ML063400438

Final Status Survey Final Report Phase IV, Appendix A5, Survey Unit Release Record 9106-0005, Discharge Canal

ML063400438
Person / Time
Site:	Haddam Neck File:Connecticut Yankee Atomic Power Co icon.png
Issue date:	11/13/2006
From:	Newson C Connecticut Yankee Atomic Power Co
To:	NRC/FSME
References
9106-0005
Download: ML063400438 (299)

Text

Final Status Survey Final Report Phase IV Appendix A5 Survey Unit Release Record 9106-0005, Discharge Canal November 2006

CYAPCO FINAL STATUS SURVEY RELEASE RECORD DISCHARGE CANAL SURVEY UNIT 9106-0005 Prepared By: Date: #( - /Q -Oa FSS Engineer Reviewed By: Date: ' /

FSS eiineer Approved By:________________ Date: _///_:/O Technical Support Manager Revision 0

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD TABLE OF CONTENTS

1. SURVEY UNIT DESCRIPTION ................................................................. 3

2. CLASSIFICATION BASIS ........................................................................ 3

3. DATA QUALITY OBJECTIVES (DQO) .................................................... 5

4. SURVEY DESIG N..................................................................................... 8

5. SURVEY IMPLEMENTATION ................................................................ 11

6. SURVEY RESULTS ............................................................................... 12

7. QUALITY CONTROL ............................................................................. 14

8. INVESTIGATIONS AND RESULTS ...................................................... 14

9. REMEDIATION AND RESULTS ............................................................. 15

10. CHANGES FROM THE FINAL STATUS SURVEY PLAN ..................... 15

11. DATA QUALITY ASSESSMENT (DQA) ................................................. 15

12. A NO MA LIES ........................................................................................... 16

13. CO NCLUSIO N ....................................................................................... 16

14. ATTACHM ENTS .......................................................................... ........... 17 14.1 Attachment 1 - Figures (10 pages including cover) 14.2 Attachment 2 - Sample and Statistical Data (271 pages including covers)

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD SURVEY UNIT DESCRIPTION Survey Unit 9106-0005 (Discharge Canal) is designated as Final Status Survey (FSS) Class 2 and consists of approximately 9,632 m2 (2.38 acres) of water covered sediment in an area located approximately 0.55 miles from the reference coordinate system benchmark used at the Haddam Neck Plant (HNP)

(see Attachment 1, Figure 1). The Discharge Canal is a man-made mile long waterway that runs parallel to, and ultimately communicates with the Connecticut River. The Discharge Canal is subdivided into fifteen (15) survey units including two (2) permanent wetland areas for FSS purposes. The survey unit is bounded as follows: Discharge Canal Survey Unit 9106-0004 is to the north (called north as orientated with the north to south flow of the Connecticut River), Survey Area 9528 is to the east, Discharge Canal Survey Unit 9106-0006 is to the south and Survey Area 9530 is to the west. The survey unit comprises the canal sediments to the depth of three (3) feet from the top of the sediment layer or the original construction depth and it extends up the canal banks to the mean high water level.

This survey unit is bounded by reference coordinates EO 17 through E023 and by S100 through S115 (refer to License Termination Plan Section 5.4.4). The reference coordinates provide the maximum dimensions of a rectangle containing this survey unit. Some areas contained in this rectangle may not be part of this survey unit. The boundary of the survey unit was defined using a Global Positioning System (GPS) based on the Connecticut State Plane System North American Datum (NAD) 1927.

2. CLASSIFICATION BASIS The survey unit was classified in accordance with Procedure RPM 5.1-10, "Survey Unit Classification." The historical information, scoping analyses and characterization results provided sufficient data to designate Survey Unit 9106-0005 as Class 2 in May 2006.

The "ClassificationBasis Summary" conducted for this survey unit consisted of:

a) A review of the 10CFR50.75 (g) (1) database, b) A review of the "InitialCharacterizationReport" and the "HistoricSite Assessment (HSA) Supplement, "

c) Historic and current survey records review, d) Visual inspections and a "walkdown."

e) Formal or informal interviews with cognizant personnel.

A review of the 10CFR50.75(g)(1) database report identified a number of events that may have impacted this survey unit. Several events indicated the potential for plant related contamination in the survey unit. These included a number of primary side system to secondary side system leakage events, Revision 0 3 Revision 0 3

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD contamination found to be present in secondary side systems and components, and unmonitored spills that drained to the discharge canal. In 1986, samples were taken from the legacy dredge spoils removed in 1979 dredged spoils area and from recently dredged canal sediment. The sample analyses indicated that the concentrations of Cs-137, Co-60 and other radionuclides were a small fraction of the DCGLs for those nuclides that could be identified by gamma spectroscopy. (refer to NE-86-RA-1142 dated 11-13-86). None the available historical information reviewed would support a conclusion that any residual activity in this survey unit is likely to be present at concentrations greater than the respective DCGLs.

Additional information was provided by several historical documents, including the "Results of Scoping Survey", (completed 9/1/98), the "Historical Site Assessment", and the HSA Supplement (dated 6-30-00). These documents presented the results of several sediment samples taken in 1997. These sample results indicated concentrations of 0.5 pCi/g for Co-60, 0.024 pCi/g for Cs-134 and 0.722 pCi/g for Cs-137.

An initial characterization survey of the Discharge Canal was performed during April and May of 2004. However, none of these samples were taken from within the footprint of survey Unit 9106-0005.

A final characterization was performed by Site Closure personnel in April of 2006 to obtain the necessary data of sufficient data quality for Final Status Survey (FSS) planning purposes. Six (6) 3-foot core sediment samples were taken from six (6) locations. All of the samples were analyzed by gamma spectroscopy. Since Hard-to-Detect (HTD) analyses were not performed and since Sr-90 was found to be a nuclide of concern in an adjacent discharge canal Survey Unit (SU 9106-0006), for conservatism it was included as a nuclide of concern in Survey Unit 9106-0005. The Sr-90 concentration statistics were also

.included in the variance calculations to determine the size of the sample population for FSS. Although no additional HTD testing was performed for characterization; four (4) of the fifteen (15) samples taken to demonstrate compliance with the release criteria during FSS were tested for the full suite of HTD nuclides to provide additional assurance that all of the radionuclides of concern were appropriately addressed. As a result of characterization, the radionuclides of concern identified for FSS planning purposes were Cs-137, Co-60 and Sr-90 (refer to Table 1).

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Minimum Value: 6.64E-02 1.16E-01 1.14E-OY Maximum Value: 2.79E-01 5.59E-01 7.16E-02 Mean: 1.73E-01 3.08E-01 4.17E-02 Median: 1.63E-01 2.64E-0I 3.94E-02 Standard Deviation: 8.09E-02 1.52E-01 2.50E-02 NOTE: The Operational DCGLs are 6.01 pCi/g for Cs-137, 2.90 pCi/g for Co-60 and 1.18 pCi/ g for Sr-90; these are used in conjunction with the unity rule to achieve nineteen (19) mremn/yr TEDE The FSS Engineer performed a visual inspection and walkdown during May 2006 to assess the physical condition of the survey unit, evaluate access points and travel paths and identify potentially hazardous conditions.

Based upon the historical information and the results of radiological surveys performed during characterization, it was concluded that there was a low probability for residual radioactivity to be present in this survey unit in concentrations greater than the Operational DCGLs justifying a final survey unit classification of Class 2 (refer to Section 3).

3. DATA QUALITY OBJECTIVES (DQO)

FSS design and planning is based on the Data Quality Objective (DQO) process as described by the LTP, Procedure RPM 5.1-11, "Preparationof Final Status Survey Plan," and the "Multi-Agency Radiation Survey and Site Investigation Manual" (MARSSIM). A summary of the main features of the DQO process are provided herein.

The DQO process incorporates hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would satisfy the release criteria objective of the FSS.

The primary objective of the Final Status Survey Plan (FSSP) was to demonstrate that the level of residual radioactivity in Survey Unit 9106-0005 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of Derived Concentration Guideline Levels (DCGLs). The DCGLs represent the concentration of radioactivity above background, equivalent to a dose-based release criterion and is presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil (called Base Case Soil DCGL),

for existing groundwater radioactivity and for future groundwater radioactivity that will be contributed by building foundations and footings.

As described in detail in the LTP, the dose model applied to the discharge canal presumes that the canal sediments are dredged to a depth of three (3) feet below the top of the sediment layer and spread for the planting of crops per the Resident Farmer Scenario. Consequently, the soil DCGLs are directly applied to the canal sediment media.

The DCGLs presented in Chapter 6 of the LTP were developed for exposures from three (3) components, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity. Equation I shows the mathematical relationship between the three (3) components and the total dose.

Equation I.

HTotal=Hsoil (sediment) + HExisting GW +/- HFuture GW The total dose under the LTP criteria is twenty-five (25) mrem/yr TEDE from all three (3) components. The allowable total dose under the Connecticut Department of Environmental Protection (CTDEP) radiological remediation standard for Connecticut Yankee (CY) is nineteen (19) mrem/yr TEDE. To satisfy both the LTP and CY CTDEP criteria, the dose from -soil must be reduced when using the groundwater dose values discussed above.

This survey unit is not affected by existing groundwater or by future groundwater (reference CY memo ISC 06-024). Therefore, dose contribution from existing and future groundwater is zero (0) mrem/yr TEDE, based on field data.

Equation 2:

19 mrem/yrTotaI= 19 mrem/yrsoi0 +0 mrem/yrExisting GW+0 mrem/yrFuture GW The allowable dose for soil in this survey unit is nineteen (19) mrem/yr TEDE as shown by Equation 2 above. The concentration of residual radioactivity resulting in nineteen (19) mrem/yr TEDE is designated as the Operational Revision 0 6 Revision 0 6

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD DCGL, and has been established for the radionuclides of concern as provided in Table 2.

Note: The survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 to conservatively account for the contribution to the total dose from existing and future groundwater which had not been established at the time of planning the FSS.

C-14 5.66E+00 4.30E+00 2.26E-01 Mn-54 1.74E+01 1.32E+O1 6.96E-0 I Fe-55 2.74E+04 2.08E+04 1.1OE+03 Co-60 3.81E+00 2.90E+00 1.52E-01 Ni-63 7.23E+02 5.49E+02 2.89E+0 I Sr-90 1.55E+00 1.18E+00 6.20E-02 Nb-94 7.12E+00 5.41 E+00 2.85E-01 Tc-99 1.26E+01 9.58E+00 5.04E-01 Ag- 108m 7.14E+00 5.43E+00 2.86E-01 Cs-134 4.67E+00 3.55E+00 1.87E-01 Cs-137 7.91 E+00 6.01E+00 3.16E-01 Eu-152 1.01E+01 7.68E+00 4.04E-01 Eu-154 9.29E+00 7.06E+00 3.72E-01 Eu-155 3.92E+02 2.98E+02 1.57E+01 Pu-238 2.96E+O1 2.25E+01 1.18E+00 Pu-239/240 2.67E+O 1 2.03E+01 1.07E+00 Pu-241 8.70E+02 6.61E+02 3.48E+01 Am-241 (5) 2.58E+01 1.96E+O1 1.03E+00 Cm-243/244 2.90E+0 I 2.20E+O 1 1.1 6E+00 (1) Bold indicates those radionuclides that are considered to be Hard to Detect (HTD)

(2) The Base Case Soil DCGLs for soil are specified by the LTP in Chapter 6 and are equivalent to twenty-five (25) mrem/yr TEDE (3) The Operational DCGL is equivalent to nineteen (19) mrem/yr TEDE (4) The required MDC is equivalent to one (1) mrem/yr TEDE (5) Americium-241 can be analyzed by gamma and alpha spectroscopy and is considered to be Easy to Detect (ETD). The preferred result is the alpha spectroscopy's when both analyses are performed.

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration variability. The radiological data that was used to support the DQO process, was provided by the characterization surveys performed in 2004 and 2006, as discussed in Section 2. Cs-137, Co-60 and Sr-90 were found to be the predominate radionuclides of concern., The basic statistical quantities (i.e., mean, standard deviation, median) for Cs-137, Co-60 and Sr-90 are provided in Table 1.

As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. Results reported as less than Minimum Detectable Concentration (<MDC) were not accepted for FSS. Sample report summaries included unique sample identification, analytical method, radionuclide, result, and uncertainty to two (2) standard deviations, laboratory data qualifiers, units, and the required and observed MDC.

4. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in Procedure RPM 5.1-11, "Preparation of Final Status Survey Plans".

This survey was initially designed to ten (10) mrem/yr TEDE. At the time when the survey was designed, the dose contribution for existing and future groundwater had not yet been determined. Consequently, a conservative value was chosen for the Operational DCGL. This approach is no longer required as the total dose from existing and future groundwater has been established. The dose for soil used for this survey unit to demonstrate compliance with the LTP criteria is nineteen (19) mrem/yr TEDE, as discussed in Section 2 of this Release Record.

The DQO process determined that Cs-137, Co-60 and Sr-90 were the radionuclides of concern (refer to Section 3). The sum of fractions or unity rule was used with the individual Operational DCGLs because multiple radionuclides (Cs-137, Co-60 and Sr-90) were considered in the survey design.

Surrogate DCGLs were not required for this survey unit based on process knowledge from FSS of nearby adjacent areas and via screening process described in LTP Section 5.4.7.3, "Gross Activity DCGLs". Sr-90 concentrations in sediment and soil were ascertained by direct analysis.

Radionuclide screening or de-selection is a process, described in LTP Section 5.4.7.2, where an individual radionuclide or aggregate may be considered insignificant and eliminated from the FSS. The criteria for de-selection are concentrations less than 5% for individual radionuclides and less than 10% for the aggregate of all radionuclides de-selected. This process was applied to analysis data for this survey unit.

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD The Elevated Measurement Comparison (EMC) did not apply to this survey unit since it is a Class 2 area and discrete, elevated areas of contamination were not expected.

The Sign Test was selected as the non-parametric statistical test to demonstrate that the null hypothesis was rejected. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. In addition, this approach is conservative since it includes background Cs-137 as part of the sample set.

The number of sediment samples for FSS was determined in accordance with Procedure RPM 5.1-12, "Determination of the Number of Samples for Final Status Survey. " The Lower Bound of the Gray Region (LBGR) was set to 0.78 in accordance with Procedure RPM 5.1-11 to maintain the relative shift (A/o) in the range of 1 and 3. The resulting relative shift was 2.0. A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of MARSSIM in support of the decommissioning license termination rule (10 CFR 20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design. This indicates that the survey unit has a high probability of rejecting the null hypothesis, assuming that the characterization data are representative of the FSS results. Survey design specified fifteen (15) sediment core samples for non-parametric statistical testing.

The grid pattern and locations of the sediment samples were determined using Visual Sample Plan (VSP) in accordance with Procedure RPM 5.1-14, "Identifying, and Marking Surface Sample Locations for Final Status Survey. "

Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy. A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate for a Class 2 area.

Judgmental sampling was included as a feature of this survey design to account for any anomalies potentially identified in the field.

Sample locations were identified using AutoCAD-LT, a commercially available plotting software package with coordinates consistent with the Connecticut State Plane System. These coordinates were integrated with a GPS to locate sample locations in the field. Sample Measurement Locations for the design are listed with the GPS coordinates in Table 3.

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Table 31-,ample Measurement Loc'ationis N~ith Associated (,S Coiordinates&

Designatiofn ~ Nprthing Easting 9106-0005-00IF 235695.70 670974.93 9106-0005-002F 235618.98 670930.64 9106-0005-003F 235618.98 671019.23 9106-0005-004F 235618.98 671107.82 9106-0005-005F 235618.98 671196.41 9106-0005-007F 235542.25 671152.11 9106-0005-008F 235542.25 671240.70 9106-0005-009F 235542.25 671329.29 9106-0005-OIOF 235542.25 671417.88 9106-0005-01 IF 235542.25 671506.47 9106-0005-013F 235465.53 671373.59 9106-0005-014F 235465.53 671462.18 9106-0005-015F 235465.53 671550.77 9106-0005-017F 235576.64 671402.01 9106-0005-018F 235550.83 671137.60 The sample location designations of Table 3 are not sequentially inclusive because of the necessity to relocate some samples due to the accessibility of the original sample locations. Sample locations 9106-0005-006F and 9106-0005-012F were found to be on dry land. Consequently, they were randomly re-located using the VSP software to two (2) new locations designated as 9106-0005-017F and 9106-0005-018F. Since sample 9106-0005-012F was randomly selected as a Quality Control (QC) split sample, sample 9106-0005-018F was designated as the replacement QC sample. Any location(s) identified by biased methods, were not included in Table 3.

One (1) biased sample was required by the sample plan. This sample was designated as sample location 9106-0005-016F. Sample results for sample location 9106-0005-016F are presented in Section 6, "Survey Results" and are also provided in Table 6.

Four (4) sediment samples were analyzed for the full suite of radionuclides specified in Table 1, exceeding the requirement to analyze 5% of the sample population for HTD analysis specified in procedure RPM 5.1-11. Two (2) of the four (4) samples were randomly selected using the Microsoft Excel "RAND" function. The two (2) samples exhibiting the highest observed radionuclide concentrations by gamma analyses were also selected.

The implementation of quality control measures as referenced by Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey, " required the collection of two (2) soil samples for "split sample" analysis by the off-site laboratory. These locations were selected randomly using the Microsoft Excel Revision 0 10 Revision 0 10

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD "RAND" function. The number of quality control samples exceeded the 5%

requirement as specified by the LTP.

Section 5.7.3.2.6 of the LTP specifies that scanning is not required for the FSS of the Discharge Canal. Table 4 provides a synopsis of the survey design.

Survey Unit 2 naseu on IuLoukiAu-L 1 anu v isuai 9,716 m Land Area Sample Plan calculations Type 1 and Type 2 errors were 0.05, Number of 15 sigma was 0.143 the LBGR was set to Measurements 0.78 to maintain Relative Shift in the range of I and 3, Relative Shift was 2.0 Grid Spacing 27.4 m Based on triangular grid 3.16 pCi/g Cs-137 Design DCGL 1.52 pCi/g Co-60 To achieve ten (10) mrem/yr TEDE 0.62 pCi/g Sr-90 6.01 pCi/g Cs-137 To achieve nineteen (19) mrem/yr Operational 2.90 pCi/g Co-60 TEDE (2) to demonstrate compliance with DCGL 1.18 pCi/g Sr-90 Equation 2 of this Release Record Scan Coverage N/A The LTP exempts this area Sediment 6.01 pCi/g Cs-137 The Operational DCGL meets the LTP Investigation 2.90 pCi/g Co-60 criteria for a Class 2 survey unit Level 1.18 pCi/g Sr-90 (1) The survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 as the total dose from existing and future groundwater had not been established at the time of planning the FSS (2) The allowable dose for soil in this survey unit is nineteen (19) mrem/yr TEDE as the bounding dose from existing and future groundwater has been established based on field data (reference CY memo ISC 06-024.)

5. SURVEY IMPLEMENTATION Final Status Survey field activities were conducted under Work Plan and Inspection Record (WP&IR) 2006-0021. The WP&IR package included a detailed FSSP, job safety analysis, job planning checklist and related procedures for reference. Daily briefings were conducted to discuss the expectations for job performance and the safety aspects of the survey. The "Daily Survey Journal" was used to document field activities and other information pertaining to the FSS.

Measurement locations were identified in North American Datum (NAD) 1927 coordinates that were supplied to the sampling vendor, Ocean Surveys, Inc.

(OSI) of Old Saybrook, Connecticut. Discharge Canal sampling was accomplished using direct push technology to collect composite samples of Revision 0 I1I Revision 0 11

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD bottom and mean high water mark sediments. Sediment cores from the Discharge Canal were obtained by OSI using a vibrating corer that is platform mounted on a sampling vessel. The core barrel was a three (3) inch diameter thin-walled aluminum tube which also served as a core liner (ten (10) feet or less). A core catcher was available to prevent the sample from sliding out of the bottom of the tube. Vessel positioning and the determination of sample locations were accomplished using a GPS interfaced with a navigation and data logging system.

After extraction, water was drained from above the sample by drilling holes above the sediment. The liner was cut, capped, sealed, labeled and turned over to site personnel who processed and controlled the samples under Chain of Custody (COC) protocols in accordance with procedure RPM 5.1-5, "Chain of Custody for Final Status Survey Samples. " Rinsing of the barrel and associated equipment was performed between sampling events. New aluminum tubes were used for each sample to prevent cross-contamination of subsequent samples.

The fifteen (15) sediment samples were collected and packaged in accordance with Haddam Neck Plant (HNP) Procedure RPM 5.1-3, "Collection of Sample Media for Final Status Survey" and FSS design. Samples were controlled, transported, stored, and transferred to the off-site laboratory using COC protocols.

Four (4) samples (9106-0005-005F, 9106-0005-009F, 9106-0005-OIOF and 9106-0005-014F) were selected for HTD radionuclide analysis by the off-site laboratory.

The implementation of quality control measures included the collection of two (2) split samples at locations 9106-0005-003F and 9106-0005-018F for comparative analysis by the off-site laboratory.

6. SURVEY RESULTS The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories (GEL) - Charleston, South Carolina. The laboratory analyzed the fifteen (15) samples taken for non-parametric statistical testing and the associated duplicates using gamma spectroscopy. Sr-90 was analyzed by gas flow proportional counting. All analyses were performed to the required MDC.

Cesium-137 was identified in twelve (12), Co-60 was identified in eight (8) and Sr-90 in four (4) of the fifteen (15) samples.

Several other radionuclides which were positively identified (i.e., a result greater than two (2) standard deviations uncertainty) could be de-selected or excluded using the 5% and 10% rule described in Section 5.4.7.2 of the LTP.

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD The off-site laboratory also processed four (4) samples for full HTD analysis as required by the sample plan. The requested analyses included alpha spectroscopy and liquid scintillation depending upon the radionuclide and the measurement method. All analyses were performed to the required MDC. Four (4) of the HTD radionuclides met the acceptance criteria for detection (i.e., a result greater than two standard deviations uncertainty) in more than one (1) sample; however, each of the positive results for HTD radionuclides could be de-selected based on the 5% and 10% rules.

None of the sample results exceeded the Operational DCGL or required further investigation. A summary of the sample results is provided in Table 5.

9106-0005-001 F 2.88E-02 1.91E-02 5.1OE-03 1.57E-02 9106-0005-002F 6.60E-02 8.95E-02 8.79E-03 4.93E-02 9106-0005-003F 3.09E-01 3.15E-01 1.15E-02 1.70E-01 9106-0005-004F 1.63E-01 2.1 OE-01 6.21 E-03 1.05E-01 9106-0005-005F -2.55E-02 9.87E-03 9.56E-03 7.28E-03 9106-0005-007F -5.19E-04 -7.92E-03 5.15E-03 1.55E-03 9106-0005-008F 1.86E-01 1.69E-01 -1.56E-03 8.80E-02 9106-0005-009F 1.81E-01 2.14E-02 1.30E-02 4.85E-02 9106-0005-010F 2.60E-0 1 1.38E+00 1.34E-02 5.31 E-0 1 9106-0005-01 IF 5.76E-02 0.OOE+00 1.49E-02 2.22E-02 9106-0005-013F 5.3 1E-02 1.55E-02 -1.93E-03 1.25E-02 9106-0005-014F 4.73E-01 1.12E+00 3.27E-03 4.68E-01 9106-0005-015F 7.09E-02 2.78E-03 6.68E-03 1.84E-02 9106-0005-017F 1.39E-01 3.43E-01 -8.59E-04 1.41E-01 9106-0005-018F 3.39E-02 4.19E-02 5.37E-02 6.57E-02 (1) The Operational DCGLs from Table 2 are 6.01 pCi/g for Cs-137, 2.90 pCi/g for Co-60 and 1.18 for Sr-90; these are used in conjunction with the unity rule to achieve nineteen (19) mrem/yr TEDE The sample location designations of Table 5 are not sequentially inclusive because of the necessity to relocate some samples due to the accessibility of the original sample locations. Sample locations 9106-0005-006F and 9106-0005-012F were found to be on dry land. Consequently, they were randomly re-located using the VSP software to two (2) new locations designated as 9106-0005-017F and 9106-0005-018F. Since sample 9106-0005-012F was randomly selected as a Quality Control (QC) split sample, sample 9106-0005-018F was designated as the replacement QC sample.

One (1) biased sample was required by the sample plan. This sample was designated as sample location 9106-0005-016F. Sample results for sample location 9106-0005-016F are presented in Table 6 below.

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Tabihe 6 - Biasei SampleResults C-17 Co-60 Sr-9O0 Fraction of the Sample Number p>i,- 1&p1/g_ pCi/g, Operational 9106-0005-016F -1.86E-02 2.07E-03 9.07E-04 -1.61E-03 The Operational DCGLs from Table 2 are 6.01 pCi/g for Cs-137, 2.90 pCi/g for Co-60 and 1.18 for Sr-90; these are used in conjunction with the unity rule to achieve nineteen (19) mrem/yr TEDE.

7. QUALITY CONTROL The two (2) split samples taken for QC were analyzed by the off-site laboratory.

The data were evaluated using USNRC acceptance criteria specified in Inspection Procedure 84750 and as detailed in HNP Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey. " One (1) split-sample (9106-0005-018F/S) did not meet the comparison criterion for Co-60. A possible cause for this anomaly could be the presence of Co-60 in the form of discrete particles. Such a physical form does not lend itself to homogenous mixing in a sediment matrix and, therefore, is not necessarily an indicator of inadequate sampling or sample preparation methodology. In this sample, K-40, a natural radioisotope, was found to be present at an acceptable level of agreement, therefore, the comparison was determined to be acceptable. For the other QC split samples, there was an acceptable level of agreement between the samples for all other detectable radionuclides.

The sample analysis vendor, GEL, maintained quality control and quality assurance plans as part of normal operation. Refer to Attachment 2 for data and data quality analysis results.

8. INVESTIGATIONS AND RESULTS One (1) sample result was found to exceed the design DCGL, but was below the nineteen (19) mrem/yr operational DCGL, as specified in Table 4. Confirmatory samples were collected to determine the extent of contamination. The extent was bounded by taking four (4) confirmatory samples, one (1) in each major compass direction (i.e., North, East, South, West), two (2) meters distant from the elevated sample location. The gamma spectroscopy results are included in Table 7.

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DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD O0OA 4.63E-02 7.70E-02 0.00442 3.80E-02 010B 9.08E-02 1.15E-01 -0.00561 5.01E-02 01OF 010C 1.92E-01 5.22E-01 0.00471 2.16E-01 010D 6.30E-01 2.24E+00 0.0219 8.97E-0I (1) The investigation of sample 01OF was initiated upon a sample result greater than the original design dose often (10) mrem/yr, prior to finalization of the dose contribution due to groundwater. Final results were evaluated against an Operational DCGL which considered the groundwater dose contribution.

(2) The Operational DCGLs are 6.01 pCi/g for Cs-137, 2.90 pCi/g for Co-60 and 1.18 for Sr-90; these are used in conjunction with the unity rule to achieve nineteen (19) mrem/yr TEDE.

The confirmatory results demonstrated that no measurements exceeded the nineteen (19) mrem/yr Operational DCGL, indicating that no further actions are warranted.

9. REMEDIATION AND RESULTS Historically, no radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to or as a result of the FSS. Health Physics TSD BCY-HP-0078, "ALARA Evaluation of Soil Remediation in Support of Final Status Survey, " determined that remediation beyond that required to meet the release criteria to be unnecessary and that the remaining residual radioactivity in soil was ALARA.

10. CHANGES FROM THE FINAL STATUS SURVEY PLAN The survey was designed to ten (10) mrem/yr TEDE which was conservative and necessary at the time of FSS planning. It is no longer required as the total dose from existing and future groundwater has been established. The dose for soil used to demonstrate compliance with the LTP and CTDEP criteria is nineteen (19) mrem/yr TEDE as discussed in Section 2 of this Release Record.

11. DATA QUALITY ASSESSMENT (DQA)

The DQO sample design and data were reviewed in accordance with Procedure RPM 5.1-23, "Data Quality Assessment. " The sample design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed on the data and compared to the original assumptions of the DQOs.

The evaluation of the Sign Test results indicates that the survey unit passes the unrestricted release criterion, thus, the null hypothesis is rejected.

Revision 0 15 Revision 0 15

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 2.

The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). The standard deviation was slightly more than the value used for the survey design. This is represented by the shift in the retrospective power curve as shown in Attachment 2f. This would indicate a need to change the original LBGR in order to maintain the number of samples at fifteen (15) to meet the Operational DCGL. However, the value of LBGR is not a critical issue as the survey unit has passed the statistical test, and the mean and median values are well below the Operational DCGL when used in conjunction with the unity rule. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power.

Therefore, the survey unit meets the unrestricted release criterion with adequate power as required by the DQOs.

The range of the data, about 3.23 standard deviations, was not unusually large.

The difference between the mean and median was 40.8% of the standard deviation which indicates some skewness in the data. The data was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot shows some positive skewness as confirmed by the calculated skew of 2.01.

All data, assessments, and graphical representations are provided in Attachment 2.

12. ANOMALIES The anomalies associated with the disagreement between the field splits has been discussed in Section 7. The source of the disagreement for Co-60, was likely due to Co-60 being present in the form of discrete particles. Such a physical form does not lend itself to homogenous mixing in a sediment matrix.

No other anomalies were identified in this survey unit.

13. CONCLUSION Survey Unit 9106-0005 has demonstrated compliance with the dose based, unrestricted release criterion. The sample data passed the Sign Test and the null hypothesis was rejected. The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved. Reclassification and remediation of this survey unit was not required.

Graphical representation of data indicates some positive skewness that is probably due to localized differences in particulate deposition rates, hydraulic velocity and sedimentation rates. The Retrospective Power Curve generated using COMPASS shows adequate power was achieved. The survey unit was properly designated as a Class 2 survey unit.

Revision 0 16 Revision 0 16

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD The dose contribution from sediment in this survey unit is 2.2 mrem/yr TEDE based on the average concentration of the samples used for non-parametric statistical sampling.

This survey unit is not affected by existing groundwater (reference CY memo ISC 06-024). It has been determined that the dose contribution from existing groundwater sources is bounded by zero (0) mrem/yr TEDE.

This survey unit is not considered impacted by future groundwater radioactive contamination, as there are no concrete foundations or footings containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component is, therefore, zero (0) mrem/yr TEDE.

The average total dose from residual radioactivity in this survey unit, including exposures from the three (3) components as described in Section 3, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity, will not exceed 2.2 mrem/yr Total Effective Dose Equivalent (TEDE).

14. ATTACHMENTS 14.1 Attachment I - Figures 14.2 Attachment 2 - Sample and Statistical Data Revision 0 17 Revision 0 17

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Attachment 1 Figures (9 pages)

ýý ý =ek,... -= fCl*,iECIT .mr1VER.[r Reference Coordinate Sj~ten Benchmark Northing - 236594.38 / Lasting - 668136.14 FiguCe 1 StoMnnecticut Yankee Atomic Power Company 9 -o o By

~~ 1 Site Map With Reference To Survey Unit9106-0005 Octobffr 206 E.S.

14 9

9 9

~)Sample Location sIaccwsble Sample Locaton WeWds 0 35 70 Feet Connecticut Yankee Atomic Power Company 9106-0005FinalStatus Survey Design

911

~) Samle Location hmkws~aAiy Sample Lowaton

-_ Wetlands 0 35 70

, MC  : Feet ConnecticutYankee Atomic Power Company 9106-0005 FinalS*tw Swvy Design InvestigationSample Locations

0.473 0

K 0.181 0

Location Inxessblc Sample Locaton Wetlnds 0 34 66 PcF,,

Note.

