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{{#Wiki_filter:October 27, 2016 Mr. John Hickman ltr* OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION Managed by ORAU for DOE U.S. Nuclear Regulatory Commission 11545 Rockville Pike Mailstop T8FS Rockville,IvID 20852 ORISE CONTRACT NO. DE-SC0014664  
{{#Wiki_filter:ltr*     OAK RIDGE INSTITUTE FOR
                                ~~ SCIENCE AND EDUCATION
                                ~ ~      Managed by ORAU for DOE October 27, 2016 Mr. John Hickman U.S. Nuclear Regulatory Commission 11545 Rockville Pike Mailstop T8FS Rockville,IvID 20852 ORISE CONTRACT NO. DE-SC0014664


==SUBJECT:==
==SUBJECT:==
LETTER REPORT FOR ANALYTICAL RESULTS FOR SIX SOIL SAMPLES ASSOCIATED WITH THE HUMBOLDT BAY POWER PLANT IN EUREKA, CALIFORNIA
LETTER REPORT FOR ANALYTICAL RESULTS FOR SIX SOIL SAMPLES ASSOCIATED WITH THE HUMBOLDT BAY POWER PLANT IN EUREKA, CALIFORNIA
[TAC NO. J00338] [DOCKET NO. 50-133](RFTA NO. 16-001) DCN: 5201-LR-04-0  
[TAC NO. J00338] [DOCKET NO. 50-133](RFTA NO. 16-001)
DCN: 5201-LR-04-0


