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{{#Wiki_filter:2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277 -- FAX (225) 381-2996 RNATIONAL American Radiation Services, Inc.Laboratory Analysis Report ARS1-08-01563 Prepared for.Nuclear Regulatory Commission (NRC)James Noggle USNRC Region 1 475 Allendale Road King of Prussia, PA,19406 James. Noggle@nrc.gov Phone: 610.337.5063 Fax:~#nager Review4 1) )'h Fr x &A il1\a" .-Management Notes: Arnencan Radiation Services, Inc. assumes no liability for (he use or intarpretation of any anflytifal results provided other than the mots of the analysis itself.Reproduction of this report in less than fut requires the written consent of the client.Contact Person: Questions regarding this analytical report should be addressed to: Project Manager ProjectManagers@amrad.com Phone: 225.381.2991 Fax: 225.381.2996 LELAP Cert#.30658 NELAP Cert# E87558 INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group: ARS1-08-01563 Client Sample ID: MW-66-21-(005)07-29/1148 Sample Collection Date: 07/29/08 11:48.Sample Matrix: Aqueous Request or PO Number: N/A ARS Sample ID: ARS1-08-01563-001 Date Received:
{{#Wiki_filter:2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277               --   FAX (225) 381-2996 RNATIONAL American Radiation Services, Inc.
8/12/2008 Report Date: 09/15/08 10:19Afal5ysis A na lys' f Analysis T ,.MC Dep o. Reslts E 2 ..............  
Laboratory Analysis Report ARS1-08-01563 Preparedfor.
....... ..MN-54 0 -o.784 0.782 2.600* l~C 1.300 Qu~al Analysis I Analysis Units Test Method S pCi/L I ARS-007/EPA 901.1* Analysis I AnislyalO ,Analysis Analysis Date/rime Technician 8/21/08 16:01 )LA Tracer/Chem RecoNer t N/A FE-59 0 952 1.529 5.140 2.570 pCi/L ARS-007/EPA 901.1 8/21/08 16:01 JLA N/A CO-58 -0.573 0.778 2.600 1.300 i pCVL .1 ARS-007/EPA 901.1 8/21/08 16:01 " LA .N/A O-60 0622 .0.650 2.240 1 1.120 1 pCi/L. ARS-007/EPA 901.1 8/21/08 16:01 31A N/A ZN-65 0.000 2.499 1 8.400 4.200 ' PCi/L ARS-007/EPA 901.1 8/21/08 16:01 .LA N/A NB-95 J -0.738 1.953 2.81D 1.405 CA 8 N/A ZR-95 0783 1264 4.240 2.120 ' pCI/L I ARS-007/EPA 901.1 8/21/08 16:01 ILA N/A CS-134 -0.289 1.169 2.960 1.480 pci/L ARS-007/EPA 901.1 8/21/08 16:01 3LA N/A C-137 -0.783 0858 1 2.850 1.425 pCI/L t ARS-007/EPA 901.1 8/21/08 16:01 JLA N/A S BA-140 " i 4.539 I .537 10.400 5.200 pCi/L AR5-O07/EPA 901.1 8/21/08 16:01 2LA N/A... ...........- -.........................
Nuclear Regulatory Commission (NRC)
ARS O-EPA 901.8/21/08 1 ..A......LA-140 -0.601 12 3.310 I 1.655 J pCI/I ARS-007/EPA 901.1 8/21/08 16:01 21LA j N/A SR'90 1.005 0.216 0.588 j 0.277 pCi/L I ARS-032/Eichrom SRW-01 { 8/28/08 17:35 8JS 58,00% i*! 130 666 163239 7,9.400 .p/I .ARS-054/EPA 906.0 : 9/8/(0 8:39 I BS N/S NI-63 3.0899 4.4642 7.4175 3.6493 pCl/L ARS-022 8910/09 2:05 B3S N/S____ __ _ Ij__ _ -_ _ _ _ _ _ i ___/___I NOTES: Shipment#
James Noggle USNRC Region 1 475 Allendale Road King of Prussia, PA,19406 James. Noggle@nrc.gov Phone: 610.337.5063 Fax:
08-152 rý=A c ~ 1 i Rr c5 i , £1 P5roct Manager keCýr -Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full requlres the written consent of the client.LELAP Certificate#
1))'h Fr       x       &A     il1\a"                   .     -
30658 NELAP Certificate I E87558  
~#nager                    Review4                                                                                      Management Revi*
-INTERNATIONAL 2609 North River Road, Port Alien, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group: ARSI-08-01563 Client Sample ID: MW-66-36-(005)07-29/1205 Sample Collection Date: 07/29/08 12:05.Sample Matrix: , Aqueous Request or PO Number: ARS Sample ID: Date Received: Report Date: N/A ARSI-08-01563-002 8/12/2008 09/15/08 10:19 Anlss Anlss .Analysis Anaysi iL Analyi Descripthon Results Error +/- 2 s M l " Ua! Units I Test MethOd -I MN-54 0.282 1 0.685 " 2.340 1.170 pCiL ARS-007/SPA 901.1 1-8 FE-59 1.794 1.079 3.5S0 1.775 pCiL ARS-007/EPA 901.1 8 Analysis Analysls Date/Time Technician
Notes: Arnencan Radiation Services, Inc. assumes no liability for (he use or intarpretation of any anflytifal results provided other than the mots of the analysis itself.
/21/08 16:00 1 LA Tracer/Chern N/A$ILA N/A/21/08 16:00 ILA N/A it___ ____ I t CO-58 0.007 0.686 2.260 1.130 pCi/L ARS-007/EPA 901.1 8/21/08 16:00 ILA N/A CO-60 0.008 0.687 F 2.450 1.225 1 pCI/I ARS-007/EPA 901.1 I 8/21/08 16:00 )LA N/A ZN-6S _ "0.101 1.311 j 4.500 2.250 pCi/Li ARS-007/EPA 901.1 8/21/08 16:00 " LA N/A NB-95 -0.715 0.732 2.440 1.220 pCi/L ARS-007/EPA 901.1 8/21/08 16:00 .A N/A ZR-95 -0.232 6.055 1 4.030 2.015 pCi/L I ARS-007/EPA 901.1 8/21/08 16:00 ILA. N/A CS-134 -0.438 2.482 2.540 1.270 pCi/L ARS-007/EPA 901.1 8/21/08 16:00 --A N/A C13.270 0.681 2.300 1.150 pCV'L j ARS-007/EPA 901.1 8/21/08 16:00 ILA N/A BA-140 -4.173 26.705 10.300 5.150 pCI/L ARS-007/EPA 901.1 8/21/08 16:00 LA I N/A LA- 140 1 r2.118 2.508 I 3.430 1.715 pCi/L ARS-007/EPA 901.1. 8/21./08 16:00 ILA -N/A SR-90 14.269 1.149 0.566 0.267 j pCi/L ARS-032/Eilchrom SRW-01 8/28/08 17:35 BS 6600%H-3 4630.409 499.979 160.739 j 79.153 pCi/ I ARS-054/EPA 906.0 9/8/08 12:47 N/S NI-63 7.4-21 4 .7 7.4096 i 3.6455 -, CI- AR--022 9/10/0-8 6I:4 8)5 N/S., ......................  
Reproduction of this report in less than fut requires the written consent of the client.
.. ........--- ----- .-....me......NOTES: Shipment#
Contact Person: Questions regarding this analytical report should be addressed to:
08-152 -* Prdject Manager n.. .Notes; American RodiaLion Services, Inc, assumes no liability for the use Or Interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report In less than full requires the written consent of the client.LELAP Certificate#
Project   Manager ProjectManagers@amrad.com Phone: 225.381.2991 Fax: 225.381.2996 LELAP Cert#.30658                                                                                                   NELAP Cert# E87558
30658 NELAP Certificate  
 
