ML063400437

Final Status Survey Final Report Phase IV, Appendix A4, Survey Unit Release Record 9106-0004, Discharge Canal

ML063400437
Person / Time
Site:	Haddam Neck File:Connecticut Yankee Atomic Power Co icon.png
Issue date:	11/14/2006
From:	Connecticut Yankee Atomic Power Co
To:	NRC/FSME
References
9106-0004
Download: ML063400437 (332)

Text

Book of 1 Final Status Survey Final Report Phase IV Appendix A4 Survey Unit Release Record 9106-0004, Discharge Canal November 2006 I

CYAPCO FINAL STATUS SURVEY RELEASE RECORD DISCHARGE CANAL SURVEY UNIT 9106-0004 Prepared By: Date: -

F S n i-eer Reviewed By: Date:

FSS§)Kgineer Approved By7O Date:

Technicar Support Manager Revision 0

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD TABLE OF CONTENTS

1. SURVEY UNIT DESCRIPTION ..................................................... 3

2. CLASSIFICATION BASIS ............................................................. 3

3. DATA QUALITY OBJECTIVES (DQO) ......................................... 5

4. SURV EY D ESIGN ........................................................................... 8

5. SURVEY IMPLEMENTATION ..................................................... 11

6. SURV EY RESULTS ....................................................................... 12

7. QUALITY CONTROL .................................................................. 14

8. INVESTIGATIONS AND RESULTS ............................................ 14

9. REMEDIATION AND RESULTS .................................................. 15

10. CHANGES FROM THE FINAL STATUS SURVEY PLAN ...... 15

11. DATA QUALITY ASSESSMENT (DQA) ..................................... 15

12. A NO MA LIE S ................................................................................. 16

13. C O N CLU SIO N ............................................................................... 16

14. A TTA CH MEN TS ............................................................................. 167 14.1 Attachment 1 - Figures (6 pages including cover) 14.2 Attachment 2 - Sample and Statistical Data (312 pages including covers)

Revision 0

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD SURVEY UNIT DESCRIPTION Survey Unit 9106-0004 (Discharge Canal) is designated as Final Status Survey (FSS) Class 2 and consists of approximately 9,900 m2 (2.45 acres) of water covered sediment in an area located approximately 0.28 miles from the reference coordinate system benchmark used at the Haddam Neck Plant (HNP)

(see Attachment 1, Figure 1). The Discharge Canal is a man-made mile long waterway that runs parallel to, and ultimately communicates with the Connecticut River. The Discharge Canal is subdivided into fifteen (15) survey units including two (2) permanent wetland areas for FSS purposes. The survey unit is bounded as follows: Discharge Canal Survey Unit 9106-0003 is to the north, (called north as orientated with the north to south flow of the Connecticut River),land surface area Survey Unit 9528-0005 is to the east, Discharge Canal Survey Unit 9106-0005 is to the south and land Surface Area 9520 is to the west. The survey unit comprises the canal sediments to the deeper of three feet or the original construction depth. It extends up the canal banks to the mean high water level.

The reference coordinates associated with this survey unit are E007 through E022 by S090 through S100 (refer to License Termination Plan Section 5.4.4).

The reference coordinates provide the maximum dimensions of a rectangle containing this survey unit. Some areas contained in this rectangle may not be part of this survey unit. The boundary of the survey unit was defined using a Global Positioning System (GPS) based on the Connecticut State Plane System North American Datum (NAD) 1927.

2. CLASSIFICATION BASIS The survey unit was classified in accordance with Procedure RPM 5.1-10, "Survey Unit Classification." The historical information, scoping analyses and characterization results provided sufficient data to designate Survey Unit 9106-0004 as Class 2 in May 2006.

The "Classification Basis Summary" conducted for this survey unit consisted of:

a) A review of the 10CFR50.75 (g) (1) database, b) A review of the "InitialCharacterizationReport" and the "HistoricSite Assessment (HSA) Supplement, "

c) Historic and current survey records review, d) Visual inspections and a "walkdown."

e) Formal or informal interviews with cognizant personnel.

A review of the 10CFR50.75(g)(1) database report identified a number of events that may have impacted this survey unit. Several events indicated the potential for plant related contamination in the survey unit. These included a number of primary side system to secondary side system leakage events, Revision 0 3 Revision 0 3

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD contamination found to be present in secondary side systems and components, and unmonitored spills that drained to the discharge canal. In 1986, samples were taken from the legacy dredge spoils removed in 1979 dredged spoils area and from recently dredged canal sediment. The sample analyses indicated that the concentrations of Cs-137, Co-60 and other radionuclides were a small fraction of the DCGLs for those nuclides that could be identified by gamma spectroscopy. (refer to NE-86-RA-1142 dated 11-13-86). None the available historical information reviewed would support a conclusion that any residual activity in this survey unit is likely to be present at concentrations greater than the respective DCGLs.

Additional information was provided by several historical documents, including the "Results of Scoping Survey", (completed 9/1/98), the "Historical Site Assessment", and the HSA Supplement (dated 6-30-00). These documents presented the results of several sediment samples taken in 1997. These sample results indicated concentrations of 0.5 pCi/g for Co-60, 0.024 pCi/g for Cs-134 and 0.722 pCi/g for Cs-137.

An initial characterization survey was implemented during April and May of 2004. Six (6) samples from three (3) coring locations were obtained by biased sampling throughout the area. The samples were analyzed off-site by gamma spectroscopy and with radiochemical analyses for Sr-90 and Tritium.

Additional Hard-to-Detect (HTD) analyses were also conducted on one (1) of the six (6) samples.

For FSS, canal sediment sample collection methodology was achieved by producing one (1) thoroughly homogenized sample from each three (3) foot column of sediment obtained at each sampling location. However, the characterization sample collection process was performed in a slightly different manner that split the top six (6) inches of the column of sediment from the rest of the column of sediment and analyzed them separately. Additionally, only the top sample was analyzed for HTD nuclides. This process may have had the effect of high biasing the HTD sample results.

Based on the characterization data, the primary radionuclides of concern were determined to be Cesium-137, Cobalt-60 and Sr-90. Three (3) HTD nuclides (C-14, Ni-63 and Tc-99) were detected at slightly above the screening criteria but were deselected as radionuclides of concern because it is believed that the characterization data was high biased for HTDs and if the entire three (3) foot column of sediment was analyzed, the concentrations would have been below the screening criteria. Cobalt-60 accounted for the majority of the dose in these samples with a maximum concentration of 3.04 pCi/g.

A final Characterization was performed by Site Closure personnel in April and May of 2006 to obtain the necessary data of sufficient data quality for final status survey (FSS) planning purposes. A 3-foot core sediment sample was Revision 0 4

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD taken from each of the six (6) locations identified. All of the samples were analyzed by gamma spectroscopy. Since five (5) of the six (6) initial characterization results tested positive for Sr-90, it was included as a nuclide of concern. No additional HTD testing was performed for characterization purposes. However, four (4) of the fifteen (15) FSS samples collected were tested for HTD nuclides. The purpose of the increased level of HTD sample analysis was to ensure that all radionuclides of concern, for this survey unit, were properly identified. The only plant-related, dose significant radionuclides identified in the samples were Cesium-137, Cobalt-60 and Sr-90 (refer to Table 1).

Median: 1.20E-01 2.1 lE-01 6.77E-02 Standard Deviation: [ 6.76E-02 I .88E-01 4.25E-02 NOTE: The Operational DCGLs are 5.38 pCi/g for Cs-137, 2.59 pCi/g for Co-60 and 1.05 for Sr-90; these are used in conjunction with the unity rule to achieve 19 mrem/yr TEDE.

The FSS Engineer performed a visual inspection and walkdown during April 2006 to assess the physical condition of the survey unit, evaluate access points and travel paths and identify potentially hazardous conditions.

The final designation was Class 2 based on historical information and the characterization survey data which provided sufficient data to conclude that FSS sample results will be less than the seventeen (17) mrem/yr Operational DCGL (refer to Section 3).

3. DATA QUALITY OBJECTIVES (DQO)

FSS design and planning is based on the Data Quality Objective (DQO) process as described by the LTP, Procedure RPM 5.1-11, "Preparationof Final Status Survey Plan," and the "Multi-Agency Radiation Survey and Site Investigation Manual" (MARSSIM). A summary of the main features of the DQO process are provided herein.

The DQO process incorporates hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual Revision 0 5

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would satisfy the release criteria objective of the FSS.

The primary objective of the Final Status Survey Plan (FSSP) was to demonstrate that the level of residual radioactivity in Survey Unit 9106-0004 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of Derived Concentration Guideline Levels (DCGLs). The DCGLs represent the concentration of radioactivity above background, equivalent to a dose-based release criterion and is presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil (called Base Case Soil DCGL),

for existing groundwater radioactivity and for future groundwater radioactivity that will be contributed by building foundations and footings.

As described in detail in the LTP, the dose model applied to the discharge canal presumes that the canal sediments are dredged to a depth of three (3) feet below the top of the sediment layer and spread for the planting of crops per the Resident Farmer Scenario. Consequently, the soil DCGLs are directly applied to the canal sediment media The DCGLs presented in Chapter 6 of the LTP were developed for exposures from three (3) components, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity. Equation 1 shows the mathematical relationship between the three (3) components and the total dose.

Equation ]:

HTotal=Hsoil (sediment) + HExisting GW + HFuture GW The total dose under the LTP criteria is twenty-five (25) mrem/yr TEDE from all three (3) components. The allowable total dose under the Connecticut Department of Environmental Protection (CTDEP) radiological remediation standard for Connecticut Yankee (CY) is nineteen (19) mrem/yr TEDE. To satisfy both the LTP and CY CTDEP criteria, the dose from soil must be reduced when using the groundwater dose values discussed above.

This survey unit is affected by existing groundwater (reference CY memo ISC 06-024). The dose contribution from existing groundwater was determined not exceed two (2) mrem/yr TEDE.

Revision 0 6 Revision 0 6

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD This survey unit is not considered impacted by future groundwater radioactive contamination, as there are no concrete foundations or footings remaining within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contributions from future groundwater, the third component is, therefore, zero (0) mrem/yr TEDE.

Equation 2:

19 mrem/yrTotal 17 mrem/yrso1 +2 mrem/yrExisting GW+O mrem/yrFuture GW The allowable dose for soil in this survey unit is seventeen (17) mrem/yr TEDE as shown by Equation 2 above. The concentration of residual radioactivity resulting in seventeen (17) mrem/yr TEDE is designated as the Operational DCGL, and has been established for the radionuclides of concern as provided in Table 2 Note: The survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 to conservatively account for the contribution to the total dose from existing and future groundwater which had not been established at the time of planning the FSS.

Revision 0 7

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD C-14 5.66E+00 3.85E+00 2.26E-01 Mn-54 1.74E+01 I. 18E+OI 6.96E-01 Fe-55 2.74E+04 1.86E+04 1.1OE+03 Co-60 3.81E+00 2.59E+00 1.52E-01 Ni-63 7.23 E+02 4.92E+02 2.89E+O1 Sr-90 1.55E+00 1.05E+00 6.20E-02 Nb-94 7.12E+00 4.84E+00 2.85E-01 Tc-99 1.26E+01 8.57E+00 5.04E-01 Ag-108m 7.14E+00 4.86E+00 2.86E-0 I Cs-134 4.67E+00 3.18E+00 1.87E-01 Cs-137 7.91 E+00 5.38E+00 3.16E-0I Eu-152 1.01E+OI 6.87E+00 4.04E-0I Eu-154 9.29E+00 6.32E+00 3.72E-01 Eu-155 3.92E+02 2.67E+02 1.57E+01 Pu-238 2.96E+01 2.01E+O1 1.18E+00 Pu-239/240 2.67E+01 1.82E+01 1.07E+00 Pu-241 8.70E+02 5.92E+02 3.48E+OI Am-241

• 2.58 E+O1 1.75E+01 1.03E+00 Cm-243/244 2.90E+O1 1.97E+OI 1.16E+00 (1) Bold indicates those radionuclides considered to be Hard to Detect (HTD)

(2) The Base Case Soil DCGLs for soil are specified by the LTP in Chapter 6 and are equivalent to twenty-five (25) mrem/yr TEDE (3) The Operational DCGL is equivalent to seventeen (17) mrem/yr TEDE (4) The required MDC is equivalent to one (1) mrem/yr TEDE (5) Americium-241 can be analyzed by gamma and alpha spectroscopy and is considered to be Easy to Detect (ETD). The preferred result is the alpha spectroscopy's when both analyses are performed.

Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration variability. The Radiological data that was used to support the DQO process was provided by the characterization surveys performed in 2004 and 2006, as discussed in Section 2. Cs-137, Co-60 and Sr-90 were found to be the predominate radionuclides of concern. The basic statistical quantities (i.e., mean, standard deviation, median) for Cs-137, Co-60 and Sr-90 are provided in Table 1.

As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. Results reported as less than Minimum Revision 0 8 Revision 0 8

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Detectable Concentration (<MDC) were not accepted for FSS. Sample report summaries included unique sample identification, analytical method, radionuclide, result, and uncertainty to two (2) standard deviations, laboratory data qualifiers, units, and the required and observed MDC.

4. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in Procedure RPM 5.1-11, "Preparationof Final Status Survey Plans".

This survey was initially designed to 10 mrem/yr TEDE. At the time when the survey was designed, the dose contribution for existing and future groundwater had not yet been determined. Subsequently, a conservative value was chosen for the Operational DCGL. This approach is no longer required as the total dose from existing and future groundwater has been established. The dose for soil used for this survey unit to demonstrate compliance with the LTP criteria is seventeen (17) mrem/yr TEDE, as discussed in Section 2 of this Release Record.

The DQO process determined that Cs-137, Co-60 and Sr-90 were the radionuclides of concern (refer to Section 3). The sum of fractions, or unity rule, was used with the individual Operational DCGLs because multiple radionuclides (Cs-137, Co-60 and Sr-90) were considered in the survey design.

A common practice is to surrogate Sr-90, a HTD nuclide, to Cs-137 or another ETD nuclide. However, Sr-90 concentrations in sediment and soil, of this survey unit, were ascertained by direct analysis.

The Elevated Measurement Comparison (EMC) did not apply to this survey unit since the survey unit is a Class 2 and discrete, elevated areas of contamination were not expected.

The Sign Test was selected as the non-parametric statistical test to demonstrate that the null hypothesis was rejected. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. In addition, this approach is conservative since it includes background Cs-137 as part of the sample set.

The number of soil samples for FSS was determined in accordance with Procedure RPM 5.1-12, "Determination of the Number of Samples for Final Status Survey. " The Lower Bound of the Gray Region (LBGR) was set in accordance with Procedure RPM 5.1-11 to 0.714 to maintain the relative shift (A/o) in the range of 1 and 3. The resulting relative shift was 2.0. A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10 CFR 20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design.

Revision 0 9 Revision 0 9

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD This indicates that the survey unit has a high probability of rejecting the null hypothesis, assuming that the characterization data are representative of the FSS results. Survey design specified fifteen (15) sediment core samples for non-parametric statistical testing.

The grid pattern and locations of the soil samples were determined using Visual Sample Plan (VSP) in accordance with Procedure RPM 5.1-14, "Identifying, and Marking Surface Sample Locations for Final Status Survey. " Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy. A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate for a Class 2 area.

Sample locations were identified using AutoCAD-LT, a commercially available plotting software package with coordinates consistent with the Connecticut State Plane System. These coordinates were integrated with a GPS to locate sample locations in the field. Sample Measurement Locations for the design are listed with the GPS coordinates in Table 3.

Table 3 -Sml laurmn oain ýihAscae P Coordinates D

Aesi nation Y.Northing Eastina~)

9106-0004-001F 235796.96 670148.53 9106-0004-002F 235796.96 670237.74 9106-0004-003 F 235796.96 670326.96 9106-0004-004F 235796.96 670416.17 9106-0004-005F 235796.96 670505.39 9106-0004-006F 235796.96 670594.60 9106-0004-007F 235796.96 670683.81 9106-0004-008F 235719.70 670103.92 9106-0004-009F 235719.70 670193.14 9106-0004-01 OF 235719.70 670549.99 9106-0004-01 IF 235719.70 670639.21 9106-0004-012F 235719.70 670728.42 9106-0004-013F 235719.70 670817.63 9106-0004-014F 235642.44 670773.03 9106-0004-015 F 235642.44 670862.24 Five (5) sediment samples were analyzed for the full suite of radionuclides specified in Table 1, exceeding the requirement to analyze 5% of the sample population for HTD analysis specified in procedure RPM 5.1-11.

The implementation of quality control measures as referenced by Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey, " included the collection of two (2) soil samples for "split sample" analysis by the off-site laboratory. These locations were selected randomly using the Microsoft Excel Revision 0 10 Revision 0 10

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD "RAND" function. The number of quality control samples exceeded the 5%

requirement.

The LTP specifies that scanning is not required for the FSS of the Discharge Canal. Table 4 provides a synopsis of the survey design.

Survey Unit Based on AutoCAD-LT and Visual 9,900 m2 Land Area Sample Plan calculations Type I and Type 2 errors were 0.05, Number of 15 sigma was 0.143 the LBGR was set to Measurements 0.714 to maintain Relative Shift in the range of 1 and 3, Relative Shift was 2.0 Grid Spacing 27.61 m Based on triangular grid 3.16 pCi/g Cs-137 Design DCGL 1.52 pCi/g Co-60 To achieve 10 mrem/yr TEDE 0.62 pCi/g Sr-90 Operational 5.38 pCi/g Cs-137 To achieve 17 mrem/yr DCGL 2.59 pCi/g Co-60 TEDE (2)to demonstrate compliance with 1.05 pCi/g Sr-90 Equation 2 of this Release Record Scan Coverage N/A The LTP exempts this area Sediment 5.38 pCi/g Cs-137 The Operational DCGL meets the LTP Investigation 2.59 pCi/g Co-60 criteria for a Class 2 survey unit Level 1.05 pCi/g Sr-90 (1) The survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 as the total dose from existing and future groundwater had not been established at the time of planning the FSS (2) The allowable dose for soil in this survey unit is 17 mrem/yr TEDE as the total dose from existing and future groundwater has been established (reference CY memo ISC 06-024)

5. SURVEY IMPLEMENTATION Final Status Survey field activities were conducted under Work Plan and Inspection Record (WP&IR) 2006-0021. The WP&IR package included a detailed FSSP, job safety analysis, job planning checklist and related procedures for reference. Daily briefings were conducted to discuss the expectations for job performance and the safety aspects of the survey. The "Daily Survey Journal" was used to document field activities and other information pertaining to the FSS.

Measurement locations were identified in North American Datum (NAD) 1927 coordinates that were supplied to the sampling vendor, Ocean Survey, Inc.

(OSI) of Old Saybrook, Connecticut. Discharge Canal sampling was accomplished using direct push technology to collect composite samples of Revision 0 I1I Revision 0 11

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD bottom and mean high water mark sediments. Sediment cores from the Discharge Canal were obtained by OSI using a vibrating corer that is platform mounted on a sampling vessel. The core barrel was a three (3) inch diameter thin-walled aluminum tube, approximately ten (10) feet long, which also served as a core liner. A core catcher was available to prevent the sample from sliding out of the bottom of the tube. Vessel positioning and the determination of sample locations were accomplished using a GPS interfaced with a navigation and data logging system.

After extraction, water was drained by drilling holes above the sediment column which would constitute the sample. The liner was cut, capped, sealed, labeled and turned over from the Ocean Surveys, Inc. to site personnel who processed and controlled each sample with a Chain-of-Custody (COC).

Rinsing of the barrel and associated equipment was performed between sampling events. New aluminum tubes were used for each sample to prevent cross-contamination of subsequent samples.

The fifteen (15) sediment samples were collected and packaged in accordance with Haddam Neck Plant (HNP) Procedure RPM 5.1-3, "Collection of Sample Mediafor Final Status Survey" and FSS design. Samples were controlled, transported, stored, and transferred to the off-site laboratory using COC protocols.

Five (5) samples (9106-0004-OOF, 9106-0004-005F, 9106-0004-013F, 9106-0004-014F and 9106-0004-015F) were selected for HTD radionuclide analysis by the off-site laboratory.

The implementation of survey specific quality control measures included the collection of two (2) split samples at locations 9106-0004-004F and 9106-0004-01 OF for "split sample" analysis by the off-site laboratory.

6. SURVEY RESULTS The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories (GEL) - Charleston, South Carolina. The laboratory analyzed the fifteen (15) samples taken for non-parametric statistical testing and the associated duplicates using gamma spectroscopy. Sr-90 was analyzed by gas flow proportional counting. All analyses were performed to the required MDC.

Cesium-137 was identified in thirteen (13), Co-60 was identified in fourteen (14) and Sr-90 in two (2) of the fifteen (15) samples.

Additionally, C-14 was positively identified (i.e., a result greater than two (2) standard deviations uncertainty) in all five (5) samples analyzed for HTD radionuclides and could not be de-selected or excluded using the 5% and 10%

rule described in Section 5.4.7.2 of the LTP. Several other radionuclides which Revision 0 12 Revision 0 12

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD were positively identified (i.e., a result greater than two (2) standard deviations uncertainty) could' be de-selected or excluded using the 5% and 10% rule described in Section 5.4.7.2 of the LTP.

None of the samples exceeded the Operational DCGL. A summary of the sample results is provided in Table 5.

9106-0004-003 F 3.55E-01 9.45E-01 1.62E-02 0.431 0.507 9106-0004-004F 1.59E-01 2.63E-01 -7.59E-03 0.131 0.185 9106-0004-005F 3.99E-0I 1.74E+00 5.86E-03 0.746 0.842 9106-0004-006F 1.12E-01 2.23E-01 1.OIE-02 0.107 0.177 9106-0004-007F -5.61E-03 1.16E-03 -6.09E-03 -0.001 0:055 9106-0004-008F 1.55E-01 2.56E-01 2.62E-02 0.128 0.214 9106-0004-009F 2.09E-02 0.OOE+00 2.16E-02 0.004 0.085, 9106-0004-01 OF 2.46E-03 7.39E-03 -1.75E-03 0.003 0.063 9106-0004-011F 2.12E-01 3.66E-01 9.13E-04 0.181 0.242 9106-0004-012F 1.59E-01 1.37E-01 -1.72E-03 0.082 0.142 9106-0004-013F 5.49E-01 1.81E+00 3.01E-03 0.801 0.873 9106-0004-014F -7.91E-03 2.85E-02 8.27E-03 0.010 0.052 9106-0004-015F 3.77E-01 7.44E-01 -1.53E-03 0.357 0.396 (1) The Operational DCGLs from Table 2 are 5.38 pCi/g for Cs-137, 2.59 pCi/g for Co-60 and 1.05 for Sr-90; these are used in conjunction with the unity rule to achieve 17 mrem/yr TEDE (2) This column is the sum of the DCGL unity fraction from identified radionuclides of concern and HTD isotope (C-14) exceeding the 5%/10% rule for one or more FSS samples. For those samples not measured for HTD isotopes, an average calculated value of 6.1% of the DCGL was added to each sample.

The off-site laboratory also processed five (5) samples for HTD analysis as required by the sample plan. The requested analyses included alpha spectroscopy, gas proportional counting, and liquid scintillation depending on the radionuclide and the measurement method. All analyses met the required MDC. Five (5) of the HTD radionuclides met the accepted criteria for detection (i.e., a result greater than two standard deviations uncertainty) in more than one (1) sample. Each of the positive results for HTD radionuclides could be de-selected based on the 5% and 10% rules, except for C-14. These results are presented in Table 6.

Revision 0 13

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Table 6-Hard-t et'ec't SampleI esults~

Sample .. . Numbher C-14 4iaction Fr~ of the

..........

. .......

.......*  : ... ; *

• I * * * **  !: O pg..ra tio n a l D C L ....

9106-0004-001F 0.268 0.0696 9106-0004-005F 0.347 0.0902 9106-0004-013F 0.267 0.0694 9106-0004-014F 0.134 0.0348 9106-0004-015F 0.156 0.0405 (1) The Operational DCGL from Table 2 is 3.85 pCi/g for C-14.

A biased sample location called for in the sample plan the (sample point 9106-0004-016F was found to be located on dry land. This point was replaced with a randomly generated sample point 9106-0004-17F. For completeness this sample result is presented in the Table below.

Table 7 -Additional Sam le Result SueNubr Cs-137 Co>> Sr9 raction ofthe 9106-0004-01 7F 3.78E-01 2.94E-01 3.46E-02 0.184 (1) The Operational DCGLs from Table 2 are 5.38 pCi/g for Cs-137, 2.59 pCi/g for Co-60 and 1.05 pCi/g for Sr-90; these are used in conjunction with the unity rule to achieve 17 mrem/yr TEDE

7. QUALITY CONTROL The off-site laboratory processed the split samples and performed gamma spectroscopy analysis. Two (2) of the samples were selected for analysis, which exceeds the 5% minimum required by the LTP. The data were evaluated using USNRC acceptance criteria specified in Inspection Procedure 84750 and as detailed in 1-NP Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey. " For one of the split-sample comparisons, Co-60 was found to not meet the comparison criterion; however this nuclide may be present in particulate form which is not necessarily an indicator of a non-homogenous mixing of the soil matrix. K-40, a natural radioisotope, was found to be present at an acceptable level of agreement, so the comparison was deemed acceptable.

There was acceptable agreement between the field split results for both of the "split sample" pairs tested.

GEL, the sample analysis vendor, maintained quality control and quality assurance plans as part of normal operation. Refer to Attachment 2 for data and data quality analysis results.

8. INVESTIGATIONS AND RESULTS Two (2) sample results were found to exceed the Design DCGL of ten (10) mrem/yr, but were below the seventeen (17) mrem/yr Operational DCGL, as specified in Table 4. Confirmatory samples were collected to determine the extent of contamination. The extent was bounded by taking four (4)

Revision 0 14

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD confirmatory samples, one in each compass direction, two (2) meters distant from the elevated sample location. The results are included in Table 8.

005F 005C I 1.13E-01 [ 2.68E-01 I 8.20E-03 1 0.132

'005D 5.03 E-01 1.72E+00 -3.22E-03 0.754 013A -1.13E-03 -5.69E-03 -3.31E-03 -0.006 013B 8.31E-02 1.96E-01 2.21E-03 0.093 013F 013C 7.89E-02 7.40E-02 -1.57E-03 0.042 013D 1.70E-01 5.66E-01 7.38E-03 0.257 (1) The Operational DCGLs from Table 2 are 5.38 pCi/g for Cs-137, 2.59 pCi/g for Co-60 and 1.05 pCi/g for Sr-90; these are used in conjunction with the unity rule to achieve seventeen (17) mrem/yr TEDE.

The confirmatory results demonstrate that no measurements exceed the 17 mrem/yr operational DCGL, indicating that no further actions are warranted.

9. REMEDIATION AND RESULTS Historically, no radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to or as a result of the FSS. Health Physics TSD BCY-HP-0078, "ALARA Evaluation of Soil Remediation in Support of Final Status Survey, " determined that remediation beyond that required to meet the release criteria to be unnecessary and that the remaining residual radioactivity in soil was ALARA.

10. CHANGES FROM THE FINAL STATUS SURVEY PLAN The survey was designed to ten (10) mrem/yr TEDE which was conservative and necessary at the time of FSS planning. It is no longer required as the total dose from existing and future groundwater has been established. The dose for soil used to demonstrate compliance with the LTP criteria is seventeen (17) mrem/yr TEDE as discussed in Section 2 of this Release Record.

Revision 0 15 Revision 0 15

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD

11. DATA QUALITY ASSESSMENT (DQA)

The DQO sample design and data were reviewed in accordance with Procedure RPM 5.1-23, "Data Quality Assessment, " for completeness and consistency.

The sampling design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The Sign Test shows that the survey unit passes FSS.

Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 2.

The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). The sample standard deviation was slightly more than the value used for the survey design. This is represented by the shift in the retrospective power curve as shown in Attachment 2g. This would indicate a change to the original LBGR to maintain the number of samples at fifteen (15) to meet the Operational DCGL. However, the value of LBGR is less of a critical issue as the survey unit has passed the statistical test, and the mean and median values are well below the Operational DCGL when used in conjunction with the unity rule. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the release criteria with adequate power as required by the DQOs.

The range of the data, about 3.02 standard deviations, was not unusually large.

The difference between the mean and median was 42.5% of the standard deviation which indicates some skewness in the data. The data was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot shows some positive skewness as confirmed by the calculated skew of 1.23.

All data, assessments, and graphical representations are provided in Attachment 2.

12. ANOMALIES The finding of C-14 in excess of the screening criteria was the only anomaly associated with the FSS of this survey unit. For conservatism, the C-14 results were factored into all statistical evaluations of the survey data for this survey unit accounting for any possible dose contributions. This action does not alter the conclusion that this survey unit meets the criteria for unconditional release.

13. CONCLUSION Survey Unit 9106-0004 has met the final DQOs of the FSS. The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved. Elevated Measurement Comparison and remediation was not required.

Revision 0 16

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD The sample data passed the Sign Test. The null hypothesis was rejected.

Graphical representation of data indicates some positive skewness that is probably due to localized differences in particulate deposition rates, hydraulic velocity and sedimentation rates. The Retrospective Power Curve generated using COMPASS shows adequate power was achieved. The survey unit was properly designated as Class 2.

The dose contribution from soil is 5.1 mrem/yr TEDE based on the average concentration of the samples used for non-parametric statistical sampling.

This survey unit is affected by existing groundwater (reference CY memo ISC 06-024 and the Final Status Survey Final Report Phase IV). It has been determined that the dose contribution from groundwater sources will not exceed two (2) mrem/yr TEDE.

This survey unit is not considered impacted by future groundwater radioactive contamination, as there are no concrete foundations or footings containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component, is therefore zero (0) mrem/yr TEDE.

The average total dose from residual radioactivity in this survey unit, including present ground water and sediment, will not exceed 7.1 mrem/yr Total Effective Dose Equivalent (TEDE).

14. ATTACHMENTS 14.1 Attachment 1 - Figures 14.2 Attachment 2 - Sample and Statistical Data Revision 0 17 Revision 0 17

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Attachment 1 Figures (5 pages)

/ V--

I 'y

!

/J 44 Lllýt r7 Connecticut Yankee Atomic Power Company Site Map With Reference To Survey Unit 9106-0004

13D 12 Sample Lomton q~ Pond Connecticut Yankee Atomic PowerCompany 9106-0004FinalStatus Survey Sample Locations

,f.

1

.0159

'f Pond 0 30 60 IFeet NOTE.

Cesium-137 zwudts am gim inpcil*

Connecticut Yankee Atomic Power Company 9106-0004 FinalStatus Survey Cesium-137 Postinz Plot

K Sample Loation V% Pond NOTE.

Cobalt-60 7ewudty am given hpin k

$

sample Locaton

'V Pond 0 30 60 NOTE.

stzvntm-90 resufs am given inpMi9 9106-0004 Fina Strontium-90

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Attachment 2 Sample and Statistical Data

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Attachment 2a Sample Data (292 Pages)

Table of Contents General Narrative .................................................................. I Chain of Custody and Supporting Documentation ........... 4 Radiological Analysis ......................................................... 12 Sample Data Summary ...................................................... 31 Q uality C ontrol D ata .......................................................... 71

General Narrative 1

CASE NARRATIVE For CONNECTICUT YANKEE RE: Sediment PO# 002332 Work Order: 162832 SDG: MSR #06-0688 June 7, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shippin2 Address:

2040 Savage Road Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina on May 12, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures except the sample container for sample 9106-0004-014F was received leaking. A Safety Technician contained the leak and salvaged the sample successfully. No other samples were affected. Analyses were conducted as normal.

The laboratory received the following sample(s):

Sample ID Client Sample ID 162832001 9106-0004-008F 162832002 9106-0004-009F 162832003 9106-0004-OIOF 162832004 9106-0004-O1OFS 162832005 9106-0004-01 IF 162832006 9106-0004-012F 162832007 9106-0004-013F 162832008 9106-0004-014F GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

PO. Box 30712 . Charleston, SC 29417 - 2040 Savage Road (29407)

Phone (843) 556-8171

• Fqý (843) 766-1178

• www.gel.com

Sample ID Client Sample ID 162832009 9106-0004-015F 162832010 9106-0004-OOIF 162832011 9106-0004-002F 162832012 9106-0004-003F 162832013 9106-0004-004F 162832014 9106-0004-004FS 162832015 9106-0004-005F 162832016 9106-0004-006F 162832017 9106-0004-007F 162832018 9106-0004-017F Items of Note:

There were no items of note.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.

Analytical Request:

Sixteen sediment samples were analyzed for FSSGAM and Sr-90.

Two sediment samples were analyzed for FSSALL.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

P.O. Box 30712

• Charleston, SC 29417 - 2040 Savage Road (29407)

Phone (843) 556-8171 - Fai (843) 766-1178 ° www.gel.com

Chain of Custody and Supporting Documentation 4

H. - Pt

• . Health Physips Prp~dure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connfctkut Yankee Atomic Power Company i362 Ijun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: HaddamNeck Decommissioning Contact Name & Phone:

Jack McCarthy - 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D.[] 14D.EI7D.

Ln Samples Shipped Via:

2 Fed Ex El uPs El Hand El Other Bill of Lading #

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06624 860-267-2556 Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D.E] 14 D. [] 7 D.

Samples Shipped Via:

[ Fed Ex El UPS

[] Hand El Other Bill of Lading #

Connecticut Yankee Statement of Work for Analytical Lab Services , CY-ISC-SOW-00 Figure 1. Sample Check-in List.

Date/Time Received: A 'Aw 0 OQ, SDG#:0 Work Order Number: "-V3Y? -.

Shipping Cditainer ID:., Chain of Custody# - 33-4 I. Custody Seals on'shipping container intact?.-

Yes [ No

2. Custody Seals dated and signed?

Yes [ No 64,

3. Chain-of-Custody record present?

Yes  ? No [I

4. Cooler temperature I C .,

5. Vermiculite/packing materials is: - Wet F,/)Dry (, k 6,* Number of samples in shipping container _

7. Sample holding times exceeded? Yes No

.8. Samples have*

• tape -hazard labels

_.. custody seals ----__.appropriate sample labels

9. Samples are'

.n good conditin...dekn o n  : , . .

• .

- broken - have air bubbles

10. Were any anomalies identified in sample receipt?

Yes No

• IL. :1. Description

.Descrption of.anomalies (include sample numbers):,.

..... "ie5Q ii\-J 3 ,_IL i O0 --

Sample Custodian/Laboratory:C j ~ ~ D te ~

Telephoned to:__ _ _ _ _ _ _ O-n By '

.7

,SAMPLE le 4S RECEIPT & REVIEW FORM o*I*rotR " yPM use only Client: i~ eV DGIARCOC) Work Order: /(L 32-D;ate Received: C5- jai I JPM(A) Review rewocn(lm ame resolved prior to siging):

Received By: (j i-e~v fi J ( A),GwLj Sample Receipt Criteria Comments/Qualifiers (Required for Non-Conforming Items)

Circle Applicable: seals broken damaged container leaking container other (describe)

Shipping containers received intact Iand sealed?

Samples requiring cold Circle Coolant # ice bags blue ice dry ice other describe) 2 preservation within (4 +/- 2 C)?

Record preservation method. I"

• Chain of custody documents CVO -S C0-b Ur included with shipment?

co-tai"e, Sample containers intact and irckCAppcablc; =15 broe danaged conai leaking conainer (odtescie sealed? - - C-M#I?- "lq- ) gq.c '

Samples requiring chemical Sample ID's. containers affected and observed pH: aFYIZ_

preservation at proper pH? - -..

VOA vials free of headspace Sample ID's and cotnainers affected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) lid's and tests affected:

8 Samples received within holding time?

Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles? _,

Date & time on COC match' date Sample ID's affected:

& time on bottles?

Number of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in no C0365 CU'L('. .LYLU i s'Uks d relinquished/rcceived sections?

?EcA- 4%-- I Air Bill ,Tracking #'s, &

Additiona1 Comments SUI T RSO RAD Receipt _

• If > x2 area background is observed on samples identified as "non-Suspected Hazard Information to =Do r -c regulated/non-radioactive", contact the Radiation Safety group for further I investigation.

Aadiological Classification? Maximum Counts Observed*:

B IPCB Regulated? Comments:

Shipped as DOIT Hazardous C jMaterial? If yes, contact Waste i Hazard Class Shipped:

[Manager or ESH Manager. I UN#:

PM (or PMA) review of Hazard classitication: Initials Date:

Y 8

k9~ SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM pIr- q(C4p~o vf 5~lyf(

- U~pI oYLW33) (

- - (2 , 6 1 0a30 ( ") "iVl 4hi5, ce(!o'e had c,. " _"__

"-L,,meLI ________________

LJ Uc", I r dI U-fe _-

9

SAMPLE RECEIPT & REVIEW FORM PM one oly IClient: (>< ya,,& , SDG/ARCOClWork Order: / Z*3 signing):

,,

, i- . PM(A) Review (ensure non-conforming items are resolved prior to Date Received: R e ( /A)l n n R eceived By: e- .-

Sample Receipt Criteria >4 t , Comments/Qualifiers (Required for Non-Conforming Items) container other (describe)

Circle Applicable: seals broken damaged container leaking 1 Shipping containers received intact and sealed? I blue ice dry ice none other describe)

Samples requiring cold Circle Coolant # ice bags 2 preservation within (4 +/- 2 C)?

.Recordpreservation method.

Chain of custody documents included with shipment? ____

4 Sample containers intact and Circle Applicable: seals broken damaged container le oaino other (describe) sealed? J '6,q)  :" 0 (oe- 0oo0j-o 'a1 "

5 Samples requiring chemical Sample ID's, containers affected and observed pH:

.preservation at proper pH?

VOA vials free of headspace Sample ID's and containers affected:

6 (defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) _

8 Samples received within holding Id's and tests affected:

time? __1 9 Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles? ___

10 Date & time on COC match date Sample ID's affected:

& time on bottles? __ll Number of containers received 1 Sample 's affected:

. match number indicated on COC?

12 COC form is properly signed in

. relinquished/received sections? X 1 40 . A_

A-. rd 14 Air Bill ,Tracking #'s, & - .. f tyL . . -AJ *e ,A .

Additional Comments

" ~~ ~P "U ' PORAD R§"- Receipt #..*'-

Suspecte~d-.ad formation  :- -t *f f> x2 area background is observed on samples identified as ,on-S f *2p regulated/non-radioactive", contact the Radiation Safety group for further

"____"____"______ _ * !investigation.

