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{{#Wiki_filter:OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION Distribution approval and concurrence
{{#Wiki_filter:OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION March 30,2007 Mr. Jim Kottan U.S. Nuclear Regulatory Commission Region I 475 Allendale Road IGng of Prussia, PA 19406
: Technical Management Team Member Quality Manager March 30,2007 InitiabA Mr. Jim Kottan U.S. Nuclear Regulatory Commission Region I 475 Allendale Road IGng of Prussia, PA 19406  


==SUBJECT:==
==SUBJECT:==
INTERIM REPORT FOR COMPLETED ANALYSES FOR SAMPLES FROM SET EIGHTEEN, FROM THE INDIAN POINT POWER STATION, BUCHANAN, NEW YORK [INSPECTION REPORT NO. 050-247/2006-0071
INTERIM REPORT FOR COMPLETED ANALYSES FOR SAMPLES FROM SET EIGHTEEN, FROM T H E INDIAN POINT POWER STATION, BUCHANAN, NEW YORK
[RFTA NO. 06-0011  
[INSPECTION REPORT NO. 050-247/2006-0071 [RFTA NO. 06-0011


==Dear Mr. Kottan:==
==Dear Mr. Kottan:==
The Oak Ridge Institute for Science and Education (ORISE) received set 18, consisting of seven water samples, associated with the Indian Point Power Station on December 7 and 8,2006. Sample analysis was initiated based on your previous direction for handling samples from ths licensee. Sample identification and collection data for the samples addressed in ths report are presented in Table 1. Gamma spectroscopy, the hard-to-detect betas (iron-55, nickel-63, and tritium), technetium-99, total radiostrontium, alpha spectroscopy, plutonium-241, and carbon-14 data are provided in Tables 2 through 8, respectively.
 
The pertinent procedure references are provided in each specific table. ORISE's Quality Control (QC) requirements were met for these analyses.
The Oak Ridge Institute for Science and Education (ORISE) received set 18, consisting of seven water samples, associated with the Indian Point Power Station on December 7 and 8,2006. Sample analysis was initiated based on your previous direction for handling samples from t h s licensee. Sample identification and collection data for the samples addressed in t h s report are presented in Table 1.
The QC fies are available for your review upon request. Additional reports wdl follow after the completion of the requested analyses.
Gamma spectroscopy, the hard-to-detect betas (iron-55, nickel-63, and tritium), technetium-99, total radiostrontium, alpha spectroscopy, plutonium-241, and carbon-14 data are provided in Tables 2 through 8, respectively. The pertinent procedure references are provided in each specific table.
ORISE has removed the Ni-59 data due to problems with the calculation associated with the concentration of thls radionuclide.
ORISEs Quality Control (QC) requirements were met for these analyses. The QC fies are available for your review upon request. Additional reports wdl follow after the completion of the requested analyses.
ORISE is discontinuing the reporting of Ni-59 data und ths problem can be resolved.
ORISE has removed the Ni-59 data due to problems with the calculation associated with the concentration of thls radionuclide. ORISE is discontinuing the reporting of Ni-59 data u n d t h s problem can be resolved.
My contact information is listed below. You may also contact Wade Ivey at 865.576.9184 with any questions or comments.
My contact information is listed below. You may also contact Wade Ivey at 865.576.9184 with any questions or comments.
Dale Condra, Manager Laboratory RDC:wPI:km Enclosures C: T. Carter, NRC/FSME/DWMEP 7518 E. IOlox-Davin, NRC/FSME/TWFN 8A23 M. Roberts, NRC Region I File 1697 E. Abelquist, ORISEg S. IGk, ORISE v7 J. White, NRC Regiony Voice: 86 5.24 1.3242 Fax: 865.241.3248 E-mad Dale.Condra @orau.org TABLE 1 ORISE Sample ID 1697W0116" 1697M006bb 1697W0117 1697M0067 1697W0118 1697M0068 SAMPLE IDENTIFICATIONS AND COLLECTION DATA INDIAN POINT POWER STATION BUCHANAN, NEW YORK NRC Region I Collection Collection Sample ID Date Time RO-543-95' 12/5/2006 11:45 1697W0116 filter 12/5/2006 11:45 P-1217 12/6/2006 10:45 1697W0117 filter 12/6/2006 10:45 Ft. Montgomery 12/5/2006 900 1697W0118 filter 12/5/2006 900 1697W0119 1697M0069 1697W0120 1697M0070 1697W0121 1697M0071 1697W0122 1697M0072 RO-18 12/5/2006 10:25 1697W0119 filter 12/5/2006 10:25 RO-543-50 12/5/2006 11:30 1697WO120 filter 12/5/2006 11:30 Mw-51-(011) 12/6/2006 11:45 1697W0121 filter 12/6/2006 11:45 MW-40-(010) 12/7/2006 9:37 1697W0122 filter 12/7/2006 937 Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Set 18 TABLE 2 ORISE Sample ID BJ NRC Region I Radionuclide Concentrations Sample ID CO-58 CO-60 cs-134 CONCENTRATIONS OF SELECTED GAMMA EMITTING RADIONUCLIDES IN WATER SAMPLES GAMMA SPECTROSCOPY CP1, REVISIOF INDIAN POINT POWER STATION BUCHANAN, NEW YORK 1697W0121 MW-51-(011)
Dale Condra, Manager Laboratory RDC:wPI:km Enclosures C:       T. Carter, NRC/FSME/DWMEP 7518                               E. Abelquist, O R I S E g E. IOlox-Davin, NRC/FSME/TWFN 8A23                           S. IGk, ORISE        v7 M. Roberts, NRC Region I                                     J. White, NRC Regiony File 1697 Distribution approval and concurrence :        InitiabA Technical Management Team Member Quality Manager Voice: 865.241.3242                   Fax: 865.241.3248     E-mad Dale.Condra @orau.org
-0.6 f. 2.7 1.1 f. 2.3 1.5 f. 2.5 1697W0122 MW-40-(010)
 