Cesum-137 embfirew given mg wlts ofpcilk.

onncticut Yankee Atomic PowerCompany 9106-0005 FinalStatus Survey Design Cesium-137PostingPlot

Sample Loc*aon Location 4L-- Wedlams 9106-0005-01OF 0 34 69 MC== =Feet 0.26 Note.

Cesiwn-137 masufta are given in units OfPcilkg Connecticut Yankee Atomic PowerCompany 9106-0005 (South End)FinalStatus Survey Investigative Samples Cesium-137PostingPlot

0O.

1.12 0.0214 0 0

&)Sample Lomaton 0.0021 &wLuccew7,le SaMPle Lomaton Wetlands 0 34 69

, Feet Note.

Cobaft-60 ivsuft~am givwi in unite ofpWi/g Connecticut Yankee Atomic PowerCompany 9106-0005FinalStatus Survey Design Cobalt-60PostingPlot

'9106-0005-010B 0.115 Sample Locadon 9106-0005-010C WetLand 0.522 9106-0005-010C 15 30 Connecticut Yankee Atomic PowerCompany 9106-0005FinalStatus Survey Design InvestigatorySamples Cobalt-60PostingPlot

0.0149 4-0.0033 0.013 6 0

sawjle Loca~on 0.0009 &)InC=]csll Sample Lomaton Wetlaads 0 34 68 Note.

S&Wntium-90 mgzlty am ginunig~t~

ofPMilg Wnecicdut Yankee Atomic Power Comp 9106-0005FinalStatus Survey Design Suontium-9oPostingPlot

ý106-0005-010B

-0.0056 Location 9106-0005-010C Locatioo 0.0047 Wetands 0 17 34 9106-0005-0101 Note:

0.0134 S&trotiw-90 g~bweni mt gim ill Units oftc/g.

ConnecticutYankee Atomic PowerCompany 9106-0005FinalStatus Survey Investgatoy Samples Stontum-90 PostingPlot

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Attachment 2 Sample and Statistical Data

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Attachment 2a Sample Data (247 Pages)

Table of Contents G eneral Narrative .................................................................. 1 Chain of Custody and Supporting Documentation ........... 4 Radiological Analysis .......................................................... 9 Sample Data Summary ...................................................... 29 Q uality C ontrol D ata ........................................................... 69

General Narrative 1

CASE NARRATIVE For CONNECTICUT YANKEE RE: Sediment PO# 002332 Work Order: 162485 SDG: MSR #06-0675 June 7, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:

2040 Savage Road Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina on May 9, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.

The laboratory received the following sample(s):

Sample ID Client Sample ID 162485001 9106-0005-OOIF 162485002 9106-0005-002F 162485003 9106-0005-003F 162485004 9106-0005-003FS 162485005 9106-0005-004F 162485006 9106-0005-007F 162485007 9106-0005-008F 162485008 9106-0005-OIOF GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

P.O. Box 30712

• Charleston, SC 29417 ° 2040 Savage Road (29407)

Phone (843) 556-8171 - Fa 2 (843) 766-1178

• www.gel.com

Sample ID Client Sample ID 162485009 9106-0005-01 IF 162485010 9106-0005-013F 162485011 9106-0005-014F 162485012 9106-0005-016F 162485013 9106-0005-015F 162485014 9106-0005-017F 162485015 9106-0005-018F 162485016 9106-0005-018FS 162485017 9106-0005-005F 162485018 9106-0005-009F Items of Note:

There are no items of note.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.

Analytical Request:

Sixteen sediment samples were analyzed for FSSGAM and Sr-90.

Two sediment samples were analyzed for FSSALL.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP INC.

P.O. Box 30712

• Charleston, SC 29417

• 2040 Savage Road (29407)

Phone (843) 556-8171

• Fa)5843) 766-1178 - www.gel.com

Chain of Custody and Supporting Documentation 4

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Health Physics Procedure GPP-GGGR-R5 104-003-Attachment B-CY-001 Major Chain of Custody Form Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 I 6.aAS5 /

k'roject Name: "aaaam Neck i~ecommisslo Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: 0 30 D. [ 14 D. R] 7 D.

Date

--.* I Samples Shipped Via:

Z Fed Ex LI ups nI Hand 3

• 2- lOther Bill of Lading #

7fgo '?15s"Y6'*S

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Health Physics Procedure GPP-GGGR-R5 104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested " Use On1*K, Contact Name & Phone: - - - - *,.

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones r(n Priority: 9 30 D. E] 14 D. [17 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservatin c2 9106-0005-OIOF 5/02/06 13:16 SE C BP x x Transferred from COC 2006-00314 QM 9106-0005-01 IF 5/02/06 13:39 SE C BP x X Transferred from COC 2006-00314 Q 9106-0005-013F 5/02/06 14:35 SE C BP x x Transferred from COC 2006-00314 9106-0005-014F 5/02/06 15:04 SE C BP x X Transferred from COC 2006-00314

! 9106-0005-016F 5/02/06 13:59 SE C BP x X Transterred from COC 2006-00314 5 9106-0005-015F 5/03/06 08:03 SE C BP X X Transferred from COC 2006-00316 U 9106-0005-017F 5/03/06 08:13 SE C BP X X Transferred from COC 2006-00316

)5 9106-0005-018F 5/03/06 09:09 SE C BP x X Transferred from COC 2006-00316

• 9106-0005-018FS 5/03/06 09:09 SE C BP X X Transferred from COC 2006-00316 NOTES: PO #: 002332 MSR #: 06-0675 SSWP# NA [ LTP QA [] Radwaste QA El Non QA Samples Shipped Via:

El FedEx EiBUPS LI Hand

1) AlinquishfBy* Date/Time 2

3) Rq*,,,--*'

• -*')(*/'/'*/*,**ql By '@ [atc/Time o l*'/ [E

[ Other

3) quished By Date/Time 4),Received&'y Date/Time _ _____

Bill of Lading #

79z6' q19S '~

Connecticut Yankee CY-ISC.SON-0OI Statement of Work for Analytical Lab Services . Y, Figure 1. Sample Check-in List Date/Time Received:

Work Order Number: \J"- L"*'* I.

Shipping Cdntainer ID:. o , 2,43*- Chain of Custody #-* ,. n L- O l - Lc I. Custody Seals od shipping container intact?.. -Yes No

2. Custody Seals dated and signed? Yes F'fNo I ].

3. Chain-of-Custody record present? Yes f No [I

4. Cooler temperature C., C C.

ICg Wet ,]Dry U,]

S. Vermiculite/packing materials is:

6.: - .Numberof samples in shipping container: * -t

7. Sample holding times exceeded? . Yes [ I No

8. Samples have:

"//tapeWhazard labels

-/-custody seals appropriate sample labels

9. Samples are" i in good condition .... leaking (*rtiwif . .)

-broken -have air bubbles

10. Were any anomalies identified in sample receipt? Yes ' ] No Il.. Description of anomalies (include sample numbers):

Sample Custodian/Laboratoay:- Date: /g . O .g"-

On By .

Telephoned to: -

7

SAMPL RECEIPT & REVIEW FORM 0P e

'+4 roR Itc" PM use only Client: 4 b Q\/A ]f7/6jSDG/ARCOC/Work Order: (,7- q285 Date Received: IPM(A) Review (ensure non formi items are resolved prior to signing):

Received By: j___________________

Sample Receipt Criteria z Comments/Qualifiers (Required for Non-Conforming Items)

Shipping containers received intact Circle Applicable: seals broken damaged container leaking container other (describe) a sealed?

Samp requiring cold Circle Coolant # ice bags blue ice dry ice none other describe) 2 preservati within (4 +/- 2 C)?

Record preserv *on method.

Chain of custody do ns included with shi mn?_____________________________

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking container other (describe) 5 Samples requiring chemical Sample ID's, containers affected and observed pH:

preservation at proper pH? S s n a VOA vials free of headspace Sample ID's and containers affected:

6 (defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) 8 Samples received within holding Id's and tests affected:

time?

9 Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles?

10 Date & time on COC match date Sample ID's affected:

& time on bottles?

Number of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in 12 relinquished/received sections?

Air Bill ,Tracking #'s, & Fi(- 7q2-iw 71095 4?52-- > /75: --

14Additional Comments iR)( 4. & -- :> [o c

, RSO RAD Receipt #

Suspected Hazard Information Sse

• '=dgar=nrm in *jf > x2 area background .. is observed on samples identified as "non-W, al regulated/non-radioactive", contact the Radiation Safety group for further 04 cd EE investigation.

SRadiological Classification? r Maximum Counts Observed*:

PC Regulated? Comments:

Shipped as DUT Hazardous " C C JMaterial? If yes, contact Waste UN#:

[Manager or ESH Manager.

PM (or PMA) review of Hazard classification: Initials Date: " o 8 0

RADIOLOGICAL ANALYSIS 9

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 162485 Method/Analysis Information Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 533471 Prep Batch Number: 528491 Dry Soil Prep GL-RAD-A-021 Batch Number: 528487 Sample ID Client ID 162485017 9106-0005-005F 162485018 9106-0005-009F 1201101117 Method Blank (MB) 1201101118 162485017(9106-0005-005F) Sample Duplicate (DUP) 1201101119 162485017(9106-0005-005F) Matrix Spike (MS) 1201101120 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

10

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162485017 (9106-0005-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information 11

Product: Alphaspec Pu, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- 11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 533472 Prep Batch Number: 528491 Dry Soil Prep GL-RAD-A-021 Batch Number: 528487 Sample ID Client ID 162485017 9106-0005-005F 162485018 9106-0005-009F 1201101121 Method Blank (MB) 1201101122 162485017(9106-0005-005F) Sample Duplicate (DUP) 1201101123 162485017(9106-0005-005F) Matrix Spike (MS) 1201101124 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 I REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162485017 (9106-0005-005F).

QC Information All of the QC samples met the required acceptance limits.

12

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- 11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 533473 Prep Batch Number: 528491 Dry Soil Prep GL-RAD-A-021 Batch Number: 528487 13

Sample ID Client ID 162485017 9106-0005-005F 162485018 9106-0005-009F 1201101125 Method Blank (MB) 1201101126 162485017(9106-0005-005F) Sample Duplicate (DUP) 1201101127 162485017(9106-0005-005F) Matrix Spike (MS) 1201101128 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162485017 (9106-0005-005F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis The tracer yield for sample 1201101127 (9106-0005-005F) was recounted due to poor resolution.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from 14

referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Gamma,Solid-FSS GAM & ALL FSS Analytical Method: EML HASL 300,4.5.2.3 Prep Method: Dry Soil Prep Analytical Batch Number: 529776 Prep Batch Number: 528487 Sample ID Client ID 162485001 9106-0005-001F 162485002 9106-0005-002F 162485003 9106-0005-003F 162485004 9106-0005-003FS 162485005 9106-0005-004F 162485006 9106-0005-007F 162485007 9106-0005-008F 162485008 9106-0005-OIOF 162485009 9106-0005-01IF 162485010 9106-0005-013F 162485011 9106-0005-014F 162485012 9106-0005-016F 162485013 9106-0005-015F 162485014 9106-0005-017F 162485015 9106-0005-018F 162485016 9106-0005-018FS 162485017 9106-0005-005F 162485018 9106-0005-009F 1201092332 Method Blank (MB) 1201092333 162485001(9106-0005-001 F) Sample Duplicate (DUP) 1201092334 Laboratory Control Sample (LCS) 15

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 11.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162485001 (9106-0005-001F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 162485002 (9106-0005-002F), 162485003 (9106-0005-003F), 162485014 (9106-0005-017F) and 162485015 (9106-0005-018F) were recounted due to high MDAs.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

16

Qualifier information Qualifier Reason Analyte Sample UI Data rejected due to interference. Europium-155 162485006 162485015 1201092333 Manganese-54 162485008 UI Data rejected due to low abundance. Cesium- 134 162485001 162485002 162485008 162485011 162485012 162485013 162485014 162485015 162485017 162485018 1201092333 Cobalt-60 162485016 U' Data rejected due to no valid peak. 162485009 Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 535512 Prep Batch Number: 528491 Dry Soil Prep GL-RAD-A-021 Batch Number: 528487 17

Sample ID Client ID 162485001 9106-0005-001F 162485002 9106-0005-002F 162485003 9106-0005-003F 162485004 9106-0005-003FS 162485005 9106-0005-004F 162485006 9106-0005-007F 162485007 9106-0005-008F 162485008 9106-0005-01OF 162485009 9106-0005-01IF 162485010 9106-0005-013F 162485011 9106-0005-014F 162485012 9106-0005-016F 162485013 9106-0005-015F 162485014 9106-0005-017F 162485015 9106-0005-018F 162485016 9106-0005-018FS 162485017 9106-0005-005F 162485018 9106-0005-009F 1201105909 Method Blank (MB) 1201105910 162335018(9106-0003-008F) Sample Duplicate (DUP) 1201105911 162335018(9106-0003-008F) Matrix Spike (MS) 1201105912 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 10.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QCQ Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162335018 (9106-0003-008F).

18

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Tc99, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 531704 Sample ID Client ID 162485017 9106-0005-005F 162485018 9106-0005-009F 1201096867 Method Blank (MB) 1201096868 162583001 (NOL-02-02-005-F-S) Sample Duplicate (DUP) 1201096869 162583001(NOL-02-02-005-F-S) Matrix Spike (MS) 1201096870 Laboratory Control Sample (LCS) 19

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 13.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162583001 (NOL-02-02-005-F-S).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

20

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 531618 Prep Batch Number: 528491 Dry Soil Prep GL-RAD-A-021 Batch Number: 528487 Sample ID Client ID 162485018 9106-0005-009F 1201096631 Method Blank (MB) 1201096632 163173001 (9304-0000-063RACR) Sample Duplicate (DUP) 1201096633 163173001(9304-0000-063RACR) Matrix Spike (MS) 1201096634 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

21

Designated QC The following sample was used for QC: 163173001 (9304-0000-063RACR).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 535483 Prep Batch Number: 528491 Dry Soil Prep GL-RAD-A-021 Batch Number: 528487 22

Sample ID Client ID 162485017 9106-0005-005F 1201105872 Method Blank (MB) 1201105873 162335018(9106-0003-008F) Sample Duplicate (DUP) 1201105874 162335018(9106-0003-008F) Matrix Spike (MS) 1201105875 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162335018 (9106-0003-008F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples were reprepped due to low/high carrier/tracer yield.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this 23

SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 531622 Prep Batch Number: 528491 Dry Soil Prep GL-RAD-A-021 Batch Number: 528487 Sample ID Client ID 162485017 9106-0005-005F 162485018 9106-0005-009F 1201096644 Method Blank (MB) 1201096645 163173001 (9304-0000-063RACR) Sample Duplicate (DUP) 1201096646 163173001(9304-0000-063RACR) Matrix Spike (MS) 1201096647 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

24

Quality Control (00 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163173001 (9304-0000-063RACR).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: LSC, Tritium Dist, Solid-HTD2,ALL FSS Analytical Method: EPA 906.0 Modified Analytical Batch Number: 531705 25

Sample ID Client ID 162485017 9106-0005-005F 162485018 9106-0005-009F 1201096877 Method Blank (MB) 1201096878 162583001(NOL-02-02-005-F-S) Sample Duplicate (DUP) 1201096879 162583001(NOL-02-02-005-F-S) Matrix Spike (MS) 1201096880 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 11.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162583001 (NOL-02-02-005-F-S).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 1201096877 (MB) was recounted due to high MDA.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from 26

referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint C14, Solid AII,FSS Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 534984 Sample ID Client ID 162485017 9106-0005-005F 162485018 9106-0005-009F 1201104745 Method Blank (MB) 1201104746 163173001 (9304-0000-063RACR) Sample Duplicate (DUP) 1201104747 163173001 (9304-0000-063RACR) Matrix Spike (MS) 1201104748 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

27

Designated QC The following sample was used for QC: 163173001 (9304-0000-063RACR).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples were reprepped due to low/high recovery.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical. method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

Reviewer/Date:" M 28

SAMPLE DATA

SUMMARY

29

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOO Connecticut Yankee Atomic Power Co.

Client SDG: MSR#06-0675 GEL Work Order: 162485 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the reporting limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by 30

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OO1F Project: YANKO 1204 Sample ID: 162485001 Client ID: YANKOOl Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 13.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSSGAM & ALL FSS Actinium-228 1.69 +/-0.251 0.0613 +/-0.251 0.131 pCi/g MJH1 06/02/06 1701 529776 1 Americium-241 U 0.064 +/-0.113 0.0919 +/-0.113 0.188 pCi/g Bismuth-212 0.887 +/-0.313 0.147 +/-0.313 0.310 pCi/g Bismuth-214 1.15 +/-0.147 0.0343 +/-0.147 0.072 pCi/g Cesium-134 UUI 0.00 +/-0.0385 0.0269 +/-0.0385 0.0561 pCi/g Cesium-137 U 0.0288 +/-0.0259 0.020 +/-0.0259 0.042 pCi/g Cobalt-60 U 0.0191 +/-0.0235 0.0194 +/-0.0235 0.0418 pCi/g Europium-152 U -0.0115 +/-0.0595 0.053 +/-0.0595 0.110 pCi/g Europium-154 U -0.0146 +/-0.0717 0.0515 +/-0.0717 0.111 pCi/g Europium-155 U 0.0293 +/-0.0678 0.0581 +/-0.0678 0.119 pCi/g Lead-212 1.62 +1-0.145 0.0311 +/-0.145 0.0639 pCi/g Lead-214 1.36 +/-0.154 0.035 +/-0.154 0.0728 pCi/g Manganese-54 U 0.0112 +/-0.0236 0.021 +/-0.0236 0.0443 pCi/g Niobium-94 U - 0.00247 +/-0.0192 0.0168 +/-0.0192 0.0353 pCi/g Potassium-40 11.3 +1- 1.05 0.148 +/-1.05 0.326 pCi/g Radium-226 1.15 +/-0.147 0.0343 +/-0.147 0.072 pCi/g Silver-108m U-0 .000679 +/-0.0191 0.0167 +/-0.0191 0.0349 pCi/g Thallium-208 0.495 +/-0.0669 0.0186 +/-0.0669 0.0391 pCi/g Rad Gas Flow Proportional Counting GFPC, S90, solid-ALL FSS Strontium-90 U 0.0051 +/-0.00834 0.00785 +/-0.00834 0.0162 pCi/g BXFI 06/06/06 2315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 31

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OOIF Proiect: YANK01204 Sample ID: 162485001 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Fracer Recovery GFPC, Sr90, solid-ALL FSS 84 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

32

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-002F Proiect: YANK01204 Sample ID: 162485002 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 24.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.01 +/-0.158 0.0602 +/-0.158 0.128 pCi/g MJHI 06/06/06 2111 529776 1 Americium-241 U 0.0239 +/-0.128 0.0948 +/-0.128 0.195 pCi/g Bismuth-212 0.970 +/-0.334 0.131 +/-0.334 0.276 pCi/g Bismuth-214 0.596 +/-0.0898 0.0351 +/-0.0898 0.0732 pCi/g Cesium-134 UUI 0.00 +/-0.040 0.0245 +/-0.040 0.0512 pCi/g Cesium-137 0.066 +/-0.028 0.0183 +/-0.028 0.0383 pCi/g Cobalt-60 0.0895 +/-0.0523 0.0192 +/-0.0523 0.0414 pCi/g Europium- 152 U 0.00476 +/-0.0525 0.0426 +/-0.0525 0.0885 pCi/g Europium- 154 U -0.094 +/-0.0729 0.054 +/-0.0729 0.116 pCi/g Europiurn-155 U 0.0792 +/-0.0731 0.0478 +/-0.0731 0.0983 pCi/g Lead-212 1.12 +/-0.0645 0.0247 +/-0.0645 0.0511 pCi/g Lead-214 0.709 +/-0.0806 0.033 +/-0.0806 0.0684 pCi/g Manganese-54 U 0.0279 +/-0.0326 0.0165 +/-0.0326 0.035 pCi/g Niobium-94 U -0.011 +/-0.0193 0.0154 +/-0.0193 0.0323 pCi/g Potassium-40 19.7 +/-1.00 0.165 +/-1.00 0.358 pCi/g Radium-226 0.596 +/-0.0898 0.0351 +/-0.0898 0.0732 pCi/g Silver-108m U -0.0068 +/-0.0174 0.0146 +/-0.0174 0.0304 pCi/g Thallium-208 0.351 +/-0.0455 0.0182 +/-0.0455 0.038 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.00879 +/-0.0124 0.0116 +/-0.0124 0.0241 pCi/g BXF1 06/06/06 2315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM1 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 33

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-002F Proiect: YANKO 1204 Sample ID: 162485002 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr9O, solid-ALL FSS 77 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

34

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-003 F Proiect: YANKO 1204 Sample ID: 162485003 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 01-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 18%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.799 +/-0.140 0.0393 +/-0.140 0.0827 pCi/g MJH 1 06/07/06 0542 529776 1 Americium-241 U 0.0143 +/-0.0558 0.0479 +1-0.0558 0.0981 pCi/g Bismuth-212 0.576 +/-0.223 0.0854 +/-0.223 0.179 pCi/g Bismuth-214 0.558 +/-0.0789 0.0206 +/-0.0789 0.0428 pCi/g Cesium-134 U 0.0211 +/-0.025 0.0143 +/-0.025 0.0297 pCi/g Cesium- 137 0.309 +/-0.0378 0.0108 +/-0.0378 0.0227 pCi/g Cobalt-60 0.315 +/-0.0352 0.0107 +/-0.0352 0.0228 pCi/g Europium-152 U -0.036 +/-0.0336 0.0288 +/-0.0336 0.0598 pCi/g Europium-154 U -0.031 +/-0.0389 0.0304 +/-0.0389 0.0648 pCi/g Europium-155 U 0.049 +/-0.0404 0.0382 +/-0.0404 0.0783 pCi/g Lead-212 0.770 +/-0.0726 0.0187 +/-0.0726 0.0384 pCi/g Lead-214 0.591 +/-0.072 0.0223 +/-0.072 0.046 pCi/g Manganese-54 U 0.0053 +/-0.0138 0.0123 +/-0.0138 0.0257 pCi/g Niobium-94 U 0.00488 +/-0.0117 0.0106 +/-0.0117 0.0221 pCi/g Potassium-40 11.1 +/-0.839 0.090 +/-0.839 0.195 pCi/g Radium-226 0.558 +/-0.0789 0.0206 +/-0.0789 0.0428 pCi/g Silver- 108m U 0.00339 +/-0.0112 0.010 +/-0.0112 0.0208 pCi/g Thallium-208 0.241 +/-0.036 0.00999 +/-0.036 0.0209 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.0115 +/-0.00646 0.00552 +/-0.00646 0.0116 pCi/g BXFI 06/06/06 2315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM1 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 35

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-003F Proiect: YANK01204 Sample ID: 162485003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrierf/racer Recovery GFPC, Sr9O, solid-ALL FSS 80 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

36

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-003FS Proiect: YANKO 1204 Sample ID: 162485004 Client ID: YANKOO I Matrix: SE Vol. Recv.:

Collect Date: 01-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 19.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.820 +/-0.171 0.0681 +/-0.171 0.146 pCi/g MJH1 06/02/06 1705 529776 1 Americium-241 U -0.213 +/-0.112 0.0853 +/-0.112 0.175 pCi/g Bismuth-212 0.487 +/-0.330 0.145 +/-0.330 0.308 pCi/g B3ismuth-214 0.660 +/-0.096 0.0359 +/-0.096 0.0759 pCi/g Cesium-134 U 0.0563 +/-0.0303 0.027 +/-0.0303 0.0569 pCi/g Cesium-137 0.331 +/-0.0533 0.0191 +/-0.0533 0.0406 pCi/g Cobalt-60 0.618 +/-0.0738 0.0204 +/-0.0738 0.0445 pCi/g Europium-152 U -0.0624 +/-0.0613 0.0496 +/-0.0613 0.104 pCi/g Europium-154 U 0.00151 +/-0.0757 0.0543 +/-0.0757 0.119 pCi/g Europium-155 U 0.0473 +/-0.0801 0.058 +/-0.0801 0.120 pCi/g Lead-212 0.789 +/-0.0601 0.0292 +/-0.0601 0.0606 pCi/g Lead-214 0.663 +/-0.099 0.0392 +/-0.099 0.0816 pCi/g Manganese-54 U 0.0192 +/-0:0257 0.0232 +/-0.0257 0.049 pCi/g Niobium-94 U -0.00129 +/-0.0203 0.0176 +/-0.0203 0.0372 pCi/g Potassium-40 11.6 +/-0.876 0.156 +/-0.876 0.349 pCi/g Radium-226 0.660 +/-0.096 0.0359 +/-0.096 0.0759 pCi/g Silver-108m U -0.00245 +/-0.0201 0.0169 +/-0.0201 0.0355 pCi/g Thallium-208 0.272 +/-0.0448 0.022 +/-0.0448 0.0462 pCi/g Rad Gas Flow Proportional Counting GFPC,S90, solid-ALL FSS Strontium-90 U 0.00413 +/-0.0087 0.00819 +/-0.0087 0.0171 pCi/g BXFI 06/06/062315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 37

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-003FS Project: YANKO 1204 Sample ID: 162485004 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 63 (25°/-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

38

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-004F Proiect: YANK01204 Sample ID: 162485005 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 15%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.988 +/-0.223 0.0833 +/-0.223 0.167 pCi/g MJHI 06/04/06 2031 529776 1 Americium-241 U 0.0868 +/-0.102 0.0899 +/-0.102 0.180 pCi/g Bismuth-212 0.795 +/-0.406 0.158 +/-0.406 0.316 pCi/g Bismuth-214 0.652 +/-0.118 0.044 +/-0.118 0.088 pCi/g Cesium-134 U 0.0438 +/-0.042 0.0264 +/-0.042 0.0527 pCi/g Cesium- 137 0.163 +/-0.040 0.0208 +/-0.040 0.0416 pCi/g Cobalt-60 0.210 +/-0.0451 0.0199 +/-0.0451 0.0398 pCi/g Europium-152 U 0.0114 +/-0.0904 0.0574 +/-0.0904 0.115 pCi/g Europium-154 U 0.0148 +/-0.069 0.0549 +/-0.069 0.110 pCi/g Europium-155 U 0.0299 +/-0.0714 0.0676 +/-0.0714 0.135 pCi/g Lead-212 0.971 +/-0.110 0.0343 +/-0.110 0.0687 pCi/g Lead-214 0.802 +/-0.122 0.0413 +/-0.122 0.0826 pCi/g Manganese-5 4 U 0.00298 +/-0.0268 0.0209 +/-0.0268 0.0417 pCi/g Niobium-94 U -0.0158 +/-0.0251 0.0187 +/-0.0251 0.0373 pCi/g Potassium-40 9.40 +/-0.987 0.171 +/-0.987 0.342 pCi/g Radium-226 0.652 +/-0.118 0.044 +/-0.118 0.088 pCi/g Silver-108m U -0.016 +/-0.0227 0.0189 +/-0.0227 0.0378 pCi/g Thallium-208 0.283 +/-0.0535 0.0232 +/-0.0535 0.0464 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid ALL FSS Strontium- 9 0 U 0.00621 +/-0.00726 0.00668 +/-0.00726 0.0139 pCi/g BXF1 06/06/062315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM I 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 39

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-004F Project: YANK01204 Sample ID: 162485005 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90,. solid-ALL FSS 81 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

40

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis

• T

• i T Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-007F Project: YANK01204 Sample ID: 162485006 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 22.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.864 +/-0.211 0.0703 +/-0.211 0.150 pCi/g MJHI 06/02/06 1814 529776 1 Americium-241 U -0.0181 +/-0.123 0.0875 +/-0.123 0.180 pCi/g Bismuth-212 0.624 +/-0.357 0.151 +/-0.357 0.320 pCi/g Bismuth-214 0.550 +/-0.117 0.0353 +/-0.117 0.0744 pCi/g Cesium-134 U 0.0386 +/-0.0448 0.0249 +/-0.0448 0.0524 pCi/g Cesium-137 U-C .000519 +/-0.0237 0.0194 +/-0.0237 0.0411 pCi/g Cobalt-60 U - -0.00792 +/-0.0276 0.0221 +/-0.0276 0.0479 pCi/g Europium-152 U - 0.00987 +/-0.0594 0.0468 +/-0.0594 0.0979 pCi/g Europium-154 U 0.0388 +/-0.0715 0.0622 +/-0.0715 0.134 pCi/g Europium-155 UUI 0.00 +/-0.101 0.0505 +/-0.101 0.104 pCi/g Lead-212 1.01 +/-0.110 0.027 +/-0.110 0.0559 pCi/g Lead-214 0.568 +/-0.109 0.0352 +/-0.109 0.0734 pCi/g Manganese-54 U - 0.00574 +/-0.025 0.0198 +/-0.025 0.0421 pCi/g Niobium-94 U 0.0306 +/-0.0288 0.0179 +/-0.0288 0.0377 pCi/g Potassium-40 15.8 +/-1.48 0.166 +/-1.48 0.370 pCi/g Radium-226 0.550 +/-0.117 0.0353 +/-0.117 0.0744 pCi/g Silver-108m U -0.0145 +/-0.0187 0.015 +/-0.0187 0.0317 pCi/g Thallium-208 0.328 +/-0.0609 0.0184 +/-0.0609 0.0389 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.00515 +/-0.0113 0.0106 +/-0.0113 0.0221 pCi/g BXFI 06/06/06 2315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 41

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 lnjun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-007F Project: YANK01204 Sample ID: 162485006 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 56 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

42

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-008F Proiect: YANKO 1204 Sample ID: 162485007 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 32.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.561 +/-0.225 0.0839 +/-0.225 0.185 pCi/g MJH1 06/02/06 1815 529776 1 Americium-241 U 0.0421 +/-0.116 0.0954 +/-0.116 0.200 pCi/g Bismuth-212 0.707 +/-0.249 0.146 +/-0.249 0.325 pCi/g Bismuth-214 0.454 +/-0.107 0.0407 +/-0.107 0.0883 pCi/g Cesium-134 U 0.0398 +/-0.0588 0.0274 +/-0.0588 0.0597 pCi/g Cesium-137 0.186 +/-0.0582 0.0245 +/-0.0582 0.0532 pCi/g Cobalt-60 0.169 +/-0.0693 0.0213 +/-0.0693 0.0491 pCi/g Europium-152 U -0.00962 +/-0.0639 0.0552 +/-0.0639 0.118 pCi/g Europium-154 U -0.0777 +/-0.0922 0.0673 +/-0.0922 0.152 pCig Europium-155 U 0.0611 +/-0.0741 0.0675 +/-0.0741 0.141 pCi/g Lead-212 0.622 +/-0.0943 0.0431 +/-0.0943 0.0899 pCi/g Lead-214 0.505 +/-0.129 0.0406 +/-0.129 0.0868 pCi/g Manganese-54 U 0.0275 +/-0.0446 0.0233 +/-0.0446 0.0512 pCi/g Niobium-94 U -0.0153 +/-0.0267 0.0207 +/-0.0267 0.0451 pCi/g Potassium-40 10.4 +/- 1.09 0.223 +/-1.09 0.510 pCi/g Radium-226 0.454 +/-0.107 0.0407 +/-0.107 0.0883 pCi/g Silver-108m U 0.00991 +/-0.0259 0.0229 +/-0.0259 0.0488 pCi/g Thallium-208 0.210 +/-0.0495 0.0263 +/-0.0495 0.0564 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00156 +/-0.00706 0.00692 +/-0.00706 0.0144 pCi/g BXF1 06/06/062315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM1 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 43

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-008F Project: YANKO 1204 Sample ID: 162485007 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier[Fracer Recovery GFPC, Sr90, solid-ALL FSS 80 (25%/o-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

44

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com CDrfifp.2fD nf A nahrci

~Ik £~LI~4R V ~YI~ SLI1I~..~L~

Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-01OF Project: YANKO 1204 Sample ID: 162485008 Client ID: YANKOOl Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 24.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid FSS GAM & ALL FSS Actinium-228 1.07 +/-0.262 0.0751 +/-0.262 0.156 pCi/g MJH1 06/02/06 1816 529776 1 Americium-241 U 0.106 +/-0.119 0.0922 +/-0.119 0.189 pCi/g Bismuth-212 0.847 +/-0.369 0.139 +/-0.369 0.291 pCi/g Bismuth-214 0.606 +/-0.101 0.0329 +/-0.101 0.0684 pCi/g Cesium-134 UUI 0.00 +/-0.044 0.0243 +/-0.044 0.0504 pCi/g Cesium-137 0.260 +1-0.0501 0.0189 +/-0.0501 0.0393 pCi/g Cobalt-60 1.38 +/-0.116 0.0195 +/-0.116 0.0414 pCi/g Europium-152 U -0.026 +/-0.0529 0.0437 +/-0.0529 0.0901 pCi/g Europium-154 U 0.00723 +/-0.0668 0.055 +/-0.0668 0.117 pCi/g Europium-155 U 0.0255 +/-0.0705 0.0421 +/-0.0705 0.0862 pCi/g Lead-212 1.10 +/-0.107 0.024 +/-0.107 0.0494 pCi/g Lead-214 0.667 +/-0.104 0.0308 +/-0.104 0.0637 pCi/g Manganese-54 UUI 0.00 +/-0.0364 0.0196 +/-0.0364 0.0409 pCi/g Niobium-94 U 0.00799 +/-0.0213 0.0175 +/-0.0213 0.0363 pCi/g Potassium-40 19.5 +/-1.58 0.162 +/-1.58 0.348 pCi/g Radium-226 0.606 +/-0.101 0.0329 +/-0.101 0.0684 pCi/g Silver-108m U 0.00878 +/-0.0183 0.0155 +/-0.0183 0.032 pCi/g Thallium-208 0.381 +/-0.062 0.0159 +/-0.062 0.0332 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr9O, solid-ALL FSS Strontium-90 U 0.0134 +/-0.00904 0.00803 +/-0.00905 0.0167 pCi/g BXF1 06/06/06 2315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 45

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010F Project: YANKO1204 Sample ID: 162485008 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits CarrierlTracer Recovery GFPC, Sr90, solid-ALL FSS 70 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

46

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Frtfpofjti nf A nAl cie k M J.

Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-011 F Project: YANKO 1204 Sample ID: 162485009 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 21.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.04 +/-0.322 0.158 +/-0.322 0.342 pCi/g MJH1 06/02/06 1816 529776 1 Americium-241 U -0.0209 +/-0.0723 0.0605 +/-0.0723 0.125 pCi/g Bismuth-212 0.798 +/-0.698 0.370 +/-0.698 0.793 pCi/g Bismuth-214 0.761 +/-0.207 0.0856 +/-0.207 0.182 pCi/g Cesium-134 U 0.0368 +/-0.0558 0.0494 +/-0.0558 0.107 pCi/g Cesium-137 U 0.0576 +/-0.053 0.0486 +/-0.053 0.104 pCi/g Cobalt-60 UUI 0.00 +/-0.0718 0.0351 +/-0.0718 0.0803 pCi/g Europium-152 U 0.0149 +/-0.126 0.106 +/-0.126 0.223 pCi/g Europium-154 U 0.101 +/-0.0992 0.136 +/-0.0992 0.298 pCi/g Europium-155 U 0.0805 +/-0.125 0.0965 +/-0.125 0.201 pCi/g Lead-212 0.965 +/-0.128 0.0608 +/-0.128 0.127 pCi/g Lead-214 0.696 +/-0.181 0.0702 +/-0.181 0.149 pCi/g Manganese-54 U 0.0519 +/-0.0609 0.054 +/-0.0609 0.115 pCi/g Niobium-94 U -0.0229 +/-0.0502 0.0406 +/-0.0502 0.087 pCi/g Potassium-40 13.2 +/-1.63 0.372 +/-1.63 0.844 pCi/g Radium-226 0.761 +/-0.207 0.0856 +/-0.207 0.182 pCi/g Silver-108m U 0.017 +/-0.046 0.0389 +/-0.046 0.0825 pCi/g Thallium-208 0.307 +/-0.106 0.0478 +/-0.106 0.102 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.0149 +/-0.0147 0.0134 +/-0.0147 0.028 pCi/g BXF1 06/06/06 2315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 47

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-01 IF Proiect: YANK01204 Sample ID: 162485009 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr9O, solid-ALL FSS 58 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

48

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-013F Project: YANKO 1204 Sample ID: 162485010 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 28.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSS GAM & ALL FSS Actinium-228 0.845 +/-0.370 0.118 +/-0.370 0.260 pCi/g MJHI 06/02/06 1816 529776 1 Americium-241 U 0.0182 +/-0.0393 0.0327 +/-0.0393 0.0687 pCi/g Bismuth-212 0.534 +/-0.723 0.226 +/-0.723 0.500 pCi/g Bismuth-214 0.502 +/-0.163 0.0695 +/-0.163 0.149 pCi/g Cesium-134 U 0.022 +/-0.0811 0.0372 +/-0.0811 0.0817 pCi/g Cesium-137 U 0.0531 +/-0.0476 0.0334 +/-0.0476 0.0728 pCi/g Cobalt-60 U 0.0155 +/-0.0421 0.0365 +/-0.0421 0.0826 pCi/g Europium-152 U 0.0486 +/-0.0961 0.0732 +/-0.0961 0.157 pCi/g Europium-154 U -0.0487 +/-0.128 0.0981 +/-0.128 0.222 pCi/g Europium-155 U 0.00245 +/-0.0732 0.0575 +/-0.0732 0.121 pCi/g Lead-212 0.953 +/-0.0988 0.0376 +/-0.0988 0.080 pCi/g Lead-214 0.522 +/-0.113 0.050 +/-0.113 0.108 pCi/g Manganese-54 U -0.0151 +/-0.044 0.0338 +/-0.044 0.0744 pCi/g Niobium-94 U 0.0023 +/-0.0308 0.0254 +/-0.0308 0.0561 pCi/g Potassium-40 14.6 +/-1.53 0.277 +/-1.53 0.652 pCi/g Radium-226 0.502 +/-0.163 0.0695 +/-0.163 0.149 pCi/g Silver-108m U 0.0221 +/-0.0309 0.0278 +/-0.0309 0.0598 pCi/g Thallium-208 0.308 +/-0.0757 0.0286 +/-0.0757 0.0626 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U -0.00193 +/-0.00896 0.00878 +/-0.00896 0.0183 pCi/g BXFI 06/06/062315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM1 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 49

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-013F Project: YANKO 1204 Sample ID: 162485010 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 69 (25%,- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

• Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

• QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

50

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-014F Project: YANK01204 Sample ID: 162485011 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 22.8%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM& ALL FSS Actinium-228 0.767 +/-0.372 0.142 +/-0.372 0.308 pCi/g MJH1 06/02/06 1817 529776 1 Americium-241 U 0.00567 +/-0.0503 0.0456 +/-0.0503 0.0945 pCi/g Bismuth-212 0.678 +/-0.625 0.288 +/-0.625 0.621 pCi/g Bismuth-214 0.568 +/-0.137 0.0579 +/-0.137 0.125 pCi/g Cesium-134 UUI 0.00 +/-0.123 0.0505 +/-0.123 0.108 pCi/g Cesium- 137 0.473 +/-0.101 0.0326 +/-0.101 0.0707 pCi/g Cobalt-60 1.12 +/-0.136 0.027 +/-0.136 0.0629 pCi/g Europium-152 U -0.0376 +/-0.092 0.0787 +/-0.092 0.167 pCi/g Europium-154 U -0.0403 +/-0.128 0.103 +/-0.128 0.231 pCi/g Europium-155 U -0.0272 +/-0.0791 0.0682 +/-0.0791 0.143 pCi/g Lead-212 0.752 +/-0.097 0.0449 +/-0.097 0.0942 pCi/g Lead-214 0.520 +/-0.136 0.0599 +/-0.136 0.127 pCi/g Manganese-54 U -0.0183 +/-0.0478 0.0378 +/-0.0478 0.0819 pCi/g Niobium-94 U 0.0317 +/-0.0391 0.0351 +/-0.0391 0.0753 pCi/g Potassium-40 10.6 +/-1.36 0.285 +/-1.36 0.660 pCi/g Radium-226 0.568 +/-0.137 0.0579 +/-0.137 0.125 pCi/g Silver-108m U - 0.00517 +/-0.0328 0.028 +/-0.0328 0.060 pCi/g Thallium-208 0.240 +/-0.0841 0.0342 +/-0.0841 0.0735 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00327 +/-0.00761 0.00719 +/-0.00761 0.015 pCi/g BXFI 06/06/06 2315 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 51

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-014F Project: YANK01204 Sample ID: 162485011 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 73 (25%-125o)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

52

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

. Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-016F Project: YANKO 1204 Sample ID: 162485012 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 36.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.892 +/-0.211 0.0546 +/-0.211 0.115 pCi/g MJHI 06/02/06 1817 529776 1 Americium-241 U 0.036 +/-0.0698 0.0577 +/-0.0698 0.118 pCi/g Bismuth-212 0.921 +/-0.305 0.118 +1-0.305 0.247 pCi/g Bismuth-214 0.623 +/-0.110 0.0294 +/-0.110 0.0612 pCi/g Cesium-134 UUI 0.00 +/-0.032 0.0203 +/-0.032 0.0422 pCi/g Cesium-137 U -0.0186 +/-0.0188 0.014 +/-0.0188 0.0294 pCi/g Cobalt-60 U 0.00207 +/-0.019 0.0155 +/-0.019 0.033 pCi/g Europium-152 U 0.011 +/-0.0492 0.041 +/-0.0492 0.0848 pCi/g Europium-154 U 0.0157 +/-0.0583 0.0481 +/-0.0583 0.102 pCi/g Europium-155 U 0.00321 +/-0.0586 0.0472 +/-0.0586 0.0967 pCi/g Lead-212 1.03 +/-0.099 0.0244 +/-0.099 0.0502 pCi/g Lead-214 0.733 +/-0.119 0.0269 +/-0.119 0.0559 pCi/g Manganese-54 U 0.0111 +/-0.0205 0.0175 +/-0.0205 0.0365 pCi/g Niobium-94 U C.000839 +/-0.0174 0.0146 +/-0.0174 0.0305 pCi/g Potassium-40 17.2 +/-1.29 0.129 +/-1.29 0.279 pCi/g Radium-226 0.623 +/-0.110 0.0294 +/-0.110 0.0612 pCi/g Silver-108m U - 0.00106 +/-0.0164 0.0134 +/-0.0164 0.0278 pCi/g Thallium-208 0.336 +/-0.0543 0.0152 +/-0.0543 0.0317 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0'.000907 +/-0.00836 0.00805 +/-0.00836 0.0168 pCi/g BXFI 06/06/06 2316 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM1 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 53

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-016F Project: YANK01204 Sample ID: 162485012 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

54

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-015F Project: YANKO 1204 Sample ID: 162485013 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 11.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.779 +/-0.111 0.0398 +/-0.111 0.0838 pCi/g MJH1 06/04/06 2021 529776 1 Americium-241 U 0.0415 +/-0.0889 0.0568 +/-0.0889 0.116 pCi/g Bismuth-212 0.716 +/-0.201 0.0882 +/-0.201 0.185 pCi/g Bismuth-214 0.693 +/-0.0601 0.0215 +/-0.0601 0.0448 pCi/g Cesium-134 UUI 0.00 +/-0.0256 0.0163 +/-0.0256 0.0337 pCi/g Cesium-137 0.0709 +/-0.0212 0.0112 +/-0.0212 0.0234 pCi/g Cobalt-60 U 0.00278 +/-0.0149 0.0126 +/-0.0149 0.0269 pCi/g Europium-152 U -0.0239 +/-0.0383 0.0328 +/-0.0383 0.0677 pCi/g Europium-154 U -0.0182 +/-0.0424 0.0343 +/-0.0424 0.0729 pCi/g Europium-155 U 0.0206 +/-0.0452 0.0394 +/-0.0452 0.0803 pCi/g Lead-212 0.762 +/-0.0411 0.0201 +/-0.0411 0.0411 pCi/g Lead-214 0.764 +/-0.0661 0.0228 +/-0.0661 0.0471 pCi/g Manganese-54 U -0.0066 +/-0.0146 0.0123 +/-0.0146 0.0258 pCi/g Niobium-94 U -0.00534 +/-0.0121 0.0104 +/-0.0121 0.0218 pCi/g Potassium-40 10.6 +/-0.537 0.0994 +/-0.537 0.215 pCi/g Radium-226 0.693 +/-0.0601 0.0215 +/-0.0601 0.0448 pCi/g Silver-108m U 0.000726 +/-0.0125 0.0108 +/-0.0125 0.0224 pCi/g Thallium-208 0.275 +/-0.0298 0.0109 +/-0.0298 0.0228 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.00668 +/-0.00736 0.00679 +/-0.00736 0.0141 pCi/g BXF1 06/06/06 2316 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 55

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-015F Proiect: YANKO 1204 Sample ID: 162485013 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 88 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

56

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-017F Proiect: YANKO 1204 Sample ID: 162485014 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 16.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.34 +/-0.186 0.0567 +/-0.186 0.118 pCi/g MJH1 06/07/06 0543 529776 1 Americium-241 U 0.074 +/-0.123 0.0919 +/-0.123 0.188 pCi/g Bismuth-212 0.895 +/-0.265 0.121 +/-0.265 0.253 pCi/g Bismuth-214 1.01 +/-0.0975 0.0317 +/-0.0975 0.0656 pCi/g Cesium-134 UUI 0.00 +/-0.0273 0.0211 +/-0.0273 0.0437 pCi/g Cesium-137 0.139 +/-0.0335 0.0184 +/-0.0335 0.0381 pCi/g Cobalt-60 0.343 +1-0.0511 0.0168 +/-0.0511 0.0355 pCi/g Europium-152 U -0.0397 +/-0.0485 0.0403 +/-0.0485 0.0832 pCi/g Europium- 154 U -0.0218 +/-0.0616 0.049 +/-0.0616 0.103 pCi/g Europium- 155 U 0.0712 +/-0.0622 0.0548 +/-0.0622 0.112 pCi/g Lead-212 1.60 +/-0.0709 0.0252 +/-0.0709 0.0518 pCi/g Lead-214 1.29 +/-0.094 0.0289 +/-0.094 0.0597 pCi/g Manganese-54 U 0.0295 +/-0.0263 0.0165 +/-0.0263 0.0344 pCi/g Niobium-94 U 0.00962 +/-0.0185 0.0154 +/-0.0185 0.0319 pCi/g Potassium-40 22.8 +/-0.878 0.140 +/-0.878 0.299 pCi/g Radium-226 1.01 +/-0.0975 0.0317 +/-0.0975 0.0656 pCi/g Silver-108m U - 0.00158 +/-0.0168 0.0141 +/-0.0168 0.0292 pCi/g Thallium-208 0.487 +/-0.0422 0.0162 +/-0.0422 0.0336 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U-C 1.000859 +/-0.00856 0.00834 +/-0.00856 0.0173 pCi/g BXF1 06/06/06 2316 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 57

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-017F Project: YANK01204 Sample ID: 162485014 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 81 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

58

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-018F Project: YANKO 1204 Sample ID: 162485015 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 17.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.02 +/-0.245 0.0737 +/-0.245 0.158 pCi/g MJH1 06/06/062355 529776 1 Americium-241 U -0.134 +/-0.127 0.0923 +/-0.127 0.191 pCi/g Bismuth-212 0.808 +/-0.337 0.155 +/-0.337 0.330 pCi/g Bismuth-214 0.608 +/-0.117 0.038 +/-0.117 0.0803 pCi/g Cesium-134 UUI 0.00 +/-0.0567 0.0308 +/-0.0567 0.0646 pCi/g Cesium-137 U 0.0339 +/-0.0308 0.0238 +/-0.0308 0.050 pCi/g Cobalt-60 U 0.0419 +/-0.0323 0.0295 +/-0.0323 0.0631 pCi/g Europium-152 U -0.0249 +/-0.0653 0.0503 +/-0.0653 0.105 pCi/g Europium-154 U -0.0153 +/-0.0841 0.0681 +/-0.08 41 0.147 pCi/g Europium-155 UUI 0.00 +/-0.0972 0.0544 +/-0.0972 0.112 pCi/g Lead-212 1.09 +/-0.121 0.0297 +/-0.121 0.0616 pCi/g Lead-214 0.665 +/-0.127 0.0364 +/-0.127 0.0762 pCi/g Manganese-54 U 0.0255 +/-0.0288 0.0246 +/-0.0288 0.0521 pCi/g Niobium-94 U 0.0151 +/-0.0247 0.0209 +/-0.0247 0.044 pCi/g Potassium-40 18.6 +/-1.71 0.203 +/-1.71 0.447 pCi/g Radium-226 0.608 +/-0.117 0.038 +/-0.117 0.0803 pCi/g Silver-108m U - 0.00395 +/-0.0202 0.0167 +/-0.0202 0.0353 pCi/g Thallium-208 0.381 +/-0.0688 0.0206 +/-0.0688 0.0436 pCi/g Rad Gas Flow Proportional Counting GFPC, Sr90, solid-ALL FSS Strontium-90 0.0537 +/-0.0144 0.011 +/-0.0145 0.023 pCi/g BXFI 06/06/06 2316 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 59

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-018F Proiect: YANKO 1204 Sample ID: 162485015 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 49 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

60

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis vT - -s

.. . ... ... . A. . ...a Company - Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-018FS Project: YANKO 1204 Sample ID: 162485016 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 24.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.15 +/-0.407 0.148 +/-0.407 0.313 pCi/g MJH1 06/04/06 2022 529776 1 Americium-241 U 0.0465 +/-0.0698 0.0523 +/-0.0698 0.107 pCi/g Bismuth-212 U 0.509 +/-0.589 0.330 +/-0.589 0.693 pCi/g Bismuth-214 0.740 +/-0.172 0.0759 +/-0.172 0.159 pCi/g Cesium-134 U 0.0988 +/-0.0652 0.0488 +/-0.0652 0.103 pCi/g Cesium-137 0.105 +/-0.0796 0.0395 +/-0.0796 0.0829 pCi/g Cobalt-60 UUI 0.00 +/-0.145 0.0515 +/-0.145 0.109 pCi/g Europium-152 U 0.0375 +/-0.119 0.0988 +/-0.119 0.205 pCi/g Europium-154 U -0.0127 +/-0.171 0.122 +/-0.171 0.260 pCi/g Europium-155 U 0.0362 +/-0.105 0.0853 +/-0.105 0.175 pCi/g Lead-212 1.25 +/-0.117 0.048 +/-0.117 0.0995 pCi/g Lead-214 0.924 +/-0.192 0.0659 +/-0.192 0.137 pCi/g Manganese-54 U 0.0155 +/-0.0534 0.0446 +/-0.0534 0.0936 pCi/g Niobium-94 U-C .000986 +/-0.0449 0.0372 +/-0.0449 0.078 pCi/g Potassium-40 20.1 +/-1.60 0.375 +/- 1.60 0.812 pCi/g Radium-226 0.740 +/-0.172 0.0759 +/-0.172 0.159 pCi/g Silver-108m U - 0.00684 +/-0.0501 0.035 +/-0.0501 0.0729 pCi/g Thallium-208 0.389 +/-0.104 0.0401 +/-0.104 0.0839 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00484 +/-0.00859 0.00803 +/-0.00859 0.0168 pCi/g BXF1 06/06/06 2316 535512 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 EPA 905.0 Modified 61

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-018FS Project: YANK01204 Sample ID: 162485016 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

62

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-005F Project: YANKO 1204 Sample ID: 162485017 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 17.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.0415 +/-0.0591 0.055 +/-0.0591 0.185 pCi/g LCW1 05/30/06 1156 533471 1 Curium-242 U -0.00755 +/-0.0634 0.0358 +/-0.0634 0.157 pCi/g Curium-243/244 U 0.00112 +/-0.0607 0.0636 +/-0.0607 0.203 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.0261 +/-0.0511 0.00 +/-0.0512 0.0707 pCi/g LCW1 05/30/06 2129 533472 2 Plutonium-239/240 U 0.0459 +/-0.0733 0.0297 +/-0.0734 0.130 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U -8.66 +/-8.72 7.70 +/-8.77 16.0 pCi/g LCW1 06/03/06 0541 533473 3 Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 +/-0.304 0.0844 +/-0.304 0.169 pCi/g MJHI 06/02/06 1826 529776 4 Americium-241 U +/-0.121 0.0993 +/-0.121 0.199 pCi/g Bismuth-212 +/-0.459 0.190 +/-0.459 0.380 pCi/g Bismuth-214 +/-0.188 0.0487 +/-0.188 0.0974 pCi/g Cesium-134 UU1 +/-0.0421 0.0364 +/-0.0421 0.0728 pCi/g Cesium-137 U - +/-0.0345 0.0274 +/-0.0345 0.0547 pCi/g Cobalt-60 U I +/-0.0303 0.0263 +/-0.0303 0.0526 pCi/g Europium-152 U +/-0.0944 0.0728 +/-0.0944 0.145 pCi/g Europium-154 U +/-0.112 0.0779 +/-0.112 0.156 pCi/g Europium-155 U +/-0.0964 0.0839 +/-0.0964 0.168 pCi/g Lead-212 +/-0.170 0.0432 +/-0.170 0.0864 pCi/g Lead-214 +/-0.181 0.0528 +/-0.181 0.106 pCi/g Manganese-54 U 0. +/-0.0388 0.029 +/-0.0388 0.0579 pCi/g Niobium-94 U - +/-0.0275 0.0234 +/-0.0275 0.0467 pCi/g Potassium-40 +/-1.29 0.222 +/-1.29 0.443 pCi/g Radium-226 +/-0.188 0.0487 +/-0.188 0.0974 pCi/g Silver-108m U -1 +/-0.0289 0.0248 +/-0.0289 0.0495 pCi/g Thallium-208 +/-0.078 0.0254 +/-0.078 0.0507 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U I 0956 +/-0.00903 0.00831 +/-0.00904 0.0172 pCi/g BXF1 06/06/06 2316 535512 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL F Tritium U 3.49 +/-6.18 5.06 +/-6.18 10.5 pCi/g NXPI 05/28/06 0323 531705 7 Liquid Scint C14, SolidAll,FSS 63

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-005F Proiect: YANK01204 Sample ID: 162485017 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Liquid Scintillation Analysis Liquid Scint C14, SolidAllFSS Carbon- 14 U 0.048 +/-0.107 0.0885 +/-0.107 0.183 pCi/g ATH2 06/03/06 1732 534984 8 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -5.82 +/-15.5 11.7 +1-15.5 24.6 pCi/g AFI 06/05/06 1626 535483 10 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -2.31 +/-4.11 3.49 +/-4.11 7.11 pCi/g SLNI 05/26/06 2217 531622 12 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.298 +/-0.271 0.218 +/-0.271 0.450 pCi/g SXEI 05/30/06 2126 531704 13 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021lB LXMI 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EML HASL 300, 4.5.2.3 5 EPA 905.0 Modified 6 EPA 905.0 Modified 7 EPA 906.0 Modified 8 EPA EERF C-01 Modified 9 EPA EERF C-01 Modified 10 DOE RESL Fe-I, Modified 11 DOE RESL Fe-1, Modified 12 DOE RESL Ni-I, Modified 13 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 96 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 82 (25%- 125%)

64

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-005F Project: YANKO 1204 Sample ID: 162485017 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 80 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 94 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 90 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 72 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

65

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Ce-rtifirnate nf Annivdi.

Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-009F Proiect: YANKO 1204 Sample ID: 162485018 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 14.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0451 +/-0.104 0.0757 +/-0.104 0.241 pCi/g LCWI 05/30/06 1156 533471 1 Curium-242 U 0.0375 +/-0.0735 0.00 +/-0.0736 0.102 pCi/g Curium-243/244 U 0.0173 +/-0.0689 0.0537 +/-0.0689 0.197 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U - 0.0133 +/-0.0575 0.0447 +/-0.0575 0.165 pCi/g LCW1 05/30/06 2129 533472 2 Plutonium-239/240 U 0.0211 +/-0.0559 0.0316 +/-0.056 0.138 pCi/g Liquid Scint Pu241, Solid ALL FSS Plutonium-241 U -4.2 +/-9.77 8.38 +/-9.78 17.5 pCi/g LCWI 06/03/06 0557 533473 3 Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.558 +/-0.165 0.0655 +/-0.165 0.131 pCi/g MJH1 06/02/06 1827 529776 4 Americium-241 U 0.0512 +/-0.0953 0.0797 +/-0.0953 0.159 pCi/g Bismuth-212 U 0.288 +/-0.274 0.224 +/-0.274 0.447 pCi/g Bismuth-214 0.541 +/-0.106 0.0381 +/-0.106 0.0762 pCi/g Cesium-134 UUI 0.00 +/-0.0381 0.0252 +/-0.0381 0.0504 pCi/g Cesium- 137 0.181 +/-0.0535 0.0218 +/-0.0535 0.0435 pCi/g Cobalt-60 U 0.0214 +/-0.0242 0.0239 +/-0.0242 0.0478 pCi/g Europium-152 U 0.0156 +/-0.0758 0.0566 +/-0.0758 0.113 pCi/g Europium-154 U - 0.0435 +/-0.0786 0.0615 +/-0.0786 0.123 pCi/g Europium-155 U 0.079 +/-0.116 0.0597 +/-0.116 0.119 pCi/g Lead-212 0.569 +/-0.0793 0.031 +/-0.0793 0.062 pCi/g Lead-214 0.445 +/-0.109 0.038 +/-0.109 0.0759 pCi/g Manganese-54 U 0.0259 +/-0.0233 0.0226 +/-0.0233 0.0452 pCi/g Niobium-94 U 0'.00303 +/-0.0254 0.0218 +/-0.0254 0.0435 pCi/g Potassium-40 10.5 +/-1.11 0.182 +/-1. 11 0.364 pCi/g Radium-226 0.541 +/-0.106 0.0381 +/-0.106 0.0762 pCi/g Silver-108m U 0'.00846 +/-0.0219 0.0198 +/-0.0219 0.0396 pCi/g Thallium-208 0.156 +/-0.058 0.0188 +/-0.058 0.0376 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 01.013 +/-0.00829 0.00722 +/-0.0083 0.0152 pCi/g BXF1 06/06/06 2316 535512 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 6.86 +/-6.34 5.06 +/-6.34 10.5 pCi/g NXPI 05/28/06 0354 531705 7 Liquid Scint C14, SolidAllFSS 66

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-009F Proiect: YANKO 1204 Sample ID: 162485018 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Liquid Scintillation Analysis Liquid Scint C14, SolidAlFSS Carbon-14 U C.043 +/-0.0961 0.0793 +/-0.0961 0.164 pCi/g ATH2 06/03/06 1934 534984 8 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 1.25 +/-22.5 17.0 +/-22.5 35.7 pCi/g SLN1 05/29/06 1526 531618 10 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -0 +/-4.99 4.21 +/-4.99 8.57 pCi/g SLNI 05/26/06 2318 531622 11 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U C.333 +/-0.298 0.239 +/-0.298 0.494 pCi/g SXEI 05/30/062142 531704 12 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM1 05/10/06 0855 528491 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 05/09/06 1829 528487 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EML HASL 300, 4.5.2.3 5 EPA 905.0 Modified 6 EPA 905.0 Modified 7 EPA 906.0 Modified 8 EPA EERF C-01 Modified 9 EPA EERF C-0I Modified 10 DOE RESL Fe-I, Modified 11 DOE RESL Ni-l, Modified 12 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 87 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 85 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 77 (25%-I125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 71 (25%-125%)

67

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-009F Project: YANKO 1204 Sample ID: 162485018 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15%- 125°%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 67 (25%6-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 65 (15%- 125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

68

.1 QUALITY CONTROL DATA I

69

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Renort Date: June 8, 2006 Client : Connecticut Yankee Atomic Power Page 1 of 9 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 162485 Parmname NOM Sample Oual QC Units RPD% REC% Range AnIst Date Time Rad Alpha Spec Batch 533471 QC1201101118 162485017 DUP Americium-241 U -0.0415 U -0.00249 pCi/g 177 (0% - 100%) CWI 05/30/06 11:55 Uncert: +/-0.0591 +/-0.0219 TPU: +/-0.0591 +/-0.0219 Curium-242 U -0.00755 U 0.0283 pCi/g 346 (0% - 100%)

Uncert: +/-0.0634 +1-0.0555 TPU: +/-0.0634 +/-0.0556 Curium-243/244 U 0.00112 U 0.0131 pCi/g 168 (0%- 100%)

Uncert: +/-0.0607 +/-0.0521 TPU: +/-0.0607 +/-0.0521 QC1201101120 LCS Americium-241 12.2 10.8 pCi/g 89 (75%-125%) 05/30/06 11:55 Uncert: +/-0.975 TPU: +/-1.73 Curium-242 U -0.0056 pCi/g Uncert: +/-0.047 TPU: +/-0.0471 Curium-243/244 14.9 12.4 pCi/g 83 (75%-125%)

Uncert: +/-1.04 TPU: +/-1.95 QCI201101117 MB Americium-241 U -0.00902 pCi/g 05/30/06 11:55 Uncert: +/-0.019 TPU: +/-0.019 Curium-242 U 0.0399 pCi/g Uncert: +/-0.0638 TPU: +/-0.064 Curium-243/244 U 0.0392 pCi/g Uncert: +/-0.0626 TPU: +/-0.0628 QCI201101119 162485017 MS Americium-241 12.7 U -0.0415 12.5 pCi/g 98 (75%-125%) 05/30/06 11:55 Uncert: +/-0.0591 +/-1.06 TPU: +/-0.0591 +/-1.96 Curium-242 U -0.00755 U 0.00 pCi/g Uncert: +/-0.0634 +/-0.0517 TPU: +/-0.0634 +/-0.0517 Curium-243/244 15.5 U 0.00112 12.6 pCi/g 81 (75%-125%)

Uncert: +/-0.0607 +/-1.06 TPU: +/-0.0607 +/-1.98 Batch 533472 QC1201101122 162485017 DUP Plutonium-238 U 0.0261 U 0.00 pCi/g (0%- 100%) .CW1 05/30/06 21:29 70

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162485 Page 2 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 533472 Uncert: +1-0.0511 +/-0.0498 TPU: +/-0.0512 +/-0.0498 Plutonium-239/240 U 0.0459 U -0.00609 pCi/g 261 (0%- 100%)

Uncert: +/-0.0733 +/-0.0511 TPU: +/-0.0734 +/-0.0512 QC1201101124 LCS Plutonium-238 0.216 pCi/g (75%-1 25%) 05/30/06 21:29 Uncert: +/-0.181 TPU: +/-0.182 Plutonium-239/240 11.3 10.3 pCi/g 91 (75%-125%)