# E87558 St PAGE 1 of 2 NRC FORM 303 U.S. NUCLEAR REGULATORY COMMISSION LABORATORY USE ONLY (4-2004) CONTROL NUMBER REQUEST FOR ANALYSIS AND CHAIN OF CUSTODY LABORATORY:
2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group:                           ARS1-08-01563                                                                           Request or PO Number:                  N/A Client Sample ID:                   MW-66-21-(005)07-29/1148                                                                       ARS Sample ID:                  ARS1-08-01563-001 Sample Collection Date:                         07/29/08 11:48                                                                                   Date Received:                 8/12/2008
SAMPLE LOCATION (LICENSEE)
                                        . Sample Matrix:                  Aqueous                                                                                            Report Date:               09/15/08 10:19 Afal5ysis
LICENSEE NUMBER DOCKET NO.INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED  
      *"                    A nalys'           f     Analysis   T             ,.MC                         Qu~al      Analysis      I                  Analysis                    Analysis
"# TOTAL TYPE -VOLUME WEIGHT DATE SAMPLES SUBMITTED PRIORITY fl ROU~iNE GROUND WATER 2000 ML -2 Kg I [] URGENT SAMPLE COLLECTION INTERVAL MONTH DAY YEAR TIME START INSPECTOR RESPONSIBLE TELEPHONE NUMBER STOP: Jim Noggle (USNRC) (610) 337-5063 LIST DESIRED LIST DESIRED ANALYSIS TO BE PERFORMED LLD (Optional)
                                                                                                                                                                                    * ,Analysis      I    AnislyalO Analysis    Tracer/Chem
OTHER TYPE OF ANALYSIS (Specify)
* l~C                                                                                  Date/rime          Technician Dep      o.            Reslts              E          2 . ............. .........                               Units                          Test Method                                                        RecoNer t    N/A MN-54                         -o.784                   00.782                 2.600           1.300             S pCi/L             I     ARS-007/EPA 901.1                     8/21/08 16:01           )LA FE-59                           0 952                   1.529                 5.140           2.570                 pCi/L                 ARS-007/EPA 901.1                     8/21/08 16:01           JLA                 N/A CO-58                         -0.573                   0.778                   2.600           1.300         i       pCVL           .1     ARS-007/EPA 901.1                     8/21/08 16:01         " LA         .         N/A O-60                         0622                 . 0.650                   2.240   1     1.120             1   pCi/L.               ARS-007/EPA 901.1                     8/21/08 16:01           31A                   N/A ZN-65                           0.000                 2.499   1             8.400           4.200       '         PCi/L                 ARS-007/EPA 901.1                   8/21/08 16:01           .LA                 N/A NB-95                 J       -0.738                   1.953                 2.81D           1.405                 CA                                                       8                                             N/A ZR-95                           0783                   1264                   4.240           2.120     '           pCI/L     I           ARS-007/EPA 901.1                   8/21/08 16:01           ILA                   N/A
LLD (Optional)
                                -0.289                   1.169                   2.960           1.480               pci/L                 ARS-007/EPA 901.1                   8/21/08 16:01           3LA                   N/A CS-134 C-137                         -0.783                   0858   1               2.850         1.425                 pCI/L           t     ARS-007/EPA 901.1                   8/21/08 16:01           JLA                   N/A BA-140 S                  " i         4.539             I     .537               10.400           5.200                 pCi/L                 AR5-O07/EPA 901.1                   8/21/08 16:01           2LA                   N/A
[Z GROSS ALPHA (GA) F-7 STRONTIUM-90 (Sr90)] GROSS BETA (GB) NICKEL-63 (Ni63)*[]GAMMA SPEC (GS) El-STRITIUM (H3) I-D CARBON-14 (C14) D D-IODINE-25 (1125)RELENQUISHED BY RECEIVED BY DATE TIME REASON FOR CHANGE OF CUSTODY-56COIRI s~ro~"wq:1-$
                    . . .
r- 8-6-2006 /030 Prer /'? jlA, FEE RECOVERABLE NO YSTAC NUMBER REMARKS:'NOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASON ARE NOTED IN REMARKS ABOVE.NRC FORM303 (4-2004)PRINTED ON RECYCLED PAPER a PAGE 2 of 2 NRC FORM 303 U.S. NUCLEAR REGULATORY COMMISSION LABORATORY USE ONLY (4-2004) CONTROL NUMBER SAMPLE RECORD -Continued LABORATORY:
                  ...         .       .......-                                                                               -.........................
SAMPLE SAMPLE NAME COLLECTION REMARKS, PRESERVATIVE NUMBER AND DESCRIPTION DATE/TIME ANALYSIS REQUESTED, ETC.MW-66-21-(005), Ground Water Split Sample of MW-66-21-(005)
ARS O-EPA 901.8/21/08                             1 .       . A......
Sample is unfiltered  
LA-140                         -0.601                   12                     3.310   I       1.655   J           pCI/I                 ARS-007/EPA 901.1                   8/21/08 16:01           21LA         j       N/A SR'90                           1.005 730.*23o*10 *!
& unpreserved.
0.216
Analyze fo c, _ _ Gamma Spec, H3, Sr9O, Ni63 MW-66-36-(005)
                                                      *130 666 0.588 163239 j     0.277 7,9.400          .
Ground Water Split Sample of MW-66-36-(005)
pCi/L p/I .
Sample is unfiltered  
I          ARS-032/Eichrom SRW-01 ARS-054/EPA 906.0
& unpreserved.
{
Analyze to__ Gamma Spec, H3, Sr9O, Ni63 NR ,OMO (420)PITDONRCCE AE NRC FORM303 (4-2004)PRINTED ON RECYCLED PAPER OA1 RCNRDATION SERVICES, INC.2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225)'381-2996  
:
*QC Results Report Sample Delivery Group: ARSI-08-01563 Date Received:
8/28/08 17:35 9/8/(0   8:39     I 8JS BS 58,00%
8/12/2008 Laboratory Control Sample Evaluation Antclysis Analyt. Analysis CSU I C) DC Expacted Report Analysis Analysis Analysis Percent Acc BItch Type I Valeu Units Test rasthod Date/Time Technidan Recovery Accaptanca N/A LCS Ni-63 237.73 55.2 8.6999 204.44 pCi/L ARS-022 9/9/08 13:28 BIS 116 75%-125%Blank Evaluation Aays 1QC1 1Analysis Ip.~ ReotAIay" Antlychs yp Analyt. Casis IEpected Report An(lysis
N/S i
* Analysis AWslyala *_atch Type R__ut_ I _ ( )
NI-63                         3.0899                 4.4642                 7.4175           3.6493                 pCl/L                 ARS-022                                         8910/09 2:05         B3S                 N/S
* ile Units Test Method Data/Tim a j Tedhnician N/A MBL Ni-63 '1.023 4.5347 7.6916 NA U pCi/L ARS-022 9/9/08 21:58 B)S RER Duplicate Evaluation Analysis QC Analysis etst CSU I( (1) Result2 CSU 2 (is) Analysils Analysis Arnlysi Analytis R cRER Batchs Type Description
____                _* __       _     Ij__               _     -       _           _       i _     _         _         _   ___/___
+/- 1 Units Tea Maehod Date/Tin.
I      NOTES: Shipment# 08-152 rý=A               ci          ~ Rri ,1 c5                   £1 P5roct Manager keCýr                           -
Techinician RER Acpanc.R N/A LCSD Ni-63 237.73 55.2 229.996 53.406 pCl/L ARS-022 9/9/08 17:42 BI5 0,07 DER Duplicate Evaluation Analys QC alyi sI (1 ) Result 2 CSU 2 () Qua Analys is Analyysi Analysis DER NAtch IType IDes 27iption 5 229.9Un96t 5e.T6t Method Dat9/Tim9 echn/ia8 74.5. 20 N/A ILCS0 NIM-63 237.73 1 55.2 1229.996 153.466 1 PCI/L ARS-022 9/9/08 17A42 -035 0.20<Projnect mi"nager Rlk" Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.LELAP Certificate#
Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full requlres the written consent of the client.
30658 NELAP Certificate
LELAP Certificate# 30658                       NELAP Certificate I E87558
* E87558 MERICAN RADIATION SERVICES, INC.2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group: ARSI-08-01563 Date Received:
 