-0.3 f. 1.7 0.3 f. 1.7 0.1 k 1.9 15 -1.0 f. 4.5 0.2 f. 1.8 1697W0116 1697W0117 1697W0118 1697W0119 b RO-543-95'  
TABLE 1 SAMPLE IDENTIFICATIONS AND COLLECTION DATA INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE        NRC Region I     Collection         Collection Sample ID       Sample ID        Date               Time 1697W0116"      RO-543-95'     12/5/2006             11:45 1697M006bb    1697W0116 filter 12/5/2006             11:45 1697W0117          P-1217     12/6/2006             10:45 1697M0067      1697W0117 filter 12/6/2006             10:45 1697W0118      Ft. Montgomery   12/5/2006             900 1697M0068      1697W0118 filter 12/5/2006             900 1697W0119           RO-18       12/5/2006             10:25 1697M0069      1697W0119 filter 12/5/2006             10:25 1697W0120        RO-543-50     12/5/2006             11:30 1697M0070      1697WO120 filter 12/5/2006             11:30 1697W0121      Mw-51-(011)     12/6/2006             11:45 1697M0071      1697W0121 filter 12/6/2006             11:45 1697W0122      MW-40-(010)     12/7/2006             9:37 1697M0072      1697W0122 filter 12/7/2006             937 Indian Point Power Station                                     projects/l697/Data Tables/2007-03-30 Data Tables Set 18
-1.5 f. 2.2 0.4 f. 2.2 -0.2 f. 2.1 P-1217 1.2 f. 2.4 0.8 f. 2.2 -0.1 f. 2.3 Ft. Montgomery 1.1 L- 1.7 0.9 k 1.7 1.0 f: 1.7 RO-18 -1.0 f. 2.4 0.9 f. 2.4 -0.7 f. 2.5 -1.8 f. 4.3 -1.6 f. 2.0 2.3 k 2.5 0.2 k 3.1 -0.4 f. 2.1 11 "The range of MDCs for the selected radionuclides is 2.8 pCi/L to 4.4 pCi/L. bUncertainties represent the 95% confidence level, based on total propagated uncertainties Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Set 18 TABLE 3 ORISE Sample ID 1697W0116 1 69W0117 1697W0118 CONCENTRATIONS OF HARD TO DETECT BETA EMITTING RADIONUCLIDES IN WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK Radionuclide Concentrationsa (pCi/L) NRC Region I Sample ID Fe-55b Ni-63" H-3d RO-543-95' 8 k 20' , 33 -5.0 k 5.5 9.7 200 k 210 , 360 P-1217 -4 k 19 33 2.3 & 5.7 9.7 80 & 200 360 Ft.Montgomery 4 & 20 , 33 0.4 ? 5.6 . 9.7 50 k 200 . 360 1697W0120 1697W0121 1697W0119 I RO-18 I 1 k 19 . 33 I 1.9 k 5.7 . 9.7 1 110 k 210 . 360 11 360 360 I MW-51-(011)  
 