SRadiologia Classifation? -Maximum Counts Observed*: /*

7]PCB Regulated? comments:

! S-ipil as DO'Y.Hazardous C Material? if yes, contact Waste Hazard Cla Shipped:

Manager or ESH Manager. UN#:

PM (or PMA) review of Hazard classification: Initials 6141 Date:

10 U

Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Chcck-in List 114 - ,,220 DateF/imc Received: .Y- i/?. 0 (, I SDG#: /14 tO0(,,- O0(,R e Work Order Number: '/-*32

'

Shipping Container ID: "lq S 315" 887Z Chain of Custody # ID 06 0T3 1

1. Custody Seals on shipping container intact? Yes j No []

2. Custody Seals dated and signed? Yes No [

3. Chain-of-Custody record present? Yes No []

4. Cooler temperature A1/4 I

5. Vermiculite/packing materials is: Wet J Dry []

6. Number of samples in shipping container:

7. Sample holding times exceeded? Yes [] No I

8. Samples have:

j( tape hazard labels

_ custody seals appropriate sample labels

9. Samples are:

____in good condition _ leaking broken _ have air bubbles

10. Were any anomalies identified in sample receipt? Yes No [ ]

11. Description of anomalies (include sample numbers):

Sample Custodian/Laboratory: *t Date: ,-1.*' a. 6 'd's :,.*vn

'7. ."* -

On B Telephoned to:

Page 45 of 56 11

RADIOLOGICAL ANALYSIS 12

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 162832 Method/Analysis Information Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 533471 Prep Batch Number: 529742 Dry Soil Prep GL-RAD-A-021 Batch Number: 529741 Sample ID Client ID 162832008 9106-0004-014F 162832010 9106-0004-001F 1201101117 Method Blank (MB) 1201101118 162485017(9106-0005-005F) Sample Duplicate (DUP) 1201101119 162485017(9106-0005-005F) Matrix Spike (MS) 1201101120 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

13

Ouality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162485017 (9106-0005-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information 14

Product: Alphaspec Pu, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- 11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 533472 Prep Batch Number: 529742 Dry Soil Prep GL-RAD-A-021 Batch Number: 529741 Sample ID Client ID 162832008 9106-0004-014F 162832010 9106-0004-001F 1201101121 Method Blank (MB) 1201101122 162485017(9106-0005-005F) Sample Duplicate (DUP) 1201101123 162485017(9106-0005-005F) Matrix Spike (MS) 1201101124 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (OC Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162485017 (9106-0005-005F).

QC Information All of the QC samples met the required acceptance limits.

15

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu-1i -RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 533473 Prep Batch Number: 529742 Dry Soil Prep GL-RAD-A-021 Batch Number: 529741 16

Sample ID Client ID 162832008 9106-0004-014F 162832010 9106-0004-0OIF 1201101125 Method Blank (MB) 1201101126 162485017(9106-0005-005F) Sample Duplicate (DUP) 1201101127 162485017(9106-0005-005F) Matrix Spike (MS) 1201101128 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162485017 (9106-0005-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis The tracer yield for sample 1201101127 (9106-0005-005F) was recounted due to poor resolution.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from 17

referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Gamma,Solid-FSS GAM & ALL FSS Analytical Method: EML HASL 300, 4.5.2.3 Prep Method: Dry Soil Prep Analytical Batch Number: 529778 Prep Batch Number: 529741 Sample ID Client ID 162832001 9106-0004-008F 162832002 9106-0004-009F 162832003 9106-0004-OIOF 162832004 9106-0004-01OFS 162832005 9106-0004-01 IF 162832006 9106-0004-012F 162832007 9106-0004-013F 162832008 9106-0004-014F 162832009 9106-0004-015F 162832010 9106-0004-001F 162832011 9106-0004-002F 162832012 9106-0004-003F 162832013 9106-0004-004F 162832014 9106-0004-004FS 162832015 9106-0004-005F 162832016 9106-0004-006F 162832017 9106-0004-007F 162832018 9106-0004-017F 1201092338 Method Blank (MB) 1201092339 162832001(9106-0004-008F) Sample Duplicate (DUP) 1201092340 Laboratory Control Sample (LCS) 18

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 11.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162832001 (9106-0004-008F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

19

Qualifier information Qualifier Reason Analyte Sample Data rejected due to high Full-Width Cobalt-60 162832002 UI Half-Maximum.

Manganese-54 162832017 UI Data rejected due to high counting uncertainty. Americium-241 162832010 Lead-212 1201092338 UI Data rejected due to interference. Manganese-54 162832001 UI Data rejected due to low abundance. Cesium- 134 162832002 162832003 162832004 162832006 162832007 162832012 162832013 162832015 162832016 162832017 162832018 1201092339 Method/Analysis Information 20

Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified

'Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 534448 Prep Batch Number: 529742 Dry Soil Prep GL-RAD-A-021 Batch Number: 529741 Sample ID Client ID 162832001 9106-0004-008F 162832002 9106-0004-009F 162832003 9106-0004-01OF 162832004 9106-0004-O1OFS 162832005 9106-0004-01 IF 162832006 9106-0004-012F 162832007 9106-0004-013F 162832008 9106-0004-014F 162832009 9106-0004-015F 162832010 9106-0004-001F 162832011 9106-0004-002F 162832012 9106-0004-003F 162832013 9106-0004-004F 162832014 9106-0004-004FS 162832015 9106-0004-005F 162832016 9106-0004-006F 162832017 9106-0004-007F 162832018 9106-0004-017F 1201103434 Method Blank (MB) 1201103435 162832001(9106-0004-008F) Sample Duplicate (DUP) 1201103436 162832001(9106-0004-008F) Matrix Spike (MS) 1201103437 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 10.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

21

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (Q) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162832001 (9106-0004-008F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 162832008 (9106-0004-014F) was recounted due to high MDA.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information 22

Product: Liquid Scint Tc99, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 531704 Sample ID Client ID 162832008 9106-0004-014F 162832010 9106-0004-001F 1201096867 Method Blank (MB) 1201096868 162583001(NOL-02-02-005-F-S) Sample Duplicate (DUP) 1201096869 162583001(NOL-02-02-005-F-S) Matrix Spike (MS) 1201096870 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 13.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162583001 (NOL-02-02-005-F-S).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

23

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 531618 Prep Batch Number: 529742 Dry Soil Prep GL-RAD-A-021 Batch Number: 529741 Sample ID Client ID 162832008 9106-0004-014F 162832010 9106-0004-001F 1201096631 Method Blank (MB) 1201096632 163173001 (9304-0000-063RACR) Sample Duplicate (DUP) 1201096633 163173001 (9304-0000-063RACR) Matrix Spike (MS) 1201096634 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.

24

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before, the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (Q) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163173001 (9304-0000-063RACR).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information 25

Product: Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 531622 Prep Batch Number: 529742 Dry Soil Prep GL-RAD-A-021 Batch Number: 529741 Sample ID Client ID 162832008 9106-0004-014F 162832010 9106-0004-001F 1201096644 Method Blank (MB) 1201096645 163173001 (9304-0000-063RACR) Sample Duplicate (DUP) 1201096646 163173001 (9304-0000-063RACR) Matrix Spike (MS) 1201096647 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (00 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163173001 (9304-0000-063RACR).

QC Information All of the QC samples met the required acceptance limits.

26

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: LSC, Tritium Dist, Solid - 1 to 2 pCi/g Analytical Method: EPA 906.0 Modified Analytical Batch Number: 531705 Sample ID Client ID 162832008 9106-0004-014F 162832010 9106-0004-001F 1201096877 Method Blank (MB) 1201096878 162583001 (NOL-02-02-005-F-S) Sample Duplicate (DUP) 1201096879 162583001 (NOL-02-02-005-F-S) Matrix Spike (MS) 1201096880 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 11.

27

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162583001 (NOL-02-02-005-F-S).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 1201096877 (MB) and 162832008 (9106-0004-014F) were recounted due to high MDAs.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information 28

Product: Liquid Scint C14, Solid AII,FSS Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 534984 Sample ID Client ID 162832008 9106-0004-014F 162832010 9106-0004-001F 1201104745 Method Blank (MB) 1201104746 163173001 (9304-0000-063RACR) Sample Duplicate (DUP) 1201104747 163173001 (9304-0000-063RACR) Matrix Spike (MS) 1201104748 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (Q0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163173001 (9304-0000-063RACR).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

29

Sample Re-prep/Re-analysis Samples were reprepped due to low/high recovery.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

Reviewer/Date:

30

SAMPLE DATA

SUMMARY

31

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOO 1 Connecticut Yankee Atomic Power Co.

Client SDG: MSR#06-0688 GEL Work Order: 162832 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the reporting limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by 32

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage .Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis cT.. t . o. ..... i s--

C et.. if..

Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-008F Project: YANKO 1204 Sample ID: 162832001 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 19.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.655 +/-0.137 0.0451 +/-0.137 0.0962 pCi/g MJH1 06/06/06 1727 529778 1 Americium-241 U 0.0325 +/-0.0823 0.0746 +/-0.0823 0.154 pCi/g Bismuth-212 0.551 +/-0.165 0.115 +/-0.165 0.241 pCi/g Bismuth-214 0.447 +/-0.0787 0.0262 +/-0.0787 0.0549 pCi/g Cesium-134 U 0.0255 +/-0.0237 0.017 +/-0.0237 0.0357 pCi/g Cesium-137 0.155 +/-0.0273 0.0123 +/-0.0273 0.026 pCi/g Cobalt-60 0.256 +/-0.046 0.0129 +/-0.046 0.028 pCi/g Europium-152 U 0.0135 +/-0.0376 0.0314 +/-0.0376 0.0656 pCi/g Europium-154 U 0.000575 +/-0.048 0.0407 +/-0.048 0.0876 pCi/g Europium-155 U 0.015 +/-0.0405 0.039 +1-0.0405 0.0803 pCi/g Lead-212 0.609 +/-0.0665 0.0195 +/-0.0665 0.0403 pCi/g Lead-214 0.566 +/-0.0835 0.0228 +/-0.0835 0.0476 pCi/g Manganese-54 UU1 0.00 +/-0.0194 0.0125 +/-0.0194 0.0266 pCi/g Niobium-94 U 0.00427 +/-0.0141 0.0123 +/-0.0141 0.026 pCi/g Potassium-40 10.8 +/-0.957 0.125 +/-0.957 0.272 pCi/g Radium-226 0.447 +/-0.0787 0.0262 +/-0.0787 0.0549 pCi/g Silver-108m U 0.00155 +/-0.0131 0.0119 +/-0.0131 0.0249 pCi/g Thallium-208 0.194 +/-0.042 0.013 +/-0.042 0.0274 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.0262 +/-0.0216 0.0193 +/-0.0217 0.0428 pCi/g BXF1 06/02/06 1547 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 33

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-008F Project: YANK01204 Sample ID: 162832001 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 33 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

34

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-009F Proiect:. YANK01204 Sample ID: 162832002 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 10.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.02 +/-0.127 0.0487 +/-0.127 0.104 pCi/g MJHl 06/06/06 1727 529778 1 Americium-241 U -0.0652 +/-0.121 0.073 +/-0.121 0.149 pCi/g Bismuth-212 0.802 +/-0.219 0.116 +/-0.219 0.244 pCi/g Bismuth-214 0.765 +/-0.0817 0.0269 +/-0.0817 0.0565 pCi/g Cesium-134 UUI 0.00 +/-0.0222 0.0212 +/-0.0222 0.0443 pCi/g Cesium-137 U 0.0209 +/-0.0277 0.0169 +/-0.0277 0.0353 pCi/g Cobalt-60 UUI 0.00 +/-0.0245 0.0151 +/-0.0245 0.0326 pCi/g Europium-152 U 0.0221 +/-0.0473 0.0425 +/-0.0473 0.0879 pCi/g Europium-154 U 0.0603 +/-0.0585 0.0478 +/-0.0585 0.102 pCi/g Europium-t55 U 0.0136 +/-0.0533 0.0506 +/-0.0533 0.104 pCi/g Lead-212 1.00 +/-0.0543 0.0256 +/-0.0543 0.0527 pCi/g Lead-214 0.967 +/-0.0836 0.0302 +/-0.0836 0.0626 pCi/g Manganese-54 U 0.0255 +/-0.0272 0.0152 +/-0.0272 0.0321 pCi/g Niobium-94 U 0.00406 +/-0.0156 0.014 +/-0.0156 0.0293 pCi/g Potassium-40 8.59 +/-0.636 0.105 +/-0.636 0.234 pCi/g Radium-226 0.765 +/-0.0817 0.0269 +/-0.0817 0.0565 pCi/g Silver-108m U-( 0.000766 +1-0.0155 0.0134 +1-0.0155 0.0279 pCi/g Thallium-208 0.355 +/-0.043 0.0138 +/-0.043 0.029 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.0216 +/-0.0169 0.0151 +/-0.0169 0.0333 pCi/g BXF1 06/02/06 1547 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 35

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-009F Project: YANKO 1204 Sample ID: 162832002 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 42 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

36

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-01OF Proiect: YANK01204 Sample ID: 162832003 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 12.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.983 +/-0.148 0.0597 +/-0.148 0.127 pCi/g MJHI 06/06/06 1727 529778 I Americium-241 U -0.00252 +/-0.0227 0.020 +/-0.0227 0.0411 pCi/g Bismuth-212 0.538 +/-0.237 0.122 +/-0.237 0.259 pCi/g Bismuth-214 0.627 +/-0.0778 0.0322 +/-0.0778 0.0675 pCi/g Cesium-134 UI 0.0529 +/-0.0292 0.0232 +/-0.0292 0.0486 pCi/g Cesium-137 U 0.00246 +/-0.0235 0.0177 +/-0.0235 0.0373 pCi/g Cobalt-60 U 0.00739 +/-0.0239 0.0204 +/-0.0239 0.0439 pCi/g Europium-152 U -0.0137 +/-0.044 0.0365 +/-0.044 0.0765 pCi/g Europium-154 U -0.0489 +/-0.062 0.0476 +/-0.062 0.104 pCi/g Europium-155 U 0.0513 +/-0.0527 0.032 +/-0.0527 0.066 pCi/g Lead-212 0.904 +/-0.0535 0.0216 +/-0.0535 0.0447 pCi/g Lead-214 0.679 +/-0.0766 0.0285 +/-0.0766 0.0596 pCi/g Manganese-54 U 0.00548 +/-0.0205 0.0173 +/-0.0205 0.0368 pCi/g Niobium-94 U 0.00502 +/-0.0179 0.0154 +/-0.0179 0.0325 pCi/g Potassium-40 12.0 +/-0.847 0.127 +/-0.847 0.285 pCi/g Radium-226 0.627 +/-0.0778 0.0322 +/-0.0778 0.0675 pCi/g Silver-108m U 0.00214 +/-0.0148 0.0132 +/-0.0148 0.0278 pCi/g Thallium-208 0.307 +/-0.0471 0.0146 +/-0.0471 0.031 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U -0.00175 +/-0.0161 0.0179 +/-0.0161 0.0394 pCi/g BXF1 06/02/06 1548 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 37

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-010F Project: YANKO 1204 Sample ID: 162832003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits CarrierfTracer Recovery GFPC, Sr90, solid-ALL FSS 37 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

• Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

38

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-01OFS Proiect: YANK01204 Sample ID: 162832004 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 15.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.05 +/-0.214 0.0808 +/-0.214 0.172 pCi/g MJHI 06/06/06 1728 529778 1 Americium-241 U 0.0328 +/-0.0355 0.0285 +/-0.0355 0.0585 pCi/g Bismuth-212 0.664 +/-0.345 0.171 +/-0.345 0.363 pCi/g Bismuth-214 0.695 +/-0.115 0.0398 +/-0.115 0.0839 pCi/g Cesium-134 UUI 0.00 +/-0.0385 0.0279 +/-0.0385 0.0589 pCi/g Cesium-137 U 0.0326 +/-0.0317 0.0224 +/-0.0317 0.0474 pCi/g Cobalt-60 U 0.0254 +/-0.0295 0.0269 +/-0.0295 0.0578 pCi/g Europium-152 U -0.0335 +/-0.0559 0.0482 +/-0.0559 0.101 pCi/g Europium-154 U -0.0475 +/-0.0946 0.0643 +/-0.0946 0.140 pCi/g Europium-155 U 0.044 +/-0.0779 0.0477 +/-0.0779 0.0983 pCi/g Lead-212 1.08 +/-0.0716 0.0256 +/-0.0716 0.0533 pCi/g Lead-214 0.807 +/-0.104 0.0381 +/-0.104 0.0794 pCi/g Manganese-54 U 0.0132 +/-0.0275 0.0237 +/-0.0275 0.0504 pCi/g Niobium-94 U 0.0108 +/-0.0238 0.0207 +/-0.0238 0.0436 pCi/g Potassium-40 13.2 +/-1.02 0.198 +/-1.02 0.438 pCi/g Radium-226 0.695 +/-0.115 0.0398 +/-0.115 0.0839 pCi/g Silver-108m U - 0.00335 +/-0.0237 0.018 +/-0.0237 0.0379 pCi/g Thallium-208 0.318 +/-0.0568 0.0211 +/-0.0568 0.0446 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U - 0.00925 +/-0.0179 0.0209 +/-0.0179 0.0452 pCi/g BXFI 06/02/06 1548 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 39

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-O1OFS Project: YANKO 1204 Sample ID: 162832004 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 39 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

• Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

40

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-011F Proiect: YANKO 1204 Sample ID: 162832005 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 20.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.09 +/-0.233 0.088 +/-0.233 0.190 pCi/g MJH1 06/06/06 2000 529778 1 Americium-241 U -0.0786 +/-0.118 0.0915 +/-0.118 0.189 pCi/g Bismuth-212 0.602 +/-0.421 0.195 +/-0.421 0.416 pCi/g Bismuth-214 0.890 +/-0.132 0.0453 +/-0.132 0.0961 pCi/g Cesium-134 U 0.0536 +/-0.0558 0.0342 +/-0.0558 0.0723 pCi/g Cesium-137 0.212 +/-0.0512 0.0247 +/-0.0512 0.0527 pCi/g Cobalt-60 0.366 +/-0.0849 0.0262 +/-0.0849 0.0576 pCi/g Europium-152 U -0.0415 +/-0.0736 0.0582 +/-0.0736 0.122 pCi/g Europium-154 U 0.0615 +/-0.0839 0.0772 +/-0.0839 0.169 pCi/g Europium-155 U 0.0805 +/-0.0913 0.062 +/-0.0913 0.129 pCi/g Lead-212 1.13 +/-0.0826 0.0317 +/-0.0826 0.0663 pCi/g Lead-214 0.910 +/-0.0991 0.0423 +/-0.0991 0.089 pCi/g Manganese-54 U 0.0269 +/-0.029 0.0262 +/-0.029 0.056 pCi/g Niobium-94 U 0.00641 +/-0.0253 0.0217 +/-0.0253 0.0464 pCi/g Potassium-40 15.0 +/-1.15 0.167 +/-1.15 0.388 pCi/g Radium-226 0.890 +/-0.132 0.0453 +/-0.132 0.0961 pCi/g Silver-108m U -0.0111 +/-0.0222 0.0187 +/-0.0222 0.0397 pCi/g Thallium-208 0.353 +/-0.0647 0.0236 +/-0.0647 0.0503 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0 .000913 +/-0.0156 0.0173 +/-0.0156 0.0384 pCi/g BXFI 06/02/06 1548 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 41

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-01 IF Project: YANK0 1204 Sample ID: 162832005 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr9O, solid-ALL FSS 51 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UJ Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

42

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-012F Project: YANKO 1204 Sample ID: 162832006 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 16.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM& ALL FSS Actinium-228 0.922 +/-0.170 0.0627 +/-0.170 0.136 pCi/g MJH 1 06/06/06 2000 529778 1 Americium-241 U -0.0134 +/-0.120 0.0779 +/-0.120 0.161 pCi/g Bismuth-212 0.782 +/-0.399 0.137 +/-0.399 0.293 pCi/g Bismuth-214 0.677 +/-0.0964 0.035 +/-0.0964 0.0742 pCi/g Cesium-134 UJUI 0.00 +/-0.0376 0.0264 +/-0.0376 0.0558 pCi/g Cesium-137 0.159 +/-0.0393 0.0175 +/-0.0393 0.0374 pCi/g Cobalt-60 0.137 +/-0.0477 0.0185 +/-0.0477 0.0409 pCi/g Europium-152 U 0.0336 +/-0.0517 0.0475 +/-0.0517 0.0998 pCi/g Europium-154 U -0.0258 +/-0.0601 0.0475 +/-0.0601 0.106 pCi/g Europium-155 U 0.106 +/-0.0614 0.0583 +/-0.0614 0.120 pCi/g Lead-212 0.872 +/-0.0676 0.0262 +/-0.0676 0.0547 pCi/g Lead-214 0.815 +/-0.108 0.0311 +/-0.108 0.0655 pCi/g Manganese-54 U -0.0175 +/-0.0212 0.0172 +/-0.0212 0.0371 pCi/g Niobium-94 U 0.0182 +/-0.0225 0.0199 +/-0.0225 0.042 pCi/g Potassium-40 10.6 +/-0.823 0.163 +/-0.823 0.364 pCi/g Radium-226 0.677 +/-0.0964 0.035 +/-0.0964 0.0742 pCi/g Silver-108m U 0.00549 +/-0.0191 0.0169 +/-0.0191 0.0357 pCi/g Thallium-208 0.308 +/-0.0518 0.0159 +/-0.0518 0.0341 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U -0.00172 +/-0.0113 0.0116 +/-0.0113 0.0249 pCi/g BXFI 06/02/06 1548 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 43

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-012F Project: YANKO1204 Sample ID: 162832006 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 40 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

44

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013F Project: YANKO 1204 Sample ID: 162832007 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 24.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.22 +/-0.297 0.146 +/-0.297 0.305 pCi/g MJH1 06/06/06 2001 529778 1 Americium-241 U 0.0867 +/-0.102 0.064 +/-0.102 0.130 pCi/g Bismuth-212 0.964 +/-0.391 0.277 +/-0.391 0.581 pCi/g Bismuth-214 0.878 +/-0.134 0.0653 +/-0.134 0.136 pCi/g Cesium-134 UUI 0.00 +/-0.106 0.0448 +/-0.106 0.0936 pCi/g Cesium-137 0.549 +/-0.100 0.0382 +/-0.100 0.0798 pCi/g Cobalt-60 1.81 +/-0.147 0.0323 +/-0.147 0.0698 pCi/g Europium-152 U -0.0133 +/-0.101 0.0856 +/-0.101 0.178 pCi/g Europium-154 U 0.0295 +/-0.141 0.105 +/-0.141 0.225 pCi/g Europium- 155 U 0.0615 +/-0.0867 0.0765 +/-0.0867 0.157 pCi/g Lead-212 1.20 +/-0.0985 0.0483 +/-0.0985 0.0996 pCi/g Lead-214 0.931 +/-0.148 0.0581 +/-0.148 0.121 pCi/g Manganese-54 U - 0.00585 +/-0.0483 0.0404 +/-0.0483 0.0846 pCi/g Niobium-94 U 0.00999 +/-0.0382 0.0331 +/-0.0382 0.0693 pCi/g Potassium-40 13.0 +/-1.30 0.241 +/-1.30 0.534 pCi/g Radium-226 0.878 +/-0.134 0.0653 +/-0.134 0.136 pCi/g Silver-108m U - 0.00427 +/-0.0382 0.032 +/-0.0382 0.0665 pCi/g Thallium-208 0.432 +/-0.0807 0.0333 +/-0.0807 0.0698 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.00301 +/-0.0174 0.0188 +/-0.0174 0.0427 pCi/g BXFI 06/02/06 1548 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 45

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013F Project: YANK01204 Sample ID: 162832007 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr9O, solid-ALL FSS 38 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

46

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-014F Proiect: YANKO 1204 Sample ID: 162832008 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 21%

Parameter. Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.00364 +/-0.0405 0.0368 +/-0.0405 0.161 pCi/g LCW1 05/30/06 1156 533471 1 Curium-242 U 0.0363 -+/-0.0711 0.00 +/-0.0712 0.0983 pCi/g Curium-243/244 U 0.0323 +/-0.0634 0.00 +/-0.0635 0.0876 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.0124 +/-0.0534 0.0415 +/-0.0534 0.153 pCi/g LCWI 05/30/06 2129 533472 2 Plutonium-239/240 U 0.0515 +/-0.0714 0.00 +/-0.0716 0.0698 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U -2.38 +/-9.97 8.47 +/-9.98 17.7 pCi/g LCW1 06/03/06 0613 533473 3 Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.23 +/-0.279 0.0824 +/-0.279 0.178 pCi/g MJH 1 06/06/06 2029 529778 4 Americium-241 U -0.0143 +/-0.0378 0.0331 +/-0.0378 0.0681 pCi/g Bismuth-212 0.868 +/-0.463 0.199 +/-0.463 0.425 pCi/g Bismuth-214 0.813 +/-0.153 0.0472 +/-0.153 0.0999 pCi/g Cesium-134 U 0.0502 -F/-0.0448 0.0345 +/-0.0448 0.0729 pCi/g Cesium-137 U -0.00791 +/-0.032 0.026 +/-0.032 0.0553 pCi/g Cobalt-60 U 0.0285 +/-0.034 0.0307 +/-0.034 0.0667 pCi/g Europium-152 U 0.0441 +/-0.0707 0.0634 +/-0.0707 0.133 pCi/g Europium-154 U -0.0149 +/-0.103 0.0724 +/-0.103 0.159 pCi/g Europium-155 U 0.0689 +/-0.0893 0.0541 +/-0.0893 0.112 pCi/g Lead-212 1.26 +/-0.165 0.0338 +/-0.165 0.0702 pCi/g Lead-214 0.876 +/-0.143 0.0419 +/-0.143 0.0881 pCi/g Manganese-54 U 0.0203 +/-0.033 0.0297 +/-0.033 0.063 pCi/g Niobium-94 U 0.00366 F/-0.0282 0.0235 +/-0.0282 0.050 pCi/g Potassium-40 19.0 +/-1.68 0.220 +/-1.68 0.493 pCi/g Radium-226 0.813 +/-0.153 0.0472 +/-0.153 0.0999 pCi/g Silver-108m U -0.0251 +/-0.025 0.0199 +/-0.025 0.0421 pCi/g Thallium-208 0.382 +/-0.0739 0.0249 +/-0.0739 0.0529 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid - 0. 025 pCi/g Strontium-90 U 0.00827 +/-0.011 0.0105 +/-0.011 0.0226 pCi/g BXFI 06/08/06 1805 534448 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid - I to 2 pCi/g Tritium U -c1.0191 +/-0.527 0.443 +/-0.527 0.905 pCi/g NXPI 06/03/06 0030 531705 6 47

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-014F Project: YANKO 1204 Sample ID: 162832008 Client ID: YANKOOl Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Liquid Scintillation Analysis Liquid Scint C14, SolidAllFSS Carbon-14 U 0.134 +/-0.103 0.0826 +/-0.103 0.171 pCi/g ATH2 06/03/06 2137 534984 7 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 2.49 +/-21.0 15.6 +/-21.0 32.9 pCi/g SLNI 05/29/06 1542 531618 9 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -2.34 +/-3.32 2.83 +/-3.32 5.77 pCi/g SLNI 05/27/06 0019 531622 10 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.0698 +/-0.246 0.209 +/-0.246 0.431 pCi/g SXEI 05/30/062232 531704 11 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-l1-RC Modified 3 DOE EML HASL-300, Pu-1 -RC Modified 4 EML HASL 300, 4.5.2.3 5 EPA 905.0 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 EPA EERF C-01 Modified 9 DOE RESL Fe-I, Modified 10 DOE RESL Ni-I, Modified 11 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 93 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 85 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 72 (25% ,125%/)

Carrier/Tracer Recovery GFPC, Sr90, solid - 0.025 pCi/g 46 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 79 (15%-125%)

48

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-014F Project: YANK01204 Sample ID: 162832008 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 77 (25%- 125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (159/6-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

U1 Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

49

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis

.a-v- t o [

Cet ... ifc Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-015F Proiect: YANK01204 Sample ID: 162832009 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 34%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.832 +/-0.213 0.0785 +/-0.213 0.168 pCi/g MJH1 06/06/06 2138 529778 1 Americium-241 U 0.0511 +/-0.106 0.088 +/-0.106 0.182 pCi/g Bismuth-212 0.623 +/-0.270 0.160 +/-0.270 0.342 pCi/g Bismuth-214 0.533 +/-0.0981 0.044 +/-0.0981 0.0927 pCi/g Cesium-134 U 0.0265 +/-0.0323 0.0253 +/-0.0323 0.0538 pCi/g Cesium-137 0.377 +/-0.0611 0.0221 +/-0.0611 0.047 pCi/g Cobalt-60 0.744 +/-0.0759 0.0218 +/-0.0759 0.0481 pCi/g Europium-152 U -0.0395 +/-0.072 0.0526 +/-0.072 0.111 pCi/g Europium-154 U 0.0498 +/-0.071 0.0658 +/-0.071 0.144 pCi/g Europium-155 U 0.0747 +/-0.0598 0.0586 +/-0.0598 0.121 pCi/g Lead-212 0.833 +/-0.0733 0.033 +/-0.0733 0.0685 pCi/g Lead-214 0.755 +/-0.0997 0.038 +/-0.0997 0.0799 pCi/g Manganese-54 U 0.0147 +/-0.0271 0.0241 +/-0.0271 0.0513 pCi/g Niobium-94 U -0.00934 +/-0.0224 0.0188 +/-0.0224 0.0401 pCi/g Potassium-40 12.3 +1- 1.05 0.178 +1-1.05 0.400 pCi/g Radium-226 0.533 +/-0.0981 0.044 +/-0.0981 0.0927 pCi/g Silver-108m U -0.0066 +/-0.023 0.019 +/-0.023 0.040 pCi/g Thallium-208 0.276 +/-0.0562 0.0201 +/-0.0562 0.0427 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00153 +/-0.0159 0.0181 +/-0.0159 0.0408 pCi/g BXF1 06/02/06 1548 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 50

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-015F Proiect: YANKO 1204 Sample ID: 162832009 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 45 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

51

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-OOIF Proiect: YANKO 1204 Sample ID: 162832010 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 26.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0. +/-0.0855 0.0458 +/-0.0857 0.169 pCi/g LCWI 05/30/06 1156 533471 1 Curium-242 U ( +/-0.0627 0.00 +/-0.0628 0.0866 pCi/g Curium-243/244 U -0. +/-0.0605 0.0563 +/-0.0605 0.190 pCi/g Alphaspec Pu,'Solid-ALL FSS Plutonium-238 U 0.00 +/-0.0693 0.00 +/-0.0693 0.0959 pCi/g LCWI 05/30/06 2129 533472 2 Plutonium-239/240 U -0.0 0849 +/-0.0713 0.0403 +/-0.0713 0.176 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U - -1.69 +/-9.07 7.68 +/-9.07 16.0 pCi/g LCWI 06/03/06 0629 533473 3 Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 +/-0.302 0.110 +/-0.302 0.237 pCi/g MJHI 06/06/06 2138 529778 4 Americium-241 UUI +/-0.0601 0.0312 +/-0.0601 0.0648 pCi/g Bismuth-212 ( +/-0.528 0.246 +/-0.528 0.525 pCi/g Bismuth-214 ( +/-0.161 0.0517 +/-0.161 0.110 pCi/g Cesium-134 U 0.0' +/-0.0697 0.039 +/-0.0697 0.0828 pCi/g Cesium-137 +/-0.0758 0.0333 +/-0.0758 0.0707 pCi/g Cobalt-60 ( +/-0.129 0.0344 +/-0.129 0.0754 pCi/g Europium-152 U -0. +/-0.0773 0.0623 +/-0.0773 0.132 pCi/g Europium-154 U -0. +/-0.102 0.0792 +/-0.102 0.176 pCi/g Europium-155 U 0.0' +/-0.0644 0.0542 +/-0.0644 0.113 pCi/g Lead-212 +/-0.0859 0.0341 +/-0.0859 0.0716 pCi/g Lead-214 C +/-0.133 0.0476 +/-0.133 0.101 pCi/g Manganese-54 U -0. +/-0.0371 0.0296 +/-0.0371 0.0638 pCi/g Niobium-94 U 0.' +/-0.0302 0.0274 +/-0.0302 0.0585 pCi/g Potassium-40 +/-1.42 0.237 +/-1.42 0.539 pCi/g Radium-226 C +/-0.161 0.0517 +/-0.161 0.110 pCi/g Silver-108m U 0.01 +/-0.0259 0.0233 +/-0.0259 0.0495 pCi/g Thallium-208 C +/-0.0627 0.029 +/-0.0627 0.0617 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.0' +/-0.017 0.0179 +/-0.017 0.0398 pCi/g BXF1 06/02/06 1548 534448 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U +/-7.01 5.61 +/-7.01 11.7 pCi/g NXPI 05/28/06 0601 531705 6 LiquidScint C04, Solid AIlFSS 52

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-OOIF Project: YANKO 1204 Sample ID: 162832010 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Liquid Scintillation Analysis Liquid Scint C14, SolidAIl, FSS Carbon- 14 0.268 +/-0.101 0.0769 +/-0.101 0.159 pCi/g ATH2 06/03/06 2339 534984 7 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 9.95 +1-15.5 11.3 +1-15.5 23.7 pCi/g SLN1 05/29/06 1559 531618 9 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -4.23 +/-3.97 3.41 +/-3.97 6.95 pCi/g SLN1 05/27/06 0120 531622 10 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.174 +/-0.269 0.220 +/-0.269 0.454 pCi/g SXEI 05/30/062248 531704 II The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EML HASL 300, 4.5.2.3 5 EPA 905.0 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 EPA EERF C-01 Modified 9 DOE RESL Fe-I, Modified 10 DOE RESL Ni-I, Modified 11 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 92 (150/- 125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 65 (15%/,125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 84 (25%l-I 25%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 46 (259/- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 74 (15'/- 125%)

53

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-OOIF Project: YANK01204 Sample ID: 162832010 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 69 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 71 15%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

54

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-002F Project: YANKO 1204 Sample ID: 162832011 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 16.8%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSSGAM & ALL FSS Actinium-228 0.590 +/-0.227 0.0948 +/-0.227 0.207 pCi/g MJH1 06/06/06 2138 529778 1 Americium-241 U 0.000531 +/-0.0361 0.0352 +/-0.0361 0.073 pCi/g Bismuth-212 U 0.439 +/-0.392 0.213 +/-0.392 0.460 pCi/g Bismuth-214 0.436 +1-0.115 0.0442 +/-0.115 0.0955 pCi/g Cesium-134 U 0.00781 +/-0.0309 0.0271 +/-0.0309 0.0592 pCi/g Cesium-137 0.171 +/-0.0522 0.0221 +/-0.0522 0.0483 pCi/g Cobalt-60 0.141 +/-0.0653 0.0252 +/-0.0653 0.0568 pCi/g Europium-152 U -0.0415 +/-0.0655 0.0577 +/-0.0655 0.123 pCi/g Europium-154 U -0.0303 +/-0.078 0.0627 +/-0.078 0.143 pCi/g Europium-155 U 0.0113 +/-0.057 0.0542 +/-0.057 0.113 pCi/g Lead-212 0.628 +/-0.067 0.0313 +/-0.067 0.0659 pCi/g Lead-214 0.506 +/-0.110 0.0414 +/-0.110 0.0881 pCi/g Manganese-54 U 0.00764 +/-0.0308 0.0269 +/-0.0308 0.0584 pCi/g Niobium-94 U -0.0101 +/-0.0309 0.0222 +/-0.0309 0.0481 pCi/g Potassium-40 9.74 +/-1.02 0.171 +/-1.02 0.407 pCi/g Radium-226 0.436 +/-0.115 0.0442 +/-0.115 0.0955 pCi/g Silver-108m U 0.0121 +/-0.0208 0.0197 +/-0.0208 0.0424 pCi/g Thallium-208 0.197 +/-0.0581 0.0243 +/-0.0581 0.0524 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U -' 9.370E- +/-0.0166 0.0187 +/-0.0166 0.0417 pCi/g BXF1 06/02/06 1548 534448 2 05 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 55

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-002F Project: YANKO 1204 Sample ID: 162832011 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr9O, solid-ALL FSS 48 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

56

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-003F Proiect: YANKO 1204 Sample ID: 162832012 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 20.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.837 +/-0.133 0.0558 +/-0.133 0.117 pCi/g MJH1 06/06/06 2139 529778 1 Americium-241 U - 0.00219 +/-0.109 0.090 +/-0.109 0.186 pCi/g Bismuth-212 0.534 +/-0.216 0.119 +/-0.216 0.249 pCi/g Bismuth-214 0.591 +/-0.0832 0.0288 +/-0.0832 0.0602 pCi/g Cesium-134 UUI 0.00 +/-0.0279 0.0197 +/-0.0279 0.041 pCi/g Cesium- 137 0.355 +/-0.0442 0.0145 +/-0.0442 0.0306 pCi/g Cobalt-60 0.945 +/-0.0626 0.0137 +/-0.0626 0.0296 pCi/g Europium- 152 U 0.00575 +/-0.0435 0.0402 +/-0.0435 0.0836 pCi/g Europium-154 U 0.0387 +/-0.0557 0.0492 +/-0.0557 0.104 pCi/g Europium- 155 U 0.0875 +/-0.0767 0.0496 +/-0.0767 0.102 pCi/g Lead-212 0.819 +/-0.0541 0.0239 +/-0.0541 0.0494 pCi/g Lead-214 0.690 +/-0.0799 0.0284 +/-0.0799 0.0592 pCi/g Manganese-54 U 0.0147 +/-0.0191 0.0176 +/-0.0191 0.0367 pCi/g Niobium-94 U 0.0131 +/-0.0167 0.0149 +/-0.0167 0.0311 pCi/g Potassium-40 12.6 +/-0.691 0.116 +/-0.691 0.253 pCi/g Radium-226 0.591 +/-0.0832 0.0288 +/-0.0832 0.0602 pCi/g Silver-108m U -0.0129 +/-0.0149 0.0128 +/-0.0149 0.0268 pCi/g Thallium-208 0.258 +/-0.0394 0.0134 +/-0.0394 0.0282 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.0162 +/-0.0189 0.018 +/-0.0189 0.0402 pCi/g BXFI 06/02/06 1549 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 57

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-003F Project: YANK01204 Sample ID: 162832012 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 45 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

58

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 lnjun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-004F Project: YANK01204 Sample ID: 162832013 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 17.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.686 +/-0.125 0.0426 +/-0.125 0.0906 pCi/g MJH1 06/06/06 2350 529778 1 Americium-241 U - 0.00826 +/-0.0518 0.0509 +/-0.0518 0.105 pCi/g Bismuth-212 0.505 +/-0.187 0.0963 +/-0.187 0.203 pCi/g Bismuth-214 0.495 +/-0.060 0.0217 +/-0.060 0.0457 pCi/g Cesium-134 UUI 0.00 +/-0.0279 0.0165 +/-0.0279 0.0345 pCi/g Cesium-137 0.159 +/-0.0305 0.0126 +/-0.0305 0.0265 pCi/g Cobalt-60 0.263 +/-0.0399 0.0109 +/-0.0399 0.0239 pCi/g Europium-152 U -0.0352 +/-0.0353 0.0291 +/-0.0353 0.0606 pCi/g Europium-154 U 0.0517 +/-0.0426 0.0409 +/-0.0426 0.0874 pCi/g Europium-155 U 0.0077 +/-0.0363 0.0348 +/-0.0363 0.0714 pCi/g Lead-212 0.731 +/-0.042 0.0183 +/-0.042 0.0378 pCi/g Lead-214 0.570 +/-0.0626 0.0228 +/-0.0626 0.0473 pCi/g Manganese-54 U 0.0131 +/-0.0163 0.0133 +/-0.0163 0.028 pCi/g Niobium-94 U 0.0134 +/-0.0199 0.0113 +/-0.0199 0.0239 pCi/g Potassium-40 10.6 +/-0.623 0.0881 +/-0.623 0.197 pCi/g Radium-226 0.495 +/-0.060 0.0217 +/-0.060 0.0457 pCi/g Silver-108m U - 0.00381 +/-0.0117 0.0106 +/-0.0117 0.0221 pCi/g Thallium-208 0.215 +/-0.0302 0.0124 +/-0.0302 0.0259 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U - 0.00759 +/-0.0173 0.020 +/-0.0173 0.0435 pCi/g BXFI 06/02/06 1833 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 59

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.comr Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-004F Project: YANKO 1204 Sample ID: 162832013 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 37 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

60

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-004FS Proiect: YANKO 1204 Sample ID: 162832014 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 20.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSS GAM & ALL FSS Actinium-228 0.947 +/-0.184 0.0494 +/-0.184 0.105 pCi/g MJHI 06/06/06 2350 529778 1 Americium-241 U 0.0029 +/-0.0207 0.0199 +/-0.0207 0.0407 pCi/g Bismuth-212 0.561 +/-0.213 0.120 +/-0.213 0.251 pCi/g Bismuth-214 0.525 +/-0.0921 0.0275 +/-0.0921 0.0574 pCi/g Cesium-134 U 0.0375 +/-0.0368 0.0188 +/-0.0368 0.0392 pCi/g Cesium-137 0.216 +/-0.042 0.0157 +/-0.042 0.0329 pCi/g Cobalt-60 0.300 +/-0,0499 0.0141 +/-0.0499 0.0305 pCi/g Europium-152 U 0.00258 +/-0.0394 0.0357 +/-0.0394 0.0741 pCi/g Europium-154 U 0.0578 +/-0.0507 0.0468 +/-0.0507 0.0997 pCi/g Europium-155 U 0.0516 +/-0.0462 0.0341 +/-0.0462 0.0699 pCi/g Lead-212 0.775 +/-0.0975 0.0201 +/-0.0975 0.0415 pCi/g Lead-214 0.573 +/-0.081 0.0257 +/-0.081 0.0533 pCi/g Manganese-54 U - 0.00468 +/-0.0177 0.0154 +/-0.0177 0.0324 pCi/g Niobium-94 U 0.0038 +/-0.0149 0.0129 +/-0.0149 0.027 pCi/g Potassium-40 11.6 +/-0.941 0.124 +/-0.941 0.271 pCi/g Radium-226 0.525 +/-0.0921 0.0275 +/-0.0921 0.0574 pCi/g Silver-108m U-0 .000154 +/-0.0141 0.0125 +/-0.0141 0.0261 pCi/g Thallium-208 0.265 +/-0.044 0.014 +/-0.044 0.0293 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00386 +/-0.0163 0.0175 +/-0.0163 0.0394 pCi/g BXF1 06/02/06 1549 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 61

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006.