==Dear Mr. Hickman:==
==Dear Mr. Hickman:==
Oak Ridge Institute for Science and Education (ORISE) received SL'i: soil samples on September 14, 2016 from the Humboldt Bay Power Plant in Eureka, Califomia.
ORISE is managed by Oak Ridge Associated Universities(ORAU) under DOE contract number DE-SC0014664.
The samples were shipped to the laboratory from the licenssee's laboratory.
The samples were received in good condition.
Per the chain of custody, the samples were analyzed for gamma emitting isotopes by gamma spectrometry.
In addition, per your request, the samples were analyzed for tritium by liquid scintillation counting.
The analytical data, along with the procedure references, are presented in the attached reports. Quality Control (QC) requirements were met for these analyses.
The QC files are available for your review upon request. Please feel free to contact me at 865.576.9184 or Forrest Smith at 865.574.9802 with any questions or comments. *Ir Ivey Laboratory Manager ORAU WPI:\'<!FS:km:lw Enclosures Electronic distribution:
T. Carter, NRC S. Roberts, ORAU E. Bailey, ORAU D. Hagemeyer, ORAU File code: 5201; Lab code: 12372 P.O. Box 117 Oak Ridge, TN 37831
* www.orau.org T. Vitkus, ORAU 
''j OAK RIDGE INSTITUTE FOR AND EDUCATION Managed by ORAU for DOE Project#:
201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 coc #: 1609-008 Analyst: smithw Client Sample ID: FSS-0757:
OOL02-01-002-F Lab Sample ID: 1237280001 Detector ID: DET07 Count Date: 912812016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 105.31 K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (< MDC) TPU = Total Propagated Uncertainty
-0.082 -0.001 -0.002 0.026 0.128 0.003 -0.07 0.033 11.9 0.025 -0.015 1.40 -0.150 MDC= Minimum Detectable Concentration Smp Qty.: 646.98 Live Time(s): 3,600 Receipt Date: 911412016 0.045 0.102 0.013 0.031 0.026 0.054 0.027 0.066 0.027 0.034 0.054 0.124 0.11 0.25 0.043 0.110 1.1 0.5 0.018 0.038 0.022 0.050 0.44 0.63 0.089 0.136 Units: grams Geometry:
LM SOP (Rev.#): CP1 (20) Collection Date: 8130/2016 pCi/g u NIA pCilg u NIA pCilg u NIA pCilg u NIA pCilg 661.71 NIA pCilg u NIA pCi/g u NIA pCilg u NIA pCilg 1461.09 NIA pCilg 835.96 u NIA pCi/g u NIA pCilg 63.22 NIA pCilg u NIA NIA N/A NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 1of8 l1fj OAK RIDGE INSTITUTE FOR II SCIENCE AND EDUCATION I Managed by ORAU for DOE Project#:
201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 coc #: 1609-008 Analyst:'
smithw Client Sample ID: FSS-0765:
OOL02-01-010-F Lab Sample ID: 1237280002 Detector ID: DET08 Count Date: 912812016 SDG: 201212372-1 Am-241 59.54 -0.143 Co-57 122.06 -0.001 Co-60 1332.49 -0.015 Cs-134 795.86 0.049 Cs-137 661.66 0.056 Eu-152 344.28 -0.028 Eu-154 723.30 -0.129 Eu-155 105.31 0.007 K-40 1460.82 15.3 Mn-54 834.85 0.010 Se-75 264.66 -0.010 U-238 by Th-234. 63.29 2.80 Zn-65 1115.54 -0.079 Qualifier Flags: U = Analyte not detected(<
MDC) TPU = Total Propagated Uncertainty MDC = Minimum Detectable Concentration Smp Qty.: 502.55 Live Time(s): 3,600 Receipt Date: 911412016 0.050 0.104 0.012 0.029 0.027 0.050 0.026 0.064 0.018 0.031 0.049 0.106 0.071 0.203 0.051 0.12Q 1.3 0.7 0.018 0.050 0.025 0.054 0.73 0.75 0.061 0.113 Units: grams Geometry:
LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCilg u NIA pCilg u NIA pCilg u NIA pCilg u NIA pCi/g 661.65 NIA pCilg u NIA pCi/g u NIA pCilg u NIA pCilg 1461.05 NIA pCilg u NIA pCilg u NIA pCilg 63.25 NIA pCilg u NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 2 of 8 l1rj OAK RIDGE INSTITUTE FOR AND EDUCATION Managed by ORAU for DOE Project#:
201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 ----------
-----Gamma Spectrometry Summary Sheet Further: Toget11er Report Date: October24, 2016, coc #: 1609-008 Analyst: smithw .Client Sample ID: FSS-0779:
OOL02-01-024-F Lab Sample ID: 1237250003 Detector ID: DET09 Count Date: 912812016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 . Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 .105.31 K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (< MDC)
* TPU = Total Propagated Uncertainty
-0.080 0.001 -0.003 -0.006 0.464 -0.024 -0.15 0.054 13.4 0.002 -0.008 2.06 -0.091 MDC = Minimum Detectable Concentration Smp Qty.: 523.29 Live Time(s): 3,600 Receipt Date: 911412016 0.043 0.097 0.013 0.031 0.025 0.049 0.014 0.063 0.055 0.034 0.044 0.100 0.11 0.22 0.032 0.069 1.2 0.5 0.024 0.053 0.024 0.057 0.58 0.69 0.078 0.139 Units: grams Geometry:
LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCilg u NIA NIA pCilg u NIA NIA pCilg u NIA N/A pCilg u NIA NIA pCilg 661.74 NIA NIA pCi/g u NIA N/A pCi/g u NIA NIA pCilg 104.93 u NIA NIA pCilg 1461.14 NIA NIA pCi/g u NIA NIA pCi/g u NIA NIA pCi/g 63.19 NIA NIA pCi/g u NIA NIA Page 3 of 8 
, fj OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION Managed by ORAU for DOE Project#:
201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 coc # : 1609-008 Analyst: smithw Client Sample ID: FSS-0782:
OOL02-01-027-F Lab Sample ID: 1237280004 Detector ID: DET10 *count Date: 912812016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154
* 723.30 Eu-155 105.31 K-40 1460.82 Mn-54 834.85" Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (< MDC) TPU = Total Propagated Uncertainty
-0.025 0.0084 -0.013 0.039 0.044 0.023 -0.133 0.037 11.1 -0.016 -0.004 0.99 -0.095 MDC = Minimum Detectable Concentration Smp Qty.: 745.59 Live Time(s): 3,600 Receipt Date: 911412016 0.087 0.212 0.0100 0.0234 0.021 0.039 0.022 0.055 0.017 0.035 0.042 0.102 0.095 0.175 0.052 0.133 1.0 0.6 0.020 0.038 0.021 0.049 0.58 1.21 0.060 0.101 Units: grams Geometry:
LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCilg u NIA pCilg 121.30 u NIA pCilg u NIA pCilg u NIA pCilg 661.97 NIA pCilg u NIA pCilg u NIA pCilg u NIA pCilg 1460.60 NIA pCilg u NIA pCi/g u NIA pCi/g 63.55 u NIA pCilg u NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 4 of 8 l1fj OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION E I Managed by ORAU for DOE Project#:
201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 coc # : 1609-008 Analyst: smithw Client Sample ID: FSS-0783:
OOL02-01-028-F Lab Sample ID: 1237250005 Detector ID: DET07 Count Date: 913012016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 105.31 K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (< MDC) TPU = Total Propagated Uncertainty 0.009 0.009 -0.014 0.025 0.218 -0.045 -0.23 0.059 15.2 -0.002 -0.006 0.66 -0.170 MDC = Minimum Detectable Concentration Smp Qty.: 628.05 Live Time(s): 3,600 Receipt Date: 911412016 0.036 0.112 0.014 0.034 0.031 0.060 0.031 0.074 0.036 0.041 0.064 0.136 0.15 0.25 0.047 0.122 1.4 0.6 0.027 0.058 0.026 0.062 0.36 0.73 0.089 0.153 Units: grams Geometry:
LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCi/g u NIA pCilg u NIA pCilg u NIA pCilg u NIA pCilg 661.74 NIA pCi/g u NIA pCilg u NIA pCilg
* u NIA pCilg 1461.00 NIA pCilg u NIA pCilg u NIA pCilg 63.39 u NIA pCilg u NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 5 of 8 J 
, Jj OAK RIDGE INSTITUTE FOR 11 SCIENCE AND EDUCATION Managed by ORAU for DOE Project#:
201212372 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Gamma Spectrometry Summary Sheet Furt11e1:
Together Report Date: October 24, 2016 coc # : 1609-008 Analyst: smithw Client Sample ID: FSS-0787:
OOL02-01-032-F Lab Sample ID: 1237280006 Detector ID: DET07 Count Date: 912812016 SDG: 201212372-1 Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 '795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 105.31 K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Qualifier Flags: U = Analyte not detected (<MDC) TPU = Total Propagated Uncertainty
-0.045 0.0085 0.017 0.002 0.478 0.024 -0.18 -0.018 12.3 0.006 -0.009 0.70 -0.133 MDC= Minimum Detectable Concentration Smp Qty.: 655.82 Live Time(s): 3,600 Receipt Date: 911412016 0.046 0.107 0.0097 0.0227 0.027 0.063 0.031 0.065 0.054 0.040 0.054 0.134 0.13 0.25 0.043 0.106 1.2 0.6 0.027 0.059 0.025 0.057 0.35 0.69 0.085 0.148 Units: grams Geometry:
LM SOP (Rev.#): CP1 (20) Collection Date: 813012016 pCilg u NIA pCilg 123.06 u NIA pCilg u NIA pCilg u NIA pCilg 661.88 NIA pCilg u NIA pCilg u NIA pCilg u NIA pCilg 1461.00 NIA pCilg u NIA pCilg u NIA pCilg 63.26 NIA pCilg u NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA NIA Page 6 of 8 l1fj OAK RIDGE INSTITUTE FOR AND EDUCATION Managed by ORAU for DOE Project#:
Project Name: Batch Number: GS0351 Client Sample ID: Lab Sample ID: BLK0351S Detector ID: DET09 Count Date: 912812016 SDG: Am-241 59.54 -1.7 Co-57 122.06 -0.9 Co-60 1332.49 -1.8 Cs-134 795.86 -1.7 Cs-137 661.66 5.1 Eu-152 344.28 3 Eu-154 723.30 . -14 Eu-155 105.31 12 K-40 1460.82 -11 Mn-54 834.85 -2.5 Se-75 264.66 -2.4 U-238 by Th-234 63.29 -27 Zn-65 1115.54 -8 Qualifier Flags: U = Analyte not detected (< MDC) TPU = Total Propagated Une;ertainty MDC= Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: October 24, 2016 COC#: Analyst: smithw Smp Qty.: 1.00 Live Time(s): 3,600 Receipt Date: 911412016 7.7 19.6 3.3 7.9 6.9 14.8 6.2 14.1 6.4 17.0 14 35 30 66 11 30 84 226 6.3 12.5 6.1 14.1 59 158 15 28 Units:* sample SOP (Rev.#): CP1 (20) Collection Date: pCilsample pCilsample pCi/sample pCilsample pCi/sample pCilsample pCilsample pCilsample pCilsample 1461.09 pCilsample pCilsample