8/12/2008 Laboratory Control Sample Evaluation Analysis QC Anetyte Analysis I (1 Expected et Qual Report Analylo Analylis Analysli Percent LCS Batch Type Results I MDc I value Units I TeWt Method Dote/Time Tachnici.n Recovery (%) AccIltlnce ARS1-B08-02293 LCS H3 1136.06 " .61.4 16 158.48416 1270.45 pCi/.L ARS-054/EPA 906.0 9/4/08 128:01 B35 89 75%-125%Blank Evaluation A Anlysis QC ] 1 Analysis CSu i (1s) MDC Expected lReport. Analysis Analysis Analysi&Btch Typ o je Results value Unit. Test Method Date/Tkne Technician ARS1-B08-02293 M8L H3 67.923 94.439817 158.41962 NA U pCVL ARS-054/EPA 906.0 9/5/08 2:16 BIS RER Duplicate Evaluation Anallysis Qc Analysis Reut1 CU1 (1 e) Result 2 AnSU Anlyi Anaysi ,Aayi Unt ER Ac Rtn Botch Type Description Res ult 1 CSU CSU 2(1 s) Qs al Unito Teat Method Date/Tim.
2609 North River Road, Port Alien, Louisiana 70767 1 (800) 401-4277           FAX (225) 381-2996
Technic ien ER Acce tn.R j I_ IF I_ I I_ _ I n_ _ F11 .ARS1-808-02293 LCSD H3 13136.06 161.4 1143.2572 161.9636 pCi/L ARS-054/EPA 906.0 9/4/08 22:09 BJS .0.02 <I DER Duplicate Evaluation Anlyi TQC1Analysias
                            -      INTERNATIONAL ARS Sample Delivery Group:                     ARSI-08-01563                                                                         Request or PO Number:                        N/A Client Sample ID:             MW-66-36-(005)07-29/1205                                                                           ARS Sample ID:                    ARSI-08-01563-002 Sample Collection Date:                 07/29/08 12:05                                                                                       Date Received:                 8/12/2008
[A~n-.i.iT AsOlysi. ] Asyao [Analyst.
                                          . Sample Matrix: ,          Aqueous                                                                                                  Report Date:               09/15/08 10:19 Analysis              Analysls Anlss     Anlss           .Analysis                                                           Anaysi       iL             Analyi                                                                   Tracer/Chern Descripthon             Results           Error +/- 2 s         M       l           "         Ua!           Units       I             Test MethOd         -             Date/Time            Technician I   MN-54                           0.282   1         0.685         "   2.340             1.170                   pCiL               ARS-007/SPA 901.1                   1-8/21/08    16:00      1    LA            $      N/A N/A FE-59                           1.794             1.079             3.5S0             1.775                   pCiL               ARS-007/EPA 901.1                       8 /21/08   16:00         ILA ILA                   N/A   it CO-58         ___ ____        0.007             0.686             2.260             1.130             I    pCi/L               ARS-007/EPA 901.1                       8/21/08 16:00       t    ILA                   N/A CO-60                           0.008             0.687   F       2.450             1.225             1     pCI/I               ARS-007/EPA 901.1                     I 8/21/08 16:00             )LA                   N/A ZN-6S   _                   "0.101               1.311   j       4.500             2.250                   pCi/Li             ARS-007/EPA 901.1                       8/21/08 16:00 "             LA                   N/A NB-95                       -0.715               0.732             2.440             1.220                   pCi/L               ARS-007/EPA 901.1                       8/21/08 16:00             .A                   N/A ZR-95                       -0.232               6.055   1       4.030             2.015                   pCi/L         I     ARS-007/EPA 901.1                       8/21/08 16:00             ILA.                   N/A CS-134                       -0.438               2.482             2.540             1.270                   pCi/L               ARS-007/EPA 901.1                       8/21/08 16:00         --   A                   N/A C13.270                                   0.681             2.300             1.150                   pCV'L         j     ARS-007/EPA 901.1                       8/21/08 16:00             ILA                   N/A BA-140                       -4.173               26.705           10.300             5.150                   pCI/L               ARS-007/EPA 901.1                       8/21/08 16:00               LA         I         N/A LA- 140               1     r2.118                 2.508   I       3.430             1.715                   pCi/L               ARS-007/EPA 901.1.                       8/21./08 16:00           ILA               -   N/A SR-90                       14.269               1.149             0.566             0.267     j             pCi/L               ARS-032/Eilchrom SRW-01                 8/28/08 17:35             BS                 6600%
DDER Anlyi DE DceRtnc Analysis Q- Tp ascripsion Result I CSU 1 (1I) Result 2 CSU 2 (1.) Qual T Meth Moisod Ata/lysi Technicayn Batch .yI Dc r I .I I I [ Units T I arpne ARS1-808-02293 LCSD H3 1136.06 161.4 1143.2572 161.9636 pCi/LI ARS-054/EPA 906.0 9/4/08 22:09 BIS 0.06 < 3 Matrix Spike Anlyal C Unspiked Report Analysis Analysis Analysis Percent LCS Anl Q A (1 ) Spike Con. Qul A ___ nc.Botch Type Results Activity Unit. Test Method Dote/Time Technicton Recovery(%)
H-3                       4630.409               499.979           160.739     j     79.153                   pCi/     I         ARS-054/EPA 906.0                         9/8/08 12:47                                   N/S NI-63                       7.4-21               4 .7             7.4096   i       3.6455 -             ,     CI-               AR--022                                   9/10/0-8 6I:4           8)5                   N/S
Acceptonce I i Range ARS1-808-02293 MS H3 13755.623 1429.035 1862.953 13970.11 pCC/L ARS-054/EPA 906.0 9/5/08 6:24 83S 85 609/o-140%
              .,......................                                                                                                                                                                                         ... . ......
Proj ct Manager l Note": American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than foll requires the written consent of the client.LELAP Certificate#
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# E87558 AMERICAN RADIATION SERVICES INC QC Results Report 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-32996 Sample Delivery Group: ARSI-08-01563 Date Received: 08/12/08 Laboratory Control Sample Evaluation Analysis Qc Ana1te Analysi sC Expected If Report Analysis Analysis I Analysis T Percent LCS BRtch Type Results I (1 6) DC Value ,Units Test Method I TeR ARS1-808-02253.
NOTES: Shipment# 08-152                                             -
LCS Sr-9 0 23.536 1.834 0.541 20.835 pCI/L ARS-032/FPA 905.0 8/28/08 14:29 BIS 113 75%-125%Blank Evaluation Analysis Qc AnalYtO Analysis su I (I.) MDC Expected i l Report "Analysis Analysis Analysis Batch Type Result. Vlue. Qul Units Test Method Dste/Time Technician ARS1-B08-02253 MBL] Sr-90 0.065 0.180 0.618 NA U pCI/L ARS-032/EPA 905.0 8/28/08 14:29 BIS RER Duplicate Evaluation Analysis Result ] CSU 1 (1 e) Result 2 CSU 2 ( Xe) QulAnaly is Analysis M DAnaelysis Analysis RER Ietch Type Description
* Prdject Manager R*          n..                               .
[Units Test Method Di/Tene Technician RA_ _.pt ARS1-B08-02253 LCSD Sr-90 23.536 1.834 21.025 1.649 pCi/L ARS-032/EPA 905.0 8/28/08 14:29 8S1 0.72 < 1 DER Duplicate Evaluation Anlysi 1 QC a Al i AnalysisAnlysie Alysi 1 DR Retch oType Descrip Bton e CSU I 1 1 Result 2 CSU 2 (1.) Q unl i Anysl lysis. D E R Units Test Method Dete/Ti. Technigan E. cceptnceR ARS1-B08-02253 LCSD Sr-90 23.536 1.834 21.025 1.649 pCi/L ARS-032/EPA 905.0 8/28/08 14:29 831 S 2.04 < 3 Proect Manager Revi Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the arlalysis itself. Reproduction of this report in less than full requires the written consent of the client.LELAP Certificate#
Notes; American RodiaLion Services, Inc, assumes no liability for the use Or Interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report In less than full requires the written consent of the client.
30658 NELAP Certificate  
LELAP Certificate# 30658                       NELAP Certificate # E87558
# E87558 QKI.'RS I INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX4aa5) 381-2996 QC Results Report Sample Delivery Group: Date Received: ARSI-08-01 563 08/12/08 'Laboratory Control Sample Evaluation Analysis QC [ Analysis S Expected Report Analysis Analysis Analysis Percent LCS Acceptance Retch Type nlt Results CS I MC Valcueo Qa Units Test Method Date Technician Recovery (%) Range ARS1-808-02204 LCS CO-60 .24779.00 495.75 200.80 25315.22 pCi/g EPA 901.1 .08/18/08 ILA 98 75%-125%ARS1-B08-02204 LCS CS-137 15083.00 359.87 137.80 15285.98 pCi/g EPA 901.1 08/18/08 ILA 99' 75%-125%ARS1-B08-02204 LCS AM-241 34007.00 1235.00 277.10 34794.33 pCi/g EPA 901.1 08/18/08 ILA 98 75%-125%Blank Evaluation Anaiysis Q Aflyte Analysis CSU 1i(1) MDC Expected Report Analysis Analysis Analysis Batch Type Results Value 1 Units Test Method Data Technician ARSI-808-02204 MBL CO-60 -0.001 0.005 0.005 NA U pCi/g EPA 901.1 08/18/08 JLA ARSI-B08-02204 MEL CS-137 0.001 0.001 0.004 NA U pCi/g EPA 901.1 08/18/08 ILA ARSI-B08-02204 MEL AM-241 -0.001 0.014 0.006 NA U pCi/g EPA 901.1 08/18/08 JLA RER Duplicate Evaluation Analysis QC Analysis Analysis Analysis Analysis Analysis RR batch Type Description Result I RF 1ca ROE al 2CU2(s Qa myi Units Test Method Date Technician RER AccltanceeRange ARSI-808-02204 LCSD CO-60 24779.00 495.75 25129.00 492.32 pCI/g EPA 901.1 08/18/08 JLA 0.35 < 1 ARS1-BO-02204 LCSD CS-137 15083.00 359.87 15425.00 341.69 pCi/g EPA 901.1 08/18/08 JLA 0.49 < I ARS1-808-02204 LCSD AM-241 34007.00 1235,00 34050.00 1247.60 pCi/g EPA 901.1 08/18/08 1LA 0.02 < I DER Duplicate Evaluation\
 