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-004FS Proiect: YANK0 1204 Sample ID: 162832014 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr9O, solid-ALL FSS 44 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

62

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005F Project: YANKO 1204 Sample ID: 162832015 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 13.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSSGAM & ALL FSS Actinium-228 1.04 +/-0.213 0.0758 +/-0.213 0.158 pCi/g MJH-1 06/06/06 2350 529778 1 Americium-241 U 0.081 +/-0.0844 0.0717 +/-0.0844 0.147 pCi/g Bismuth-212 0.744 +/-0.264 0.147 +/-0.264 0.306 pCi/g Bismuth-214 0.666 +/-0.0896 0.0323 +/-0.0896 0.0672 pCi/g Cesium-134 UUI 0.00 +/-0.0355 0.0245 +/-0.0355 0.0509 pCi/g Cesium-137 0.399 +/-0.0533 0.0189 +/-0.0533 0.0393 pCi/g Cobalt-60 1.74 +/-0.0845 0.0184 +/-0.0845 0.0393 pCi/g Europium-152 U 0.016 +/-0.052 0.0457 +/-0.052 0.0944 pCi/g Europium-154 U 0.0483 +/-0.0602 0.0551 +/-0.0602 0.117 pCi/g Europium-155 U 0.028 +/-0.0485 0.0467 +/-0.0485 0.0956 pCi/g Lead-212 0.976 +/-0.0593 0.0274 +/-0.0593 0.0562 pCi/g Lead-214 0.756 +/-0.0846 0.033 +/-0.0846 0.0682 pCi/g Manganese-54 U -0.00383 +/-0.0252 0.0214 +/-0.0252 0.0445 pCi/g Niobium-94 U 0.0245 +/-0.0192 0.0178 +/-0.0192 0.0369 pCi/g Potassium-40 10.5 +/-0.695 0.136 +/-0.695 0.297 pCi/g Radium-226 0.666 +/-0.0896 0.0323 +/-0.0896 0.0672 pCi/g Silver-108m U 0.00682 +/-0.0196 0.0169 +/-0.0196 0.035 pCi/g Thallium-208 0.335 +/-0.0501 0.0169 +/-0.0501 0.0353 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00586 +/-0.0183 0.0193 +/-0.0183 0.0432 pCi/g BXFI 06/02/06 1549 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 63

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005F Project: YANK01204 Sample ID: 162832015 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 45 (25- 125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

64

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-006F Project: YANKO 1204 Sample ID: 162832016 Client ID: YANKOO1 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 15.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.984 +/-0.130 0.046 +/-0.130 0.0966 pCi/g MJH1 06/06/06 2351 529778 1 Americium-241 U -0.0148 +/-0.087 0.0606 +/-0.087 0.124 pCi/g Bismuth-212 0.638 +/-0.246 0.101 +/-0.246 0.211 pCi/g Bismuth-214 0.774 +/-0.0668 0.0237 +/-0.0668 0.0493 pCi/g Cesium-134 UU1 0.00 +/-0.0296 0.017 +/-0.0296 0.0354 pCi/g Cesium-137 0.112 +/-0.0208 0.0134 +/-0.0208 0.028 pCi/g Cobalt-60 0.223 +/-0.0348 0.0129 +/-0.0348 0.0277 pCi/g Europium-152 U -0.0103 +1-0.035 0.0319 +/-0.035 0.066 pCi/g Europium-154 U -0.0358 +/-0.0508 0.0343 +/-0.0508 0.0734 pCi/g Europium-155 U 0.0827 +/-0.0422 0.0419 +/-0.0422 0.0855 pCi/g Lead-212 0.983 +/-0.0474 0.0203 +/-0.0474 0.0416 pCi/g Lead-214 0.823 +/-0.0628 0.024 +/-0.0628 0.0496 pCi/g Manganese-54 U 0.0093 +/-0.0151 0.0139 +/-0.0151 0.0291 pCi/g Niobium-94 U 0.0043 +/-0.0138 0.0121 +/-0.0138 0.0252 pCi/g Potassium-40 9.75 +/-0.555 0.105 +/-0.555 0.229 pCi/g Radium-226 0.774 +/-0.0668 0.0237 +/-0.0668 0.0493 pCi/g Silver-108m U -0.00725 +/-0.0123 0.0108 +/-0.0123 0.0224 pCi/g Thallium-208 0.351 +/-0.0337 0.0127 +/-0.0337 0.0264 pCi/g Rad Gas Flow Proportional Counting GFPC,S90, solid-ALL FSS Strontium-90 U 0.0101 +/-0.0157 0.0155 +/-0.0157 0.0342 pCi/g BXFI 06/02/06 1833 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 65

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-006F Project: YANKO 1204 Sample ID: 162832016 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 42 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

66

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-007F Project: YANK01204 Sample ID: 162832017 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 19.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.74 +/-0.191 0.0672 +/-0.191 0.141 pCi/g MJHI 06/06/06 2351 529778 1 Americium-241 U -0.0148 +/-0.0357 0.0336 +/-0.0357 0.0683 pCi/g Bismuth-212 1.11 +/-0.288 0.163 +/-0.288 0.337 pCi/g Bismuth-214 1.27 +/-0.0993 0.0373 +/-0.0993 0.0773 pCi/g Cesium-134 UUI 0.00 +/-0.0481 0.0291 +/-0.0481 0.0601 pCi/g Cesium-137 U -0.00561 +/-0.0253 0.0222 +/-0.0253 0.0459 pCi/g Cobalt-60 U 0.00116 +/-0.0253 0.0217 +/-0.0253 0.0458 pCi/g Europium-152 U -0.0221 +/-0.0593 0.0522 +/-0.0593 0.107 pCi/g Europium-154 U -0.0434 +/-0.0719 0.0597 +/-0.0719 0.126 pCi/g Europium-155 U 0.0586 +/-0.0584 0.0546 +/-0.0584 0.111 pCi/g Lead-212 1.67 +/-0.0714 0.0298 +/-0.0714 0.061 pCi/g Lead-214 1.32 +/-0.0886 0.0358 +/-0.0886 0.0737 pCi/g Manganese-54 UUI 0.00 +/-0.0532 0.019 +/-0.0532 0.0398 pCi/g Niobium-94 U 0.0256 +/-0.0217 0.020 +/-0.0217 0.0414 pCi/g Potassium-40 11.4 +/-0.713 0.167 +/-0.713 0.357 pCi/g Radium-226 1.27 +/-0.0993 0.0373 +/-0.0993 0.0773 pCi/g Silver-108m U -0.0132 +/-0.0203 0.0172 +/-0.0203 0.0355 pCi/g Thallium-208 0.539 +/-0.0503 0.0204 +/-0.0503 0.0422 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U -0.00609 +/-0.0118 0.0147 +/-0.0118 0.0333 pCi/g BXF1 06/02/06 1549 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 67

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-007F Project: YANK01204 Sample ID: 162832017 Client ID: YANKOOl Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits CarrierfIracer Recovery GFPC, Sr90, solid-ALL FSS 52 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J. Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

68

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-017F Project: YANKO 1204 Sample ID: 162832018 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 21%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid FSS GAM & ALL FSS Actinium-228 0.779 +/-0.129 0.0463 +/-0.129 0.0977 pCi/g MJHI 06/06/06 2351 529778 1 Americium-241 U-0.000356 +/-0.0171 0.0159 +/-0.0171 0.0326 pCi/g Bismuth-212 0.610 +/-0.204 0.0972 +/-0.204 0.204 pCi/g Bismuth-214 0.505 +/-0.0714 0.0229 +/-0.0714 0.0479 pCi/g Cesium-134 UU1 0.00 +/-0.0239 0.017 +/-0.0239 0.0355 pCi/g Cesium-137 0.378 +/-0.0359 0.0129 +/-0.0359 0.0271 pCi/g Cobalt-60 0.294 +/-0.0383 0.0124 +/-0.0383 0.0268 pCi/g Europium-152 U 0.0128 +/-0.0344 0.0305 +/-0.0344 0.0633 pCi/g Europium-154 U -0.0423 +/-0.0448 0.0346 +/-0.0448 0.0746 pCi/g Europium-155 U 0.027 +/-0.0385 0.0238 +/-0.0385 0.0489 pCi/g Lead-212 0.741 +/-0.0393 0.017 +/-0.0393 0.0351 pCi/g Lead-214 0.614 +/-0.0628 0.0222 +/-0.0628 0.0461 pCi/g Manganese-54 U 0.0061 +/-0.0159 0.0137 +/-0.0159 0.0289 pCi/g Niobium-94 U 0.000512 +/-0.0139 0.012 +/-0.0139 0.0252 pCi/g Potassium-40 11.0 +/-0.600 0.0952 +/-0.600 0.210 pCi/g Radium-226 0.505 +/-0.0714 0.0229 +/-0.0714 0.0479 pCi/g Silver-108m U -0.00685 +/-0.0111 0.00983 +/-0.0111 0.0206 pCi/g Thallium-208 0.281 +/-0.0349 0.0126 +/-0.0349 0.0264 pCi/g Rad Gas Flow Proportional Counting GFPC, SO9O, solid-ALL FSS Strontium-90 U 0.0346 +/-0.0241 0.0215 +/-0.0242 0.0474 pCi/g BXFI 06/02/06 1549 534448 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B MXP2 05/15/06 0846 529742 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/14/06 1230 529741 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 69

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 9, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-017F Proiect: YANKO 1204 Sample ID: 162832018 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 46 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

70

QUALITY CONTROL DATA I

71

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: June 9, 2006 Client : Connecticut Yankee Atomic Power Page 1 of 9 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 162832

• dl Ilil*'.l NJ""

II J lo.,amps Q I e *ua

ý1 OC Units RPD% REC% Ranee Anist Date Time Rad Alpha Spec Batch 533471 QC1201101118 162485017 DUP Americium-241 U -0.0415 U -0.00249 pCi/g 177 (0%- 100%) CWI 05/30/06 11:55 Uncert: +/-0.0591 +/-0.0219 TPU: +/-0.0591 +/-0.0219 Curium-242 U -0.00755 U 0.0283 pCi/g 346 (0%- 100%)

Uncert: +/-0.0634 +/-0.0555 TPU: +/-0.0634 +/-0.0556 Curium-243/244 U 0.00112 U 0.0131 pCi/g 168 (0% - 100%)

Uncert: +/-0.0607 +/-0.0521 TPU: +/-0.0607 +/-0.0521 QC1201101120 LCS Americium-241 12.2 10.8 pCi/g 89 (75%-125%) 05/30/06 11:55 Uncert: +/-0.975

.TPU: +/-1.73 Curium-242 U -0.0056 pCi/g Uncert: +/-0.047 TPU: +/-0.0471 Curium-243/244 14.9 12.4 pCi/g 83 (75%-125%)

Uncert: +/-1.04 TPU: +/-I.95 QC1201101117 MB Americium-241 U -0.00902 pCi/g 05/30/06 11:55 Uncert: +/-0.019 TPU: +/-0.019 Curium-242 U 0.0399 pCi/g Uncert: +/-0.0638 TPU: +/-0.064 Curium-243/244 U 0.0392 pCi/g Uncert: +/-0.0626 TPU: +/-0.0628 QC1201101119 162485017 MS Americium-241 12.7 U -0.0415 12.5 pCi/g 98 (75%-125%) 05/30/06 11:55 Uncert: +/-0.0591 +/-1 .06 TPU: +/-0.0591 +/-1.96 Curium-242 U -0.00755 U 0.00 pCi/g Uncert: +/-0.0634 +/-0.0517 TPU: +/-0.0634 +/-0.0517 Curium-243/244 15.5 U 0.00112 12.6 pCi/g 81 (75%-125%)

Uncert: +/-0.0607 +/-1 .06 TPU: +/-0.0607 +/-1.98 Batch 533472 QC1201101122 162485017 DUP Plutonium-238 U 0.0261 U 0.00 pCi/g (0%- 100%) CWI 05/30/06 21:29 72

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162832 Page 2 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 533472 Uncert: +/-0.0511 +/-0.0498 TPU: +/-0.0512 +/-0.0498 Plutonium-239/240 U 0.0459 U -0.00609 pCi/g 261 (0%- 100%)

Uncert: +/-0.0733 +/-0.0511 TPU: +/-0.0734 +/-0.0512 QC1201101124 LCS Plutonium-238 0.216 pCilg (75%-125%) 05/30/06 21:29 Uncert: +/-0.181 TPU: +/-0.182 Plutonium-239/240 11.3 10.3 pCi/g 91 (75%-125%)

Uncert: +/-1.21 TPU: +/-1.76 QCI201101121 MB Plutonium-238 U -0.00623 pCi/g 05/31/06 07:44 Uncert: +/-0.0692 TPU: +/-0.0693 Plutonium-239/240 U -0.0274 pCi/g Uncert: +/-0.100 TPU: +/-0.100 QC1201101123 162485017 MS Plutonium-238 U 0.0261 U 0.0634 pCi/g (75%-125%) 05/30/06 21:29 Uncert: +/-0.0511 +/-0.0787 TPU: +/-0.0512 +/-0.079 Plutonium-239/240 11.7 U 0.0459 10.7 pCi/g 92 (75%-125%)

Uncert: +/-0.0733 +/-0.971 TPU: +/-0.0734 +/-1.52 Batch 533473 QC1201101126 162485017 DUP Plutonium-241 U -8.66 U -6.36 pCi/g 0 (0% - 100%) LCW I 06/03/06 07:35 Uncert: +/-8.72 +/-6.79 TPU: +/-8.77 +/-6.82 QC1201101128 LCS Plutonium-241 131 106 pCi/g 81 (75%-125%) 06/03/06 08:07 Uncert: +/-12.3 TPU: +/-16.4 QC1201101125 MB Plutonium-241 U -1.18 pCi/g 06/03/06 07:18 Uncert: +/-9.02 TPU: +/-9.02 QC1201101127 162485017 MS Plutonium-24 I 135 U -8.66 146 pCi/g 108 (75%-125%) 06/03/06 07:51 Uncert: +/-8.72 +/-14.7 TPU: +/-8.77 +/-20.1 Rad Gamma Spec Batch 529778 QC1201092339 162832001 DUP Actinium-228 0.655 0.804 pCi/g 20 (0% - 100%) MJHI 06/06/06 23:52 Uncert: +/-0.137 +/-0.0979

+/-0.0979 73

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162832 Page 3 of 9 Parmname NOM Sample Qual OC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 529778 TPU: +/-0.137 Americium-241 u 0.0325 U 0.0192 pCi/g 52 (0%- 100%)

Uncert: +/-0.0823 +/-0.0754 TPU: +/-0.0823 +/-0.0754 Bismuth-212 0.551 0.361 pCi/g 42 (0%- 100%)

Uncert: +/-0.165 +/-0.163 TPU: +/-0.165 +/-0.163 Bismuth-214 0.447 0.498 pCi/g 1I (0%- 100%)

Uncert: +/-0.0787 +/-0.0532 TPU: +/-0.0787 +/-0.0532 Cesium- 134 U 0.0255 UUI 0.00 pCi/g 53 (0%- 100%)

Uncert: +/-0.0237 +/-0.0216 TPU: +/-0.0237 +/-0.0216 Cesium- 137 0.155 0.252 pCi/g 48 (0%- 100%)

Uncert: +/-0.0273 +/-0.0264 TPU: +/-0.0273 +/-0.0264 Cobalt-60 0.256 0.361 pCi/g 34 (0%- 100%)

Uncert: +/-0.046 +/-0.0362 TPU: +/-0.046 +/-0.0362 Europium- 152 U 0.0135 U -0.03 pCi/g 528 (0%- 100%)

Uncert: +/-0.0376 +/-0.0305 TPU: +/-0.0376 +/-0.0305 Europium- 154 U 0.000575 U 0.00301 pCi/g 136 (0%- 100%)

Uncert: +/-0.048 +/-0.0385 TPU: +/-0.048 +/-0.0385 Europium- 155 U 0.015 U 0.0377 pCi/g 86 (0%- 100%)

Uncert: +/-0.0405 +/-0.0364 TPU: +/-0.0405 +/-0.0364 Lead-212 0.609 0.785 pCi/g 25 (0%- 20%)

Uncert: +/-0.0665 +/-0.0398 TPU: +/-0.0665 +/-0.0398 Lead-214 0.566 0.640 pCi/g 12 (0%- 20%)

Uncert: +/-0.0835 +/-0.053 TPU: +/-0.0835 +/-0.053 Manganese-54 UU1 0.00 U -0.00338 pCi/g 239 (0%- 100%)

Uncert: +/-0.0194 +/-0.014 TPU: +/-0.0194 +/-0.014 Niobium-94 U 0.00427 U 0.00622 pCi/g 37 (0%- 100%)

Uncert: +/-0.0141 +/-0.0108 TPU: +/-0.0141 +/-0.0108 Potassium-40 10.8 12.9 pCi/g 18 (0%- 20%)

Uncert: +/-0.957 +/-0.513 TPU: +/-0.957 +/-0.513 Radium-226 0.447 0.498 pCi/g 1I (0%- 100%)

Uncert: +/-0.0787 +/-0.0532 TPU: +/-0.0787 +/-0.0532 Silver- 108m U 0.00155 U 0.000741 pCi/g 71 (0%- 100%)

Uncert: +/-0.0131 +/-0.0105 74

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162832 Page 4 of 9

'<.

NJ 1Nin"l nuall OC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 529778 TPU: +/-0.0131 +1-0.0105 Thallium-208 0.194 0.230 pCi/g 17 (0%-100%)

Uncert: +/-0.042 +/-0.0259 TPU: +/-0.042 +/-0.0259 QC1201092340 LCS Actinium-228 U 0.589 pCi/g 06/06/06 20:05 Uncert: +/-0.539 TPU: +/-0.539 Americium-24 l 23.4 21.4 pCi/g 91 (75%-125%)

Uncert: +/-3.52 TPU: +/-3.52 Bismuth-212 U -0.211 pCi/g Uncert: +/-1.02 TPU: +/-1.02 Bismuth-214 U -0.102 pCi/g Uncert: +/-0.244 TPU: +/-0.244 Cesium- 134 U -0.0153 pCi/g Uncert: +/-0.147 TPU: +/-0.147 Cesium-137 9.64 10.1 pCi/g 105 (75%-125%)

Uncert: +/-0.792 TPU: +/-0.792 Cobalt-60 15.1 *, 15.3 pCi/g 102 (75%-125%)

Uncert: +/-1.14 TPU: +/-1.14 Europium- 152 U -0.0723 pCi/g Uncert: +/-0.330 TPU: +/-0.330 Europium- 154 U -0.186 pCi/g Uncert: +/-0.319 TPU: +/-0.319 Europium- 155 U -0.00538 pCi/g Uncert: +/-0.364 TPU: +/-0.364 Lead-212 U 0.193 pCi/g Uncert: +/-0.187 TPU: +/-0.187 Lead-214 U -0.117 pCi/g Uncert: +/-0.232 TPU: +/-0.232 Manganese-54 U 0.0588 pCi/g Uncert: +/-0.137 TPU: +/-0.137 Niobium-94 U 0.00234 pCi/g Uncert: +/-0.126 TPU: +/-0.126 Potassium-40 U -0.473 pCi/g 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162832 Page 5 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 529778 Uncert: +/-1.12 TPU: +/-1.12 Radium-226 U -0.102 pCi/g (75%-125%)

Uncert: +/-0.244 TPU: +/-0.244 Silver-I 08m U -0.00368 pCi/g Uncert: +/-0.117 TPU: +/-0.117 Thallium-208 U -0.0624 pCi/g Uncert: +/-0.137 TPU: +/-0.137 QC1201092338 MB Actinium-228 U 0.0718 pCi/g 06/06/06 23:51 Uncert: +/-0.0476 TPU: +/-0.0476 Americium-241 U 0.00824 pCi/g Uncert: +/-0.0133 TPU: +/-0.0133 Bismuth-212 U 0.026 pCi/g Uncert: +/-0.164 TPU: +/-0.164 Bismuth-214 U 0.00907 pCi/g Uncert: +/-0.0339 TPU: +/-0.0339 Cesium-134 U 0.00557 pCi/g Uncert: +/-0.0132 TPU: +/-0.0132 Cesium-137 U -0.0114 pCi/g Uncert: +/-0.0125 TPU: +/-0.0125 Cobalt-60 U 0.000917 pCi/g Uncert: +/-0.0131 TPU: +/-0.0131 Europium- 152 U 0.0155 pCi/g Uncert: +/-0.0264 TPU: +/-0.0264 Europium- 154 U 0.00784 pCi/g Uncert: +/-0.0345 TPU: +/-0.0345 Europium-155 U 0.016 pCi/g Uncert: +/-0.0209 TPU: +/-0.0209 Lead-212 UUI 0.00 pCi/g Uncert: +/-0.0304 TPU: +/-0.0304 Lead-214 U 0.0403 pCi/g Uncert: +/-0.0337 TPU: +/-0.0337 76

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162832 Page 6 of 9 NnN'A Qý I " ý1 NI* I ]nltc g pl*o/* Rl*r o/* R2nao Anlcf N*fD Tim*

nr ll..*. Dpno/- Rvco/- Ran . A.1.* ný# Ir.

Rad Gamma Spec Batch 529778 Manganese-54 U 0.00515 pCi/g Uncert: +/-0.0114 TPU: +/-0.0114 Niobium-94 U 0.00872 pCi/g Uncert: +/-0.0117 TPU: +/-0.0117 Potassium-40 U 0.0972 pCi/g Uncert: +/-0.106 TPU: +/-0.106 Radium-226 U 0.00907 pCi/g Uncert: +/-0.0339 TPU: +/-0.0339 Silver- 108m U 0.0115 pCi/g Uncert: +/-0.00907 TPU: +/-0.00907 Thallium-208 U 0.00346 pCi/g Uncert: +/-0.0168 TPU: +/-0.0168 Rad Gas Flow Batch 534448 QC1201103435 162832001 DUP Strontiurn-90 U 0.0262 U 0.00157 pCi/g 0 (0% - 100%) BXFI 06/02/06 15:47 Uncert: +/-0.0216 +/-0.0157 TPU: +/-0.0217 +/-0.0157 QCI201103437 LCS Strontium-90 1.41 1.16 pCi/g 82 (75%-125%) 06/02/06 15:47 Uncert: +/-0.0871 TPU: +/-0.0923 QC1201103434 MB Strontium-90 U -0.000243 pCi/g 06/02/06 15:47 Uncert: +/-0.0111 TPU: +/-0.0111 QC1201103436 162832001 MS Strontium-90 1.51 U 0.0262 1.16 pCi/g 77 (75%-125%) 06/02/06 15:47 Uncert: +/-0.0216 +/-0.0901 TPU: +/-0.0217 +/-0.0968 Rad Liquid Scintillation Batch 531618 QC1201096632 163173001 DUP Iron-55 U 10.3 U 5.38 pCi/g 0 (0% - 100%) SLNI 05/31/06 12:49 Uncert: +/-20.1 +/-18.0 TPU: +/-20.1 +/-18.1 QC1201096634 LCS Iron-55 437 428 pCi/g 98 (75%-125%) 05/31/06 13:22 Uncert: +/-40.6 TPU: +/-62.3 QC1201096631 MB Iron-55 U 3.58 pCi/g 05/31/06 12:32 77

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162832 Page 7 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Liquid Scintillation Batch 531618 Uncert: +/-24.7 TPU: +/-24.7 QC0201096633 163173001 MS Iron-55 569 U 10.3 544 pCi/g 96 (75%-125%) 05/31/06 13:05 Uncert: +/-20.1 +/-39.3 TPU: +/-20.1 +/-69.3 Batch 531622 QC1201096645 163173001 DUP Nickel-63 U -6.64 U -5.49 pCi/g 0 (0% - 100%) SLNI 05/28/06 01:38 Uncert: +/-7.30 +/-4.33 TPU: +/-7.31 +/-4.33 QC1201096647 LCS Nickel-63 362 301 pCi/g 83 (75%-125%) 05/28/06 03:40 Uncert: +/-7.49 TPU: +/-11.1 QC1201096644 MB Nickel-63 U -1.66 pCi/g 05/28/06 00:37 Uncert: +/-3.41 TPU: +/-3.41 QC1201096646 163173001 MS Nickel-63 460 U -6.64 395 pCi/g 86 (75%-125%) 05/28/06 02:39 Uncert: +/-7.30 +/-9.22 TPU: +/-7.31 +/-14.9 Batch 531704 QC1201096868 162583001 DUP Technetium-99 U 0.161 U 0.239 pCi/g 0 (0% - 100%) SXEI 05/31/06 00:27 Uncert: +/-0.254 +/-0.273 TPU: +/-0.255 +/-0.273 QC1201096870 LCS Technetium-99 12.5 11.1 pCi/g 89 (75%-125%) 05/31/06 01:00 Uncert: +/-0.474 TPU: +/-0.545 QC1201096867 MB Technetium-99 U 0.163 pCi/g 05/31/06 00:11 Uncert: +/-0.214 TPU: +/-0.214 QC1201096869 162583001 MS Technetium-99 13.1 U 0.161 11.6 pCi/g 89 (75%-125%) 05/31/06 00:44 Uncert: +/-0.254 +/-0.583 TPU: +/-0.255 +/-0.649 Batch 531705 QC1201096878 162583001 DUP Tritium U 1.17 U 6.01 pCi/g 0 (0%- 100%) NXPI 05/28/06 09:10 Uncert: +/-4.09 +/-4.70 TPU: +/-4.09 +/-4.70 QC1201096880 LCS Tritium 41.4 44.8 pCi/g 108 (75%-125%) 05/28/06 10:14 Uncert: +/-5.68 TPU: +/-5.73 78

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162832 Page 8 of 9 Parmname NOM Samnie Oual OC Units RPD% REC% Range Anist Date Time Rad Liquid Scintillation Batch 531705 QC1201096877 MB Tritium U 0.0641 pCi/g 06/03/06 05:11 Uncert: +/-0.533 TPU: +/-0.533 QC1201096879 162583001 MS Tritium 45.7 U 1.17 52.3 pCi/g 114 (75%-125%) 05/28/06 09:42 Uncert: +/-4.09 +/-6.44 TPU: +/-4.09 +/-6.50 Batch 534984 QC1201104746 163173001 DUP Carbon- 14 U 0.00714 U 0.00246 pCi/g 0 (0%- 100%) ATH2 06/05/06 03:00 Uncert: +/-0.0996 +/-0.103 TPU: +/-0.0996 +/-0.103 QC1201104748 LCS Carbon- 14 12.1 11.3 pCi/g 94 (75%-125%) 06/05/06 05:20 Uncert: +/-0.855 TPU: +/-0.873 QC0201104745 MB Carbon-14 U -0.0368 pCi/g 06/05/06 00:57 Uncert: +/-0.101 TPU: +/-0.101 QC1201104747 163173001 MS Carbon- 14 12.9 U 0.00714 12.1 pCi/g 94 (75%-125%) 06/05/06 05:02 Uncert: +/-0.0996 +/-0.917 TPU: +/-0.0996 +/-0.936 Notes:

The Qualifiers in this report are defined as follows:

A quality control analyte recovery is outside of specified acceptance criteria Result is less than value reported Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

U1 Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL Preparation or preservation holding time was exceeded 79

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162832 Page 9 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time h

N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

80

Table of Contents General Narrative ................................................................... 1 Chain of Custody And Supporting Dpcumentation ........... 5 Radiological Analysis ........................................................... 12 Sample Data Summary ............................ 18 Q uality C ontrol D ata ............................................................ 60

General Narrative 1

CASE NARRATIVE For CONNECTICUT YANKEE RE: Soil PO# 002332 Work Order: 170256 SDG: MSR #06-1160 September 6, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:

2040 Savage Road' Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC,' (GEL) in Charleston, South Carolina on August 25, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and. signatures.

The laboratory received the following sample(s):

Sample 11) Client Sample ID 170256001 9106-0006-005A 170256002 9106-0006-005B

.170256003 9106-0006-005C 170256004 9106-0006-005D 170256005 9106-0005-0IOA 170256006 9106-0005-OIOB 170256007 9106-0005-OIOC 170256008 9106-0005-OIOD 170256009 9106-0014-033A GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

P.O. Box 30712 - Charlesion, SC 29417

• 2040 Savage Road (29407)

Phone (843) 556-8171

• Fax 243) 766-1178 - www.gel.com

170256010 9106-0014-033B 170256011 9106-0014-033C 170256012 9106-0014-033D 170256013 9106-0004-013A 170256014 9106-0004-013B 170256015 9106-0004-013C 170256016 9106-0004-013D 170256017 9106-0004-005A 170256018 9106-0004-005B 170256019 9106-0004-005C 170256020 9106-0004-005D Items of Note:

There are no items of note.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engiil eering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.

Analytical Request:

Twenty soil samples were analyzed for FSSGAM and Sr-90.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically aid for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or.ja designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP INC. !i P.O. Box 30712 - Charleston, SC 29417 - 2040 Savage Road (29407)

Phone (843) 556-8171

• Fax*f43) 766-1178 - www.gel.com

List of current GEL Certifications as of 06 September 2006 State Certification Alaska UST-062 Arizona AZ0668 Arkansas 88-0651

_. CLIA " 42DO004*6. .

0)1151iCA ... .

California

]Colorado- _ __

(enEngLabs

[ Conecticut PH-0169 I Dept. of Navy ----

RFES I 4 13j EPA WG-tI5J Florida/NELAP E7 156 Georgia E87156 (FL/NELAP)

Idaho N/A Illinois 200029 Indiana Kansas E-10332 Kentucky 90129 Maryland Massachusetts M-SCO12 Michigan -

_____ 9903

_ __ Nevada SC12 SC002.-

New Jersey New York North Carolina 233 North Carolina Drinking W .... . . 457609 North Dakota _R-158 i Oklahoma 9904 Pennsylvania 68-485 South Carolina 10120001/10585001/1 0120002 Tennessee 02934 Texas TX213-2006A

- U.S. Dept.of Agriculture §-52597 .

US Army Corps of Engineer N/A Utah 8037697376 GEL Vermont N/A Virginia 00151 .

Washington C223 I 4

Chain of Custody And Supporting Documentation 5

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00511 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407

• 843 556 8t71. Attn. Cheryl Jones U rA' V Priority: [] 30 D. 2 14 D. [E 7 D. Container 'f

______Sample Size- C -z Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample 1D 9106-0006-005A 8/8/06 14:35 SE C BP X X Transferred from COC # 2006-00488 9106-0006-005B 8/8/06 15:08 SE C BP X X Tranrsferred from COC # 2006-00488 9106-0006-005C 8/9/06 07:46 SE C BP X X Transferred from COC # 2006-00307 9106-0006-005D 8/9/06 08:18 SE C BP X X Transferred from COC # 2006-00307 NOTES: PO#: 002332 MSR#: 06-1160 SSWP#NA SLTP QA El Radwaste QA 1-El Non QA Samples Shipped Via: Internal Container E Fed Ex Temp.: Deg. C El ups ElHand Custody Sealed?

YO - N E

1) Relinquished By Date/Time 2)",vedBy Date/Time Custody Seal Intact?

JAI M*6- *- ý-OV1/340 o ,, (I,- 1 k/.g4&l* ogo0 El Other

3) Relinquished By Date/Time 4) ROceived By' f-1" Date/Time YC NO Bill of Lading #

V00' 4~3 641f

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00512 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State)

General Engineering Laboratories o 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones C n Priority: [1] 30 D. 0 14 D. El 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0005-OIOA 8/9/06 09:03 SE C BP x x Transferred from COC # 2006-00489 9106-0005-01OB 8/9/06 09:33 SE C BP X X Transferred from COC # 2006-00489 9106-0005-01OC 8/9/06 10:04 SE C BP X x Transferred from COC # 2006-00489 9106-0005-01OD 8/9/06 10:56 SE C BP X X Transferred from COC # 2006-00489 NOTES: PO #: 002332 MSR #: 06- 110 SSWP# NA Z LTP QA [] Radwaste QA El Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.: __ Deg. C El ups C1 Hand Custody Sealed?

YQ NO

1) Relinquished By Dat /Time 2) ceived By D te/Time Custody Seal Intact?

[ Other

3) Relinquished By I6ate/rime 49fceived By L -- 1ate/Ttme YO NO Bill of Lading #

?qV0 4631 6419

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 1 Major 1, Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00513 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 C 843 556 8171. Attn. Cheryl Jones Container 7 D.

Priority: [ 30 D. Z 14 D. El Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0014-033A 8/11/06 07:58 SE C BP X X Transfenre 'from COC # 2006-00493 39106-0014-033B 8/11/06 08:24 SE C BP X X Transferred from C0C # 2006-00493 9106-0014-033C 8/11/06 08:45 SE C BP X X Transferred from COC #2006-00493 9106-0014-033D 8/11/06 09:16 SE C BP X X Transferred from COC # 2006-00493 NOTES: PO #: 002332 MSR #: 06-1160 SSWP# NA Z LTP QA El Radwaste QA E] Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.: - Deg. C F1 UPS

[] Hand - Custody Sealed? -

YE] NE]

1) Relinquished By Da e/Time 2) ived By Date/Time Custody Seal Intact?

RelnqusheTB 01)1 71349 Df2-/4 4o By (Xh "- & X4)0 V.

El Other

3) Relinquished By Date/Time 4) R4ed By D7late/rime YE] NO Bill of Lading #

ý9oo 40q' 6'44q

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00520 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State)

General Engineering Laboratories (c 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Q CA W Priority: El 30 D. 10 14 D. E] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0004-013A 8/9/06 12:53 SE C BP X X Transferred from COC 2006-00490 9106-0004-013B 8/9/06 13:27 SE C BP X X Transtfrred from COC 2006-00490 "9106-0004-013C 8/9/06 13:57 SE C BP X X Transferred from COC 2006-00490 9106-0004-013D 8/9/06 14:28 SE C BP X X Transferred from COC 2006-00490 9106-0004-OOSA 8/9/06 14:58 SE C BP x x Transferred from COC 2006-00490 9106-0004-005B 8/10/06 07:41 SE C BP X X Transferred from COC 2006-00491 9106-0004-OOSC 8/10/06 08:09 SE C BP X X Transferred from COC 2006-00491 9106-0004-005D 8/10/06 08:49 SE C BP X X Transferred from COC 2006-00491 NOTES: PO #: 002332 MSR#: 06-110e3 SSWP#NA Z LTP QA El Radwaste QA [] Non QA Samples Shipped Via:

Z Fed Ex Internal Container Temp.: _ Deg. C

[] ups

[1 Hand Custody Sealed?

-- --*"

Yr N l) Relinquished By Date ime 2) Re ved By Date/Time Custody Seal Intact?

[] Other

3) Relinquished By Date/Time 46ceived By YD N0 Bill of Lading #

79,9o 46ý3?14(

Connecticut Yankee Statement of Work for Analytical Lab Services _CylSCS0w_001 CY-lsc-sOw-o0l Figure 1. Sample Check-in List Date/Time Received:

SDG#: / . -O.-- O ..

Work Order Number.

I.

Shipping Cdntainer ID:A_ f3 .. Chain of Custody# 605-1pa 1.. Custody Seals ori shipping container intact?.