pCi/sample 63.48 pCilsample Further. Together Geometry:
Oak Ridge Institute for Science and Education (ORISE) received SL'i: soil samples on September 14, 2016 from the Humboldt Bay Power Plant in Eureka, Califomia. ORISE is managed by Oak Ridge Associated Universities(ORAU) under DOE contract number DE-SC0014664. The samples were shipped to the laboratory from the licenssee's laboratory. The samples were received in good condition. Per the chain of custody, the samples were analyzed for gamma emitting isotopes by gamma spectrometry. In addition, per your request, the samples were analyzed for tritium by liquid scintillation counting. The analytical data, along with the procedure references, are presented in the attached reports.
LM u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA NIA u .NIA NIA u NIA NIA u NIA NIA Page 7 of 8 l1fj OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION I Managed by ORAU for DOE Project#:
Quality Control (QC) requirements were met for these analyses. The QC files are available for your review upon request.
Project Name: Batch Number: GS0351 Client Sample ID: Lab Sample ID: LCS0351S Detector ID: DET08 Count Date: 912812016 SDG: Am-241 59.54 Co-57 122.06 Co-60 1332.49 Cs-134 795.86 Cs-137 661.66 Eu-152 344.28 Eu-154 723.30 Eu-155 105.31 .K-40 1460.82 Mn-54 834.85 Se-75 264.66 U-238 by Th-234 63.29 Zn-65 1115.54 Electronically Validated By: Roxanne Nagle-10/512016 09:23 Electronically Approved By:
Please feel free to contact me at 865.576.9184 or Forrest Smith at 865.574.9802 with any questions or comments.
Yr Wade Ivey 10/2412016 13:01 Qualifier Flags: U = Analyte not detected(<
S~cerely,       ~    *Ir \J>&#xb5;;~'(-
MDC) TPU = Total Propagated Uncertainty 9.04 2.96 5.62 0.07 3.73 ' 0.051 -0.13 0.122 0.14 -0.57 35 -14.6 -0.1 MDC= Minimum Detectable Concentration Gamma Spectrometry Summary Sheet Report Date: October24, 2016 COC#: Analyst: smithw Smp Qty.: 514.39 Live Time(s): 3,600 Receipt Date: 911412016 0.27 0.12 0.35 0.59 0.25 0.12 0.14 *0.29 0.25 0.07 0.089 0.202 0.20 0.40 0.097 0.234 0.20 0.47 0.66 1.26 35 81 3.5 1.0 3.1 7.1 Units: grams SOP (Rev.#): CP1 (20) Collection Date: pCilg 59.45 pCilg 121.95 pCilg 1332.69 pCilg* pCilg 661.67 pCilg pCilg pCilg pCilg 1461.21 pCilg pCi/g. 263.79 pCi/g pCilg Further. Togetl1er Geometry:
  ~ '6,L~
250LM NIA 0.96 NIA N/A NIA NIA u NIA NIA NIA 0.95 u NIA NIA u NIA NIA u NIA NIA u NIA NIA u NIA N/A u NIA N/A u NIA N/A u N/A N/A Page 8 of 8 Liquid Scintillation Analysis Summary Results by Analyte \1rl. OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION Managed by ORAU for DOE Analyte: H-3 Project Name:: Humboldt Bay PP 09-2016 Project#:
~Je Ivey Laboratory Manager ORAU WPI:\'<!FS:km:lw Enclosures Electronic distribution: T. Carter, NRC            S. Roberts, ORAU                  T. Vitkus, ORAU E. Bailey, ORAU          D. Hagemeyer, ORAU File code: 5201; Lab code: 12372 P.O. Box 117 Oak Ridge, TN 37831
201212372 SOP (Rev.#): AP6 (21) SDG #: 201212372-1
* www.orau.org
*ro_.-:1c.*//*u.::-r Report Date: 10/11/2016
*----*_, .,-. :;
* ' * *, * * * -** ... ...
FSS-0757:00L02-01-002-F FS5-0765:00L02-01-010-F . F55-0765:00L02-01-010-F


F55-0779:00L02-01-024-F FS5-0782:00L02-01-027-F F55-0783:00L02-01-028-F F55-0787:00L02-01-032-F 1237250001
      'j OAK RIDGE INSTITUTE FOR
  ~ ~ Managed by ORAU for DOE
  ~~SCIENCE AND EDUCATION                              Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016
  'Project#: 201212372                          coc #:    1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351                          Analyst: smithw Client Sample ID: FSS-0757: OOL02-01-002-F Lab Sample ID: 1237280001                    Smp Qty.: 646.98                    Units: grams            Geometry: LM Detector ID: DET07                            Live Time(s): 3,600                SOP (Rev.#): CP1 (20)
Count Date:      912812016                    Receipt Date:  911412016          Collection Date:  8130/2016 SDG:      201212372-1 Am-241                  59.54              -0.082      0.045          0.102            pCi/g                    u          NIA          NIA Co-57                  122.06            -0.001      0.013          0.031            pCilg                    u          NIA          N/A Co-60                  1332.49            -0.002      0.026          0.054            pCilg                    u          NIA          NIA Cs-134                  795.86              0.026      0.027          0.066            pCilg                    u          NIA          NIA Cs-137                  661.66              0.128      0.027           0.034            pCilg    661.71                      NIA          NIA Eu-152                  344.28              0.003      0.054          0.124            pCilg                    u          NIA          NIA Eu-154                  723.30              -0.07        0.11            0.25            pCi/g                    u          NIA          NIA Eu-155                  105.31              0.033      0.043          0.110            pCilg                    u          NIA          NIA K-40                    1460.82              11.9        1.1            0.5            pCilg    1461.09                    NIA          NIA Mn-54                  834.85              0.025      0.018          0.038            pCilg    835.96          u          NIA          NIA Se-75                  264.66            -0.015      0.022          0.050            pCi/g                    u          NIA          NIA U-238 by Th-234        63.29                1.40        0.44            0.63            pCilg    63.22                      NIA          NIA Zn-65                  1115.54            -0.150      0.089          0.136            pCilg                    u          NIA          NIA Qualifier Flags:
U = Analyte not detected (< MDC)                                                                                                            Page 1of8 TPU =      Total Propagated Uncertainty MDC=        Minimum Detectable Concentration


1237250002 12372S0002Dup 1237250003 1237250004 1237250005 1237250006 Validated By: Date: Approved By: tr/ l/i.#W j? J.1 0 L Date: I 0 / J 'I J) b I / Qualifier Flags: U= Analyte not detected (<MDC) TPU= Total Propagated Uncertainty MDC= Minimum Detectable Concentration 0.6 -0.9 0.2 -1.4 -0.9 0.2 -0.5 3.4 5.9 pCi/g u HB0362 2.9 5.2 pCi/g u HB0362 2.8 4.9 pCi/g u HB0362 2.1 3.8 pCi/g u HB0362 2.7 4.8 pCi/g u HB0362 2.9 5.0 pCi/g u HB0362 2.6 4.6 pCi/g u HB0362 Page 1 of 1}}
l1fj OAK RIDGE INSTITUTE FOR II        SCIENCE AND EDUCATION
  ~ I Managed by ORAU for DOE Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 Project#: 201212372                          coc #:    1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351                          Analyst:' smithw Client Sample ID: FSS-0765: OOL02-01-010-F Lab Sample ID: 1237280002                    Smp Qty.: 502.55                  Units: grams              Geometry: LM Detector ID: DET08                            Live Time(s): 3,600                SOP (Rev.#): CP1 (20)
Count Date:      912812016                    Receipt Date:  911412016          Collection Date:  813012016 SDG:      201212372-1 Am-241                  59.54              -0.143      0.050          0.104            pCilg                    u          NIA          NIA Co-57                  122.06            -0.001      0.012          0.029            pCilg                    u          NIA          NIA Co-60                  1332.49            -0.015      0.027          0.050            pCilg                    u          NIA          NIA Cs-134                  795.86            0.049        0.026          0.064            pCilg                    u          NIA          NIA Cs-137                  661.66            0.056        0.018          0.031            pCi/g    661.65                      NIA          NIA Eu-152                  344.28            -0.028      0.049          0.106            pCilg                    u          NIA          NIA Eu-154                  723.30            -0.129      0.071          0.203            pCi/g                    u          NIA          NIA Eu-155                  105.31              0.007      0.051          0.12Q            pCilg                    u          NIA          NIA K-40                    1460.82              15.3        1.3            0.7            pCilg    1461.05                    NIA          NIA Mn-54                  834.85              0.010      0.018          0.050            pCilg                    u          NIA          NIA Se-75                  264.66            -0.010      0.025          0.054            pCilg                    u          NIA          NIA U-238 by Th-234.        63.29              2.80        0.73            0.75            pCilg    63.25                      NIA          NIA Zn-65                  1115.54            -0.079      0.061          0.113            pCilg                    u          NIA          NIA Qualifier Flags:
U =  Analyte not detected(< MDC)                                                                                                            Page 2 of 8 TPU  =      Total Propagated Uncertainty MDC  =    Minimum Detectable Concentration
 
