ML20126H646

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Rev 12 to Procedure 1-18-4, Spent Resin Storage & Processing
ML20126H646
Person / Time
Site: Maine Yankee
Issue date: 05/10/1985
From:
Maine Yankee
To:
Shared Package
ML20126H622 List:
References
1-18-4, NUDOCS 8506100377
Download: ML20126H646 (15)


Text

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' COMPLETED: Dept. Head h 3g Proc. No.1-18-4 Plt. Mgr. f ud . Class. A DATE/ TIME PORC g a .- - Rev. No. 12 74 Mgr. of Ops /.EF Issue Date 5-10-84 U' P.S.S.' REVIEW Review Date 5/86 l-18-4 SPENT RESIN STORAGE AND PROCESSING W NtFonssA m N T s...

DISCUSSION  %. r.. . , , ,, .__

This procedure provides the operator with specific steps required to store,'

condition.and solidify Spent Resins.

R 4.0 Spent Resin Conditioning in the Waste Resin Storage Tank TK 85 & Resin itidup Tk-lO9 4.1 Spent Resin Conditioning in TK-85 and Water Transfer to TK-109 4.2 Resin & Water Transfer from TK-85 to TK-109 4.3 Dewatering Resin Holdup TK-109 4.4 Resin Transfer from TK-85 to Liner 4.5 Transfer' of Resin from TK-109 to Liner 6- 1.0 OBJECTIVE

-To store, condition and prepare Spent Resins for processing.

i To pr'ocess Spent Resins to achieve a free standing solid in a suitable shipping p container.

2.0 PRECAUTIONS j 2.1 Always observe the radiation reading in mr/hr on the panel prior to entrance 1 to the Waste Holoup Tank Cubicle. Personnel should have a radiation survey meter when entering this cubicle.

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l 2.2 Be aware of high radiation levels in waste resin storage area, RCA, and waste

". holdup tank during these opirations.

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( 2.3 Ensure there is room in the ADT's to receive water when dewatering TK-lO9 to the ADT's.

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2.4 .When operating the dewatering pump, ensure oiler in air supply is full.

- 3.0 INITIAL CONDITIONS INITIALS 3.1 Ensure that the RCA Storage Building Ventilation System is in

. operation.

3.2 ' Proper plastic, paper or canvas has been applied to the RCA Building floor or Decon Pad to assure that the truck trailer or container is not contaminated.

3.3 A Radiation Work Permit has oeen obtaineo for all phases of solidification / Resin Transfer.

3.4. Spent Resin has been sluiced to the Waste Resin Storage Tank for storage and decay.

3.5' Fill out batch report attached and return to HP. Ensure PEQAG nas r checked liner for. free standing water prior to covering up. liner.

h- - 3.6. Ensure all outside doors to the RCA are closed when_ waste is being processed.

3.7 Have the Chemistry Dept. sample the waste holdup tank bottoms.

NOTE: Chemistry must have activity levels for cask shipping '

' records.

' . 3.8 . To prevent rupturing FL-90 when starting the dewatering pump, (P-145) ensure it has a discharge path, and air regulator is set at 15 psi i ~or less.

}' -3.9 Obtain or manufacture a rig for determining water content in cask via 1 cewatering pump (P-123) discharge.

4 3.10 Vendors procedure available for use.

J 3.11' Flexible hose is connected to WSS-91 and WSS-72 for resin fill and 1

( dewatering.

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Rev. No. 12 Page 3 of 15 INITIALS

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3.12 Assure that the Waste Solidification System Flush Tank, TK-80, level

.within the operating bano as inoicated by the Level Gage Glass.

Keep water level in the RED ZOE.

3.13 Assure that the Waste Solidification System Flush Tank, TK-80 is

. pressurized to 85-100 psig and is open to the Service Air System.

3.13.1 I'f makeup to TK-80 is necessary, open PW-17 to admit primary water and maintain TK-80 pressure at 100 psig by throttling the muffled vent, SA-206. .

3.14 Assure that the main Flush Water Isolation Valve, WSS-65 is open.

NOTE: This valve should De left open.

