ML19330A360

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Operating Procedure 2-OP-12.1,Revision 1, Sampling Sys.
ML19330A360
Person / Time
Site: North Anna Dominion icon.png
Issue date: 07/11/1980
From: Harvey S
VIRGINIA POWER (VIRGINIA ELECTRIC & POWER CO.)
To:
Shared Package
ML19330A354 List:
References
2-OP-12.1, NUDOCS 8007170183
Download: ML19330A360 (30)
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Text

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2-OP-12.1 3

Page 1 of 29 07-11-80 9

VIRGINIA ELECTRIC AND POWER COMPATI NORTH ANNA PCWER STATION UNIT 2 SAMPLING SYSTEM

REFERENCES:

1. ESK - 4A Sample System Panel
2. NAS - 185 Sample Coolers
3. FSAR - 9.3.2 Sampling System
4. 12050-FM - 89A, B Sampling System Valve Operating Diagram
5. 12050-FM - 33A, B Sample System Flow Diagram
6. Nureg - 0578
7. Stone & Webster sketch number N313 REV. NO.: 1 PAGE: Entire DATE: 07-11-80 APPROVAL: bd((

. RECOMMEND APPROVAL: in gg ;d APPROVED BY: , ub . t, 4 /__

CHAIRMAN jfrATION NGCLEAR' SAFETY /

AND GPERATING COMMInu.

DATE: 07-11-80 5 l 8691L7G.LB3 ,

'%' 2-OP-12.1 Page 2 of 29 07-11-80 VIRGINIA ELECTRIC AND POWER COMPANY NORTH ANNA POWER STATION UNIT 2 SAMPLING SYSTEM 1.0 Purpose 1.1 This procedure provides the Sampling System normal valve lineup and detailed instructions for conducting primary and seco:-iary .

fluid and gaseous samples for anslysis, continuous monitoring of the steam generator blowdown and various conductivity, PH, and dissolved 0 samples from points within the plant.

2 1.1.1 Influent Liquid Sample for Chemical and Volume Control System Dem'.neralizers.

1.1.2 Chemical and Volume Control System Mixed Bed Demin-eralizer 2-CH-I-1A or 13 Effluent Liquid Sample 1.1.3 Chemical and Volume control System Cation Demineralizer 2-CH-I-2 Effluent Liquid Sample 1.1.4 Chemical and lolume Control System Deborating Demin-eralizer 2-CH-I-3A or 33 Effluent Liquid Sample 1.1.5 Charging Pump Discharge 2-CH-P-1A or 1B or 1C Liquid Sample l.1.6 Volume Contrel Tank (2-CH-TK-2) Liquid Sample 1, t . 7 Volume Control Tank Gaseous Sample 1.1.8 Residual Heat Removal Outlet (or Inlet) Liquid Sample 1.1.9 Pressurizer Liquid Sample l

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l' 2-OP-12.1 Page 3 of 29 07-11-80 1.0 Purpose (cont')

1.1.10 Pressurizer Gaseous Sample 1.1.11 Primary Coolant Eat Leg Influent Liquid to Steam Gene-rator, Loop A, B, or C (or Loop B Reactor Side) 1.1.12 Primary Coolant Cold Leg Effluent Liquid from Steam Generator (Loop A, B or C) 1.1.13 Pressurizer Relief Tank (2-RC-TK-2) Gaseous 1.1.14 Steam Generator Blowdown Liquid Sample (Loop A, B or C) 1.1.15 Feedwater Liquid Sample 1.1.16 Condensate Pump Discharge Liquid Sample 1.1.17 Main Steam Liquid Sample (Loop No. A, B or C) 1.1.18 Flash Evaporator Distillate Liquid Sample 1.1.19 Flash Evaporator Demineralizer Effluent Liquid Sample 1.1.20 Flash Evapor.itor Recycle Pump Discharge Liquid Sample 1.1.21 Steam Generator Surface Liquid Sample 1.1.22 Post Accident Sampling of the Reactor Coolant System

, 2-OP-12.1 Paga 4 of 29 s 07-11-80 2.0 Initial Conditions 2.1 Sample System Instrumentation calibrated and in service.