Analysis Qc Analysis Result 1 rSU 1 (1 6) Result 2 CSU 2 ( Is AnalysI Analyasi Analysis Analyss DER DER batch Type Description Units Test Method Date Technician AcceptanceRage.
NRC FORM 303 St      U.S. NUCLEAR REGULATORY COMMISSION                   LABORATORY USE ONLY PAGE 1 of 2 (4-2004)                                                                                 CONTROL NUMBER REQUEST FOR ANALYSIS AND CHAIN OF CUSTODY LABORATORY:
ARS1-B08-02204 LCSD CO-60 24779.00 495.75 25129.00 492.32 pCI/g EPA 901.1 08/18/08 31LA 1.00 " 3 APRS1-B08-02204 LCSD CS-137 -15083.00 " 359.87 15425.00 341.69 pCl/u EPA 901.1 08/18/08 ILA 1.38 < 3 ARS1-BOB-02204 LCSD AM-241 34007.00 1235.00 34050.00 1247.60 pCi/O EPA 901.1 08/18/08 ILA 0.05 < 3 QulyAssurance Notes: American Radiation Services, inc. assumes no liability for the use or interpretation of any analytital results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.LELAP Certificate#
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30658 NELAP Certificate  
INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED                                                 "
# E87558 2609 North River Road -Port Allen, Louisiana 70767 RS CA1 (800) 401-4277 FAX (225) 381-2996 AMENAN RDIAION SEAVICES, INC.Notes: Comments: 1.0) Soil and Sludge analysis are reported on a wet basis or an as received basis unless otherwise indicated.
        # TOTAL                   TYPE             -VOLUME               WEIGHT         DATE SAMPLES SUBMITTED         PRIORITY fl   ROU~iNE GROUND WATER               2000 ML             -2   Kg                               I   []   URGENT SAMPLE COLLECTION INTERVAL MONTH   DAY   YEAR     TIME START INSPECTOR RESPONSIBLE                                               TELEPHONE NUMBER STOP:
2.0) The data in this report are within the limits of uncertainty specified inthe reference method unless specified.
Jim Noggle (USNRC)                         (610) 337-5063 LIST DESIRED                                                       LIST DESIRED ANALYSIS TO BE PERFORMED               LLD (Optional)         OTHER TYPE OF ANALYSIS (Specify)           LLD (Optional)
3.0) Modified analysis procedures are procedures that are modified to meet the certain specifications.
[Z     GROSS ALPHA (GA)                                           F-7     STRONTIUM-90 (Sr90)
An example may be the use of a water method to analyze a solid matrix due to the, lack of an officially recognized procedure for the analysis of the solid matrix.4.0) Derived Air Concentrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.5.0) Total activity is actually total gamma activity and is determined utilizing the prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides.
        ]   GROSS BETA (GB)                                                   NICKEL-63 (Ni63)
Total activity may be lower than~the actual total activity due to the extent of secular equilibrium achieved In the various decay chains at the time of analysis.
      *[]GAMMA SPEC (GS)                                               El-STRITIUM (H3)                                               I-D       CARBON-14 (C14)                                           D D-IODINE-25 (1125)
The total activity is not representative of nuclides that emit solely alpha or beta particles.
RELENQUISHED BY             RECEIVED BY             DATE           TIME             REASON FOR CHANGE OF CUSTODY
6.0) Ra-228 is determined via secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).7.0) U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).8.0) All gamma spectroscopy was performed utilizing high purity germanium'detectors (HPGe).9.0) ARS makes every attempt to match sample density to calibrated density; however, in some cases, it is not practical or possible to do so and data results may be affected.Method  
  -56COIRI s~ro~"wq:1-$                     r-     8-6-2006         /030           Prer     /'?       jlA, FEE RECOVERABLE             NO         YSTAC                           NUMBER REMARKS:'
NOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASON ARE NOTED IN REMARKS ABOVE.
NRC FORM303 (4-2004)                                                                                           PRINTED ON RECYCLED PAPER
 
NRC FORM 303                                     U.S. NUCLEAR REGULATORY COMMISSION a        LABORATORY USE ONLY PAGE 2 of 2 (4-2004)                                                                               CONTROL NUMBER SAMPLE RECORD - Continued LABORATORY:
SAMPLE                             SAMPLE NAME                   COLLECTION           REMARKS, PRESERVATIVE NUMBER                           AND DESCRIPTION                   DATE/TIME         ANALYSIS REQUESTED, ETC.
MW-66-21-(005),       Ground Water Split Sample of MW-66-21-(005)                   Sample is unfiltered &unpreserved. Analyze fo c, _ _       Gamma Spec, H3, Sr9O, Ni63 MW-66-36-(005)         Ground Water Split Sample of MW-66-36-(005)                   Sample is unfiltered & unpreserved. Analyze to
__        Gamma Spec, H3, Sr9O, Ni63 NR               ,OMO (420)PITDONRCCE                                                                                                       AE NRC FORM303 (4-2004)                                                                                         PRINTED ON RECYCLED PAPER
 
2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277     FAX (225)'381-2996
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QC Results Report                                                                                                     Sample Delivery Group: ARSI-08-01563 Date Received: 8/12/2008 Laboratory Control Sample Evaluation Antclysis             Q*      Analyt.         Analysis       CSU I C)             DC       Expacted           Report         Analysis           Analysis         Analysis BItch              Type                     Resul*s                                    I   Valeu               Units     Testrasthod          Date/Time       Technidan     Percent Recovery Acc Accaptanca N/A               LCS       Ni-63           237.73           55.2         8.6999       204.44               pCi/L       ARS-022         9/9/08 13:28           BIS         116 75%-125%
Blank Evaluation Antlychs N/A Aays 1QC1 yp Type
_atch MBL Analyt.
Ni-63 1Analysis R__ut_
                                                    '1.023 I  Casis IEpected
_
4.5347
(   )
Ip.~
7.6916
* ile NA        U ReotAIay" Report Units pCi/L An(lysis Test Method ARS-022
* Analysis Data/Tim 9/9/08 21:58 aj  AWslyala
* Tedhnician B)S RER Duplicate Evaluation Analysis Batchs QC Type Analysis Description etst 1 +/-  CSU I( (1)       Result2     CSU 2 (is) Q.*l  Analysils Units Analysis Tea Maehod Arnlysi Date/Tin.
Analytis Techinician R
RER cRER Acpanc.R N/A               LCSD       Ni-63           237.73           55.2         229.996       53.406               pCl/L       ARS-022         9/9/08 17:42           BI5         0,07 DER Duplicate Evaluation Analys               QC         alyi       sI                       (1 )   Result 2     CSU 2 ()   Qua   Analys is       Analyysi           Analysis                                 DER NAtch         IType       IDes             27iption           5           229.9Un96t     5e.T6t                               Method       Dat9/Tim974.5. echn/ia8         20 N/A           ILCS0         NIM-63         237.73       1     55.2       1229.996     153.466 1               PCI/L       ARS-022         9/9/08 17A42           -035       0.20<
Projnect mi"nager         Rlk" Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.
LELAP Certificate# 30658                           NELAP Certificate
* E87558
 