l1rj OAK RIDGE INSTITUTE FOR
    ~~
    ~~SCIENCE AND EDUCATION Managed by ORAU for DOE Gamma Spectrometry Summary Sheet Further: Toget11er Report Date: October24, 2016, Project#: 201212372                            coc #:    1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351                          Analyst: smithw
    .Client Sample ID: FSS-0779: OOL02-01-024-F Lab Sample ID: 1237250003                     Smp Qty.: 523.29                  Units: grams              Geometry: LM Detector ID: DET09                            Live Time(s): 3,600                SOP (Rev.#): CP1 (20)
Count Date:      912812016                    Receipt Date:   911412016          Collection Date:   813012016 SDG:     201212372-1 Am-241                  59.54              -0.080        0.043          0.097            pCilg                      u          NIA          NIA Co-57                  122.06              0.001        0.013          0.031            pCilg                      u          NIA          NIA
. Co-60                  1332.49            -0.003      0.025          0.049            pCilg                      u          NIA          N/A Cs-134                  795.86              -0.006      0.014          0.063            pCilg                      u          NIA          NIA Cs-137                  661.66              0.464        0.055          0.034            pCilg    661.74                      NIA          NIA Eu-152                  344.28              -0.024      0.044            0.100          pCi/g                      u          NIA          N/A Eu-154                  723.30              -0.15        0.11            0.22          pCi/g                      u          NIA          NIA Eu-155                  .105.31            0.054        0.032            0.069          pCilg      104.93          u          NIA          NIA K-40                    1460.82              13.4        1.2              0.5          pCilg      1461.14                    NIA          NIA Mn-54                  834.85              0.002      0.024          0.053            pCi/g                      u          NIA          NIA Se-75                  264.66              -0.008      0.024            0.057          pCi/g                      u          NIA          NIA U-238 by Th-234        63.29                2.06        0.58            0.69          pCi/g      63.19                      NIA          NIA Zn-65                  1115.54            -0.091      0.078            0.139          pCi/g                      u          NIA          NIA Qualifier Flags:
U =  Analyte not detected (< MDC)
* Page 3 of 8 TPU  =      Total Propagated Uncertainty MDC  =      Minimum Detectable Concentration
 
  ,~I fj OAK RIDGE INSTITUTE FOR
  ~ ~ Managed by ORAU for DOE SCIENCE AND EDUCATION                      Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 Project#: 201212372                          coc # :  1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351                          Analyst: smithw Client Sample ID: FSS-0782: OOL02-01-027-F Lab Sample ID: 1237280004                    Smp Qty.: 745.59                  Units: grams              Geometry: LM Detector ID: DET10                            Live Time(s): 3,600                SOP (Rev.#): CP1 (20)
    *count Date:    912812016                    Receipt Date:  911412016          Collection Date: 813012016 SDG:      201212372-1 Am-241                  59.54            -0.025      0.087          0.212            pCilg                    u          NIA          NIA Co-57                    122.06          0.0084      0.0100          0.0234            pCilg    121.30          u          NIA          NIA Co-60                    1332.49          -0.013      0.021            0.039            pCilg                    u          NIA          NIA Cs-134                  795.86            0.039      0.022            0.055            pCilg                    u          NIA          NIA Cs-137                  661.66            0.044      0.017            0.035            pCilg    661.97                      NIA          NIA Eu-152                  344.28            0.023      0.042            0.102            pCilg                    u          NIA          NIA Eu-154
* 723.30            -0.133      0.095            0.175            pCilg                    u          NIA          NIA Eu-155                  105.31            0.037      0.052            0.133            pCilg                    u          NIA          NIA K-40                    1460.82            11.1        1.0              0.6            pCilg    1460.60                    NIA          NIA Mn-54                    834.85"          -0.016      0.020            0.038            pCilg                    u          NIA          NIA Se-75                    264.66            -0.004      0.021            0.049            pCi/g                    u          NIA          NIA U-238 by Th-234          63.29              0.99        0.58            1.21            pCi/g    63.55          u          NIA          NIA Zn-65                    1115.54          -0.095      0.060            0.101            pCilg                    u          NIA          NIA Qualifier Flags:
U =  Analyte not detected (< MDC)                                                                                                          Page 4 of 8 TPU  =      Total Propagated Uncertainty MDC  =    Minimum Detectable Concentration
 
l1fj OAK RIDGE INSTITUTE FOR
  ~I SCIENCE AND EDUCATION                              Gamma Spectrometry Summary Sheet EI        Managed by ORAU for DOE                                                                                      Further. Together Report Date: October 24, 2016 Project#: 201212372                          coc # :  1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351                          Analyst: smithw Client Sample ID: FSS-0783: OOL02-01-028-F Lab Sample ID: 1237250005                    Smp Qty.: 628.05                  Units: grams              Geometry: LM Detector ID: DET07                            Live Time(s): 3,600                SOP (Rev.#): CP1 (20)
Count Date:      913012016                    Receipt Date:  911412016          Collection Date:  813012016 SDG:      201212372-1 Am-241                  59.54              0.009      0.036          0.112            pCi/g                    u          NIA          NIA Co-57                  122.06              0.009      0.014          0.034            pCilg                    u          NIA          NIA Co-60                  1332.49            -0.014      0.031          0.060            pCilg                    u          NIA          NIA Cs-134                  795.86              0.025      0.031          0.074            pCilg                    u          NIA          NIA Cs-137                  661.66              0.218      0.036          0.041            pCilg    661.74                      NIA          NIA Eu-152                  344.28            -0.045      0.064          0.136            pCi/g                    u          NIA          NIA Eu-154                  723.30              -0.23        0.15            0.25            pCilg                    u          NIA          NIA Eu-155                  105.31              0.059      0.047          0.122            pCilg
* u          NIA          NIA K-40                    1460.82              15.2        1.4            0.6            pCilg    1461.00                    NIA          NIA Mn-54                  834.85            -0.002      0.027          0.058            pCilg                    u          NIA          NIA Se-75                  264.66            -0.006      0.026          0.062            pCilg                    u          NIA          NIA U-238 by Th-234        63.29                0.66        0.36            0.73            pCilg    63.39          u          NIA          NIA Zn-65                  1115.54            -0.170      0.089          0.153            pCilg                    u          NIA          NIA Qualifier Flags:
U = Analyte not detected (< MDC)                                                                                                             Page 5 of 8 TPU =     Total Propagated Uncertainty MDC =     Minimum Detectable Concentration
 