Uncert: +/-1.21 TPU: +/-1.76 QC1201101121 MB Plutonium-238 U -0.00623 pCi/g 05/31/06 07:44 Uncert: +/-0.0692 TPU: +/-0.0693 Plutonium-239/240 U -0.0274 pCi/g Uncert: +/-0.100 TPU: +/-0.100 QC1201101123 162485017 MS Plutonium-238 U 0.0261 U 0.0634 pCi/g (75%-125%) 05/30/06 21:29 Uncert: +1-0.0511 +/-0.0787 TPU: +/-0.0512 +/-0.079 Plutonium-239/240 11.7 U 0.0459 10.7 pCi/g 92 (75%-125%)

Uncert: +/-0.0733 +/-0.971 TPU: +/-0.0734 +/-1.52 Batch 533473 QC1201101126 162485017 DUP Plutonium-24 I U -8.66 U -6.36 pCi/g 0 (0% - 100%) LCWI 06/03/06 07:35 Uncert: +/-8.72 +/-6.79 TPU: +/-8.77 +/-6.82 QC1201101128 LCS Plutonium-241 131 106 pCi/g 81 (75%-125%) 06/03/06 08:07 Uncert: +/-12.3 TPU: +/-16.4 QC1201101125 MB Plutonium-241 U -1.18 pCi/g 06/03/06 07:18 Uncert: +/-9.02 TPU: +/-9.02 QC1201101127 162485017 MS Plutonium-241 135 U -8.66 146 pCi/g 108 (75%-125%) 06/03/06 07:51 Uncert: +/-8.72 +/-14.7 TPU: +/-8.77 +/-20.1 Rad Gamma Spec Batch 529776 QC1201092333 162485001 DUP Actinium-228 1.69 1.64 pCi/g 7 (0%- 100%) MJHI 06/04/06 20:23 Uncert: +/-0.251 +/-0.254

+/-0.254 71

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162485 Page 3 of 9 Parmname NOM Sample Qual OC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 529776 TPU: +/-0.251 Americium-241 U 0.064 U -0.0181 pCi/g 137 (0%- 100%)

Uncert: +/-0.113 +/-0.0823 TPU: +/-0.113 +/-0.0823 Bismuth-212 0.887 0.973 pCi/g 21 (0%- 100%)

Uncert: +/-0.313 +/-0.274 TPU: +/-0.313 +/-0.274 Bismuth-214 1.15 1.17 pCi/g 4 (0%- 20%)

Uncert: +/-0.147 +/-0.142 TPU: +/-0.147 +/-0.142 Cesium- 134 UUI 0.00 UUI 0.00 pCi/g 25 (0%- 100%)

Uncert: +/-0.0385 +/-0.0358 TPU: +/-0.0385 +/-0.0358 Cesium- 137 U 0.0288 U 0.0105 pCi/g 78 (0%- 100%)

Uncert: +/-0.0259 +/-0.0211 TPU: +/-0.0259 +/-0.0211 Cobalt-60 u 0.0191 U 0.00611 pCi/g 18 (0%- 100%)

Uncert: +/-0.0235 +/-0.0196 TPU: +/-0.0235 +/-0.0196 Europium- 152 u -0.0115 U -0.0143 pCi/g 1550 (0%- 100%)

Uncert: +/-0.0595 +/-0.0523 TPU: +/-0.0595 +/-0.0523 Europium- 154 u -0.0146 U -0.0672 pCi/g 515 (0%- 100%)

Uncert: +/-0.0717 +/-0.0591 TPU: +/-0.0717 +/-0.0591 Europium-155 U 0.0293 UUI 0.00 pCi/g 153 (0%- 100%)

Uncert: +/-0.0678 +/-0.100 TPU: +/-0.0678 +/-0.100 Lead-212 1.62 1.68 pCi/g 5 (0% - 20%)

Uncert: +/-0.145 +/-0.148 TPU: +/-0.145 +/-0.148 Lead-214 1.36 1.39 pCi/g 6 (0% - 20%)

Uncert: +/-0.154 +/-0.153 TPU: +/-0.154 +/-0.153 Manganese-54 U 0.0112 U 0.0321 pCi/g 282 (0%- 100%)

Uncert: +/-0.0236 +/-0.0318 TPU: +/-0.0236 +/-0.0318 Niobium-94 U -0.00247 U 0.0167 pCi/g 54 (0%- 100%)

Uncert: +/-0.0192 +/-0.0171 TPU: +/-0.0192 +/-0.0171 Potassium-40 11.3 10.7 pCi/g 9 (0%- 20%)

Uncert: +/-1.05 +/-0.964 TPU: +/-1.05 +/-0.964 Radium-226 1.15 1.17 pCi/g 4 (0%- 100%)

Uncert: +/-0.147 +/-0.142 TPU: +/-0.147 +/-0.142 Silver- 108m U -0.000679 U 0.0103 pCi/g 19 (0%- 100%)

Uncert: +/-0.0191 +/-0.017 72

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162485 Page 4 of 9 Parmname NOM Sample Qual OC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 529776 TPU: +/-0.0191 +/-0.017 Thallium-208 0.495 0.525 pCi/g 2 (0%- 20%)

Uncert: +/-0.0669 +/-0.0635 TPU: +/-0.0669 +/-0.0635 QC1201092334 LCS Actinium-228 U 0.508 pCi/g 06/03/06 15:39 Uncert: +/-0.559 TPU: +/-0.559 Americium-241 23.4 21.0 pCi/g 90 (75%-125%)

Uncert: +/-3.45 TPU: +/-3.45 Bismuth-212 U 0.361 pCi/g Uncert: +/-1.07 TPU: +/-1.07 Bismuth-214 U 0.102 pCi/g Uncert: +/-0.286 TPU: +/-0.286 Cesium-134 U -0.0467 pCi/g Uncert: +/-0.181 TPU: +/-0.181 Cesium-137 9.64 9.06 pCi/g 94 (75%-125%)

Uncert: +/-0.729 TPU: +/-0.729 Cobalt-60 15.1 15.9 pCi/g 106 (75%-125%)

Uncert: +/-1.18 TPU: +/-1.18 Europium- 152 U -0.0491 pCi/g Uncert: +/-0.335 TPU: +/-0.335 Europium- 154 U -0.249 pCi/g Uncert: +/-0.328 TPU: +/-0.328 Europium- 155 U 0.077 pCi/g Uncert: +/-0.360 TPU: +/-0.360 Lead-212 U -0.0006 I pCi/g Uncert: +/-0.196 TPU: +/-0.196 Lead-214 U 0.0856 pCi/g Uncert: +/-0.227 TPU: +/-0.227 Manganese-54 U -0.0065 pCi/g Uncert: +/-0.133 TPU: +/-0.133 Niobium-94 U 0.101 pCi/g Uncert: +/-0.118 TPU: +/-0.118 Potassium-40 U 1.38 pCi/g 73

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162485 Page 5 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 529776 Uncert: +/-1.23 TPU: +/-1.23 Radium-226 U 0.102 pCi/g (75%-125%)

Uncert: +/-0.286 TPU: +/-0.286 Silver- 108m U 0.0169 pCi/g Uncert: +/-0.119 TPU: +/-0.119 Thallium-208 U 0.0217 pCi/g Uncert: +/-0.131 TPU: +/-0.131 QC1201092332 MB Actinium-228 U 0.0231 pCi/g 06/04/06 20:22 Uncert: +/-0.0503 TPU: +/-0.0503 Americium-241 U -0.0485 pCi/g Uncert: +/-0.0565 TPU: +/-0.0565 Bismuth-212 U 0.100 pCi/g Uncert: +/-0.114 TPU: +/-0.114 Bismuth-214 U -0.00311 pCi/g Uncert: +/-0.0254 TPU: +/-0.0254 Cesium- 134 U 0.00344 pCi/g Uncert: +/-0.0146 TPU: +/-0.0146 Cesium- 137 U 0.0114 pCi/g Uncert: +/-0.0135 TPU: +/-0.0135 Cobalt-60 U 0.00208 pCi/g Uncert: +/-0.0154 TPU: +/-0.0154 Europium- 152 U 0.0236 pCi/g Uncert: +/-0.0367 TPU: +/-0.0367 Europium- 154 U -0.0158 pCi/g Uncert: +/-0.0399 TPU: +/-0.0399 Europium- 155 U 0.00786 pCi/g Uncert: +/-0.0328 TPU: +/-0.0328 Lead-212 U 0.0278 pCi/g Uncert: +/-0.0312 TPU: +/-0.0312 Lead-214 U 0.0263 pci/g Uncert: +/-0.0251 TPU: +/-0.0251 74

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162485 Page 6 of 9 Parmname NOM Samole Oual QC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 529776 Manganese-54 U 0.0016 pCi/g Uncert: +/-0.015 TPU: +1-0.015 Niobium-94 U -0.000762 pCi/g Uncert: +/-/-0.0129 TPU: +/-0.0129 Potassium-40 U 0.145 pCi/g Uncert: +/-0.122 TPU: +/-0.122 Radium-226 U -0.00311 pCi/g Uncert: +/-0.0254 TPU: +/-0.0254 Silver- 108m U -0.00522 pCi/g Uncert: +/-0.0117 TPU: +/-0.0117 Thallium-208 U 0.00116 pCi/g Uncert: +/-0.0158 TPU: +/-0.0158 Rad Gas Flow Batch 535512 QC1201105910 162335018 DUP Strontium-90 U 0.00669 U 0.012 pCi/g 0 (0% - 100%) BXFI 06/06/06 23:16 Uncert: +/-0.00923 +/-0.00902 TPU: +/-0.00923 +/-0.00902 QC1201105912 LCS Strontium-90 1.43 1.19 pCi/g 83 (75%-125%) 06/07/06 10:08 Uncert: +/-0.081 TPU: +/-0.0854 QC1201105909 MB Strontium-90 U 0.0107 pCi/g 06/06/06 23:16 Uncert: +/-0.00663 TPU: +/-0.00664 QC1201105911 162335018 MS Strontium-90 1.54 U 0.00669 1.54 pCi/g 100 (75%-125%) 06/07/06 10:08 Uncert: +/-0.00923 +/-0.107 TPU: +/-0.00923 +/-0.115 Rad Liquid Scintillation Batch 531618 QC1201096632 163173001 DUP Iron-55 U 10.3 U 5.38 pCi/g 0 (0% - 100%) SLNI 05/31/06 12:49 Uncert: +/-20.1 +/-18.0 TPU: +/-20.1 +/-18.1 QC1201096634 LCS Iron-55 437 428 pCi/g 98 (75%-125%) 05/31/06 13:22 Uncert: +/-40.6 TPU: +/-62.3 QC1201096631 MB Iron-55 U 3.58 pCi/g 05/31/06 12:32 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162485 Page 7 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Liquid Scintillation Batch 531618 Uncert: +/-24.7 TPU: +/-24.7 QC1201096633 163173001 MS Iron-55 569 U 10.3 544 pCi/g 96 (75%-125%) 05/31/06 13:05 Uncert: +/-20.1 +/-39.3 TPU: +/-20.1 +/-69.3 Batch 531622 QC1201096645 163173001 DUP Nickel-63 U -6.64 U -5.49 pCi/g 0 (0% - 100%) SLNI 05/28/06 01:38 Uncert: +/-7.30 +/-4.33 TPU: +/-7.31 +/-4.33 QC1201096647 LCS Nickel-63 362 301 pCi/g 83 (75%-125%) 05/28/06 03:40 Uncert: +/-7.49 TPU: +/- 11.1 QC1201096644 MB Nickel-63 U -1.66 pCi/g 05/28/06 00:37 Uncert: +/-3.41 TPU: +/-3.41 QC1201096646 163173001 MS Nickel-63 460 U -6.64 395 pCi/g 86 (75%-125%) 05/28/06 02:39 Uncert: +/-7.30 +/-9.22 TPU: +/-7.31 +/-14.9 Batch 531704 QC1201096868 162583001 DUP Technetium-99 U 0.161 U 0.239 pCi/g 0 (0% - 100%) SXEI 05/31/06 00:27 Uncert: +/-0.254 +/-0.273 TPU: +/-0.255 +/-0.273 QC1201096870 LCS Technetium-99 12.5 11.1 pCi/g 89 (75%-125%) 05/31/06 01:00 Uncert: +/-0.474 TPU: +/-0.545 QC1201096867 MB Technetium-99 U 0.163 pCi/g 05/31/06 00:11 Uncert: +/-0.214 TPU: +/-0.214 QC1201096869 162583001 MS Technetium-99 13.1 U 0.161 11.6 pCi/g 89 (75%-125%) 05/31/06 00:44 Uncert: +/-0.254 +/-0.583 TPU: +/-0.255 +/-0.649 Batch 531705 QC1201096878 162583001 DUP Tritium U 1.17 U 6.01 pCi/g 0 (0% - 100%) NXPI 05/28/06 09:10 Uncert: +/-4.09 +/-4.70 TPU: +/-4.09 +/-4.70 QC1201096880 LCS Tritium 41.4 44.8 pCi/g 108 (75%-125%) 05/28/06 10:14 Uncert: +/-5.68 TPU: +/-5.73 76

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com QC Summary Workorder: 162485 Page 8 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Liquid Scintillation Batch 531705 QC1201096877 MB Tritium U 0.0641 pCi/g 06/03/06 05:11 Uncert: +/-0.533 TPU: +/-0.533 QC1201096879 162583001 MS Tritium 45.7 U 1.17 52.3 pCi/g 114 (75%-125%) 05/28/06 09:42 Uncert: +/-4.09 +/-6.44 TPU: +/-4.09 +/-6.50 Batch 534984 QC0201104746 163173001 DUP Carbon- 14 U 0.00714 U 0.00246 pCi/g 0 (0%- 100%) ATH2 06/05/06 03:00 Uncert: +/-0.0996 +/-0.103 TPU: +/-0.0996 +/-0.103 QC1201104748 LCS Carbon- 14 12.1 11.3 pCi/g 94 (75%-125%) 06/05/06 05:20 Uncert: +/-0.855 TPU: +/-0.873 QC1201104745 MB Carbon-14 U -0.0368 pCi/g 06/05/06 00:57 Uncert: +/-0.101 TPU: +/-0.101 QC1201104747 163173001 MS Carbon- 14 12.9 U 0.00714 12.1 pCi/g 94 (75%-125%) 06/05/06 05:02 Uncert: +/-0.0996 +/-0.917 TPU: +/-0.0996 +/-0.936 Batch 535483 QC0201105873 162335018 DUP Iron-55 U -15.8 U 0.079 pCi/g 0 (0%-100%) AFI 06/05/06 17:00 Uncert: +/-16.9 +/-20.4 TP1J: +/-17.0 +/-20.4 QCI201105875 LCS Iron-55 485 492 pCi/g 101 (75%-125%) 06/05/06 17:33 Uncert: +/-39.7 TPU: +/-61.9 QC1201105872 MB Iron-55 U 5.04 pCi/g 06/05/06 16:43 Uncert: +/-22.8 TPU: +/-22.8 QC1201105874 162335018 MS Iron-55 655 U -15.8 628 pCi/g 96 (75%-125%) 06/05/06 17:16 Uncert: +/-16.9 +/-39.8 TPU: +/-17.0 +/-71.2 Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported 77

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 162485 Page 9 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time

> Result is greater than value reported A The TIC is a suspected aldol-condensation product BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of-+/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

78

Table of Contents General Narrative ................................................................... I Chain of Custody And Supporting Dpcumentation ........... 5 Radiological Analysis ........................................................... 12 Sample Data Summary ....................................................... 18 Q uality C ontrol D ata .......................................................... . 60

General Narrative I.

CASE NARRATIVE For CONNECTICUT YANKEE RE: Soil PO# 002332 Work Order: 170256 SDG: MSR #06-1160 September 6, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:

2040 Savage Road' Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina on August 25, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.

The laboratory received the following sample(s):

Sample ID Client Sample ID 170256001 9106-0006-005A 170256002 9106-0006-005B 170256003 9106-0006-005C 170256004 9106-0006-005D 170256005 9106-0005-0IOA 170256006 9106-0005-0IOB 170256007 9106-0005-OIOC 170256008 9106-0005-OIOD 170256009 9106-0014-033A GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

P.O. Box 30712 - Charleston, SC 29417 - 2040 Savage Road (29407)

Phone (843) 556-8171 ° Fax 243) 766-1178 - www.gel.com

170256010 9106-0014-033B 170256011 9106-0014-033C 170256012 9106-0014-033D 170256013 9106-0004-013A 170256014 9106-0004-013B 170256015 9106-0004-013C 170256016 9106-0004-013D 170256017 9106-0004-005A 170256018 9106-0004-005B 170256019 9106-0004-005C 170256020 9106-0004-005D Items of Note:

There are no items of note.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engir eering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analyticail parameter.

Analytical Request:

Twenty soil samples were analyzed for FSSGAM and Sr-90.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically aid for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager orla designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP INC. T P.O. Box 30712 - Charleston, SC 29417 - 2040 Savage Road (29407)

Phone (843) 556-8171 - Fax 43) 766-1178 - www.gel.com

List of current GEL Certifications as of 06 September 2006 State Certification Alaska UST-062 Arizona AZO668 Arkansas 88-0651 CLIA 42D0904046 California 0115 ICA

,-.Colorado GenEngLabs

-- Connecticut PH-0169 Dept. of Navy _ - NFESC 413.

EPA W6-1J . .

Florida/NELAP E87156 Georgia E87156 (FL1NELAP)

Idaho N/A Illinois 200029 Indiana C-SC-0I Kansas E-10332 Kentucky 90129 Maryland 270 Massachusetts M-SCO12

-- Michigan Nevada SC New Jersey SC002 New York 11501

~1 North Carolina 233 North Carolina Drinking W 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania 68-48-5_

South Carolina 10120001/10585001/1 0120002 Tennessee -02934 Texas TX213-2006A U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah .. .

-8037697376 GEL Vermont N/A Virginia 00151 Washington C223 4

Chain of Custody And Supporting Documentation 5

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00511 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 0 843 556 8171. Attn. Cheryl Jones cc Priority: E] 30 D. 0 14 D. [] 7 D. Container I/

Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comnment, Preservation Lab Sample ID 9106-0006-OOSA 8/8/06 14:35 SE C BP X X Transferred from COC # 2006-00488 9106-0006-005B 8/8/06 15:08 SE C BP X X Transferred from COC # 2006-00488 9106-0006-005C 8/9/06 07:46 SE C BP X X Transferred from COC # 2006-00307 9106-0006-005D 8/9/06 08:18 SE C BP X X Transferred from COC H2006-00307 SSWP#NA SLTP QA El Radwaste QA 13 Non QA Samples Shipped Via: Internal Container NOTES: PO#: 002332 MSR#: 06-11iO [ Fed Ex Temp.: ___ Deg. C mUps

[]Hand Custody Sealed?

YD- NO]

1) Relinquished By Date/Time 2) Rec *ved By Date/Time Custody Seal Intact?

13 Other

3) Relinquished By Date/Time 4) 4ceived By *-Date/Time YE NO Bill of Lading #

V7-OO 4*1 f 64 L

V.

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major (1 Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00512 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddarn Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 ,

843 556 8171. Attn. Cheryl Jones rA Priority: [] 30 D. M 14 D. [] 7 D. Container Sample Size.

Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0005-OIOA 8/9/06 09:03 SE C BP X X Transferred from COO # 2006-00489 9106-0005-0IOB 8/9/06 09:33 SE C BP X X Transferred from COC # 2006-00489 9106-0005-01OC 8/9/06 10:04 SE C BP X X Transferred from COC #2006-00489 9106-0005-010D 8/9/06 10:56 SE C BP x x Transferred from COC # 2006-00489 NOTES: PO #: 002332 MSR #: 06- IlS0 SSWP# NA SLTP QA El Radwaste QA El Non QA Samples Shipped Via: Internal Container

[ Fed Ex Temp.: __ Deg. C E] ups Custody Sealed?

El Hand Yc* No

1) Relinquished By DatI/T ime 2) ceivedB D te/Time Custody Seal Intact?

of- Z44-0 1'71t34-0 El Other

3) Relinquished By Date/Time 49eceived By /DateTne YIJ NO Bill of Lading #

ýqO 4 J63

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-00 1 Major ,

Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00513 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Cn Priority: E] 30 D. 0 14 D. Li 7 D. Container Sample Size-Media Type &Type Comment, Preservation Lab Sample ID Sample Designation Date Time Code Code Code , C 9106-0014-033A 8/11/06 07:58 SE C BP X X Transferred from COC # 2006-00493 39106-0014-033B 8/I 1/06 08:24 SE C BP X X Transferred from COC # 2006-00493 9106-0014-033C 8/11/06 08:45 SE C BP X x Transferred from COC # 2006-00493 9106-0014-033D 8/11/06 09:16 SE C BP X X Transferred from COC # 2006-00493 NOTES: PO #: 002332 MSR #: 06-1160 SSWP# NA SLTP QA [] Radwaste QA [] Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.: _ Deg. C El UPS Li Hand . .. _Custody Sealed?

YO NO

1) Relinquished By Da~e/Time 2) ived By Date/Time Custody Seal Intact?

Li Other

3) Relinquished By Date/Time 4) l ed DBy ate/Time Yo NO]

Bill of Lading #

9?wo 40q 6*44'

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00520 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-3924 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones r c C/

Priority: [] 30 D. 1Z 14 D. E] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0004-013A 8/9/06 12:53 SE C BP X X Transferred from COC 2006-00490 9106-0004-013B 8/9/06 13:27 SE C BP X X Transferred from COC 2006-00490 "9106-0004-013C 8/9/06 13:57 SE C BP x x Transferred from COC 2006-00490 9106-0004-013D 8/9/06 14:28 SE C BP X X Transferred from COC 2006-00490 9106-0004-005A 8/9/06 14:58 SE C BP X X Transferred from COC 2006-0G490 91 06-0004-005B 8/10/06 07:41 SE C BP X X Transferred from COC 2006-00491 9106-0004-005C 8/10/06 08:09 SE C BP X X Transferred from COC 2006-00491 9106-0004-005D 8/10/06 08:49 SE C BP X X Transferred from COC 2006-00491 NOTES: PO #: 002332 MSR#: 06- 1) C' SSWP# NA SLTP QA ] Radwaste QA E Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.: _ Deg. C

[3 UPS

[] Hand Custody Sealed?

YVE ND l)-Relinquished By Date/,ime 2) Re ived By - Date/Time Custody Seal Intact?

LI Other

3) Relinquished By Date/Time 4&ceived By Date/Time YD NO Bill of Lading #

7900 4 67 61444f

Connecticut Yankee Statement of Work for Analytical Lab Services -CY-isc-sow-001 CY-ISC-SOW-OOl Figure 1. Sample Checkin List Date/Time Received:

SDG#: Y 0 W Work Order Number:b,  :'..O* j.i j Shipping Cdatainer ID:7Y&D A43 4y Chain of Custody#

I. Custody Seals. on shipping container intact?.. :Yes I.j1~o I(I

2. Custody Seals dated and signed? Yes A' [Iý

3. Chain-of-Custody record present? " YesJ-M H[jb

.4- Cooler temperature

5. Vermiculite/packing materials is: -'*

ýWet 6.' -Numberof samples in shipping container: AZ,

7. Sample holding times exceeded?

Yes

8. Samples have:'

Sl.hazard labels

_.:.:fwtody seals . appropriate Sample labels H

9. Samples are-

. 'ood condition -leaking "broken .' have air bubbles

10. Were any anomalies identified in sample receipt? , ' Yes [ ] No [-r,

11. Description of anomalies (include sample numbers):

Telephoned 10

Connecticut Yankee Statement of Work for Analytical Lab Services L -CY-ISC-SOW-001 LCY-ISC-SOW-OOl Figure 1. Sample Check-in List Date/Time Recved:.

SDG#: I Work Order Nurnber: -

Shipping Cdntainer ID: 0 I hi of Custody # Zetý 6 - taQ

1. Custody Seals od shipping container intact?. Yes t.-jr 1N

2. Custody Seals dated and signed? Yes -1,, 0o ["

3. Chain-of-Custody record present? Yes K,,N"o

4. Cooler temperature ,,2 "*

5. Vermiculite/packing materials is: Wet ]

6' Number of samples in shipping container: _ _ _ __.

2

7. Sample holding times exceeded? Yes L.-]" o [I]

!I-I5

-8. Samples have:

.- '.." hazard labels

-6ustody seals -appropriate sample labels

9. Samples are:

. -in goqd condition hav aibng

&-e.Z roke -

• have air bubbles 10.

11.

Were any anomalies identified "i sample receipt?

.Description ofanomalies, (include sample numbers): ."z*

Yes

- */t frNo

. ~ -O i

/ I.La y

/"i, 11

RADIOLOGICAL ANALYSIS 12

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 170256 Method/Analysis Information Product: Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Analytical Method: EML HASL 300, 4.5.2.3 Prep Method: Dry Soil Prep Analytical Batch Number: 563436 Prep Batch Number: 562444 Sample ID Client ID 170256001 9106-0006-005A 170256002 9106-0006-005B 170256003 9106-0006-005C 170256004 9106-0006-005D 170256005 9106-0005-01OA 170256006 9106-0005-OIOB 170256007 9106-0005-OIOC 170256008 9106-0005-OIOD 170256009 9106-0014-033A 170256010 9106-0014-033B 170256011 9106-0014-033C 170256012 9106-0014-033D 170256013 9106-0004-013A 170256014 9106-0004-013B 170256015 9106-0004-013C 170256016 9106-0004-013D 170256017 9106-0004-005A 170256018 9106-0004-005B 170256019 9106-0004-005C 170256020 9106-0004-005D 1201171525 Method Blank (MB) 1201171526 170256001(9106-0006-005A) Sample Duplicate (DUP) 1201171527 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this 13

narrative has been analyzed in accordance with GL-RAD-A-013 REV# 12.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (Q0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 170256001 (9106-0006-005A).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 170256007 (9106-0005-010C), 170256016 (9106-0004-013D) and 170256019 (9106-0004-005C) were recounted due to high MDAs.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information 14

Qualifier Reason Analyte Sample UI Data rejected due to high counting uncertainty Bismuth-212 170256009 UI Data rejected due to interference. Europium- 155 170256003 170256009 170256019 170256020 U' Data rejected due to low abundance. Bismuth-214 170256008 Cesium- 134 170256005 170256007 170256008 170256012 170256013 170256019 1201171526 Europium- 155 170256018 Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 562563 Prep Batch Number: 562478 Dry Soil Prep GL-RAD-A-021 Batch Number: 562444 15

Sample ID Client ID 170256001 9106-0006-005A 170256002 9106-0006-005B 170256003 9106-0006-005C 170256004 9106-0006-005D 170256005 9106-0005-01OA 170256006 9106-0005-010B 170256007 9106-0005-OIOC 170256008 9106-0005-OIOD 170256009 9106-0014-033A 170256010 9106-0014-033B 170256011 9106-0014-033C 170256012 9106-0014-033D 170256013 9106-0004-013A 170256014 9106-0004-013B 170256015 9106-0004-013C 170256016 9106-0004-013D 170256017 9106-0004-005A 170256018 9106-0004-005B 170256019 9106-0004-005C 170256020 9106-0004-005D 1201169421 Method Blank (MB) 1201169422 170256002(9106-0006-005B) Sample Duplicate (DUP) 1201169423 170256002(9106-0006-005B) Matrix Spike (MS) 1201169424 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 10.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 170256002 (9106-0006-005B).

16

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples were recounted due to low/high recovery.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

Reviewer/Date: I** 6 IS/*:L 17

SAMPLE DATA

SUMMARY

18

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Report for YANKOO Connecticut Yankee Atomic Power Co.