-2 k 19 , 33 0.2 k 5.6 , 9.7 70 & 200 . RO-543-50
TABLE 2 CONCENTRATIONS OF SELECTED GAMMA EMITTING RADIONUCLIDES I N WATER SAMPLES BJ GAMMA SPECTROSCOPY CP1, REVISIOF 15 INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE                    NRC Region I                                  Radionuclide Concentrations Sample ID                      Sample I D                        CO-58              CO-60          cs-134 b
-5 f. 19 , 33 1.4 k 5.7 9.7 260 t 220 1697W0122 I MW-40-(010)
1697W0116                     RO-543-95'                     -1.5 f. 2.2           0.4 f. 2.2 -0.2 f. 2.1             -1.8    f. 4.3 1697W0117                          P-1217                     1.2 f. 2.4           0.8 f. 2.2 -0.1 f. 2.3             -1.6    f. 2.0 1697W0118                  Ft. Montgomery                     1.1 L- 1.7           0.9 k 1.7     1.0 f: 1.7           2.3      k    2.5 1697W0119                          RO-18                     -1.0 f. 2.4           0.9 f. 2.4 -0.7 f. 2.5               0.2    k    3.1
I 13 & 20 , 33 I 1.8 k 5.7 9.7 I 290 k 220 , 360 "The MDCs for each radionuclide are after the comma. "e-55 analyzed using procedure AP13, Revision 4. 'Ni-63 analyzed using procedure AP17, Revision 0. d11-3 analyzed using procedure AP2, Revision
                                                                                                                              -0.4    f. 2.1    1 1697W0121                    MW-51-(011)                    -0.6 f. 2.7          1.1 f. 2.3     1.5 f. 2.5           -1.0    f. 4.5 1697W0122                    MW-40-(010)                    -0.3 f. 1.7          0.3 f. 1.7    0.1 k 1.9            0.2     f. 1.8 "The range of MDCs for the selected radionuclides is 2.8 pCi/L to 4.4 pCi/L.
: 15. eUncertainties represent the 95%
bUncertainties represent the 95% confidence level, based on total propagated uncertainties Indian Point Power Station                                                                     projects/l697/Data Tables/2007-03-30 Data Tables Set 18
confidence level, based on total propagated uncertainties.
 
Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Set 18 TABLE 4 ORISE NRC Region I Sample ID Sample ID 1697WOl16 RO-543-95' 1697W0117 P-1217 1697W0118 Ft. Montgomery 1697W0119 RO-18 1697W0120 RO-543-50  
TABLE 3 CONCENTRATIONS OF HARD TO DETECT BETA EMITTING RADIONUCLIDES I N WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK Radionuclide Concentrationsa(pCi/L)
ORISE                    NRC Region I Sample ID                     Sample I D                            Fe-55b                     Ni-63"                               H-3d 1697W0116                    RO-543-95'                     8   k 20' , 33             -5.0 k 5.5           9.7     200       k     210       , 360 169W0117                          P-1217                   -4 k 19                 33   2.3 &     5.7       9.7       80       &     200           360 1697W0118                  Ft.Montgomery                     4   & 20 , 33             0.4 ?     5.6     . 9.7       50       k     200       . 360 1697W0119             I           RO-18                 I   1   k 19       . 33 I 1.9 k 5.7       . 9.7   1   110       k     210       . 360 11 1697W0120 1697W0121 1697W0122            I RO-543-50 MW-51-(011)
MW-40-(010)
                                                                -5 f. 19 , 33
                                                                -2 k 19 , 33 I 13    & 20 , 33            I 1.4 k 5.7 0.2 k 5.6 1.8 k 5.7 9.7 9.7 9.7 I 260 70 290 t
k 220 200 220
                                                                                                                                                      . 360
                                                                                                                                                      , 360 I
"The MDCs for each radionuclide are after the comma.
"e-55   analyzed using procedure AP13, Revision 4.
'Ni-63 analyzed using procedure AP17, Revision 0.
d11-3 analyzed using procedure AP2, Revision 15.
eUncertainties represent the 95% confidence level, based on total propagated uncertainties.
Indian Point Power Station                                                                   projects/l697/Data Tables/2007-03-30 Data Tables Set 18
 
TABLE 4 CONCENTRATIONS OF TECHNETIUM-99 (Tc-99)
IN WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS AP5, REVISION 16; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE         NRC Region I           Radionuclide Sample I D        Sample I D      Concentrationsa (pCi/L) 1697WOl16          RO-543-95'      5.0    t 8.3b , 14.0 1697W0117            P-1217        3.4    k      8.2    ,  14.0 1697W0118        Ft. Montgomery    2.7    2      8.2    , 14.0 1697W0119            RO-18        -1.8    k      8.1    , 14.0 1697W0120          RO-543-50        6.4    t 8.3 , 14.0 1697WO 121        MW-5 1-(011)    -2.7    +_    8.1    , 14.0 1697W0122        MW-40-(010)      5.2    ?      8.3    , 14.0 Indian Point Power Station                                        projects/l697/Data Tables/2007-03-30 Data Tables Sct 18
 
TABLE 5 ORISE      NRC Region I        Radionuclide Concentrations, Sample ID       Sample ID         TPUs, and MDCS"@Ci/L) 11    1697\)(10116 I  RO-543-95'     I  0.29    ?        0.36b      . 0.60      11 1      1697W0117   I      P-1217       I -0.09    k        0.39        ,    0.69    1 1697W0118     Ft. Montgomery     -0.08    &        0.34        ,    0.60 1697W0119          RO-18          -0.10    k        0.37        , 0.66 1697W0120        RO-543-50        0.18    k        0.39        . 0.66
                    .1697W0121      MW-51-(011)        0.37    ?        0.36        ,    0.61 1697W0122      Mw-40-(010)        0.61    k        0.35        ,    0.56 Indian Point Power Station                                    projects/l697/Data Tables/2007-03-30 Data 'Tables Set 18
 