3.15 Assure that the main Instrument Air Isolation Valve, IA-201, is open.

-NOTE: This valve is located behind the RCA Storage Building Condensate Return Unit.

R 3'.16 Ensure P-108 suction aligned to TK-85.

NOTE: RS-14 is located in a High Radiation, Airborne Acitivity Area and does not have a reach rod. This valve is visible from above and should be checked in this manner.

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Proc. No.1-18-4 Rev. No. 12

. Page 4 of 15

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4.0 . SPENT RESIN CONDITIONING IN THE WASTE RESIN STORAGE TANK / RESIN HOLOUP TANK DISCUSSION This section gives two methods of transferring and processing resin. The old method of transfer to the radwaste holdup tank (TK-85) allows no means of returning the cecant back to the ADT's. The new method allows transfer of water and resin to the resin holdup tank (TK-109) from TX-85. The resin may then be transferred to TK-95 for. solidification or directly to a liner. The water may-be pumped to the ADT's or TK-85.

The maximum capacity of TK-85 is 100 ft3 of resin or three charges. This assures that the resin level is below the 3 inch sluice line. Normally, processing of resin should be considered when two charges have been stored in

- TK-85 for at least 90 days and longer if possible.

The maximum capacity of TK-109 is 704 ft3 of resin or 22 charges. Charts at rear of this procedure and at TK-109 correlate tank level with number of charges and gallons of water to tank level.

NOTE: Prior to transferring spent resin to the Spent Resin Storage Tank'(TK-85), the water level in the Spent Resin Storage Tank

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must be reduced to achieve a pumpable slurry. This will be accomplished by recircing the spent resin bed for 30 minutes with C"- the SCREEN PLUG CLOSED, After this operation, the excess water-will be pumped to TK-109. After this operation has been accomplished, the spent resin is ready for transfer to the Waste Solidification System.

INITIALS 4.1 Spent Resin 00nditioning in TK-85 and Water Transfer to TK-109. .

4.1.1 Assure that the Resin Storage. Tank SCREEN PLUG IS CLOSED.

4.1.2 Place the MODE SELECTOR SWITCH in 'RESINS.

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  • Proc..No. 1-18-4 Rev. No. 12

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INITIALS 4.1.3 - Place the PHASE SELECTOR on FILL HOPPER.

4.1.4 Close the RESIN INLET VALVE, WSS-A-28.

4.1.5 .Open the Resir! Transfer pump Recirc. Valve, RS-15.

R 4.1.6 Cneck shut RS-27 Hope Connection. ,

R 4.1.7_ Close WSS-89 Resin Transfer to TK 95 manual stop and WSS-92 P-144 Resin Transfer to TK 85/TK 95.

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NOTE: With WSS-89 closed, we will be filling TK-109, not the hopper.

-4.1.8 Hook up the air hose, to the air supply connection to TK-85.

Fully open the air valve at the tank and then crack open 1/2 turn the air supply root valve to allow air to be injected into the tank for agitation of resin.

CAUTION: 'The root valve at the air supply line should just be cracked to prevent blowing resin out of the tank.

CAUTION: If level in TK-85 reaches 100%, secure air to TK-85.

Restore minimal air flow after TK-85 level has decreased and stabilized.-

4.1.9 Start the Resin Transfer Pump, P-108.

4.1.10 ' Run in tnis mode for 30 minutes, or until radiation levels stacilize.

. NOTE: The resin bed above the screen will purify the recirc.

stream and capture any resin beads below tne screen.

4.1.11 Open WSS-90, TK-109 inlet. ,

b 4.1.12 Transfer excess water to TK-109 by opening tne RESINS INLET VALVE, WSS-A-28 and closing recirc. valve RS-15.

4.1.13 Ccntinue decant transfer until Waste Resin Storage Tank level decreases to 35%.

CAUTION: At levels less than 35%, resin clogging of P-108 ,

may occur.

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Proc. No. 1-18-4, Rev. No. 12 Page 6 of 15 1

INITIALS 4.1.14 Stop resin transfer pump P-108.

R 4.1.15 Close WSS-A-28 TK-85 Resin Inlet.

4.1.16 .Open recire. valve RS-15.