2.2 Component Cooling Water System is operable per 2-0P-51 for auxiliary building sample.

2.3 Chemical and Volume Control System is operable per 2-OP-8.

2.4 Baron Recovery System operable per 1-OP-10.

2.5 Compressed Air System is operable per 2-OP-46. ,

2.6 Ventilation System is operable per 1-OP-21.

2.7 Radiation Monitoring System is operable per 2-0?-62.

2.8 Bearing Cooling Water System is operable per 2-CP-50 for turbine building samples.

2.9 ,

Sample System Valve Checkoff List 2-OP-1.2A has been completed.

2-OP-12.1 i Page 5 of 29 07-11-80 3.0 Precautions and Limitations 3.1 Extreme caution must be exercised while taking samples due to possible high temperatures, pressures, and radiation levels.

3.2 The RVP (Radiation Work Permit) will be strictly adhered to at all times while obtaining radioactive or potentially radio -

active samples.

3.3 Open all valves slowly to prevent flashing.

3.4 Wear protective clothing when obtaining samples, i.e. , lab coat, rubber gloves, and face shield or eyeglasses when ob-taining samples out of primary sample sink.

3.5 To ensure a representative sample, purge all samples to their associated purge headers for specific quantities or volumes.

3.6 To prevent damage to the sample coolers, insure cooling water discharge temperature is less than 150*F.

3.7 To prevent damage ta the Radiation Monitors RM-222, 223, 224, (Steam Generator Blowdown), insure the Steam Generator Blowdown Sample coolers 2-SS-E-3A, 33 and 3C discharge terperatrres do not exceed 115"F. The rate of temperature change is critical on the Sodium Iodide crystal and should be less than 10 C/Hr.

3.8 If at any time during the process of sampling, a radiation alarm occurs on Pd-RMS-156 (Sa yle Area Monitor), stop sampling, leave area, and inform the Control Room.

3.9 Inform Control Room Operator prior to and after drawing any Reactor Coolant Syste= sample located in the Auxiliary Building Sampling Room.

. 2-OP-12.1 Page 6 of 29 07-11-80 3.0 Precautions and Lbsitations (cont')

3.10 To prevent any out leakage of radioactive or potentially radio-active gas into the Auxiliary Building Sample Room, ensure that the tell tale indicates air flow into the sample sink when any sample sink door is open.

3.11 During abnormal valve lineups, verify the origin of all. samples.

Due ta the versatility of some systems, samples may not be as marked.

3.12 When sampling high pressure systems, use the stain.less steel sampling bomb.

3.13 When isolating sample bombs, close the ischarge valve before closing inlet valve.

3.14 In the event of an accident that =ay cause core damage observe the following:

3.14.1 Health Physics will generate a special radiation work permit to obtain and analyre the coolant sample based upon current radiological conditions and anticipated radiological harards. Consider use of special dosi-metry; e.g. extremities, head, etc.

3.14.2 Health Physics will . provide continuous dose control coverage while obtaining and analyzing the reactor coolant sample.

3.14.3 Individuals shall not exceed 2.5 rem whole-body and/or 15 rem extremity exposure for the current quarter in the performance of this procedure. l 3.14.4 Reactor coolant samples will be obtained and tra'asported in the appropriate shielded cask.

3.14.5 Sample analysis shall be performed in a fame hood.

1

., f 2-OP-12.1 Page 7 of 29 07-11-80 Initials 4.0 Procedure 4.1 Influent Liquid Sample to Chemical and Volume Control System Demineralizers.

4.1.1 Initial Conditions are noted and satisfied.

4 3 4.1.2 Precautions and Limitations are noted.

4.1.3 Open 2-SS-132 and purge to Volume Control Tank.

4.1.4 Observe flow on FI-SS-212.

4.1.5 After purging at least one (1) gallon, close 2-SS-132.

4.1.6 Take desired sample, using 2-SS-133 as sample valve.

4.1.7 After desired sample has been obtained, close 2-SS-133.

Completed By:

, Date:

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2-OP-12.1

/ Page 8 of 29 07-11-80 Initials 4.0 Procedure 4.2 Chemical and Volume Control System Mixed Bed Demineralizer 2-CH-I-1A or 13 Effluent Liquid Sample.

4.2.1 Initial Conditions are noted and satisfied.

4.2.2 Precautions and Limitations are noted.

4.2.3 Open 2-SS-134 and purge to Volume Control Tank.

4.2.4 Observe flow on FI-SS-212.

4.2.5 After purging at least one (1) gallon, close 2-SS-134.

4.2.6 Take desired sample uaing 2-SS-135 as sample valve.

4.2.7 After desired sample has been obtained, close 2-SS-135.

Completed By:

Date:

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2-OP-12.1 Page 9 of 29 07-11-80 Initials 4.0 Procedure 4.3 Che:sical and Volume Control System Cation Demineralizer 2-CH-I-2 Effluent Liquid Sample.