-Yes I.j1~o (1 Yes HS"ocI

2. Custody Seals dated and signed? Yes'ý- h "

3. Chain-of-Custody record present?

.4. Cooler temperature _ ' "" T

5. Vermiculite/packing materials is: .Wet wo 1,j HiTry (;,,

6. Number of samples in shipping container:

7. Sample holding times exceeded? Yes [,No [ i

.8.

8. Samples have:'

..-.. hazard labels i

_,etwitody seals -appropriate sample labels

9. Samples are:'

w0gogd condition leaking  !

-"broken .. Jiave air bubbles

10. Were any anomalies identified in sample receipt? . Yes [ No [.j*

11. .Description of anomalies (include sample numbers):

/' .

Telephoned i 10

Connecticut Yankee "

-CY-SC-SOW-OO1 Statement of Work for Analytical Lab Services -I Figure 1. Sample Check-in List.

Datefrime Received. 5 /4 I -

SDG #:/ V- or -

Work Order Nuntber: i tiD t2 0 Chain o utd# .4 T Shipping Cdhtatner of Custo.edy #. 2 - "

1. Custody Seals od shipping container intact?_ Yes [4 o \ ]

2. Custody Seals dated and signed? Yesk No f[J"

3. Chain-of-Custody record present? Yes E.hNo.

Cooler temperature .22 -

4.

5. Vermiculile/packing materials is: Wet W-'5ry, I 6 .' Number of sainples in shipping container:

7. Sample holding times exc'eeded? Yes Lr,,"o [

Le4l(,

11

RADIOLOGICAL ANALYSIS 12

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 170256 Method/Analysis Information Product: Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Analytical Method: EML HASL 300, 4.5.2.3 Prep Method: Dry Soil Prep Analytical Batch Number: 563436 Prep Batch Number: 562444 Sample ID Client ID 170256001 9106-0006-005A 170256002 9106-0006-005B 170256003 9106-0006-005C 170256004 9106-0006-005D 170256005 9106-0005-O1OA 170256006 9106-0005-OIOB 170256007 9106-0005-OIOC 170256008 9106-0005-OIOD 170256009 9106-0014-033A 170256010 9106-0014-033B 170256011 9106-0014-033C 170256012 9106-0014-033D 170256013 9106-0004-013A 170256014 9106-0004-013B 170256015 9106-0004-013C 170256016 9106-0004-013D 170256017 9106-0004-005A 170256018 9106-0004-005B 170256019 9106-0004-005C 170256020 9106-0004-005D 1201171525 Method Blank (MB) 1201171526 170256001(9106-0006-005A) Sample Duplicate (DUP) 1201171527 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this 13

narrative has been analyzed in accordance with GL-RAD-A-013 REV# 12.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (Q0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 170256001 (9106-0006-005A).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 170256007 (9106-0005-010C), 170256016 (9106-0004-013D) and 170256019 (9106-0004-005C) were recounted due to high MDAs.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information 14

Qualifier Reason Analyte Sample U' Data rejected due to high counting uncertainty Bismuth-212 170256009 UI Data rejected due to interference. Europium- 155 170256003 170256009 170256019 170256020 U' Data rejected due to low abundance. Bismuth-214 170256008 Cesium- 134 170256005 170256007 170256008 170256012 170256013 170256019 1201171526 Europium- 155 170256018 Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 562563 Prep Batch Number: 562478 Dry Soil Prep GL-RAD-A-021 Batch Number: 562444 15

Sample ID Client ID 170256001 9106-0006-005A 170256002 9106-0006-005B 170256003 9106-0006-005C 170256004 9106-0006-005D 170256005 9106-0005-OIOA 170256006 9106-0005-OIOB 170256007 9106-0005-OIOC 170256008 9106-0005-OIOD 170256009 9106-0014-033A 170256010 9106-0014-033B 170256011 9106-0014-033C 170256012 9106-0014-033D 170256013 9106-0004-013A 170256014 9106-0004-013B 170256015 9106-0004-013C 170256016 9106-0004-013D 170256017 9106-0004-005A 170256018 9106-0004-005B 170256019 9106-0004-005C 170256020 9106-0004-005D 1201169421 Method Blank (MB) 1201169422 170256002(9106-0006-005B) Sample Duplicate (DUP) 1201169423 170256002(9106-0006-005B) Matrix Spike (MS) 1201169424 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 10.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 170256002 (9106-0006-005B).

16

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples were recounted due to low/high recovery.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

K 1/ex-a Reviewer/Date:

17

SAMPLE DATA

SUMMARY

18

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOO Connecticut Yankee Atomic Power Co.

Client SDG: MSR#06-1160 GEL Work Order: 170256 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by 19

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005A Project: YANK0 1204 Sample ID: 170256001 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 08-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 15.8%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.966 +/-0.192 0.0743 +/-0.192 0.149 pCi/g MJH1 09/01/06 1057 563436 1 Americium-241 U 0.0375 +/-0.0387 0.0329 +/-0.0387 0.0658 pCi/g Bismuth-212 0.366 +/-0.306 0.175 +/-0.306 0.350 pCi/g Bismuth-214 0.650 +/-0.135 0.042 +/-0.135 0.0839 pCi/g Cesium-134 U 0.0366 +/-0.0355 0.0288 +/-0.0355 0.0576 pCi/g Cesium-137 0.0666 +/-0.0355 0.0236 +/-0.0355 0.0472 pCi/g Cobalt-60 0.104 +/-0.0726 0.0286 +/-0.0726 0.0573 pCi/g Europium-152 U 0.00636 +/-0.0728 0.0538 +/-0.0728 0.108 pCi/g Europium-154 U -0.0788 +/-0.0938 0.0718 +/-0.0938 0.143 pCi/g Europium-155 U 0.0672 +/-0.0554 0.0518 +/-0.0554 0.104 pCi/g Lead-212 0.871 +/-0.0971 0.0305 +/-0.0971 0.061 pCi/g Lead-214 0.727 +/-0.105 0.0379 +/-0.105 0.0757 pCi/g Manganese-54 U -0.00916 +/-0.0319 0.0232 +/-0.0319 0.0465 pCi/g Niobium-94 U 0.0101 +/-0.0244 0.0223 +/-0.0244 0.0445 pCi/g Potassium-40 11.3 +/-0.986 0.201 +/-0.986 0.403 pCi/g Radium-226 0.650 +/-0.135 0.042 +/-0.135 0.0839 pCi/g Silver-108m U -0.0067 +/-0.0208 0.018 +/-0.0208 0.036 pCi/g Thallium-208 0.283 +/-0.0618 0.0212 +/-0.0618 0.0423 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0254 +/-0.0193 0.0126 +/-0.0193 0.0298 pCi/g KSDI 09/07/06 1742 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 20

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005A Project: YANKO1204 Sample ID: 170256001 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 96 (251/6-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

21

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Certificateof Analvsis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005B Proiect: YANK01204 Sample ID: 170256002 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 14.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.606 +/-0.152 0.0599 +/-0.152 0.131 pCi/g MJHI 09/01/06 1220 563436 1 Americium-241 U 0.101 +/-0.114 0.0861 +/-0.114 0.179 pCi/g Bismuth-212 0.685 +/-0.232 0.134 +/-0.232 0.290 pCi/g Bismuth-214 0.435 +/-0.0852 0.0332 +/-0.0852 0.0708 pCi/g Cesium- 134 U 0.0313 +/-0.0286 0.0238 +/-0.0286 0.0507 pCi/g Cesium-137 0.114 +/-0.0348 0.0206 +/-0.0348 0.0438 pCi/g Cobalt-60 0.436 +/-0.0586 0.0151 +/-0.0586 0.0345 pCi/g Europium-152 U -0.0448 +/-0.0525 0.0416 +/-0.0525 0.0882 pCi/g Europium-154 U -0.0186 +/-0.0685 0.0562 +/-0.0685 0.124 pCi/g Europium-155 U 0.0423 +/-0.0579 0.0552 +/-0.0579 0.114 pCi/g Lead-212 0.643 +/-0.0623 0.0268 +/-0.0623 0.056 pCi/g Lead-214 0.462 +/-0.0885 0.033 +/-0.0885 0.0696 pCi/g Manganese-54 U -0.0167 +/-0.0261 0.0174 +/-0.0261 0.0377 pCi/g Niobium-94 U 0.00909 +/-0.0195 0.0173 +/-0.0195 0.0369 pCi/g Potassium-40 11.1 +/-0.983 0.179 +/-0.983 0.399 pCi/g Radium-226 0.435 +/-0.0852 0.0332 +/-0.0852 0.0708 pCi/g Silver-108m U -0.00194 +/-0.0168 0.0149 +/-0.0168 0.0317 pCi/g Thallium-208 0.243 +/-0.0457 0.0176 +/-0.0457 0.0377 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.00501 +/-0.0149 0.0117 +/-0.0149 0.0278 pCi/g KSD1 09/07/06 1742 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 22

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005B Proiect: YANKO 1204 Sample ID: 170256002 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrierf[racer Recovery GFPC, Sr90, solid-ALL FSS 101 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery, limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

23

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005C Project: YANKO1204 Sample ID: 170256003 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 31.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.07 +/-0.284 0.101 +/-0.284 0.215 pCi/g MJHI 09/01/06 1221 563436 1 Americium-241 U 0.0251 +/-0.0367 0.0332 +/-0.0367 0.0683 pCi/g Bismuth-212 0.684 +/-0.424 0.178 +/-0.424 0.383 pCi/g Bismuth-214 0.673 +/-0.121 0.0445 +/-0.121 0.0947 pCi/g Cesium-134 U 0.0516 +/-0.0548 0.0344 +/-0.0548 0.0729 pCi/g Cesium-137 0.317 +/-0.0544 0.0247 +/-0.0544 0.0528 pCi/g Cobalt-60 0.821 +/-0.0911 0.0294 +/-0.0911 0.064 pCi/g Europium-152 U -0.049 +/-0.0652 0.0539 +/-0.0652 0.114 pCi/g Europium-154 U 0.0883 +/-0.0913 0.0839 +/-0.0913 0.182 pCi/g Europium-155 UI 0.00 +/-0.0926 0.0506 +/-0.0926 0.105 pCi/g Lead-212 1.01 +/-0.0819 0.0329 +/-0.0819 0.0685 pCi/g Lead-214 0.828 +/-0.117 0.0423 +/-0.117 0.089 pCi/g Manganese-54 U -0.0228 +/-0.0296 0.0238 +/-0.0296 0.0513 pCi/g Niobium-94 U -0.0353 +/-0.0279 0.0205 +/-0.0279 0.044 pCi/g Potassium-40 12.4 +/-1.15 0.189 +/-1.15 0.431 pCi/g Radium-226 0.673 +/-0.121 0.0445 +/-0.121 0.0947 pCi/g Silver-108m U 0.00475 +/-0.0263 0.0227 +/-0.0263 0.0477 pCi/g Thallium-208 0.382 +/-0.0567 0.0242 +/-0.0567 0.0515 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.00738 +/-0.0142 0.0107 +/-0.0142 0.0255 pCi/g KSD1 09/07/06 1745 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 24

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005C Project: YANK01204 Sample ID: 170256003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 104 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

25

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis o .. .... i s*-

..

et ..

if c .... t C

Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005D Proiect: YANKO 1204 Sample ID: 170256004 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 28.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.01 +/-0:197 0.0659 +/-0.197 0.143 pCi/g MJHI 09/01/06 1221 563436 1 Americium-241 U 0.0605 +/-0.132 0.088 +/-0.132 0.182 pCi/g Bismuth-212 0.534 +/-0.328 0.168 +/-0.328 0.358 pCi/g Bismuth-214 0.594 +/-0.105 0.0384 +/-0.105 0.0813 pCi/g Cesium-134 U 0.0478 +/-0.046 0.0253 +/-0.046 0.0537 pCi/g Cesium-137 0.103 +/-0.0401 0.0181 +/-0.0401 0.0389 pCi/g Cobalt-60 0.148 +/-0.0644 0.0204 +/-0.0644 0.045 pCi/g Europium-152 U 0.00143 +/-0.0589 0.0517 +/-0.0589 0.109 pCi/g Europium-154 U 0.0154 +/-0.0766 0.0653 +/-0.0766 0.142 pCi/g Europium-155 U 0.0625 +/-0.0643 0.0586 +/-0.0643 0.121 pCi/g Lead-212 0.900 +/-0.0831 0.0345 +/-0.0831 0.0714 pCi/g Lead-214 0.854 +/-0.106 0.0372 +/-0.106 0.078 pCi/g Manganese-54 U -0.013 +/-0.0244 0.0203 +/-0.0244 0.0434 pCi/g Niobium-94 U 0.0144 +/-0.022 0.0192 +/-0.022 0.0408 pCi/g Potassium-40 11.6 +/-0.886 0.177 +/-0.886 0.396 pCi/g Radium-226 0.594 +/-0.105 0.0384 +1-0.105 0.0813 pCi/g Silver-108m U 0.0118 +/-0.0187 0.0169 +/-0.0187 0.0357 pCi/g Thallium-208 0.310 +/-0.0591 0.0199 +/-0.0591 0.0422 pCi/g Rad Gas Flow Proportional Counting GFPC,S90, solid-ALL FSS Strontium-90 U 0.000446 +/-0.0198 0.0166 +/-0.0198 0.0376 pCi/g KSDI 09/07/06 1740 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 26

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005D Project: YANKO 1204 Sample ID: 170256004 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 50 (25%-.125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

27

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OIOA Project: YANKO 1204 Sample ID: 170256005 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 60.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.22 +/-0.394 0.120 +/-0.394 0.255 pCi/g MJH1 09/01/06 1221 563436 1 Americium-241 U 0.0503 +/-0.0522 0.0424 +/-0.0522 0.0872 pCi/g Bismuth-212 0.628 +/-0.547 0.277 +/-0.547 0.584 pCi/g Bismuth-214 0.834 +/-0.160 0.0633 +/-0.160 0.133 pCi/g Cesium-134 UI 0.00 +/-0.0832 0.0429 +/-0.0832 0.0903 pCi/g Cesium-137 U 0.0463 +/-0.0542 0.0333 +/-0.0542 0.0703 pCi/g Cobalt-60 U 0.077 +/-0.0516 0.0472 +/-0.0516 0.100 pCi/g Europium-152 U 0.00822 +/-0.0958 0.0766 +/-0.0958 0.160 pCi/g Europium- 154 U-0.000512 +/-0.129 0.0917 +/-0.129 0.199 pCi/g Europium-155 U 0.0659 +1-0.115 0.0674 +1-0.115 0.139 pCi/g Lead-212 0.933 +/-0.111 0.0593 +/-0.111 0.122 pCi/g Lead-214 0.787 +/-0.146 0.0602 +/-0.146 0.125 pCi/g Manganese-54 U -0.0199 +/-0.0442 0.0342 +/-0.0442 0.0725 pCi/g Niobium-94 U -0.0359 +/-0.0364 0.0275 +/-0.0364 0.0583 pCi/g Potassium-40 20.0 +1-1.50 0.288 +/-1.50 0.634 pCi/g Radium-226 0.834 +/-0.160 0.0633 +/-0.160 0.133 pCi/g Silver-108m U -0.00415 +/-0.0338 0.0282 +/-0.0338 0.0591 pCi/g Thallium-208 0.347 +/-0.0918 0.0332 +/-0.0918 0.0698 pCi/g Rad Gas Flow Proportional Counting GFPC,S90, solid-ALL FSS Strontium-90 U 0.00442 +/-0.0146 0.0116 +/-0.0146 0.0274 pCi/g KSD1 09/07/06 1745 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 28

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010A Project: YANK01204 Sample ID: 170256005 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 103 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

29

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010B Proiect: YANKO 1204 Sample ID: 170256006 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 61.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSSGAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.10 +/-0.245 0.0778 +/-0.245 0.168 pCi/g MJHI 09/01/06 1221 563436 1 Americium-241 U -0.00576 +/-0.0366 0.0263 +/-0.0366 0.0543 pCi/g Bismuth-212 0.760 +/-0.351 0.189 +/-0.351 0.402 pCi/g Bismuth-214 0.576 +/-0.139 0.0442 +/-0.139 0.0936 pCi/g Cesium-134 U 0.0332 +/-0.0438 0.0314 +/-0.0438 0.0665 pCi/g Cesium-137 0.0908 +/-0.0468 0.0231 +/-0.0468 0.0493 pCi/g Cobalt-60 0.115 +/-0.0522 0.0225 +/-0.0522 0.0499 pCi/g Europium-152 U 0.00833 +/-0.068 0.0546 +/-0.068 0.115 pCi/g Europium-154 U -0.0828 +/-0.106 0.0808 +/-0.106 0.175 pCi/g Europium-155 U 0.0871 +/-0.0591 0.0504 +/-0.0591 0.104 pCi/g Lead-212 1.08 +/-0.0778 0.0306 +/-0.0778 0.0636 pCi/g Lead-214 0.812 +/-0.0928 0.0385 +/-0.0928 0.081 pCi/g Manganese-54 U 0.0145 +/-0.0313 0.0262 +/-0.0313 0.0557 pCi/g Niobium-94 U 0.00876 +/-0.0271 0.0226 +/-0.0271 0.0479 pCi/g Potassium-40 19.3 +/-1.35 0.236 +/-1.35 0.521 pCi/g Radium-226 0.576 +/-0.139 0.0442 +/-0.139 0.0936 pCi/g Silver-108m U -0.00887 +/-0.0232 0.0191 +/-0.0232 0.0403 pCi/g Thallium-208 0.282 +/-0.0641 0.0224 +/-0.0641 0.0475 pCi/g Rad Gas Flow Proportional Counting GFPC,S90, solid-ALL FSS Strontium-90 U -0.00561 +/-0.0185 0.0162 +/-0.0185 0.0368 pCi/g KSD1 09/07/06 1746 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 30

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010B Project: YANKO 1204 Sample ID: 170256006 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 89 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

31

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-01OC Project: YANK01204 Sample ID: 170256007 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 49.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.05 +/-0.196 0.0698 +/-0.196 0.148 pCi/g MJH1 09/05/06 2124 563436 1 Americium-241 U 0.00111 +/-0.108 0.0862 +/-0.108 0.177 pCi/g Bismuth-212 0.539 +/-0.392 0.142 +/-0.392 0.300 pCi/g Bismuth-214 0.626 +/-0.101 0.0371 +/-0.101 0.0775 pCi/g Cesium-134 UI 0.00 +/-0.0318 0.025 +/-0.0318 0.0524 pCi/g Cesium-137 0.192 +/-0.0408 0.0197 +/-0.0408 0.0414 pCi/g Cobalt-60 0.522 +/-0.0639 0.0211 +/-0.0639 0.0453 pCi/g Europium-152 U -0.0379 +/-0.0596 0.0464 +/-0.0596 0.0966 pCi/g Europium-154 U -0.0318 +/-0.0732 0.0585 +/-0.0732 0.126 pCi/g Europium-155 U 0.0641 +/-0.0925 0.0488 +/-0.0925 0.100 pCi/g Lead-212 1.14 +/-0.0696 0.0264 +/-0.0696 0.0544 pCi/g Lead-214 0.753 +/-0.0911 0.0337 +/-0.0911 0.070 pCi/g Manganese-54 U 0.0134 +/-0.0217 0.0193 +/-0.0217 0.0408 pCi/g Niobium-94 U 0.0073 +/-0.0216 0.0181 +/-0.0216 0.038 pCi/g Potassium-40 17.9 +/-1.02 0.190 +/-1.02 0.412 pCi/g Radium-226 0.626 +/-0.101 0.0371 +/-0.101 0.0775 pCi/g Silver-108m U 0.00496 +/-0.0191 0.0165 +/-0.0191 0.0344 pCi/g Thallium-208 0.354 +/-0.0504 0.0183 +/-0.0504 0.0384 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00471 +/-0.0144 0.0114 +/-0.0145 0.027 pCi/g KSDI 09/07/06 1758 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 32

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OIOC Project: YANKO1204 Sample ID: 170256007 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 101 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

33

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OIOD Project: YANKO 1204 Sample ID: 170256008 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 58.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.920 +/-0.431 0.163 +/-0.431 0.345 pCi/g MJHI 09/01/06 1222 563436 1 Americium-241 U 0.159 +/-0.0868 0.0423 +/-0.0868 0.0871 pCi/g Bismuth-212 0.975 +/-0.615 0.310 +/-0.615 0.654 pCi/g Bismuth-214 UI 0.00 +/-0.170 0.126 +/-0.170 0.259 pCi/g Cesium- 134 UI 0.00 +/-0.0619 0.0563 +/-0.0619 0.118 pCi/g Cesium-137 0.630 +1-0.105 0.037 +/-0.105 0.0784 pCi/g Cobalt-60 2.24 +/-0.161 0.0361 +/-0.161 0.0793 pCi/g Europium-152 U 0.0801 +/-0.100 0.0874 +/-0.100 0.182 pCi/g Europium-154 U 0.159 +/-0.180 0.124 +/-0.180 0.267 pCi/g Europium-155 U 0.0923 +/-0.117 0.0649 +/-0.117 0.134 pCi/g Lead-212 1.10 +/-0.108 0.0414 +/-0.108 0.086 pCi/g Lead-214 0.707 +/-0.194 0.0578 +/-0.194 0.121 pCi/g Manganese-54 U 0.0291 +1-0.050 0.0419 +1-0.050 0.0886 pCi/g Niobium-94 U 0.0114 +/-0.0446 0.0367 +/-0.0446 0.0774 pCi/g Potassium-40 16.4 +/-1.57 0.341 +/-1.57 0.753 pCi/g Radium-226 0.761 +/-0.170 0.0744 +/-0.170 0.156 pCi/g Silver-108m U 0.00643 +/-0.0377 0.0316 +/-0.0377 0.0662 pCi/g Thallium-208 0.396 +/-0.103 0.0362 +/-0.103 0.0763 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.0219 +/-0.0196 0.0135 +/-0.0196 0.0315 pCi/g KSDI 09/07/06 1805 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 34

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OIOD Proiect: YANKO1204 Sample ID: 170256008 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 97 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

35

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033A Proiect: YANKO 1204 Sample ID: 170256009 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 11-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 26.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.28 +/-0.272 0.0796 +/-0.272 0.171 pCi/g MJHl 09/01/06 1223 563436 1 Americium-241 U 0.0199 +/-0.0632 0.0541 +/-0.0632 0.112 pCi/g Bismuth-212 UI 0.00 +/-0.484 0.171 +/-0.484 0.363 pCi/g Bismuth-214 0.920 +/-0.139 0.0421 +/-0.139 0.089 pCi/g Cesium-134 U 0.0188 +/-0.0338 0.0298 +/-0.0338 0.0628 pCi/g Cesium-137 0.709 +/-0.0983 0.0246 +/-0.0983 0.0519 pCi/g Cobalt-60 0.697 +/-0.0935 0.0267 +/-0.0935 0.0577 pCi/g Europium-152 U -0.0119 +/-0.0643 0.0538 +/-0.0643 0.113 pCi/g Europium-154 U 0.0763 +/-0.0741 0.0675 +/-0.0741 0.147 pCi/g Europium-155 Ut 0.00 +/-0.0951 0.052 +/-0.0951 0.108 pCi/g Lead-212 1.13 +/-0.134 0.0457 +/-0.134 0.0938 pCi/g Lead-214 1.04 +/-0.151 0.0416 +/-0.151 0.0871 pCi/g Manganese-54 U -0.0049 +/-0.0275 0.023 +/-0.0275 0.049 pCi/g Niobium-94 U 0.014 +/-0.0236 0.0211 +/-0.0236 0.0446 pCi/g Potassium-40 14.3 +/-1.30 0.185 +/-1.30 0.412 pCi/g Radium-226 0.920 +/-0.139 0.0421 +/-0.139 0.089 pCi/g Silver-108m U3.080E-05 +/-0.0263 0.0202 +/-0.0263 0.0424 pCi/g Thallium-208 0.405 +/-0.066 0.0235 +/-0.066 0.0495 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 0.0366 +/-0.0205 0.0124 +/-0.0205 0.0291 pCi/g KSD1 09/07/06 1807 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 36

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033A Proiect: YANK01204 Sample ID: 170256009 Client ID: YANKOOl Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 99 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

U! Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

37

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd

• East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033B Proiect: YANK01204 Sample ID: 170256010 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 11-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 16.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.03 +/-0.272 0.113 +/-0.272 0.225 pCi/g MJHI 09/01/06 1559 563436 1 Americium-241 U 0.037 +/-0.0519 0.0353 +/-0.0519 0.0705 pCi/g Bismuth-212 0.897 +/-0.563 0.237 +/-0.563 0.473 pCi/g Bismuth-214 0.681 +/-0.143 0.057 +/-0.143 0.114 pCi/g Cesium-134 U 0.062 +/-0.0748 0.0371 +/-0.0748 0.0742 pCi/g Cesium- 137 0.862 +/-0.117 0.0301 +/-0.117 0.0601 pCi/g Cobalt-60 0.944 +/-0.113 0.0281 +/-0.113 0.0562 pCi/g Europium-152 U 0.00733 +/-0.118 0.0695 +/-0.118 0.139 pCi/g Europium-154 U 0.00812 +/-0.115 0.0959 +/-0.115 0.192 pCi/g Europium-155 U 0.0592 +/-0.0677 0.0595 +/-0.0677 0.119 pCi/g Lead-212 0.896 +/-0.109 0.0377 +/-0.109 0.0754 pCi/g Lead-214 0.773 +/-0.141 0.0491 +/-0.141 0.0981 pCi/g Manganese-54 U -0.0465 +/-0.0487 0.032 +/-0.0487 0.0639 pCi/g Niobium-94 U 0.00334 +/-0.0333 0.029 +/-0.0333 0.0579 pCi/g Potassium-40 11.6 +/-1.25 0.247 +/-1.25 0.494 pCi/g Radium-226 0.681 +/-0.143 0.057 +/-0.143 0.114 pCi/g Silver-108m U - 0.00313 +/-0.0324 0.0274 +/-0.0324 0.0548 pCi/g Thallium-208 0.278 +/-0.0682 0.0296 +/-0.0682 0.0592 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00794 +/-0.015 0.0113 +/-0.015 0.0268 pCi/g KSDI 09/07/06 1807 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 38

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033B Project: YANK0 1204 Sample ID: 170256010 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 103 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

39

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East, Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033C Project: YANKO 1204 Sample ID: 170256011 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 11-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 14.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.841 +/-0.277 0.100 +/-0.277 0.212 pCi/g MJHI 09/01/06 1829 563436 1 Americium-241 U 0.028 +/-0.048 0.0331 +/-0.048 0.068 pCi/g Bismuth-212 0.476 +/-0.345 0.223 +/-0.345 0.468 pCi/g Bismuth-214 0.628 +/-0.128 0.0439 +/-0.128 0.0928 pCi/g Cesium-134 U 0.0398 +/-0.0385 0.0344 +/-0.0385 0.0721 pCi/g Cesium- 137 0.609 +/-0.0698 0.0277 +/-0.0698 0.0581 pCi/g Cobalt-60 0.916 -F/-0.0989 0.0255 +/-0.0989 0.0552 pCi/g Europium-152 U -0.0803 -+/-0.0732 0.0581 +/-0.0732 0.121 pCi/g Europium-154 U -0.0175 +/-0.0895 0.0738 +/-0.0895 0.159 pCi/g Europium-155 U 0.0335 - F/-0.0642 0.0553 +/-0.0642 0.114 pCi/g Lead-212 0.710 +/-0.0819 0.0392 +/-0.0819 0.0808 pCi/g Lead-214 0.810 +/-0.110 0.0428 +/-0.110 0.0895 pCi/g Manganese-54 U -0.0149 +/-0.0338 0.0272 +/-0.0338 0.0575 pCi/g Niobium-94 U -0.00772 -+/-0.0304 0.0254 +/-0.0304 0.0533 pCi/g Potassium-40 11.0 +/- 1.00 0.220 +/-1.00 0.484 pCi/g Radium-226 0.628 +/-0.128 0.0439 +/-0.128 0.0928 pCi/g Silver-108m U 0.0295 +/-0.0254 0.0239 +/-0.0254 0.0499 pCi/g Thallium-208 0.237 F/-0.0761 0.0244 +/-0.0761 0.0513 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U -0.0326 +/-0.013 0.0158 +/-0.013 0.0359 pCi/g KSDI 09/07/06 1842 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 40

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033C Proiect: YANKO1204 Sample ID: 170256011 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 90 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

41

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033D Proiect: YANKO 1204 Sample ID: 170256012 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 1 I-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 11.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.800 +/-0.169 0.0584 +/-0.169 0.125 pCi/g MJHI 09/05/06 0531 563436 1 Americium-241 U -0.00757 +/-0.0849 0.0733 +/-0.0849 0.151 pCi/g Bismuth-212 0.514 +/-0.239 0.125 +/-0.239 0.265 pCi/g Bismuth-214 0.496 +/-0.079 0.0289 +/-0.079 0.0614 pCi/g Cesium-134 UI 0.00 +/-0.0333 0.0215 +/-0.0333 0.0454 pCi/g Cesium-137 0.240 +/-0.0466 0.0172 +/-0.0466 0.0365 pCi/g Cobalt-60 0.329 +/-0.0616 0.0159 +/-0.0616 0.0349 pCi/g Europium-152 U -0.0221 +/-0.047 0.0418 +/-0.047 0.0875 pCi/g Europium-154 U -0.0277 +/-0.0651 0.0444 +/-0.0651 0.0974 pCi/g Europium-155 U 0.0409 +/-0.050 0.0464 +/-0.050 0.0959 pCi/g Lead-212 0.618 +/-0.0549 0.0246 +/-0.0549 0.0511 pCi/g Lead-214 0.582 +/-0.0773 0.0304 +/-0.0773 0.0635 pCi/g Manganese-54 U 0.0209 +/-0.0191 0.0165 +/-0.0191 0.0352 pCi/g Niobium-94 U 0.0124 +/-0.0174 0.0157 +/-0.0174 0.0331 pCi/g Potassium-40 10.8 +/-0.796 0.144 +/-0.796 0.320 pCi/g Radium-226 0.496 +/-0.079 0.0289 +/-0.079 0.0614 pCi/g Silver-108m U -0.00363 +/-0.0168 0.0148 +/-0.0168 0.0312 pCi/g Thallium-208 0.222 +/-0.040 0.0156 +/-0.040 0.033 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.020 +/-0.0174 0.0117 +/-0.0174 0.0276 pCi/g KSDI 09/07/06 1842 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 42

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033D Project: YANK01204 Sample ID: 170256012 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 103 (25%6-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

43

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013A Project: YANKO 1204 Sample ID: 170256013 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 17.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.15 +/-0.162 0.0511 +/-0.162 0.109 pCi/g MJHI 09/01/06 1830 563436 1 Americium-241 U 0.0596 +/-0.0865 0.0665 +/-0.0865 0.136 pCi/g Bismuth-212 0.731 +/-0.295 0.115 +/-0.295 0.242 pCi/g Bismuth-214 0.959 +/-0.0845 0.0284 +/-0.0845 0.0597 pCi/g Cesium- 134 UI 0.00 +/-0.0287 0.0195 +/-0.0287 0.041 pCi/g Cesium-137 U -0.00113 +/-0.0196 0.0162 +/-0.0196 0.034 pCi/g Cobalt-60 U -0.00569 +/-0.0174 0.0139 +/-0.0174 0.0301 pCi/g Europium- 152 U -0.0275 +/-0.0539 0.0402 +/-0.0539 0.0837 pCi/g Europium- 154 U -0.0292 +/-0.0495 0.0385 +/-0.0495 0.0835 pCi/g Europium- 155 U 0.0375 +/-0.0594 0.0534 +/-0.0594 0.110 pCi/g Lead-212 1.19 +/-0.0671 0.0261 +/-0.0671 0.0537 pCi/g Lead-214 1.08 +/-0.090 0.0305 +/-0.090 0.0634 pCi/g Manganese-54 U 0.0199 +/-0.0202 0.0165 +/-0.0202 0.0347 pCi/g Niobium-94 U -6.020E- +/-0.0164 0.0143 +/-0.0164 0.030 pCi/g 05 Potassium-40 14.3 +/-0.771 0.130 +/-0.771 0.283 pCi/g Radium-226 0.959 +/-0.0845 0.0284 +/-0.0845 0.0597 pCi/g Silver-108m U -0.00566 +/-0.0152 0.0128 +/-0.0152 0.0268 pCi/g Thallium-208 0.423 +/-0.0539 0.0142 +/-0.0539 0.030 pCi/g Rad Gas Flow Proportional Counnting GFPC,Sr9O, solid-ALL FSS Strontium-90 U -0.00331 +/-0.0151 0.0131 +/-0.0151 0.0304 pCi/g KSDI 09/07/06 1842 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 44

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013A Proiect: YANK01204 Sample ID: 170256013 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 101 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

U1 Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

45

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis t *-i o T

Cet -- ifc --

Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013B Project: YANKO 1204 Sample ID: 170256014 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 19.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.23 +/-0.302 0.0948 +/-0.302 0.190 pCi/g MJH1 09/01/062110 563436 1 Americium-241 U 0.0581 +/-0.0456 0.0383 +/-0.0456 0.0765 pCi/g Bismuth-212 0.606 +/-0.361 0.199 +/-0.361 0.399 pCi/g Bismuth-214 0.990 +/-0.154 0.046 +/-0.154 0.0919 pCi/g Cesium-134 U 0.0447 F/-0.0383 0.033 +/-0.0383 0.066 pCi/g Cesium-137 0.0831 +/-0.037 0.0286 +/-0.037 0.0571 pCi/g Cobalt-60 0.196 F/-0.0645 0.0258 +/-0.0645 0.0515 pCi/g Europium-152 U 0.0248 +/-0.116 0.061 +/-0.116 0.122 pCi/g Europium-154 U 0.0401 +/-0.106 0.0809 +/-0.106 0.162 pCi/g Europium-155 U 0.067 F/-0.0826 0.0584 +/-0.0826 0.117 pCi/g Lead-212 1.32 +/-0.136 0.0337 +/-0.136 0.0674 pCi/g Lead-214 0.989 +/-0.153 0.0431 +/-0.153 0.0862 pCi/g Manganese-54 U -0.00696 F/-0.0306 0.0262 +/-0.0306 0.0523 pCi/g Niobium-94 U 0.00306 F/-0.0256 0.0228 +/-0.0256 0.0455 pCi/g Potassium-40 9.89 +/-0.996 0.207 +/-0.996 0.414 pCi/g Radium-226 0.990 +/-0.154 0.046 +/-0.154 0.0919 pCi/g Silver-108m U -0.017 +/-0.0253 0.0211 +/-0.0253 0.0422 pCi/g Thallium-208 0.456 +/-0.084 0.0253 +/-0.084 0.0505 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00221 /-0.0172 0.0143 +/-0.0172 0.0316 pCi/g KSDI 09/07/06 1843 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 46

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013B Project: YANK01204 Sample ID: 170256014 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 103 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

47

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013C Proiect: YANK01204 Sample ID: 170256015 Client ID: YANKOO1 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 17.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.07 +/-0.236 0.0703 +/-0.236 0.154 pCi/g MJHI 09/01/06 2118 563436 1 Americium-241 U --0.00337 +/-0.0367 0.034 +/-0.0367 0.0701 pCi/g Bismuth-212 0.808 +/-0.311 0.157 +/-0.311 0.341 pCi/g Bismuth-214 0.614 +/-0.118 0.0422 +/-0.118 0.0899 pCi/g Cesium-134 U 0.0481 +/-0.0502 0.033 +/-0.0502 0.0699 pCi/g Cesium-137 0.0789 +/-0.0569 0.0226 +/-0.0569 0.0484 pCi/g Cobalt-60 0.074 +/-0.0564 0.0239 +/-0.0564 0.0531 pCi/g Europium-152 U -0.0203 +/-0.0622 0.0547 +/-0.0622 0.115 pCi/g Europium-154 U -0.0129 +/-0.0828 0.0688 +/-0.0828 0.152 pCi/g Europium-155 U 0.0479 +/-0.0527 0.0529 +/-0.0527 0.109 pCi/g Lead-212 0.903 +/-0.0714 0.0332 +/-0.0714 0.069 pCi/g Lead-214 0.651 +/-0.103 0.0431 . +/-0.103 0.0904 pCi/g Manganese-54 U -0.0163 +/-0.0298 0.0235 +/-0.0298 0.0506 pCi/g Niobium-94 U -0.022 +/-0.0284 0.0226 +/-0.0284 0.0481 pCi/g Potassium-40 12.9 +/-1.11 0.250 +/-1.11 0.553 pCi/g Radium-226 0.614 +/-0.118 0.0422 +/-0.118 0.0899 pCi/g Silver-108m U 0.00256 +/-0.0199 0.0177 +/-0.0199 0.0378 pCi/g Thallium-208 0.248 +/-0.0569 0.0239 +/-0.0569 0.0508 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00157 +/-0.0143 0.0123 +/-0.0143 0.0289 pCi/g KSDI 09/07/06 1845 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 48

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013C Proiect: YANK01204 Sample ID: 170256015 Client ID: YANKOO 1 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 98 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

• QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

49

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013D Proiect: YANKO 1204 Sample ID: 170256016 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 25.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.03 +/-0.160 0.0664 +/-0.160 0.142 pCi/g MJH1 09/05/06 0521 563436 1 Americium-241 U 0.0216 +/-0.0981 0.0845 +/-0.0981 0.174 pCi/g Bismuth-212 0.420 +/-0.350 0.142 +/-0.350 0.301 pCi/g Bismuth-214 0.689 +/-0.0898 0.0339 +/-0.0898 0.0715 pCi/g Cesium-134 U 0.0488 +/-0.0307 0.0247 +/-0.0307 0.0519 pCi/g Cesium-137 0.170 +/-0.0491 0.019 +/-0.0491 0.0402 pCi/g Cobalt-60 0.566 +/-0.0694 0.0198 +/-0.0694 0.0431 pCi/g Europium-152 U 0.0265 +/-0.0524 0.0453 +/-0.0524 0.0946 pCi/g Europium-154 U 0.0628 +/-0.0639 0.0591 +/-0.0639 0.127 pCi/g Europium-155 U 0.0541 +/-0.0561 0.0528 +/-0.0561 0.109 pCi/g Lead-212 0.958 +/-0.0653 0.0265 +/-0.0653 0.055 pCi/g Lead-214 0.784 +/-0.0896 0.0297 +/-0.0896 0.0623 pCi/g Manganese-54 U 0.00917 +/-0.0221 0.019 +/-0.0221 0.0403 pCi/g Niobium-94 U 0.0056 +/-0.019 0.0164 +/-0.019 0.0347 pCi/g Potassium-40 12.6 +/-0.931 0.166 +/-0.931 0.367 pCi/g Radium-226 0.689 +/-0.0898 0.0339 +/-0.0898 0.0715 pCi/g Silver-108m U -0.00656 +/-0.0175 0.0151 +/-0.0175 0.0318 pCi/g Thallium-208 0.314 +/-0.0426 0.0189 +/-0.0426 0.0398 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.00738 +/-0.0147 0.0112 +/-0.0147 0.0265 pCi/g KSDI 09/07/06 1846 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 50