2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277         FAX (225) 381-2996 MERICAN RADIATION SERVICES, INC.
QC Results Report                                                                                                         Sample Delivery Group: ARSI-08-01563 Date Received: 8/12/2008 Laboratory Control Sample Evaluation Analysis               QC       Anetyte       Analysis     I       (1                         et Expected   Qual     Report           Analylo               Analylis     Analysli         Percent       LCS
                                                                                                                .61.4 Batch             Type                       Results                     I   MDc     I   value               Units   I   TeWt Method             Dote/Time     Tachnici.n     Recovery (%) AccIltlnce ARS1-B08-02293             LCS         H3         1136.06         " 16           158.48416     1270.45             pCi/.L   ARS-054/EPA 906.0         9/4/08 128:01       B35             89     75%-125%
Blank Evaluation A
Anlysis
      &Btch QC Typ
                                ] o 1 Analysisi je  Results CSu   (1s)         MDC       Expected value lReport.
Unit.
Analysis Test Method Analysis Date/Tkne Analysi Technician ARS1-B08-02293           M8L         H3           67.923         94.439817       158.41962       NA         U     pCVL     ARS-054/EPA 906.0         9/5/08 2:16         BIS RER Duplicate Evaluation Anallysis             Qc       Analysis       Reut1           CU1 (1 e)         Result 2                       AnSU Unt              Anlyi               Anaysi       ,Aayi                 ER   Ac Botch             Type     Description     Res     1ult  CSU                         CSU 2(1     Qs s)     alUnito        Teat Method             Date/Tim.     Technic   ien       ER     AcceR*llRtn tn.R   j I_IF I_                                                 I                                                 _    I_               _ F11 I                                   n_ .
ARS1-808-02293           LCSD         H3       13136.06             161.4       1143.2572     161.9636             pCi/L     ARS-054/EPA 906.0       9/4/08 22:09         BJS           .0.02         <I DER Duplicate Evaluation Analysis Batch Anlyi
                    .
TQC1Analysias Tp Q-yI    Dc I .
ascripsion r
Result I I
CSU 1 (1I)
I Result 2 I
CSU 2 (1.)   Qual
[A~n-.i.iT
[  Units T
T AsOlysi.
Meth Moisod
                                                                                                                                                      ]        Anlyi Asyao Ata/lysi I
[Analyst.
Technicayn DE DDER DceRtnc arpne ARS1-808-02293           LCSD         H3         1136.06           161.4       1143.2572     161.9636             pCi/LI   ARS-054/EPA 906.0       9/4/08 22:09         BIS             0.06         < 3 Matrix Spike Anlyal Anl                  QC        naly*        A                    (1  )    Unspiked                         Report           Analysis             Analysis       Analysis       Percent         LCS Spike Con. Qul                                       ___                                            A     nc.
Botch             Type                     Results                           Activity                         Unit.       Test I  iMethod          Dote/Time     Technicton     Recovery(%)   Acceptonce Range ARS1-808-02293           MS           H3       13755.623         1429.035       1862.953   13970.11               pCC/L     ARS-054/EPA 906.0         9/5/08 6:24       83S               85     609/o-140%
Proj ct Manager             l Note": American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than foll requires the written consent of the client.
LELAP Certificate# 30658                         - NELAP Certificate # E87558
 
2609 North River Road,             Port Allen, Louisiana 70767 1 (800) 401-4277           FAX (225) 381-32996 AMERICAN RADIATION SERVICES INC QC Results Report                                                                                                                      Sample Delivery Group: ARSI-08-01563 Date Received:     08/12/08 Laboratory Control Sample Evaluation Analysis BRtch Qc Type Ana1te           Analysi Results sC I (1 6)           DC Expected Value If        Report
                                                                                                                      ,Units AnalysisI Test Method Analysis I
Analysis TeR T  Percent        LCS 9
ARS1-808-02253.           LCS       Sr- 0           23.536         1.834           0.541         20.835                 pCI/L     ARS-032/FPA 905.0       8/28/08 14:29       BIS         113       75%-125%
Blank Evaluation Analysis             Qc       AnalYtO         Analysis       su I (I.)         MDC         Expected     i l     Report         "Analysis             Analysis     Analysis Batch               Type                       Result.                                       Vlue.     Qul       Units         Test Method           Dste/Time     Technician ARS1-B08-02253           MBL]       Sr-90             0.065       0.180           0.618           NA         U       pCI/L       ARS-032/EPA 905.0       8/28/08 14:29       BIS RER Duplicate Evaluation Analysis Ietch Type    Description Result   ]   CSU 1 (1 e)     Result 2
[Units CSU 2 ( Xe) QulAnaly is                     M Analysis Test Method DAnaelysis Di/Tene Analysis Technician       RA_ _.pt RER ARS1-B08-02253           LCSD       Sr-90           23.536         1.834         21.025           1.649               pCi/L       ARS-032/EPA 905.0       8/28/08 14:29       8S1         0.72           < 1 DER Duplicate Evaluation 1   QC                                                                                       a   Al       i       AnalysisAnlysie                     Alysi     1             D DR E    R Anlysi Retch                       Descrip oType         Bton     e       CSU I   1 1     Result 2     CSU 2 (1.)     Q   unl             i           lysis.
Anysl Test Method           Dete/Ti.     Technigan         E.         cceptnceR Units ARS1-B08-02253           LCSD       Sr-90           23.536         1.834         21.025           1.649               pCi/L       ARS-032/EPA 905.0       8/28/08 14:29       831S        2.04           < 3 Proect Manager Revi Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the arlalysis itself. Reproduction of this report in less than full requires the written consent of the client.
LELAP Certificate# 30658                         NELAP Certificate # E87558
 
2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277           FAX4aa5) 381-2996 QKI.'RS I                  INTERNATIONAL QC Results Report                                                                                                                     Sample Delivery Group:         ARSI-08-01 563 Date Received:      08/12/08   '
Laboratory Control Sample Evaluation Analysis Retch QC Type        nlt
[   Analysis Results S
CS       I       MC Expected Valcueo   Qa Report Units Analysis Test Method Analysis Date Analysis Technician Percent Recovery (%)
LCS Acceptance Range ARS1-808-02204       LCS       CO-60         .24779.00         495.75       200.80       25315.22                 pCi/g         EPA 901.1             .08/18/08         ILA         98         75%-125%
ARS1-B08-02204       LCS       CS-137         15083.00         359.87         137.80     15285.98                 pCi/g         EPA901.1               08/18/08       ILA         99'         75%-125%
ARS1-B08-02204       LCS       AM-241         34007.00       1235.00       277.10       34794.33                 pCi/g         EPA901.1               08/18/08       ILA         98         75%-125%
Blank Evaluation Anaiysis         Q         Aflyte         Analysis     CSU 1i(1)         MDC         Expected               Report           Analysis               Analysis     Analysis Batch         Type                         Results                                         1 Value                 Units         Test Method               Data       Technician ARSI-808-02204     MBL         CO-60           -0.001           0.005         0.005           NA         U       pCi/g         EPA901.1               08/18/08       JLA ARSI-B08-02204     MEL         CS-137           0.001           0.001         0.004           NA         U       pCi/g         EPA901.1               08/18/08       ILA ARSI-B08-02204     MEL       AM-241           -0.001           0.014         0.006           NA         U       pCi/g         EPA 901.1               08/18/08       JLA RER Duplicate Evaluation Analysis         QC       Analysis                                                                   Qa        myi                                                                RF              ROE batch         Type     Description       Result I           1ca         al   2CU2(s                       Analysis          Analysis              Analysis      Analysis                      RR Units         Test Method               Date       Technician     RER     AccltanceeRange ARSI-808-02204     LCSD       CO-60           24779.00         495.75     25129.00         492.32                 pCI/g         EPA 901.1             08/18/08         JLA         0.35             < 1 ARS1-BO-02204     LCSD       CS-137         15083.00         359.87     15425.00         341.69               pCi/g         EPA 901.1             08/18/08         JLA         0.49             < I ARS1-808-02204     LCSD       AM-241         34007.00       1235,00     34050.00         1247.60               pCi/g         EPA 901.1             08/18/08         1LA         0.02             < I DER   Duplicate Evaluation\
Analysis         Qc       Analysis         Result 1     rSU 1 (1 6)     Result 2     CSU2 (       Is       AnalysI           Analyasi               Analysis     Analyss       DER             DER batch         Type     Description                                                                           Units         Test Method               Date       Technician             AcceptanceRage.
ARS1-B08-02204     LCSD       CO-60           24779.00       495.75       25129.00         492.32                 pCI/g         EPA 901.1             08/18/08         31LA       1.00         "   3 APRS1-B08-02204   LCSD       CS-137 -       15083.00       " 359.87     15425.00         341.69                 pCl/u         EPA 901.1             08/18/08         ILA         1.38             < 3 ARS1-BOB-02204     LCSD       AM-241         34007.00       1235.00     34050.00         1247.60               pCi/O         EPA 901.1             08/18/08         ILA         0.05             < 3 QulyAssurance Notes: American Radiation Services, inc. assumes no liability for the use or interpretation of any analytital results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.
LELAP Certificate# 30658                         NELAP Certificate # E87558
 