4.3.1 Initial Conditions are noted and satisfied.

4.3.2 Precautions and Limitations are noted.

4.3.3 Open 2-SS-136 and purge to Volume Control Tank.

4.3.4 Observe flow on FI-SS-212.

4.3.5 After purging at least one (1) gallon, close 2-SS-136.

4.3.6 Take desired sample using 2-SS-137 as sample valve.

4.3.7 After desired sample has been obtained, close 2-SS-137.

Completed By:

e Date:

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s 2-OP-12.1

. Page 10 of 29 07-11-80 Initials 4.0 Procedure 4.4 Chemical and Volume Control System Deborating Demineralizer 2-CH-I-3A or 3B Effluent Liquid Sample.

4.4.1 Initial Conditions are noted and satisfied.

4.4.2 Precautions and Limitations are noted.

4.4.3 Open 2-SS-138 and purge to volume Control Tank.

4.4.4 Observe flow on FI-SS-212.

4.4.5 After purging at least one (1) gallon, close 2-SS-138.

4.4.6 Take desired sample using 2-SS-139 as sample valve.

4.4.7 After desired sample has '_een obtained, close 2-SS-139.

Completed By:

Date:

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2-OP-12.1 J Page 11 of 29 07-11-80 Initials 4.0 Procedure 4.5 Charging Pump Discharge 2-G-P-1A,1B, or 1C Liquid Sacple.

4.5.1 Initial Conditions are noted and satisfied.

4.5.2 Precautions and Limitations are noted.

4.5.3 On the Sampling System Panel, select the charging pump discharge to be sampled by opening TV-SS-210A for 2-G-P-1A, TV-SS-210B for 2-G-P-13 or TV-SS-210C for 2-G-P-lC .

NOTE: Open only the TV on the charging pump discharge to be sampled, ensure the other two are closed.

4.5.4 open 2-SS-140 and purge at least 1/2 gallon to Volume Control Tank.

4.5.5 Observe flow on FI-SS-212 and pressure on PI-SS-211.

4.5.6 After purge is complete, close 2-SS-140.

4.5.7 Take desired sample using 2-SS-141 as sample valve.

4.5.8 After desired sample has been obtained, close 2-SS-141.

4.5.9 Close charging pump dischar g le trip valve TV-SS-210A, B or C.

Completed By:

Date:

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. 2-OP-12.1

.. Page 12 of 29 07-11-80 Initials-4.0 Procedure 4.6 Volume Control Tank Liquid Sample.

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4.6.1 Initial Conditions are noted and satisfied.

4.6.2 Precautions and Limitations are noted.

4.6.3 Open 2-SS-143 and purge to Sample Sink.

4.6.4 After purging at least one (1) gallon, take desired sample using 2-SS-143 as sample valve.

4.6.5 After desired sample has been obtained, close 2-SS-143.

Completed By:

Date:

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2-OP-12.1 Page 13 of 29 07-11-80 Initials 4.0 Procedure 4.7 Volume Control tank Gaseous Saa:ple.

4.7.1 Initial Conditions are noted and satisfied.

4.7.2 Precautions and Lic2itations are noted.

4.7.3 Open 2-SS-144 and purge to gas stripper.

4.7.4 Observe flow cn FI-SS-100.

4.7.5 After purging 0.25 ft 3, close 2-SS-144.

4.7.6 Take desired sample using 1-SS-145 as saarple valve.

4.7.7 After desired smnple has been obtained, close 2-SS-145.

Completed By:

Date:

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2-OP-12.1 Page 14 of 29 07-11-80 Initials 4.0 Procedure 4.8 Residual Heat Removal Outlet or Inlet Liquid Sample.

4.8.1 Initial Conditions are noted and satisfied.

4.8.2 Precautions and Limitations are noted.

4.8.3 On the Sampling System Panel, select the section of Residual Heat Removal System to be sampled by opening TV-SS-207A for RHR heat exchanger outlet or TV-SS-207B for RHR heat exchanger inlet.

NOTE: Open only the TV for the section to be sampled, ensure the other one is closed.