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013D Project: YANK01204 Sample ID: 170256016 Client ID: YANKOOl Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/[racer Recovery GFPC, Sr90, solid-ALL FSS 106 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with .this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

51

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005A Project: YANKO 1204 Sample ID: 170256017 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 17.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.975 +/-0.164 0.0814 +/-0.164 0.174 pCi/g MJHI 09/01/06 2119 563436 1 Americium-241 U 0.0504 +/-0.0306 0.030 +/-0.0306 0.0616 pCi/g Bismuth-212 0.804 +/-0.393 0.165 +/-0.393 0.351 pCi/g Bismuth-214 0.647 +/-0.112 0.0371 +/-0.112 0.0787 pCi/g Cesium-134 U 0.0288 +/-0.0288 0.0271 +/-0.0288 0.0574 pCi/g Cesium-137 0.249 +/-0.0491 0.0255 +/-0.0491 0.0537 pCi/g Cobalt-60 0.682 +/-0.0884 0.0206 +/-0.0884 0.0453 pCi/g Europium-152 U 0.0893 +/-0.0683 0.0526 +/-0.0683 0.110 pCi/g Europium-154 U 0.0167 +/-0.0707 0.0611 +/-0.0707 0.134 pCi/g Europium-155 U 0.00619 +/-0.0524 0.0476 +/-0.0524 0.0982 pCi/g Lead-212 0.912 +/-0.0658 0.0281 +/-0.0658 0.0584 pCi/g Lead-214 0.747 +/-0.0939 0.036 +/-0.0939 0.0755 pCi/g Manganese-54 U 0.0235 +/-0.0494 0.0228 +/-0.0494 0.0486 pCi/g Niobium-94 U - 0.00608 +/-0.0244 0.0201 +/-0.0244 0.0426 pCi/g Potassium-40 10.5 +/-0.910 0.155 +/-0.910 0.351 pCi/g Radium-226 0.647 +/-0.112 0.0371 +/-0.112 0.0787 pCi/g Silver-108m U 0.00189 +/-0.0202 0.0178 +/-0.0202 0.0376 pCi/g Thallium-208 0.322 +/-0.0462 0.0209 +/-0,0462 0.0442 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U - 0.00262 +/-0.0137 0.012 +/-0.0137 0.0286 pCi/g KSDI 09/07/06 1857 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 . 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 52

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005A Proiect: YANKO1204 Sample ID: 170256017 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 92 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

53

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com C~~r*ifpofa -f A nh-SLI~J~.LtLL ~J1 £~IiLtI V ~I3 Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005B Project: YANKO 1204 Sample ID: 170256018 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 10-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 14%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.787 +/-0.187 0.0725 +/-0.187 0.153 pCi/g MJHI 09/02/06 1713 563436 1 Americium-241 U 0.0759 +/-0.0649 0.0382 +/-0.0649 0.0789 pCi/g Bismuth-212 0.403 +/-0.233 0.139 +/-0.233 0.294 pCi/g Bismuth-214 0.636 +/-0.108 0.0306 +/-0.108 0.0647 pCi/g Cesium-134 U 0.0378 +/-0.0274 0.0229 +/-0.0274 0.0482 pCi/g Cesium-137 0.181 +/-0.0421 0.019 +/-0.0421 0.040 pCi/g Cobalt-60 0.710 +/-0.0716 0.0155 +/-0.0716 0.034 pCi/g Europium-152 U 0.0183 +/-0.0466 0.0421 +/-0.0466 0.0881 pCi/g Europium-154 U 0.0204 +/-0.0516 0.0449 +/-0.0516 0.0982 pCi/g Europium-155 UI 0.00 +/-0.0804 0.0458 +/-0.0804 0.0944 pCi/g Lead-212 0.722 +/-0.086 0.0317 +/-0.086 0.0651 pCi/g Lead-214 0.832 +/-0.115 0.0288 +/-0.115 0.0605 pCi/g Manganese-54 U 0.0204 +/-0.0232 0.0192 +/-0.0232 0.0406 pCi/g Niobium-94 U 0.0129 +/-0.0173 0.0161 +/-0.0173 0.0339 pCi/g Potassium-40 9.30 +/-0.895 0.130 +/-0.895 0.291 pCi/g Radium-226 0.636 +/-0.108 0.0306 +/-0.108 0.0647 pCi/g Silver-108m U 0.0081 +/-0.0194 0.0154 +/-0.0194 0.0324 pCi/g Thallium-208 0.299 +1-0.0505 0.0157 +/-0.0505 0.0332 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.0109 +/-0.0167 0.0123 +/-0.0167 0.0293 pCi/g KSDI 09/07/06 1857 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 54

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005B Project: YANKO 1204 Sample ID: 170256018 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 95 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

55

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005C Project: YANKO 1204 Sample ID: 170256019 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 10-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 24.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.810 +/-0.116 0.0431 +/-0.116 0.090 pCi/g MJHI 09/05/06 2143 563436 1 Americium-241 U 0.0147 +/-0.0176 0.0169 +/-0.0176 0.0345 pCi/g Bismuth-212 0.365 +/-0.171 0.099 +/-0.171 0.206 pCi/g Bismuth-214 0.623 +/-0.0633 0.0212 +/-0.0633 0.044 pCi/g Cesium-134 UI 0.00 +/-0.0297 0.0166 +/-0.0297 0.0343 pCi/g Cesium-137 0.113 +/-0.0242 0.0124 +/-0.0242 0.0257 pCi/g Cobalt-60 0.268 +/-0.0379 0.012 +/-0.0379 0.0254 pCi/g Europium-152 U -0.00617 +/-0.0317 0.0284 +/-0.0317 0.0585 pCi/g Europium-154 U -0.0248 +/-0.0417 0.0337 +/-0.0417 0.0714 pCi/g Europium-155 UI 0.00 +/-0.0407 0.0265 +/-0.0407 0.054 pCi/g Lead-212 0.840 +/-0.0404 0.0162 +/-0.0404 0.0332 pCi/g Lead-214 0.686 +/-0.0505 0.0197 +1-0.0505 0.0406 pCi/g Manganese-54 U 0.00306 +/-0.0143 0.0127 +/-0.0143 0.0265 pCi/g Niobium-94 U 0.0053 +/-0.013 0.0112 +/-0.013 0.0232 pCi/g Potassium-40 10.2 +/-0.535 0.0857 +/-0.535 0.186 pCi/g Radium-226 0.623 +/-0.0633 0.0212 +/-0.0633 0.044 pCi/g Silver-108m U -0.0071 +/-0.0113 0.00971 +/-0.0113 0.0201 pCi/g Thallium-208 0.288 +/-0.031 0.0115 +/-0.031 0.0239 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0082 +/-0.0158 0.012 +/-0.0158 0.0284 pCi/g KSDI 09/07/06 1857 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 56

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis of Analvsis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005 C Project: YANKO 1204 Sample ID: 170256019 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 96 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

57

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Cprtifienti- nf AnAlv~ii Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005D Proiect: YANK01204 Sample ID: 170256020 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 10-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 19.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.995 +/-0.411 0.146 +/-0.411 0.291 pCi/g MJH1 09/02/06 1725 563436 1 Americium-241 U 0.0557 +/-0.0479 0.0365 +/-0.0479 0.0729 pCi/g Bismuth-212 0.635 +/-0.589 0.261 +/-0.589 0.521 pCi/g Bismuth-214 0.760 +/-0.165 0.0601 +/-0.165 0.120 pCi/g Cesium-134 U 0.0627 +/-0.0504 0.0463 +/-0.0504 0.0926 pCi/g Cesium-137 0.503 +/-0.0894 0.0338 +/-0.0894 0.0676 pCi/g Cobalt-60 1.72 +/-0.132 0.0307 +/-0.132 0.0614 pCi/g Europium-152 U 0.00265 +/-0.0988 0.0745 +/-0.0988 0.149 pCi/g Europium-154 U 0.0538 +/-0.114 0.0996 +/-0.114 0.199 pCi/g Europium-155 UI 0.00 +/-0.119 0.0591 +/-0.119 0.118 pCi/g Lead-212 1.09 +/-0.126 0.0386 +/-0.126 0.0772 pCi/g Lead-214 0.802 +/-0.135 0.0517 +/-0.135 0.103 pCi/g Manganese-54 U 0.0185 +/-0.0434 0.0383 +/-0.0434 0.0766 pCi/g Niobium-94 U -0.0168 +/-0.0366 0.0309 +/-0.0366 0.0618 pCi/g Potassium-40 10.7 +/- 1. 11 0.276 +/-1.11 0.551 pCi/g Radium-226 0.760 +/-0.165 0.0601 +/-0.165 0.120 pCi/g Silver-108m U -0.021 +/-0.0301 0.0247 +/-0.0301 0.0494 pCi/g Thallium-208 0.343 +/-0.0887 0.0298 +/-0.0887 0.0595 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00322 +/-0.0146 0.0127 +/-0.0146 0.0299 pCi/g KSDI 09/07/06 1857 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 58

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PON 002332 Client Sample ID: 9106-0004-005D Project: YANKO 1204 Sample ID: 170256020 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 99 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

59

QUALITY CONTROL DATA 60

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn QC Summary Report Date: September 8, 2006 Client : Connecticut Yankee Atomic Power Page 1 of 5 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 170256 Parmname NOM Sample Qual - QC Units RPD% REC% Range AnIst Date Time Rad Gamma Spec Batch 563436 QC1201171526 170256001 DUP Actinium-228 0.966 1.01 pCi/g 4 (0%- 100%) MJHI 09/02/06 17:26 Uncert: +/-0.192 +/-0.200 TPU: +/-0.192 +/-0.200 Americium-24 I U 0.0375 U 0.0258 pCi/g 37 (0%- 100%)

Uncert: +/-0.0387 +/-0.075 TPU: +/-0.0387 +/-0.075 Bismuth-212 0.366 0.592 pCi/g 47 (0%- 100%)

Uncert: +/-0.306 +/-0.276 TPU: +/-0.306 +/-0.276 Bismuth-214 0.650 0.690 pCi/g 6 (0%- 100%)

Uncert: +/-0.135 +/-0.0955 TPU: +/-0.135 +/-0.0955 Cesium- 134 U 0.0366 UI 0.00 pCi/g 56 (0%- 100%)

Uncert: +/-0.0355 +/-0.035 TPU: +/-0.0355 +/-0.035 Cesium- 137 0.0666 0.0611 pCi/g 9 (0%- 100%)

Uncert: +/-0.0355 +/-0.0415 TPU: +/-0.0355 +/-0.0415 Cobalt-60 0.104 0.159 pCi/g 41 (0%- 100%)

Uncert: +/-0.0726 +/-0.0325 TPU: +/-0.0726 +/-0.0325 Europium- 152 U 0.00636 U -0.00858 pCi/g 1350 (0%- 100%)

Uncert: +/-0.0728 +/-0.0624 TPU: +/-0.0728 +/-0.0624 Europium- 154 U -0.0788 U 0.00919 pCi/g 253 (0%- 100%)

Uncert: +/-0.0938 +/-0.0602 TPU: +/-0.0938 +/-0.0602 Europium- 155 U 0.0672 U 0.0817 pCi/g 20 (0%- 100%)

Uncert: +/-0.0554 +/-0.0557 TPU: +/-0.0554 +/-0.0557 Lead-212 0.871 0.847 pCi/g 3 (0%- 20%)

Uncert: +/-0.0971 +/-0.0867 TPU: +/-0.0971 +/-0.0867 Lead-214 0.727 0.699 pCi/g 4 (0%- 20%)

Uncert: +/-0.105 +/-0.102 TPU: +/-0.105 +/-0.102 Manganese-54 U -0.00916 U -0.00665 pCi/g 32 (0%- 100%)

Uncert: +/-0.0319 +/-0.0225 TPU: +/-0.0319 +/-0.0225 Niobium-94 U 0.0101 U -0.00339 pCi/g 402 (0%- 100%)

Uncert: +/-0.0244 +/-0.0176 TPU: +/-0.0244 +/-0.0176 61

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 170256 Page 2 of 5 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 563436 Potassium-40 11.3 11.7 pCi/g 3 (0% - 20%)

Uncert: +/-0.986 +/-1.03 TPU: +/-0.986 +/- 1.03 Radium-226 0.650 0.690 pCi/g 6 (0%- 100%)

Uncert: +/-0.135 +/-0.0955 TPU: +/-0.135 +/-0.0955 Silver- 108m U -0.0067 U 0.000104 pCi/g 206 (0%- 100%)

Uncert: +/-0.0208 +/-0.018 TPU: +/-0.0208 +/-0.018 Thallium-208 0.283 0.283 pCi/g 0 (0% - 100%)

Uncert: +/-0.0618 +/-0.048 TPU: +/-0.0618 +/-0.048 QC1201171527 LCS Actinium-228 U 0.254 pCi/g 09/03/06 22:31 Uncert: +/-0.565 TPU: +/-0.565 Americium-241 23.4 24.1 pCi/g 103 (75%-125%)

Uncert: +/-1.28 TPU: +/-1.28 Bismuth-212 U 0.575 pCi/g Uncert: +/-0.944 TPU: +/-0.944 Bismuth-214 U 0.0248 pCi/g Uncert: +/-0.213 TPU: +/-0.213 Cesium- 134 U 0.00032 pCi/g Uncert: +/-0.147 TPU: +/-0.147 Cesium-137 9:58 9.84 pCi/g 103 (75%-125%)

Uncert: +/-0.487 TPU: +/-0.487 Cobalt-60 14.5 14.7 pCi/g 101 (75%-125%)

Uncert: +/-0.660 TPU: +/-0.660 Europium- 152 U 0.125 pCi/g Uncert: +/-0.292 TPU:. +/-0.292 Europium- 154 U 0.0779 pCi/g Uncert: +/-0.277 TPU: +/-0.277 Europium-155 U -0.0876 pCi/g Uncert: +/-0.277 TPU: +/-0.277 Lead-212 U 0.0524 pCi/g Uncert: +/-0.155 TPU: +1-0.155 Lead-214 U -0.103 pCi/g Uncert: +/-0.212 62

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 170256 Page 3 of 5 Parmname NOM Sample Oual OC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 563436 TPU: +/-0.212 Manganese-54 U 0.0306 pCi/g Uncert: +/-0.135 TPU: +/-0.135 Niobium-94 U -0.0513 pCi/g Uncert: +/-0.115 TPU: +1-0.115 Potassium-40 U 0.769 pCi/g Uncert: +/-1.10 TPU: +/-1.10 Radium-226 U 0.0248 pCi/g (75%-1 25%)

Uncert: +/-0.213 TPU: +/-0.213 Silver- 108m U 0.0782 pCi/g Uncert: +1-0.105 TPU: +1-0.105 Thallium-208 U 0.180 pCi/g Uncert: +/-0.177 TPU: +/-0.177 QC1201171525 MB Actinium-228 U 0.0216 pCi/g 09/02/06 17:16 Uncert: +/-0.0479 TPU: +/-0.0479 Americium-241 U -0.0654 pCi/g Uncert: +/-0.0396 TPU: +/-0.0396 Bismuth-212 U 0.110 pCi/g Uncert: +/-0.0705 TPU: +/-0.0705 Bismuth-214 U 0.00843 pCi/g Uncert: +/-0.0317 TPU: +/-0.0317 Cesium- 134 U -0.00203 pCi/g Uncert: +/-0.012 TPU: +/-0.012 Cesium- 137 U -0.00757 pCi/g Uncert: +/-0.0117 TPU: +/-0.0117 Cobalt-60 U -0.00589 pCi/g Uncert: +/-0.0128 TPU: +/-0.0128 Europium- 152 U -0.0169 pCi/g Uncert: +/-0.0308 TPU: +/-0.0308 Europium- 154 U 0.00802 pCi/g Uncert: +/-0.0305 TPU: +/-0.0305 Europium- 155 U -0.00342 pCi/g 63

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 170256 Page 4 of 5 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date. Time Rad Gamma Spec Batch 563436 Uncert: +/-0.0294 TPU: +/-0.0294 Lead-212 U 0.0151 pCi/g Uncert: +/-0.028 TPU: +/-0.028 Lead-214 U 0.00738 pCi/g Uncert: +/-0.0252 TPU: +/-0.0252 Manganese-54 U 0.0127 pCi/g Uncert: +/-0.0111 TPU: +/-0.0111 Niobium-94 U -0.00293 pCi/g Uncert: +/-0.012 TPU: +/-0.012 Potassium-40 U 0.112 pCi/g Uncert: +/-0.173 TPU: +/-0.173 Radium-226 U 0.00843 pCi/g Uncert: +*-0.0317 TPU: +/-0.0317 Silver-108m U 0.00354 pCi/g Uncert: +/-0.0115 TPU: +1-0.0115 Thallium-208 U -0.011 pCi/g Uncert: +/-0.0157 TPU: +/-0.0157 Rad Gas Flow Batch 562563 QC1201169422 170256002 DUP Strontium-90 U 0.00501 U 0.00534 pCi/g 0 (0% - 100%) KSDI 09/07/06 18:59 Uncert: +/-0.0149 +/-0.0155 TPU: +/-0.0149 +1-0.0155 QCI201169424 LCS Strontium-90 1.74 1.57 pCi/g 90 (75%-125%) 09/07/06 19:16 Uncert: +/-0.140 TPU: +/-0.147 QC1201169421 MB Strontium-90 U 0.0172 pCi/g 09/07/06 18:59 Uncert: +/-0.0185 TPU: +/-0.0185 QC1201169423 170256002 MS Strontium-90 1.74 U 0.00501 1.32 pCilg 76 (75%-125%) 09/07/06 19:16 Uncert: +/-0.0149 +/-0.124 TPU: +/-0.0149 +/-0.130 Notes:

The Qualifiers in this report are defined as follows:

64

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 170256 Page 5 of 5 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

65

General Narrative Page 1 of 105

CASE NARRATIVE For CONNECTICUT YANKEE RE: Soil PO# 002332 Work Order: 168404 SDG: MSR #06-0652, 06-0675, 06-0687, 06-0688, 06-0707, 06-0743, 06-0755 August 15, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:

2040 Savage Road Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina on May 5, May 9, May 12, May 17, May 26, June 2, June 8, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.

The laboratory received the following sample(s):

Sample ID Client Sample ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006. 9106-0004-015F 168404007 9106-0005-01 OF 168404008 9106-0005-014F 168404009 9106-0006-005F GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP INC.

P.O. Box 30712

• Charleston, SC 29417

• 2040 Savage Road (29407)

Page 2 of 105 Phone (843) 556-8171

• Fax (843) 766-1178

• www.gel.com

168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F Items of Note:

At the request of Dale Randall on July 20, 2006, GEL analyzed the above samples according to the spreadsheet in the attached email.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.

Analytical Request:

Seven soil samples were reanalyzed for FSSALL, except gamma and Sr-90.

Four soil samples were reanalyzed for FSSALL, except gamma and Ni-63.

Two soil samples were reanalyzed for FSSALL, except gamma.

Two soil samples were reanalyzed for FSALL, except gamma, Sr-90 and Ni-63.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

PO. Box 30712

• Charleston, SC 29417 ° 2040 Savage Road (29407)

Phone (843) 556-8171

• Fax (843) 766-1178

• www.gel.com Page 3 of 105

. I I:

Additional HTD analyses

Subject:

Additional HTD analyses 1(, 8,LI 0 (4,1, From: "Dale Randall" <randall@cyapco.com>

Date: Thu, 20 Jul 2006 11:04:54 -0400 To: "Cheryl Jones" <cj @gel.corn>

CC: "Clyde Newson" <Newson@CYAPCO.com>, "John McCarthy" <McCarthy@ CYAPCO.com>

Cheryl:

Per our earlier discussion, attached is a list of samples that we would like to have analyzed to the FSSALL protocol. I have included a list of test protocols performed on each sample to date. Once you have had an opportunity to determine our options for each sample please call or e-mail me at your convenience.

Thank You, Dale (860) 267-3133 Content-Description: GEL FSSALL analyses request.xis GEL FSSALL analyses request.xls Content-Type: application/vnd.ms-excel Content-Encoding: base64 Page 4 of 105

,Iof I 8/2/2006 7:04 PM

Done To be done Previous IGEL ID CY sample location IDs FSS Gain Sr-90 N,-63 Am Pu SrgO Pu241 Fe55 Ni63 Tc99 H3 C14 lq164220008 9106-0002-007F x x x x x x x x x x U,164220012 9106-0002-011 F x x x x x x x x x x p 162335004 9106-0003-004F x x x x x x x x x x

.1162335014 .9106-0003-015F x x x x x- x x x x _x

• 162832015 9106-0004-005F x xx x x x x x x x 162832009 9106-0004-015F x x x x x x x x x X 162485008 9106-0005-01 5F x x x x x x x x x x 162485011 9106-0005-014F x x x x x x x x x x 162850014 9106-0006-005F x x x_ _ x x x x x x 163741005 9106-0008-006F x x x x x x x x x x 163741009 9106-0008-008F x x x x x x x x x x 164542008 9106-0009-002F x x x x x x x x x x 164542003 9106-0009-017F x x x x x x x x x x 163105009 9106-0010-001 F x x x x x x x x x x 163105016 9106-0010-012F x x x x x x x x x x

Chain of Custody and Supporting Documentation Page 6 of 105

1462: o L(

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major

~Chain of Custody Form Connecticut Yankee Atomic Power Company No. 2006-00371 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones o u* SL Priority: [ 30 D. [ 14 D. [ 7 D. container Sample Size-. L 47J2q _Z Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0002-OO1F 5/17/06 10:42 SE C BP X X Transferred from COC 2006-00357 9106-0002-002F 5/18/06 09:43 SE C BP X Trans*rred from COC 2006-00361 9106-0002-003F 5/18/06 10:14 SE C BP x x Transferred fromi COC 2o06-00361 91 06-0002-004F 5/18/06 10:39 SE C BP x x Transferred from COC 2006-00361 9106-0002-005F 5/18/06 12:49 SE C BP x x Transferred from COC 2006-00364 9106-0002-006F 5/18/06 13:14 SE C BP X X Transferred from COC 2006-00364 9106-0002-006FS 5/18/06 13:14 SE C BP X X Transferred from COC 2006-00364 9106-0002-007F 5/18/06 13:37 SE C BP X X Transferred from COC 2006-00364 9106-0002-008F 5/18/06 14:04 SE C BP X X Transferred from COC 2006-00364 NOTES: PO #: 002332 MSR #: 06- SSWP# NA Z LTP QA [] Radwaste QA [ Non QA Samples Shipped Via: Internal

[15 Fed Ex Container UPS Temp.:

Deg. C

[ Hand Custody Sealed?

I Re q, h Date/Time 2, l~ived By

2) Date/Time Custody Seal

O Cý1 (Other Intact?

• Relinquish-ed Date/Time 4) Received By Date/Time BillofLading ___YO No

-5)Relinquished By Bill of Lading #5 Date/Time 6) Received By Date/Time 7 ' '"65 /

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 1 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00372 CD 00 362 Injun Hollow Road, East Hampton, CT 06424 q 860-267-2556 Project Name: Iaddam Neck Decommissioning Analyses Requested Comments:ly

" Lab Use Only Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones C a container Priority: Z 30 D. ] 14 D. El 7 D.

Sample Size-SampleDesignation SM leDsintinmediaDate Time CMde Type Code &Type Code Comment, Preservation Lab Sample ID 9106-0002-009F 5/18/06 14:28 SE C BP x Transferred from COC 2006-00364 9106-0002-01OF 5/18/06 14:50 SE C BP x x Transferred frm COC 2006-00364 9106-0002-01IF 5/19/06 08:10 SE C BP x x Transferred from COC 2006-00365 9106-0002-012F 5/19/06 08:31 SE C BP x x Transferred from COC 2006-00365 9106-0002-013F 5/19/06 09:00 SE C BP X X Transferred from COC 2006-00365 9106-0002-014F 5/19/06 09:58 SE C BP X X Transferred from COC 2006-00365 9106-0002-014FS 5/19/06 09:58 SE C BP X X Transferred from COC 2006-00365 9106-0002-015F 5/19/06 10:29 SE C BP x x Transferred from COC 2006-00365 9106-0002-016F 5/19/06 13:19 SE C BP x x Transferred from COC 2006-00365 NOTES: PO #: 002332 MSR #: 06- SSWP# NA (9 LTP QA El Radwaste QA fl Non QA Samples Shipped Via: Internal 0'755 E Fed Ex Container 0 UPS Temp.: _

Deg. C C Hand Custody fReln~he* Sealed?

1 . Date/Time- 2) R*e~ved By' Dat§(Time Custody Seal M u~ - 4r C Other Intact?

3)'lelinquished By Date/Time 4) Received By Date/Time _ __ _ Y N Bill of Lading

5) Relinquished By Date/Time 6) Received By Date/Time 7W09 Y/176

Connecticut Yankee Statement of Work for Analytical Lab Services ("- .CY-ISC-SOW-O01 Figure 1. Sample Check-in List Date/Time Received* * '

SDG#: - (0 6 5 Work Order Number: (GLI'd Z ) .

Shipping Container ID iOý_ ,  %/95591 Chain of Custody 40o oo- 9

1. Custody Seals oni shipping container intact?.. Yes No [ ]

2. Custody Seals dated and signed? Yes No [.

3. Chain-of-Custody record present? Yes No ]

.4. Cooler temperature "

5. Vermiculite/packing materials is:. Wet [] Dry 6:w -Number of samples in shipping container: _

7. Sample holding times exceeded? Yes [ 3 No

8. Samples have:

-*___ hazard labels

_2.ustody seals *appropriate sample labels

9. Samples are:

-- in good condition . leaking

-broken -have air bubbles

10. Were any anomalies identified in sample receipt? Yes[ ] NOX]

IL.. Description of anomalies (include sample numbers):

Sample Custodiaa/Laboratory(: i izti* Dates ,* -O(o Telephoned to:_ On By t*

Page 9 of 105

Connecticut Yankee

-CY-ISC-SOW-OOI Statement of Work for Analytical Lab Services Figure 1. Sample Check-in List Date/Time Received? '  %

SDG#: AAx-SfO(O O"-$j Work Order Number: i(0ckzz (,

Shipping Cdhtaiaer ID.- -5902." Chain of Custody#* 0 OV (t7 I. Custody Seals or shipping container intact? Yes No [)

2. Custody Seals dated and signed? Yes No [ I

3. Chain-of-Custody record present? (Q Yes ] No.[]

4. Cooler temperature Wet [ ] Dry 1J~.

5. Vermiculite/pacling materials is:

6. Number of samples in shipping container. -

7. Sample holding times exceeded? Yes []No.

8. sam.Sms have:.

_tape . h hazard labels

_custody seals .aporaesample labels

9. Samples are-.

good condition leakig

---broken -have air bubbles

10. Were any anomalies identified in sample receipt? Yes [I No

11. Description of anomalies (include sample numbers):

Samn ie usdian/Laboratorv- C(Algj 2L'i Date.. ~

Telephoned to: On 1:hJ

• J Page 10 of 105

SSAMPLE ESAMPLE RECEIPT & REVIEW FORM

-. 'S VIIO I" Mueol Client: ('ot~)flna?4-jr,c Ank%- 1 es SDG/ARCOC/Work Order:- Y{~

Date Received: (, P10 PM(A) Review (ensure non-contorming items are resolved prior to signing);

jReceived By: C_)"

Sample Receipt Criteria i Comments/Qualifiers (Required for Non-Conforming Items)

Circle Applicable: seals broken damaged conainelC container other (describe)

Shipping containers received intact and sealed? 7 Samples requiring cold Circle Coolain # ice bags blue ice dry ice none other describe) 2 preservation within (4 +/- 2 C)?

Record preservation inethod. 7 Chain of custody documents - "

included with shipment?

Sample containers intact and imcic Applicab e.

5 s broken damaged container leaking container other (describe) sealed? 7" 5 Samples requiring chemical .536iD's. continers affected and observed pH:

preservation at proper pH? I'll..

VOA vials free of headspace Sample ID's and containers affected:

6(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) ,__ _

holding Id's and tests affected:

8 Samples received wi l time? ___O_

9 Sample ID's C match ID's Sample ID's and containers affected:

on bottles?ý Date &xmeon COC match date Sample ID's affected:

& tiro6 on bottles?

N4v er of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in relinquished/received sections? Co'.c* 00Q - 003 -1 14Air Bill ,Tracking Fs, &

Additional Comments Sset'in" I

• RSO RAD Receipt #

• Hfa>x2 area background is observed on samples identified as "non-Suspected Hazard Information ' * ~ *, regulated/non-radioactive", contact the Radiation Safety group for fIurther investigation.

A lRadioh-icalClassficin?

l 1MxmrConsOsre* , 6 Cpe7e7 BPCB Regulated? V " rnomlenls:

gShipped as D01' Hazardous C Material? If yes, contact Waste -azard Class Shipped:

JN#:

.Manager or ESH Manager.

I PM (or PMA) review of Hazard classiticarion: Initials (.L- Date-LO/47,I.

I Page 11 of 105 ti,

SAMPLE RECEIPT & REVIEW FORM PM use only Client: ?m vpl;tQ Y ric SID/ARCOC/Work Order: /C.9'ZW(

PM(A) Review ( e ofor i e resolved prior to signing):

Date Received: - O~o "Received ,I!-

By:

Sample Receipt Criteria Comments/Qualifrers equired for Non-Conforming Items)

J sirdecontainers received intact Shipping I APpliCable: seals brkcoaner leaking container dry ice none othe (describe) other describe) ooant 2LI# Tags blue ice

.iarprI e Is uiring old 2 jpreservation within (4 +/- 2 C)?

1Record preservation method. I . I 3 'Chain °of custody documents included with shipment? ic pplicable: Seals broken damaged container lenking contaie h0er (describe) and Sample containers intact 4[sealed?

fSamples requiring chemical Sample ID's. containers affected and observed PH:

Jpreservation at proper pH?

j S Sample ID's, and containers aff.cte.d.

6 IVOA vials free of headspace I(defined as <z 6mm hiihhlel?--,

fAre Encore containers present?

7 [(If yes, immediately deliver to

[.VOA laboratory) 8tSamples received within holdin Id's and tests affecte*:

time?

9Sample ID's on COC matc D's Sam.ple ID's and containers affected:

on bottles? am* .Ds 10Date 10Dt ie onnCC

& time COC thdt thdate apeI' fetd fetd

& time on bottles?

Number of contamine received Sample ID's affected:

match number indic ted on COC?

1 Clform is pro ny signed in reiguse/rec~eved_.7 sections? O-" .* -E,, O ,[l, 14 Air Bill ,Tracking #'s, &

Additional Comments Z RSO RAD Receipt #_____ ________

Suspected Hazard Information -.

• -2 " n*If > x2 area background is observed on samples identified as -on.o

~r A . regulated/non-radioactive" contact the Radiation Safety group for fur-ther 4Z4 a investigation.

M Observed*a

.adiologicalCous A

OU "" Coments:

C Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. UN#:

PM (or PMA) review of Hazard classification: Initials Date:

V Page 12 of 105

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-00 I Major Chain of Custody Form M* Connecticut Yankee Atomic Power Company

-362 Injun Hollow Road, East Hampton, CT 06424 :Z 4 .

860-267-2556 Q 0 Project Name: Haddam Neck Decommissioning Analyses Requested _Lab Use Only Contact Name & Phone: '2oments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories < 0 2040 Savage Road. Charleston SC. 29407 0 9 843 556 8171. Attn. Cheryl Jones C Priority: Z 30 D.E] 14 D. [3 7 D. Container Sample Size-Media Type &Type Lb" Sample Designation Date Time Code Code Code Comment, Preservation Lab Sampi:iple .

tO 9106-0003-OOIF 4/24/06 14:13 SE C BP x Transferred from COC2006-00221 P 9106-0003-002F 4/24/06 14:39 SE C BP X Transferred from COC2006-00221

! 9106-0003-003F 4/24/06 15:01 SE C BP X Transferred from COC2006-00221 9106-0003-004F 4/25/06 08:41 SE C BP X Transferred from COC2006-00223 9106-0003-004FS 4/25/06 08:41 SE C BP X Transferred from COC2006-00223 9'106-0003-05F 9106-0003-006F 4/25/06 4/25/06 09:2 1 SE C BP X "Transferred from COC2006-00223 09:46 SE C BP X Transferred from COC2006-00223 0 9106-0003-007F 4/25/06 10:28 SE C BP X Transferred from COC2006-00223 9106-0003-008F 4/25/06 11:15 SE C BP I X Transferred from COC2006-00223 NOTES: PO #: 002332 MSR #: 06-0" SSWP# NA ED LTP QA E Radwaste QA Non QA Samples Shipped Via: .nternalfl.iraer Combined samples 9106-0003-003F taken on 4/25/06 (@08:19 and 9106-0003-003FB taken on 4/25/06@ 08:19 in order to have sufficient sample for counting. [ Fed Ex ,eýP;.J Deg. r El UPS .... ,:,:", ,.:

UHandCstdSal?

1) Relinquished

.ec.ived By Date/Time 2) By 1 Date Time CtustOdy Seal.Itact-'?

{(,Y'*'j ),oa, td  %'..*/s/t IO L] Other

3) Relinquished By Date/Time 4) Received By Dab/TimeN Bill of Lading #

5) Relinquished By Date/Time 6) Received By Date/Time

• V 2 - 'c/-

.2 0 2 40

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Helh hscsPoedr GPGGRR 0403Atahmn -C-0I iao Chain of Custody Form Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 c

860-267-2556 --- -ny R e , °/.

Project Name: Haddam Neck Decommissioning Analyses Requestei -

L, Contact Name & Phone: will, Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 0 c 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D.E] 14 D.[] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation ")i ple 112 A 9106-0003-009F 4/25/06 13:00 SE C BP X Transferred from CCC 2006-00236 .

0ii0 9106-0003-OIOF 4/25/06 13:23 SE C BP X Transferred from COC 2006-00236

\ 9106-0003- 010FS 4/2 5/06 13 :23 SE C BP x Tr.nsferred from COC-2006-00236 4/25/06 15:12 SE C BP X Transferred from COC 2006-00236 tk 9106-0003-012F 4/25/06 14:21 SE C BP X Transferred from COC 2006-00236 0t 9106-0003-013F 0Cj 9106-0003-013F 4/25/06 14:48 SE C BP x Transferred from COC 2006"0236 9106-0003-014F 4/25/06 14:48 SE C BP X Transferred from COC 2006-00236 0

i, 9106-0003-015F 4/26/06 08:16 SE C BP xXTransferred Transferred from COC 2006-00237 1:..*, .-

C 9106-0003-016F /2/6 041 S C BP from COC 2006-00237 I"*'*: * .2.;""

.:-.:":.:.i:*":

9106-0003-017F 4/26/06 09:18 SE C BP x Transferred from CCC 2006-00237 ..

9106-0003-018F of 4/26/06 4/6/06 08:59 08:5 SE C BP x Transferred from COC 2006-00237 "

• NOTES: PO #: 002332 MSR #: 0 6 - 0&2- SSWP#NA S LTP QA [I RadwasteQA E] Non QA Samples Shipped Via:

Z Fed Ex UPS Jre~p Sc'pW.

LI Hand

1) Relinquished By Date/ime 2) Received By Datfl'ime eal'E 3J)Reli4nzquich S-By Dte/5mO e 4 0ReeiBy c_5° LI Other D/iOme1

3) Relinquished By Date/Time 4) Received By Date/Time Bill of Lading #

TWy2O-gY/Žl'- 0261

Connecticut Yankee CY-ISC-SOW-O01 Statement of Work for Analytical Lab Services Figure 1. Sample Cheek-in List Date/Time Received: ., t {/O*-

SDG#: o &&2-Work Order Number:- (Z -

17t(3 6 VU'-6 O I Chain of Custody##)U? (, .

Shipping Cdotainer ID:.

,.. It OZ-IC) y . 0 1.

• [ ] No '

1. Custody Seals. od shipping container intact?

2. Custody Seals dated and signed? Yes [ jNo

3. Chain-of-Custody record present? Yes No [L

4. Cooler temperature , C_

5. Vermiculite/packing materials is: Wet [] Dry.'] fl /_

6.. Number of samples in shipping container: nt .I - "

7- Sample holding times exceeded? Yes [ No JKL

.8. Sapls

-tape __hazard labels

• c*cutody seals .appropriate sample labels

9. Samples are:

good condition *":*leaking

-broken -___have air bubbles

10. Were any anomalies identified in sample receipt? Yes [ ] No Q4

11. :Description of anomalies (include sample numbers):

Sample Custodian/Laboratory: L* f*L.i*' CC4"L Date.: .ý51 -) .

Telephoned to: On By.

Page 15 of 105

0 SAMPLE RECEIPT & REVIEW FORM i.

PMuaneomly jV(a 2 33 Client: ,SDG/ARCOC/Work Order:

Date Received: ra ?)4 5 6 (e. PM(A) Review (ensure atncu tm are resolved prior to signing):

Sample Receipt Criteria Z Comments/Qualifiers (Required for Non-Conforming Items)

Circle Applicable: seals broken danmaged container leaking container ohr (describe)

I Shipping containers received intact and sealed? , _t= I'll Samples requiring cold Circle Coolant # ice bags blue ice dry ice none aib e 2 preservation within (4 +/- 2 C)?

Record preservation method. _.. Pen n..

Chain of custody documents included with shipment?

4 Sample containers intact and Circle Applicable: seals broken damaged comainer leaking container odier (describ) sealed?

Samples requiring chemical Sample ID's, containers affected and observed pH:

preservation at proper pH?

VOA vials free of headspace Sample ID's and containers affected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)

Id's and w afeted 8 Samples received within holding time?

9 Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles?

Date & time on COC match date Sample In's affected:

& time on bottles?

Number of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in V relinquished/received sections?

Air Bill ,Tracking #'s, & de 4-- C-Additional Comments C.-- 0 "a a RSO RAD Receipt#

Suspected Hazard Information 8SsceH ad-o

- *If > x2 area background is observed on samples identified as "non-

. - U regulated/non-radioactive", contact the Radiation Safety group for further 1I investigation.

A lRadiological Classification? Maximum Counts Observed*:

[B PCB Regulated? . Comments:

hippea'as HazardousS' COa C Material? If yes, contact Waste Hazard Class Shipped:

[Manager or ESH Manager. UN/:

PM (or PMA) review of Hazard classification: Initials Date:

t I Page 16 of 105 a*

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-00 1 Major Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424

ýProject Name: Haddam Neck Decommissic

ýDontact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: 0 30 D.] 14 D. El 7D.