Client SDG: MSR#06-1160 GEL Work Order: 170256 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by 19

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005A Proiect: YANKO 1204 Sample ID: 170256001 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 15.8%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.966 +/-0.192 0.0743 +/-0.192 0.149 pCi/g MJHI 09/01/06 1057 563436 1 Americium-241 U 0.0375 +/-0.0387 0.0329 +/-0.0387 0.0658 pCi/g Bismuth-212 0.366 +/-0.306 0.175 +/-0.306 0.350 pCi/g Bismuth-214 0.650 +/-0.135 0.042 +/-0.135 0.0839 pCi/g Cesium-134 U 0.0366 +/ 0.0355 0.0288 +1-0.0355 0.0576 pCi/g Cesium-137 0.0666 +1-0.0355 0.0236 +1-0.0355 0.0472 pCi/g Cobalt-60 0.104 +1-0.0726 0.0286 +/-0.0726 0.0573 pCi/g Europium-152 U 0.00636 +1-0.0728 0.0538 +/-0.0728 0.108 pCi/g Europium- 154 U -0.0788 +1-0.0938 0.0718 +/-0.0938 0.143 pCi/g Europium-155 U 0.0672 +1-0.0554 0.0518 +/-0.0554 0.104 pCi/g Lead-212 0.871 +1-0.0971 0.0305 +/-0.0971 0.061 pCi/g Lead-214 0.727 +/-0.105 0.0379 +/-0.105 0.0757 pCi/g Manganese-54 U -0.00916 +/-0.0319 0.0232 +/-0.0319 0.0465 pCi/g Niobium-94 U 0.0101 +/-0.0244 0.0223 +/-0.0244 0.0445 pCi/g Potassium-40 11.3 +/-0.986 0.201 +/-0.986 0.403 pCi/g Radium-226 0.650 +/-0.135 0.042 +/-0.135 0.0839 pCi/g Silver-108m U -0.0067 +/-0.0208 0.018 +/-0.0208 0.036 pCi/g Thallium-208 0.283 +/-0.0618 0.0212 +/-0.0618 0.0423 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.0254 +/-0.0193 0.0126 +/-0.0193 0.0298 pCi/g KSDI 09/07/06 1742 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 20

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005A Project: YANK01204 Sample ID: 170256001 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 96 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

21

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005B Project: YANK01204 Sample ID: 170256002 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 14.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSSGAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.606 +/-0.152 0.0599 +/-0.152 0.131 pCi/g MJHI 09/01/06 1220 563436 1 Americium-241 U 0.101 +/-0.114 0.0861 +/-0.114 0.179 pCi/g Bismuth-212 0.685 +/-0.232 0.134 +/-0.232 0.290 pCi/g Bismuth-214 0.435 +/-0.0852 0.0332 +/-0.0852 0.0708 pCi/g Cesium-134 U 0.0313 +/-0.0286 0.0238 +/-0.0286 0.0507 pCi/g Cesium-137 0.114 +/-0.0348 0.0206 +/-0.0348 0.0438 pCi/g Cobalt-60 0.436 +/-0.0586 0.0151 +/-0.0586 0.0345 pCi/g Europium-152 U -0.0448 +/-0.0525 0.0416 +/-0.0525 0.0882 pCi/g Europium- 154 U -0.0186 +/-0.0685 0.0562 +/-0.0685 0.124 pCi/g Europium-155 U 0.0423 +/-0.0579 0.0552 +/-0.0579 0.114 pCi/g Lead-212 0.643 +/-0.0623 0.0268 +/-0.0623 0.056 pCi/g Lead-214 0.462 +/-0.0885 0.033 +/-0.0885 0.0696 pCi/g Manganese-54 U -0.0167 +/-0.0261 0.0174 +/-0.0261 0.0377 pCi/g Niobium-94 U 0.00909 +/-0.0195 0.0173 +/-0.0195 0.0369 pCi/g Potassium-40 11.1 +/-0.983 0.179 +/-0.983 0.399 pCi/g Radium-226 0.435 +/-0.0852 0.0332 +/-0.0852 0.0708 pCi/g Silver-108m U -0.00194 +/-0.0168 0.0149 +/-0.0168 0.0317 pCi/g Thallium-208 0.243 +/-0.0457 0.0176 +/-0.0457 0.0377 pCi/g Rad Gas Flow Proportional Counting GFPC,S90, solid-ALL FSS Strontium-90 U 0.00501 +/-0.0149 0.0117 +/-0.0149 0.0278 pCi/g KSD1 09/07/06 1742 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 22

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005B Proiect: YANKO 1204 Sample ID: 170256002 Client Vol. Recv.: YANKOOI ID:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 101 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

23

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005C Proiect: YANKO 1204 Sample ID: 170256003 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 31.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.07 +/-0.284 0.101 +/-0.284 0.215 pCi/g MJH1 09/01/06 1221 563436 1 Americium-241 U 0.0251 +/-0.0367 0.0332 +/-0.0367 0.0683 pCi/g Bismuth-212 0.684 +/-/-0.424 0.178 +/-0.424 0.383 pCi/g Bismuth-214 0.673 +/-0.121 0.0445 +/-0.121 0.0947 pCi/g Cesium-134 U 0.0516 -+/-0.0548 0.0344 +/-0.0548 0.0729 pCi/g Cesium-137 0.317 +/-0.0544 0.0247 +/-0.0544 0.0528 pCi/g Cobalt-60 0.821 -+/-0.09l I 0.0294 +/-0.0911 0.064 pCi/g Europium-152 U -0.049 -+/-0.0652 0.0539 +/-0.0652 0.114 pCi/g Europium-154 U 0.0883 -+/-0.0913 0.0839 +/-0.0913 0.182 pCi/g Europium-155 UI 0.00 -F/-0.0926 0.0506 +/-0.0926 0.105 pCi/g Lead-212 1.01 -ý/-0.08 19 0.0329 +/-0.0819 0.0685 pCi/g Lead-214 0.828 +/-0.117 0.0423 +/-0.117 0.089 pCi/g Manganese-54 U -0.0228 ý/-0.0296 0.0238 +/-0.0296 0.0513 pCi/g Niobium-94 U -0.0353 ý/-0.0279 0.0205 +/-0.0279 0.044 pCi/g Potassium-40 12.4 +1-1.15 0.189 +1-1.15 0.431 pCi/g Radium-226 0.673 +/-0.121 0.0445 +/-0.121 0.0947 pCi/g Silver-108m U 0.00475 F/-0.0263 0.0227 +/-0.0263 0.0477 pCi/g Thallium-208 0.382 F/-0.0567 0.0242 +/-0.0567 0.0515 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.00738 +/-0.0142 0.0107 +/-0.0142 0.0255 pCi/g KSDI 09/07/06 1745 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 24

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005C Project: YANKO 1204 Sample ID: 170256003 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 104 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria Result is less than value reported Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

25

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005D Project: YANK01204 Sample ID: 170256004 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 28.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.01 +/-0.197 0.0659 +/-0.197 0.143 pCi/g MJH1 09/01/06 1221 563436 1 Americium-241 U 0.0605 +/-0.132 0.088 +/-0.132 0.182 pCi/g Bismuth-212 0.534 +/-0.328 0.168 +/-0.328 0.358 pCi/g Bismuth-214 0.594 +/-0.105 0.0384 +/-0.105 0.0813 pCi/g Cesium-134 U 0.0478 +/-0.046 0.0253 +/-0.046 0.0537 pCi/g Cesium-137 0.103 +/-0.0401 0.0181 +/-0.0401 0.0389 pCi/g Cobalt-60 0.148 +/-0.0644 0.0204 +/-0.0644 0.045 pCi/g Europium-152 U 0.00143 +/-0.0589 0.0517 +/-0.0589 0.109 pCi/g Europium-154 U 0.0154 +/-0.0766 0.0653 +/-0.0766 0.142 pCi/g Europium-155 U 0.0625 +/-0.0643 0.0586 +/-0.0643 0.121 pCi/g Lead-212 0.900 +/-0.0831 0.0345 +/-0.0831 0.0714 pCi/g Lead-214 0.854 +/-0.106 0.0372 +/-0.106 0.078 pCi/g Manganese-54 U -0.013 +/-0.0244 0.0203 +/-0.0244 0.0434 pCi/g Niobium-94 U 0.0144 +/-0.022 0.0192 +/-0.022 0.0408 pCi/g Potassium-40 11.6 +/-0.886 0.177 +/-0.886 0.396 pCi/g Radium-226 0.594 +1-0.105 0.0384 +/-0.105 0.0813 pCi/g Silver-108m U 0.0118 +/-0.0187 0.0169 +/-0.0187 0.0357 pCi/g Thallium-208 0.310 +/-0.0591 0.0199 +/-0.0591 0.0422 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.000446 +/-0.0198 0.0166 +/-0.0198 0.0376 pCi/g KSDI 09/07/06 1740 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 26

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005D Project: YANK01204 Sample ID: 170256004 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 50 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

27

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010A Project: YANKO 1204 Sample ID: 170256005 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 60.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.22 +/-0.394 0.120 +/-0.394 0.255 pCi/g MJH1I 09/01/06 1221 563436 1 Americium-241 U 0.0503 +/-0.0522 0.0424 +/-0.0522 0.0872 pCi/g Bismuth-212 0.628 +/-0.547 0.277 +/-0.547 0.584 pCi/g Bismuth-214 0.834 +/-0.160 0.0633 +/-0.160 0.133 pCi/g Cesium-134 UI 0.00 +/-0.0832 0.0429 +/-0.0832 0.0903 pCi/g Cesium-137 U 0.0463 +/-0.0542 0.0333 +/-0.0542 0.0703 pCi/g Cobalt-60 U 0.077 +/-0.0516 0.0472 +/-0.0516 0.100 pCi/g Europium-152 U 0.00822 +/-0.0958 0.0766 +/-0.0958 0.160 pCi/g Europium-154 U-0.000512 +/-0.129 0.0917 +/-0.129 0.199 pCi/g Europium-155 U 0.0659 +/-0.115 0.0674 +/-0.115 0.139 pCi/g Lead-212 0.933 +/-0.111 0.0593 +/-0.111 0.122 pCi/g Lead-214 0.787 +/-0.146 0.0602 +/-0.146 0.125 pCi/g Manganese-54 U -0.0199 +/-0.0442 0.0342 +/-0.0442 0.0725 pCi/g Niobium-94 U -0.0359 +/-0.0364 0.0275 +/-0.0364 0.0583 pCi/g Potassium-40 20.0 +/-1.50 0.288 +/-1.50 0.634 pCi/g Radium-226 0.834 +/-0.160 0.0633 +/-0.160 0.133 pCi/g Silver-108m U -0.00415 +/-0.0338 0.0282 +/-0.0338 0.0591 pCi/g Thallium-208 0.347 +/-0.0918 0.0332 +/-0.0918 0.0698 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.00442 +/-0.0146 0.0116 +/-0.0146 0.0274 pCi/g KSDI 09/07/06 1745 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 28

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010A Proiect: YANKO 1204 Sample ID: 170256005 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 103 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

29

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-0IOB Proiect: YANKO 1204 Sample ID: 170256006 Client ID: YANKOO0 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 61.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.10 +/-0.245 0.0778 +/-0.245 0.168 pCi/g MJHI 09/01/06 1221 563436 1 Americium-241 U -0.00576 +/-0.0366 0.0263 +/-0.0366 0.0543 pCi/g Bismuth-212 0.760 +/-0.351 0.189 +/-0.351 0.402 pCi/g Bismuth-214 0.576 +/-0.139 0.0442 +/-0.139 0.0936 pCi/g Cesium-134 U 0.0332 +/-0.0438 0.0314 +/-0.0438 0.0665 pCi/g Cesium-137 0.0908 +/-0.0468 0.0231 +/-0.0468 0.0493 pCi/g Cobalt-60 0.115 +/-0.0522 0.0225 +/-0.0522 0.0499 pCi/g Europium-152 U 0.00833 +/-0.068 0.0546 +/-0.068 0.115 pCi/g Europium-154 U -0.0828 +/-0.106 0.0808 +/-0.106 0.175 pCi/g Europium-155 U 0.0871 +/-0.0591 0.0504 +/-0.0591 0.104 pCi/g Lead-212 1.08 +/-0.0778 0.0306 +/-0.0778 0.0636 pCi/g Lead-214 0.812 +/-0.0928 0.0385 +/-0.0928 0.081 pCi/g Manganese-54 U 0.0145 +/-0.0313 0.0262 +/-0.0313 0.0557 pCi/g Niobium-94 U 0.00876 +/-0.0271 0.0226 +/-0.0271 0.0479 pCi/g Potassium-40 19.3 +/-1.35 0.236 +/- 1.35 0.521 pCi/g Radium-226 0.576 +/-0.139 0.0442 +/-0.139 0.0936 pCi/g Silver-108m U -0.00887 +/-0.0232 0.0191 +/-0.0232 0.0403 pCi/g Thallium-208 0.282 +/-0.0641 0.0224 +/-0.0641 0.0475 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U -0.00561 +/-0.0185 0.0162 +/-0.0185 0.0368 pCi/g KSDI 09/07/06 1746 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 30

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010B Proiect: YANK01204 Sample ID: 170256006 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 89 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

31

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010C Project: YANKO 1204 Sample ID: 170256007 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 49.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GainmaSolid-FSSGAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.05 +/-0.196 0.0698 +/-0.196 0.148 pCi/g MJH1 09/05/06 2124 563436 1 Americium-241 U 0.00111 +/-0.108 0.0862 +/-0.108 0.177 pCi/g Bismuth-212 0.539 +/-0.392 0.142 +/-0.392 0.300 pCi/g Bismuth-214 0.626 +/-0.101 0.0371 +/-0.101 0.0775 pCi/g Cesium-134 UI 0.00 +/-0.0318 0.025 +/-0.0318 0.0524 pCi/g Cesium- 137 0.192 +/-0.0408 0.0197 +/-0.0408 0.0414 pCi/g Cobalt-60 0.522 +/-0.0639 0.0211 +/-0.0639 0.0453 pCi/g Europium-152 U -0.0379 +/-0.0596 0.0464 +/-0.0596 0.0966 pCi/g Europium-154 U -0.0318 +/-0.0732 0.0585 +/-0.0732 0.126 pCi/g Europium-155 U 0.0641 +/-0.0925 0.0488 +/-0.0925 0.100 pCi/g Lead-212 1.14 +/-0.0696 0.0264 +/-0.0696 0.0544 pCi/g Lead-214 0.753 +/-0.0911 0.0337 +/-0.0911 0.070 pCi/g Manganese-54 U 0.0134 +/-0.0217 0.0193 +/-0.0217 0.0408 pCi/g Niobium-94 U 0.0073 +/-0.0216 0.0181 +/-0.0216 0.038 pCi/g Potassium-40 17.9 +/-1.02 0.190 +/-1.02 0.412 pCi/g Radium-226 0.626 +/-0.101 0.0371 +/-0.101 0.0775 pCi/g Silver-108m U 0.00496 +/-0.0191 0.0165 +/-0.0191 0.0344 pCi/g Thallium-208 0.354 +/-0.0504 0.0183 +/-0.0504 0.0384 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.00471 +/-0.0144 0.0114 +/-0.0145 0.027 pCi/g KSDI 09/07/06 1758 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 32

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010C Proiect: YANKO 1204 Sample ID: 170256007 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, SrO0, solid-ALL FSS 101 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

33

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OIOD Project: YANKO 1204 Sample ID: 170256008 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 58.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamnnia,Solid-FSSGAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.920 +/-0.431 0.163 +/-0.431 0.345 pCi/g MJHI 09/01/06 1222 563436 1 Americium-241 U 0.159 +/-0.0868 0.0423 +/-0.0868 0.0871 pCi/g Bismuth-212 0.975 +/-0.615 0.310 +/-0.615 0.654 pCi/g Bismuth-214 U! 0.00 +/-0.170 0.126 +/-0.170 0.259 pCi/g Cesium-134 UI 0.00 +/-0.0619 0.0563 +/-0.0619 0.118 pCi/g Cesium- 137 0.630 +1-0.105 0.037 +/-0.105 0.0784 pCi/g Cobalt-60 2.24 +/-0.161 0.0361 +/-0.161 0.0793 pCi/g Europium-152 U 0.0801 +/-0.100 0.0874 +/-0.100 0.182 pCi/g Europium-154 U 0.159 +/-0.180 0.124 +/-0.180 0.267 pCi/g Europium-155 U 0.0923 +/-0.117 0.0649 +/-0.117 0.134 pCi/g Lead-212 1.10 +/-0.108 0.0414 +/-0.108 0.086 pCi/g Lead-214 0.707 +/-0.194 0.0578 +/-0.194 0.121 pCi/g Manganese-54 U 0.0291 +1-0.050 0.0419 +1-0.050 0.0886 pCi/g Niobium-94 U 0.0114 +/-0.0446 0.0367 +/-0.0446 0.0774 pCi/g Potassium-40 16.4 +/-1.57 0.341 +/-1.57 0.753 pCi/g Radium-226 0.761 +/-0.170 0.0744 +/-0.170 0.156 pCi/g Silver-108m U 0.00643 +/-0.0377 0.0316 +/-0.0377 0.0662 pCi/g Thallium-208 0.396 +/-0.103 0.0362 +/-0.103 0.0763 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.0219 +/-0.0196 0.0135 +/-0.0196 0.0315 pCi/g KSDI 09/07/06 1805 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description.

I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 34

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010D Project: YANK01204 Sample ID: 170256008 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 97 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

35

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033A Proiect: YANK01204 Sample ID: 170256009 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 1 I-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 26.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSSGAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.28 +/-0.272 0.0796 +/-0.272 0.171 pCi/g MJH1 09/01/06 1223 563436 1 Americium-241 U 0.0199 +/-0.0632 0.0541 +/-0.0632 0.112 pCi/g Bismuth-212 UI 0.00 +/-0.484 0.171 +/-0.484 0.363 pCi/g Bismuth-214 0.920 +/-0.139 0.0421 +/-0.139 0.089 pCi/g Cesium-134 U 0.0188 +/-0.0338 0.0298 +/-0.0338 0.0628 pCi/g Cesium-137 0.709 +/-0.0983 0.0246 +/-0.0983 0.0519 pCi/g Cobalt-60 0.697 +/-0.0935 0.0267 +/-0.0935 0.0577 pCi/g Europium-152 U -0.0119 +/-0.0643 0.0538 +/-0.0643 0.113 pCi/g Europium-154 U 0.0763 +/-0.0741 0.0675 +/-0.0741 0.147 pCi/g Europium-155 UI 0.00 +/-0.0951 0.052 +/-0.0951 0.108 pCi/g Lead-212 1.13 +/-0.134 0.0457 +/-0.134 0.0938 pCi/g Lead-214 1.04 +/-0.151 0.0416 +1-0.151 0.0871 pCi/g Manganese-54 U -0.0049 +/-0.0275 0.023 +/-0.0275 0.049 pCi/g Niobium-94 U 0.014 +/-0.0236 0.0211 +/-0.0236 0.0446 pCi/g Potassium-40 14.3 +/-1.30 0.185 +/-1.30 0.412 pCi/g Radium-226 0.920 +/-0.139 0.0421 +/-0.139 0.089 pCi/g Silver-108m U3.080E-05 +/-0.0263 0.0202 +/-0.0263 0.0424 pCi/g Thallium-208 0.405 +/-0.066 0.0235 +/-0.066 0.0495 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 0.0366 +/-0.0205 0.0124 +/-0.0205 0.0291 pCi/g KSDI 09/07/06 1807 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 36

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis

.Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033A Project: YANKO 1204 Sample ID: 170256009 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr9O, solid-ALL FSS 99 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria.

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

37

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis

..... i Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033B Proiect: YANKO 1204 Sample ID: 170256010 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 11-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 16.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamnma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.03 +/-0.272 0.113 +/-0.272 0.225 pCi/g MJHI 09/01/06 1559 563436 1 Americium-241 U 0.037 +/-0.0519 0.0353 +/-0.0519 0.0705 pCi/g Bismuth-212 0.897 +/-0.563 0.237 +/-0.563 0.473 pCi/g Bismuth-214 0.681 +/-0.143 0.057 +/-0.143 0.114 pCi/g Cesium-134 U 0.062 +/-0.0748 0.0371 +/-0.0748 0.0742 pCi/g Cesium-137 0.862 +/-0.117 0.0301 +/-0.117 0.0601 pCi/g Cobalt-60 0.944 +/-0.113 0.0281 +/-0.113 0.0562 pCi/g Europium-152 U 0.00733 +/-0.118 0.0695 +/-0.118 0.139 pCi/g Europium-154 U 0.00812 +/-0.115 0.0959 +/-0.115 0.192 pCi/g Europium-155 U 0.0592 +/-0.0677 0.0595 +/-0.0677 0.119 pCi/g Lead-212 0.896 +/-0.109 0.0377 +/-0.109 0.0754 pCi/g Lead-214 0.773 +/-0.141 0.0491 +/-0.141 0.0981 pCi/g Manganese-54 U -0.0465 +/-0.0487 0.032 +/-0.0487 0.0639 pCi/g Niobium-94 U 0.00334 +/-0.0333 0.029 +/-0.0333 0.0579 pCi/g Potassium-40 11.6 +/-1.25 0.247 +/-1.25 0.494 pCi/g Radium-226 0.681 +/-0.143 0.057 +/-0.143 0.114 pCi/g Silver-108m U - 0.00313 +/-0.0324 0.0274 +/-0.0324 0.0548 pCi/g Thallium-208 0.278 +/-0.0682 0.0296 +/-0.0682 0.0592 pCi/g Rad Gas Flow Proportional Counting GFPC,SrOO, solid-ALL FSS Strontium-90 U 0.00794 +/-0.015 0.0113 +/-0.015 0.0268 pCi/g KSD1 09/07/06 1807 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 38

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033B Project: YANKO 1204 Sample ID: 170256010 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 103 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

39

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033C Project: YANK01204 Sample ID: 170256011 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 1 I-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 14.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.841 +/-0.277 0.100 +/-0.277 0.212 pCi/g MJHI 09/01/06 1829 563436 1 Americium-241 U 0.028 +/-0.048 0.0331 +/-0.048 0.068 pCi/g Bismuth-212 0.476 +/-0.345 0.223 +/-0.345 0.468 pCi/g Bismuth-214 0.628 +/-0.128 0.0439 +/-0.128 0.0928 pCi/g Cesium-134 U 0.0398 +/-0.0385 0.0344 +/-0.0385 0.0721 pCi/g Cesium-137 0.609 +/-0.0698 0.0277 +/-0.0698 0.0581 pCi/g Cobalt-60 0.916 +/-0.0989 0.0255 +/-0.0989 0.0552 pCi/g Europium-152 U -0.0803 +/-0.0732 0.0581 +/-0.0732 0.121 pCi/g Europium-154 U -0.0175 +/-0.0895 0.0738 +/-0.0895 0.159 pCi/g Europium- 155 U 0.0335 +/-0.0642 0.0553 +/-0.0642 0.114 pCi/g Lead-212 0.710 +/-0.0819 0.0392 +/-0.0819 0.0808 pCi/g Lead-214 0.810 +/-0.110 0.0428 +/-0.110 0.0895 pCi/g Manganese-54 U -0.0149 +/-0.0338 0.0272 +/-0.0338 0.0575 pCi/g Niobium-94 U -0.00772 +/-0.0304 0.0254 +/-0.0304 0.0533 pCi/g Potassium-40 11.0 +/- 1.00 0.220 +/- 1.00 0.484 pCi/g Radium-226 0.628 +/-0.128 0.0439 +/-0.128 0.0928 pCi/g Silver-108m U 0.0295 +/-0.0254 0.0239 +/-0.0254 0.0499 pCi/g Thallium-208 0.237 +/-0.0761 0.0244 +/-0.0761 0.0513 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U -0.0326 +/-0.013 0.0158 +/-0.013 0.0359 pCi/g KSD1 09/07/06 1842 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 40

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033C Project: YANK01204 Sample ID: 170256011 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 90 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ut Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

41

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033D Project: YANKO 1204 Sample ID: 170256012 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 1 I-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 11.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.800 +/-0.169 0.0584 +/-0.169 0.125 pCi/g MJHI 09/05/06 0531 563436 1 Americium-241 U -0.00757 +/-0.0849 0.0733 +/-0.0849 0.151 pCi/g Bismuth-212 0.514 +/-0.239 0.125 +/-0.239 0.265 pCi/g Bismuth-214 0.496 +/-0.079 0.0289 +/-0.079 0.0614 pCi/g Cesium-134 UI 0.00 +/-0.0333 0.0215 +/-0.0333 0.0454 pCi/g Cesium- 137 0.240 +/-0.0466 0.0172 +/-0.0466 0.0365 pCi/g Cobalt-60 0.329 +/-0.0616 0.0159 +/-0.0616 0.0349 pCi/g Europium-152 U -0.0221 +/-0.047 0.0418 +/-0.047 0.0875 pCi/g Europium-154 U -0.0277 +/-0.0651 0.0444 +/-0.0651 0.0974 pCi/g Europium-155 U 0.0409 +1-0.050 0.0464 +1-0.050 0.0959 pCi/g Lead-212 0.618 +/-0.0549 0.0246 +/-0.0549 0.0511 pCi/g Lead-214 0.582 +/-0.0773 0.0304 +/-0.0773 0.0635 pCi/g Manganese-54 U 0.0209 +/-0.0191 0.0165 +/-0.0191 0.0352 pCi/g Niobium-94 U 0.0124 +/-0.0174 0.0157 +/-0.0174 0.0331 pCi/g Potassium-40 10.8 +/-0.796 0.144 +/-0.796 0.320 pCi/g Radium-226 0.496 +/-0.079 0.0289 +/-0.079 0.0614 pCi/g Silver-108m U -0.00363 +/-0.0168 0.0148 +/-0.0168 0.0312 pCi/g Thallium-208 0.222 +/-0.040 0.0156 +/-0.040 0.033 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.020 +/-0.0174 0.0117 +/-0.0174 0.0276 pCi/g KSDI 09/07/06 1842 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 42

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0014-033D Project: YANK01204 Sample ID: 170256012 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 103 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

43

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013A Proiect: YANKO 1204 Sample ID: 170256013 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 17.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.15 +/-0.162 0.0511 +/-0.162 0.109 pCi/g MJHI 09/01/06 1830 563436 Americium-241 U 0.0596 +/-0.0865 0.0665 +/-0.0865 0.136 pCi/g Bismuth-212 0.731 +/-0.295 0.115 +/-0.295 0.242 pCi/g Bismuth-214 0.959 +/-0.0845 0.0284 +/-0.0845 0.0597 pCi/g Cesium-134 UI 0.00 +/-0.0287 0.0195 +/-0.0287 0.041 pCi/g Cesium-137 U -0.00113 +/-0.0196 0.0162 +/-0.0196 0.034 pCi/g Cobalt-60 U -0.00569 +/-0.0174 0.0139 +/-0.0174 0.0301 pCi/g Europium-152 U -0.0275 +/-0.0539 0.0402 +/-0.0539 0.0837 pCi/g Europium-154 U -0.0292 +/-0.0495 0.0385 +/-0.0495 0.0835 pCi/g Europium-155 U 0.0375 +/-0.0594 0.0534 +/-0.0594 0.110 pCi/g Lead-212 1.19 +/-0.0671 0.0261 +/-0.0671 0.0537 pCi/g Lead-214 1.08 +/-0.090 0.0305 +/-0.090 0.0634 pCi/g Manganese-54 U 0.0199 +/-0.0202 0.0165 +/-0.0202 0.0347 pCi/g Niobium-94 U -6.020E- +/-0.0164 0.0143 +/-0.0164 0.030 pCi/g 05 Potassium-40 14.3 +/-0.771 0.130 +/-0.771 0.283 pCi/g Radium-226 0.959 +/-0.0845 0.0284 +/-0.0845 0.0597 pCi/g Silver-108m U -0.00566 +/-0.0152 0.0128 +/-0.0152 0.0268 pCi/g Thallium-208 0.423 +/-0.0539 0.0142 +/-0.0539 0.030 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00331 +/-0.0151 0.0131 +/-0.0151 0.0304 pCi/g KSDI 09/07/06 1842 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 44

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013A Project: YANKO 1204 Sample ID: 170256013 Client ID: YANK001 Vol. Recv,:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrierf[racer Recovery GFPC, Sr90, solid-ALL FSS 101 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

45

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013B Project: YANK01204 Sample ID: 170256014 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 19.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.23 +/-0.302 0.0948 +/-0.302 0.190 pCi/g MJHl 09/01/062110 563436 1 Americium-241 U 0.0581 +/-0.0456 0.0383 +/-0.0456 0.0765 pCi/g Bismuth-212 0.606 +/-0.361 0.199 +/-0.361 0.399 pCi/g Bismuth-214 0.990 +/-0.154 0.046 +/-0.154 0.0919 pCi/g Cesium-134 U 0.0447 +/-0.0383 0.033 +/-0.0383 0.066 pCi/g Cesium- 137 0.0831 +/-0.037 0.0286 +/-0.037 0.0571 pCi/g Cobalt-60 0.196 +/-0.0645 0.0258 +/-0.0645 0.0515 pCi/g Europium-152 U 0.0248 +/-0.116 0.061 +/-0.116 0.122 pCi/g Europium-154 U 0.0401 +/-0.106 0.0809 +/-0.106 0.162 pCi/g Europium-155 U 0.067 +/-0.0826 0.0584 +/-0.0826 0.117 pCi/g Lead-212 1.32 +/-0.136 0.0337 +/-0.136 0.0674 pCi/g Lead-214 0.989 +/-0.153 0.0431 +/-0.153 0.0862 pCi/g Manganese-54 U -0.00696 +/-0.0306 0.0262 +/-0.0306 0.0523 pCi/g Niobium-94 U 0.00306 +/-0.0256 0.0228 +/-0.0256 0.0455 pCi/g Potassium-40 9.89 +/-0.996 0.207 +/-0.996 0.414 pCi/g Radium-226 0.990 +/-0.154 0.046 +/-0.154 0.0919 pCi/g Silver-108m U -0.017 +/-0.0253 0.0211 +/-0.0253 0.0422 pCi/g Thallium-208 0.456 +/-0.084 0.0253 +/-0.084 0.0505 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00221 +/-0.0172 0.0143 +/-0.0172 0.0316 pCi/g KSD1 09/07/06 1843 562563 2 The following Prep Methodswere performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 46

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013B Project: YANK01204 Sample ID: 170256014 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 103 (25%-0125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

47

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-01 3C Project: YANK01204 Sample ID: 170256015 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 17.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.07 +/-0.236 0.0703 +/-0.236 0.154 pCi/g MJHI 09/01/062118 563436 1 Americium-241 U -0.00337 +/-0.0367 0.034 +/-0.0367 0.0701 pCi/g Bismuth-212 0.808 +/-0.311 0.157 +/-0.311 0.341 pCi/g Bismuth-214 0.614 +/-0.118 0.0422 +/-0.118 0.0899 pCi/g Cesium-134 U 0.0481 +/-0.0502 0.033 +/-0.0502 0.0699 pCi/g Cesium-137 0.0789 +/-0.0569 0.0226 +/-0.0569 0.0484 pCi/g Cobalt-60 0.074 +/-0.0564 0.0239 +/-0.0564 0.0531 pCi/g Europium-152 U -0.0203 +/-0.0622 0.0547 +/-0.0622 0.115 pCi/g Europium-154 U -0.0129 +/-0.0828 0.0688 +/-0.0828 0.152 pCi/g Europium-155 U 0.0479 +/-0.0527 0.0529 +/-0.0527 0.109 pCi/g Lead-212 0.903 +/-0.0714 0.0332 +/-0.0714 0.069 pCi/g Lead-214 0.651 +/-0.103 0.0431 +/-0.103 0.0904 pCi/g Manganese-54 U -0.0163 +/-0.0298 0.0235 +/-0.0298 0.0506 pCi/g Niobium-94 U -0.022 +/-0.0284 0.0226 +/-0.0284 0.0481 pCi/g Potassium-40 12.9 +/-1.11 0.250 +/-1.11 0.553 pCi/g Radium-226 0.614 +/-0.118 0.0422 +/-0.118 0.0899 pCi/g Silver-108m U 0.00256 +/-0.0199 0.0177 +/-0.0199 0.0378 pCi/g Thallium-208 0.248 +/-0.0569 0.0239 +/-0.0569 0.0508 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U -0.00157 +/-0.0143 0.0123 +/-0.0143 0.0289 pCi/g KSDI 09/07/06 1845 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 48

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013C Project: YANK01204 Sample ID: 170256015 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 98 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

U! Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

49

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013D Proiect: YANKO 1204 Sample ID: 170256016 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 25.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSSGAM & ALL FSS 226 Ingrowth Waived Actinium-228 1.03 +/-0.160 0.0664 +/-0.160 0.142 pCi/g MJHI 09/05/06 0521 563436 1 Americium-241 U 0.0216 +/-0.0981 0.0845 +/-0.0981 0.174 pCi/g Bismuth-212 0.420 +/-0.350 0.142 +1-0.350 0.301 pCi/g Bismuth-214 0.689 +/-0.0898 0.0339 +/-0.0898 0.0715 pCi/g Cesium-134 U 0.0488 +/-0.0307 0.0247 +/-0.0307 0.0519 pCi/g Cesium-137 0.170 +/-0.0491 0.019 +/-0.0491 0.0402 pCi/g Cobalt-60 0.566 +/-0.0694 0.0198 +/-0.0694 0.0431 pCi/g Europium-152 U 0.0265 +/-0.0524 0.0453 +/-0.0524 0.0946 pCi/g Europium-154 U 0.0628 +/-0.0639 0.0591 +/-0.0639 0.127 pCi/g Europium-155 U 0.0541 +/-0.0561 0.0528 +/-0.0561 0.109 pCi/g Lead-212 0.958 +/-0.0653 0.0265 +/-0.0653 0.055 pCi/g Lead-214 0.784 +/-0.0896 0.0297 +/-0.0896 0.0623 pCi/g Manganese-54 U 0.00917 +/-0.0221 0.019 +/-0.0221 0.0403 pCi/g Niobium-94 U 0.0056 +/-0.019 0.0164 +/-0.019 0.0347 pCi/g Potassium-40 12.6 +/-0.931 0.166 +/-0.931 0.367 pCi/g Radium-226 0.689 +/-0.0898 0.0339 +/-0.0898 0.0715 pCi/g Silver-108m U - 0.00656 +/-0.0175 0.0151 +/-0.0175 0.0318 pCi/g Thallium-208 0.314 +/-0.0426 0.0189 +/-0.0426 0.0398 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid ALL FSS Strontium-90 U 0.00738 +/-0.0147 0.0112 +/-0.0147 0.0265 pCi/g KSD1 09/07/06 1846 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 50

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-013D Proiect: YANK01204 Sample ID: 170256016 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 106 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