4.1.17 Close WSS-90 TK 109 Inlet. .

R 4.1.18 Open WSS-89 Resin Transfert at TK 95 manual stop.

4.1.19 Place the Phase Selector on Recirc.

4.1.20 Refer to Section 5.3 to return oecant to ADT's.

AUX. OPERATOR DATE/ TIME 4.2 Resin and Water Transfer from TK-85 to TK-lO9 -

4.2.1 Check open the resin transfer pump (P-108) suction valve, RS-14.

4.2.2 Open recirc. valve RS-15. -

4.2.3 ' Hook up the air hose to the air supply connection to TK-85.

Fully open.the air. valve at the tank and then' crack open .

1/2 turn the air supply root valve to allow air to be injected for agitation.

CAUTION: The root valve should just= be_ cracked to prevent blowing resin out of the tank.

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CAUTION: If TK-85 level reaches 100%, secure air to TK-85.J Restore minimal air flow after TK-85 level has l decreased and stabilized.

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4.2.4 Start the resin transfer ptnp, P-108.

[ 4.2.5 After 15 minute recirc. stop P-108 and close RS-15.

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4. 2.6 _ Open the spent resin storage tank screen plug.

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R -- 4.2.7 Close WSS-69 Resin Transfer to TK 95 man stop ar.d close WSS-92 '

P-144 Resin Transfer to TK 85/TK 95.

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e I4. 2. 8 ' Place the MODE SELECTOR ON RESINS.

4.2.9 = Place tne SELECTOR ON FILL HOPPER.

i NOTE: With WSS-89 closed we will be~ filling TK-109, not the hopper.

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- 4.2.'10 J Open WSS-90, inlet .to TK-109.

- 4.2.11 l Open WSS-A-28.

4.2.12 Start transfer of spent -resin to TK-109 by starting the waste

. resin transfer. pump, P-108.

' 4.2.13 Continue resin transfer until the hign level alarm is reached in TK-109.

4.2.14 Stop P-108.

4.'2.15 Dewater TK-109 'as 'per Step 6.3.

- NOTEi If all resin has been transferred to TK-109, do not

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dewater as this water will act as shielding.

4.2.16 Transfer remaining resin and water to~ TK-109 by, starting- P-108.

4.2.17 If hign' level is not reached before all resin is transferred fill TX-109 witn primary water by' closing WSS-102 and WSS-98

.c and opening WSS-102 if shielding is needed. Reference TK-109, -

P Volume Curve attached.

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NOTE:- Do not use more water than needed for shielding.

Bi; NOTE: : There is no automatic protection against overfilling 0;

with water. . .

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p 4.2.18 Stop P-108 and close WSS-A-28 when transfer is complete. ,

v 4.2.19 'Close RS-15 and WSS-90. -

4 4.2.20 Place phase selector in recire.

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  • INITIALS

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R'4.3 Dewatering Resin Holdup Tank, TK-109 to ADT or WHT 4.3.1 Ensure there is room in ADT's-to accept decant.

--~. R .. 4.3.2- Close WSS-98 P-145 Bypass.

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~4.3.3' ~Open WSS-97 FL-89 Inlet. ,

R 4.3.4 Open WSS-99 P-145 Outlet.

R 4.3.5 Open WSS-100 FL-90 IQtlet. ,

-R 4.3.6 Open WSS-101 FL-90 Outlet.

R- 4'.3.7 To send decant to WHT open RS-20. RS-20 Open

- To send decant to ADT open RS-21. RS-21 Open

'4.3.8 Close vent WSS-103 (in pipe just above WSS-101).

R 4.3.9 Close WSS 102 nose c6nnection.

4.~3.10 - Using 15 psi or less start dewatering pump P-145.

CAUTION: Do not use greater than 15 psi or FL-90 could rupture - adjust as necessary after start.

CAUTION: When' operating P-145, ensure air line oiler is full.

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4.3.11 When dewatering 'is complete stop P-145.