4.8.4 Open 2-SS-129 and purge to Volume Control Tani.

4.8.5 Observe flow on FI-SS-212 and pressure on PI-SS-211.

4.8.6 After purging at leist three (3) gallons, close 2-SS-129.

4.8.7 Take desired sample using 2-55-120 as sample valve.

4.8.8 After desired sanple has been ob 2ined, close 2-SS-130.

_ 4.8.9 Close Residual Heat Removal sample trip valve TV-SS-207A, or B.

Cc=pleted By:

Date:

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. 2-OP-12.1

, Page - 15 of 29 07-11-80 Initials 4.0 Procedure 4.9 Pressuriser Liquid Sample.

4.9.1 Initial Conditions are noted and satisfied.

4.9.2 Precautions and Li:::itations are noted.

4.9.3 Open 2-SS-121 and purge to Volt::re Control Tank.

4.9.4 Observe flow on FI-SS-212 and pressure on PI-SS-211.

4.9.5 After purging at least four (4) gallons, close 2-SS--

121.

4.9.6 Take desired sample using 2-SS-122 as sample valve.

4.9.7 After desired sample has been obtained, close 2-SS-122.

l Completed By:

Date:

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  • 2-OP- 12.1 Page 16 of 29 07-11-80 Initials 4.0 Procedure 4.10 Pressurizer Gaseous Sample 4.10.1 Initial Conditions are noted and satisfied.

4.10.2 Precautions and Limitations are noted.

4.10.3 Open 2-SS-114 and purge to Gas Stripper.

4.10.4 Observe flow on FI-SS-100 and temperature on TI-SS-101.

4.10.5 After purging I ft3, at system pressure close 2-SS-114.

4.10.6 Take desired sample, using 2-SS-115 as sample valve.

4.10.7 After desired sample has been obtained, close 2-SS-115.

Completed By:

Date:

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2-OP-12.1 Page 17 of 29 07-11-80 Initials 4.0 Procedure 4.11 Primary Coolant Hot Leg, Influent to Steam Oenerators, Loop 2A, 2B or 2C (or Loop 23 Reactor Side) Sample 4.11.1 Initial Conditions are noted and satisfied.

4.11.2 Precautions and Limitations are noted.

4.11.3 On the Sampling System Panel, select the hot leg to be sampled by opening TV-SS-208A for loop 2A, TV-SS-2083 for loop 2B, TV-SS-208C for loop 2C or TV-SS-208D for reactor side of loop 2B hot leg isolation valve.

NOTE: Open only the TV on the hot leg to be sampled, ensure the other three are closed.

4.11.4 Open 2-SS-108 and purge to Volume Control Tank.

4.11.5 Observe flow on FI-SS-212 and pressure on PI-SS-211.

4.11.6 After purging at least four (4) gallons, close 2-SS-108.

4.11.7 Take desired sample using 2-SS-109 as sample valve.

, 4.11.8 After desired sample has been obtained, close 2-SS-109.

4.11.9 Close Hot Leg Sample trip valve TV-SS-20SA,B,C, or D.

Ccmpleted By:

Date:

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2-0P-12.1

, Page 18 of 29 07-11-80 Initials 4.0 Procedure 4.12 Primarf Coolant Cold Leg, Effluent from Steam Generators, Loop 2A, 23 or 2C Sample.

4.12.1 Initial Conditions are noted and satisfied.

4.12.2 Precautions and limitations are noted.

4.12.3 On the Sampling System Panel, select the cold leg to be sampled by opening TV-SS-209A for loop A, TV-SS-2093 for loop B, or TV-SS-209C for loop C.

NOTS: Open caly the TV on the cold leg to be sampled, en.ure the other two are closed.

4 4.12.4 Open 1-SS-172,1-SS-175 and 1-SS-177 and purge to Volume Control Tank.

4.12.5 Observe flow on FI-SS-212 and pressure on PI-SS-211.

4.12.6 After purging at least four (4) gallons, close 1-SS-172, 1-SS-175 and 1-S5-177.

4.12.7 Take desired sample using 1-5S-172 and 1-SS-173 as sample valve.

i 4.12.8 After desired sa=ple has been obt.ained, close 1-5S-172 .

and 1-SS-173.

4.12.9 Close Cold leg sample trip valve TV-SS-209A, B, or C.

Completed By:

Date.

