ML21335A323
| ML21335A323 | |
| Person / Time | |
|---|---|
| Site: | 07000925 |
| Issue date: | 11/11/2021 |
| From: | Jay Robinson GEL Labs |
| To: | Lux J Environmental Properties Management, Office of Nuclear Material Safety and Safeguards |
| Smith J | |
| Shared Package | |
| ML21335A315 | List: |
| References | |
| Download: ML21335A323 (24) | |
Text
=Ill ILaboratories LLc $ OO PO Box ~0712 Cha~eston. SC 29417 a member of The GEL Group IN C 2040SmgeRoad ChaMeston SC29407 P 843_556.8171 F 843-766.1178 ge l. com November 11, 2021 Mr. Jeff Lux Environmental Properties Management, LLC 615 N. Hudson Suite 200 Oklahoma City, Oklahoma 73102 Re: Uranium Daughter Activities Evaluation Work Order: 559068
Dear Mr. Lux:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the following analytical results for the sample(s) we received on October 15, 2021. This original data report has been prepared and reviewed in accordance with GELs standard operating procedures.
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies of GELs accreditations and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289.
Sincerely, Grace PM_SIGN_HERE Bodiford for Julie Robinson Project Manager Purchase Order: 176069 Chain of Custody: 2021-059 Enclosures
Table of Contents Case Narrative....................................................................................1 Chain of Custody and Supporting Documentation.........................4 Laboratory Certification....................................................................7 Radiological Analysis.........................................................................9 Case Narrative..........................................................................10 Sample Data Summary............................................................14 Quality Control Summary.......................................................19
Case Narrative Page 1 of 22 SDG: 559068
CASE NARRATIVE for Burns & McDonnell Uranium Daughter Activities Evaluation SDG:559068 November 11, 2021 Laboratory Identification:
GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary Sample receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on October 15, 2021 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt.
Items of Note There are no additional items of note concerning this SDG.
Sample Identification The laboratory received the following samples:
Laboratory ID Client ID 559068001 TMW-13 559068002 02W02 559068003 02W01 559068004 TMW-09 Case Narrative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package.
Data Package The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry.
GEL Laboratories u.c PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 www.gal.com Page 2 of 22 SDG: 559068
This data package, to the best of my knowledge, is in compliance with technical and administrative requirements.
Grace PM_SIGN_HERE Bodiford for Julie Robinson Project Manager GEL Laboratories u.c PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P843.556.8171 F 843.766.1178 www.gal.com Page 3 of 22 SDG: 559068
Chain of Custody and Supporting Documentation Page 4 of 22 SDG: 559068
Page 5 of 22 J J *1 rJl Do I CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST coc # : 2021-059 - J DJ;U(::
SHIP TO: SHIP FROM: ANALYSIS REQUESTED Company Name: GEL Laboratories LLC SDG: 559068 Address: 2040 Savage Road Environmental Properties Management ~
~
Address: Charleston, SC 29407 100 North Highway 74 0
Ol 0 Guthrie, OK 73044 0 Contact Person: Julie Robinson <( (')
- a. ...I Phone: 843-769-7393 ~ (/)
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I ATTEST THAT THE PROPER FIELD SAMPLING PROCEDURES WERE USED DURING THE
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Contact Person: Jeff Lux c-:i co COLLECTION OF THESE SAMPLES. ' ~ ro (')
- a. N SAMPLER SIGNATURE: ., Phone: 405-642-5152 ::,
- t6 SITE
- SAMPLE TYPE c-
- i (')
CIMARRON FACILITY ***-** ******* .c I- <';,'
WATER :::>
SOLID i ..,;
ID ..
SAMPLE DATE
.. TIME NO.
CONTAINER lTYPE SIZE SOIL
.. OTHER "X"IF WATER PRESERV. FILTERED
.45µ YIN
~
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- rMW-13 10/13/2021 945 1 p 2L X HNO3 y X TMW-13 10/13/2021 945 1 p 500ml X HNO3 y X 02W02 10/13/2021 1125 1 p 2L X HNO3 y X 02W02 10/13/2021 1125 1 p 500ml X HNO3 y X 02W01 10/13/2021 1450 1 p 2L X HNO3 y X 02W01 10/13/2021 1450 1 p 500ml X HNO3 y X TMW-09 10/13/2021 1550 1 p 2L X HNO3 y X
- - * * - f**-**** .....