Date Samples Shipped Via:

0 Fed Ex 0l uPs 0] Hand

[I Other Bill of Lading #

"-Health Phys,,Pr~edure GPP-GGGR-R5104-003-Attachment B-CY-00 1 Major Yankee Atomic Power Company

".. j*junHollow Road, East Hampton, CT 06424 860-267-2556 t Name: Haddam'Neck Decommissioning Contact Name & Phone:

Jack McCarthy" 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: M 30 D. [] 14 D. M 7 D.

Samples Shipped Via:

[ Fed Ex O UPS

[] Hand

[] Other Bill of Lading N 477/c/7:3xlrF9Z

Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Check-in List Datc/Timc Rcccivcd: X_ Z2. 0G 69 , ,,2a SDG#: /6tf ( O6, Work Order Number:- &-' 3 2 1 Shipping ContainerlD: "1i 9Z,15" 8812- Chain of Custody #.- ooo - 60S3.7

1. Custody Seals on shipping container intact? Yes No [3

2. Custody Seals dated and signed? Yes No []

3. Chain-of-Custody record present? Yes No []

4. Cooler temperature ..

I

5. Vermiculite/packing materials is: Wet JA Dry [ ]

6. Number of samples in shipping container:.

7. Sample holding times exceeded? Yes [ ] No

8. Samples have:

_. tape hazard labels

. custody seals appropriate sample labels

9. Samples are:

_ in good condition __.jeaking broken have air bubbles

10. Were any anomalies identified in sample receipt? Yes No [I II. Description of anomalies (include sample numbers):

Sample Custodian/Laboratory: J -.i, ' Date: *.o 6. -,,.o Telephoned to: On By Page 45 of 56 Page 19 of 105

Connecticut Yankee

-Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Chcck-in List Date/ime Received.

SDG#:

Work Order Number:_ ___ ___ __

hippin. Chain of Custody I. Custody Sea.ls oi shipping container intact?.. -Yes [ J No No

2. Custody Seals dated and signed? Yes[ ].No

3. Chain-of-Custody record present? Yes '4 No []

4. Cooler temperature

5. VermiculJtedlpacng materials is: Wet E, Dry t\]

6. 1Number of samples in shipping container' _ _ _ _"_"_; _ _

7. Sample *holding times exceeded?

-N Yes [],.No

10. Were,any anomlies identified nsamplereceipt? Yes ' No [in Ii .Decipton of anOnaliies(include sample nmes:~ I~a

-~

~ - i~~

$ampjeý~(Y Cusori-----------

• Sample C~zr C." .

t~dianLaborat

.

~ .

(J~)*~~D

.

ate :_ _ _ _ __

..

_

.

_

.-- ,=,7Y.

_

tyo- Onch~e Page 20 of 105 r"

S SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM

-Fed F. Y- Tvk-ni csI, (tKo r ,-

--- -- anln kc(\ OO3 0

--:5,u C(. ")

-'-iq(a 1055 Asxmai 0(3 53 0 -: i Y,*

.* _- _________-- o_ _5_, __,_-_________

1 00 ls_ __ _ _ V_ _

hLL5Pcnje- 5 CLr oLi.

Page 21 of 105

,!1I

SAMPLE RECEIPT & REVIEW FORM PM use only Client: iSDGIARCOCWork Order: 1(e 2' 37-ate Received: , FM(A) Review (ensare non-conforming items are resolved prior 6o signing).

eceived By:- _ _._ _ _ _ _,_,

Sample Receipt Criteria

• Comments/Qualifiers (Required for Non-Conforming Items)

Shipping containers received intact Circle Applicable: seals broken damaged container leaking container other (describe) 1and sealed? x Samples requiring cold ircle Coolant # ice bags blue ice dry ice noe oher describ) 2 preservation within (4 + /- 2 C)?

Record preservation method.___________ _____________

Chain included of custody documents with shipment?..

SiSample containers intact and Circle Applicable: seals broken damaged container l<E taw other (describe) sealed?

5 Samples requiring chemical A -( 'N:

Smple JDs.con*.aine 91 -e- 0 01-affected and obsered pH1

_preservation at proper pH?..

6 VOA vials free of headspace Sample ID's and containers affected:

6(defined as < 6mm bubble)?__________________________

Are Encore containers present?

7 (If yes, immediately deliver to

-VOA laboratory) 8 Samples received within holding Id's and tests affected:

time?

Sa M's and continr aff '

9 on Sample ID's on COC match ID's bottles? ,_i Date & time on COC match date 1 a le ID's affected:

10 & time on bottles? __ _

Number of containers received Sample ID's affected:

11" match number indicated on COC?

COC form is properly signed in 2relinuihed/recived sec*tions?1 . A -* o4 jc,.,.,,i*

Air Bill ,Tracing Ps, &

Additional Comments

.. *HA. Kece"pti____________________

JDRAD Receipt #.:.

• If>x2 area b roun is oberved on sples idnifed as u-.non-Suspected -Hazard Information z0 regulated/non-radioactive", contact the Radiation Safety group forfurther u--I investigaion.

A I'Atdrologicad .0asific~iin. 'sift u1111Counts Oberved*: <

.B CB Regulated?

,as .IJ Hazardous 1

1 C Material? If yes, contact Waste Flazard'Clms Shipped; I.

Manager or ESH* Manager.

y P~j~fj~yj~w of Hazard classific2rinn' J Illlleall*

-1,oeM V c of Haar clsifctinate.,5 UI

SAMPLE RECEIPT & REVIEW FORM Phi use only client:

Date Received:

Received By:

Vrin Vo C c cC=

I SDG/ARCOCIWork Order:

PM(A) Rfvr

.

/6 Z I' 2- A.

mloIm km. resolved prior to sigting):

. . I Sample Receipt Criteria i Comments/Quallfiers (Required for Non-Conforming Items)

Shipping containers received intact 1icle Aplktable ses brken daMaged container leaking cormiw odwr (describe) and s-aled? __..-._-__ _ _ _ _

otr describe)

.

Samples requiring cold Circle CoWlaN I ice bags blue ice dry ieC 2 preservation within (4 +/- 2 C)?

Record preservation method.

Chain of custody documents U) Us C I_> \ t-LV included with shipment? Vcn0e Sample containers intact and G* ¶!m ' dartiged cotainer ,lting com'r , (d

-sealed? k %,7)/

Samples requiring chemical S ID's. containers affected and observed pH:

preservation at proper pH? 1 VOA vials free of headspace Sample ID's and containers affeced:

6 (defined as < 6mm bubble)? ,_ _ _... ...

Are Encore containers present?

7 (If yes, immedialely deliver to VOA laboratory)__

Id's amd tesu affected 8 Samples received within holding time?

9 Sample ID's on COC match ID's Sanp ID°Y and co..nie-- affecied:

on bottles?

Date & time on COC match date Satl-i_ Io's affected:

& time on bottles?

Number of containers received ID'S affecd:

match number indicated on COC?

COC form is properly signed in AC) CG,*Cs " , y1 ru t 7;i C*C(

relinquished/received sections? .. .. ....

Is CACifp) 1Cd- _.-.-

Air Bill ,Tracking #'s, & E Additional Comments

[O RAD Receipt _

pcte *If > x2 areabackground is observed on samples identified as non-Suspected Hazard Information f

@0gulaled/non-radioacive'. contact the Radiation Safety group for further

_investigation.

A Raiological Classification? Maximum Counts Observed-:

'C!j Regulated? 1VComments:

ripped as Hazardous a o =

c Material? If yes, contact Waste H r Class Shipped:

NManager or ESH Manager. UN#:

PM (or L FA) review of Hazard class1*aon: I Fage 23 of In,;

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major HelhPyisPoeueGPGG-51403Atcmn B-C ii0 Mao Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424

)jectName: Haddam Neck Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D.[] 14 D. M 7 D.

0] Other Bill of Lading #

7'q9Z 1 '9S

Connecticut Yankee Statement of Work for Analytical Lab Services .CY-ISC-SOW-O01 Figure 1. Sample Check-in List Date/Time Receivei':

• oc.

SDGj#:

Work Order Number:- L- ,

Shipping CCntainer ID: , t%" 5-2 . Chain of Custody I& e,0 3L I. Custody Seals ori shipping container intact? .Yes4No[]

2. Custody Seals dated and signed? Yes 4".No [.

3. Chain-of-Custody record present? " Yes IlNo NO

.4. Cooler temperature Ig q -.°'

5. Vermiculite/packing materials is:

Wet (

t\Dry

6. Number ofsamples in shipping container:

7- Sample holding times exceeded?

Yes [NoL4

10. Were any anomalies identified in sample receipt? Yes [ No I*"

11. .Descriptionof anomalies. (include sample numbers):

• : ' " ' " " ' " °.

,.Page 25 of 105

SAMPLE RECEIPT & REVIEW FORM PM use only ClientSDG/ARCOCWork Order: (( Z 8 Date Received: PM(A) Review (ensure non-coiiro g items are resolved prior to signing):

Sample Receipt Criteria  ; Comments/Qualifiers (Required for Non-Conforming Items)

'," Shipping containers received intact Circle Applicable: seals broken damaged container leaking container oftr (describe) a"i*msealed? I..

Samp requiring cold Circle Coolant # ice bags blue ice dry ice none other describe) 2 preservai'within (4 +/- 2 C)?

• Record preserv' *n method.

3Chain of custody d nts included with shipment? _ ____ __

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking comainer other (describe) sealed? I Samples requiring chemical Sample ID's. containers affecwd and observed pH:

preservation at proper pH? 1_ _,_..

6 VOA vials free of headspace IsnuSle ID's and containers affected:

(defined as < 6mm bubble)? *x /},

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)"6LP 8 Samples received within holding Id's and t time?

Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles? ,.. ...

10 Date & time on COC match date Sample ID's affected:

& time on bottles?

Number of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in 12 relinquished/received sections?

"q 1 5 4?5 /70 14 Air Bill ,Tracking #'s, &

Additional Comments q2&o, q*c- -

W RSORAD Receipt # __

Sr *If > x2 area background is observed on samples identified as "non-S Ha n regulated/non-radioactive", contact the Radiation Safety group for further F investigation.

A JRadiological Classification? Maximum Counts Observed*:

PCB Regulated? 0, Comnmrlrts:

fShipped as IJUr Hazardous .00 t ardCssSip:

C Materi? If yes, contact Waste Hazard Class Shipped:

NManager or ESH Manager. I PM (or PMA) review of Hazard classification: initials D 77 j /o U

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424

.860-267-2556

"?roject Name: Haddam Neck Decommissioning

ý2ontact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D. [] 14 D. EI 7 D.

Samples Shipped Via:

0 Fed Ex El ups 0J Hand

[] Other Bill of Lading # 4,411

-7 o- 9.00o-

Connecticut Yankee Statement of Work for Analytical Lab Services Cy-ISC-S0W-001 Figure 1. Sample Check-in List.

DaterTime Received: 4 11 o , *(i" SD G #: A. A.7-( (0 .0 Work Order Number _ _4.7_ _ _ _ _ _

Shipping .Coaner 113:ý 3M 0'_

ShppngchtainrD (f ýSE.

)v~??t Chain of Custody'# ~4' coysk'- (--

I. Custody Seals olishipping container intact?. -Y Ye. No  :

2. Custody Seals dated and. signed?

Yes- No

3. Chain-of-Custody record present?

Yes A).No [

-4. Coolertmperature . ".

5. Vermiculite/packing materials is: - Wet oDry \J]

6: .' Numerofsan-ipes hppiSngcontai. 3 ()x 'An-

¥..

7. Sample.holding tims exceeded?

Yes [ J No L)

8. Samples havei-

.. __hazard labels S" *custodyseals -.. _-appropriate sample labels .

9. Samples are; - ..

-i-ngood condition-leakin

• ' .........have air bubbl"s

10. Were any anormalies identifJed insamnpereceipt-Yes []No [)

11.. .Descriptionofanomalies(include sample numbers):

Sample CustodianALaboratory.

ae Telephoned to: .

Page 28 of 105

SAMLERECEIPT & REVIEW FORM 0T~ CA1 f, a, 1V1.UZ-7 Vt PMo SDG/ARCOCIWork Order: 16 Z 93 /-

LatcIivd Client:

R 5-J

'___________________________

PM(A) Review (srn.cuforsln~

- "

itemi are resalved priom to sigaing):

Sample Receipt Criteria Commentsl/Qualiriers (Required for Non-Conforming Items) seals broken damaged container leaking container oaer (describe)

Applicable; Dirck I Shipping containers received intact and sealed?

Samples requiring cold

____

Circlk Codlmt ice bags blue ice dry c ( oierdesri&)

2 preservation within (4 + /- 2 C)?

Record preservation method. ,_ ,. __,_....... ..

Chain of custody documents C.OUs a 6 \/W ,Uk included with shipment? . , ,

Sample containers intact and inic abkcaIb ea darnaged coainer eaki cainer adi1ct (describc) sealed? Wo S c.ooll," *-jqI q.**4%6 a:rx=

Samples requiring chemical sipk W3. conaine affecd and observed pH.-

preservation at proper pH? r VOA vials free of headspace Sm ID' and conwtiners aftected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)

Id's and ts afece:

8 Samples received within holding

,ime?

9 Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles?

Date & time on COC match date Sample Ws affected:

& time on bottles?

received Number of containers match number indicated on COC?

COC form is properly signed in relinquished/received sections?

no .c.a5..v .iL i va d To -* Is . C (C )U .C,4- ()

Air Bill ,Tracking #'s, &

Additional Comments

-* RSORAD Receipt I Suspected Hazard Information ._0 *If > x2 area background is observed on samples identified as -non-Sd regulated/non-radioacive. comact dhe Radiation Safety group for fiurther

___ investigation.

A laadiological Classification? Maximum =Counts Observed*:

IB lCB Regulated? Comments:

fSHipped as IXtI Hazardous C Material? If yes, contact Waste I Hazard Class Shipped:

_Manager or ESH Manager. UNI; PM (or PMA) review of Hazard classification: initials Date: ti D1A Ci age 7> U 105 V

SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM VAm 16,7 94Z.32 16f 9a5-

-1' (0L q 0l 50 "

-r C"0C ) a (.,.)r i hc~d kcIC, o0 .... "_"

5st *..e hiado

__

JLfsf Page 30 of 105

• 1T1in.

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00367 362 Injun Hollow Road, East Hampton, CT 06424 860.267-2556 3-7_________________ ___________________________

0 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones C A .

14 Z Priority

Z 30 D. [] 14 D. E] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0008-001F 5/05/06 11:13 SE C BP X X X Transferred from COC #2006-00324 9106-0008-003F 5/5/06 13:35 SE C BP X X X Transferred from COC # 2006-00325 9106-0008-004F 5/5/06 13:51 SE C BP x x x Transferred from COC # 2006-00325 9106-0008-005F 5/5/06 14:17 SE C BP x x x Transferred from COC # 2006-00325 9106-0008-006F 5/5/06 14:36 SE C BP x x x Transferred from COC # 2006-00325 9106-0008-006FS 5/5/06 14:36 SE C BP x x x Transferred from COC #2006-00325 9106-0008-007F 5/5/06 15:03 SE C BP X Transferred from COC #2006-00325 9106-0008-002F 5/5/06 13:10 SE C BP x X X Transferred from COC #2006-00325 NOTES: PO #: 002332 MSR#: 06-7'"q,3 SSWP# NA Z LTP QA E] Radwaste QA E] Non QA Samples Shipped Via: Internal Container

[ Fed Ex Temp.: _ Deg. C El Hand Custody Sealed?

YO NO

1) elinqu she Date/Time 2) e ived ate/Time Custody Seal Intact?

El Other

3) i*enquished By ,J Date/Time 4) RieeiveZ y ime YO NEI Bill of Lading #

R V 564/ 11(P2_

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Health Physics Procedure GPP-GGGR-R5 104-003-Attachment B-CY-O0 1 Major Chain of Custody Form Connecticut Yankee Atomic Power Company UJ 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Ao__ LP V.

Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only U Contact Name & %one: ~Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road, Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones W Cn Z Priority: Z 30 D. [ 14 D. 7 7 D. Container Sample Size-

"DMedia Type &Tye Comment, Preservation Lab Sample ID Sample Designation Date Time Code Code Code CmetPrsvainabSplI (0 9106-0008-008F 5/08/06 08:01 SE C BP X X X Transferred from COC #2006-00327 0 9106-0008-009F 5/08/06 08:3 2 SE C BP X X X __" _ Transferred from COC #2006-00327 0ol 9106-0008-010F 5/08/06 09:09 SE C BP ol 9106-0008-01OFS 5/08/06 X X X Transferred from COC 09:09 SE C BP X X X Transferred from COC ##2006-00327 2006-00327 011 9106-0008-01OF 5/08/06 09:30 SE C BP x X X Transferred from COC # 2006-00327

)Iý. 9106-0008-012F 5/08/06 09:53 SE C BP X Transferred from COC #2006-00327

ýItt 9106-0008-013F 5/08/06 10:16 SE C BP X X x Transferred from COC # 2006-00327 N5 9106-0008-014F 5/08/06 10:47 SE C BP x x x Transferred from COC # 2006-00327 NOTES: PO #: 002332 MSR #: 06-Jq3 SSWP#NA SLTP QA Dl Radwaste QA E] Non QA Samples Shipped Via: Internal Container 0 Fed Ex Temp.: "ZIDeg. C

[] UPS E] Hand Custody Sealed?

YO0 N)

1) Relinquished By Date/Time 2) Received By Date/Time Custody Seal Intact?

Dl Other

3) Relinquished By Date/Time 4) Received By Date/Time Y50 NO Bill of Lading #

163274. w Connecticut Yankee Statement of Work for Analytical Lab Services -CY-ISC-SOW-O0l Figure 1. Sample Check-in List.

Date/Time Received: .A bmo SDG#:

Work Order Number:

Shipping Cdntainer ID:M. - Chain of Custody#""

1. Custody Seals oii shipping container intact? -Yes [*No II

2. Custody Seals dated and signed? Yes' 7 No [,

3. Chain-of-Custody record present? " Yes [.-]"o I ]

.4. Cooler temperature I

5. Vermiculite/packing materials is: Wet M , J IVAJ.o J Dry container: "  ;

6: Number of samples in shipping

7. Sample holding times exceeded? Yes [ ] No

10. Were any anomalies identified in sample receipt? Yes [] No

11. Description of anomalies (include sample numbers):

Telephoned to:. n y on *.. By. ..

Page 33 of 105

SAMPLE RECEIPT & REVIEW FORM

1. I PM UKe 00 Bade: SD/A1RC1OCMMWorVkOrde:

f~at Reeirii.-C)

,

(A)W~w(am"ur nou*tW~ftMU ~Ite are mol~ved Kprim ft" Recei-ved BY!

Sainple Recept Criteria gI ConuneutslQualilers (Required for Non-Conforming Items) and sealed? /)

,hee C"ho-- ice bar blae ice dry ice otbeeO&M Samples requiring cold 2 preservaation within (4 +/-2 C)/

Record preservation method. _ -__

_ _.......

3Chain of custody documents included with shi _ ?.......

SampLe containersintact and 4-scaled? Q ippli"cahWe sas broke dimapdwiconer leakin cnbwe adwc(descnifc)

_______________

....

Samples requiring chemical / ID's..

ls m'. affecoed and observed pH:

preservation at proper pH? .......

6 VOA vials free of headspace ID', as com.imes aracwd; (defined as < 6mm bubble)? /

Are Encore containers present?

7 (If yes. Imnndiately deliver to VOA laboratory) i 8 Samples received within holding time?

/Id' and fs ftcW:

-- _ __----

9 p D's on COC match ID's / s aM*

m* nies affeceed;

-on bottles? _____________________

Dafte&lime on COC match date ID's affeemd:

& time on bottles?

Number of contafi-rs received :D'saffeeed:

match number indicated on COC?

12 COC form is properly signed in relinquhedlreceived sections?

4Air Bill ,Tracking #'s, &

Additional Comn~ts I

A Suspected Hazard Information n ....

j

. ......

601UUIOOg5C8

'A egulted?

.

%.asasflcation?(fut'

'4

'

I V t-X S0 Ag

.

• O~RAD~ cIpII________________

2 a Rr*a bckgr o iscontact eceipx 9htdflnon-radioctive",

Counts Observed ob"erethe C40 h--1 d o n sM le s k f ie edas O n'.

Radiation Safety grou for furthe 3--ZJ asMT.Hazardous N~lP~ - -

CMaterial?. if ye, contact Waste "/ HlaZwd Class Shipped:

Manager or ESH Manager. LINO:

I I'M (or PMA) review of Hazard classification:

'fltl~aJD -, /J-z4'/&k Date:

Page 34 of 105

0 SAMPLERECEIPT & REVIEW FORM

~PM use onl Client:

Date Received:

Received By:

yan~keu ~SDGIARCOC/Work I

Order: ()74//j jcoPM(A Review (ensure noo-confortning item wre resolved prior to signing): J Sample Receipt Criteria 4 Comments/Qualiflers (Required for Non-Conforming Itenis)

Shipping containers received intact Circle Applicable: seals broken damaged container leaking container other (describe) and sealed? __

Samples requiring cold Circle Coolant 9 ice bags blue ice dry ice other describe) 2 preservation within (4 +/- 2 C)?

Record preservation method. .21/ '

Chain of custody documents included with shipment?

4 Sample containers intact and Circle Apica**e: seals broken damaged con*tiner leaking consa*ner oter-(describe) sealed?

Samples requiring chemical Sample ID's. containers affected and observed pH:

preservation at proper pH?

VOA vials free of headspace Sample ID's and containers affected:

6 (defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)

Id's and sea affected:

8 Samples received within holding ___

lime?

9 Sample ID's on COC match ID's Sample 1.,s and containers affected:

on bottles?

Sample ID's affected:

10 Date & time on COC match date

& time on bottles?

Number of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in [ c-.-- 1 .t.l arnq.1Jkd relinquished/received sections?

_t - -e La c

'j V c -'I 1c 1 4 Air B ill ,T r ac k ing # 's ,

&

Additional Comments Iv V let.'

ifI > x2 area background is observed on samples identified as "non-Suspected Hazard Information Ian' regulated/non-radioactive', contact the Radiation Safety group for further investigation.

IRSO RAD Receipt #

A lRadsological Classification'! !2-4 FV I Maximum Counts Observed*: Vf CA44 B PCB Regu Shipped as DOIi Hazardous C Material? If yes, contact Waste Manager or ESH Manager.

L ,,

PM (or PMA) review of Hazard classification:

Comments:

Hazard Class Shipped:

UN#:

Initials Z Date:

I Page 35 of 105

Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Check-in List Date/Time Received: 57'! taI ( 003z.

SDG#:

Work Order Number:

Shipping Cdntainer ID: -79c Z I 1 173 Chain of Custody'# "L_a(S?3-1 " LaC.,

I. Custody Seals oni shipping container intact?- Yes k 0 []

2. Custody Seals dated and signed? .1Yes , o []

3. Chaia-of-Custody record present? Yes Ilo []

4. Cooler temperature

5. Vermiculite/packing materials is: Wet Dry i']

6. Number of samples in shipping container: Y._A h tk

7. Sample holding times exceeded? Yes-[ ] No

8. Samples have:

tape ____hazard labels custody seals ____appropriate sample labels

9. Samples are:

.i°"in good condition leaking

__._broken have air bubbles

10. Were any anomalies *identified in sample receipt? Yes [ ] No [-<

• 11Pescription of anomalies (include sample numbers): "_IA Sample. Custodian/Laboratory: ('e/,e4-lC2* Date-____/_*__&_/_____

Telephoned to: On By Page 36 of 105

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major I"Lj g%/_1 J h-r HLet dG - R 14 Aa e B Y I a Chain of Custody Form No. 2006-00380 CD Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 o 860-267-2556 2 Project Name: Haddam Neck Decommissioning Analyses Requested ':LabYfUse Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage 8171.Road.

843 556 Attn.Charleston Cheryl JonesSC. 29407

• Z Priority: Z 30 D. D 14 D. E 7 D. Container Sample Size-Media Type &Type, . C La S" Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID

,1 9106-0009-016F 5/15/06 13:28 SE C BP x x Transferred from COC 2006-00352 p 9106-0009-016FS 5/15/06 13:28 SE C BP X X Transferred from COC 2006-00352 9106-0009-017F 5115/06 14:03 SE C BP X X Transferred from COC 2006-00352 9106-0009-01 IF 5/15/06 08:05 SE C BP x Transferred from COC 2006-00351

• p 9106-0009-013F 5/15/06 08:35 SE C BP X X Transferred from COC 2006-00351 "9106-0009-013FS

_5 5/15/06 08:3_5 SE C BP X x Transferred from COC 2006-00351 P 9106-0009-014F 5/15/06 08:59 SE C BP X Transferred from COC 2006-00351 9106-0009-015F 5/15/06 09:36 SE C BP X X TransferredfromCOC 2006-00351 NOTES: PO #: 002332 MSR #: 06-O/S4 SSWP# NA Z LTP QA D] Radwaste QA E] Non QA Samples Shipped Via:

[ Fed Ex Internal Container Temp.: __ Deg. C IZUPS Hand H Custody Sealed?

YD NO

1) Relinquis~ed By Date/Time 2) RecV d y Date/Time Custody Seal Intact?

E] Other

3) Relinquished By Date/Time 4) Releive By Date/Time Y[7 Nfl Bill of Lading#

-rq1_1 I?6/-

Health Physics Procedure

/1~-/1 $

e- I- I I GPP-GGGR-R5104-003-Attachrnent B-CY-001 Major or Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00381 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only C

LU Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D. E] 14 D.E] 7 D. Container Med ia Sample Size-Sample Designation Typ e &Ty peC Date Time CodeC o m n , P e e v t oL Comment, Preservation Laa Sample S mp eID I

1' 9106-0009-001F 5/11/06 13:22 SE C BP x x TransferredfromCOC2006-00347

) 9106-0009-002F 5/11/06 13:46 SE C BP x X o0 9106-0009-003F TransferredfromCOC2006-00347 5/11/06 14:06 SE C BP X X Transferred from COC 2006-00347 9106-0009-004F 5/11/06 14:30 SE C BP X X Transferred from COC 2006-00347

• ( 9106-0009-005F 5/11/06 14:55 SE C Bp X x Transferred from COC 2006-00347 j.. 9106-0009-007F 5/12/06 07:44 SE C BP X X Transferred from COC 2006-00348 0(J 9106-0009-008F 5/12/06 08:16 SE C BP X X Transferred from COC 2006-00348

(* 9106-0009-009F 5/12/06 08:35 SE C BP X X Transferred from COC 2006-00348 01(

9106-0009-01OF 5/12/06 09:07 SE C BP XX Transferred from COC 2006-00348 NOTES: PO #: 002332 MSR #: 06- SSWP# NA EJ Radwaste QA Samples Shipped Via:

Z LTP QA F1 Non QA Internal Container

[ Fed Ex Temp.: _ Deg. C LUPS EHand Custody Sealed?

YE] NO0

1) Relinquished By Date/Time 2) R'ecee y Date/Time Custody Seal Intact?

L] Other

3) Relinquished By Date/Time 4) Received by Date/Time YE N17 Bill of Lading #

4q Il /7/ýr'

I " -P5iX; F4 (2. . ILI)

Connecticut Yankee Statement of Work for Analytical Lab Services -CY-lsC-sOw-o00 Figure 1. Sample Check-in List L01~f Date/Time Received: - - - 0 k, SDG#: _\S RJ.ýk CA, -- 0 IIt Work Order Number:

Shipping Cdhtainer ID:. - Chain of Custody# .- ., a

1. Custody Seals orf shipping container intac t?.. Yes D4 No[]

2. Custody Seals dated and signed? Yes*[ ]No [

3. Chain-of-Custody reord present? Yes M No t I

4. Cooler temperature .AIQor.

5. Vermiculite/packing materials is: Wet [].Dry*

6.' Number of samples in shipping container:

7. Sample holding times exceeded? Yes [)( No [I)

.8. Samnple~s have:

Žitapc .hazad labels

"< custody seals -... appropriate sample labels

9. Samples are:'

• ,-in good condition . leaking

-bmken i.ihave air bubbles

10. Were any anomalies identified in sample receipt? Yes [] No

11. .Description of anomalies. (include sample numbers):

Sample Custodian/Laboratory: . Date: . .- 71ý Telephoned to"  : On By_. _ "

Page 39 of 105

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00349 362 Injun Hollow Road, East Hampton, CT 06424 4 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones co Priority: Z 30 D. El 14 D. E] 7 D. Sample Size-/

Container /O.

Media Type &Type Saample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID a 9106-0010-001F 5/04/06 10:49 SE C BP X X Transfmred from COC 2006-00321 6tO 9106-0010-002F 5/04/06 11:12 SE C BP x x Transferred from COC 2006-00321 Olt 9106-0010-004F 5/04/06 12:48 SE C BP X X Transferred from COC 2006-00321 9106-0010-006F 5/04/06 13:34 SE C BP X X Transferred from COC 2006-00321 9106-0010-007F 5/04/06 13:21 SE C BP X x Transferred from COC 2006-00321

-9106-0010-009F 5/04/06 14:01 SE C BP X X Transferred from COC 2006-00321 9106-0010-OIOF 5/04/06 14:21 SE C BP X X Transferred from COC 2006-00321

-9106-0010-012F 5/04/06 14:44 SE C BP X X Transferred from"COC 2006-00321 9106-0010-013F 5/04/06 15:06 SE C BP X Transferred from COC 2006-00321 NOTES: PO #: 002332 MSR#: 06- 070" SSWP#NA SLTP QA El Radwaste QA E] Non QA Samples Shipped Via:

[ Fed Ex Internal Container Temp.: Z7Deg. C

[]UPS

[] Hand CustodSealed?

Yff" NO 1)RelinquishelBy Date/TF e 2) Received y Date/Time Custody Seal Intact?

F] Other 3)Relinquished By Date/Time 4) Received By I Date/Time YVN 0 Bill of LadingII

.ý q04 -3 1;

Connecticut Yankee CY-ISC-SOW-O01 Statement of Work for Analytical Lab Services Figure 1. Sample Check-in List Date/T'ime Received: 9L/7 S / .06 SDG#,: O 1. 0~7j2 -7 Work Order Number:

Shipping Cdftainer ID: -O7 3110 55 ?l Chain of Custody#' 6- 3,/7 I. Custody Seals oni shipping container intact?.. -Yes. [" No [1

2. Custody Seals dated and signed? Yes [j] No []

3. Chain-of-Custody record present? " Yes No[]

.4. Cooler temperature (7* C

5. Vermiculite/packing materials is: Wet ] Dry ]

6.* Number of samples in shipping container: . _:_ _ _

7. Sample holding times exceeded? Yes I No PJ

8. Samples have:

-_hazard labels

_tape

_.._ custody seals - .appropriate sample labels

9. Samples are:

_._n good condition _Vleaking

-broken . have air bubbles

10. Were any anomalies identified in sample receipt? Yes [] No IXQ 11....Description of anomalies (include sample numbers): .__,

.Smple.Custodian/Laboratory: .. Date.: . * --- "

Telephoned to: On By.

Page 41 of 105 I,111l

-11111

SAMPLE RECEIPT & REVIEW FORM 00 Jro0R 0-" P'M ueonly Client: rlt y £6g SD/ROCW Ordr Date Received: 5'- -ob PM(A) Review ( I items are resolved prior to signing):

Received By: *Lk-. .

Sample Receipt Criteria Z Z Com ents/Qualifiers (Required for Non-Conforming Items)

Circle Applicable: seals broken damaged container leaking container other (describe)

Shipping containers received intact and sealed? I Samples requiring cold Circle Coolant # ice bags blue ice dry ice jjtZne other describe) 2 preservation within (4 +/- 2 C)?

Record preservation method. ..

Chain of custody documents included with shipment?

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking container other (describe) sealed?

5 Samples requiring chemical Sample ID's. containers affecled and observed pH:

Preservation at proper pH?

6 VOA vials free of headspace Sample ID's and containers affected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) 8 Samples received within holding Id's and tests affected:

time?

Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles?

10 Date & time on COC match date Sample ID's affected:

& time on bottles?

Sample ID's affected:

Number of containers received match number indicated on COC? O COC form is properly signed in 2 relinquished/received sections?

4 Air Bill ,Tracking #'s, & h/'I Additional Comments 7 YI/ 3 ('*/

" ' - RSO RAD Receipt #

S*If > x2 area background is observed on samples identified as "non-Suspected Hazard Information r Z a , regulatedlon-radioactive". contact the Radiation Safety group for further A investigation.

A BRadiological Classification? Maximum Counts Observed*:

BB IMp Regulated? HaCardonts:

rShipped as DOI' Hazardous C fMaterial? If yes, contact Waste Hazard Class Shipped:

lManager or ESH Manager.  !.UN#:

PM (or PMA) review of Hazard classification: Initials Date: /7,,4 Page 42 of 105

List of current GEL Certifications as of 15 August 2006 State Certification Alaska UST-062

• _

_ -AZO_6_68_._- .7 [ -7 Arizona

[. ~ ~Arkansas '-_."

88-0651 CLIA 42D0904046

!California --.-

.. . .. .Colo~rado .. . [ _.. .['.

... 01I51CA GenE-ngLabs .....

....- .,

Connecticut PH-0_169------ -

Dept. of Navy - NFRSC 413 EPAj Florida/NELAP E87 156 __

Georgia E87156 (FL/NELAP)

Idaho NIA Illinois 200029 C-SC-01I Indiana Kansas E-10332 Kentucky 90129 Maryland 270 Massachusetts M-SCO12 Michigan 9903 Nevada SC12

- -New Jersey New York 11501 North Carolina 233 North Carolina Drinking W _45_7097 North Dakota R-15 Oklahoma 994 Pen ns yl vania 68-485 -

South Carolina 10120001/10585001/10120002 Tennessee 02934 Texas 213 U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah 8037697376 GEL Vermont N/A Virginia 00151

--- Washington C223 Page 43 of 105

RADIOLOGICAL ANALYSIS Page 44 of 105

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 168404 Method/Analysis Information Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555696 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-00 1F 168404015 9106-0010-012F 1201153129 Method Blank (MB) 1201153130 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153131 168340011(9304-01-005C) Matrix Spike (MS) 1201153132 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Page 45 of 105

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 168404003 (9106-0003-004F) was recounted due to high MDA.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 46 of 105

Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 557837 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Sample ID Client ID 168404009 9106-0006-005F 168404010 9106-0008-006F 1201158316 Method Blank (MB) 1201158317 168404009(9106-0006-005F) Sample Duplicate (DUP) 1201158318 168404009(9106-0006-005F) Matrix Spike (MS) 1201158319 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404009 (9106-0006-005F).

QC Information Page 47 of 105

All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: AIphaspec Pu, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu-I -RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555697 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 48 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OO1F 168404015 9106-0010-012F 1201153133 Method Blank (MB) 1201153134 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153135 168340011(9304-01-005C) Matrix Spike (MS) 1201153136 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (OC Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Page 49 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- I1-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 1 555698 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 50 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OOIF 168404015 9106-0010-012F 1201153137 Method Blank (MB) 1201153138 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153139 168340011 (9304-01-005C) Matrix Spike (MS) 1201153140 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QCQ Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Page 51 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 556350 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 52 of 105

Sample ID Client ID 168404003 9106-0003-004F 168404004 9106-0003-015F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201154644 Method Blank (MB) 1201154645 168404003(9106-0003-004F) Sample Duplicate (DUP) 1201154646 168404003(9106-0003-004F) Matrix Spike (MS) 1201154647 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 10.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404003 (9106-0003-004F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Page 53 of 105

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Samples 1201154644 (MB), 1201154645 (9106-0003-004F), 1201154646 (9106-0003-004F),

1201154647 (LCS), 168404003 (9106-0003-004F), 168404004 (9106-0003-015F), 168404012 (9106-0009-002F), 168404013 (9106-0009-017F), 168404014 (9106-0010-001F) and 168404015 (9106-0010-012F) were dried and reweighed due to low matrix spike/laboratory control sample recovery.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Tc99, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 554580 Page 54 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-00 1F 168404015 9106-0010-012F 1201150561 Method Blank (MB) 1201150562 168340012(9304-02-003C) Sample Duplicate (DUP) 1201150563 168340012(9304-02-003C) Matrix Spike (MS) 1201150564 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 13.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (OC Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Page 55 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555722 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 56 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201153222 Method Blank (MB) 1201153223 168340012(9304-02-003C) Sample Duplicate (DUP) 1201153224 168340012(9304-02-003C) Matrix Spike (MS) 1201153225 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Page 57 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555723 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 58 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404009 9106-0006-005F 1201153226 Method Blank (MB) 1201153227 168340012(9304-02-003C) Sample Duplicate (DUP) 1201153228 168340012(9304-02-003C) Matrix Spike (MS) 1201153229 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Page 59 of 105

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: LSC, Tritium Dist, Solid-HTD2,ALL FSS Analytical Method: EPA 906.0 Modified Analytical Batch Number: 554582 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01 OF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201150569 Method Blank (MB) 1201150570 168340011(9304-01-005C) Sample Duplicate (DUP) 1201150571 168340011(9304-01-005C) Matrix Spike (MS) 1201150572 Laboratory Control Sample (LCS)

Page 60 of 105

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 12.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 168404010 (9106-0008-006F) was recounted due to high MDA.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Page 61 of 105

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint C14, Solid AII,FSS Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 554583 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201150573 Method Blank (MB) 1201150574 168404003(9106-0003-004F) Sample Duplicate (DUP) 1201150575 168404003(9106-0003-004F) Matrix Spike (MS) 1201150576 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Page 62 of 105

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QCQ Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404003 (9106-0003-004F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

Page 63 of 105

The following data validator verified the information presented in this case narrative:

Reviewer/Date: *1/I§]zd  :

Page 64 of 105

SAMPLE DATA

SUMMARY

Page 65 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOO Connecticut Yankee Atomic Power Co.