  • 2-OP-12.1 Page 19 of 29 07-11-80 Initials 4.0 Procedure 4.13 Pressurizer Relief Tank Gaseous 4.13.1 Initial Conditions are noted and satisfied.

4.13.2 Precautions and Limitations are noted.

4.13.3 Connect Sample Bomb to 2-SS-97 and 2-SS-96.

4.13.4 Open 2-SS-96 and slowly open 2-SS-97, and purge 1 f t.

at relief tank pressure, to gas stripper as observed on j FI-SS-100. Close 2-SS-96.

4.13.5 Take sample using 2-SS-97 as sample valve.

4.13.6 After desired sample has been obtained, close 2-SS-97.

Completed By:

J Date:

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4 2-0P-12.1 Page 20 of 29 07-11-80 Initials 4.0 Procedure 4.14 Steam Generator Blowdown Liquid Sample (Loop A, B, or C).

4.14.1 Initial Conditions are noted and satisfici.

4.14.2 Precautions and Limitations are noted.

4.14.3 Open sample valve on loop to be sampled 2-SS-82 for loop A, 2-SS-66 for loop B, or 2-SS-59 for loop C and purge line to sample sink for about 5 seconds.

NOTE: Open only the sample valve on the loop to be sa= pled.

4.14.4 Take desired sample.

4.14.5 After desired sample has been obtained, close sacple valve 2-SS-82, 2-SS-66, or 2-SS-59.

Completed By:

Date:

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. 2-OP-12.1 Page 21 of 29 07-11-80 Initials

, 4.0 Procedure 4.15 Feedwater Liquid Sample 4.15.1 Initial Conditions .: e noted and satisfied.

4. 15.2 Precautions and L.. .:stions are noted.

4.15.3 Fully open sample v41ve 2-SS-48 and purge line to sample sink for about 5 seconds.

4. 15.4 Take desired cample using 2-SS-48 as sample valve.

4.15.5 Af ter sample has been obtained, close 2-SS-43.

Completed By:

Date:

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't 2-o?-12.1 Page 22 of 29 07-11-80 Initial's 4.0 Procedure 4.16 Condensate Pump Discharge Liquid Sample (Common) 4.16.1 Initial Conditions are noted and satisfied.

4.16.2 Precautions and Limitations are noted.

4.16.3 Fully open sample valve 2-SS-37 and purge line to sample sink for about 5 seconds.

4.16.4 Take desired sample using 2-SS-37 as sample valve.

4.16.5 After desired sample has been obtained, close 2-SS-37.

Completed By:

i Date:

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.- 2-0P-??.1 Page 23 of 29 67-11-80 Initials

f. . O : Procedure 4.17 Main Steam Liquid Sample (Loop A, B, or C).

4.17.1 Initial Conditions are noted and satisfied.

4.17.2 Precautions and Limitations are noted.

4.17.3 (2-SS-22 loop A)-(2-SS-18 loop B) and (2-SS-14 loop C) are to be continuously purged to condenser hotwell, observe flow on FI-SS-218.

4.17.4 Fully open sample valve on loop to be sampled 2-SS-23 for loop A, 2-SS-19 for loop B, or 2-SS-15 for loop C and purge line to sample sink for about 5 seconds.

NOTE:

Open only the sample valve on the loop to be sampled.

4.17.5 Take desired sample.

4.17.6 After desired sample has been obtained, close sacple valve 2-SS-23, 2-SS-19 or 2-SS-15.

Cc=pleted By:

Date:

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2-OP-12.1

[' Page 24 of 29 07-11-80 Initials 4.0 T .cc eedure 4.18 Flash Evaporator Distillate Sample 4.18.1 Initia) Conditions sre noted and satisfied.

4.18.2 Precautions and Limitations are noted.

4.18.3 2-SS-8 will be continuously purged to condenser hotwell.

4.18.4 Fully open sample valve 2-SS-9 and purge line to sample sink for about 5 seconds.

4.18.5 Take desired sample using 2-SS-9 as sample valve.

4.18.6 After desired sample has been obtained, close 2-SS-9.

Ccmpleted By:

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. *' 2-OP-12.1 Page 25 of 29 07-11-80 Initials 4.0 Procedure 4.19 Flash Evaporator Demineralizer Effluent Sample.

4.19.1 Initial Conditions are noted and satisfied.

4.19.2 Precautiens and Limitations are noted.

_ 4.19.3 2-SS-4 sill be continuously purged to condenser hot-well.