  , Jj OAK 11 RIDGE INSTITUTE FOR
  ~ ~ Managed by ORAU for DOE SCIENCE AND EDUCATION                      Gamma Spectrometry Summary Sheet Furt11e1: Together Report Date: October 24, 2016 Project#: 201212372                          coc # :  1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351                          Analyst: smithw Client Sample ID: FSS-0787: OOL02-01-032-F Lab Sample ID: 1237280006                    Smp Qty.: 655.82                    Units: grams            Geometry: LM Detector ID: DET07                            Live Time(s): 3,600                SOP (Rev.#): CP1 (20)
Count Date:      912812016                    Receipt Date:  911412016          Collection Date:  813012016 SDG:      201212372-1 Am-241                  59.54              -0.045      0.046            0.107            pCilg                    u            NIA          NIA Co-57                  122.06            0.0085      0.0097          0.0227            pCilg    123.06          u            NIA          NIA Co-60                  1332.49            0.017      0.027            0.063            pCilg                    u            NIA          NIA Cs-134                '795.86              0.002      0.031            0.065            pCilg                    u            NIA          NIA Cs-137                  661.66              0.478      0.054            0.040            pCilg    661.88                      NIA          NIA Eu-152                  344.28              0.024      0.054            0.134            pCilg                    u            NIA          NIA Eu-154                  723.30              -0.18        0.13            0.25            pCilg                    u            NIA          NIA Eu-155                  105.31            -0.018      0.043            0.106            pCilg                    u            NIA          NIA K-40                    1460.82              12.3        1.2              0.6            pCilg      1461.00                    NIA          NIA Mn-54                  834.85              0.006      0.027            0.059            pCilg                    u            NIA          NIA Se-75                  264.66            -0.009      0.025            0.057            pCilg                    u            NIA          NIA U-238 by Th-234        63.29                0.70        0.35            0.69            pCilg    63.26                        NIA          NIA Zn-65                    1115.54          -0.133      0.085            0.148            pCilg                    u            NIA          NIA Qualifier Flags:
U = Analyte not detected (<MDC)                                                                                                              Page 6 of 8 TPU =      Total Propagated Uncertainty MDC=        Minimum Detectable Concentration
 
l1fj OAK RIDGE INSTITUTE FOR
  ~~
  ~~SCIENCE AND EDUCATION Managed by ORAU for DOE Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 Project#:                                    COC#:
Project Name:
Batch Number: GS0351                        Analyst: smithw Client Sample ID:
Lab Sample ID: BLK0351S                      Smp Qty.: 1.00                    Units:* sample        Geometry: LM Detector ID: DET09                          Live Time(s): 3,600                SOP (Rev.#): CP1 (20)
Count Date:      912812016                  Receipt Date:  911412016          Collection Date:
SDG:
Am-241                  59.54              -1.7        7.7            19.6         pCilsample                u            NIA        NIA Co-57                  122.06              -0.9       3.3            7.9          pCilsample                u            NIA        NIA Co-60                  1332.49            -1.8        6.9            14.8          pCi/sample                u            NIA        NIA Cs-134                  795.86              -1.7        6.2            14.1          pCilsample                u            NIA        NIA Cs-137                  661.66              5.1        6.4            17.0         pCi/sample                u            NIA        NIA Eu-152                  344.28                3          14              35          pCilsample                u            NIA        NIA Eu-154                  723.30 .            -14        30              66          pCilsample                u            NIA        NIA Eu-155                  105.31                12        11              30          pCilsample                u            NIA        NIA K-40                    1460.82              -11        84            226          pCilsample  1461.09      u            NIA        NIA Mn-54                  834.85              -2.5        6.3            12.5          pCilsample                u            NIA        NIA Se-75                  264.66              -2.4        6.1            14.1         pCilsample                u          .NIA        NIA U-238 by Th-234        63.29                -27        59            158          pCi/sample  63.48        u            NIA        NIA Zn-65                  1115.54              -8        15              28          pCilsample                u            NIA        NIA Qualifier Flags:
U = Analyte not detected (< MDC)                                                                                                        Page 7 of 8 TPU =      Total Propagated Une;ertainty MDC=        Minimum Detectable Concentration
 
l1fj OAK RIDGE INSTITUTE FOR
    ~I SCIENCE AND EDUCATION                              Gamma Spectrometry Summary Sheet I  ~ Managed by ORAU for DOE                                                                                      Further. Togetl1er Report Date: October24, 2016 Project#:                                    COC#:
Project Name:
Batch Number: GS0351                        Analyst: smithw Client Sample ID:
Lab Sample ID: LCS0351S                      Smp Qty.: 514.39                  Units: grams          Geometry: 250LM Detector ID: DET08                          Live Time(s): 3,600                SOP (Rev.#): CP1 (20)
Count Date:      912812016                  Receipt Date:  911412016          Collection Date:
SDG:
Am-241                  59.54              9.04        0.27            0.12            pCilg    59.45                    NIA          0.96 Co-57                    122.06              2.96        0.35            0.59            pCilg    121.95                  NIA          N/A Co-60                    1332.49            5.62        0.25            0.12            pCilg    1332.69                  NIA          NIA Cs-134                  795.86            0.07        0.14          *0.29            pCilg*                u          NIA          NIA Cs-137                  661.66              3.73        0.25            0.07            pCilg    661.67                  NIA          0.95 Eu-152                  344.28          ' 0.051      0.089          0.202            pCilg                  u          NIA          NIA Eu-154                  723.30            -0.13        0.20            0.40            pCilg                  u          NIA          NIA Eu-155                  105.31            0.122      0.097          0.234            pCilg                  u          NIA          NIA
.K-40                    1460.82            0.14        0.20            0.47            pCilg    1461.21      u          NIA          NIA Mn-54                    834.85            -0.57        0.66            1.26            pCilg                  u          NIA          N/A Se-75                    264.66              35          35              81            pCi/g. 263.79      u          NIA          N/A U-238 by Th-234          63.29              -14.6        3.5             1.0            pCi/g                  u          NIA          N/A Zn-65                    1115.54            -0.1        3.1            7.1            pCilg                  u          N/A          N/A Electronically Validated By:
Roxanne Nagle- 10/512016 09:23 Electronically Approved By:
  &#xb5;;~fl Yr Wade Ivey 10/2412016 13:01 Qualifier Flags:
U = Analyte not detected(< MDC)                                                                                                          Page 8 of 8 TPU =      Total Propagated Uncertainty MDC=        Minimum Detectable Concentration
 