4.3.12 Close WSS-97, 99,.100, and 101.

4.3.13 Close RS-21 and 20 as opened above.

AUX. OPERATOR 0 ATE / TIME

.4;4. RESIN TRANSFER FROM TK-85 TO LINER DISCUSSION

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During this evolution, the discharge of the dewatering pump is directed back J'-~ c to TK-85. A level increase in TK-85 should be noted soon after cask b S? dewatering is started. Resin transfer should be considered complete when f E- ~ radiation levels on the liner fill line drop significantly.,.

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l Proc. No.1-18-4 Rev. No. 12 Page 9 of 15 INITIALS 4.4.1- Perform the following valve line ups.

'4.4.1.1. TK-85 cubicle.

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NOTE: RS-14 is located in a High Radiation, Aircorne P '

Activity Area and does not have a reach rod. j This valve is visible from above and should be I checked in this manner.

l k:- a). .. RS-14', P-108 suction . Check open b) RS-15, TK-108 recirc Open c) TK-85, screen plug valve Open

p. d)' TK-85 air sparger supply valve Open e) ' WSS-67 P-123 air supply

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.Open f) WSS-68 P-123 air supply Open

. g) .WSS-34 P-123 suction Closed I

!. R 4.4.1.2 Waste Solidification Panel-(; a) WSS-A-28 Resin Inlet to TK 85. Closed l l-.

b) WSS-A-35 TK-85 suction of P 123. Closed l q

4.4.1.3 TK-109 Cubicle L a) - WSS-93, ik-109 recirc Closed t-b) WSS-94, P-144 discharge Closed c) WSS-91, liner fill stop Closed I d) WSS-92, P-108 discharge Open  !

e) WSS-95, TK-109 H.C. Closed 4.4.2 Hookup flexible hose from WSS-91 to connection at Liner IAW ,

b Vendor instructions, r

4.4.3 Hook up dewatering hose IAW Vendor instructions.

4.4.4 Check Service Air supply to TK-85 sparger closed, then hook up air hose to service air supply valve.

l 4.4.5 Start P-108 to recirc TK-85 for at least 15 minutes.

4.4.6 Crack open the Service Air supply valve to agitate resin, open no more tnan 1/2 turn to prevent blowing resin out of tank.

CAUTION: If level in TK-85 reaches 100%, secure air to TK-85. Restore minimal air flew after TK-85 level ~

has decreased and stabilizeo.

NOTE: If P-108 should clog with resin, secure P-108, shut .

RS-14 connect hose from flush water upstream of RS-27, f ./. <

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and flusn system thru P-108 to liner by opening RS-27. ,

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INITIALS-4'.4.7 ' When recirc is complete, open WSS-91 and close RS-IS to transfer resin to liner.

CAUTION: Radiation levels _ at'the top of the cask may reach as hign as 25 rem /hr. Use a temporary mirror at the top of the cask to visually ~ determine level.

-4.4.8- Open liner dewatering hose isolation WSS-72.

4.4.9 Start the dewatering pump'(P-123) when liner level reaches 2.5" r' _ from fill heao. Adjust pump speed to maintain a slowly decreasing level. Ensure WSS-A-44 opens. Note level increase in TK-85.

NOTE: When operating P-123 ensure air line oiler is full.

4.4.10 When resin transfer is complete, perform the following:

4.4.10.1 -Stop P-108.

4.4.10.2 Shut WSS-91.

_4'.4.10.3 Shut the Service Air supply valve to TK-85.

-4.4.11 Cbntinue oewatering Liner IAW Vendor instructions.

NOTE: To measure the amount of water in cask, hook up a temporary leak rig to discharge of P-123 and run P-123 in accordance with vendors ~proceedure.

b 4.4.12 Stop dewatering pump when liner is dewatered and disconnect hose IAW Vendors instructions.

L 4.4.13 Drain hose into liner.

4.4.14 Place hose in yellow poly bag and return to its storage area.

j 4.4.15 Perform the following valve line ups: -

P' 4.4.15.1 TK-85 cubicle.

a) RS-15, TK-85 recirc Closed b) TK-85 screen plug valve Closed c) TK-85 air sparger supply valve Closed 4.4.15.2' Waste Solidification Panel.

a) WSS-A-28 Auto

[ b) WSS-A-35 Auto

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Rev. No. 12 Page 11 of 15 PCR No.84-520, 84-521-84-522 INITIALS 4.4.15.3 On wall near WSS-91.