4.19.4 Fully open sample v11ve 2-SS-5 and purge line to sample sink for about- 5 seconds.

4.19.5 Take sample using 2-SS-5 ts sample valve.

4.19.6 After sample has been obtained, close 2-SS-5.

Completed By:

Date:

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  • 2-OP- 12.1 Page 26 of 29 07-11-80 Initials 4.0 Procedure 4.20 Flash Evaporator Recycle Pump Discharge Sample 4.20.1 Initial Conditions are noted and satisfied.

4.20.2 Precautions and Limitations are noted.

4.20.3 Open sample valve 2-SS-3 and purge about 2 liters to sample sink.

4.20.4 Take sample using 2-SS-3 as sample valve.

4.20.5 After sample has been obtained, close 2-SS-3.

' Completed By:

Date:

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  • 2-OP-12.1
Page 27 of 29 C7-11-80 Initials 4.0 Procedure 4.21 Steam Generator Surface Liquid Sample.

4.21.1 Initial Conditions are noted and satisfied.

4.21.2 Precautions and Limitations are noted.

4.21.3 Close 2-SS- Loop C Steam Generator Blowdown Sample Isolation Valve.

4.21.4 Open 1-SS-225 Steam Generator Surface Sample Header Isolation Valve.

4.21.5 On the Sampling System Panel, select the Steam Gene-rator to be sampled by opening TV-SS-lllA for loop A, TV-SS-lllB for loop B or TV-SS-111C for loop C.

NOTE: Open only. the TV on the steam generator to be sampled, ensure the other two are closed.

4.21.6 Open sample valve 1-SS-153 to sample and drain about 5 gallons.

4.21.7 Take sample using 1-SS-153 as sample valve.

4.21.8 After sample has been obtaii.ed, close 1-SS-153.

4.21.9 Close Steam Generator Surface Sample trip valve TV-SS-llLA, B, or C.

4.21.10 Close 1-SS-2 5.

4.21.11 Open 1-SS-226.

Completed By:

Date: -

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  • 2-OP-12.1 Page 23 of 29 07-11-80 Initials 4.0 Procedure 4.22 Post Accident Sample as per Attachment 1.

4.22.1 Reset phase "A" isolation just pri.or to step 4.22.3.

4.22.2 Observe Precautions and Limitations with special atten-tion to 3.14.

4.22.3 ".tve operations open 2-TV-SS-206A & B. (Hot leg sample isolation valves) 4.22.4 Shut or check shut valves 2-SS-108 (Hot i.ig sample

~

recirc.) and 2-SS-109 & 110 (Hot leg sample points in sarole sink).

4.22.5 C' eck sample holding tank empty and depressurized by opening valves "F" and "N". Then shut valves "F" and "N" (Drain and vent valves for holding tank,a 4.22.6 Insure valves "C", "D", "F", "G", "H" , "K" , "L" , "M " ,

and "N" are shut. Op-n valves "Y.", "I" and "J" . Check open the-pressure gage isolation valve.

4.22.7 Open 2-TV-SS-208D.

CAUTION: High activity sa. ple flow will coc:mence at the following step.

4.22.8 Open valve "D" 1/4 to 1/2 turn. When pressure gage reads about 20 psig, shut valve "E" and continue to purge the sample to the holding tank through valves "I" and "J".

4.22.9 tihen the pressure gage reads 100 psig it valves "D",

"I", "J", and 2-TV-SS-208D. -

4.22.10 With sample case (" PIG") in place and connected, open valves "K" and "L", adjust the N2 pressure regulator to 10 psig and open valve "G".

ap _ _ - ._ .

- . ,t ' 2-OP-12.1 Page 29 of 29 07-11-80 Initials -

4.0' Procedure 4.22.11 Shut "G", "K", and "L" (the sample collected in the shielded cask is diluted by a factor of 1000). Other dilutions can be used at the discretion of the person obtaining the sample.

4.22.12 Disconnect the shielded cask from the sample system, lower the lid onto the sample, and transport the shielded cask containing the sample to the Chemistry Hot Lab.

4.22.13 Perfor:n the necessary chemical analyses in the fume 4

hood using appropriate Chemistry procedures. e.g.

CP-11 and CP-32.

NOTE: Since excessive radioactivity may be present, pay speci.al attention to radiological precautions and pro tection.

Completed By:

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.g 2-OP-12.1

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