TMW-09 10/13/2021 1550 1 p 500ml X HNO3 y X
" --- -*--**-~- -,---*
Potential Hazardous Characteristics Sample Disposal llil Non-Haz 0 RCRA 0001,2&3, or 4 0 RCRA Listed [] Radioactive 0 Unknown Ill Disposal Lab [J Return to Client 0 Holding pending further instructions PROJECT NAME: Uranium Daughter Activities Evaluation PO#: 176069 THIS SAMPLE MEETS ALL APPROPRIATE RADIOLOGICAL REQUIREMENTS: HP!NITIAL: Ric, NOTES:
TIME:
Distribution:
RELINQUISHED BY SAMPLER: DATE: TIME: RECEIVED BY : DATE n-RELINQUISHED BY
- t&{fif/ir DATE:
ft*r*tt",
lXfV\../
TIME:
-~/
~DBY:
flz,l:)l DATE:
\
TIME:
~~
Standard GEL EDD & GEL lab report in .pdf format to:
- jlux@envpm.com
- slawrence@burnsmcd.com
- jmaisler@enercon.com EQulS EDD to:
- jlux@envpm.com
- dhorne@burnsmcd.com PAGE 1 OF DOCUMENT CONTROL: DATE: 1~A~/
Rev.1
Laboratories uc:
SAMPLE RECEIPT & REVIEW .FORM Client: /~,ZtV SDG/A.R/COC/Work Order:
Received Bv: BE Date Received:
~ Circle App!ic,1hh!:
II':.
~ FedE, Grn,"d UPS Fidd Smklii C.,ci" Od<<
Carrier and Tracking Number df3.48' ?vi'::/- £41 I Q ii 51 C/64::z -s 7-s=t-Suspected Hazard lnfornmtion ~ i. *If Net Counts> IOOcpm on samples not marked "radioactive". contact the Radiation Sar1f yGroup for further investigation.
Hazard Clnss Shipped: UN#: I!
\ ff UN2910. Is the Radioactive Shipment Smvey Compliant? Yes_ No__;,
A)Shipped ns a DOT Hazardous'! I!
B) Did the client designate the samples arc to be received ns radioactive?
\ COC notation or radioactive stickers on conrniners equal client designation. JLF Maximum Net Counts Obse1vcd* (Observed Coui11s -Arca Background Counts): ~CPl\-.i) mR/1-fr C) Did the RSO clnssify the samples ns radioactiv~? \ Clnssificd us: Rad l Rad 2 Rud 3 I~
COC notation or hn1.ard labels on containers equal client designation.
D) Did the client dcsi!!Tlatc sanmles arc hazardous?
If Dor Eis yes. select Hazards below.
E) Did the RSO identifv possible hazards? I\ PCB's Flammable Foreign Soil RCRA Asbestos Beryllium Smnple Receipt Criteria ~ ~ t Comments/Qualifiers (Rc11uircd for Non-Confonni\ig Items) t-~----------------+-
1 Shipping containers received intact aml Circle Applicable: Seitls broken IJamagcd eonlaincr Leaking container Other (describe) seakd?
Chain of custody documents included
\ Circle Applicable: Client contac1ed and pro1idcd COC COC crt!'1ttt!d upon rccdpt i
2 with shipment?
Preservation Method: Wet lee lee Packs D,y ice ,Allone JO1her:
3 Samples requiring cold preservation within (0 < 6 deg. C)?* \ "all temperatures ar~ recorded in Celsius I.__..,' TEMP:
Daily check performed and passed on IR Tcmpcrutt:rc Dc\'kC Serini tl:.-"IR~2~-""?~1_ _ _ __
4 temperature gun?
v' Sccondruy Tempemlurc Device Serial It (If Applicable):
Circle Applicabfo: Si:-als broken Oanrne.ed container Leotking container 01hcr (dcscrµ.,e) 5 Sample containers intact and scaled?