F a                                                          TABLE 6 9
g n                                            CONCENTRATIONS OF SELECTED ALPHA EMITTING RADIONUCLIDES IN SUSPENDED AND DISSOLVED FRACTIONS OF WATER SAMPLES AP11, REVISION 3; CP2, REVISION 12 INDIAN POINT POWER STATION BUCHANAN, NEW YORK 1697W0119       RO-18         0.11 f: 0.18 , 0.31    0.00 f  0.09 , 0.20  0.07 f: 0.17 , 0.30  0.02 k  0.08 , 0.16 1697M0069  1697W0119 filter  0.01 f 0.02 , 0.04    0.00 f  0.01 , 0.02  0.00 f: 0.02 , 0.04  0.01 k  0.01 , 0.01 1697W0120     RO-543-50       0.17 k 0.21 , 0.34    -0.02 f  0.10 , 0.23  0.06 f  0.16 , 0.30  -0.02 f  0.08 , 0.20 CD . 1697M0070  1697W0120 filter  0.02 f 0.02 , 0.04    0.00 f: 0.01 , 0.02  0.01 f  0.02 , 0.03  0.00 k  0.02 , 0.06
+
2U
--. 1697W0121    nnXr-51-(011)    0.09 f: 0.15 , 0.26  0.05 f  0.08 , 0.13  -0.05 f: 0.11 , 0.26  -0.06 k  0.10 , 0.26 2  16971110071 1697W0121 filter  0.01 f 0.02 , 0.04    0.01 f  0.01 , 0.02  0.00 f  0.02 , 0.04 -0.002 f 0.005 , 0.02 1697W0122    MW-40-(010)      0.23 f: 0.21 , 0.33  0.02 f  0.09 , 0.19  -0.02 f: 0.13 , 0.28  0.06 k  0.07 , 0.06
\
1697M0072  1697W0122 filter  0.01 k 0.02 , 0.04    0.00 f  0.01 , 0.03  0.00 f  0.02 , 0.04  -0.01 f 0.01 , 0.03 7 J
 
TABLE 6 (Continued)
CONCENTRATIONS OF SELECTED ALPHA EMITTING RADIONUCLIDES IN SUSPENDED AND DISSOLVED FRACTIONS O F WATER SAMPLES AP11, REVISION 3; CP2, REVISION 12 INDIAN POINT POWER STATION BUCHANAN, N E W YORK 5
N
  %e MDCs are after the comma.
8  buncertainties represent the 95% confidence level, based on total propagated uncertainties.
$  'Zero values are due to rounding.
dSignificantfigures expanded tn avoid repnrting a TPLT of 7ero at the request of the inspector U
E 2
B E
F+
W