Client SDG: 168404 GEL Work Order: 168404 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by Page 66 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-007F Project: YANK01204 Sample ID: 168404001 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 18-MAY-06 Receive Date: 02-JUN-06 Collector: Client Moisture: 20.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.(0762 +/-0.102 0.00 +/-0.102 0.0956 pCi/g BXL1 08/11/06 1336 555696 1 Curium-242 U 0.00 +/-0.0995 0.00 +/-0.0995 0.138 pCi/g Curium-243/244 U -0.0( 0853 +/-0.0717 0.0405 +/-0.0717 0.177 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0 .199 +/-0.228 0.181 +/-0.229 0.444 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0.10341 +/-0.129 0.120 +/-0.129 0.323 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 10.0 +/-6.64 5.08 +/-6.72 10.7 pCi/g BXL1 08/16/06 1220 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 4.17 +/-6.67 5.28 +/-6.67 11.4 pCi/g DFAI 08/09/06 1128 554582 4 Liquid Scint C14, SolidAllFSS Carbon- 14 U 0.t 0813 +/-0.0797 0.0634 +/-0.0797 0.132 pCi/g ATH2 08/09/06 0324 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 9.90 +/-48.1 32.0 +/-48.1 65.9 pCi/g MXPI 08/12/06 1633 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.02 +/-6.39 5.18 +/-6.40 10.6 pCi/g MXPI 08/11/06 0738 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0 .139 +/-0.213 0.173 +/-0.213 0.360 pCi/g EGD1 08/11/06 2027 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-1I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified Page 67 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-007F Proiect: YANKO 1204 Sample ID: 168404001 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA EERF C-01 Modified 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid/ ALL 80 (15%-/125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 100 (15/o-I125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL LF5 98 (25%-i125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 75 (15%-/125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25%-I125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 74 (15%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 68 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-011F Project: YANKO 1204 Sample ID: 168404002 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 19-MAY-06 Receive Date: 02-JUN-06 Collector: Client Moisture: 17.4%

Parameter Qualifier Ri esult Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U ( ).120 +1-0.154 0.0683 +/-0.155 0.251 pCi/g BXLI 08/11/06 1336 555696 1 Curium-242 U -0. 0146 +/-0.122 0.0692 +/-0.123 0.303 pCi/g Curium-243/244 U -0. 0103 +/-0.0861 0.0487 +/-0.0862 0.213 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0. 0121 +/-0.125 0.127 +/-0.125 0.344 pCi/g BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U 0. 0254 +/-0.0675 0.0381 +/-0.0675 0.167 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 6.72 +/-7.02 5.56 +/-7.05 11.7 pCi/g BXLI 08/16/06 1237 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U -0 1.521 +/-7.03 5.94 +/-7.03 12.8 pCi/g DFAI 08/09/06 1143 554582 4 Liquid Scint C14, SolidAll,FSS Carbon-14 U C1.023 +/-0.0828 0.0685 +/-0.0828 0.143 pCi/g ATH2 08/09/06 0426 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 3.93 +/-47.7 31.9 +/-47.7 65.7 pCi/g MXP1 08/12/06 1649 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.52 +/-5.81 4.68 +/-5.81 9.60 pCi/g MXP1 08/11/06 0825 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0I.173 +/-0.203 0.164 +/-0.203 0.341 pCi/g EGD 1 08/11/06 2043 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-1I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 69 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-01 IF Project: YANK01204 Sample ID: 168404002 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 76 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 100 ( 15%- 125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 88 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15%- 125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 79 (15%/-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 70 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Project: YANKO 1204 Sample ID: 168404003 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 25-APR-06 Receive Date: 05-MAY-06 Collector: Client Moisture: 23.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.027 +/-0.117 0.153 +/-0.117 0.488 pCi/g BXL1 08/13/06 0819 555696 1 Curium-242 U 0.112 +/-0.315 0.245 +/-0.315 0.781 pCi/g Curium-243/244 U 0.0217 +/-0.206 0.205 +/-0.206 0.594 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.061 +/-0.189 0.176 +/-0.189 0.449 pCi/g BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0551 +/-0.103 0.0584 +/-0.103 0.215 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 8.31 +/-5.73 4.40 +/-5.78 9.25 pCi/g BXLI 08/16/06 1253 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00343 +/-0.0203 0.0172 +/-0.0203 0.036 pCi/g BXFI 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.603 +/-8.25 6.87 +/-8.25 14.8 pCi/g DFA I 08/09/06 1159 554582 5 Liquid Scint C14, SolidAlLFSS Carbon-14 U 0.0937 +/-0.0813 0.0642 +/-0.0813 0.134 pCi/g ATH2 08/09/06 0529 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 7.68 +/-51.2 34.2 +/-51.2 70.4 pCi/g MXP1 08/12/06 1706 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 5.74 +/-7.12 6.58 +/-7.13 13.6 pCi/g MXP I 08/11/06 0912 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.0643 +/-0.198 0.169 +/-0.198 0.351 pCi/g EGD 1 08/11/06 2059 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified Page 71 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Project: YANK0 1204 Sample ID: 168404003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-I, Modified 9 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 42 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 92 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 113 (25%-i125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 59 (25%-6125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 71 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 83 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 76 (15%-,125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded Page 72 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Ci-rtifirntP of Annlvqir Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Proiect: YANKO 1204 Sample ID: 168404003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd The above sample is reported on a dry weight basis.

Page 73 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Proiect: YANKO 1204 Sample ID: 168404004 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 25-APR-06 Receive Date: 05-MAY-06 Collector: Client Moisture: 22.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0456 +/-0.155 0.139 +1-0.155 0.387 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.113 +/-0.181 0.0733 +/-0.182 0.321 pCi/g Curium-243/244 U 0.180 +/-0.239 0.181 +/-0.240 0.472 pCi/g Alphaspec Pu, Solid-ALL FSS 0.118 Plutonium-238 U 0.0196 +/-0.121 +/-0.121 0.324 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0326 +/-0.0639 0.00 +/-0.064 0.0884 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 6.63 +/-6.19 4.86 +/-6.22 10.2 pCi/g BXLI 08/16/06 1309 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.00477 +/-0.0216 0.0179 +/-0.0216 0.0375 pCi/g BXFI 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 1.03 +/-7.06 5.85 +/-7.06 12.6 pCi/g DFA I 08/09/06 1215 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 0.156 +/-0.0912 0.0699 +/-0.0913 0.146 pCi/g ATI-12 08/09/06 0632 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -9.99 +/-42.7 28.7 +/-42.7 59.2 pCi/g MXPI 08/12/06 1722 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 0.939 +/-10.1 10.3 +/-10.1 21.6 pCi/g MXPI 08/11/06 1001 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.237 +/-0.213 0.170 +/-0.213 0.353 pCi/g EGD1 08/11/06 2115 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I 1-RC Modified Page 74 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Project: YANK01204 Sample ID: 168404004 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-1, Modified 9 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 78 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 94 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 101 (25%-/125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 58 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 75 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 62 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%/,125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded Page 75 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Project: YANKO 1204 Sample ID: 168404004 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd The above sample is reported on a dry weight basis.

Page 76 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005F Project: YANKO 1204 Sample ID: 168404005 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 15.4%

Parameter Qualifier R esult Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U - +/-0.123 0.157 +/-0.123 0.437 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0 +/-0.033 0.080 +/-0.0331 0.350 pCi/g Curium-243/244 U -0 +/-0.227 0.247 +/-0.227 0.619 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0 +/-0.163 0.181 +/-0.163 0.444 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U -0 +/-0.0791 0.128 +/-0.0795 0.337 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 9.52 +/-6.00 4.57 +/-6.07 9.61 pCi/g BXLI 08/16/06 1326 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid HTD2,ALL FSS Tritium U 0.854 +/-5.88 4.87 +/-5.88 10.5 pCi/g DFA1 08/09/06 1231 554582 4 Liquid Scint C14, SolidAllFSS Carbon- 14 0.347 +/-0.097 0.0674 +/-0.0972 0.141 pCi/g ATH2 08/09/06 0734 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -1.57 +/-46.0 30.7 +/-46.0 63.2 pCi/g MXPI 08/12/06 1738 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 6.39 +/-7.62 7.40 +/-7.62 15.5 pCi/g MXPI 08/11/06 1017 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.0198 +/-0.187 0.156 +/-0.187 0.324 pCi/g EGD1 08/11/06 2131 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu- I 1-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 77 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005F Proiect: YANKO1204 Sample ID: 168404005 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 65 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 95 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu24 1, Solid-ALL FS 105 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 78 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 80 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 80 (15%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 78 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-015F Proiect: YANKO 1204 Sample ID: 168404006 Client ID: YANKOOl Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 26.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0. +/-0.203 0.178 +/-0.203 0.469 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0. +/-0.0301 0.0729 +/-0.0302 0.319 pCi/g Curium-243/244 U -0. +/-0.251 0.300 +/-0.251 0.713 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0. +/-0.213 0.210 +/-0.213 0.521 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U -( +/-0.108 0.191 +/-0.109 0.483 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 6.64 +/-6.53 5.16 +/-6.57 10.8 pCi/g BXLI 08/16/06 1342 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U -2.9 +/-7.59 6.60 +/-7.59 14.2 pCi/g DFAI 08/09/06 1247 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 U 0. 0352 +/-0.0868 0.0713 +/-0.0868 0.149 pCi/g ATH2 08/09/06 0837 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 1.88 +/-46.8 31.3 +/-46.8 64.4 pCi/g MXPI 08/12/06 1754 555722 6 Liquid Scint Ni63, Solid ALL FSS Nickel-63 U 3.88 +/-7.46 7.40 +/-7.46 15.5 pCi/g MXPI 08/11/06 1033 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0. 0894 +/-0.198 0.163 +/-0.198 0.338 pCi/g EGD1 08/11/06 2147 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534. 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I l-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 79 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-015F Project: YANK01204 Sample ID: 168404006 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 72 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 72 (15%-9125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL F5 94 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 73 (159-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 80 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 78 (15%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 80 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-01 OF Proiect: YANKO 1204 Sample ID: 168404007 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 56.2%

Parameter Qualifier R4esult Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -( 1.128 +/-0.0939 0.142 +/-0.0942 0.385 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0. 0115 +/-0.128 0.147 +/-0.128 0.450 pCi/g Curium-243/244 U -0. 0333 +/-0.122 0.149 +/-0.122 0.401 pCi/g AIphaspec Pu, Solid-ALL FSS Plutonium-238 U 0. 0548 +/-0.169 0.158 +/-0.170 0.403 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0. 0195 +/-0.121 0.117 +/-0.121 0.322 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 10.4 +/-6.89 5.27 +/-6.97 11.1 pCi/g BXLI 08/16/06 1358 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.00 +/-6.86 5.76 +/-6.86 12.4 pCi/g DFA1 08/09/06 1303 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.'0636 +/-0.0801 0.0644 +/-0.0801 0.135 pCi/g ATH2 08/09/06 1017 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 36.1 +/-44.1 28.7 +/-44.1 59.0 pCi/g MXP1 08/12/06 1811 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.26 +/-10.2 10.0 +/-10.2 20.9 pCi/g MXPI 08/11/06 1049 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U - 0.05 +/-0.199 0.169 +/-0.199 0.351 pCi/g EGD1 08/11/06 2203 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA ERRF C-01 Modified Page 81 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-0IOF Project: YANK01204 Sample ID: 168404007 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-l, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 85 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15°/-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 92 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 81 (15%--125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 64 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 77 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 82 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis . ..... 1----s Certificateo T Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-014F Proiect: YANK01204 Sample ID: 168404008 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 32.3%

Parameter Qualifier R esult Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0 +/-0.219 0.231 +/-0.219 0.608 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U - +/-0.0554 0.134 +/-0.0557 0.494 pCi/g Curium-243/244 U 0. +/-0.261 0.249 +/-0.261 0.646 .pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0. +/-0.106 0.160 +/-0.106 0.434 pCi/g BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U -0. +/-0.098 0.127 +/-0.0981 0.369 pCi/g Liquid Scint Pu2 41, Solid-ALL FSS Plutonium-241 U 4.68 +/-8.01 6.48 +/-8.02 13.6 pCi/g BXLI 08/16/06 1415 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 6.02 +/-6.38 4.90 +/-6.38 10.6 pCi/g DFA1 08/09/06 1319 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 U 0. 0892 +/-0.0827 0.0655 +/-0.0827 0.137 pCi/g ATH2 08/09/06 1424 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 19.8 +/-46.3 30.6 +/-46.3 62.9 pCi/g MXPI 08/12/06 1827 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 5.41 +/-7.91 7.77 +/-7.91 16.2 pCi/g MXPI 08/11/06 1106 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -C1.134 +/-0.192 0.167 +/-0.192 0.346 pCi/g EGD1 08/11/06 2218 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 83 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-014F Proiect: YANK01204 Sample ID: 168404008 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALl 50 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 61 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 74 (25%- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 76 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-1125°01)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

• QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 84 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com

¢*f A nhri SLIRI~.i*LL, ~JR 1~IIUI V~

Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005F Project: YANKO 1204 Sample ID: 168404009 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 28-APR-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 16.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis AIphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.0851 +/-0.136 0.106 +/-0.136 0.390 pCi/g BXL1 08/16/06 0949 557837 1 Curium-242 U -0.0253 +/-0.0495 0.120 +/-0.0496 0.525 pCi/g Curium-243/244 U -0.0479 +/-0.0542 0.131 +1-0.0545 0.443 pCi/g Alphaspec Pu, Solid-ALL FSS 0.303 pCi/g Plutonium-238 U 0.0183 +/-0.113 0.110 +/-0.113 BXLI 08/11/06 1633 555697 3 Plutonium-239/240 U 0.00122 +/-0.0662 0.0694 +/-0.0662 0.221 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 4.43 +/-5.83 4.67 +/-5.85 9.82 pCi/g BXLI 08/16/06 1431 555698 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U - 2.02 +/-6.67 5.76 +/-6.67 12.4 pCi/g DFAI 08/09/06 1335 554582 5 Liquid Scint C14, Solid AIlFSS Carbon-14 ( 1.142 +/-0.0798 0.061 +/-0.0799 0.127 pCi/g ATH2 08/09/06 1719 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 12.6 +/-47.6 31.7 +/-47.6 65.3 pCi/g MXPI 08/12/06 1843 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.70 +/-9.56 9.31 +/-9.56 19.5 pCi/g MXPI 08/11/06 1122 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.00659 +/-0.185 0.156 +/-0.185 0.323 pCi/g EGDI 08/11/06 2234 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu- 11-RC Modified 4 DOE EML HASL-300, Pu-I I-RC Modified 5 EPA 906.0 Modified Page 85 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005F Project: YANKO 1204 Sample ID: 168404009 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-I, Modified 9 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 76 (15°/.-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 93 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 105 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15%-.125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 64 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 81 (15%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 86 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006F Proiect: YANK01204 Sample ID: 168404010 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 34.8%

Parameter Qualifier R esult Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U +/-0.195 0.0758 +/-0.196 0.332 pCi/g BXLI 08/16/06 0949 557837 1 Curium-242 U +/-0.202 0.00 +/-0.203 0.280 pCi/g Curium-243/244 U -0 +/-0.0316 0.0766 +/-0.0317 0.335 pCi/g Alphaspec Pu, Solid-ALL FSS 0.275 pCi/g Plutonium-238 U -0 +/-0.0711 0.0967 +/-0.0712 BXLI 08/11/06 1633 555697 3 Plutonium-239/240 U 0.C +/-0.113 0.118 +/-0.113 0.317 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 14.9 +/-6.37 4.64 +/-6.51 9.75 pCi/g BXL1 08/16/06 1447 555698 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.00 +/-6.06 5.09 +/-6.06 10.7 pCi/g DFA1 08/10/06 2150 554582 5 Liquid Scint C04, SolidAll,FSS Carbon-14 U 0.107 +/-0.0846 0.0664 +/-0.0846 0.139 pCi/g ATH2 08/09/06 1822 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 15.1 +/-41.4 27.5 +/-41.4 56.6 pCi/g MXPI 08/12/06 1900 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.258 +/-0.225 0.179 +/-0.225 0.373 pCi/g EGD1 08/11/062251 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 DOE EML HASL-300, Pu-I I-RC Modified 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified Page 87 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006F Proiect: YANK01204 Sample ID: 168404010 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 77 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 94 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 103 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15°/-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 71 (15%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UT Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 88 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-008F Project: YANKO 1204 Sample ID: 168404011 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 35.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF. Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U C +/-0.192 0.152 +/-0.193 0.426 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -( +/-0.142 0.132 +/-0.142 0.446 pCi/g Curium-243/244 U -( +/-0.202 0.240 +/-0.203 0.603 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -c +/-0.096 0.125 +/-0.096 0.328 pCi/g BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U -c +/-0.114 0.137 +/-0.114 0.353 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 11.5 +/-6.72 5.08 +/-6.80 10.7 pCi/g BXLI 08/16/06 1504 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FS,'

Tritium U 0.00 +/-5.92 4.97 +/-5.92 10.7 pCi/g DFA1 08/09/06 1407 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 U -C1.0238 +/-0.0745 0.0636 +/-0.0745 0.133 pCi/g ATH2 08/09/06 1924 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -10.7 +/-40.9 27.5 +/-40.9 56.8 pCi/g MXP1 08/12/06 1916 555722 6 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0'.0956 +/-0.211 0.174 +/-0.211 0.361 pCi/g EGDI 08/11/06 2307 554580 7 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified 6 DOE RESL Fe-1, Modified Page 89 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of An'alysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-008F Proiect: YANK01204 Sample ID: 168404011 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 7 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 65 (15°-125°%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 98 (15%/-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 96 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 76 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 74 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 90 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-002F Project: YANKO 1204 Sample ID: 168404012 Client ID: YANKO0I Matrix: SE Vol. Recv.:

Collect Date: 11-MAY-06 Receive Date: 08-JUN-06 Collector: Client Moisture: 33%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.0 +1-0.155 0.166 +/-0.155 0.458 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0. +/-0.145 0.135 +/-0.145 0.455 pCi/g Curium-243/244 U I +/-0.268 0.281 +/-0.268 0.687 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.0 +/-0.0493 0.0279 +/-0.0494 0.122 pCi/g BXL1 08/11/06 1632 555697 2 Plutonium-239/240 U 0. +/-0.0492 0.0278 +/-0.0493 0.122 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-24 I 13.6 +/-6.90 5.13 +/-7.01 10.8 pCi/g BXLI 08/16/06 1520 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0. 0151 +/-0.0146 0.0114 +/-0.0146 0.0242 pCi/g BXFl 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 4.12 +/-8.36 6.70 +/-8.36 14.5 pCi/g DFAI 08/09/06 1422 554582 5 Liquid Scint C14, SolidAllFSS Carbon- 14 U ).046 +/-0.0755 0.0613 +/-0.0755 0.128 pCi/g ATH2 08/09/06 2027 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 12.9 +/-40.6 26.8 +/-40.6 55.2 pCi/g MXPI 08/12/06 1932 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U ).078 +/-0.203 0.168 +/-0.203 0.348 pCi/g EGD1 08/11/06 2323 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-11 -RC Modified 3 DOE EML HASL-300, Pu-11 -RC Modified 4 EPA 905.0 Modified Page 91 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wwwgel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-002F Project: YANK01204 Sample ID: 168404012 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 61 (15/-1125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 98 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 94 (25%-125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 81 (150/-125%%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%o7-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 92 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-017F Project: YANK01204 Sample ID: 168404013 Client ID: YANKOO I Matrix: SE Vol. Recv.:

Collect Date: 15-MAY-06 Receive Date: 08-JUN-06 Collector: Client Moisture: 28.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0755 +/-0.242 0.230 +/-0.243 0.574 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.0957 +/-0.220 0.171 +/-0.220 0.509 pCi/g Curium-243/244 U -0.073 +/-0.214 0.256 +/-0.214 0.627 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.00629 +/-0.0529 0.0299 +/-0.0529 0.131 pCi/g BXLI 08/11/06 1632 555697 2 Plutonium-239/240 U 0.0262 +/-0.0513 0.00 +/-0.0514 0.0709 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 13.3 +/-6.66 4.95 +/-6.77 10.4 .pCi/g BXLI 08/16/06 1536 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.0205 +/-0.0151 0.0116 +/-0.0151 0.0246 pCi/g BXFI 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.583 +/-7.98 6.65 +/-7.98 14.4 pCi/g DFAI 08/09/06 1438 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.0271 +/-0.0759 0.0625 +/-0.0759 0.131 pCi/g ATH2 08/09/06 2129 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -61.9 +/-150 102 +/-150 210 pCi/g MXPI 08/12/06 1949 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.0628 +/-0.200 0.165 +/-0.200 0.343 pCi/g EGDI 08/11/062338 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified Page 93 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-017F Project: YANK01204 Sample ID: 168404013 Client ID: YANKOOl Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 64 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 96 (25%-125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 73 (15/-,125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 79 (15%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

• Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 94 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-OO1F Proiect: YANK01204 Sample ID: 168404014 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 17-MAY-06 Collector: Client Moisture: 27.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, SolidALL FSS Americium-241 U 0.00677 +/-0.227 0.238 +/-0.227 0.628 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.0854 +/-0.167 0.00 +/-0.168 0.231 pCi/g Curium-243/244 U 0.0361 +/-0.242 0.241 +/-0.242 0.634 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.173 +/-0.181 0.143 +/-0.182 0.331 pCi/g BXL1 08/11/06 2250 555697 2 Plutonium-239/240 U -0.0342 +/-0.0865 0.0951 +/-0.0866 0.235 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 13.0 +/-6.44 4.78 +/-6.54 10.0 pCi/g BXLI 08/16/06 1553 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.0128 +/-0.0141 0.0125 +/-0.0141 0.0262 pCi/g BXFI 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.548 +/-7.50 6.25 +/-7.50 13.5 pCi/g DFA1 08/09/06 1454 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.0555 +/-0.0809 0.0655 +/-0.0809 0.137 pCi/g ATH2 08/09/06 2232 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -18.1 +/-47.6 32.3 +/-47.6 66.6 pCi/g MXPI 08/12/06 2005 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.134 +/-0.205 0.167 +/-0.205 0.347 pCi/g EGDI 08/11/06 2354 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300. Am-05-RC Modified DOE EML HASL-300, Pu- 1l-RC Modified 2

DOE EML HASL-300, Pu-I I-RC Modified 3

4 EPA 905.0 Modified Page 95 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-OOIF Proiect: YANK01204 Sample ID: 168404014 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 50 (15°%o- 125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 85 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu24 1,Solid-ALL Fý 99 (25%- 125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 74 (25°/o- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 70 (15%-9125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 96 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-012F Project: YANK01204 Sample ID: 168404015 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 17-MAY-06 Collector: Client Moisture: 28.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.110 +/-0.184 0.140 +/-0.184 0.386 pCi/g BXL1 08/11/06 1434 555696 1 Curium-242 U -0.0547 +/-0.141 0.192 +/-0.141 0.544 pCi/g Curium-243/244 U -0.126 +/-0.184 0.245 +/-0.185 0.597 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.00157 +/-0.126 0.122 +/-0.126 0.291 pCi/g BXL1 08/11/062250 555697 2 Plutonium-239/240 U 0.0867 +/-0.0869 0.0406 +/-0.0872 0.128 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 8.31 +/-6.16 4.77 +/-6.21 10.0 pCi/g BXLI 08/16/06 1609 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00771 +/-0.0144 0.0124 +/-0.0144 0.0263 pCi/g BXF1 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.896 +/-6.17 5.11 +/-6.17 11.0 pCi/g DFAI 08/09/06 1510 554582 5 Liquid Scint C14, Solid All,FSS Carbon-14 U 0.0162 +/-0.0763 0.0633 +/-0.0763 0.132 pCi/g ATH2 08/09/06 2334 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 23.3 +/-49.3 32.5 +/-49.3 67.0 pCi/g MXPI 08/12/06 2021 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.0577 +/-0.206 0.171 +/-0.206 0.354 pCi/g EGDI 08/12/06 0010 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I 1-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified Page 97 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-012F Project: YANK01204 Sample ID: 168404015 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-i, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 81 (15%-/125°%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL F5 99 (25%-/125%)

Carrier/Tracer Recovery' GFPC, Sr90, solid-ALL FSS 68 (25%- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 74 (15%-/125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 98 of 105

QUALITY CONTROL DATA Page 99 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: August 21, 2006 Client : Connecticut Yankee Atomic Power Page 1 of 6 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 168404 NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 555696 QC1201153130 168340011 DUP Americium-241 U -0.000522 U 0.0578 pCi/g 204 (0%- 100%) BXLI 08/11/06 14:34 Uncert: +/-0.0385 +/-0.278 TPU: +/-0.0385 +/-0.279 Curium-242 U 0.00 U -0.0405 pCi/g 200 (0%- 100%)

Uncert: +/-0.0756 +/-0.0562 TPU: +/-0.0756 +/-0.0565 Curium-243/244 U -0.0177 U -0.0517 pCi/g 98 (0%- 100%)

Uncert: +/-0.0764 +/-0.257 TPU: +/-0.0765 +/-0.257 QC1201153132 LCS Americium-24 I 12.8 12.8 pCi/g 100 (75%-125%)

Uncert: +/-1.84 TPU: +/-2.70 Curium-242 U -0.0328 pCi/g Uncert: +/-0.0454 TPU: +/-0.0457 Curium-243/244 15.5 14.3 pCi/g 92 (75%-125%)

Uncert: +/-1.94 TPU: +/-2.92 QC1201153129 MB Americium-241 U 0.0471 pCi/g Uncert: +/-0.157 TPU: +/-0.157 Curium-242 U -0.0469 pCi/g Uncert: +/-0.0459 TPU: +/-0.0464 Curium-243/244 U -0.00385 pCi/g Uncert: +/-0.210 TPU: +/-0.210 QC1201153131 168340011 MS Americium-24 l 13.3 U -0.000522 12.0 pCi/g 91 (75%-125%)

Uncert: +/-0.0385 +/-1.38 TPU: +/-0.0385 +/-2.08 Curium-242 U 0.00 U 0.0427 pCi/g Uncert: +/-0.0756 +/-0.0837 TPU: +/-0.0756 +/-0.0839 Curium-243/244 16.1 U -0.0177 15.9 pCi/g 99 (75%-125%)

Uncert: +/-0.0764 +/-1.58 TPU: +/-0.0765 +/-2.61 Batch 555697 QC1201153134 168340011 DUP Plutonium-238 U -0.0155 U 0.0237 pCi/g 956 (0%- 100%) BXLI 08/11/06 22:51 Page 100 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 2 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 555697 Uncert: +/-0.0215 +/-0.0465 TPU: +/-0.0216 +/-0.0466 Plutonium-239/240 U 0.0414 U -0.0489 pCi/g 2410 (0%- 100%)

Uncert: +/-0.0934 +/-0.124 TPU: +/-0.0935 +/-0.124 QC1201153136 LCS Plutonium-238 U 0.155 pCi/g (75%-125%)

Uncert: +/-0.141 TPU: +/-0.142 Plutonium-239/240 11.8 11.5 pCi/g 98 (75%-125%)

Uncert: +/-0.856 TPU: +/-1.32 QC1201153133 MB Plutonium-238 U 0.0552 pCi/g 08/11/06 22:50 Uncert: +/-0.186 TPU: +/-0.186 Plutonium-239/240 U -0.0978 pCi/g Uncert: +/-0.0892 TPU: +/-0.0899 QC1201153135 168340011 MS Plutonium-238 u -0.0155 U 0.0539 pCi/g (75%-125%) 08/11/06 22:51 Uncert: +/-0.0215 +/-0.112 TPU: +/-0.0216 +/-0.112 Plutonium-239/240 12.3 U 0.0414 10.3 pCi/g 84 (75%-125%)

Uncert: +/-0.0934 +/-0.796 TPU: +/-0.0935 +/-1.19 Batch 555698 QC1201153138 168340011 DUP Plutonium-241 U 7.28 U 10.1 pCi/g 0 (0% - 100%) BXL I 08/16/06 16:41 Uncert: +/-6.30 +/-6.39 TPU: +/-6.35 +/-6.46 QC1201153140 LCS Plutonium-241 137 145 pCi/g 106 (75%-125%) 08/16/06 17:14 Uncert: +/-12.5 TPU: +/-19.9 QC1201153137 MB Plutonium-241 U 8.57 pCi/g 08/16/06 16:25 Uncert: +/-6.93 TPU: +/-6.98 QC1201153139 168340011 MS Plutonium-241 138 U 7.28 142 pCi/g 103 (75%-125%) 08/16/06 16:58 Uncert: +/-6.30 +/-12.4 TPU: +/-6.35 +/-19.7 Batch 557837 QC1201158317 168404009 DUP Americium-241 U -0.0851 U 0.167 pCi/g 616 (0%- 100%) BXLI 08/16/06 09:49 Uncert: +/-0.136 +/-0.220 TPU: +/-0.136 +/-0.221 Curium-242 u -0.0253 U 0.241 pCi/g 247 (0% - 100%)

Page 101 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 3 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 557837 Uncert: +/-0.0495 +/-0.334 TPU: +/-0.0496 +/-0.335 Curium-243/244 U -0.0479 U 0.0761 pCi/g 879 (0% - 100%)

Uncert: +/-0.0542 +/-0.149 TPU: +/-0.0545 +/-0.149 QC1201158319 LCS Americium-241 24.5 25.4 pCi/g 104 (75%-125%)

Uncert: +/-2.47 TPU: +/-4.16 Curium-242 U 0.0477 pCi/g Uncert: +/-0.127 TPU: +/-0.127 Curium-243/244 29.7 27.0 pCi/g 91 (75%-125%)

Uncert: +/-2.54 TPU: +/-4.38 QC1201158316 MB Americium-241 U 0.234 pCi/g Uncert: +/-0.275 TPU: +/-0.277 Curium-242 U 0.00 pCi/g Uncert: +/-0.152 TPU: +/-0.152 Curium-243/244 U -0.0551 pCi/g Uncert: +/-0.0624 TPU: +/-0.0628 QC1201158318 168404009 MS Americium-241 26.4 U -0.0851 29.1 pCi/g 10 (75%-125%)

Uncert: +/-0.136 +/-2.97 TPU: +/-0.136 +/-5.01 Curium-242 U -0.0253 U 0.126 pCi/g Uncert: +/-0.0495 +/-0.247 TPU: +/-0.0496 +/-0.248 Curium-243/244 32.4 U -0.0479 31.7 pCi/g 98 (75%-125%)

Uncert: +/-0.0542 +/-3.12 TPU: +/-0.0545 +/-5.39 Rad Gas Flow Batch 556350 QC1201154645 168404003 DUP Strontium-90 U -0.00343 U -0.00637 pCi/g 0 (0% - 100%) BXFI 08/14/06 08:33 Uncert: +/-0.0203 +/-0.0152 TPU: +/-0.0203 +/-0.0152 QC1201154647 LCS Strontium-90 1.56 1.30 pCi/g 83 (75%-125%)

Uncert: +/-0.0563 TPU: +/-0.0881 QC1201154644 MB Strontium-90 U 0.0176 pCi/g Uncert: +/-0.018 TPU: +/-0.018 Page 102 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 4 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Gas Flow Batch 556350 QC1201154646 168404003 MS Strontium-90 1.58 U -0.00343 1.29 pCi/g 82 (75%-125%)

Uncert: +/-0.0203 +/-0.0535 TPU: +/-0.0203 +/-0.0813 Rad Liquid Scintillation Batch 554580 QC1201150562 168340012 DUP Technetium-99 U 0.0338 U 0.266 pCi/g 0 (0% - 100%) EGDI 08/12/06 00:42 Uncert: +/-0.192 +/-0.226 TPU: +/-0.192 +/-0.226 QC1201150564 LCS Technetium-99 13.1 13.6 pCi/g 103 (75%-125%) 08/12/06 01:14 Uncert: +/-0.496 TPU: +/-0.599 QC1201150561 MB Technetium-99 U 0.0311 pCi/g 08/12/06 00:26 Uncert: +/-0.177 TPU: +/-0.177 QC1201150563 168340012 MS Technetium-99 13.0 U 0.0338 12.0 pCi/g 92 (75%-125%) 08/12/06 00:58 Uncert: +/-0.192 +/-0.523 TPU: +/-0.192 +/-0.602 Batch 554582 QC1201150570 168340011 DUP Tritium U 1.77 U 1.62 pCi/g 0 (0% - 100%) DFA I 08/09/06 15:42 Uncert: +/-8.20 +/-7.47 TPU: +/-8.20 +/-7.47 QC1201150572 LCS Tritium 68.3 76.2 pCi/g 11 (75%-125%) 08/09/06 16:14 Uncert: +/-14.0 TPU: +/-14.1 QC1201150569 MB Tritium U 0.586 pCi/g 08/09/06 15:26 Uncert: +/-8.01 TPU: +/-8.01 QC1201150571 168340011 MS Tritium 61.3 U 1.77 61.8 pCi/g 101 (75%-125%) 08/09/06 15:58 Uncert: +/-8.20 +/-12.2 TPU: +/-8.20 +/-12.3 Batch 554583 QC1201150574 168404003 DUP Carbon- 14 U 0.0937 U 0.0422 pCi/g 0 (0% - 100%) ATH2 08/10/06 01:39 Uncert: +/-0.0813 +/-0.075 TPU: +/-0.0813 +/-0.0751 QC1201150576 LCS Carbon- 14 7.27 7.14 pCi/g 98 (75%-125%) 08/10/06 03:00 Uncert: +/-0.508 TPU: +/-0.520 QC1201150573 MB Page 103 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 5 of 6 Parmname NOM Sample Qual OC Units RPD% REC% Range AnIst Date Time Rad Liquid Scintillation Batch 554583 Carbon- 14 U -0.0315 pCi/g Uncert: +/-0.0776 TPU: +/-0.0776 QCI201150575 168404003 MS Carbon-14 15.1 U 0.0937 13.8 pCi/g 92 (75%-125%) 08/10/06 02:43 Uncert: +/-0.0813 +/-1.00 TPU: +/-0.0813 +/-1.03 Batch 555722 QC1201153223 168340012 DUP Iron-55 U -26.5 U 5.83 pCi/g 0 (0%- 100%) vIXPI 08/12/06 20:54 Uncert: +/-65.1 +/-36.9 TPU: +/-65.1 +/-36.9 QC1201153225 LCS Iron-55 641 660 pCi/g 103 (75%-125%) 08/12/06 21:27 Uncert: +/-56.2 TPU: +/-67.2 QC1201153222 MB Iron-55 U 18.2 pCi/g 08/12/06 20:38 Uncert: +/-39.6 TPU: +/-39.6 QC1201153224 168340012 MS Iron-55 717 U -26.5 688 pCi/g 96 (75%-125%) 08/12/06 21:11 Uncert: +/-65.1 +/-60.2 TPU: +/-65.1 +/-71.6 Batch 555723 QC1201153227 168340012 DUP Nickel-63 U 3.79 U 6.68 pCi/g 0 (0% - 100%) vIXPI 08/I 1/06 11:55 Uncert: +/-5.39 +/-7.43 TPU: +/-5.40 +/-7.43 QC1201153229 LCS Nickel-63 512 479 pCi/g 94 (75%-125%) 08/11/06 12:27 Uncert: +/-22.4 TPU: +/-27.1 QC1201153226 MB Nickel-63 U 15.7 pCi/g 08/11/06 11:38 Uncert: +/-9.92 TPU: +/-9.93 QC1201153228 168340012 MS Nickel-63 530 U 3.79 511 pCi/g 96 (75%-125%) 08/11/06 12:11 Uncert: +/-5.39 +/-23.5 TPU: +/-5.40 +/-28.7 Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported Result is greater than value reported Page 104 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 6 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 105 of 105

Table of Contents General Narrative ................................................................ 1 Chain of Custody And Supporting Documentation .......... 5 Radiological Analysis .......................................................... 14 Sample Data Summary ..................................................... 28 Quality Control Data .......................................................... 32

General Narrative 1

CASE NARRATIVE For CONNECTICUT YANKEE RE: Soil PO# 002332 Work Order: 172071 SDG: MSR #06-0688 September 27, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:

2040 Savage Road Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina on May 12, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures. Sample 9106-0004-013F was relogged for additional analyses at the request of Dale Randall via email on September 19, 2006.

The laboratory received the following sample(s):

Sample ID Client Sample ID 172071001 9106-0004-013F Items of Note:

There are no items of note.

I.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.

Analytical Request:

One soil sample was analyzed for Carbon-14, Tritium, Americium, Plutonium, Plutonium-241, Iron 55, Nickel-63, and Tc-99.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP, INC.

P.O. Box 30712 ° Charleston, SC 29417

• 2040 Savage Road (29407)

Phone (843) 556-8171

• Fax (843) 766-1 17

• www.gel.com

List of current GEL Certifications as ofZ, September 2006 State - Certifiation Alaska UST-062 Arizona AZ066&

Arkansas 89s-0651 42D0904046

• " CCalifornia........ 01 15,1CA Colorado GenEngLabs Connecticut PH-0169 NFiSC 413

. .Dept. of Navy EPA WGt-I E87T56J Florida/NELAP

. Georgia . . E87156 (FLINELAP)

N/A Hawaii Idaho ..... NiA.........

N/A Illinois Indiana C-SC-OI B.-10332 kansas Kentucky -90T29 Louisiana 03046 Maryland 27/0 Massachusetts M-SCOt12 Michigan 9903 SCI2 Nevada New Jersey SCO02

" New Mexico

._. LA-E87I56.

New York 11501 North Carolina 233 North Carolina'Drinking W 45709 North Dakota R-158 Oklahoma 9 90 Pennsylvania South Carolina 10 120001168-00485

-585001/1b12-002 Tennessee 02934 Texas TX7l3-2006A Texas NELAP T1047fl4235-06-TX U.S. Dep. of Agriculture S-52597 -

Army Corps of Engineer NIA Utah . 8037697376 GEL Vermont 'V1T87156 Virginia 00151

-C164t1 - .

Washington 4

Chain of Custody And Supporting Documentation 5

'Health. Physiý edure GPP-GGGR-R5104-003 -Attachment B-CY-00 I Major Cqnn cocul Yankee Atomic Power Company

.ijun Hollow Road, East Hampton, CT 06424 860-267-2556 Name: HaddamiNeck Decommissionin2 I1 Contact Name & Phone:

Jack McCarthy-' 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State) fRelbg samrple 91 06-0004-01 3F per th~e request of General Engineering Laboratories Dale Randall on 9/19/06. See attached email.

2040 Savage Road.. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D.E] 14 D. 0 7 D.

Samples Shipped Via:

(9 Fed Ex 0I uPs LI Hand El Other Bill of Lading #

Health Physics Procedure GPP-GGGR-R5104-003-AffachmeiitB-CY-001 Major HelhPyic rcdreGPGl 510-0-ttcmnI-C-0 ao Chain of Custody Form no. 2006-00336 Company Connecticut Yankee Atomic Power 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested *L.bJ:s'Oai . .

Contact Namne & Phone: - en, Jack McCarthy 860-267-2556 Ext. 3024 . ..

Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407  ; "

843 556 8171. Attn. Cheryl Jones V) .Tr Priority: Z 30 D.l 14 D.[] 7 D. Container Sample Size- " "- .',"-

Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation La, Sample ID 9106-0004-O0IF 05/3/06 09:37 SE C BP x x Transferred from COC 2006-00316 9106-0004-002F 05/3/06 09:56 SE C BP X X Transferred from COC 2006-00316 9106-0004-003F - 05/3/06 10:28 SE C BP x x Transferred from COC 2006-00316 9106-0004-004F ' 05/3/06 10:48 SE C BP X X Transferred from COC 2006-00316 J 9106-0004-004FS - 05/3/06 10:48 SE C BP X X Transferred from COC 2006-00316 9106-0004-005F 05/3/06 11:07 SE C BP X X Transferred from COC 2006-00316 9106-0004-006F 05/3/06 12:46 SE C BP x x Transferred from COC 2006-00317"'

9106-0004-007F 05/4/06 07:55 SE C BP X X Transferred from COC 2006-00320 9106-0004-017F 05/4/06 09:27 SE C BP X X Transferred from COC 2006-00320 ,__ ,,__.,,,....-

NOTES: P0 #: 002332 MSR #: 06- o*gP- SSWP# NA Z LTP QA [E Radwaste QA El Non QA Samples Shipped Via:

21 Fed Ex IT e&n~Cna MI uPs 0I Hand

1) Relinquished By Date/Time 2) Received By *Pate/Time 1 e,"

, -4ý MW El

,Q'L Other Vu~dSa nat

3) Relinquished By Date/Time 4) Received By r Date/Time Bill of Lading #

L J ~ 1'.

Connecticut Yankee Statement of Work for Analytical Lab Services .CY-ISC-SOW-f01 Figure 1. -Sample Check-in List.

Date/Time Received: . ,.. .

SDG#: .

- Work Order Number: G' -:-,."1.

Shipping Cdbtainer ID:j. -- E3 *Chain of Custody# - 33qO(

. " .. Custody Seals o0ishipping container intact?::.

Yes t Noje 2- Custody Seals dated and signed?

Yes [ j No ( "

3. Chain-of-Custody record present?

-

• " Yes No ]

.4. Cooler.temperature

5. Verniculitelpacking materials is:

Wet [WDry (j" 6": Number of samples in shipping container-.

__""

7. Sample holding times exc*eded?

Yes [ J No

.8.. Samples have:.

-... k2tape S " hazard labels

" -.A2custody seals " -. appropriate sample labels

9. Samples are:

-in good condition 2Cileaking

."..broken " ""- have air bubbles

10. :Were anY anomalies identified in sarnplo receipt?* Yes. No[]

i.: Description ofanomalies(includes O

Sampe IICustodian/Laboratory a .

. .--.

Telephonedo: o On

SAMPLE RECEIPT & REVIEW FORM PM use only Client: 4-1 nl V/6 SDG/ARCOC/Work Order: /6 z rgZ t Date Received:_

_ _ " 5-1-al

__ (-An Review (esre 001--confo,*M 'tem r resolved prior to sng):

Received By:_ C Ir-lexf1i Sample Receipt Criteria V Comments/Qualifiers (Required for Non-Conforming Items)

Circle Applicable: seals broken damaged container leaking container other (describe)

!Shipping containers received intact and sealed? ,,la...,p- _

Samples requiring cold Circle Coolant # ice bags blue ice dry ice (2f) other describe) 2 preservation within (4 +1- 2 C)?

Record preservation method. _ . C._..-__

Chain of custody documents ,CO Us o-,v Z V t-included with shipment? O Sample containers intact and irlc Appbeale: seals brjkcn damaged container leaking container sealsed? vq/ c:,oNt c s]

Samples requiring chemical Sample ID's. containers affected and observed pH:

preservation at proper pH? I VOA vials free of headspace Sample IO's and containers affected:

(defined as < 6mrm bubble)? I_ ,

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)

Id's and teast affecited:

8 Samples received within holding time? s Sample ID's on COC ID's Satch 11's and containers affected:

Sample on bottles? _ __._ __,

1Date & time on COC match- date Sample iD's affected:

& time on bottles?

Number of containers received L/ Sample ID's affected:

match number indicated on COC?

COC form is properly signed in V10r* CbG5 c-'V, 0t vLU.irVwtic Ad

,

relinquished/received sections? __,_

di.& Ies- CE(\U t*.ip-Air Bill ,Tracking #'s, & 1 1Additional Comments

.U RSOnRAD Receipt #

Tu Sa o *f > x2 area background is observed on samples identified as *non-Suspected Hazard Information fZ regulatedinon-radioactive". contact the Radiation Safety group for further 6Zi investigation.

A Radiological Classi fication.. Maximum Counts Observed*:

B PCB Regulated? ___ Comments:

Shipped as DOI Hazardous C Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. I N#:

PM (or PMA) review of Hazard classification: Initials CK(* Date: .7- .c V

44j-SAMPLE RECEIPT & REVIEW FORM 7 'tip CONTINUATION FORM 010A .

alc Y-cRot C0G,4:r ol ontra (a1.Q55J (0ý) I (4hi5 Ccoý):ei Yccd a __________

b Lsp c1Z5CL M r~

f, 046

/0:

0 SAMPLE RECEIPT & REVIEW FORM r

PM use only Client: (7< q/4.,-K . SDG/ARCOC[Work Order: I4' ZI .....

Date Received: <V. ,,q

• C, PM(A) Review (ensure non-conforming items are resolved prior to signing):

Sample Receipt Criteria

• Comments/Qualifiers (Required for Non-Conforming Items) other (describe)

Circle Applicable: seals broken damaged container leaking container I Shipping containers received intact and sealed? - I Samples requiring cold Circle Coolant # ice bags blue ice dry ice none other describe) 2 preservation within (4 +/- 2 C)?

Record preservation method. __._ .

3 Chain of custody documents included with shipment? Y C 4 Sample containers intact and Circle Applicable: seals broken damaged container lq<1ther11ascribe) sealed? -. 4. , 90A): ao Ooa,*-6001 a1 'f-

. Samples requiring chemical Sample ID's, containers affected and observed pH:

preservation at proper pH? - -

6 !VOA vials free of headspace Sample ID's and containers affected:

6(defined as < 6mm bubble)?_.

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) -

8 Samples time? received within holding

• I a tssafce:

iSample ID's on COC match ID'S Sample lbs and contains affected:

on bottles? ,

10 Date & time on COC match date Sample ID'3 affected:

& time on bottles? 1 -

U Number of containers received Sample lD's affected:

match number indicated on COG? 1 COC form is properly signed in relinquished/received sections? - o  ! re-/.' -

. - ,. -61 -, -

14 Air Bill ,Tracking #'s, &

Additional Comments "u AD*PReceipt #___________

Suspected Hazard Information *If > x2 area background is observed on samples identified as'non.

Sn regulated/non-radioactive", contact the Radiation Safety group forfurther i' investigation.

A Radiologieal .Clagsification? - Maxim .u.a nta

.. Observedl*: "

x axirm < '

B JP Regul a tLed?

Shi'ppe as D5M.Hazardous c-sa, c jMaterial.? -ifyes, contact Waste Hazard Clas Shipped:

[Manager or .ESH Manager. N#./,.

PM (or PMA) review of Hazard classification: Initials Date: o. 1.

U/

A

Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-o01 Figure 1. Sample Check-in List

-j ,,?

a Datc/Timc Rcceived:  %.*'. L'. 0of 0(8 '

SDG#: /K4c -06 1?

Work Order Number: /(Z -*32- "

Shipping Container ID: -'I * *Y 5 8&7Z Chain of Custody # oeo., 1. 1. - 60 I. Custody Seals on shipping container intact? Yes No (

2. Custody Seals dated and signed? Yes NO

3. Chain-of-Custody record present? Yes No [

4. Cooler temperature A//s

5. Vermiculite/packing materials is: wet 9 Dry [3]

6. Number of samples in shipping container:.

7. Sample holding times exceeded? Yes [] No

8. Samples have:

Y, tape hazard labels

_,rcustody seals appropriate sample labels

9. Samples are:

in good condition _4_,eaking broken have air bubbles

10. Were any anomalies identified in sample receipt? Yes ( No [3

11. Description of anomalies (include sample numbers):

Sample Custodian/Laboratory . -Date: , 'ý/.? "6 f 9 g'o Telephoned to: On By- __

Page 45 of 56 12

One additional Sample that needs to be measured to FSSALL

Subject:

One additional Sample that needs to be measured to FSSALL From: "Dale Randall" <randall@cyapco.com>

Date: Tue, 19 Sep 2006 09:14:28 -0400 To: "Cheryl Jones" <cj@gel.com>

CC: "Clyde Newson" <Newson@CYAPCO.com>, "John McCarthy" <McCarthy@CYAPCO.com>

Cheryl:

We need to add sample 9106-0004-013F to our list of samples at GEL requiring further analyses to the FSSALL protocol. It has already been measured for FSSGAM and Sr-90. Once you have had an opportunity to verify that you have enough sample aliquot and can estimate the turn around time (TAT) please call or e-mail me at your earliest convenience.

Thank You, Dale (860) 267-3133 I oflI 13 9/25/2006 1:29 PM

RADIOLOGICAL ANALYSIS 14

Radiochemistry Case Narrative Connecticut Yankee AtomiePower Co. (YANK)

Work Order 172071 Method/Analysis Information Product: Aiphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 570544 Prep Batch Number: 570368 Dry Soil Prep GL-RAD-A-021 Batch Number: 570366 Sample ID Client ID 172071001 9106-0004-013F 1201187914 Method Blank (MB) 1201187915 172071001 (9106-0004-013F) Sample Duplicate (DUP) 1201187916 172071001 (9106-0004-013F) Matrix Spike (MS) 1201187917 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 I REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geon-tty as the calibration standards.

15

Quality Control (OC Information:

Blank Information The blank volume is representative of the sample volumes in this batch.

Designated QC The following sample was used for QC: 172071001 (9106-0004-013F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Batch was recounted due to a high Matrix Spike recovery.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual. documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analvsis Information 16

Product: Alphaspec Pu, Solid-ALL FSS Analytical Method: DOE IEL HASL-300, Pu- 1I-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 570545 Prep Batch Number: 570368 Dry Soil Prep GL-RAD-A-021 Batch Number: 570366 Sample ID Client ID 172071001 9106-0004-013F 1201187918 Method Blank (MB) 1201187919 172071001(9106-0004-013F) Sample Duplicate (DUP) 1201187920 172071001(9106-0004-013F) Matrix Spike (MS) 1201187921 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 I REV# 14..

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 172071001 (9106-0004-013F).

QC Information All of the QC samples met the required acceptance limits.

17

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- 11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 570546 Prep Batch Number: 570368 Dry Soil Prep GL-RAD-A-021 Batch Number: 570366 18

Sample MI Client ID 172071001 9106-0004-013F 1201187922 Method Blank (MB) 1201187923 172071001(9106-0004-013F) Sample Duplicate (DUP) 1201187924 172071001(9106-0004-01;3F) Matrix Spike (MS) 1201187925 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC Information:

Blank.Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 172071001 (9106-0004-013F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Tine All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this 19

SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Tc99, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 570909 Sample ID Client ID 172071001 9106-0004-013F 1201188720 Method Blank (MB) 1201188721 172071001(9106-0004-013F) Sample Duplicate (DUP) 1201188722 172071001(9106-0004-013F) Matrix Spike (MS) 1201188723 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 13.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (0C1 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

20

Designated QC The following sample was used for QC: 172071001 (9106-0004-013F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for-this sample set.

Qualifier information Manual qualifiers were not required.

MethodlAnalysis Information Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-I, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 573887 Prep Batch Number: 570368 Dry Soil Prep GL-RAD-A-021 Batch Number: 570366 21

Sample ID Client ID 172071001 9106-0004-013F 1201195366 Method Blank (MB) 1201195367 172071001(9106-0004-013F) Sample Duplicate (DUP) 1201195368 172071001(9106-0004-013F) Matrix Spike (MS) 1201195369 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 172071001 (9106-0004-013F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 172071001 (9106-0004-013F) was recounted due to ihe quench number being outside the calibration range. Samples were reprepped due to low/high recovery.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from 22

referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 570908 Prep Batch Number: 570368 Dry Soil Prep GL-RAD-A-021 Batch Number: 570366 Sample ED Client ID 172071001 9106-0004-013F 1201188716 Method Blank (MB) 1201188717 172071001 (9106-0004-013F) Sample Duplicate (DUJP) 1201188718 172071001(9106-0004-013F) Matrix Spike (MS) 1201188719 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

23

Quality Control (OC') Information:-

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 172071001 (9106-0004-013F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Gualifier information Manual qualifiers were not required.

Method/Analysis Information Product: LSC, Tritium Dist, Solid-HTD2,ALL FSS Analytical Method: EPA 906.0 Modified Analytical Batch Number: 570910 24

Sample ID Client ID 172071001 9106-0004-013F 1201188728 Method Blank (MB) 1201188729 172071001(9106-0004-013F) Sample Duplicate (DUP) 1201188730 172071001(9106-0004-013F) Matrix Spike (MS) 1201188731 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 13.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 172071001 (9106-0004-013F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this 25

SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint C14, Solid AII,FSS Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 570914 Sample ID Client ID 172071001 9106-0004-013F 1201188734 Method Blank (MB) 1201188735 172071001(9106-0004-013F) Sample Duplicate (DUP) 1201188736 172071001(9106-0004-013F) Matrix Spike (MS) 1201188737 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 172071001 (9106-0004-013F).

26

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis

.None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

ReviewerfDate: CU-IA. , kI 10 12-10 (

27

SAMPLE DATA

SUMMARY

28

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANK00 I Connecticut Yankee Atomic Power Co.

Client SDG: MSR#06-0688 GEL Work Order: 172071 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by 29

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: October 2,2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013F Proiect: YANK01204 Sample ID: 172071001 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 25.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mti Rad Alpha Spec Analysis Alphaspec Am24J, Cm, Solid ALL FSS Americium-241 U 0.0475 +/--0.105 0.064 +/-0.106 0.207 pCi/g TCI 09/30/06 0836 570544 1 Curium-242 U 0.0419 +/-0.111 0.0495 +1-0.111 0.248 pCi/g Curium-243/244 U -0.104 +/-0.106 0.127 +/-0.106 0.334 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.114 +/-0.111 0.0319 +1-0.112 0.132 pCi/g TCI 09/28/06 0937 570545 3 Plutonium-239/240 U 0.0883 +/-0.0997 0.0318 +/-0.100 0.132 pCilg Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U -4.69 +/-9.90 8.51 +1-9.90 17.8 pCi/g TCI 09/29/06 1603 570546 4 Rad Liquid Scintiliation Analysis LSC, Tritiumn Dist, Solid-HTD2,ALL FSS Tritium U -1.6 +1-6.64 5.69 +"-6.64 12-3 pCi/g DFAI 09/23/060750 570910 5 Liquid Scint C14, Solid All, FSS Carbon-14 0-265 +1-0.0958 0.0684 +"--.0959 0.144 pCi/g AXD2 09/23/06 1841 570914 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 16.4 +/-40.0 27.9 +/-40.0 58.3 pCi/g MXPI 10/02/06 1453 573887 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 0.712 +1-10.1 8.44 +1-10.1 17.3 pCi/g MXP1 09/26/06 1504 570908 l1 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.147 +/-0.259 0.213 +W-0.260 0.441 pCi/g KXR1 09/27/06 1734 570909 11 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 09/21/06 1329 570366 The following Analytical Methods were performed Method Description DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 DOE EML HASL-300, Pu-1I1-RC Modified 30

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: October 2, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013F Project: YANK01204 Sample ID: 172071001 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mt, 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Fe-I, Modified 9 DOE RESL Fe-1, Modified 10 DOE RESL Ni-l, Modified II DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 94 (1596-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 90 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FK 89 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 65 (159o-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 64 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 77 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy-Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

31

QUALITY CONTROL DATA 32

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Reuort Date: October 2, 2006 Client: Connecticut Yankee Atomic Power Page 1 of 5 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 172071 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 570544 QC1201187915 172071001 DUP Americium-241 U 0.0475 U 0.0677 pCi/g 35 (0% - 100%) TCI 09/30/06 08:36 Uncert: +1-0.105 +1-0.129 TPU: +/-0.106 +/-0.129 Curium-242 U 0.0419 U 0.0444 pCi/g 6 (0% - 100%)

Uncert: +/-0.111 W--0.118 TPU: +/-0.111 +/-0.118 Curium-243/244 U -0.104 U 0.104 pCilg 0 (0%-100%)

Uncert: +/-0.106 +/-0.142 TPU: +1-0.106 +1-0.143 QC1201187917 LCS Americium-241 11.0 11.5 pCi/g 105 (75%-125%)

Uncert: +/-1.13 TPU" +/-1.80 Curium-242 U '-0.0143 pCilg Uncert +1-0.0198 TPU: +1-0.0198 Curium-243/244 13.2 13.8 pCi/g 105 (75%-125%)

Uncert: +/-1.24 TPU: +/-2.09 QC1201187914 MB Americium-241 U -0.0325 pCi/g Uncert: +/-0.0788 TPU: +/-0.0789 Curium-242 U 0.0258 pCilg Uncert: 0.0727 TPU: +/-0.0728 Curium-243/244 U 0.0173 pCi/g Uncert: +/-0.127 TPU: +/-0127 QC1201187916 172071001 MS Americium-241 11.0 U 0.0475 12.4 pCi/g 113 (75%-125%)

Uncert +1-0.105 +1-1.26 TPU: +/-0.106 +1-2.02 Curium-242 U 0.0419 U 0.0176 pCi/g Uncert: +/-0.111 +1-0.133 TPU: +/-0.111 +"-0133 Curium-243/244 13.4 U -0.104 13.1 pCil/g 98 (75%-125%)

Uncert: +/-0.106 +/-131 TPU: +1-0.106 W-2-13 Batch 570545 QC1201187919 172071001 DUP Plutonium-238 U 0.114 U 0.0215 pCi/g 137 (0% - 100%) TCI 09128/06 09:37 33

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Chareston SC 29407- (843) 556-8171 - www.gel.com QC Summary Workorder: 172071 Page 2 of 5 Parnname NOM Sample Qual QC Units RPD% REC% Range Anist Date Timee Rad Alpha Spec Batch 570545 Uncert: +/-0.111 +/-0.0796 TPU: +/-0.112 +/-0.0796 Plutonium-239/240 u 0.0883 U 0.0278 pCi/g 104 (0%-100%)

Uncert: +1-0.0997 +/-0.0783 TPU: +/-0.100 +/-0.0784 QC1201187921 LCS Plutoriium-238 U 0.0774 pCi/g (750/o-125%) 09/28/06 09:37 Uncert: +1-0.0812 TPU: +/40817 Plutonium-239/240 10.1 9.41 PCi/g 93 (75%-125%)

Uncert: +1-0.863 TPU: +1-1-36 QC12011 87918 MB Plutonium-238 U -0.0052 PCi/g 09/28/06 09:37 Uncert +1-0.0436 TPU: +/-0.0437 Plutonium-239/240 U 0.0338 Uncert: +1/0.0776 TPU: +/-0.0777 QC1201187920 172071001 MS Plutonhim-238 u 0.114 U 0.0355 PCi/g (75%-125%) 09/28/06 09:37 Uncert: +/-0.111 +/-0.0666 TPU: +/-0.112 +1-0.0667 Plutonium-2391240 10.! U 0.0883 10.8 PCi/g 107 (75%-125%)

Uncert: +/-0.0997 +4.981 TPU: +1-0.100 +I-1.58 Batch 570546 QC1201187923 172071001 DUP Plutonium-241 U -4.69 U -0.734 pCi/g 0 (0% - 100%) TCI 09/29/06 16:35 Uncu-t +/-9.90 +/-9.49 TPU: +/-9.90 +1-9.49 QC 1201187925 LCS Plutonium-241 134 119 p(7i/g 89 (75%-125%) 09/29/06 17:07 Uncert: +/-16.4 TPU: +1-21.0 QC1201187922 MB Plutonium-241 U -136 pCi/g 09/29/06 16:19 Uncert: +/-8.76 TPU: +1-&76 QC1201187924 172071001 MS Plutonium-241 136 U -4.69 121 pCi/g 89 (75%-125%) 09/29/06 16:51 Uncert +1-9.90 W-16.3 TPU: +/-9.90 +1-21.2 Rad Liquid Scintillation Batch 570908 QC1201188717 172071001 DUP Nickel-63 U 0.712 U -3.16 pCi/g 0(0% - 100%) VXPI 09/26/06 16:08 Uncert: +/-10.1 +"-835

+14-35 34

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 172071 Page 3 of 5 Parmname NOM Sample Qual Units RPD% REC% Ranve Artist Thte Time Rad Liquid Scintillation Batch 570908 TPU: 4-/-10.1 QC1201188719 LCS Nickel-63 530 487 pCilg 92 (75%-125%) 09/26/06 17:11 Uncert: +/-17.1 TPU: +1-233 QC1201188716 MB Nickel-63 U -4.05 pCi/g 09/26/06 15:36 Uncert: +/-9.33 TPU: +/-9.33 QC1201188718 172071001 MS Nickel-63 572 U 0.712 526 pCi/g 92 (75%-125%) 09/26106 16:39 Uncert: +/-10.1 +/-18.1 TPU: +/-10.1 +/-25.4 Batch 570909 QC1201188721 172071001 DUP Technetium-99 U 0.147 U 0.117 pCi/g 0 (0% - 100%) KXRI 09/27/06 18:06 Uncert: +/-0.259 +"-0.269 TPU: +1-0.260 +/-0.269 QC1201188723 LCS Technetium-99 13.1 13.4 pCi/g 103 (75%-125%) 09/27/06 18:38 Uncert: +1-0.550 TPU: +/-0.629 QC1201188720 MB Technetium-99 U 0.163 pCi/g 09/27106 17:50 Uncert +/-0.244 TPU: +/-0.244 QC1201188722 172071001 MS Technetium-99 13.1 U 0.147 13.5 103 (75%-125%) 09/27/06 18:22 Uncert: +1-0.259 +/-0.606 TPU: +/-0.260 +1/0.680 Batch 570910 pCi/g.

QC1201188729 172071001 DUP Tritium U -1.6 U 2.28 0 (0%- 100%) DFAI 09/23106 08:22 Uncert: +/-6.64 +/-6.40 TPU: +/-6.64 +1-6.40 pCi/g QC1201188731 LCS Tritium 51.0 42.0 82 (75%-125%) 09/23106 08:55 Uncert: +1-8.08 TPU: +1-8.11 QC1201188728 MB Tritium U 0.215 pCi/g 09/23106 08:06 Uncert: W-5.20 TPU: +1-520 QC1201188730 172071001 MS Tritium 52.1 U -1.6 48.1 pcr/g 92 (75%-125%) 09/23106 08:39 Uncert: W-6.64 +1-8.61 TPU: +/-6.64 +t-8.65 Batch 570914 QC1201188735 172071001 DUP 35

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 - www.gel.com QC Summary Workorder: 172071 Page 4 of 5 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Liquid Scintillation Batch 570914 Carbon-14 0.265 0.260 pCi/g 2 (0% - 100%) kXD2 09/23/06 20:16 Uncert: +/-0.0958 +/-0.0933 TPU: +1-0.0959 +1-0.0933 QC1201188737 LCS Carbon-14 6.77 6.46 pCi/8 95 (75%-125%) 09/23/06 21:21 Uncert: -W-0.443 TPU: +1-0.454 QC1201188734 MB Carbon- 14 U -0.0248 pCilg 09/23/06 19:28 Uncert: +/-0U0842 TPU: +/R0.0842 QC1201188736 172071001 MS Carbon-14 7.13 0.265 6.69 pCi,/g 90 (75%-125%) 09/23/06 21:03 Uncert: +/-0.0958 +1-0.466 TPU: +/-0.0959 +/-0A78 Batch 573887 QC1201195367 172071001 DUP Iron-55 16.4 U 11.8 pCi/g 0 (0% - 100%) MXPI 10/02/06 09:34 Uncert: +1-40.0 +/-41.4 TPU: +1-40.0 +/-41.4 QC1201195369 LCS Iron-55 637 601 pCi/g 94 (75%-125%) 10/02/06 10:07 Uncert: +/-52.5 TPU: +/-66.2 QC1201195366 MB Iron-55 U -19.2 pCi/g 10/02/06 09:17 Uncert: +/-32.4 TPU: +/-32.4 QC1201195368 172071001 MS Iron-55 734 16.4 769 pCi/g 105 (75%-125%) 10/02/06 09:50 Uncert: +/-40.0 W/-64.2 TPU: +/-40.0 +1-83.8 Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more 36

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 172071 Page 5 of 5 Parmname NOM Sample Qua] QC Units RPD% REC% Range Arist Date Time N/A R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

37

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Attachment 2b Split Sample Assessment Forms (2 Pages)

Connecticut Yankee Decommissioning Project Health 24265-000-GPR-GGGR-R5124-000 Attachment A Physics Procedure Split Sample Assessment Form Survey Area Survey 0004 Survey Discharge Canal 90 Unit #: Unit Name:

Sample Plan or WPIR#: 2006-021 SML #: 9106-0004-004FS Sample

Description:

Comparison of split samples collected from sample measurement location #04 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The standard sample was 9106-0004-004F the comparison sample was 9106-0004-004FS.

STANDARD COMPARISON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable (Y/N)

Value Error Range Value Error Ratio Cs-137 1.59E-01 1.53E-02 10 0.6 1.66 2.16E-01 2.10E-02 1.36 Y Co-60 2.63E-01 2.OOE-02 13 0.6 1.66 3.OOE-01 2.50E-02 1.14 Y Sr-90 -7.59E-03 8.65E-03 -1 NONE 3.86E-03 8.15E-03 -0.51 N/A Uomments/Corrective Actions: in consideration ot Sr-vu results, I ale is proviaedi to snow acceptance criteria used guidance for agreement ranges, obtained from USNRC to assess split samples.

Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of acceptability for such Resolution Agreement Range rations cannot be made. Since other radionuclides of concern 4 7 0.50 2.00 were found to be present at an acceptable level of agreement, 8 15 0.60 1.66 therefore, no further action is warranted. 16 50 0.75 1.33 51 200 0.80 1.25

> 200 0.85 1.18 Performed By: Reviewed By: Date:

(ýýa WPIR - Work Plan and Inspection Record SML - Sample Measurement Location designation Page l of I

Connecticut Yankee Decommissioning Project Health 24265-000-GPR-GGGR-R5124-000 Attachment A Physics Procedure Split Sample Assessment Form Survey 9106 Survey 0004 Survey Unit Discharge Canal Area#: IUnit #: Name:

Sample Plan or WPIR#: 2006-0021 SML #: 9106-0004-OIOFS Sample

Description:

Comparison of split samples collected from sample measurement location #10 and analyzec using gamma spectroscopy by an off-site vendor laboratory. The standard sample was 9106-0003-010F, the comparison sample was 9106-0003-01 OFS.

STANDARD COMPARI SON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable (Y/N)

Value Error Range Value Error Ratio Cs-137 2.46E-03 1.18E-02 0 NONE 3.26E-02 1.59E-02 13.25 N/A Co-60 7.39E-03 1.20E-02 1 NONE 2.54E-02 1.48E-02 3.44 N/A Sr-90 -1.75E-03 8.05E-03 0 NONE -9.25E-03 8.95E-03 5.29 N/A K-40 1.20E+01 4.24E-01 28 0.75 1.33 1.32E+01 5.10E-01 1.10 Y Comments/Corrective Actions: In consideration of Cs- 13 7, Co- Table is provided to show acceptance criteria used 60 & Sr-90 results, guidance for agreement ranges, obtained to assess split samples.

from USNRC Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of Resolution Agreement Range acceptability for such rations cannot be made. Since none of the 4 7 0.50 2.00 radionuclides of concern were in a comparable range, K-40 was 8 15 0.60 1.66 used to make the comparison and was found to be present at an 16 50 0.75 1.33 acceptable level of agreement, therefore, no further action is 51 200 0.80 1.25 warranted.

> 200 0.85 1.18 Performed By:

&1! xlord WPIR - Work Plan and Inspection Record 6ý'

SML - Sample Measurement Location designation Page I of I

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Attachment 2c Preliminary Data Forms (1 Page)

Health Physics Procedure GPP-GGGR-R5]2 1-001 Attachment B, Rev. CY-00 I MAJOR Health Physics Procedure GPP-GGGR-R5121-001 Attachment B, Rev. CY-0O1 MAJOR Preliminary Data Review Form - Samples for the Sign Test Survey Unit: 9106- 0004 Survey Unit Name: Discharge Canal Classification: 2 Survey Media: Sediment Type of Survey: Final Status Survey Type of Measurement: Radionuclide Specific Number of Measurements: 15 Operational DCGL: 1 BASIC STATISTICAL QUANTITIES Cs-137 Co-60 Sr-90 Minimum Value: -7.91E-03 0.OOE+00 -7.59E-03 Maximum Value: 5.49E-01 1.8 1E+00 2.62E-02 Mean: 2.07E-01 5.08E-01 5.3 1E-03 Median: 1.59E-01 2.56E-01 3.01 E-03 Standard Deviation: 1.79E-01 6.07E-01 9.82E-03 RADIONUCLIDE CONCENTRATION (pCi/g)

NUMBER Cs-137 Co-60 Sr-90 Identified?

9106-0004-OO1F 4.51E-01 9.53E-01 6.33E-03 Y Y N 9106-0004-002F 1.71E-01 1.41E-01 -9.37E-05 Y Y N 9106-0004-003F 3.55E-01 9.45E-01 1.62E-02 Y Y N 9106-0004-004F 1.59E-01 2.63E-01 -7.59E-03 Y Y N 9106-0004-005F 3.99E-01 1.74E+00 5.86E-03 Y Y N 9106-0004-006F 1.12E-01 2.23E-01 1.01E-02 Y Y N 9106-0004-007F -5.61 E-03 1.16E-03 -6.09E-03 N N N 9106-0004-008F 1.55E-01 2.56E-01 2.62E-02 Y Y Y 9106-0004-009F 2.09E-02 0.OOE+00 2.16E-02 N N Y 9106-0004-01 OF 2.46E-03 7.39E-03 -1.75E-03 N N N 9106-0004-01 IF 2.12E-01 3.66E-01 9.13E-04 Y Y N 9106-0004-012F 1.59E-01 1.37E-01 -1.72E-03 Y Y N 9106-0004-013F 5.49E-01 1.81E+00 3.01 E-03 Y Y N 9106-0004-014F -7.91 E-03 2.85E-02 8.27E-03 N N N 9106-0004-015F 3.77E-01 7.44E-01 -1.53E-03 Y Y N Performed By: ( 7C Date:

Independent Review: e 4 Date:

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Attachment 2d Graphical Representation of Data (6 Pages)

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Quantile Plot For Cesium - 137 Survey Unit: 9106-0004 Survey Unit Name: Discharge Canal Mean: 2.07E-01 pCi/g Cs-1 37 Rank Percentage

-7.91 E-03 1 3 %

-5.61E-03 2 10 %

2.46E-03 3 17 %

2.09E-02 4 23 %

1.12E-01 5 30 %

1.55E-01 6 37 %

1.59E-01 7 43 %

1.59E-01 8 50 %

1.71E-01 9 57 %

2.12E-01 10 63 %

3.55E-01 11 70 %

3.77E-01 12 77 %

3.99E-01 13 83 %

4.51 E-01 14 90 %

5.49E-01 15 97 %

Prepared By: X",/ý Date: lo - 2 S - OZ Reviewed By: Date: -

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Quantile Plot For Cobalt - 60 Survey Unit: 9106-0004 Survey Unit Name: Discharge Canal Mean: 5.08E-01 pCi/g 2.00E+00 1.80E+00 ---- -

1.60E+00 CL. 1.40E+00 r 1.20E+00 1.OOE+O0 ,

0 8.00E-01 u 6.OOE-01 o0 4.00E-01 -

2.00E-01 --

• O.OOE+O0 . - .

0 20 40 60 80 100 Percentage Co-60 Rank Percentage 0.OOE+00 1 3 %

1.16E-03 2 10 %

7.39E-03 3 17 %

2.85E-02 4 23 %

1.37E-01 5 30 %

1.41E-01 6 37%

2.23E-01 7 43 %

2.56E-01 8 50 %

2.63E-01 9 57 %

3.66E-01 10 63 %

7.44E-01 11 70 %

9.45E-01 12 77 %

9.53E-01 13 83 %

1.74E+00 14 90 %

1.81E+00 15 97 %

Prepared By: 14L2

-. Date: / 2 ,-

Reviewed By:. V --!5ý eh- Date: Xerr

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Health Physics Procedure GGGR-R5123-Rev.CY-OO1 Attachment C Quantile Plot For Strontium-90 Survey Unit: 9106-0004 Survey Unit Name: Discharge Canal Mean: 5.31E-03 pCi/g 3.OOE-02 2.50E-02 2.OOE-02 C, 1.50E-02 0.

1.OOE-02 0 5.OOE-03 O.OOE+00 0

-5.OOE-03

-1.OOE-02 Percentage 0 Rank Percentage

-7.59E-03 1 3 %

-6.09E-03 2 10 %

-1.75E-03 3 17 %

-1.72E-03 4 23 %

-1.53E-03 5 30 %

-9.37E-05 6 37 %

9.13E-04 7 43 %

3.01E-03 8 50 %

5.86E-03 9 57 %

6.33E-03 10 63 %

8.27E-03 11 70 %

1.01E-02 12 77  %

1.62E-02 13 83  %

2.16E-02 14 90  %

2.62E-02 15 97  %

Prepared By: Date: /o- ZS-,O*

Reviewed By: Date:

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Cesium - 137 Survey Unit: 9106-0004 Survey Unit Name: Discharge Canal Mean: 0.207 pCi/g 6

5 4-C) 3-2-

U-1-

0- 11 i== -F -I IF -K i i 0.1 0.2 0.3 0.4 0.5 0.6 0.8 1 Upper End Value (pCilg)

Upper End Observation Observation Value Frequency Frequency 0.1 4 27%

0.2 5 33%

0.3 1 7%

0.4 3 20%

0.5 1 7%

0.6 1 7%

0.8 0 0%

1 0 0%

Total 15 100%

Prepared By: Date: /a-2.9-Q1 Reviewed By: Date: 2SK/

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Cobalt - 60 Survey Unit: 9106-0004 Survey Unit Name:

Mean: 0.508 pCi/g 6

5 4

1., 3 2

LL 1

0 0.1 0.3 0.5 0.7 0.9 1.1 1.3 1.5 1.7 1.9 Upper End Value (pCi/g)

Upper End Observation Observation Value Frequency Frequency 0.1 4 27%

0.3 5 33%

0.5 1 7%

0.7 0 0%

0.9 1 7%

1.1 2 13%

1.3 0 0%

1.5 0 0%

1.7 0 0%

1.9 2 13%

Total 15 100%

Prepared By: Date: /0 - 2 Reviewed By: Date: "

I./

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Strontium - 90 Survey Unit: 9106-0004 Survey Unit Name: Discharge Canal Mean: 0.207 pCi/g Observatio Observatio Upper End n n Value Frequency Frequency 0 6 40%

0.005 2 13%

0.01 3 20%

0.015 1 7%

0.02 1 7%

0.025 1 7%

0.3 1 7%

Total 15 100%

Prepared By: 65le6 A, "",/, /,001, Date: 6-Reviewed By: *6By:

Reviewed ~ Date: 1/ 5

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Attachment 2e Sign Test Calculation (1 Page)

Health Physics Procedure GPP-GGGR-R512 1-000 Attachment A, Rev. CY-00 I MAJOR Health Physics Procedure GPP-GGGR-R5121-000 Attachment A, Rev. CY-001 MAJOR Sign Test Calculation Sheet For Multiple Radionuclisdes Survey Unit Number: 0004 Survey Unit Name: Discharge Canal WP&IR#: 2006-021 Classification : 2 ýYPE I (ca error):0.01 TYPE I (P3error):0.05 I Radionuclides: Cs-137 Co-60 Sr-90 Survey Design DCGL (pCi/g): 5.38 2.59 1.05 Weighted Sum (W,)

Results Cs-137 Results Co-60 Results Sr-90 (includes C-14 DCGL-Result Sign component) 4.5 1E-01 9.53E-01 6.33E-03 5.27E-01 4.73E-01 1.71E-01 1.41E-01 -9.37E-05 1.47E-01 8.53E-01 3.55E-01 9.45E-01 1.62E-02 5.07E-0 I 4.93E-01 1.59E-01 - 2.63E-01 -7.59E-03 1.85E-01 8.15E-01 3.99E-0 1 1.74E+00 5.86E-03 8.42E-01 1.58E-01 1.12E-01 2.23E-01 1.0 1E-02 1.77E-01 8.23E-01

-5.61E-03 1.16E-03 -6.09E-03 5.45E-02 9.45E-01 1.55E-01 2.56E-0 I 2.62E-02 2.14E-01 7.86E-0 I 2.09E-02 0.OOE+00 2.16E-02 8.54E-02 9.15E-01 2.46E-03 7.39E-03 -1.75E-03 6.25E-02 9.37E-01 2.12E-01 3.66E-01 9.13E-04 2.42E-0 I 7.58E-01 1.59E-01 1.37E-01 -1.72E-03 1.42E-01 8.58E-01 5.49E-0 1 1.81E+00 3.01 E-03 8.73E-01 1.27E-01

-7.91 E-03 2.85E-02 8.27E-03 5.22E-02 9.48E-01 3.77E-01 7.44E-0 1 -1.53E-03 3.96E-01 6.04E-01 Number of Positive Differences (S+): 15 Critical Value: 11 Survey Unit: Meets Acceptance Criterion Performed By: 4:2 Date: /0 S -0/

Independent Review-:.** Date: I .,,

DISCHARGE CANAL SURVEY UNIT 9106-0004 RELEASE RECORD Attachment 2f COMPASS DQA Surface Soil Report with Retrospective Power Curve (4 Pages)

DQA Surface Soil Report Assessment Summary Site: 9106-0004 w/C-14 Planner(s): Dale Randall Survey Unit Name: 9106-0004 Report Number: 2 Survey Unit Samples: 15 Reference Area Samples: 0 Test Performed: Sign Test Result: Not Performed Judgmental Samples: 0 EMC Result: Not Performed Assessment

Conclusion:

Reject Null Hypothesis (Survey Unit PASSES)

Retrospective Power Curve U

1 0.9 ZZZD_, _

0.8 m'I- _ _ __ I

=

0.7 _ _ *I _ _

0.6 li- , -i 0.5 L. 0.4 __ - -,

C, 0.3

• _ _ " _

_"- -i--

0.2 A-

[- 0.1 0

0.0 0.2 0.4 0.6 0.8 1.0 1.2 Unity Rule Sum-of-Ratios, including background

- - Prospective Power U i-beta .... Actual Power

- LBGR - - Estimated Power DCGL ---- Retrospective Power COMPASS vl.0.0 10/2512006 Page1I