Samples requiring chemical preservution
\ Somplc ID's and Contoincrs Affccled:
I 6
at proper pH? ff Prcsenution oddcrl. Lot/I:
lf*Ycs, arc Encores or Soil Kits present for solids? Yes_ No_ NA_(lfycs, tal<~ to VOi\' Freezer)
Do liquid VOA vials contain acid preservation? Yes_ No_ NA_(lf unknown.[sclcct No)
Do any samples require Volatile 7
Analysis? Arc liquid VOA vials free of headspace? Yes_ No_ NA_ I Sumplc ID's and containers :iffcctcd:
!D's and tests affccicd:
8 Samples received within hole.ling time?
\
Sumple !D's 01rCOC match ID's on !D's and containers affected:
9 bottles? \
Date & time on COC match date & time Circle Applicable: No dates on containers No times on containers COC missing inft Other (describe)
IO on bottles? \ I Number of containers rcccivcc.l match Circle Applicable: No container count on COC Oiher (describe) 11 number imlicatcc.l on COC? \
Arc sample containers identifiable as 12 GEL orovic.led by use of GEL labels?
COC form is properly signed in
'- Circle Applicable: Not relinquished Other (describe) 13 rclinquishctl/recei vet! sections?
Comments (Use Continuation f'orm if needed):
l I "
PM (or PM Al review: Initials !'- IICJ,2- Date I 01'u IO Iii 'G l Page _J of _J_
Page 6 of 22 SDG: 559068 GL-CHL-SR-001 Rev 7
Laboratory Certification Page 7 of 22 SDG: 559068
List of current GEL Certifications as of 11 November 2021 State Certification Alabama 42200 Alaska 17018 Alaska Drinking Water SC00012 Arkansas 880651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH0169 DoD ELAP/ ISO17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P3301500283, P3301500253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana CSC01 Kansas NELAP E10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (AI33904)
Maine 2019020 Maryland 270 Massachusetts MSC012 Massachusetts PFAS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NEOS2613 Nevada SC0001220211 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R158 Oklahoma 2019165 Pennsylvania NELAP 6800485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 Texas NELAP T1047042352119 Utah NELAP SC00012202136 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 8 of 22 SDG: 559068
Radiological Analysis Page 9 of 22 SDG: 559068
Case Narrative Page 10 of 22 SDG: 559068
Radiochemistry Technical Case Narrative Burns & McDonnell SDG #: 559068 Product: Alphaspec U, Liquid Analytical Method: DOE EML HASL-300, U-02-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 28 Analytical Batch: 2191040 The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 559068001 TMW-13 559068002 02W02 559068003 02W01 559068004 TMW-09 1204943045 Method Blank (MB) 1204943046 559068001(TMW-13) Sample Duplicate (DUP) 1204943047 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
Product: Gammaspec, Gamma, Liquid Analytical Method: EPA 901.1 Analytical Procedure: GL-RAD-A-013 REV# 27 Analytical Batch: 2186917 The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID# Client Sample Identification 559068001 TMW-13 559068002 02W02 559068003 02W01 559068004 TMW-09 1204934355 Method Blank (MB) 1204934356 559068001(TMW-13) Sample Duplicate (DUP) 1204934357 Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on an "as received" basis.
Page 11 of 22 SDG: 559068
Data Summary:
There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable.
Qualifier Information Client Qualifier Reason Analyte Sample Sample Results are considered a false positive due to UI Thorium-234 559068004 TMW-09 high peak-width.
Results are considered a false positive due to UI Thorium-231 559068001 TMW-13 interference.
Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 12 of 22 SDG: 559068
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Qualifier Definition Report for CMRN001 Burns & McDonnell Client SDG: 559068 GEL Work Order: 559068 The Qualifiers in this report are defined as follows:
- A quality control analyte recovery is outside of specified acceptance criteria
UI Gamma Spectroscopy--Uncertain identification Review/Validation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package.