Liquid Scintillation Analysis Summary Results by Analyte
    \1rl. OAK RIDGE INSTITUTE FOR
    ~~ SCIENCE AND EDUCATION
    ~ ~ Managed by ORAU for DOE
                                                                                                            <=>~t=1Jrt''<-~r. *ro_.-:1c.*//*u.::-r Analyte: H-3                                          SOP (Rev.#): AP6 (21)            Report Date:                  10/11/2016 Project Name:: Humboldt Bay PP 09-2016 Project#: 201212372                                        SDG #: 201212372-1
                                                                                  *'          *                                  *,                * ** '~
                            -~
*_,  ~-.                      .,- .:;
                                      -~::':.'.~~~~:~~.'~'.~~ ~~N':::'f.**:;:**'.
    ... :cri~n_t,$.i!rfi:R!i:ib~      -                * * ***>+/--~--<*.~-~                              ~    ~                                  ~@ ...
FSS-0757:00L02-01-002-F                    1237250001                0.6          3.4       5.9     pCi/g           u                       HB0362 FS5-0765:00L02-01-010-F .                  1237250002              -0.9          2.9       5.2     pCi/g           u                       HB0362 F55-0765:00L02-01-010-F                  12372S0002Dup              0.2          2.8       4.9     pCi/g           u                       HB0362 F55-0779:00L02-01-024-F                    1237250003              -1.4          2.1       3.8     pCi/g           u                       HB0362 FS5-0782:00L02-01-027-F                    1237250004              -0.9          2.7       4.8     pCi/g           u                       HB0362 F55-0783:00L02-01-028-F                    1237250005                0.2          2.9       5.0     pCi/g           u                       HB0362 F55-0787:00L02-01-032-F                    1237250006              -0.5          2.6       4.6     pCi/g           u                       HB0362 Validated By:
Date:
Approved By:        tr/l/i.#W          j?  J.10  L Date:          I 0/  J 'I J) b            I    /
Qualifier Flags:
U= Analyte not detected (<MDC)
TPU= Total Propagated Uncertainty MDC= Minimum Detectable Concentration Page 1 of 1}}

Latest revision as of 21:33, 4 February 2020

Letter Report for Analytical Results for Six Soil Samples Associated with the Humboldt Bay Power Plant in Eureka, California
ML16344A259
Person / Time
Site: Humboldt Bay
Issue date: 10/27/2016
From: Ivey W
Oak Ridge Institute for Science & Education
To: John Hickman
Office of Nuclear Material Safety and Safeguards
References
DCN: 5201-LR-04-0, DE-SC0014664, RFTA 16-001, TAC J00338
Download: ML16344A259 (10)
v • d • e


Text

ltr* OAK RIDGE INSTITUTE FOR

~~ SCIENCE AND EDUCATION

~ ~ Managed by ORAU for DOE October 27, 2016 Mr. John Hickman U.S. Nuclear Regulatory Commission 11545 Rockville Pike Mailstop T8FS Rockville,IvID 20852 ORISE CONTRACT NO. DE-SC0014664

SUBJECT:

LETTER REPORT FOR ANALYTICAL RESULTS FOR SIX SOIL SAMPLES ASSOCIATED WITH THE HUMBOLDT BAY POWER PLANT IN EUREKA, CALIFORNIA

[TAC NO. J00338] [DOCKET NO. 50-133](RFTA NO.16-001)

DCN: 5201-LR-04-0

Dear Mr. Hickman:

Oak Ridge Institute for Science and Education (ORISE) received SL'i: soil samples on September 14, 2016 from the Humboldt Bay Power Plant in Eureka, Califomia. ORISE is managed by Oak Ridge Associated Universities(ORAU) under DOE contract number DE-SC0014664. The samples were shipped to the laboratory from the licenssee's laboratory. The samples were received in good condition. Per the chain of custody, the samples were analyzed for gamma emitting isotopes by gamma spectrometry. In addition, per your request, the samples were analyzed for tritium by liquid scintillation counting. The analytical data, along with the procedure references, are presented in the attached reports.

Quality Control (QC) requirements were met for these analyses. The QC files are available for your review upon request.

Please feel free to contact me at 865.576.9184 or Forrest Smith at 865.574.9802 with any questions or comments.

S~cerely, ~ *Ir \J>µ;~'(-

~ '6,L~

~Je Ivey Laboratory Manager ORAU WPI:\'<!FS:km:lw Enclosures Electronic distribution: T. Carter, NRC S. Roberts, ORAU T. Vitkus, ORAU E. Bailey, ORAU D. Hagemeyer, ORAU File code: 5201; Lab code: 12372 P.O. Box 117 Oak Ridge, TN 37831

  • www.orau.org

'j OAK RIDGE INSTITUTE FOR

~ ~ Managed by ORAU for DOE

~~SCIENCE AND EDUCATION Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016

'Project#: 201212372 coc #: 1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Analyst: smithw Client Sample ID: FSS-0757: OOL02-01-002-F Lab Sample ID: 1237280001 Smp Qty.: 646.98 Units: grams Geometry: LM Detector ID: DET07 Live Time(s): 3,600 SOP (Rev.#): CP1 (20)

Count Date: 912812016 Receipt Date: 911412016 Collection Date: 8130/2016 SDG: 201212372-1 Am-241 59.54 -0.082 0.045 0.102 pCi/g u NIA NIA Co-57 122.06 -0.001 0.013 0.031 pCilg u NIA N/A Co-60 1332.49 -0.002 0.026 0.054 pCilg u NIA NIA Cs-134 795.86 0.026 0.027 0.066 pCilg u NIA NIA Cs-137 661.66 0.128 0.027 0.034 pCilg 661.71 NIA NIA Eu-152 344.28 0.003 0.054 0.124 pCilg u NIA NIA Eu-154 723.30 -0.07 0.11 0.25 pCi/g u NIA NIA Eu-155 105.31 0.033 0.043 0.110 pCilg u NIA NIA K-40 1460.82 11.9 1.1 0.5 pCilg 1461.09 NIA NIA Mn-54 834.85 0.025 0.018 0.038 pCilg 835.96 u NIA NIA Se-75 264.66 -0.015 0.022 0.050 pCi/g u NIA NIA U-238 by Th-234 63.29 1.40 0.44 0.63 pCilg 63.22 NIA NIA Zn-65 1115.54 -0.150 0.089 0.136 pCilg u NIA NIA Qualifier Flags:

U = Analyte not detected (< MDC) Page 1of8 TPU = Total Propagated Uncertainty MDC= Minimum Detectable Concentration

l1fj OAK RIDGE INSTITUTE FOR II SCIENCE AND EDUCATION

~ I Managed by ORAU for DOE Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 Project#: 201212372 coc #: 1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Analyst:' smithw Client Sample ID: FSS-0765: OOL02-01-010-F Lab Sample ID: 1237280002 Smp Qty.: 502.55 Units: grams Geometry: LM Detector ID: DET08 Live Time(s): 3,600 SOP (Rev.#): CP1 (20)

Count Date: 912812016 Receipt Date: 911412016 Collection Date: 813012016 SDG: 201212372-1 Am-241 59.54 -0.143 0.050 0.104 pCilg u NIA NIA Co-57 122.06 -0.001 0.012 0.029 pCilg u NIA NIA Co-60 1332.49 -0.015 0.027 0.050 pCilg u NIA NIA Cs-134 795.86 0.049 0.026 0.064 pCilg u NIA NIA Cs-137 661.66 0.056 0.018 0.031 pCi/g 661.65 NIA NIA Eu-152 344.28 -0.028 0.049 0.106 pCilg u NIA NIA Eu-154 723.30 -0.129 0.071 0.203 pCi/g u NIA NIA Eu-155 105.31 0.007 0.051 0.12Q pCilg u NIA NIA K-40 1460.82 15.3 1.3 0.7 pCilg 1461.05 NIA NIA Mn-54 834.85 0.010 0.018 0.050 pCilg u NIA NIA Se-75 264.66 -0.010 0.025 0.054 pCilg u NIA NIA U-238 by Th-234. 63.29 2.80 0.73 0.75 pCilg 63.25 NIA NIA Zn-65 1115.54 -0.079 0.061 0.113 pCilg u NIA NIA Qualifier Flags:

U = Analyte not detected(< MDC) Page 2 of 8 TPU = Total Propagated Uncertainty MDC = Minimum Detectable Concentration

l1rj OAK RIDGE INSTITUTE FOR

~~

~~SCIENCE AND EDUCATION Managed by ORAU for DOE Gamma Spectrometry Summary Sheet Further: Toget11er Report Date: October24, 2016, Project#: 201212372 coc #: 1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Analyst: smithw

.Client Sample ID: FSS-0779: OOL02-01-024-F Lab Sample ID: 1237250003 Smp Qty.: 523.29 Units: grams Geometry: LM Detector ID: DET09 Live Time(s): 3,600 SOP (Rev.#): CP1 (20)

Count Date: 912812016 Receipt Date: 911412016 Collection Date: 813012016 SDG: 201212372-1 Am-241 59.54 -0.080 0.043 0.097 pCilg u NIA NIA Co-57 122.06 0.001 0.013 0.031 pCilg u NIA NIA

. Co-60 1332.49 -0.003 0.025 0.049 pCilg u NIA N/A Cs-134 795.86 -0.006 0.014 0.063 pCilg u NIA NIA Cs-137 661.66 0.464 0.055 0.034 pCilg 661.74 NIA NIA Eu-152 344.28 -0.024 0.044 0.100 pCi/g u NIA N/A Eu-154 723.30 -0.15 0.11 0.22 pCi/g u NIA NIA Eu-155 .105.31 0.054 0.032 0.069 pCilg 104.93 u NIA NIA K-40 1460.82 13.4 1.2 0.5 pCilg 1461.14 NIA NIA Mn-54 834.85 0.002 0.024 0.053 pCi/g u NIA NIA Se-75 264.66 -0.008 0.024 0.057 pCi/g u NIA NIA U-238 by Th-234 63.29 2.06 0.58 0.69 pCi/g 63.19 NIA NIA Zn-65 1115.54 -0.091 0.078 0.139 pCi/g u NIA NIA Qualifier Flags:

U = Analyte not detected (< MDC)

  • Page 3 of 8 TPU = Total Propagated Uncertainty MDC = Minimum Detectable Concentration

,~I fj OAK RIDGE INSTITUTE FOR

~ ~ Managed by ORAU for DOE SCIENCE AND EDUCATION Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 Project#: 201212372 coc # : 1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Analyst: smithw Client Sample ID: FSS-0782: OOL02-01-027-F Lab Sample ID: 1237280004 Smp Qty.: 745.59 Units: grams Geometry: LM Detector ID: DET10 Live Time(s): 3,600 SOP (Rev.#): CP1 (20)

  • count Date: 912812016 Receipt Date: 911412016 Collection Date: 813012016 SDG: 201212372-1 Am-241 59.54 -0.025 0.087 0.212 pCilg u NIA NIA Co-57 122.06 0.0084 0.0100 0.0234 pCilg 121.30 u NIA NIA Co-60 1332.49 -0.013 0.021 0.039 pCilg u NIA NIA Cs-134 795.86 0.039 0.022 0.055 pCilg u NIA NIA Cs-137 661.66 0.044 0.017 0.035 pCilg 661.97 NIA NIA Eu-152 344.28 0.023 0.042 0.102 pCilg u NIA NIA Eu-154
  • 723.30 -0.133 0.095 0.175 pCilg u NIA NIA Eu-155 105.31 0.037 0.052 0.133 pCilg u NIA NIA K-40 1460.82 11.1 1.0 0.6 pCilg 1460.60 NIA NIA Mn-54 834.85" -0.016 0.020 0.038 pCilg u NIA NIA Se-75 264.66 -0.004 0.021 0.049 pCi/g u NIA NIA U-238 by Th-234 63.29 0.99 0.58 1.21 pCi/g 63.55 u NIA NIA Zn-65 1115.54 -0.095 0.060 0.101 pCilg u NIA NIA Qualifier Flags:

U = Analyte not detected (< MDC) Page 4 of 8 TPU = Total Propagated Uncertainty MDC = Minimum Detectable Concentration

l1fj OAK RIDGE INSTITUTE FOR

~I SCIENCE AND EDUCATION Gamma Spectrometry Summary Sheet EI Managed by ORAU for DOE Further. Together Report Date: October 24, 2016 Project#: 201212372 coc # : 1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Analyst: smithw Client Sample ID: FSS-0783: OOL02-01-028-F Lab Sample ID: 1237250005 Smp Qty.: 628.05 Units: grams Geometry: LM Detector ID: DET07 Live Time(s): 3,600 SOP (Rev.#): CP1 (20)

Count Date: 913012016 Receipt Date: 911412016 Collection Date: 813012016 SDG: 201212372-1 Am-241 59.54 0.009 0.036 0.112 pCi/g u NIA NIA Co-57 122.06 0.009 0.014 0.034 pCilg u NIA NIA Co-60 1332.49 -0.014 0.031 0.060 pCilg u NIA NIA Cs-134 795.86 0.025 0.031 0.074 pCilg u NIA NIA Cs-137 661.66 0.218 0.036 0.041 pCilg 661.74 NIA NIA Eu-152 344.28 -0.045 0.064 0.136 pCi/g u NIA NIA Eu-154 723.30 -0.23 0.15 0.25 pCilg u NIA NIA Eu-155 105.31 0.059 0.047 0.122 pCilg

  • u NIA NIA K-40 1460.82 15.2 1.4 0.6 pCilg 1461.00 NIA NIA Mn-54 834.85 -0.002 0.027 0.058 pCilg u NIA NIA Se-75 264.66 -0.006 0.026 0.062 pCilg u NIA NIA U-238 by Th-234 63.29 0.66 0.36 0.73 pCilg 63.39 u NIA NIA Zn-65 1115.54 -0.170 0.089 0.153 pCilg u NIA NIA Qualifier Flags:

U = Analyte not detected (< MDC) Page 5 of 8 TPU = Total Propagated Uncertainty MDC = Minimum Detectable Concentration

, Jj OAK 11 RIDGE INSTITUTE FOR

~ ~ Managed by ORAU for DOE SCIENCE AND EDUCATION Gamma Spectrometry Summary Sheet Furt11e1: Together Report Date: October 24, 2016 Project#: 201212372 coc # : 1609-008 Project Name: Humboldt Bay PP 09-2016 Batch Number: GS0351 Analyst: smithw Client Sample ID: FSS-0787: OOL02-01-032-F Lab Sample ID: 1237280006 Smp Qty.: 655.82 Units: grams Geometry: LM Detector ID: DET07 Live Time(s): 3,600 SOP (Rev.#): CP1 (20)