2609 North River Road - Port Allen, Louisiana 70767 RS AMENANCA1 RDIAION                                            (800) 401-4277       FAX (225) 381-2996 SEAVICES, INC.
Notes:
Comments:
1.0)       Soil and Sludge analysis are reported on a wet basis or an as received basis unless otherwise indicated.
2.0)       The data in this report are within the limits of uncertainty specified inthe reference method unless specified.
3.0)       Modified analysis procedures are procedures that are modified to meet the certain specifications. An example may be the use of a water method to analyze a solid matrix due to the, lack of an officially recognized procedure for the analysis of the solid matrix.
4.0)       Derived Air Concentrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.
5.0)       Total activity is actually total gamma activity and is determined utilizing the prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides. Total activity may be lower than~the actual total activity due to the extent of secular equilibrium achieved In the various decay chains at the time of analysis. The total activity is not representative of nuclides that emit solely alpha or beta particles.
6.0)       Ra-228 is determined via secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).
7.0)       U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).
8.0)       All gamma spectroscopy was performed utilizing high purity germanium'detectors (HPGe).
9.0)       ARS makes every attempt to match sample density to calibrated density; however, in some cases, it is not practical or possible to do so and data results may be affected.
Method  


==References:==
==References:==


1.0) EPA 600/4-80-032, Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.2.0) Standard Methods for Examination of Water and Waste Water, 18 t 1992.3.0) EPA SW-846, Test Methods for Evaluating Solid Waste, Third Edition, (9/86). (Updated through 1995).4.0) EPA 600/4/79-020, Methods for Chemical Analysis of Water and Waste, March 1983.5.0) HASL 300 Definitions:
1.0)       EPA 600/4-80-032, Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.
1.0) BDL Analyte not detected because the value was below the detection limit.2.0) ND Not detected above the detection limit.3.0) Detection Limit The minimum amount of the analyte that ARS can detect utilizing the specific analysis.4.0) B Method Blank 5.0) D Method Duplicate 6.0) MS Matrix Spike 7.0) S Spike 8.0) RS Reference Spike 9.0) *SC Subcontracted out to another qualified laboratory 10.0) NR Not Referenced 11.0) N/A Not Applicable 12.0) .Reported as a calculated value 13.0) False Positive due to interference from Bi-214 Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires.the written consent of the client.LELAP Cert# 30658 NELAP Cert# E87558}}
2.0)       Standard Methods for Examination of Water and Waste Water, 18t 1992.
3.0)       EPA SW-846, Test Methods for Evaluating Solid Waste, Third Edition, (9/86). (Updated through 1995).
4.0)       EPA 600/4/79-020, Methods for Chemical Analysis of Water and Waste, March 1983.
5.0)       HASL 300 Definitions:
1.0)       BDL                   Analyte not detected because the value was below the detection limit.
2.0)       ND                     Not detected above the detection limit.
3.0)       Detection Limit       The minimum amount of the analyte that ARS can detect utilizing the specific analysis.
4.0)       B                     Method Blank 5.0)       D                     Method Duplicate 6.0)       MS                     Matrix Spike 7.0)       S                     Spike 8.0)       RS                     Reference Spike 9.0)       *SC                   Subcontracted out to another qualified laboratory 10.0)     NR                     Not Referenced 11.0)     N/A                   Not Applicable 12.0)         .                   Reported as a calculated value 13.0)                             False Positive due to interference from Bi-214 Notes:     American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires.the written consent of the client.
LELAP Cert# 30658                                   NELAP Cert# E87558}}

Revision as of 09:43, 14 November 2019

American Radiation Services, Inc. Laboratory Analysis Report No. ARS1-08-01563
ML090540702
Person / Time
Site: Indian Point  Entergy icon.png
Issue date: 09/15/2008
From:
American Radiation Services
To: Noggle J
NRC Region 1
References
ARS1-08-01563
Download: ML090540702 (10)
v • d • e


Text

2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277 -- FAX (225) 381-2996 RNATIONAL American Radiation Services, Inc.

Laboratory Analysis Report ARS1-08-01563 Preparedfor.

Nuclear Regulatory Commission (NRC)

James Noggle USNRC Region 1 475 Allendale Road King of Prussia, PA,19406 James. Noggle@nrc.gov Phone: 610.337.5063 Fax:

1))'h Fr x &A il1\a" . -

~#nager Review4 Management Revi*

Notes: Arnencan Radiation Services, Inc. assumes no liability for (he use or intarpretation of any anflytifal results provided other than the mots of the analysis itself.

Reproduction of this report in less than fut requires the written consent of the client.

Contact Person: Questions regarding this analytical report should be addressed to:

Project Manager ProjectManagers@amrad.com Phone: 225.381.2991 Fax: 225.381.2996 LELAP Cert#.30658 NELAP Cert# E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group: ARS1-08-01563 Request or PO Number: N/A Client Sample ID: MW-66-21-(005)07-29/1148 ARS Sample ID: ARS1-08-01563-001 Sample Collection Date: 07/29/08 11:48 Date Received: 8/12/2008

. Sample Matrix: Aqueous Report Date: 09/15/08 10:19 Afal5ysis

  • " A nalys' f Analysis T ,.MC Qu~al Analysis I Analysis Analysis
  • ,Analysis I AnislyalO Analysis Tracer/Chem
  • l~C Date/rime Technician Dep o. Reslts E 2 . ............. ......... Units Test Method RecoNer t N/A MN-54 -o.784 00.782 2.600 1.300 S pCi/L I ARS-007/EPA 901.1 8/21/08 16:01 )LA FE-59 0 952 1.529 5.140 2.570 pCi/L ARS-007/EPA 901.1 8/21/08 16:01 JLA N/A CO-58 -0.573 0.778 2.600 1.300 i pCVL .1 ARS-007/EPA 901.1 8/21/08 16:01 " LA . N/A O-60 0622 . 0.650 2.240 1 1.120 1 pCi/L. ARS-007/EPA 901.1 8/21/08 16:01 31A N/A ZN-65 0.000 2.499 1 8.400 4.200 ' PCi/L ARS-007/EPA 901.1 8/21/08 16:01 .LA N/A NB-95 J -0.738 1.953 2.81D 1.405 CA 8 N/A ZR-95 0783 1264 4.240 2.120 ' pCI/L I ARS-007/EPA 901.1 8/21/08 16:01 ILA N/A

-0.289 1.169 2.960 1.480 pci/L ARS-007/EPA 901.1 8/21/08 16:01 3LA N/A CS-134 C-137 -0.783 0858 1 2.850 1.425 pCI/L t ARS-007/EPA 901.1 8/21/08 16:01 JLA N/A BA-140 S " i 4.539 I .537 10.400 5.200 pCi/L AR5-O07/EPA 901.1 8/21/08 16:01 2LA N/A

. . .

... . .......- -.........................

ARS O-EPA 901.8/21/08 1 . . A......

LA-140 -0.601 12 3.310 I 1.655 J pCI/I ARS-007/EPA 901.1 8/21/08 16:01 21LA j N/A SR'90 1.005 730.*23o*10 *!

0.216

  • 130 666 0.588 163239 j 0.277 7,9.400 .

pCi/L p/I .