1697 WO 12 1 MW-5 1-(011) 1697W0122 MW-40-(010)
TABLE 7 CONCENTRATIONS OF PLUTONIUM-241 I N SUSPENDED AND DISSOLVED FRACTIONS OF WATER SAMPLES BY LIQUID SCINTILUTION ANALYSIS AP10, REVISION 2; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE                        NRC Region I                      Radionuclide Concentrationsa @Ci/g of sediment in 100 mL or pCi/L for Sample ID                            Sample ID water) 1697W0116                            RO-543-95'                         -13          f.       35b       ,       60 1697M0066                        1697W0116 filter                         1.6         &         4.5       ,       7.6 1697W0117                              I?-1217                           8           k         33         ,       57 1697M0067                        1697W0117 filter                         1.6
CONCENTRATIONS OF TECHNETIUM-99 (Tc-99) IN WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS AP5, REVISION 16; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK Radionuclide Concentrationsa (pCi/L) 14.0 5.0 t 8.3 , 3.4 k 8.2 , 14.0 2.7 2 8.2 , 14.0 -1.8 k 8.1 , 14.0 6.4 t 8.3 , 14.0 -2.7 +_ 8.1 , 14.0 5.2 ? 8.3 , 14.0 b Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Sct 18 TABLE 5 ORISE Sample ID NRC Region I Radionuclide Concentrations, Sample ID TPUs, and MDCS" @Ci/L) 11 1697\)(10116 I RO-543-95' I 0.29 ? 0.36b . 0.60 11 1697W0118 1697W0119 1697W0120 11 1697W0117 I P-1217 I -0.09 k 0.39 , 0.69 11 Ft. Montgomery
* 4.5                 7.7 1697W0118                       Ft. Montgomery                           8
-0.08 & 0.34 , 0.60 RO-18 -0.10 k 0.37 , 0.66 RO-543-50 0.18 k 0.39 . 0.66 .1697W0121 1697W0122 MW-51-(011) 0.37 ? 0.36 , 0.61 Mw-40-(010) 0.61 k 0.35 , 0.56 Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data 'Tables Set 18 F TABLE 6 a 9 -. CD --. 8 --. 2 2 + U \ 7J' g n 1697W0119 RO-18 0.11 f: 0.18 , 0.31 0.00 f 0.09 , 0.20 0.07 f: 0.17 , 0.30 0.02 k 0.08 , 0.16 1697M0069 1697W0119 filter 0.01 f 0.02 , 0.04 0.00 f 0.01 , 0.02 0.00 f: 0.02 , 0.04 0.01 k 0.01 , 0.01 1697W0120 RO-543-50 0.17 k 0.21 , 0.34 -0.02 f 0.10 , 0.23 0.06 f 0.16 , 0.30 -0.02 f 0.08 , 0.20 1697M0070 1697W0120 filter 0.02 f 0.02 , 0.04 0.00 f: 0.01 , 0.02 0.01 f 0.02 , 0.03 0.00 k 0.02 , 0.06 1697W0121 nnXr-51-(011) 0.09 f: 0.15 , 0.26 0.05 f 0.08 , 0.13 -0.05 f: 0.11 , 0.26 -0.06 k 0.10 , 0.26 16971110071 1697W0121 filter 0.01 f 0.02 , 0.04 0.01 f 0.01 , 0.02 0.00 f 0.02 , 0.04 -0.002 f 0.005 , 0.02 1697W0122 MW (0 1 0) 0.23 f: 0.21 , 0.33 0.02 f 0.09 , 0.19 -0.02 f: 0.13 , 0.28 0.06 k 0.07 , 0.06 1697M0072 1697W0122 filter 0.01 k 0.02 , 0.04 0.00 f 0.01 , 0.03 0.00 f 0.02 , 0.04 -0.01 f 0.01 , 0.03 CONCENTRATIONS OF SELECTED ALPHA EMITTING RADIONUCLIDES IN SUSPENDED AND DISSOLVED FRACTIONS OF WATER SAMPLES AP11, REVISION 3; CP2, REVISION 12 INDIAN POINT POWER STATION BUCHANAN, NEW YORK TABLE 6 (Continued)
* 33         ,       56 1697M0068                        1697W0118 filter                       -2.6         f.       4.9         ,       8.5 1697W0119                              RO-18                             3           f.       35         Y       61 1697M0069                        1697W0119 filter                         3.5         k         4.5                 7.4 1        1697W0120               I           RO-543-50 1697M0070                        1697W0120 filter                         1           f.         10         ,       17 1697W0121                          MW-51-(011)                           23           &         34         ,       57 1697M0071                        1697W0121 filter                       -0.3         k         4.3         ,       7.4 1697W0122                          MW-40-(010)                           14           &         35                 60 9
CONCENTRATIONS OF SELECTED ALPHA EMITTING RADIONUCLIDES IN SUSPENDED AND DISSOLVED FRACTIONS OF WATER SAMPLES AP11, REVISION 3; CP2, REVISION 12 INDIAN POINT POWER STATION BUCHANAN, NEW YORK 5 %e MDCs are after the comma. 8 buncertainties represent the 95% confidence level, based on total propagated uncertainties.
1697M0072                      1697WO122 filter                       -0.2                   4.2                 7.2 "The MDCs are after the comma.
$ 'Zero values are due to rounding.
          'Uncertainties represent the 95% confidence level, based on total propagated uncertainties Indian Point Power Station                                                                           projects/l697/Data Tables/2007-03-30 Data Tables Set 18
U N dSignificant figures expanded tn avoid repnrting a TPLT of 7ero at the request of the inspector E 2 F B E + W TABLE 7 ORISE Sample ID 1697W0116 1697M0066 1697W0117 1697M0067 CONCENTRATIONS OF PLUTONIUM-241 IN SUSPENDED AND DISSOLVED FRACTIONS OF WATER SAMPLES BY LIQUID SCINTILUTION ANALYSIS AP10, REVISION 2; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK Radionuclide Concentrationsa  
@Ci/g of sediment in 100 mL or pCi/L for water) NRC Region I Sample ID RO-543-95'  
-1 3 f. 35b , 60 1697W0116 filter 1.6 & 4.5 , 7.6 I?-1217 8 k 33 , 57 1697W0117 filter 1.6
* 4.5 7.7 1697W0118 1697M0068 1697W0119 1697M0069 Ft. Montgomery 8
* 33 , 56 1697W0118 filter  
-2.6 f. 4.9 , 8.5 RO-18 3 f. 35 Y 61 1697W0119 filter 3.5 k 4.5 7.4 11 1697W0120 I 1697M0070 1697W0121 1697M0071 1697W0122 1697M0072 RO-543-50 1697W0120 filter 1 f. 10 , 17 MW-51-(011) 23 & 34 , 57 1697W0121 filter  
-0.3 k 4.3 , 7.4 MW-40-(010) 14 & 35 9 60 1697WO122 filter -0.2
* 4.2 7.2 "The MDCs are after the comma. 'Uncertainties represent the 95% confidence level, based on total propagated uncertainties Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Set 18 TABLE 8 ORISE Sample ID 1697w0116 CONCENTRATIONS OF CARBON-14 IN WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS AP9, REVISION 3; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK NRC Region I Radionuclide Concentrations, Sample ID TPUs, and MDCS" (pCi/L) RO-543-95' 4 k 1 2b . 20 1697W0117 1697W0118