Count Date: 912812016 Receipt Date: 911412016 Collection Date: 813012016 SDG: 201212372-1 Am-241 59.54 -0.045 0.046 0.107 pCilg u NIA NIA Co-57 122.06 0.0085 0.0097 0.0227 pCilg 123.06 u NIA NIA Co-60 1332.49 0.017 0.027 0.063 pCilg u NIA NIA Cs-134 '795.86 0.002 0.031 0.065 pCilg u NIA NIA Cs-137 661.66 0.478 0.054 0.040 pCilg 661.88 NIA NIA Eu-152 344.28 0.024 0.054 0.134 pCilg u NIA NIA Eu-154 723.30 -0.18 0.13 0.25 pCilg u NIA NIA Eu-155 105.31 -0.018 0.043 0.106 pCilg u NIA NIA K-40 1460.82 12.3 1.2 0.6 pCilg 1461.00 NIA NIA Mn-54 834.85 0.006 0.027 0.059 pCilg u NIA NIA Se-75 264.66 -0.009 0.025 0.057 pCilg u NIA NIA U-238 by Th-234 63.29 0.70 0.35 0.69 pCilg 63.26 NIA NIA Zn-65 1115.54 -0.133 0.085 0.148 pCilg u NIA NIA Qualifier Flags:

U = Analyte not detected (<MDC) Page 6 of 8 TPU = Total Propagated Uncertainty MDC= Minimum Detectable Concentration

l1fj OAK RIDGE INSTITUTE FOR

~~

~~SCIENCE AND EDUCATION Managed by ORAU for DOE Gamma Spectrometry Summary Sheet Further. Together Report Date: October 24, 2016 Project#: COC#:

Project Name:

Batch Number: GS0351 Analyst: smithw Client Sample ID:

Lab Sample ID: BLK0351S Smp Qty.: 1.00 Units:* sample Geometry: LM Detector ID: DET09 Live Time(s): 3,600 SOP (Rev.#): CP1 (20)

Count Date: 912812016 Receipt Date: 911412016 Collection Date:

SDG:

Am-241 59.54 -1.7 7.7 19.6 pCilsample u NIA NIA Co-57 122.06 -0.9 3.3 7.9 pCilsample u NIA NIA Co-60 1332.49 -1.8 6.9 14.8 pCi/sample u NIA NIA Cs-134 795.86 -1.7 6.2 14.1 pCilsample u NIA NIA Cs-137 661.66 5.1 6.4 17.0 pCi/sample u NIA NIA Eu-152 344.28 3 14 35 pCilsample u NIA NIA Eu-154 723.30 . -14 30 66 pCilsample u NIA NIA Eu-155 105.31 12 11 30 pCilsample u NIA NIA K-40 1460.82 -11 84 226 pCilsample 1461.09 u NIA NIA Mn-54 834.85 -2.5 6.3 12.5 pCilsample u NIA NIA Se-75 264.66 -2.4 6.1 14.1 pCilsample u .NIA NIA U-238 by Th-234 63.29 -27 59 158 pCi/sample 63.48 u NIA NIA Zn-65 1115.54 -8 15 28 pCilsample u NIA NIA Qualifier Flags:

U = Analyte not detected (< MDC) Page 7 of 8 TPU = Total Propagated Une;ertainty MDC= Minimum Detectable Concentration

l1fj OAK RIDGE INSTITUTE FOR

~I SCIENCE AND EDUCATION Gamma Spectrometry Summary Sheet I ~ Managed by ORAU for DOE Further. Togetl1er Report Date: October24, 2016 Project#: COC#:

Project Name:

Batch Number: GS0351 Analyst: smithw Client Sample ID:

Lab Sample ID: LCS0351S Smp Qty.: 514.39 Units: grams Geometry: 250LM Detector ID: DET08 Live Time(s): 3,600 SOP (Rev.#): CP1 (20)

Count Date: 912812016 Receipt Date: 911412016 Collection Date:

SDG:

Am-241 59.54 9.04 0.27 0.12 pCilg 59.45 NIA 0.96 Co-57 122.06 2.96 0.35 0.59 pCilg 121.95 NIA N/A Co-60 1332.49 5.62 0.25 0.12 pCilg 1332.69 NIA NIA Cs-134 795.86 0.07 0.14 *0.29 pCilg* u NIA NIA Cs-137 661.66 3.73 0.25 0.07 pCilg 661.67 NIA 0.95 Eu-152 344.28 ' 0.051 0.089 0.202 pCilg u NIA NIA Eu-154 723.30 -0.13 0.20 0.40 pCilg u NIA NIA Eu-155 105.31 0.122 0.097 0.234 pCilg u NIA NIA

.K-40 1460.82 0.14 0.20 0.47 pCilg 1461.21 u NIA NIA Mn-54 834.85 -0.57 0.66 1.26 pCilg u NIA N/A Se-75 264.66 35 35 81 pCi/g. 263.79 u NIA N/A U-238 by Th-234 63.29 -14.6 3.5 1.0 pCi/g u NIA N/A Zn-65 1115.54 -0.1 3.1 7.1 pCilg u N/A N/A Electronically Validated By:

Roxanne Nagle- 10/512016 09:23 Electronically Approved By:

µ;~fl Yr Wade Ivey 10/2412016 13:01 Qualifier Flags:

U = Analyte not detected(< MDC) Page 8 of 8 TPU = Total Propagated Uncertainty MDC= Minimum Detectable Concentration

Liquid Scintillation Analysis Summary Results by Analyte

\1rl. OAK RIDGE INSTITUTE FOR

~~ SCIENCE AND EDUCATION

~ ~ Managed by ORAU for DOE

<=>~t=1Jrt<-~r. *ro_.-:1c.*//*u.::-r Analyte: H-3 SOP (Rev.#): AP6 (21) Report Date: 10/11/2016 Project Name:: Humboldt Bay PP 09-2016 Project#: 201212372 SDG #: 201212372-1

  • ' * *, * ** '~

-~

  • _, ~-. .,- .:;

-~::':.'.~~~~:~~.'~'.~~ ~~N':::'f.**:;:**'.

... :cri~n_t,$.i!rfi:R!i:ib~ - * * ***>+/--~--<*.~-~ ~ ~ ~@ ...

FSS-0757:00L02-01-002-F 1237250001 0.6 3.4 5.9 pCi/g u HB0362 FS5-0765:00L02-01-010-F . 1237250002 -0.9 2.9 5.2 pCi/g u HB0362 F55-0765:00L02-01-010-F 12372S0002Dup 0.2 2.8 4.9 pCi/g u HB0362 F55-0779:00L02-01-024-F 1237250003 -1.4 2.1 3.8 pCi/g u HB0362 FS5-0782:00L02-01-027-F 1237250004 -0.9 2.7 4.8 pCi/g u HB0362 F55-0783:00L02-01-028-F 1237250005 0.2 2.9 5.0 pCi/g u HB0362 F55-0787:00L02-01-032-F 1237250006 -0.5 2.6 4.6 pCi/g u HB0362 Validated By:

Date:

Approved By: tr/l/i.#W j? J.10 L Date: I 0/ J 'I J) b I /

Qualifier Flags:

U= Analyte not detected (<MDC)

TPU= Total Propagated Uncertainty MDC= Minimum Detectable Concentration Page 1 of 1

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