2.4E+02 0.001 931 2-0001-017-I Nb 941 5.60E-02 0.047 8.63E-02

+

1.6E+01 0.012 931 2-0001-018-I Amn241 7.88E-02 0.074 2.39E-02 1.6E+01 0.005 REVISION 0 Pg f

Page 3 of 4

CONTAINMENT SURVEY UNIT 9312-0001 RELEASE RECORD Sample ID Isotope Re I

2cr M

Identified ICLp Fato (pCi/g)

_____j(pCi1g)

(Pcilg) of DCGL 931 2-0001-023-1 Cs-134 7,29E-02 0.062 9.21E-02

+

2.8E+00 0.026 9312-0001-024-1 Cs-134 9.81 E-02 0.084 1.02E-01

+

2.8E+00 0.035 9312-0001-025-1 Cs-i 34 8,54E-02 0.070 9.08E-02

+

2.8E+00 0.031 931 2-0001-026-I Cs-i 34 9.79E-02 0.072 1.04E-01

+

2.8E+00 0.035 931 2-0001-026-1 Mn-54 5.70E-02 0.045 8.59E-02

+

1 OE+01 0.005 REVISION 0Pae4o4 Page 4 of 4

CONTAiNMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD ATTACHMENT 4B (GRAPHICAL REPRESENTATION OF DATA)

Revision 0

FREQUENCY PLOT FOR CESIUM-137 Survey Unit: 9312-0001 Survey Unit Name: RCA - Containment (CTMT)

Mean: 2.15E-02 pCi/g Frequency Plot For Cs-I 37 10 C.)

U-6-

4-2 -

0 I

II

-3.60E-03 1.31E-02 2.98E-02 4.65E-02 6.32E-02 7.99E-02 Upper End Value (pCilg)

Upper End Observation Observation Value Frequency Frequency

-3.60E-03 3

20%

1.3 1E-02 6

40%

2.98E-02 1

7%

4.65E-02 1

7%

6.32E-02 1

7%

7.99E-02 3

20%

Total:

15 100%

I

. WomxoW iA L'

,411%]0-7 S miftedb ~by Date

/4i'--

/ý-a7 Review-ed by/Date 1 of 1

QUANTILE PLOT FOR CESIUM-i137 Survey Unit: 9312-0001 Survey Unit Name: RCA - Containment (CTMT)

Mean: 2.15E-02 pCi/g Quantile Plot For Cs-I 37 l.OQE-0l 8.OOE-02 f-r+-1--1

-- l1---

6. OOE-02 S4. OOE-02 0

'-2.

OOE-02

-2.OOE-02 1~

-I--

U 4--

11 T

I I

IU 0

20 40 60 80 100 Percentage Cs-137 Rank Percentage

-2.03E-02

-6.46E-03

-6.43 E-03

-2.30E-03

-2.1 7E-03 0.OOE+/-00 4.70E-03 1.20E-02 1.28E-02 1.38E-02 4.12E-02 5.55E-02 6.82E-02 7.15E-02 7.99E-02 1

2 3

.4 5

6 7

8 9

10 11 12 13 14 15 3.3%

10.0%

16.7%

23.3%

30.0%

36.7%

43.3%

50.0%

56.7%

63.3%

70.0%

76.7%

83.3%

90.0%

96.7%

~7I~-~v 1111~ 107 S,4mitted bý9 Date Reviewed by/Date

FREQUENCY PLOT FOR COBALT-60 Survey Unit: 93 12-0001 Survey Unit Name: RCA - Containment (CTMT)

Mean: 5.43E-03 pCi/g Frequency Plot For Co-60 10 8-U.

6 -I 4-2-

0-5.33E-04 5.57E-03 1.06E-02 1.56E-02 2.07E-02 2.57E-02 Upper End Value (pCilg)

Upper End Observation Observation Value Frequency Frequency 5.33E-04 4

27%

5.57E-03 7

47%

1.06E-02 0

0%

1.56E-02 2

13%

2.07E-02 0

0%

2.57E-02 2

13%

Total:

15 100%

1411R 10-7 Sý mitted b Date Reviewýe-d by/Date 1o 1 of 1

QUANTILE PLOT FOR COBALT-60 Survey Unit: 93 12-0001 Survey Unit Name: RCA - Containment (CTMTr)

Mean: 5.43E-03 pCi/g Quantile Plot For Co-60 0.

0.

(3 3.00E-02

2. 50E-02 2.00E-02 1.50E-02 1.00E-02 5.00E-03 0.00E+00

-5.00E-03

-1.00E-02 U

Hf U

U U

U U

0 80 100 40 0

20 40 60 80 100 Percentage Co-60 Rank Percentage

-4. 50E-03

-4.23E-03

-1.85E-03

-7.8 1 E-04 4.22E-04 2.01 E-03 2.02E-03 2.14E-03 2.37E-03 3.94E-03 3.97E-03 1.22E-02 1.39E-02 2.42E-02 2.57E-02 1

2 3

.4 5

6 7

8 9

10 11 12 13 14 15 3.3%

10.0%

16.7%

23.3%

30.0%

36.7%

43.3%

50.0%

56.7%

63.3%

70.0%

76.7%

83.3%

90.0%

96.7%

ý1-0.