1697W0119 1697W0120 P-1217 4 t 12 Y 20 Ft. Montgomery 6 k 12 Y 20 RO-18 0" k 12 Y 20 RO-543-50 4 t 12 . 20 1697W0121 1697W0122 "MDCs are after the comma. buncertainties represent the 95"/0 confidence level, based on total propagated uncertainties.  
TABLE 8 CONCENTRATIONS OF CARBON-14 I N WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS AP9, REVISION 3; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE                        NRC Region I                          Radionuclide Concentrations, Sample ID                          Sample ID                            TPUs, and MDCS"(pCi/L) 1697w0116                          RO-543-95'                            4          k        12b        .      20 1697W0117                              P-1217                             4           t         12         Y     20 1697W0118                      Ft. Montgomery                           6           k         12         Y     20 1697W0119                              RO-18                             0"           k         12       Y       20 1697W0120                          RO-543-50                             4           t         12         .     20 1697W0121                         MW-5 1-(011)                          0          k        12        Y      20 1697W0122                         Mw-40-(010)                            1          k        12        .      20 "MDCs are after the comma.
'Zero values are due to rounding.
buncertainties represent the 95"/0 confidence level, based on total propagated uncertainties.
MW-5 1 -(011) 0 k 12 Y 20 Mw-40-(010) 1 k 12 . 20 Indian Point Power Station projccts/l697/Data Tables/2007-03-30 Data Tables Set 18}}
              'Zero values are due to rounding.
Indian Point Power Station                                                                           projccts/l697/Data Tables/2007-03-30 Data Tables Set 18}}

Latest revision as of 14:06, 13 March 2020

Orise Interim Report for Completed Analyses for Samples from Set Eighteen, from the Indian Point Power Station, Buchanan, Ny, Dtd 03/30/07
ML071900442
Person / Time
Site: Indian Point Entergy icon.png
Issue date: 03/30/2007
From: Condra D
Oak Ridge Institute for Science & Education
To: Kottan J
NRC Region 1
References
IR-06-007, RFTA 06-001
Download: ML071900442 (10)
v • d • e


Text

OAK RIDGE INSTITUTE FOR SCIENCE AND EDUCATION March 30,2007 Mr. Jim Kottan U.S. Nuclear Regulatory Commission Region I 475 Allendale Road IGng of Prussia, PA 19406

SUBJECT:

INTERIM REPORT FOR COMPLETED ANALYSES FOR SAMPLES FROM SET EIGHTEEN, FROM T H E INDIAN POINT POWER STATION, BUCHANAN, NEW YORK

[INSPECTION REPORT NO. 050-247/2006-0071 [RFTA NO. 06-0011

Dear Mr. Kottan:

The Oak Ridge Institute for Science and Education (ORISE) received set 18, consisting of seven water samples, associated with the Indian Point Power Station on December 7 and 8,2006. Sample analysis was initiated based on your previous direction for handling samples from t h s licensee. Sample identification and collection data for the samples addressed in t h s report are presented in Table 1.

Gamma spectroscopy, the hard-to-detect betas (iron-55, nickel-63, and tritium), technetium-99, total radiostrontium, alpha spectroscopy, plutonium-241, and carbon-14 data are provided in Tables 2 through 8, respectively. The pertinent procedure references are provided in each specific table.

ORISEs Quality Control (QC) requirements were met for these analyses. The QC fies are available for your review upon request. Additional reports wdl follow after the completion of the requested analyses.

ORISE has removed the Ni-59 data due to problems with the calculation associated with the concentration of thls radionuclide. ORISE is discontinuing the reporting of Ni-59 data u n d t h s problem can be resolved.

My contact information is listed below. You may also contact Wade Ivey at 865.576.9184 with any questions or comments.

Dale Condra, Manager Laboratory RDC:wPI:km Enclosures C: T. Carter, NRC/FSME/DWMEP 7518 E. Abelquist, O R I S E g E. IOlox-Davin, NRC/FSME/TWFN 8A23 S. IGk, ORISE v7 M. Roberts, NRC Region I J. White, NRC Regiony File 1697 Distribution approval and concurrence : InitiabA Technical Management Team Member Quality Manager Voice: 865.241.3242 Fax: 865.241.3248 E-mad Dale.Condra @orau.org

TABLE 1 SAMPLE IDENTIFICATIONS AND COLLECTION DATA INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE NRC Region I Collection Collection Sample ID Sample ID Date Time 1697W0116" RO-543-95' 12/5/2006 11:45 1697M006bb 1697W0116 filter 12/5/2006 11:45 1697W0117 P-1217 12/6/2006 10:45 1697M0067 1697W0117 filter 12/6/2006 10:45 1697W0118 Ft. Montgomery 12/5/2006 900 1697M0068 1697W0118 filter 12/5/2006 900 1697W0119 RO-18 12/5/2006 10:25 1697M0069 1697W0119 filter 12/5/2006 10:25 1697W0120 RO-543-50 12/5/2006 11:30 1697M0070 1697WO120 filter 12/5/2006 11:30 1697W0121 Mw-51-(011) 12/6/2006 11:45 1697M0071 1697W0121 filter 12/6/2006 11:45 1697W0122 MW-40-(010) 12/7/2006 9:37 1697M0072 1697W0122 filter 12/7/2006 937 Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Set 18