The following data validator verified the information presented in this data report:
Signature: ~~c Name: Theresa Austin Date: 11 NOV 2021
Title:
Group Leader Page 13 of 22 SDG: 559068
Sample Data Summary Page 14 of 22 SDG: 559068
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Environmental Properties Address : Management, LLC 615 N. Hudson Suite 200 Oklahoma City, Oklahoma 73102 Report Date: November 11, 2021
Contact:
Mr. Jeff Lux Project: Uranium Daughter Activities Evaluation Client Sample ID: TMW-13 Project: CMRN00620 Sample ID: 559068001 Client ID: CMRN001 Matrix: Water Collect Date: 13-OCT-21 Receive Date: 15-OCT-21 Collector: Client Parameter Qualifier Result Uncertainty MDC TPU RL Units PF DF Analyst Date Time Batch Mtd.
Rad Alpha Spec Analysis Alphaspec U, Liquid "As Received" Uranium-233/234 602 +/-21.8 1.84 +/-130 1.00 pCi/L BV1 11/10/21 1131 2191040 1 Uranium-235/236 38.4 +/-6.14 1.21 +/-10.2 1.00 pCi/L Uranium-238 364 +/-16.9 1.51 +/-79.3 1.00 pCi/L Rad Gamma Spec Analysis Gammaspec, Gamma, Liquid "As Received" Protactinium-234 U 24.4 +/-30.3 71.2 +/-42.6 pCi/L MXR1 10/25/21 0845 2186917 2 Thorium-231 UI 0.000 +/-108 107 +/-110 pCi/L Thorium-234 U 80.3 +/-311 585 +/-314 pCi/L The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, U-02-RC Modified 2 EPA 901.1 Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Uranium-232 Tracer Alphaspec U, Liquid "As Received" 2191040 30.1 (15%-125%)
Notes:
The MDC is a sample specific MDC.
TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Mtd.: Method DL: Detection Limit PF: Prep Factor Lc/LC: Critical Level RL: Reporting Limit MDA: Minimum Detectable Activity TPU: Total Propagated Uncertainty MDC: Minimum Detectable Concentration Page 15 of 22 SDG: 559068
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Environmental Properties Address : Management, LLC 615 N. Hudson Suite 200 Oklahoma City, Oklahoma 73102 Report Date: November 11, 2021
Contact:
Mr. Jeff Lux Project: Uranium Daughter Activities Evaluation Client Sample ID: 02W02 Project: CMRN00620 Sample ID: 559068002 Client ID: CMRN001 Matrix: Water Collect Date: 13-OCT-21 Receive Date: 15-OCT-21 Collector: Client Parameter Qualifier Result Uncertainty MDC TPU RL Units PF DF Analyst Date Time Batch Mtd.
Rad Alpha Spec Analysis Alphaspec U, Liquid "As Received" Uranium-233/234 418 +/-17.5 2.12 +/-88.9 1.00 pCi/L BV1 11/10/21 1131 2191040 1 Uranium-235/236 38.2 +/-5.91 1.13 +/-9.93 1.00 pCi/L Uranium-238 309 +/-15.1 1.71 +/-66.1 1.00 pCi/L Rad Gamma Spec Analysis Gammaspec, Gamma, Liquid "As Received" Protactinium-234 U -14.5 +/-26.3 49.0 +/-31.8 pCi/L MXR1 10/25/21 0845 2186917 2 Thorium-231 U 2.05 +/-77.5 128 +/-77.5 pCi/L Thorium-234 U -247 +/-321 577 +/-344 pCi/L The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, U-02-RC Modified 2 EPA 901.1 Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Uranium-232 Tracer Alphaspec U, Liquid "As Received" 2191040 30.7 (15%-125%)
Notes:
The MDC is a sample specific MDC.
TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Mtd.: Method DL: Detection Limit PF: Prep Factor Lc/LC: Critical Level RL: Reporting Limit MDA: Minimum Detectable Activity TPU: Total Propagated Uncertainty MDC: Minimum Detectable Concentration Page 16 of 22 SDG: 559068
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Environmental Properties Address : Management, LLC 615 N. Hudson Suite 200 Oklahoma City, Oklahoma 73102 Report Date: November 11, 2021
Contact:
Mr. Jeff Lux Project: Uranium Daughter Activities Evaluation Client Sample ID: 02W01 Project: CMRN00620 Sample ID: 559068003 Client ID: CMRN001 Matrix: Water Collect Date: 13-OCT-21 Receive Date: 15-OCT-21 Collector: Client Parameter Qualifier Result Uncertainty MDC TPU RL Units PF DF Analyst Date Time Batch Mtd.
Rad Alpha Spec Analysis Alphaspec U, Liquid "As Received" Uranium-233/234 1040 +/-35.3 3.22 +/-281 1.00 pCi/L BV1 11/10/21 1356 2191040 1 Uranium-235/236 74.2 +/-10.5 1.15 +/-22.4 1.00 pCi/L Uranium-238 604 +/-26.9 2.05 +/-164 1.00 pCi/L Rad Gamma Spec Analysis Gammaspec, Gamma, Liquid "As Received" Protactinium-234 U 3.89 +/-38.5 79.2 +/-38.8 pCi/L MXR1 10/25/21 0846 2186917 2 Thorium-231 U 77.6 +/-145 109 +/-145 pCi/L Thorium-234 U -222 +/-322 559 +/-342 pCi/L The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, U-02-RC Modified 2 EPA 901.1 Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Uranium-232 Tracer Alphaspec U, Liquid "As Received" 2191040 18.4 (15%-125%)
Notes:
The MDC is a sample specific MDC.
TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Mtd.: Method DL: Detection Limit PF: Prep Factor Lc/LC: Critical Level RL: Reporting Limit MDA: Minimum Detectable Activity TPU: Total Propagated Uncertainty MDC: Minimum Detectable Concentration Page 17 of 22 SDG: 559068
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Environmental Properties Address : Management, LLC 615 N. Hudson Suite 200 Oklahoma City, Oklahoma 73102 Report Date: November 11, 2021
Contact:
Mr. Jeff Lux Project: Uranium Daughter Activities Evaluation Client Sample ID: TMW-09 Project: CMRN00620 Sample ID: 559068004 Client ID: CMRN001 Matrix: Water Collect Date: 13-OCT-21 Receive Date: 15-OCT-21 Collector: Client Parameter Qualifier Result Uncertainty MDC TPU RL Units PF DF Analyst Date Time Batch Mtd.
Rad Alpha Spec Analysis Alphaspec U, Liquid "As Received" Uranium-233/234 950 +/-29.3 1.97 +/-216 1.00 pCi/L BV1 11/10/21 1356 2191040 1 Uranium-235/236 58.0 +/-8.08 1.61 +/-15.4 1.00 pCi/L Uranium-238 660 +/-24.4 1.74 +/-151 1.00 pCi/L Rad Gamma Spec Analysis Gammaspec, Gamma, Liquid "As Received" Protactinium-234 U -13.4 +/-47.6 84.7 +/-50.4 pCi/L MXR1 10/25/21 0854 2186917 2 Thorium-231 U -8.39 +/-95.9 165 +/-95.9 pCi/L Thorium-234 UI 0.000 +/-815 530 +/-843 pCi/L The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, U-02-RC Modified 2 EPA 901.1 Surrogate/Tracer Recovery Test Batch ID Recovery% Acceptable Limits Uranium-232 Tracer Alphaspec U, Liquid "As Received" 2191040 26.7 (15%-125%)
Notes:
The MDC is a sample specific MDC.
TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
Column headers are defined as follows:
DF: Dilution Factor Mtd.: Method DL: Detection Limit PF: Prep Factor Lc/LC: Critical Level RL: Reporting Limit MDA: Minimum Detectable Activity TPU: Total Propagated Uncertainty MDC: Minimum Detectable Concentration Page 18 of 22 SDG: 559068
Quality Control Summary Page 19 of 22 SDG: 559068
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: November 11, 2021 Client : Environmental Properties Management, LLC Page 1 of 3 615 N. Hudson Suite 200 Oklahoma City, Oklahoma
Contact:
Mr. Jeff Lux Workorder: 559068 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 2191040 QC1204943046 559068001 DUP Uranium-233/234 602 553 pCi/L 8.45 (0%-20%) BV1 11/10/21 13:56 Uncert: +/-21.8 +/-20.2 TPU: +/-130 +/-120 Uranium-235/236 38.4 32.7 pCi/L 16.2 (0%-20%)
Uncert: +/-6.14 +/-5.48 TPU: +/-10.2 +/-8.88 Uranium-238 364 339 pCi/L 7.03 (0%-20%)
Uncert: +/-16.9 +/-15.8 TPU: +/-79.3 +/-74.3 QC1204943047 LCS Uranium-233/234 26.0 pCi/L BV1 11/10/21 13:56 Uncert: +/-2.57 TPU: +/-4.32 Uranium-235/236 1.39 pCi/L Uncert: +/-0.692 TPU: +/-0.716 Uranium-238 27.1 28.4 pCi/L 105 (75%-125%)
Uncert: +/-2.67 TPU: +/-4.63 QC1204943045 MB Uranium-233/234 U -0.0464 pCi/L BV1 11/10/21 13:56 Uncert: +/-0.258 TPU: +/-0.258 Uranium-235/236 U 0.0245 pCi/L Uncert: +/-0.256 TPU: +/-0.256 Uranium-238 U 0.252 pCi/L Uncert: +/-0.351 TPU: +/-0.353 Rad Gamma Spec Batch 2186917 QC1204934356 559068001 DUP Protactinium-234 U 24.4 U -41.4 pCi/L 0 N/A MXR1 10/25/21 11:07 Uncert: +/-30.3 +/-45.0 TPU: +/-42.6 +/-68.1 Thorium-231 UI 0.000 U 43.4 pCi/L 0 N/A Uncert: +/-108 +/-106 TPU: +/-110 +/-106 Thorium-234 U 80.3 U 241 pCi/L 0 N/A Uncert: +/-311 +/-430 TPU: +/-434 Page 20 of 22 SDG: 559068
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 559068 Page 2 of 3 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 2186917
+/-314 QC1204934357 LCS Americium-241 1.09E+05 1.18E+05 pCi/L 109 (75%-125%) MXR1 10/25/21 09:15 Uncert: +/-2070 TPU: +/-11100 Cesium-137 37800 39900 pCi/L 105 (75%-125%)
Uncert: +/-676 TPU: +/-3450 Cobalt-60 21400 22700 pCi/L 106 (75%-125%)
Uncert: +/-614 TPU: +/-2140 Protactinium-234 U 70.5 pCi/L Uncert: +/-1200 TPU: +/-1210 Thorium-231 U 93.4 pCi/L Uncert: +/-990 TPU: +/-991 Thorium-234 U -1060 pCi/L Uncert: +/-2650 TPU: +/-2700 QC1204934355 MB Protactinium-234 U 3.80 pCi/L MXR1 10/25/21 08:46 Uncert: +/-41.5 TPU: +/-41.7 Thorium-231 U 19.8 pCi/L Uncert: +/-45.4 TPU: +/-46.3 Thorium-234 U -185 pCi/L Uncert: +/-219 TPU: +/-238 Notes:
TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).
The Qualifiers in this report are defined as follows:
- Analyte is a Tracer compound
< Result is less than value reported
> Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.
H Analytical holding time was exceeded J See case narrative for an explanation J Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
Page 21 of 22 SDG: 559068
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 559068 Page 3 of 3 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time M M if above MDC and less than LLD M REMP Result > MDC/CL and < RDL N/A RPD or %Recovery limits do not apply.
N1 See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
UI Gamma Spectroscopy--Uncertain identification UJ Gamma Spectroscopy--Uncertain identification UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y Other specific qualifiers were required to properly define the results. Consult case narrative.
^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable.
- Indicates analyte is a surrogate/tracer compound.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
Page 22 of 22 SDG: 559068