U1 Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

51

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis

..... i Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 91 06-0004-005A Project: YANKO 1204 Sample ID: 170256017 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 09-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 17.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Ganmma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.975 +/-0.164 0.0814 +/-0.164 0.174 pCi/g MJH1 09/01/06 2119 563436 1 Americium-241 U 0.0504 f-I-0.0306 0.030 +/-0.0306 0.0616 pCi/g Bismuth-212 0.804 +/-0.393 0.165 +/-0.393 0.351 pCi/g Bismuth-214 0.647 +/-0.112 0.0371 +/-0.112 0.0787 pCi/g Cesium-134 U 0.0288 +/-0 .0288 0.0271 +/-0.0288 0.0574 pCi/g Cesium-137 0.249 +/-0.049 1 0.0255 +/-0.0491 0.0537 pCi/g Cobalt-60 0.682 +/-0.0884 0.0206 +/-0.0884 0.0453 pCi/g Europium-152 U 0.0893 +/-0.0683 0.0526 +/-0.0683 0.110 pCi/g Europium-154 U 0.0167 +I-0.0707 0.0611 +/-0.0707 0.134 pCi/g Europium-155 U 0.00619 +/-0.0524 0.0476 +/-0.0524 0.0982 pCi/g Lead-212 0.912 +/-0.0658 0.0281 +/-0.0658 0.0584 pCi/g Lead-214 0.747 +/-0.0939 0.036 +/-0.0939 0.0755 pCi/g Manganese-54 U 0.0235 +/-0.0494 0.0228 +/-0.0494 0.0486 pCi/g Niobium-94 U - 0.00608 +I-0.0244 0.0201 +/-0.0244 0.0426 pCi/g Potassium-40 10.5 +/-0.910 0.155 +/-0.910 0.351 pCi/g Radium-226 0.647 +/-0. 112 0.0371 +/-0.112 0.0787 pCi/g Silver-108m U 0.00189 +/-0.0202 0.0178 +/-0.0202 0.0376 pCi/g Thallium-208 0.322 +/-0.0462 0.0209 +/-0.0462 0.0442 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U - 0.00262 +/-0.0137 0.012 +/-0.0137 0.0286 pCi/g KSDI 09/07/06 1857 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 52

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005A Proiect: YANKO 1204 Sample ID: 170256017 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 92 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

53

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005 B Project: YANKO 1204 Sample ID: 170256018 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 10-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 14%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.787 +/-0.187 0.0725 +/-0.187 0.153 pCi/g MJHI 09/02/06 1713 563436 1 Americium-241 U 0.0759 +/-0.0649 0.0382 +/-0.0649 0.0789 pCi/g Bismuth-212 0.403 +/-0.233 0.139 +/-0.233 0.294 pCi/g Bismuth-214 0.636 +/-0.108 0.0306 +/-0.108 0.0647 pCi/g Cesium-134 U 0.0378 +/-0.0274 0.0229 +/-0.0274 0.0482 pCi/g Cesium-137 0.181 +/-0.0421 0.019 +/-0.0421 0.040 pCi/g Cobalt-60 0.710 +/-0.0716 0.0155 +/-0.0716 0.034 pCi/g Europium-152 U 0.0183 +/-0.0466 0.0421 +/-0.0466 0.0881 pCi/g Europium-154 U 0.0204 +/-0.0516 0.0449 +/-0.0516 0.0982 pCi/g Europium-155 UI 0.00 +/-0.0804 0.0458 +/-0.0804 0.0944 pCi/g Lead-212 0.722 +/-0.086 0.0317 +/-0.086 0.0651 pCi/g Lead-214 0.832 +/-0.115 0.0288 +/-0.115 0.0605 pCi/g Manganese-54 U 0.0204 +/-0.0232 0.0192 +/-0.0232 0.0406 pCi/g Niobium-94 U 0.0129 +/-0.0173 0.0161 +/-0.0173 0.0339 pCi/g Potassium-40 9.30 +/-0.895 0.130 +/-0.895 0.291 pCi/g Radium-226 0.636 +/-0.108 0.0306 +/-0.108 0.0647 pCi/g Silver-108m U 0.0081 +/-0.0194 0.0154 +/-0.0194 0.0324 pCi/g Thallium-208 0.299 +/-0.0505 0.0157 +1-0.0505 0.0332 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.0109 +/-0.0167 0.0123 +/-0.0167 0.0293 pCi/g KSDI 09/07/06 1857 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 54

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005B Proiect: YANK01204 Sample ID: 170256018 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 95 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL hI Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

55

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005C Proiect: YANKO 1204 Sample ID: 170256019 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 10-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 24.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.810 +/-0.116 0.0431 +/-0.116 0.090 pCi/g MJH1 09/05/06 2143 563436 1 Americium-241 U 0.0147 +/-0.0176 0.0169 +/-0.0176 0.0345 pCi/g Bismuth-212 0.365 +/-0.171 0.099 +/-0.171 0.206 pCi/g Bismuth-214 0.623 +/-0.0633 0.0212 +/-0.0633 0.044 pCi/g Cesium-134 Ul 0.00 +/-0.0297 0.0166 +/-0.0297 0.0343 pCi/g Cesium-137 0.113 +/-0.0242 0.0124 +/-0.0242 0.0257 pCi/g Cobalt-60 0.268 +/-0.0379 0.012 +/-0.0379 0.0254 pCi/g Europium-152 U -0.00617 +/-0.0317 0.0284 +/-0.0317 0.0585 pCi/g Europium-154 U -0.0248 +/-0.0417 0.0337 +/-0.0417 0.0714 pCi/g Europium-155 UI 0.00 +/-0.0407 0.0265 +/-0.0407 0.054 pCi/g Lead-212 0.840 +/-0.0404 0.0162 +/-0.0404 0.0332 pCi/g Lead-214 0.686 +/-0.0505 0.0197 +1-0.0505 0.0406 pCi/g Manganese-54 U 0.00306 +/-0.0143 0.0127 +/-0.0143 0.0265 pCi/g Niobium-94 U 0.0053 +/-0.013 0.0112 +/-0.013 0.0232 pCi/g Potassium-40 10.2 +/-0.535 0.0857 +1-0.535 0.186 pCi/g Radium-226 0.623 +/-0.0633 0.0212 +/-0.0633 0.044 pCi/g Silver-108m U -0.0071 +/-0.0113 0.00971 +/-0.0113 0.0201 pCi/g Thallium-208 0.288 +/-0.031 0.0115 +/-0.031 0.0239 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.0082 +/-0.0158 0.012 +/-0.0158 0.0284 pCi/g KSDI 09/07/06 1857 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 56

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005C Project: YANK01204 Sample ID: 170256019 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits CarrierFTracer Recovery GFPC, Sr90, solid-ALL FSS 96 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

57

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005D Proiect: YANKO 1204 Sample ID: 170256020 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: I0-AUG-06 Receive Date: 25-AUG-06 Collector: Client Moisture: 19.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Ganmma,Solid-FSS GAM & ALL FSS 226 Ingrowth Waived Actinium-228 0.995 +/-0.411 0.146 +/-0.411 0.291 pCi/g MJH1 09/02/06 1725 563436 1 Americium-241 U 0.0557 +/-0.0479 0.0365 +/-0.0479 0.0729 pCi/g Bismuth-212 0.635 +/-0.589 0.261 +/-0.589 0.521 pCi/g Bismuth-214 0.760 +/-0.165 0.0601 +/-0.165 0.120 pCi/g Cesium-134 U 0.0627 +/-0.0504 0.0463 +/-0.0504 0.0926 pCi/g Cesium-137 0.503 +/-0.0894 0.0338 +/-0.0894 0.0676 pCi/g Cobalt-60 1.72 +/-0.132 0.0307 +/-0.132 0.0614 pCi/g Europium-152 U 0.00265 +/-0.0988 0.0745 +/-0.0988 0.149 pCi/g Europium-154 U 0.0538 +/-0.114 0:0996 +/-0.114 0.199 pCi/g Europium-155 UI 0.00 +/-0.119 0.0591 +/-0.119 0.118 pCi/g Lead-212 1.09 +/-0.126 0.0386 +/-0.126 0.0772 pCi/g Lead-214 0.802 +/-0.135 0.0517 +/-0.135 0.103 pCi/g Manganese-54 U 0.0185 +/-0.0434 0.0383 +/-0.0434 0.0766 pCi/g Niobium-94 U -0.0168 +/-0.0366 0.0309 +/-0.0366 0.0618 pCi/g Potassium-40 10.7 +/- 1. 11 0.276 +/-1.11 0.551 pCi/g Radium-226 0.760 +/-0.165 0.0601 +/-0.165 0.120 pCi/g Silver-108m U -0.021 +/-0.0301 0.0247 +/-0.0301 0.0494 pCi/g Thallium-208 0.343 +/-0.0887 0.0298 +/-0.0887 0.0595 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U -0.00322 +/-0.0146 0.0127 +/-0.0146 0.0299 pCi/g KSD1 09/07/06 1857 562563 2 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/27/06 1545 562444 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits 58

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: September 8, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005D Proiect: YANKO 1204 Sample ID: 170256020 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 99 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

59

QUALITY CONTROL DATA 60

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: September 8, 2006 Client : Connecticut Yankee Atomic Power Page 1 of 5 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 170256 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 563436 QCI201171526 170256001 DUP Actinium-228 0.966 1.01 pCi/g 4 (0%- 100%) MJHI 09/02/06 17:26 Uncert: +/-0.192 +/-0.200 TPU: +/-0.192 +/-0.200 Americium-241 U 0.0375 U 0.0258 pCi/g 37 (0%- 100%)

Uncert: +/-0.0387 +/-0.075 TPU: +/-0.0387 +/-0.075 Bismuth-212 0.366 0.592 pCi/g 47 (0%- 100%)

Uncert: +/-0.306 +/-0.276 TPU: +/-0.306 +/-0.276 Bismuth-214 0.650 0.690 pCi/g 6 (0%- 100%)

Uncert: +/-0.135 +/-0.0955 TPU: +/-0.135 +/-0.0955 Cesium- 134 U 0.0366 U1 0.00 pCi/g 56 (0%- 100%)

Uncen: +/-0.0355 +/-0.035 TPU: +/-0.0355 +/-0.035 Cesium- 137 0.0666 0.0611 pCi/g 9 (0%- 100%)

Uncert: +/-0.0355 +/-0.0415 TPU: +/-0.0355 +/-0.0415 Cobalt-60 0.104 0.159 pCi/g 41 (0%- 100%)

Uncert: +/-0.0726 +/-0.0325 TPU: +/-0.0726 +/-0.0325 U 0.00636 Europium- 152 U -0.00858 pCi/g 1350 (0%- 100%)

Unceri: +/-0.0728 +/-0.0624 TPU: +/-0.0728 +/-0.0624 Europium- 154 U -0.0788 U 0.00919 pCi/g 253 (0%- 100%)

Uncert: +/-0.0938 +/-0.0602 TPU: +/-0.0938 +/-0.0602 Europium- 155 U 0.0672 U 0.0817 pCi/g 20 (0%- 100%)

Uncert: +/-0.0554 +/-0.0557 TPU: +/-0.0554 +/-0.0557 Lead-212 0.871 0.847 pCi/g 3 (0%- 20%)

Uncert: +/-0.0971 +/-0.0867 TPU: +/-0.0971 +/-0.0867 Lead-214 0.727 0.699 pCi/g 4 (0%- 20%)

Uncert: +1-0,105 +/-0.102 TPU: +/-0.105 +/-0.102 Manganese-54 U -0.00916 U -0.00665 pCi/g 32 (0% - 100%)

Uncert: +/-0.0319 +/-0.0225 TPU: +/-0.0319 +/-0.0225 Niobium-94 U 0.0101 U -0.00339 pCi/g 402 (0%- 100%)

Uncert: +/-0.0244 +/-0.0176 TPU: +/-0.0244 +/-0.0176 61

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 170256 Page 2 of 5 Parmname NOM Samnle Oual OC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 563436 Potassium-40 11.3 11.7 pCi/g 3 (0% - 20%)

Uncert: +/-0.986 +/-1.03 TPU: +/-0.986 +/-1.03 Radium-226 0.650 0.690 pCi/g 6 (0%- 100%)

Uncert: +/-0.135 +/-0.0955 TPU: +/-0.135 +/-0.0955 Silver- 108m U -0.0067 U 0.000104 pCi/g 206 (0%- 100%)

Uncen: +/-0.0208 +/-0.018 TPU: +/-0.0208 +/-0.018 Thallium-208 0.283 0.283 pCi/g 0 (0%- 100%)

Uncert: +/-0.0618 +/-0.048 TPU: +/-0.0618 +/-0.048 QC12O1171527 LCS Actinium-228 U 0.254 pCi/g 09/03/06 22:31 Uncert: +/-0.565 TPU: +/-0.565 Americium-241 23.4 24.1 pCi/g 103 (75%-125%)

Uncert: +/-1.28 TPU: +/-1.28 Bismuth-212 U 0.575 pCi/g Uncert: +/-0.944 TPU: +/-0.944 Bismuth-214 U 0.0248 pCi/g Uncert: +/-0.213 TPU: +/-0.213 Cesium- 134 U 0.00032 pCi/g Uncert: +/-0.147 TPU: +/-0.147 Cesium-137 9.58 9.84 pCi/g 103 (75%-125%)

Uncert: +/-0.487 TPU: +/-0.487 Cobalt-60 14.5 14.7 pCi/g 101 (75%-125%)

Uncert: +/-0.660 TPU: +/-0.660 Europium- 152 U 0.125 pCi/g Uncert: +/-0.292 TPU: +/-0.292 Europium- 154 U 0.0779 pCi/g Uncert: +/-0.277 TPU: +/-0.277 Europium- 155 U -0.0876 pCi/g Uncert: +/-0.277 TPU: +/-0.277 Lead-212 U 0.0524' pCi/g Uncert: +/-0.155 TPU: +/-0.155 Lead-214 U -0.103 pCi/g Uncen: +/-0.212 62

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 170256 Page 3 of 5 Parmname NOM SamDle Oual OC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 563436 TPU: +/-0.212 Manganese-54 U 0.0306 pCi/g Uncert: +/-0.135 TPU: +/-0.135 Niobium-94 U -0.0513 pCi/g Uncert: +/-0.115 TPU: +/-0.115 Potassium-40 U 0.769 pCi/g Uncert: +/-1.10 TPU: +/-1.10 Radium-226 U 0.0248 pCi/g (75%-1 25%)

Uncert: +/-0.213 TPU: +/-0.213 Silver-108m U 0.0782 pCi/g Uncert: +/-0.105 TPU: +/-0.105 Thallium-208 U 0.180 pCi/g Uncert: +/-0.177 TPU: +/-0.177 QC1201171525 MB Actinium-228 U 0.0216 pCi/g 09/02/06 17:16 Uncert: +/-0.0479 TPU: +/-0.0479 Americium-241 U -0.0654 pCi/g Uncert: +/-0.0396 TPU: +/-0.0396 Bismuth-212 U 0.110 pCi/g Uncert: +/-0.0705 TPU: +/-0.0705 Bismuth-214 U 0.00843 pCi/g Uncert: +/-0.0317 TPU: +/-0.0317 Cesium-134 U -0.00203 pCi/g Uncert: +/-0.012 TPU: +/-0.012 Cesium- 137 U -0.00757 pCi/g Uncert: +/-0.0117 TPU: +/-0.0117 Cobalt-60 U -0.00589 pCi/g Uncert: +/-0.0128 TPU: +/-0.0128 Europium- 152 U -0.0169 pCi/g Uncert: +/-0.0308 TPU: +/-0.0308 Europium- 154 U 0.00802 pCi/g Uncert: +/-0.0305 TPU: +/-0.0305 Europium-155 U -0.00342 pCi/g 63

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 170256 Page 4 of 5 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 563436 Uncert: +/-0.0294 TPU: +/-0.0294 Lead-212 U 0.0151 pCi/g Uncert: +/-0.028 TPU: +/-0.028 Lead-214 U 0.00738 pCi/g Uncert: +/-0.0252 TPU: +/-0.0252 Manganese-54 U . 0.0127 pCi/g Uncert: +/-0.0111 TPU: +/-0.0111 Niobium-94 U -0.00293 pCi/g Uncert: +/-0.012 TPU: +/-0.012 Potassium-40 U 0.112 pCi/g Uncert: +/-0.173 TPU: +/-0.173 Radium-226 U 0.00843 pCi/g Uncert: +/-0.0317 TPU: +/-0.0317 Silver-108m U 0.00354 pCi/g Uncert: +/-0.0115 TPU: +/-0.0115 Thallium-208 U -0.011 pCi/g Uncert: +/-0.0157 TPU: +/-0.0157 Rad Gas Flow Batch 562563 QC1201169422 170256002 DUP Strontium-90 U 0.00501 U 0.00534 pCi/g 0 (0% - 100%) KSDI 09/07/06 18:59 Uncert: +/-0.0149 +/-0.0155 TPU: +/-0.0149 +/-0.0155 QC1201169424 LCS Strontium-90 1.74 1.57 pCi/g 90 (75%-125%) 09/07/06 19:16 Uncert: +/-0.140 TPU: +/-0.147 QC1201169421 MB Strontium-90 U 0.0172 pCi/g 09/07/06 18:59 Uncert: +/-0.0185 TPU: +/-0.0185 QC1201169423 170256002 MS Strontium-90 1.74 U 0.00501 1.32 pCi/g 76 (75%-125%) 09/07/06 19:16 Uncert: +/-0.0149 +/-0.124 TPU: +/-0.0149 +/-0.130 Notes:

The Qualifiers in this report are defined as follows:

64

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 170256 Page 5 of 5 Parmname NOM Sample Qual OC Units RPD% REC% Ranue Anist Date Time

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike con centration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concen ning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5 X the RL h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

65

General Narrative Page l of 105

CASE NARRATIVE For CONNECTICUT YANKEE RE: Soil PO# 002332 Work Order: 168404 SDG: MSR #06-0652, 06-0675, 06-0687, 06-0688, 06-0707, 06-0743, 06-0755 August 15, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:

2040 Savage Road Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina on May 5, May 9, May 12, May 17, May 26, June 2, June 8, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.

The laboratory received the following sample(s):

Sample ID Client Sample ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01 OF 168404008 9106-0005-014F 168404009 9106-0006-005F GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

P.O. Box 30712

• Charleston, SC 29417

• 2040 Savage Road (29407)

Page 2 of 105 Phone (843) 556-8171

• Fax (843) 766-1178

• www.gel.com

168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 16840401.5 9106-0010-012F Items of Note:

At the request of Dale Randall on July 20, 2006, GEL analyzed the above samples according to the spreadsheet in the attached email.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.

Analytical Request:

Seven soil samples were reanalyzed for FSSALL, except gamma and Sr-90.

Four soil samples were reanalyzed for FSSALL, except gamma and Ni-63.

Two soil samples were reanalyzed for FSSALL, except gamma.

Two soil samples were reanalyzed for FSALL, except gamma, Sr-90 and Ni-63.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

P.O. Box 30712 ° Charleston, SC 29417

• 2040 Savage Road (29407)

Phone (843) 556-8171

• Fax (843) 766-1178 - www.gel.com Page 3 of 105

. I I!

Additional HTD analyses

Subject:

Additional HTD analyses U&Lfowlt II From: "Dale Randall" <randall @cyapco.com>

Date: Thu, 20 Jul 2006 11:04:54 -0400 To: "Cheryl Jones" <cj @gel.com>

CC: "Clyde Newson" <Newson@CYAPCO.com>, "John McCarthy" <McCarthy@ CYAPCO.com>

Cheryl:

Per our earlier discussion, attached is a list of samples that we would like to have analyzed to the FSSALL protocol. I have included a list of test protocols performed on each sample to date. Once you have had an opportunity to determine our options for each sample please call or e-mail me at your convenience.

Thank You, Dale (860) 267-3133 Content-Description: GEL FSSALL analyses request.xls GEL FSSALL analyses request.xls ! Content-Type: application/vnd.ms-excel Content-Encoding: base64 I oflI Page 4 of 105 8/2/2006 7:04 PM

Done To be done Previous GEL ID CY sample location IDs FSS Gam Sr-90 Ni-63 Am Pu Sr9O Pu241 Fe55 Ni63 Tc99 H3 C14 7164220008 9106-0002-007F x x x x x x x x x X 164220012 9106-0002-011F x x x x x x x x x x c 162335004 9106-0003-004F x x x x x x x x x x 162335014 9106-0003-015F x x x x x x x x x x 162832015 9106-0004-005F x x x x x x x x x x 162832009 9106-0004-015F x x x x x x x x x x 162485008 9106-0005-01OF x x x x x x x x x x 162485011 9106-0005-014F x x x x x x x x x .x 162850014 9106-0006-005F x x x x x x x x x x 163741005 9106-0008-006F x x x x x x x x x x 163741009 9106-0008-008F x x x x x x x x x x 164542008 9106-0009-002F x x x x x x x x x x 164542003 9106-0009-017F x x x x x x x x x x 163105009 9106-0010-001 F x x x x x x x x x x 163105016 9106-0010-012F x x x x x x x x x x

Chain of Custody and Supporting Documentation Page 6 of 105

kV61 o !Eýff ')Lý q Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major SChain of Custody NoForm007 Connecticut Yankee Atomic Power Company No. 2006-00371 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 4 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones co i, Priority: X 30 D. E] 14 D. [] 7 D. Container V[aL-2* ZO:<

Sample size-* . . ."

Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0002-OO1F 5/17/06 10:42 SE C BP x x -"_Transfesred from COC 2006-00357 9106-0002-002F 5/18/06 09:43 SE C BP x Transferred from COC 2006-00361 9106-0002-003F 5/18/06 10:14 SE C BP X X Transferred from COC 2006-00361 9106-0002-004F 5/18/06 10:39 SE C BP X X Transferred from COC 2006-00361 9106-0002-005F 5/18/06 12:49 SE C BP X x Transferred from COC 2006-00364 9106-0002-006F 5/18/06 13:14 SE C BP x x Transferred from COC 2006-00364 9106-0002-006FS 5/18/06 13:14 SE C BP x x Transferred from COC 2006-00364 9106-0002-007F 5/18/06 13:37 SE C BP x x Transferred from COC 2006-00364 9106-0002-008F 5/18/06 14:04-M SE C BP X x Transferred from COC 2006-00364 NOTES: PO #: 002332 MSR #: 06- SSWP# NA [ LTP QA 0 Radwaste QA LI Non QA Samples Shipped Via: Internal 05 Fed Ex Container 0-1 UPS Temp.:

Deg. C E] Hand Custody Sealed?

IR quDate/Time h 2) =ived By Date/Time Custody Seal o~~( 0C$) Other Intact?

ýrgelinquishled BJ Date/Time 4) Received By Date/Time YO__ NC Bill of Lading #

5) Relinquished By Date/Time 6) Received By Date/Time 7C i951 ,

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-00 I Major

~Chain of Custody Form M

(0 Connecticut Yankee Atomic Power Company ChinofCutoy3or No. 2006-00372 00 362 Injun Hollow Road, East Hampton, CT 06424 O 860-267-2556 ,

5 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 0 843 556 8171. Attn. Cheryl Jones Cn V)

Priority: N 30 D. E] 14 D. [] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0002-009F 5/18/06 14:28 SE C BP - x Transferred from COC 2006-00364 9106-0002-01OF 5/18/06 14:50 SE C BP x X TransferredfromCOC2006-00364 9106-0002-01IF 5/19/06 08:10 SE C BP X X Transferred from COC 2006-00365 9106-0002-012F 5/19/06 08:31 SE C BP X X Transferred from COC 2006-00365 9106-0002-013F 5/19/06 09:00 SE C BP X x Transferred from COC 2006-00365 9106-0002-014F 5/19/06 09:58 SE C BP X x Transferred from COC 2006-00365 9106-0002-014FS 5/19/06 09:58 SE C BP X X Transferred from COC 2006-00365 9106-0002-015F 5/19/06 10:29 SE C BP x x Transferred from COC 2006-00365 9106-0002-016F 5/19/06 13:19 SE C BP X x Transferred from COC 2006-00365 NOTES: P0 #: 002332 MSR #: 06- SSWP# NA [K LTP QA C?5S 0 Radwaste QA El Non QA Samples Shipped Via: Internal

[Z Fed Ex Container ED UPS Temp.:

Deg. C fl Hand Custody Sealed?

SlRelin ishe Date/Time 2) Re ived By DatpTime Custody Seal

/6ý _ _ _ _ _ _ X__

_ _ _ _ _ _ _f Other Intact?

3)"Ielinquished By Date/Time 4) Received By Date/Time BillofLading_#___ xY

' N 0

5) Relinquished By Date/Time Bill of Lading #

6) Received By Date/Time '1 " 7 79

Connecticut Yankee Statement of Work for Analytical Lab Services - .CY-ISC-SOW-001 Figure 1. -Sample Check-in List DateiTime Received& - V (0  :

SDG#: NýS9.-*$ 0(o-0 "-6S Work Order Number: , ( , t_[ 'Z .

Shipping Cdatainer IDnYIO_ LU (559/O Chain of Custody#0 ( r /

I. Custody Seals on shipping container intact?. Yes D\1"No []

2. Custody Seals dated and signed? Yes No[]

3. Chain-of-Custody record present? Yes No [

4. Cooler temperature . _""

5. Verniiculite/packing materials is:. Wet [ ] Dry t\ ]

6 " Number of samples in shipping container: __

7. Sample holding times exceeded? Yes 11 No VI

8. Samples have' tape __ hazard labels

_i custody seals - appropriate sample labels

9. Samples are:

-_ ia good condition . leaking

._._broken .have air bubbles

10. Were any anomalies identified in sample receipt? Yes ' [ NoX ]

11. . Description of anomalies (include sample numbers):

Sample Custodia Laboratory: Date  :

Telephoned to: On By Page 9 of.105

Connecticut Yankee Statement of Work for Analytical Lab Services -lC-owoo

-CY-ISC-SOW-001 .

I Figure 1. Sample Check-in List Datefrime Receive&d",f) & .2 f SDG#: 6&~#(-Or Work Order Number: ( ,Q*{ZZO 1.

Shipping Cdntainer ID <P..*Lt5

" .59 "f Chain of Custody #.)2ov C, v 3/2 I. Custody Seals. oii shipping container intact?,. Yes 'No I

2. Custody Seals dated and signed? Yes No [ ].

3. Chain-of-Custody record present? Yes I Not]

4. Cooler temperature .P,

5. Vermiculite/packing materials is: W et [] Dry I ',]* fJ.

6: Number of samples in shipping container __ _

7- Sample holding times exceeded? Yes [ No 1

8. Saj lesth e.

_vape

-hazard labels

-cstody seals -appropriate sample labels

9. Sam ples are-..

n$ii'good condition 2eln

-broken .have air bubbles

10. Were any anomalies identified in sample receipt?. Yes [ ]No

. .. Description

.. of anomalies, (include sample numbers):

Sample Custodian/Laboratory: (X*4.i, ' ,A.Date. , -o b Telephoned to: On By Page 10 of:105  ;.7

SSAMPLE RECEIPT & REVIEW FORM I7Clnt 7P7 01P ^ t Mueol 4.'a --up ~ A _ SDGIARCOC/Work Order: I (

Date Received: & a .'Q10 PM(A) Review (ensure non-conrormi'ng items are resolved prior to sigaing);

Received By: Uk Sample Receipt Criteria Z Z CommentslQualifiers (Required for Non-Conforming Items)

Circle Applicable: seals broken damaged containe* lear g container other (describe)

Shipping containers received intact I and sealed?

/

CircleCoolant # blue ice dry ice none other describe)

Samples requiring cold ice bags 2 preservation within (4 +/- 2 C)?

_ Record preservation method. ....

Chain of custody documents 3included with shipment? __ _

Sample containers intact and ircle Applicablesdas broken damaged container leaking container other (describe) 4 sealed?1-5 Samples requiring chemical  !,1 ID's. containers affected anid observed pH:

ýSa preservation at proper pH?

- prservtionat poperpHSample ID's and containers affected:

6 VOA vials free of headspace (defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) i holding td'aand tes, affectred 8 Samples received time?

9oSample ID's COC match ID's Sample ID's and containers affected:

-on bottles?.______________________________

Date & me on COC match date Sample ID's affected-

& tiYon bottles?

Nu her of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in relin2uishedlreceived sections? 2,0" 0e 14 Air Bill ,Tracking #s, &

Additional Comments T RSO RAD Receipt##_'

S t zt *If > x2 area background is observed on samples identified as "non-Suspected Hazard Information * * . regulated/non-radioactive-, contact the Radiation Safety group for further

_____i: *investigation.

(A )Radiological Classification? Maximum Counts Obserd*.

B PCB Regulated? i Comments:

Shipped as DOI Hazardous C Material? If yes, contact Waste Hazard Class Shipped:

Manager or _SH Manager. N#:

PM (or PMA) review of Hazard class.iticaion : Initials Date: Lo Z'7 10(,'

Page 11 of 105 U

ze,0 SAMPLE RECEIPT & REVIEW FORM 0 PM use onlyV

~

Cliet: (C' SDGIARcCOCIWOrk Order: Al C:v"

,PM(A) Review ereslved prior to signing).

Date Received: c Received By:. _

Sample Receipt Criteria Comments/Qualifier leq'uired for Non-Conforming Items)

Circle Applicable: seals broke damaged container leaking container other (describe) containers received intact 1 Shipping and sealed? 1______ooant _______________bue __edy__e none_ other__escrib Circ Colant # blue ice dry ice none other describe)

Samples requiring cold I1ags 2 preservation within (4 +/- 2 C)? /

Record preservation method. -ii 3 Chain of custody documents included with shipment?

Sample containers intact and Cire plifcable: seals broken damaged container leaking container other (describe) 4sealed? -

Samples requiring chemical Sample IDs. containers affected and observed pH:

preservation at proper pH? A Sample ID' and containers affected:

6 VOA vials free of headspace (defined as < 6mm bubble)? /

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)

8. Samples received within holdin Id' and tests affected; time? /

Sample ID's on COC matc ID's Sample IDs and containers affected:

on bottles?7_

10 Date & time on COC tch date Sample ID's affected:

10&time on bottles?f Number of containe received Sample ID's affected:

match number indic/ted on COC?

COC form is prop rly signed in 12 relinquished/rIgived sections?

1 CoC." Z.oOCP - 4), .... j- &*1,&I1 Air Bill ,Tracking Fs, &

Additional Comments T RSO RAD Receipt #

S e Ha I *If > x2 area background is observed on samples identified as "non-St - regulated/non-radioactive", contact the Radiation Safety group for further

__ __ investigation.

A Radiological Classification? - ,/ Miximum Counts Observed*: W, c Pi/n B PCB Regulated? Comments:

Shipped as DOT Hazardousm-c Material? If yes, contact Waste Hazard Class Shipped:

r Manager or ESH Manager.B UNN:

PM (or PMA) review of Hazard classification: Initials - Date: -

Page 12 of 105 C/

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 1 Major

~Chain of Custody Form No. 2006-00312 Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 4 /43 324/C 5 860-267-2556 01 "

Project Name: Haddam Neck Decommissioning ' Analyses Requested Lab Use Only Contact Name & Phone: COments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories "

2040 Savage Road. Charleston SC. 29407 1I".

843 556 8171. Attn. Cheryl Jones rV) V CA Priority: 0 30 D. ] 14D., 71D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code CComment,, Preservation rL t._ab Samp__i_

m .

9106-0003-001F 4/24/06 14:13 SE C BP X Transferred from COC2006-00221 it 9106-0003-002F 4/24/06 14:39 SE C BP x Transferred from C0C2006-00221 91- 9106-0003-003F 4/24/06 15:01 SE C BP X Transferred from COC2006-00221 0 9106-0003-004F 4/25/06 08:41 SE C BP X Transferred from COC2006-00223 9106-0003-004FS 4/25/06 08:41 SE C BP X Transferred from COC2006-00223 9106-0003-005F 4/25/06 09:241 SE C BP x Transferred from COC2006-00223 9106-0003-006F 4/25/06 09:46 SE C BP x Transferred from COC2006-00223

• 9106-0003-007F 4/25/06 10:28 SE C BP X Transferred from COC2006-00223 9106-0003-008F 4/25/06 11:15 SE C BP X " Transferred from COC2006-00223 NOTES: PO #: 002332 MSR #: 06- SSWP# NA Zj LTP QA FJ Radwaste QA U Non QA Samples Shipped Via: AnternaCl."o tCter..