-a) WSS-92 Clocec

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. 4. 4.- 16 Fill out attached data sheet and forvtard to Chemistry /HP.

AUX. OPERATOR DATE/TDE 4.5 Transfer of Resin from TK-109 to ' Liner CAUTION: Ensure there is enough room in TK-85 to receive decant from liner prior to commencing the following steps.

4.5.1 Hook flexible hose from WSS-91 to connection at liner.

^PCR #84-520 4.5.2 Install two stand' pipes and level electrodes - Hittman liner as

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per Westinghouse - H1Hnan Procedure STD P-03-010 Rev. 5, Section 5, equipment set up.

[ 4.5.3~ Connect air hose to WSS-102 for resin agitation.

PCR #84-521

.4.5.4 Open WSS-96 P-144 suction from TK-109 and check closed WSS-90

[ ;, and WSS-92.

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-4.5.5 Open WSS-94'P-144 discharge.

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  1. R 4.5.6 Open WSS-93 P-144 discharge' to TK 109.

R. 4.5.7 Close WSS-91 flexible hose connection.

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"i 4.5.8 . Start P-144 from solidification control panel and open WSS-102

.1 and air' supply to reirc. and agitate resin for 15 minutes.

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'4.5.9 When recirc. is conplete open WSS-91 and close WSS-93 to .

.j . transfer resin to liner, following Hittman Procedure STD-P-03-010

4. Rev. 5, Section 6.0, transfer and dewatering.

.f j- / CAUTION: Radiation levels at top of the cask may reach as high

.i as 25 rem /hr.' use a temporary mirror at the top of

[- the cask to visually determine level.

I ' 4.5.10 ' Place the control switch for WSS-A-35 in the closed position. j 5- ,

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INITIALS-

.. 4.5.11 0 pen liner dewatering hose isol. valve WSS-72.

4.5.12 Verify that the dewatering pump air supply isol. valves, WSS-67 and WSS-68 are open.

PCR #84-523 4.5.13 Start the dewatering pump (P-123) and follow Hittman Procedure STD-P-03-010 Rev. 5, Section 6.0, transfer and dewatering.

NOTE: When operating P-123 ensure air line oiler is full.

4.5.14 When resin transfer is complete perform the following:

4.5.14.1 Stop P-144.

4.5.14.2 Close WSS-96.

4.5.14.3 Connect primary water hose to WSS-95, then open WSS-95 ano start P-144.

4.5.14.4 After clear flush water issues from hose open WSS-93, h.) close WSS-91 and flush recirc. line for 1 minutes.

4.5.14.5 Stop P-144.

4.5.14.6 Close WSS-96.

4.5.14.7 Close WSS-95.

4.5.14.8 Close WSS-93.

4.5.14.9 Close WSS-94.

4.5.14.10 Shut WSS-102 and air supply to secure agitation.

PCR #84-524 4.5.15 Stop dewatering pump following Hittman Procedure.STD-P-03-010, Section 6, transfer and dewatering. -

NOTE: Well point will be left in the liner to be shipoed off site with the resin.

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NOTE: To measure the amcunt of water in cask, hook up temporary rig to discharge of P-123 and run P-123 in 7 accordance with vendors procedure. .

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4.5.16 Drain hoses into liner.

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1 4.5.17 Place yellow poly bag around hose and return to its storage area.

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g-: INITIALS

4.5.18 - - Ensure resin liner is dewatered prior to capping.

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p gi  : 4.5.19 . Fill out attached data sheet and forward to Chem /lf. -

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u 1-18-4 ' WASTE SOLIDIFICATION DATA SHEET ,

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(HP) CONTAIER SERIAL #

.(OPS) WASTE TYPE: EV-1, EV-2, Resin Decant, Resin, Primary Water, Other (Circle One) i: -. .

(CEM) WASTE pH 1(OPS) ~ WASTE TRANSFER START TIME

.(OPS) WASTE TRANSFER CO W LETION TIME

.(OPS) . TOTAL- WASTE TRANSFERRED-

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