WO1VO uJ LA VC

~~j~1g J~7 StOý ntte by/Date C-V Revi=~ by/Date

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD ATTACHMENT 4C (SIGN TEST)

Revision 0

Connecticut Yankee Decommissioning Project Health Physics Procedure GPP-GGGR-R5121-001 Attachment B, Rev.CY-OQI MAJOR Sign Test Calculation Sheet for Multiple Radionuclides Survey Area Number:

9312 JSurvey Unit Number:

0001 WPIR #:

N/A Survey Area Name:

Containment (CTMVT)

~Classification:

1 TYPE I (a error):

0.05 N:

15 Radionuclides:

lst Radionuclide 2 nd Radionuclide 3rd Radionuclide 4 th Radionuclide Cs-i 37 Co-60 Sr-90 DCGL:

4.75E+00 2,29E+00 9.30E-01 Results lst Results 2 nd Results 3 Id Results 4 th Weighted Sum 1 -W, Sign Radionuclide Radionuclide Radionuclide Radionuclide (WI)

(pCi/g)

(pCilg)

(pCi/g)

(pCi/g) 1.28E-02 1.39E-02

-1.1 7E-02 0.00 1.00

+___

I___

7.15E-02

-7.81 E-04 1.83E-03 0.02 0.98

+1 0.OOE+00 2.42E-02

-1.77E-02

-0.01 1.01

+1 6.82E-02 4.22E-04

-3.71 E-03

_______0.01 0.99+1 5.55E-02 2.14E-03

-1.35E-02 0.00 1.00

+1 4.12E-02 2.O1 E-03 8.37E-04

________0.01 0.99

+1

-6,43E-03

-4.50E-03

-4.23E-03

-0.01 1.01

+1

-2.17E-03 2.37E-03 2.82E-02 0.03 0.97

+1 ___

4370E-03

-4,23E-03 2.66E-03 0.00 1.00

+1 7.99E-02 3.97E-03 7.90E-03

________0.03 0.97

+1

-2.03E-02 2.57E-02

-1.62E-02

-0.01 1.01

+1 1.20E-02 3.94E-03 8.40E-03 0.01 0.99

+ 1 1.38E-02 2.02E-03

-7.40E-04

________0.00 1.00

+ 1

-6,46E-03

-1.85E-03

-3.49E-02

-0.04 1.04

+ I

-2.30E-03 1.22E-02 1.67E-04

________0.01 0.99

+1 Number of positive differences (S+)l 15 Meets

-the Acceptance Criteria Performed by:

Date:

Date:

4/17/2007 Independent Review by:

Page 1 of I

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD ATTACHMENT 4D (QC SPLIT RESULTS)

Revision 0

Health Physics Procedure 24265-000-G]:'P-CjGCjR-R5124-000-Rev.(,'Y-000 Attachment A 1-Icaith Physics Procedure 24265-000-GPP-GGGR-R5 124-000-Rcv.CY-000 Attachment A Split Sample Assessment Form Survey Area #:

9312 Survey Unit II 0001 Survey Unit Name:

R.CA -Containment (CTMIT)

Sample Plan or WPIR#:

N/A MJ:

9 200-0 Sample D.escription: Comparison of split samples collected from sample measurement location #3 and analyzed using gamma spectroscopy by off-site Vendor L.aboratory. The standard sample was 931l2-0001-003F2, the comparison sample was 9312-000 1-0031'S.

STANDARD COMP~ARISON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable Value Error Range Value Error Ratio (YIN)

K-40 1.5711-4 01 0.620 25 0.75 - t.33 1.57E+01 0.730 1.00 Y

CommentsIL/-UIL Vret' ve~t ons:.

S-.1 I Was2) not Me=tLL n

III >Uient' quantities in the field split results at location 9312-0001-003F to evaluate in accordance with procedure. Evaluation using the reported results tor K-40 resulted in acceptable agreement between the field-split results at these locations.. Since K-40 was found to be present at an acceptable level of agreement, no further action is warranted.

I able' is p[ovided to sho{w accpitance critei used toC assess split samples.

Resolufion 4 -7 8-15 16-50 51-200

>200 Aareuncnt..Mv&.

0

-2,0 0.6 -1.66 0.75 - 1.33 0.80 -1.25 0.85 -1.18 I iate:

Page I of 1

CONTAINMENT (FORMER RADIOLOGICALLY CONTROLLED AREA)

SURVEY UNIT 93 12-0001 RELEASE RECORD ATTACHMENT 4E (COMPASS POWER CURVE)

Revision 0

DQA Surface Soil Report Assessment Summary Siteý Planner(s).

Survey Unit Name&

Report Number:

Survey Unit Samples:

Reference Area Samples:

Test Performed:

Judgmental Samples:

Assessment

Conclusion:

9312 Wojo 9312-0001 1

15 0

Sign Test Result:

Not Performed 0

EMVC Result:

Not Performed Reject Null Hypothesis (Survey Unit PASSES)

Retrospective Power Curve S07 S0.6

-015 S0.6

• 035 0 04 S01 II I

d

.z~Iz_

-~__

-111111

-- 4

~iz~

0ý0 0,2 04 0.6 0.8 1 0 Unity Rule Sum-of-Ratios, including background Prospective Power a

1 -beta Actual Power LBGR Estimated Power DCGL Retrospective Power 12 COMPASS 0l.0.0 41107Pg 4/18/2007 Page 1