Combined samples 9106-0003-003F taken on 4/25/06 @08:19 and 9106-0003-003FB taken on 4/25/06 @ 08:19 in order to have sufficient sample for counting. Fed Ex Deg . C bT.

ED ups ,. : -: - ::

E Hand Custody.Sealed.

1)Relinquished By Date/Time 2)/ec ived By iDate Time .Custody Se1l Intact?

.-JA " tu4 t .5-4"-c /,..,[] (d / ,g 1 Other

3) Relinquished By Date/Time 4) Received By DatýTime Nf.

q___-____._____.__.

Bill of Lading # J

5) Relinquished By Date/Time 6) Received By Date/Time *.7. 2-0  ?'i;0- 0 2 4 "

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-00 I Major Health Physics Procedure GPP-GGGR-RS 104-003-Attachment B-CY-00 I Major Chain of Custody Form No. 2006-00313 CD Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 /(o2-3-5o/.

860-267-2556 "Z:3_,___. _.. ____ /

__* _ 5 7o/ , _-"

Project Name: Haddam Neck Decommissioning Analyses Requested Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories .< * "

2040 Savage Road. Charleston SC. 29407 ,b 0%

843 556 8171. Attn. Cheryl Jones Priority: Z 30 D. L14 D. ] 7 D. Container Sample Size-Media Type &Type 1". '

Sample Designation Date Time Code Code Code Comment, Preservation .i, IP 9106-0003-009F 4/25/06 13:00 SE C BP X Transferred from COC 2006-00236 ,.

9106-0003-01OF 4/25/06 13:23 SE C BP X - -Tnsferredfrom COC 2006-00236 Otc 9106-0003-010FS 4/25/06 13:23 SE C BP X TransferredfromCOC2006-00236 __._.._____._.._.

0~ 9106-0003-012F 4/25/06 15:12 SE C BP X Transferred from COC 2006-00236 9106-0003-013F 4/25/06 14:21 SE C BP X Transferred from COC 2006-00236 9106-0003-014F 4/25/06 14:48 SE C BP x Transferred from COC 2006-00236 - .. .,

4/26/06 08:16 SE C BP x 0* 9106-0003-015F Transferred from COC 2006-00237 9106-0003-016F 4/26/06 09:41 SE C BP x Transferred from COC 2006-00237 .

01 9106-0003-017F 4/26/06 09:18 SE C BP x Transferred from COC 2006-00237 . ,

,9106-0003-018F 4/26/06 08:59 SE C BP Transferred from COC 2006-00237 NOTES: PO #: 002332 MSR #: 06 -**& SSWP#NA SLTP QA []I Radwaste. Q)A E] Non QA Samples Shipped Via:

N Fed Ex F1 uPs

[] Hand ,rer.0tbdy SialtC.

1) Relinquished By Date/Time 2) Received By Date/lTime El Other

3) Relinquished By Date/Time 4) Received By Date/Time y j Bill of Lading #

-Y*2/ -*i-8' - 02a1

Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Check-in List Date[/Time Received: 101 Work Order Number: -I (Z---3 -S 9 (30o "- 0*: '

Shipping Cdotainer ID: "']VL0 OZ. I'L ChainofCustody#

"' O1 o 00o 13

1. Custody Seals or shipping container intact?.- -Yes No *

2. Custody Seals dated and signed? Yes [ I No

3. Chain-of-Custoly record present? Yes No [ ]

.4. Cooler temperature C C.,

5. Vermiculite/packing materials is: Wet [ Dry 1 n/-

6 Number ofsamples in shipping container: [i .]. 'r 7- Sample holding times exceeded? Yes j I No 8 amp~eps

- tape -hazard labels

__Zcutody seals _appropriate sample labels

9. Samples are:-

good condition ...2-lIeaking

-broken

• have air bubbles

10. Were any anomalies identified in sample receipt? Yes [] No

11. .Description of anomalies (include sample numbers):

S'ampleCustodian/Laboratory:- ((' . rcpft' 1/4c*-

Telephoned to: BOn By_ _ _ _

Page 15 of 105

• 1

0 SAMPLE RECEIPT & REVIEW FORM PM oeant 00YI( 21 Client: 'SDG/ARCOC/Work Order:f o- M Dat Rceve: 1 64oPM(A) Review (ensure no-o! F g items are resolved prior to signing):

Received By: ( Ca _ _ _ _ _ _ __ _ _ _ _ _ _

Sample Receipt Criteria Z Z Comments/Qualiflers (Required for Non-Conforming Items) 1 Shipping containers received intact Circle Applicable: seals broken damaged container leaking container oder (describe) and sealed?

Samples requiring cold Circle Coolant # ice bags blue ice dry ice none 2 preservation within (4 +/- 2 C)?

Record preservation method. _ _ _n__ _ _ _ _ _ _ _s Chain of custody documents included with shipment?__=_

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking container other (describe) sealed?

Samples requiring chemical Sample ID's. containers affected and observed pH:

5 preservation at proper pH? .. . ... .. . . ....

6 VOA vials free of headspace Sampl ID's and containers affected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) ,_,

Samples received within holding Id's and tests affected; time?

Sample ID's on COC match ID's Smpl ID's and conaiers affect:

on bottles?

Date & time on COC match date Sample ID's affected:

& time on bottles?

Sample ID's affected:

Number of containers received match number indicated on COC?

COC form is properly signed in 1relinquished/received sections?

Air Bill ,Tracking #'s, & F-' d to  % I Additional Comments %k z..

V - RSO RAD ReceiptI# __________

SfInformation . f> x2 area background is observed on samples identified as 'non-dm regulated/non-radioactive", contact the Radiation Safety group for further

~ ailgclCasfctoMaximum

,_

• investigation. Coulnts Observed*:

B' PCB Regulate? Conzritents:

-hipped as trot Hazardous C Material? If yes, contact Waste Hazard Class Shipped:

_Manager or ESH Manager. UN#:

PM (or- PMA) review of Hazard classification: ..-'.Date:,,

I Page 16 of 105

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 1 Major Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Name: Haddanm, Neck

,Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones I

Priority: ER 30 D.E 14 D. E] 7D.

Samples Shipped Via:

[ Fed Ex El uPs El Hand El Other Bill of Lading #

Health Phys,,Proedure GPP-GGGR-R5104-003-Attachment B-CY-00 1Major

Cquntn Yankee Atomic Power Company

" n " un Hollow Road, East Hampton, CT 06424 860-267-2556 ProjectName: Haddarn Neck Decommissic Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road, Charleston SC, 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D. [] 14 D. [17 D.

Samples Shipped Via:

[ Fed Ex El uPS C] Hand El Other Bill of Lading #

Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Check-in List Datc/Time Received: -- i-2. 20 SDG#: A4,5R:t-LO 0,R F Work Order Number: /-'32 I Shipping ContainerID: M714 9315 Chain ofCustody# ooG- 6oS.'y

1. Custody Seals on shipping container intact? Ycs No J

2. Custody Seals dated and signed? Yes No [J

3. Chain-of-Custody record present? Yes No [J

4. Cooler temperature

5. Venniculite/packing materials is: Wet J4 Dry [

6. Number of samples in shipping container: 9

7. Sample holding times exceeded? Yes [] No

10. Were any anomalies identified in sample receipt? Yes Noo N

11. Description of anomalies (include sample numbers):

Sample Custodian/Laboratory: ý 0a. , 6(, daq, Date:

Telephoned to: On By__________

Page 45 of 56 Page 19 of 105

Connecticut Yankee Statement of Work for Analytical Lab Services cy-ISC-SOW-001 Figure 1. Sample Check-in List.

Date/Time Received': 'i,(& ( (q " "

SDG#: W Oc-Work Order Number:--

Shipping Cdhtainer ID_ Chain of Custody# - &O&( -- 0()334

1. Custody Scals oni shipping container intact?. -Y Ye No

2. Custody Seals dated and signed? Yes[ ] No

3. Chain-of-Custody record present? Yes 'V No [ "

4. Cooler temperature ) 13 C-S. VermiculitcePacking materials is:

Wet f,/Dry tDr

]

-Numberofsamples in shipping container: _ _"_"_;__"

7. SYes Sample holding tiMes exceeded? ]Na &a

8. Sample-, have.'

~.k2.ape-hazard labels A2.custody Seals -appropiate sample labels

! 9.Samples arei

-In good condition

. . -. have a"r bubbles

10. Were any anomalies identified in sample rewipt?

Yes L* No [.

Pag 2oescription ofaO4alles(include sample numbers).

Sample CustiAaborar, to On__________ -L Page 20of 105-

SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM

-127,0 QF?- ( R F*.-.,,:V A.oory (* 0,IS3 A .r<>,-r,

- ((vl a~0t~- L33)(u v (n55 u A OO3 09 5i3 6 C

_-_--__ 3 _ _ _ UMc- 5 (00--)n(,i,*.

ti5secL ble haf~d nl o ~ e (CC, G Aso_______

d*mi.j AJ __v__.,->-,H__  :

JI Page 21 of 105

) 1! 1

0 SAMPLE RECEIPT & REVIEW FORM PM use only Client: C'" , . SDIARCOC/Work Order: /4, 2e 3 Date Received:

kReceived By: eA. I: j PM(A) Review (ensure non-conforming items are resolved prior to signing):

Sample Receipt Criteria Comments/Qualifiers (Required for Non-Conforming Items) other (describe) containers received intact Circle Applicable: seals broken damaged container leaking container Shipping I land sealed? x

- Samples requiring cold Circle Coolant # ice bags blue ice dry ice nw other describe) 2 preservation within (4 +/- 2 C)?

Record Preservation method.

Chain of custody documents included with shipment? n C 4 Sample containers intact and Circle Applicable: seals broken damaged container 1< "atr (decrib) sealed? .' .' 9o(1 ooo(

000 - o-- -

5Samples requiring chemical ISmple ID's, containen affected and obsered pHS:

.preservation at proper pH?__________________________

of headspace Sample ID's and containers affected:

6 6 VOA (defined as free vials < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) _ ____.

Samples received within holding Id's and test affectd:

8time?______________________ ___

9 Sample ID's on COC match ID's Smle ID's and containers a2feted:

on bottles?

Date & time on COC matchdate " ID's'affected:

10 & time on bottles? I __

Number of containers received 1 Sun* 's afeted:

" match number indicated on COC? __

COC form is properly signed in

- relinquishedreceived seetions? l AoL. el Air Bill ,Tracking #s, &

Additional Comnments

_ _ _ .. _ _ _ _ _ _ _ __._"_ .. . . . . h3.. ,

s IK t t(AtD Receipt #_ _ _ _-

Suspected*I1a0rd Information I *If > x2 area background is observed on samples identified as "ton-regulatedinon-radioactive", contact the Radiation Safety group for further I I I = I a I rEal 4jinvestigatiro.

A IRI ilgcalfigc~ikii? VWximum Counts Observed: <, .a.

B IPCB Regulate~ ?.

SWM as Hazardous l" -

ýOrnments: c-C Materiat? If yes, contact Waste iazard' Class Shipped:

-Manager or jSH Manager.

I'fp~t~f~I7~.yTCYtcw of Hazard PM4( laftik1creview of Hazard classification:

clasitifi~atinn Initials Date:5 .- 7z (I

0 SAMPLE RECEIPT & REVIEW FORM 01 PM use only iClient:

Date Receive*d:

Received By:

.J-n Vp U n" , PM(A) Review (waure J____________________________

,JSDARCOC/Work Order: /(2r37-.,

oma-coormbraq ftm,- re**resolved prior to signing):

Sample Receipt Criteria A Comments/Qualirmirs (Required for Non-Conforming Items)

Shipping containers received intact Circle AppW~kble: seals broken damaged container leaking conmimar olber (describe) and sealed? -N=Q-Samples requiring cold Circle Coolanl # ice bags blue ice dry ice odier describe) 2 preservation within (4 +/-- 2 C)?

Record preservation method. l1¢'-,

Chain of custody documents CO U's CY C> v' k+-

included with shipment? ant Sample containers intact and V,.,iruk=e sealit damaged couincr leaking aodiaer sealed? .- (e s27cb Samples requiring chemical Sample IDI,. containers affected and observed pH:

preservation at proper pH?

VOA vials free of headspace Sample ID's ard ontainers affected:

_(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)_

Id's and sens affected:

8 Samples received within holding time?

Sample ID's on COC match ID's Sample ID's and oaminers aftected:

on bottles?

Date & time on COC match date Sample ID's affected:

10 1

& time on bottles?

Number of containers received Sarrie 11's affeteld:

match number indicated on COC?

COC form is properly signed in AC) C -)G5 .at..., V .L OU i 7-relin uished/received sections? -- _I__e_______

Air Bill ,Tracking #'s, & _ C¢f*+/-,Y>UOdJo f0 * .hiL Additional Commnts 0 RAD Receipt Se *af > x2 area background is observed on samples identified as 'non-S eo regulated/non-radioactive*. contact the Radiation Safety group for further OX CA investigation.

A Radiological Cassification. Maximum Counts Observed*:

PBm Regulated? Conunents:

IShi-ppW as 001~ Hazardous i ..

c Material? If yes, contact Waste I Hazard Class Shipped:

iaONs:

PManager or ESH Manager.

.PM (or PMA), nereviewyof_ Hazrl* classification:,

,, _.'" nitials .... n '. Date: **'~-.*/~o',

& %J V

• r

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Health Physics Procedure GPP-GGGR-R5 104-003 -Attachment B-CY-O0 1 Major Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556

)ject Name: Haddam Neck Decommissioning - -

Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Ig 30 D. [] 14 D. [ 7 D.

Samples Shipped Via:

[ Fed Ex LI UPS Hand E] Other Bill of Lading #I

'7q"c '71,6 '3:S

Connecticut Yankee Statement of Work for Analytical Lab Services .CY-ISC-SOW-O01 Figure 1. Sample Check-in List.

Dateime R ived: 5 3 SDg# -:*

Work Order Number:--- LA "J, Shipping Cdntainer ID: 5-'z, '6 3 Chain of Custody #

L. Custody Seals onishipping container intact? .Yes /No[.

2. Custody Seals dated and signed? Yes' ,fNo (1

3. Chain-of-Custody record present? Yes JANo [ ]

'4. Cooler temperature jC , q

5. Vermiculite/packing materials is:

.Wet [W.Dry j-ý]

6.' -Numberofsamples in shipping container:

7. Sample .holding times exceeded?

Yes [ ] No

10. Were any anomalies identified in sample receipt? Yes [ No <

11. . Description of anomalies (include sample numbers): "_-

a numbers):

-Page 25 of 105 111 1

9 SAMPLE RECEIPT & REVIEW FORM ff PM use only Client:I , SDG/ARCOC/Work Order: IGZLt85 DPM(A) Review (ensure non-confo items are resolved prior to signing):

Received By: 19p -_i* * /'- ...

.Sample Receipt Criteria , Z Comments/Qualifiers (Required for Non-Conforming Items)

I Shipping containers received intact Circle Applicable: seals broken damaged container leaking container other (describe) requiring cold Circle Coolan, # ice bags blue ice dry ice nmne other describe)

Samp Spreservati ~dthirn (4 +1- 2 CQ?

Record reserv n method.

-Chain of custody- d n" included with shipment?

4 ISample containers intact and CircIc Applicable: seals broken damaged container leaking container other (describc) sealed?

. lSamples requiring chemical Sample ID's. containe-, affected and observed pH:

preservation at proper pH?

6VOA vials free of headspace NSamle ID's and containers affected:

6 (defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) I ad 8 Samples received within holding and test affect:

lime?

9oSample ID's on COC match ID's Sampl ID's and containe affected:

9on bottles?

10 Date & time on COC match date Sample ID's affected:

& time on bottles?

11 Number of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in 12 relinquished/received sections?

14 Air Bill ,Tracking #'s, &

Additional Comments F' 1q2- ' 19 9*4"a' --

17t.

(1'6>

-T RSO RAD Receipt #

t -if > x2 area background is observed on samples identified as *non-Su ua regulated/non-radioactive", contact the Radiation Safety group for further

'L' investigation.

A lRadiological Classification? / Maximum Couns. Observed*:

_ PCB Regulated? _ Comments:

Shipped as Do'r"Hazardous C Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. UN#:

PM (or PMA) review of Hazard classification: Initials Date:

Fa- t 40 ,01 IUD::'

U

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 I Major Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424

-860-267-2556 iect Name: Haddam

ýContact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D.[] 14 D. [] 7 D.

Samples Shipped Via:

9 Fed Ex El ups LI Hand DI Other Bill of Lading #

92,o- ?.lo- 6Wyf

. Connecticut Yankee CY-ISC-SOW-O01 Statement of Work for Analytical Lab Services C C W Figure 1. Sample Check-in List Datetaime, Received: ~2 ( ~ (

Work Order Number. -

shipping Cdhtfiferl Cf+ C infutd# S (V?{S"-

1. Custody Seals onishipping container intact?,..

-Yes tINo[ 4)

2. Custody Seals dated and signed? Yes*[( No

3. Chain-of-Custody record present?

4.

Yes WL)No [1]

Cooler temperature

_ l i

5. Vermiculite/packing materials is: . Wet VC) Dry [

6: Numbcr of samples in shipping container.' )t". cc) - "

7. Sample holding times cxceeded?

Yes [ No

.8. Samples have.

toja e -hazard labels

• ýcustody seals -appropriate sample labels

9. samples are..,

A1-ngood condition leak ng broken -have air bubbles

10. Were any anomalies identified insample receipt?' Yes []No )

I I.  :.Description of anomalies (include sample nurber)

Samplek Custodiail~abomratzy: 2 ~~j~ . ae./L2/5 Telephoned to:_________ ___B Page 28 of f05

SAMLERECEIPT & REVIEW FORM 70iu P4r e$SML I'm we onl Client:. 1,7 is*,Z8L, SDGIARCOC/Work Order: ,,

Date Receied: PM(A) Review (esure nou-ionfurin itemsare resolved prio to sgunhg):

,eceived By: Ctrle *icd(-I__., . _ ... _ __ _ _ _ _ _

Sample Receipt Criteria CommentslQualifris (Required for Non-Coforming Items) urde Aplicable: wals broken damged conmter leaking container oder (descrie)

Shipping containers received intact and sealed? I r Samples requiring cold Circle Caoam # ice bags blue ice dry ice Q otrdribe) 2 preservation within (4 +/- 2 C)?

0 C Record preservation method.

Chain of custody documents /0COus o.x , \ LA-included with shipment? I-Sample containers intact and sealed? txx(A S V" daraged comaier leaking coma..erud !I Samples requiring chemical in"i ID's. conitaimS affected and obscrved pH:

preservation at proper pH? r VOA vials free of headspace Sample ID'S and cotaiens affecd:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, inunediately deliver to VOA laboratory) .... .......

id's and ,et affected:

9 Samples received within holding time?

Sample ID's on COC match ID's Sample ID'S and coanainems affected:

on bottles?

Date & time on COC match date Sampe ID's affected:

& time on bottles?

Sampl I'S afeced Number of containers received match number indicated on COC?

COC form is properly signed in relinquished/received sections?

no CbC,* "-'L, v.LU I3 . d Air Bill ,Tracking #'s, & . CC'CI+/-)LL6uk- (i JI.--

Additional Comments V RSO RAD Receipt I__

e- as *f > x2 area background is observed on samples identified as -non-Suspected Hazard Information regutd/non-radioactive contact the Radiation Safety group for further logad i investigation.

AJRadiological Classification? Maximum Counts Observed*: 4' Id r.-'[

B IP'C Regulated? Comments:

[Shipped as DOU" Hazardous C Material? If yes, contact Waste , Hazard Class Shipped:

lManager or ESH Manager.

PM (or PMA) review of .Hazardclassification: Initials Date: 1 T 0o D in, Ir .I)-

ari%; 0t)

U 1.*V ,)

11.11. 11,

9 SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM kl", k 1, 7-/,

F32

'S, u( I k 0(--') IM ( il ci4#~ coolp uc*uw?4 Ann+((flsr

-gq'qt q*, __,_____, ___O _ (*1 ) SzeJvq

-qqifCl Sq:5 <:6-% 1{t aq*

,3f*AniZL,  %

--- *'q'b duO*_,-" op 30') ( Cf') n.i

( i4 cjev-v h ad m_'

btsfe ..cl* ' n pm i~ a A c.4' Page 30 of 105 11 [IT

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00367 362 Injun Hollow Road, East Hampton, CT 06424 C 860-267-2556 163-746e' Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only 0 Comments:

(J~ Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones C*.

• • z Priority: Z 30 D. E] 14 D. 1] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code code Comment, Preservation Lab Sample ID 9106-0008-001F 5/05/06 11:13 SE C BP x x x Transferred from COC #2006-00324 9106-0008-003F 5/5/06 13:35 SE C BP X X X Transferred from COC # 2006-00325 9106-0008-004F 5/5/06 13:51 SE C BP X X X Transferred from COC # 2006-00325 9106-0008-005F 5/5/06 14:17 SE C BP X X X Transferred from COC # 2006-00325 9106-0008-006F 5/5/06 14:36 SE C BP X X X Transferred from COC # 2006-00325 9106-0008-006FS 5/5/06 14:36 SE C BP x x x Transferred from COC # 2006-00325 9106-0008-007F 5/5/06 15:03 SE C BP x Transferred from COC #2006-00325 9106-0008-002F 5/5/06 13:10 SE C BP x x x Transferred from COC #2006-00325 NOTES: PO #: 002332 MSR #: 0 6 --0 7q3 SSWP#NA Z LTP QA E Radwaste QA E] Non QA Samples Shipped Via: Internal Container Temp.: __ Deg. C

[ Fed Ex Eups EHand Custody Sealed?

YO NO 1)jRelmq~in* Date/Time 2)*.ived to/Time Custody Seal Intact?

E Other

3) keinquished By Date/Time 4) Redeive~iry v I I~ateiTime YO NO Bill of Lading #

P2? 515z1//(v2-

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 1 Major (D Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00366 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 ____ 1637 11o3-7 L. 7 V_

Project Name: Haddamn Neck Decommissioning C)Comments: Analyses Requested Lab Use Only V Contact Name & %hone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 '

843 556 8171. Attn. Cheryl Jones W Z Priority: Z 30 D. [] 14 D. El 7 D. Conainer Sample Size-Media Type &Type .. ...

Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 1jp 9106-0008-008F 5/08/06 08:01 SE C BP X X X Transferred from COC # 2006-00327 0 9106-0008-009F 5/08/06 08:32 SE C BP X X x Transferred from COC #2006-00327 01i 9106-0008-01OF 5/08/06 09:09 SE C BP X X X Transferred from COC #2006-00327 01*/ 9106-0008-010FS 5/08/06 09:09 SE C BP X x X Transferred from COC # 2006-00327

)l 9106-0008-01 IF 5/08/06 09:30 SE C BP x X X Transferred from CC #2006-00327

)g 9106-0008-012F 5/08/06 09:53 SE C BP X Transferred from COC # 2006-00327

)R 9106-0008-013F 5/08/06 10:16 SE C BP X X x Transferred from COC # 2006-00327 N 9106-0008-014F 5/08/06 10:47 SE C BP X X X Transferred from COC # 2006-00327 NOTES: PO #: 002332 MSR #: 06-6 7 /*3 SSWP# NA SLTP QA Fl Radwaste QA E] Non QA Samples Shipped Via: Internal Container 0 Fed Ex Temp.: *Z-J Deg. C El UPS 0 Hand Custody Sealed?

YO0 N*'

1) Relinquished By Date/Time 2) Received By Date/Time Custody Seal Intact?

D Other

3) Relinquished By Date/Time 4) Received By Date/Time Y5 NO Bill of Lading #

. Connecticut Yankee Lk"7*'/

Statement of Work for Analytical Lab Services CY-ISC-SOW--001 Figure 1. Sample Check-in List DatefTime Received: AQ14t)U _C1)A26J SDG#:

Work Order Number:.

Shipping Container ID:.r. '*q I Chain of Custody #. OO'D (4f')

1. Custody Seals. on'shipping container intact?. Yes [-r-o [1

2. Custody Seals dated and signed? Yesj[ I No [

3. Chain-of-Custody record present? Yes [-j]'Jo [I

.4. Cooler ýtmperature

5. Vermiculite/packing materials is: Wet [IDry  %. A)iAI 6' Number of samples in shipping container: f'

7. Sample holding times exceeded? Yes [ ] No

8. Samples have:'

Zitape *.hazard labels

-custody seals Y_.Zappropriate sample labels

9. Samples are-

• in good condition

.... -leaking broken -have air bubbles

10. Were any anomalies identified in sample receipt? Yes [' No 11.,. .Description. ofanomalies,(include sample numbers):

Telephoned to:___ _ "_By._._._'

Page 33 of 105

sell

• ~S AMPLE RECEIPT & REVIEW FORM

• PA*,--.** 1 PM -eol ber of containers received h number indicated on COC? I form is properly signed in puished/received sections?

Bill ,Trarking #'s, &

litional Comnmems S 6(4 1k 0 RAD Reeipt __"___ ______

> x2 area background is observed on samples identied as non uiatedlnon-radioactivel, contact the Radiation Safety group for findher Observed*: c3p' h-~-- ) -pa&- k~5c lazard Clas Shipped:

NI:

Initials .l2/-~~

Date:

F-Page 34 of 105

SAMPLE RECEIPT & REVIEW FORM "POOR1r,.t PM U Oly Client: Van kee& SDIR0f O rde, /~37i Date Received: 3rLd* IU- PM(A) Review (ensure non1-corormiug items are resolved or to signing):

Received By: C A('* ¢ott) __ ____

Sample Receipt Criteria Z CommentslQualiflers (Required for Non-Conforming Items)

Shipping containers received intac! Circle Applicable: seals broken damaged container leaking container other (describe) and sealed? _ d ecie Sample cl iSamples reqluiring cod requiing - -Circei Coolant # ice bags blue ice dry icc ole ecie 2 preservation within (4 +/- 2 C)?

Record preservation method. ._/ I Chain of custody documents included with shipment?

4Sample containers intact and Circle Applicable: seals broken darmaged container leaking container other (describe) sealed?_______________________________

Samples requiring chemical Sample ID's. containers affecled and observed pH:

- preservation at proper pH?

6 VOA vials free of headspace Sanmle ID's and continers affected:

(defined as < 6mm bubble)?_

Are Encore containers present?

7(If yes, immediately deliver to VOA laboratory).

Id'sand s affeced.

8 Samples received within holding time?

SSample ID 's on COC match ID 's Sam pleID's and commurs affectei:

on bottles?

Date & time on COC match date Sample ID's affected:

& time on bottles? I Number of containers received Sample ID's affected:

match number indicated on COC?

12COC form is properly signed in t o4 " Isfl'L4/Jku d relinquished/received sections?

-41 " /53-/'5-.

14 Air Bill ,Tracking #s, &

Additional Comments

- -Z RSO RAD Receipt #

Suspected Hazard Information = *if> x2 area background is observed on samples identified as 'non-0 regulated/non-radioactive". contact the Radiation Safety group for further Ix 9 investigation.

A lKaG 0logiCal futassiticatlont  !¶" -v IMaximum Counts Observed*: ,

B PCB Regulated?

Shipped as W T Hazardous C Material? If yes, contact Waste Manager or ESH Manager.

L -

Comrents:

Hazard Class Shipped:

UNI:

PM (or PMA) review of Hazard classification: Initials c) Date:

/ /

Page 35 of 105

Connecticut Yankee Statement of Work for Analytical Lab Services cY-iSC-soW-001 Figure 1. Sample Check-in List Date/Time Received: t. 0"/,G @ O "

SDG#:

Work Order Number:

Shipping Cdntainer ID:, 71 Z 5 6 4 1* i 7n Chain of Custody.# " ip " (a.,

1. Custody Seals oni shipping container intact?. -Yes f'0]

2. Custody Seals dated and signed? Yes Lý. o [I -

3. Chaia-of-Custody record present? 'Yes [-o [

4. Cooler temperature [/"

5. Vermiculite/packing materials is: Wet VDry [1%

6.' ;Number of samples in shipping container: h

7. Sample holding times exceeded? Yes-[ ] No

.8. Samples have:

'"tpe ______hazard labels custody seals ____appropriate sample labels

9. Samples are:

_t* in good condition -leaking

-broken -have air bubbles

10. Were any anomaliesidentified in sample receipt? Yes [] No E-<

11. Description of anomalies, (include sample numbers): '

Sample Custodian/Laboratory: ( ,f _2"4 , -. Date:__________________

Telephoned to: On- By_

Page 36 of 105

" .11rý

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 I Major iI1~I5qg 1' 9~~~~ .-

~Chain of Custody Form Connecticut Yankee Atomic Power Company No. 2006-00380 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556

" Project Name: Haddam Neck Decommissioning Analyses Requested LaUse, Only#1 Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories <

2040 Savage Road. Charleston SC. 29407 <

843 556 8171. Attn. Cheryl Jones V)

Priority: Z 30 D. E] 14 D. [] 7 D. Container DI Sample Size-Media Type &Type m I 0 Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0009-016F 5/15/06 13:28 SE C BP x x Transferred from COC 2006-00352 9106-0009-016FS 5/15/06 13:28 SE C BP x x Transferred from COC 2006-00352 9106-0009-017F 5/15/06 14:03 SE C BP X x Transferred from COC 2006-00352 9106-0009-01 IF 5/15/06 08:05 SE C BP x Transferred from COC 2006-00351 9106-0009-013F 5/15/06 08:35 SE C BP X X Transferred from COC 2006-00351 9106-0009-013FS 5/15/06 08:35 SE C BP X X Transferred from COC 2006-00351 1 9106-0009-014F 5/15/06 08:59 SE C BP x Transferred from COC 2006-00351 9106-0009-015F 5/15/06 09:36 SE C BP X X Transferred from COC 2006-00351 NOTES: PO #: 002332 MSR #: 06-OS/' SSWP# NA Z LTP QA EI Radwaste QA ED Non QA Samples Shipped Via: Internal Container

[ Fed Ex Temp.: __ Deg. C LIUPS Hand HI Custody Sealed?

YO] NO 1)Relinquised By Date/Time 2) Re Date/Time Custody Seal Intact?

Mc ' d y El Other

-L

3) Min 11uhh 1 A By1 NE!

uate/ fime 4) Ke eive~I By

/ Date/Time Bill of Lading #

-q71-/f ?6- 2AI YE]

Health Physics Procedure

, ,, /W1'd-J

- l -

5-4.1 -/.

", I GPP-GGGR-R5104-003-Attachment B-CY-001 Major CtChain Connecticut Yankee Atomic Power Company of Custody Form No. 2006-00381 362 Injun Hollow Road, East Hampton, CT 06424 0ý 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only

• Contact Name & Phone: -Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories rn 2040 Savage Road. Charleston SC. 29407 0rn 843 556 8171. Attn. Cheryl Jones 0 z Priority: Z 30 D. [] 14 D.V] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0009-001F 5/11/06 13:22 SE C BP x x Transferred from COC 2006-00347

• 9106-0009-002F 5/11/06 13:46 SE C BP x x Transferred from COC 2006-00347 o4 9106-0009-003F 5/11/06 14:06 SE C BP X x Transferred from COC 2006-00347 1 9106-0009-004F 5/11/06 14:30 SE C BP x . x Transferred from COC 2006-00347 otIt 9106-0009-005F 5/11/06 14:55 SE C BP x X -. Transferred from COC 2006-00347 j*, 9106-0009-007F 5/12/06 07:44 SE C BP x X Transferred from COC 2006-00348 003 9106-0009-008F 5/12/06 08:16 SE C BP X X Transferred from COC 2006-00348

( 9106-0009-009F 5/12/06 08:35 SE C BP X x Transferred from COC 2006-00348 0(

'* 9106-0009-01OF 5/12/06 09:07 SE C BP x x Transferred from COC 2006-00348 NOTES: PO #: 002332 MSR #: 06- SSWP# NA Z LTP QA 71 Radwaste QA E Non QA Samples Shipped Via: Internal Container

[K Fed Ex Temp.: _ Deg. C El UPS M Hand Custody Scaled?