TABLE 2 CONCENTRATIONS OF SELECTED GAMMA EMITTING RADIONUCLIDES I N WATER SAMPLES BJ GAMMA SPECTROSCOPY CP1, REVISIOF 15 INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE NRC Region I Radionuclide Concentrations Sample ID Sample I D CO-58 CO-60 cs-134 b

1697W0116 RO-543-95' -1.5 f. 2.2 0.4 f. 2.2 -0.2 f. 2.1 -1.8 f. 4.3 1697W0117 P-1217 1.2 f. 2.4 0.8 f. 2.2 -0.1 f. 2.3 -1.6 f. 2.0 1697W0118 Ft. Montgomery 1.1 L- 1.7 0.9 k 1.7 1.0 f: 1.7 2.3 k 2.5 1697W0119 RO-18 -1.0 f. 2.4 0.9 f. 2.4 -0.7 f. 2.5 0.2 k 3.1

-0.4 f. 2.1 1 1697W0121 MW-51-(011) -0.6 f. 2.7 1.1 f. 2.3 1.5 f. 2.5 -1.0 f. 4.5 1697W0122 MW-40-(010) -0.3 f. 1.7 0.3 f. 1.7 0.1 k 1.9 0.2 f. 1.8 "The range of MDCs for the selected radionuclides is 2.8 pCi/L to 4.4 pCi/L.

bUncertainties represent the 95% confidence level, based on total propagated uncertainties Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Set 18

TABLE 3 CONCENTRATIONS OF HARD TO DETECT BETA EMITTING RADIONUCLIDES I N WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK Radionuclide Concentrationsa(pCi/L)

ORISE NRC Region I Sample ID Sample I D Fe-55b Ni-63" H-3d 1697W0116 RO-543-95' 8 k 20' , 33 -5.0 k 5.5 9.7 200 k 210 , 360 169W0117 P-1217 -4 k 19 33 2.3 & 5.7 9.7 80 & 200 360 1697W0118 Ft.Montgomery 4 & 20 , 33 0.4 ? 5.6 . 9.7 50 k 200 . 360 1697W0119 I RO-18 I 1 k 19 . 33 I 1.9 k 5.7 . 9.7 1 110 k 210 . 360 11 1697W0120 1697W0121 1697W0122 I RO-543-50 MW-51-(011)

MW-40-(010)

-5 f. 19 , 33

-2 k 19 , 33 I 13 & 20 , 33 I 1.4 k 5.7 0.2 k 5.6 1.8 k 5.7 9.7 9.7 9.7 I 260 70 290 t

k 220 200 220

. 360

, 360 I

"The MDCs for each radionuclide are after the comma.

"e-55 analyzed using procedure AP13, Revision 4.

'Ni-63 analyzed using procedure AP17, Revision 0.

d11-3 analyzed using procedure AP2, Revision 15.

eUncertainties represent the 95% confidence level, based on total propagated uncertainties.

Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Set 18

TABLE 4 CONCENTRATIONS OF TECHNETIUM-99 (Tc-99)

IN WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS AP5, REVISION 16; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE NRC Region I Radionuclide Sample I D Sample I D Concentrationsa (pCi/L) 1697WOl16 RO-543-95' 5.0 t 8.3b , 14.0 1697W0117 P-1217 3.4 k 8.2 , 14.0 1697W0118 Ft. Montgomery 2.7 2 8.2 , 14.0 1697W0119 RO-18 -1.8 k 8.1 , 14.0 1697W0120 RO-543-50 6.4 t 8.3 , 14.0 1697WO 121 MW-5 1-(011) -2.7 +_ 8.1 , 14.0 1697W0122 MW-40-(010) 5.2  ? 8.3 , 14.0 Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Sct 18

TABLE 5 ORISE NRC Region I Radionuclide Concentrations, Sample ID Sample ID TPUs, and MDCS"@Ci/L) 11 1697\)(10116 I RO-543-95' I 0.29  ? 0.36b . 0.60 11 1 1697W0117 I P-1217 I -0.09 k 0.39 , 0.69 1 1697W0118 Ft. Montgomery -0.08 & 0.34 , 0.60 1697W0119 RO-18 -0.10 k 0.37 , 0.66 1697W0120 RO-543-50 0.18 k 0.39 . 0.66

.1697W0121 MW-51-(011) 0.37  ? 0.36 , 0.61 1697W0122 Mw-40-(010) 0.61 k 0.35 , 0.56 Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data 'Tables Set 18