I ARS-032/Eichrom SRW-01 ARS-054/EPA 906.0

{

8/28/08 17:35 9/8/(0 8:39 I 8JS BS 58,00%

N/S i

NI-63 3.0899 4.4642 7.4175 3.6493 pCl/L ARS-022 8910/09 2:05 B3S N/S

____ _* __ _ Ij__ _ - _ _ i _ _ _ _ ___/___

I NOTES: Shipment# 08-152 rý=A ci ~ Rri ,1 c5 £1 P5roct Manager keCýr -

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report in less than full requlres the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate I E87558

2609 North River Road, Port Alien, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996

- INTERNATIONAL ARS Sample Delivery Group: ARSI-08-01563 Request or PO Number: N/A Client Sample ID: MW-66-36-(005)07-29/1205 ARS Sample ID: ARSI-08-01563-002 Sample Collection Date: 07/29/08 12:05 Date Received: 8/12/2008

. Sample Matrix: , Aqueous Report Date: 09/15/08 10:19 Analysis Analysls Anlss Anlss .Analysis Anaysi iL Analyi Tracer/Chern Descripthon Results Error +/- 2 s M l " Ua! Units I Test MethOd - Date/Time Technician I MN-54 0.282 1 0.685 " 2.340 1.170 pCiL ARS-007/SPA 901.1 1-8/21/08 16:00 1 LA $ N/A N/A FE-59 1.794 1.079 3.5S0 1.775 pCiL ARS-007/EPA 901.1 8 /21/08 16:00 ILA ILA N/A it CO-58 ___ ____ 0.007 0.686 2.260 1.130 I pCi/L ARS-007/EPA 901.1 8/21/08 16:00 t ILA N/A CO-60 0.008 0.687 F 2.450 1.225 1 pCI/I ARS-007/EPA 901.1 I 8/21/08 16:00 )LA N/A ZN-6S _ "0.101 1.311 j 4.500 2.250 pCi/Li ARS-007/EPA 901.1 8/21/08 16:00 " LA N/A NB-95 -0.715 0.732 2.440 1.220 pCi/L ARS-007/EPA 901.1 8/21/08 16:00 .A N/A ZR-95 -0.232 6.055 1 4.030 2.015 pCi/L I ARS-007/EPA 901.1 8/21/08 16:00 ILA. N/A CS-134 -0.438 2.482 2.540 1.270 pCi/L ARS-007/EPA 901.1 8/21/08 16:00 -- A N/A C13.270 0.681 2.300 1.150 pCV'L j ARS-007/EPA 901.1 8/21/08 16:00 ILA N/A BA-140 -4.173 26.705 10.300 5.150 pCI/L ARS-007/EPA 901.1 8/21/08 16:00 LA I N/A LA- 140 1 r2.118 2.508 I 3.430 1.715 pCi/L ARS-007/EPA 901.1. 8/21./08 16:00 ILA - N/A SR-90 14.269 1.149 0.566 0.267 j pCi/L ARS-032/Eilchrom SRW-01 8/28/08 17:35 BS 6600%

H-3 4630.409 499.979 160.739 j 79.153 pCi/ I ARS-054/EPA 906.0 9/8/08 12:47 N/S NI-63 7.4-21 4 .7 7.4096 i 3.6455 - , CI- AR--022 9/10/0-8 6I:4 8)5 N/S

.,...................... ... . ......

--- -----. me......

-....

NOTES: Shipment# 08-152 -

  • Prdject Manager R* n.. .

Notes; American RodiaLion Services, Inc, assumes no liability for the use Or Interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report In less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

NRC FORM 303 St U.S. NUCLEAR REGULATORY COMMISSION LABORATORY USE ONLY PAGE 1 of 2 (4-2004) CONTROL NUMBER REQUEST FOR ANALYSIS AND CHAIN OF CUSTODY LABORATORY:

SAMPLE LOCATION (LICENSEE) LICENSEE NUMBER DOCKET NO.

INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED "

  1. TOTAL TYPE -VOLUME WEIGHT DATE SAMPLES SUBMITTED PRIORITY fl ROU~iNE GROUND WATER 2000 ML -2 Kg I [] URGENT SAMPLE COLLECTION INTERVAL MONTH DAY YEAR TIME START INSPECTOR RESPONSIBLE TELEPHONE NUMBER STOP:

Jim Noggle (USNRC) (610) 337-5063 LIST DESIRED LIST DESIRED ANALYSIS TO BE PERFORMED LLD (Optional) OTHER TYPE OF ANALYSIS (Specify) LLD (Optional)

[Z GROSS ALPHA (GA) F-7 STRONTIUM-90 (Sr90)

] GROSS BETA (GB) NICKEL-63 (Ni63)

RELENQUISHED BY RECEIVED BY DATE TIME REASON FOR CHANGE OF CUSTODY

-56COIRI s~ro~"wq:1-$ r- 8-6-2006 /030 Prer /'? jlA, FEE RECOVERABLE NO YSTAC NUMBER REMARKS:'

NOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASON ARE NOTED IN REMARKS ABOVE.

NRC FORM303 (4-2004) PRINTED ON RECYCLED PAPER

NRC FORM 303 U.S. NUCLEAR REGULATORY COMMISSION a LABORATORY USE ONLY PAGE 2 of 2 (4-2004) CONTROL NUMBER SAMPLE RECORD - Continued LABORATORY:

SAMPLE SAMPLE NAME COLLECTION REMARKS, PRESERVATIVE NUMBER AND DESCRIPTION DATE/TIME ANALYSIS REQUESTED, ETC.

MW-66-21-(005), Ground Water Split Sample of MW-66-21-(005) Sample is unfiltered &unpreserved. Analyze fo c, _ _ Gamma Spec, H3, Sr9O, Ni63 MW-66-36-(005) Ground Water Split Sample of MW-66-36-(005) Sample is unfiltered & unpreserved. Analyze to

__ Gamma Spec, H3, Sr9O, Ni63 NR ,OMO (420)PITDONRCCE AE NRC FORM303 (4-2004) PRINTED ON RECYCLED PAPER

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225)'381-2996

  • OA1 RCNRDATION SERVICES, INC.

QC Results Report Sample Delivery Group: ARSI-08-01563 Date Received: 8/12/2008 Laboratory Control Sample Evaluation Antclysis Q* Analyt. Analysis CSU I C) DC Expacted Report Analysis Analysis Analysis BItch Type Resul*s I Valeu Units Testrasthod Date/Time Technidan Percent Recovery Acc Accaptanca N/A LCS Ni-63 237.73 55.2 8.6999 204.44 pCi/L ARS-022 9/9/08 13:28 BIS 116 75%-125%

Blank Evaluation Antlychs N/A Aays 1QC1 yp Type

_atch MBL Analyt.

Ni-63 1Analysis R__ut_

'1.023 I Casis IEpected

_

4.5347

( )

Ip.~

7.6916

  • ile NA U ReotAIay" Report Units pCi/L An(lysis Test Method ARS-022
  • Analysis Data/Tim 9/9/08 21:58 aj AWslyala
  • Tedhnician B)S RER Duplicate Evaluation Analysis Batchs QC Type Analysis Description etst 1 +/- CSU I( (1) Result2 CSU 2 (is) Q.*l Analysils Units Analysis Tea Maehod Arnlysi Date/Tin.

Analytis Techinician R

RER cRER Acpanc.R N/A LCSD Ni-63 237.73 55.2 229.996 53.406 pCl/L ARS-022 9/9/08 17:42 BI5 0,07 DER Duplicate Evaluation Analys QC alyi sI (1 ) Result 2 CSU 2 () Qua Analys is Analyysi Analysis DER NAtch IType IDes 27iption 5 229.9Un96t 5e.T6t Method Dat9/Tim974.5. echn/ia8 20 N/A ILCS0 NIM-63 237.73 1 55.2 1229.996 153.466 1 PCI/L ARS-022 9/9/08 17A42 -035 0.20<

Projnect mi"nager Rlk" Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate

  • E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 MERICAN RADIATION SERVICES, INC.

QC Results Report Sample Delivery Group: ARSI-08-01563 Date Received: 8/12/2008 Laboratory Control Sample Evaluation Analysis QC Anetyte Analysis I (1 et Expected Qual Report Analylo Analylis Analysli Percent LCS

.61.4 Batch Type Results I MDc I value Units I TeWt Method Dote/Time Tachnici.n Recovery (%) AccIltlnce ARS1-B08-02293 LCS H3 1136.06 " 16 158.48416 1270.45 pCi/.L ARS-054/EPA 906.0 9/4/08 128:01 B35 89 75%-125%

Blank Evaluation A

Anlysis

&Btch QC Typ

] o 1 Analysisi je Results CSu (1s) MDC Expected value lReport.

Unit.

Analysis Test Method Analysis Date/Tkne Analysi Technician ARS1-B08-02293 M8L H3 67.923 94.439817 158.41962 NA U pCVL ARS-054/EPA 906.0 9/5/08 2:16 BIS RER Duplicate Evaluation Anallysis Qc Analysis Reut1 CU1 (1 e) Result 2 AnSU Unt Anlyi Anaysi ,Aayi ER Ac Botch Type Description Res 1ult CSU CSU 2(1 Qs s) alUnito Teat Method Date/Tim. Technic ien ER AcceR*llRtn tn.R j I_IF I_ I _ I_ _ F11 I n_ .

ARS1-808-02293 LCSD H3 13136.06 161.4 1143.2572 161.9636 pCi/L ARS-054/EPA 906.0 9/4/08 22:09 BJS .0.02 <I DER Duplicate Evaluation Analysis Batch Anlyi

.