F a TABLE 6 9

g n CONCENTRATIONS OF SELECTED ALPHA EMITTING RADIONUCLIDES IN SUSPENDED AND DISSOLVED FRACTIONS OF WATER SAMPLES AP11, REVISION 3; CP2, REVISION 12 INDIAN POINT POWER STATION BUCHANAN, NEW YORK 1697W0119 RO-18 0.11 f: 0.18 , 0.31 0.00 f 0.09 , 0.20 0.07 f: 0.17 , 0.30 0.02 k 0.08 , 0.16 1697M0069 1697W0119 filter 0.01 f 0.02 , 0.04 0.00 f 0.01 , 0.02 0.00 f: 0.02 , 0.04 0.01 k 0.01 , 0.01 1697W0120 RO-543-50 0.17 k 0.21 , 0.34 -0.02 f 0.10 , 0.23 0.06 f 0.16 , 0.30 -0.02 f 0.08 , 0.20 CD . 1697M0070 1697W0120 filter 0.02 f 0.02 , 0.04 0.00 f: 0.01 , 0.02 0.01 f 0.02 , 0.03 0.00 k 0.02 , 0.06

+

2U

--. 1697W0121 nnXr-51-(011) 0.09 f: 0.15 , 0.26 0.05 f 0.08 , 0.13 -0.05 f: 0.11 , 0.26 -0.06 k 0.10 , 0.26 2 16971110071 1697W0121 filter 0.01 f 0.02 , 0.04 0.01 f 0.01 , 0.02 0.00 f 0.02 , 0.04 -0.002 f 0.005 , 0.02 1697W0122 MW-40-(010) 0.23 f: 0.21 , 0.33 0.02 f 0.09 , 0.19 -0.02 f: 0.13 , 0.28 0.06 k 0.07 , 0.06

\

1697M0072 1697W0122 filter 0.01 k 0.02 , 0.04 0.00 f 0.01 , 0.03 0.00 f 0.02 , 0.04 -0.01 f 0.01 , 0.03 7 J

TABLE 6 (Continued)

CONCENTRATIONS OF SELECTED ALPHA EMITTING RADIONUCLIDES IN SUSPENDED AND DISSOLVED FRACTIONS O F WATER SAMPLES AP11, REVISION 3; CP2, REVISION 12 INDIAN POINT POWER STATION BUCHANAN, N E W YORK 5

N

%e MDCs are after the comma.

8 buncertainties represent the 95% confidence level, based on total propagated uncertainties.

$ 'Zero values are due to rounding.

dSignificantfigures expanded tn avoid repnrting a TPLT of 7ero at the request of the inspector U

E 2

B E

F+

W

TABLE 7 CONCENTRATIONS OF PLUTONIUM-241 I N SUSPENDED AND DISSOLVED FRACTIONS OF WATER SAMPLES BY LIQUID SCINTILUTION ANALYSIS AP10, REVISION 2; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE NRC Region I Radionuclide Concentrationsa @Ci/g of sediment in 100 mL or pCi/L for Sample ID Sample ID water) 1697W0116 RO-543-95' -13 f. 35b , 60 1697M0066 1697W0116 filter 1.6 & 4.5 , 7.6 1697W0117 I?-1217 8 k 33 , 57 1697M0067 1697W0117 filter 1.6

  • 4.5 7.7 1697W0118 Ft. Montgomery 8
  • 33 , 56 1697M0068 1697W0118 filter -2.6 f. 4.9 , 8.5 1697W0119 RO-18 3 f. 35 Y 61 1697M0069 1697W0119 filter 3.5 k 4.5 7.4 1 1697W0120 I RO-543-50 1697M0070 1697W0120 filter 1 f. 10 , 17 1697W0121 MW-51-(011) 23 & 34 , 57 1697M0071 1697W0121 filter -0.3 k 4.3 , 7.4 1697W0122 MW-40-(010) 14 & 35 60 9

1697M0072 1697WO122 filter -0.2 4.2 7.2 "The MDCs are after the comma.

'Uncertainties represent the 95% confidence level, based on total propagated uncertainties Indian Point Power Station projects/l697/Data Tables/2007-03-30 Data Tables Set 18

TABLE 8 CONCENTRATIONS OF CARBON-14 I N WATER SAMPLES BY LIQUID SCINTILLATION ANALYSIS AP9, REVISION 3; CP4, REVISION 3 INDIAN POINT POWER STATION BUCHANAN, NEW YORK ORISE NRC Region I Radionuclide Concentrations, Sample ID Sample ID TPUs, and MDCS"(pCi/L) 1697w0116 RO-543-95' 4 k 12b . 20 1697W0117 P-1217 4 t 12 Y 20 1697W0118 Ft. Montgomery 6 k 12 Y 20 1697W0119 RO-18 0" k 12 Y 20 1697W0120 RO-543-50 4 t 12 . 20 1697W0121 MW-5 1-(011) 0 k 12 Y 20 1697W0122 Mw-40-(010) 1 k 12 . 20 "MDCs are after the comma.

buncertainties represent the 95"/0 confidence level, based on total propagated uncertainties.

'Zero values are due to rounding.

Indian Point Power Station projccts/l697/Data Tables/2007-03-30 Data Tables Set 18

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