TQC1Analysias Tp Q-yI Dc I .

ascripsion r

Result I I

CSU 1 (1I)

I Result 2 I

CSU 2 (1.) Qual

[A~n-.i.iT

[ Units T

T AsOlysi.

Meth Moisod

] Anlyi Asyao Ata/lysi I

[Analyst.

Technicayn DE DDER DceRtnc arpne ARS1-808-02293 LCSD H3 1136.06 161.4 1143.2572 161.9636 pCi/LI ARS-054/EPA 906.0 9/4/08 22:09 BIS 0.06 < 3 Matrix Spike Anlyal Anl QC naly* A (1 ) Unspiked Report Analysis Analysis Analysis Percent LCS Spike Con. Qul ___ A nc.

Botch Type Results Activity Unit. Test I iMethod Dote/Time Technicton Recovery(%) Acceptonce Range ARS1-808-02293 MS H3 13755.623 1429.035 1862.953 13970.11 pCC/L ARS-054/EPA 906.0 9/5/08 6:24 83S 85 609/o-140%

Proj ct Manager l Note": American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than foll requires the written consent of the client.

LELAP Certificate# 30658 - NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-32996 AMERICAN RADIATION SERVICES INC QC Results Report Sample Delivery Group: ARSI-08-01563 Date Received: 08/12/08 Laboratory Control Sample Evaluation Analysis BRtch Qc Type Ana1te Analysi Results sC I (1 6) DC Expected Value If Report

,Units AnalysisI Test Method Analysis I

Analysis TeR T Percent LCS 9

ARS1-808-02253. LCS Sr- 0 23.536 1.834 0.541 20.835 pCI/L ARS-032/FPA 905.0 8/28/08 14:29 BIS 113 75%-125%

Blank Evaluation Analysis Qc AnalYtO Analysis su I (I.) MDC Expected i l Report "Analysis Analysis Analysis Batch Type Result. Vlue. Qul Units Test Method Dste/Time Technician ARS1-B08-02253 MBL] Sr-90 0.065 0.180 0.618 NA U pCI/L ARS-032/EPA 905.0 8/28/08 14:29 BIS RER Duplicate Evaluation Analysis Ietch Type Description Result ] CSU 1 (1 e) Result 2

[Units CSU 2 ( Xe) QulAnaly is M Analysis Test Method DAnaelysis Di/Tene Analysis Technician RA_ _.pt RER ARS1-B08-02253 LCSD Sr-90 23.536 1.834 21.025 1.649 pCi/L ARS-032/EPA 905.0 8/28/08 14:29 8S1 0.72 < 1 DER Duplicate Evaluation 1 QC a Al i AnalysisAnlysie Alysi 1 D DR E R Anlysi Retch Descrip oType Bton e CSU I 1 1 Result 2 CSU 2 (1.) Q unl i lysis.

Anysl Test Method Dete/Ti. Technigan E. cceptnceR Units ARS1-B08-02253 LCSD Sr-90 23.536 1.834 21.025 1.649 pCi/L ARS-032/EPA 905.0 8/28/08 14:29 831S 2.04 < 3 Proect Manager Revi Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the arlalysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX4aa5) 381-2996 QKI.'RS I INTERNATIONAL QC Results Report Sample Delivery Group: ARSI-08-01 563 Date Received: 08/12/08 '

Laboratory Control Sample Evaluation Analysis Retch QC Type nlt

[ Analysis Results S

CS I MC Expected Valcueo Qa Report Units Analysis Test Method Analysis Date Analysis Technician Percent Recovery (%)

LCS Acceptance Range ARS1-808-02204 LCS CO-60 .24779.00 495.75 200.80 25315.22 pCi/g EPA 901.1 .08/18/08 ILA 98 75%-125%

ARS1-B08-02204 LCS CS-137 15083.00 359.87 137.80 15285.98 pCi/g EPA901.1 08/18/08 ILA 99' 75%-125%

ARS1-B08-02204 LCS AM-241 34007.00 1235.00 277.10 34794.33 pCi/g EPA901.1 08/18/08 ILA 98 75%-125%

Blank Evaluation Anaiysis Q Aflyte Analysis CSU 1i(1) MDC Expected Report Analysis Analysis Analysis Batch Type Results 1 Value Units Test Method Data Technician ARSI-808-02204 MBL CO-60 -0.001 0.005 0.005 NA U pCi/g EPA901.1 08/18/08 JLA ARSI-B08-02204 MEL CS-137 0.001 0.001 0.004 NA U pCi/g EPA901.1 08/18/08 ILA ARSI-B08-02204 MEL AM-241 -0.001 0.014 0.006 NA U pCi/g EPA 901.1 08/18/08 JLA RER Duplicate Evaluation Analysis QC Analysis Qa myi RF ROE batch Type Description Result I 1ca al 2CU2(s Analysis Analysis Analysis Analysis RR Units Test Method Date Technician RER AccltanceeRange ARSI-808-02204 LCSD CO-60 24779.00 495.75 25129.00 492.32 pCI/g EPA 901.1 08/18/08 JLA 0.35 < 1 ARS1-BO-02204 LCSD CS-137 15083.00 359.87 15425.00 341.69 pCi/g EPA 901.1 08/18/08 JLA 0.49 < I ARS1-808-02204 LCSD AM-241 34007.00 1235,00 34050.00 1247.60 pCi/g EPA 901.1 08/18/08 1LA 0.02 < I DER Duplicate Evaluation\

Analysis Qc Analysis Result 1 rSU 1 (1 6) Result 2 CSU2 ( Is AnalysI Analyasi Analysis Analyss DER DER batch Type Description Units Test Method Date Technician AcceptanceRage.

ARS1-B08-02204 LCSD CO-60 24779.00 495.75 25129.00 492.32 pCI/g EPA 901.1 08/18/08 31LA 1.00 " 3 APRS1-B08-02204 LCSD CS-137 - 15083.00 " 359.87 15425.00 341.69 pCl/u EPA 901.1 08/18/08 ILA 1.38 < 3 ARS1-BOB-02204 LCSD AM-241 34007.00 1235.00 34050.00 1247.60 pCi/O EPA 901.1 08/18/08 ILA 0.05 < 3 QulyAssurance Notes: American Radiation Services, inc. assumes no liability for the use or interpretation of any analytital results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

2609 North River Road - Port Allen, Louisiana 70767 RS AMENANCA1 RDIAION (800) 401-4277 FAX (225) 381-2996 SEAVICES, INC.

Notes:

Comments:

1.0) Soil and Sludge analysis are reported on a wet basis or an as received basis unless otherwise indicated.

2.0) The data in this report are within the limits of uncertainty specified inthe reference method unless specified.

3.0) Modified analysis procedures are procedures that are modified to meet the certain specifications. An example may be the use of a water method to analyze a solid matrix due to the, lack of an officially recognized procedure for the analysis of the solid matrix.

4.0) Derived Air Concentrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.

5.0) Total activity is actually total gamma activity and is determined utilizing the prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides. Total activity may be lower than~the actual total activity due to the extent of secular equilibrium achieved In the various decay chains at the time of analysis. The total activity is not representative of nuclides that emit solely alpha or beta particles.

6.0) Ra-228 is determined via secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).

7.0) U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).

8.0) All gamma spectroscopy was performed utilizing high purity germanium'detectors (HPGe).

9.0) ARS makes every attempt to match sample density to calibrated density; however, in some cases, it is not practical or possible to do so and data results may be affected.

Method

References:

1.0) EPA 600/4-80-032, Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.

2.0) Standard Methods for Examination of Water and Waste Water, 18t 1992.

3.0) EPA SW-846, Test Methods for Evaluating Solid Waste, Third Edition, (9/86). (Updated through 1995).

4.0) EPA 600/4/79-020, Methods for Chemical Analysis of Water and Waste, March 1983.

5.0) HASL 300 Definitions:

1.0) BDL Analyte not detected because the value was below the detection limit.

2.0) ND Not detected above the detection limit.

3.0) Detection Limit The minimum amount of the analyte that ARS can detect utilizing the specific analysis.

4.0) B Method Blank 5.0) D Method Duplicate 6.0) MS Matrix Spike 7.0) S Spike 8.0) RS Reference Spike 9.0) *SC Subcontracted out to another qualified laboratory 10.0) NR Not Referenced 11.0) N/A Not Applicable 12.0) . Reported as a calculated value 13.0) False Positive due to interference from Bi-214 Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires.the written consent of the client.

LELAP Cert# 30658 NELAP Cert# E87558

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