YO ND

1) Relinquished By Date/Time 2) Rece y Date/Time Custody Seal Intact?

J)ReiC ouis By Datc/Tim R

4) , FLO ( m 6 V fl Other

3) Relinquished By Date/Time 4)Received tby Date/Time YO ND Bill of Lading #

!¢lf /yI*z3 r*

Connecticut Yankee Statement of Work for Analytical Lab Services

.cY-1SC-SOw-ooI Figure 1. Sample Check-in List VV 1 Date/Time Received: - - 0 (e SDG#*.*Q.k *-0*

~, o~~i~<

Work Order Number:

Shipping C.ntainer ID: ,' -'I' - Chain of Custody# -c B

1. Custody Seals. oti shipping container intact? -Yes Di No (1

2. Custody Seals dated and signed? Yes[ l No

3. Chain-of-Custody record present? Yes No t ]

.4. Cooler temperature . 0 ,

5. Vermiculite/packing materials is: Wet [1Dry

6. "Number of samples in shipping container:

7. Sample holding times exceeded? Yes K No [ ]

.8. Samples have' Stape " ___hazard labels

( -custody seals - appropriate sample labels 9.9Samples arc:'

i in good condition .. "leaking

. broken have air bubbles

10. Were any anomalies identified in sample receipt? Yes [] No 11....Description of anomalies (include sample numbers): -.

Sample Custodian/Laboratory:-,.2 Date: -,t 0, Telephoned to: On By_

Page 39 of 105

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00349 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories <

2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones 00 z Priority: Z 30 D. [] 14 D. E] 7 D. Container Media Type &Type Sample Desigation Date Time Code Code Code Comment, Preservation Lab Sample ID l 9106-0010-OOIF 5/04/06 10:49 SE C BP X X Transferred from COC 2006-00321 51O 9106-0010-002F 5/04/06 11:12 SE C BP X X Transferred from COC 2006-00321 01 9106-0010-004F 5/04/06 12:48 'SE C BP x X Transferred from COC 2006-00321 p1( 9106-0010-006F 5/04/06 13:34 SE C BP X X Transferred fromCOC_200"-0321 9106-0010-007F 5/04/06 13:21 SE C BP X X Transferred from COC 2006-00321 9106-0010-009F 5/04/06 14:01 SE C BP X X Transferred from COC 2006-00321 9106-0010-019F 5/04/06 14:21 SE C BP X X Transferred from COC 2006-00321

-9106-0010-012F 5/04/06 14:44 SE C BP X X Transferred from COC 2006-00321 9106-0010-013F 5/04/06 15:06 SE C BP X Transferred from COC 2006-00321 NOTES: PO #: 002332 MSR #: 06- 0707 SSWP# NA [9 LTP QA El Radwaste QA [I Non QA Samples Shipped Via: Internal Container

[ Fed Ex Temp.: /7Deg. C EUPS E] Hand Custody.Sealed?

YF', N 0

1) RelinquisheoBy Datefr e 2) cve Date/Time Dy Custody Seal Intact?

[] Other 3)Relinquished By Date ime 4) Received By Date/Time Y 0 0N Bill of Lading #

3 904.-3 iI5-g1

Connecticut Yankee CY-ISC-SOW-001 Statement of Work for Analytical Lab Services Figure 1. Sample Check-in List

,t" -~ I I -

(714: [0/0o Date/Time Received:

-07, *7 Work Order Number:.

Shipping Cdntainer ID: ?1O'1 1I? b3 'l Chain of Custody# . - 6,

1. Custody Seals ori shipping container intact?. -Yes "No[]

2. Custody Seals dated and signed? Yes[.No N]

• 3. Chain-of-Custody record present? Yes [~ No j ]

.4. Cooler temperature (7 C

5. Vermiculite/packing materials is: Wet Pq Dry I "t

6.' Number of samples in shipping container:.

7. Sample holding times exceeded? Yes [ I No P

8. Samples have:

-tape -hazard labels

_._custody seals -appropriate sample labels

9. Samples are:

._ n good condition _ aking

-broken have air bubbles

10. Were any anomalies identified in sample receipt? Yes [ J No PQ 11.. Description of anomalies (include sample numbers):

Sample Custodian/Laboratory:.Date: "-)'1-- 4 Telephoned to: On By. k.

Page 41 of 105

- t1ý,,.,I t

0 SAMPLE RECEIPT & REVIEW FORM ff 6#64vL- PM use only Date Received: PM(A) Review ( e g items a resolved prior to signing):

, ~ - ,

,Received By: A -rsle Sample Sae Receipt Ra Criteria Couments/Qualifiers (Required for Non-Conforming Items)

Z container other (describe)

Circle Applicable: seals broken damaged container leaking I Shipping containers received intact and sealed? I ice bags blue ice dry ice M other describe)

Samples requiring cold Circlc Coolant #

2 preservation within (4 +/- 2 C)?

Record preservation method.

Chain of custody documents included with shipment? __

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking container other (describe) sealed?

5 Samples requiring chemical Sample ID's. containers affected and observed pH:

preservation at proper pH?

Sample ID's and containers affected:

6 VOA vials free of headspace (defined as < 6mm bubble?

Are Encore containers present?

7 (If yes, immediately deliver to

- VOA laboratory) 8 Samples received within holding ld~s and tests affected:

time?

9 Sample ID's on COC match ID's Sampie ID's and containers affected:

9 on bottles?

Sample ID's affected:

10 Date & time on COC match date

& time on bottles?

Sampk ID's affected:

Number of containers received on COC?

match number indicated 12 COC form is properly signed in relinquished/received sections?

14 Air Bill ,Tracking #'s, & 7 0%

Additional Comments 1

, - RSO RAD Receipt At

5 *ff> x2 area background is observed on samples identified as "non-S HI i regulated/non-radioactive", contact the Radiation Safety group for further

• PCBRegul  ? Cinvestigation.

A fRadiological Classification? Maximum Counts Observed*: 6 16 B ]PB Reulatd? *Comments; Shipped as DUT Hazar ouas C Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. UN/:

PM (or PMA) review of Hazard classification: Initials Date: V" 7 .

P" /

Page 42 of 105

List of current GEL Certifications as of 15 August 2006

[ ...

. .. . . State . . . . Certification Alaska UST-062 SArizona AZ0668 Arkansas 88-0651 42D0904046 -

CLIA 01151ICA A California

. ... Ge__ng_*abs .. . . . --I Colorado Connecticut PH-0169 Dept. of Navy NFESC 413 EPA Florida/NELAP E87156 Georgia E97 156 (FIJNELAP)

N/A Idaho Illinois 200029-Indiana C-SC-0 I Kansas E- 10332 Kentucky Maryland 270 Massachusetts -

Michigan 9903 Nevada SC012 New Jersey SCO02 New York 11501

+ North Carolina North Carolina Drinking W 233 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania 68-485 South Carolina 101 20001/i 0585001/l0120002 Tennessee 02934 Texas TX213-2006A U.S. Dept. of Agriculture S-52597 US Army Corps of Engineer N/A Utah -8037697376 GEL Vermont Virginia 00151 Washington C223 Page 43 of 105

RADIOLOGICAL ANALYSIS Page 44 of 105

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 168404 Method/Analysis Information Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555696 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-0117F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201153129 Method Blank (MB) 1201153130 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153131 168340011(9304-01-005C) Matrix Spike (MS) 1201153132 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Page 45 of 105

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 168404003 (9106-0003-004F) was recounted due to high MDA.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 46 of 105

Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 557837 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Sample ID Client ID 168404009 9106-0006-005F 168404010 9106-0008-006F 1201158316 Method Blank (MB) 1201158317 168404009(9106-0006-005F) Sample Duplicate (DUP) 1201158318 168404009(9106-0006-005F) Matrix Spike (MS) 1201158319 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (Q0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404009 (9106-0006-005F).

QC Information Page 47 of 105

All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Alphaspec Pu, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555697 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 48 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201153133 Method Blank (MB) 1201153134 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153135 168340011(9304-01-005C) Matrix Spike (MS) 1201153136 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Guality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Page 49 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- 11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555698 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 50 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OO1F 168404015 9106-0010-012F 1201153137 Method Blank (MB) 1201153138 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153139 168340011(9304-01-005C) Matrix Spike (MS) 1201153140 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (0C) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Page 51 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 556350 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 52 of 105

Sample ID Client ID 168404003 9106-0003-004F 168404004 9106-0003-015F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201154644 Method Blank (MB) 1201154645 168404003(9106-0003-004F) Sample Duplicate (DUP) 1201154646 168404003(9106-0003-004F) Matrix Spike (MS) 1201154647 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 10.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404003 (9106-0003-004F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Page 53 of 105

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Samples 1201154644 (MB), 1201154645 (9106-0003-004F), 1201154646 (9106-0003-004F),

1201154647 (LCS), 168404003 (9106-0003-004F), 168404004 (9106-0003-015F), 168404012 (9106-0009-002F), 168404013 (9106-0009-017F), 168404014 (9106-0010-001F) and 168404015 (9106-0010-012F) were dried and reweighed due to low matrix spike/laboratory control sample recovery.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Tc99, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 554580 Page 54 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201150561 Method Blank (MB) 1201150562 168340012(9304-02-003C) Sample Duplicate (DUP) 1201150563 168340012(9304-02-003C) Matrix Spike (MS) 1201150564 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 13.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Guality Control (0C0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Page 55 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555722 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 56 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201153222 Method Blank (MB) 1201153223 168340012(9304-02-003C) Sample Duplicate (DUP) 1201153224 168340012(9304-02-003C) Matrix Spike (MS) 1201153225 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Page 57 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555723 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 58 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404009 9106-0006-005F 1201153226 Method Blank (MB) 1201153227 168340012(9304-02-003C) Sample Duplicate (DUP) 1201153228 168340012(9304-02-003C) Matrix Spike (MS) 1201153229 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Page 59 of 105

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: LSC, Tritium Dist, Solid-HTD2,ALL FSS Analytical Method: EPA 906.0 Modified Analytical Batch Number: 554582 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OO1F 168404015 9106-0010-012F 1201150569 Method Blank (MB) 1201150570 168340011(9304-01-005C) Sample Duplicate (DUP) 1201150571 168340011(9304-01-005C) Matrix Spike (MS) 1201150572 Laboratory Control Sample (LCS)

Page 60 of 105

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 12.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 168404010 (9106-0008-006F) was recounted due to high MDA.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Page 61 of 105

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint C14, Solid AII,FSS Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 554583 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OO1F 168404015 9106-0010-012F 1201150573 Method Blank (MB) 1201150574 168404003(9106-0003-004F) Sample Duplicate (DUP) 1201150575 168404003(9106-0003-004F) Matrix Spike (MS) 1201150576 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Page 62 of 105

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404003 (9106-0003-004F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

Page 63 of 105

The following data validator verified the information presented in this case narrative:

Reviewer/Date: I§  % * ,

Page 64 of 105

SAMPLE DATA

SUMMARY

Page 65 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOO Connecticut Yankee Atomic Power Co.

Client SDG: 168404 GEL Work Order: 168404 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by Page 66 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-007F Proiect: YANKO 1204 Sample ID: 168404001 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 18-MAY-06 Receive Date: 02-JUN-06 Collector: Client Moisture: 20.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0 .0762 +/-0.102 0.00 +/-0.102 0.0956 pCi/g BXLI 08/11/06 1336 555696 1 Curium-242 U 0.00 +/-0.0995 0.00 +/-0.0995 0.138 pCi/g Curium-243/244 U -0.0 10853 +/-0.0717 0.0405 +/-0.0717 0.177 pCi/g AIphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.199 +/-0.228 0.181 +/-0.229 0.444 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0 .0341 +/-0.129 0.120 +/-0.129 0.323 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 10.0 +/-6.64 5.08 +/-6.72 10.7 pCi/g BXL1 08/16/06 1220 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 4.17 +/-6.67 5.28 +/-6.67 11.4 pCi/g DFAI 08/09/06 1128 554582 4 Liquid Scint C14, SolidAlI,FSS Carbon-14 U 0.0813 +/-0.0797 0.0634 +/-0.0797 0.132 pCi/g ATH2 08/09/06 0324 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 9.90 +/-48.1 32.0 +/-48.1 65.9 pCi/g MXPI 08/12/06 1633 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.02 +/-6.39 5.18 +/-6.40 10.6 pCi/g MXPI 08/11/06 0738 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.139 +/-0.213 0.173 +/-0.213 0.360 pCi/g EGD1 08/11/06 2027 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-11-RC Modified 3 DOE EML HASL-300, Pu-1 I-RC Modified 4 EPA 906.0 Modified Page 67 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-007F Project: YANK01204 Sample ID: 168404001 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA EERF C-01 Modified 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 80 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 100 (15%--125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 98 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 75 (15°/w--125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 74 (15%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 68 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-01 IF Project: YANK01204 Sample ID: 168404002 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 19-MAY-06 Receive Date: 02-JUN-06 Collector: Client Moisture: 17.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.120 +/-0.154 0.0683 +/-0.155 0.251 pCi/g BXLI 08/11/06 1336 555696 1 Curium-242 U -0.0146 +/-0.122 0.0692 +/-0.123 0.303 pCi/g Curium-243/244 U -0.0103 +/-0.0861 0.0487 +/-0.0862 0.213 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.0121 +/-0.125 0.127 +/-0.125 0.344 pCi/g BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0254 +/-0.0675 0.0381 +/-0.0675 0.167 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 6.72 +/-7.02 5.56 +/-7.05 11.7 pCi/g BXLI 08/16/06 1237 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U -0.521 +/-7.03 5.94 +/-7.03 12.8 pCi/g DFAI 08/09/06 1143 554582 4 Liquid Scint C14, Solid All,FSS Carbon-14 U 0.023 +/-0.0828 0.0685 +/-0.0828 0.143 pCi/g ATH2 08/09/06 0426 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 3.93 +/-47.7 31.9 +/-47.7 65.7 pCi/g MXP1 08/12/06 1649 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.52 +/-5.81 4.68 +/-5.81 9.60 pCi/g MXPI 08/11/06 0825 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.173 +/-0.203 0.164 +/-0.203 0.341 pCi/g EGD1 08/11/06 2043 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-11-RC Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 69 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-011F Proiect: YANK01204 Sample ID: 168404002 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-1, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 76 (15°16-12501.)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 100 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 88 (25%o-125°%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15 'o-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25/-,125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 79 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 70 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Project: YANKO 1204 Sample ID: 168404003 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 25-APR-06 Receive Date: 05-MAY-06 Collector: Client Moisture: 23.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.027 +/-0.117 0.153 +/-0.117 0.488 pCi/g BXL1 08/13/06 0819 555696 1 Curium-242 U 0.112 +/-0.315 0.245 +1-0.315 0.781 pCi/g Curium-243/244 U 0.0217 +/-0.206 0.205 +/-0.206 0.594 pCi/g AIphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.061 +/-0.189 0.176 +/-0.189 0.449 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0551 +/-0.103 0.0584 +/-0.103 0.215 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 8.31 +/-5.73 4.40 +/-5.78 9.25 pCi/g BXLI 08/16/06 1253 555698 3 Rad Gas Flow Proportional Counting GFPC,So9o, solid-ALL FSS Strontium-90 U -0.00343 +/-0.0203 0.0172 +/-0.0203 0.036 pCi/g BXFI 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.603 +/-8.25 6.87 +/-8.25 14.8 pCi/g DFA1 08/09/06 1159 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.0937 +/-0.0813 0.0642 +/-0.0813 0.134 pCi/g ATH2 08/09/06 0529 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 7.68 +/-51.2 34.2 +/-51.2 70.4 pCi/g MXPI 08/12/06 1706 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 5.74 +/-7.12 6.58 +/-7.13 13.6 pCi/g MXPI 08/11/06 0912 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.0643 +/-0.198 0.169 +/-0.198 0.351 pCi/g EGDI 08/11/06 2059 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I 1-RC Modified Page 71 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Project: YANKO 1204 Sample ID: 168404003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE EML HASL-300, Pu-I1-RC Modified 4 EPA 905.0 Modified 5 EPA 906.0 Modified 6 EPA EERF C-0I Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-I, Modified 9 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 42 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 92 (15%-125% )

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 113 (25%- 125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 59 (25/.- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 71 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 83 (25%-I125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 76 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded Page 72 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Project: YANKO 1204 Sample ID: 168404003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd The above sample is reported on a dry weight basis.

Page 73 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Proiect: YANKO 1204 Sample ID: 168404004 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 25-APR-06 Receive Date: 05-MAY-06 Collector: Client Moisture: 22.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, SolidALL FSS Americium-241 U 0.0456 +1-0.155 0.139 +/-0.155 0.387 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.113 +/-0.181 0.0733 +/-0.182 0.321 pCi/g Curium-243/244 U 0.180 +/-0.239 0.181 +/-0.240 0.472 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.0196 +/-0.121 0.118 +/-0.121 0.324 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0326 +/-0.0639 0.00 +/-0.064 0.0884 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 6.63 +/-6.19 4.86 +/-6.22 10.2 pCi/g BXLI 08/16/06 1309 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.00477 +/-0.0216 0.0179 +/-0.0216 0.0375 pCi/g BXFI 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 1.03 +/-7.06 5.85 +/-7.06 12.6 pCi/g DFA1 08/09/06 1215 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 0.156 +/-0.0912 0.0699 +/-0.0913 0.146 pCi/g ATH2 08/09/06 0632 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -9.99 +/-42.7 28.7 +/-42.7 59.2 pCi/g MXP1 08/12/06 1722 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 0.939 +/-10.1 10.3 +/-10.1 21.6 pCi/g MXP I 08/11/06 1001 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.237 +/-0.213 0.170 +/-0.213 0.353 pCi/g EGD1 08/11/06 2115 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-lI-RC Modified Page 74 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Project: YANK0 1204 Sample ID: 168404004 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-I, Modified 9 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 78 ( 150/o- 1250/6)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 94 (150-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 101 (25%- 125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 58 (25/- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 75 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 62 (25%-1250/o)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded Page 75 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis

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T .. ~

TT - o .. ... lv -- -

Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Project: YANKO 1204 Sample ID: 168404004 Client ID: YANK001 Vol. Recv.:

Parameter

• Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd The above sample is reported on a dry weight basis.

Page 76 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005F Project: YANKO 1204 Sample ID: 168404005 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 15.4%

Parameter Qualifier Result Uncertainty. LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.036 +/-0.123 0.157 +/-0.123 0.437 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U - -0.0169 +/-0.033 0.080 +/-0.0331 0.350 pCi/g Curium-243/244 U - -0.0129 +/-0.227 0.247 +/-0.227 0.619 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U - -0.0217 +/-0.163 0.181 +/-0.163 0.444 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U - -0.0708 +/-0.0791 0.128 +/-0.0795 0.337 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 9.52 +/-6.00 4.57 +/-6.07 9.61 pCi/g BXLI 08/16/06 1326 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.854 +/-5.88 4.87 +/-5.88 10.5 pCi/g DFAI 08/09/06 1231 554582 4 Liquid Scint C14, SolidAllFSS Carbon- 14 0.347 +/-0.097 0.0674 +/-0.0972 0.141 pCi/g ATH2 08/09/06 0734 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -1.57 +/-46.0 30.7 +/-46.0 63.2 pCi/g MXPI 08/12/06 1738 555722 6 Liquid Scint Ni63, Solid ALL FSS Nickel-63 U 6.39 +/-7.62 7.40 +/-7.62 15.5 pCi/g MXPI 08/11/06 1017 555723 7 LiquidScint Tc99, Solid-ALL FSS Technetium-99 U 0.0198 +/-0.187 0.156 +/-0.187 0.324 pCi/g EGDI 08/11/062131 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 77 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005F Project: YANKO 1204 Sample ID: 168404005 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 65 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 95 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 105 (25%-0125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 78 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 80 (25%o- 125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 80 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 78 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-015F Project: YANK01204 Sample ID: 168404006 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 26.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.10823 +/-0.203 0.178 +/-0.203 0.469 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0.( 0154 +/-0.0301 0.0729 +/-0.0302 0.319 pCi/g Curium-243/244 U -0.' 0994 +/-0.251 0.300 +/-0.251 0.713 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.10466 +/-0.213 0.210 +/-0.213 0.521 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U -0 ).142 +/-0.108 0.191 +/-0.109 0.483 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 6.64 +/-6.53 5.16 +/-6.57 10.8 pCi/g BXLI 08/16/06 1342 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U -2.9 +/-7.59 6.60 +/-7.59 14.2 pCi/g DFAI 08/09/06 1247 554582 4 Liquid Scint C14, SolidAll,FSS Carbon-14 U 0.10352 +/-0.0868 0.0713 +/-0.0868 0.149 pCi/g ATH2 08/09/06 0837 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 1.88 +/-46.8 31.3 +/-46.8 64.4 pCi/g MXPI 08/12/06 1754 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 3.88 +/-7.46 7.40 +/-7.46 15.5 pCi/g MXP1 08/11/06 1033 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.( 0894 +/-0.198 0.163 +/-0.198 0.338 pCi/g EGDI 08/11/06 2147 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 79 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-015F Project: YANKO1204 Sample ID: 168404006 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-1, Modified 7 DOE RESL Ni-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 72 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 72 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 94 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 73 (15%-/125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 80 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 78 (15%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 80 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OIOF Project: YANKO 1204 Sample ID: 168404007 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 56.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -' 0.128 +/-0.0939 0.142 +/-0.0942 0.385 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0 .0115 +/-0.128 0.147 +/-0.128 0.450 pCi/g Curium-243/244 U -0 .0333 +/-0.122 0.149 +/-0.122 0.401 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0 .0548 +/-0.169 0.158 +/-0.170 0.403 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0 .0195 +/-0.121 0.117 +/-0.121 0.322 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 10.4 +/-6.89 5.27 +/-6.97 11.1 pCi/g BXL1 08/16/06 1358 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.00 +/-6.86 5.76 +/-6.86 12.4 pCi/g DFAI 08/09/06 1303 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.0636 +/-0.0801 0.0644 +/-0.0801 0.135 pCi/g ATH2 08/09/06 1017 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 36.1 +/-44.1 28.7 +/-44.1 59.0 pCi/g MXPI 08/12/06 1811 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.26 +/-10.2 10.0 +/-10.2 20.9 pCi/g MXPI 08/11/06 1049 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.05 +/-0.199 0.169 +/-0.199 0.351 pCi/g EGD1 08/11/06 2203 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-] I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 81 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-010F Project: YANK01204 Sample ID: 168404007 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 85 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-/125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 92 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 81 (15°/-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 64 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 77 (15%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 82 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-014F Proiect: YANKO 1204 Sample ID: 168404008 Client ID: YANKOO I Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 32.3%

Parameter Qualifier Rt esult Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0' 0591 +/-0.219 0.231 +/-0.219 0.608 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U - 0.04 +/-0.0554 0.134 +/-0.0557 0.494 pCi/g Curium-243/244 U 0. 0634 +/-0.261 0.249 +/-0.261 0.646 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.0694 +/-0.106 0.160 +/-0.106 0.434 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U -0. 0287 +/-0.098 0.127 +/-0.0981 0.369 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 4.68 +/-8.01 6.48 +/-8.02 13.6 pCi/g BXLI 08/16/06 1415 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 6.02 +/-6.38 4.90 +/-6.38 10.6 pCi/g DFA 1 08/09/06 1319 554582 4 Liquid Scint C14, SolidAllFSS Carbon- 14 U 0.( 0892 +/-0.0827 0.0655 +/-0.0827 0.137 pCi/g ATH2 08/09/06 1424 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 19.8 +/-46.3 30.6 +/-46.3 62.9 pCi/g MXPI 08/12/06 1827 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 5.41 +/-7.91 7.77 +/-7.91 16.2 pCi/g MXPI 08/11/06 1106 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0 '.134 +/-0.192 0.167 +/-0.192 0.346 pCi/g EGDI 08/11/06 2218 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I 1-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 83 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21,2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-014F Project: YANK01204 Sample ID: 168404008 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-1, Modified 7 DOE RESL Ni-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 50 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 61 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 74 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 76 (15%-/125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 84 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005 F Project: YANKO 1204 Sample ID: 168404009 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 28-APR-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 16.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0. 0851 +/-0.136 0.106 +/-0.136 0.390 pCi/g BXL1 08/16/06 0949 557837 1 Curium-242 U -0. 0253 +/-0.0495 0.120 +/-0.0496 0.525 pCi/g Curium-243/244 U -0.10479 +/-0.0542 0.131 +/-0.0545 0.443 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.40183 +/-0.113 0.110 +/-0.113 0.303 pCi/g BXL1 08/11/06 1633 555697 3 Plutonium-239/240 U 0.040122 +/-0.0662 0.0694 +/-0.0662 0.221 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 4.43 +/-5.83 4.67 +/-5.85 9.82 pCi/g BXL1 08/16/06 1431 555698 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U - 2.02 +/-6.67 5.76 +/-6.67 12.4 pCi/g DFAI 08/09/06 1335 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 0p.142 +/-0.0798 0.061 +/-0.0799 0.127 pCi/g ATH2 08/09/06 1719 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 12.6 +/-47.6 31.7 +/-47.6 65.3 pCi/g MXPI 08/12/06 1843 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.70 +/-9.56 9.31 +/-9.56 19.5 pCi/g MXP1 08/11/06 1122 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.01 0659 +/-0.185 0.156 +/-0.185 0.323 pCi/g EGDI 08/11/06 2234 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 DOE EML HASL-300, Pu-11-RC Modified 5 EPA 906.0 Modified Page 85 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005F Project: YANKO 1204 Sample ID: 168404009 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 EPA EERF C-Ol Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-I, Modified 9 DOE EML HASL-300. Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 76 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 93 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 105 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 64 (25%--125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 81 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 86 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006F Project: YANK01204 Sample ID: 168404010 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 34.8%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U ( +/-0.195 0.0758 +/-0.196 0.332 pCi/g BXL1 08/16/06 0949 557837 1 Curium-242 U ( +/-0.202 0.00 +/-0.203 0.280 pCi/g Curium-243/244 U -0. +/-0.0316 0.0766 +/-0.0317 0.335 pCi/g Alphaspec Pu, Solid-ALL FSS pCi/g Plutonium-238 U -0.' +/-0.0711 0.0967 +/-0.0712 0.275 BXL1 08/11/06 1633 555697 3 Plutonium-239/240 U 0.01 +/-0.113 0.118 +/-0.113 0.317 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 14.9 +/-6.37 4.64 +/-6.51 9.75 pCi/g BXL1 08/16/06 1447 555698 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.00 +/-6.06 5.09 +/-6.06 10.7 pCi/g DFAI 08/10/06 2150 554582 5 Liquid Scint C14, SolidAllFSS Carbon- 14 U C1.107 +/-0.0846 0.0664 +/-0.0846 0.139 pCi/g ATH2 08/09/06 1822 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 15.1 +/-41.4 27.5 +/-41.4 56.6 pCi/g MXPI 08/12/06 1900 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0'.258 +/-0.225 0.179 +/-0.225 0.373 pCi/g EGD1 08/11/062251 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 DOE EML HASL-300, Pu-I I-RC Modified 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified Page 87 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006F Project: YANKO 1204 Sample ID: 168404010 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 77 (15%-I125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 94 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 103 (25%-.125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15%-/125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 71 (15%-I125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GCIMS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 88 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-008F Proiect: - YANK01204 Sample ID: 168404011 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 35.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0969 +/-0.192 0.152 +/-0.193 0.426 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0.0482 +/-0.142 0.132 +/-0.142 0.446 pCi/g Curium-243/244 U -0.0576 +/-0.202 0.240 +/-0.203 0.603 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.0397 +/-0.096 0.125 +/-0.096 0.328 pCi/g BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U -0.0315 +/-0.114 0.137 +/-0.114 0.353 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 11.5 +/-6.72 5.08 +/-6.80 10.7 pCi/g BXL1 08/16/06 1504 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.00 +/-5.92 4.97 +/-5.92 10.7 pCi/g DFA1 08/09/06 1407 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 U -0.0238 +/-0.0745 0.0636 +/-0.0745 0.133 pCi/g ATH2 08/09/06 1924 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -10.7 +/-40.9 27.5 +/-40.9 56.8 pCi/g MXPI 08/12/06 1916 555722 6 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.0956 +/-0.211 0.174 +/-0.211 0.361 pCi/g EGDI 08/11/06 2307 554580 7 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300.Am-05-RC Modified 2 DOE EML HASL-300, Pu-11-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified 6 DOE RESL Fe-l, Modified Page 89 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-008F Proiect: YANKO 1204 Sample ID: 168404011 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 7 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 65 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 98 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 96 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 76 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 74 (15%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 90 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 91 06-0009-002F Proiect: YANK01204 Sample ID: 168404012 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 11-MAY-06 Receive Date: 08-JUN-06 Collector: Client Moisture: 33%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -( 0.00144 +1-0.155 0.166 +1-0.155 0.458 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.0192 +/-0.145 0.135 +/-0.145 0.455 pCi/g Curium-243/244 U 0.013 +/-0.268 0.281 +/-0.268 0.687 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -( 0.00587 +/-0.0493 0.0279 +/-0.0494 0.122 pCi/g BXLI 08/11/06 1632 555697 2 Plutonium-239/240 U 0.0186 +/-0.0492 0.0278 +/-0.0493 0.122 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 13.6 +/-6.90 5.13 +/-7.01 10.8 pCi/g BXLI 08/16/06 1520 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.0151 +/-0.0146 0.0114 +/-0.0146 0.0242 pCi/g BXFI 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 4.12 +/-8.36 6.70 +/-8.36 14.5 pCi/g DFAI 08/09/06 1422 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.046 +/-0.0755 0.0613 +/-0.0755 0.128 pCi/g ATH2 08/09/06 2027 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 12.9 +/-40.6 26.8 +/-40.6 55.2 pCi/g MXPI 08/12/06 1932 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.078 +/-0.203 0.168 +/-0.203 0.348 pCi/g EGDI 08/11/06 2323 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-i 1-RC Modified 3 DOE EML HASL-300, Pu-1 1-RC Modified 4 EPA 905.0 Modified Page 91 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-002F Proiect: YANK01204 Sample ID: 168404012 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 61 (15°/-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 98 ( 15%-/125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 94 (25%-/125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 69 (25/-I125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 81 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 92 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - ww.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-017F Project: YANKO 1204 Sample ID: 168404013 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 15-MAY-06.

Receive Date: 08-JUN-06 Collector: Client Moisture: 28.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0. +/-0.242 0.230 +/-0.243 0.574 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0. +/-0.220 0.171 +/-0.220 0.509 pCi/g Curium-243/244 U -( +/-0.214 0.256 +/-0.214 0.627 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.C +/-0.0529 0.0299 +/-0.0529 0.131 pCi/g BXLI 08/11/06 1632 555697 2 Plutonium-239/240 U 0. +/-0.0513 0.00 +/-0.0514 0.0709 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 +/-6.66 4.95 +/-6.77 10.4 pCi/g BXLI 08/16/06 1536 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0. +/-0.0151 0.0116 +/-0.0151 0.0246 pCi/g BXFI 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U I +/-7.98 6.65 +/-7.98 14.4 pCi/g DFAI 08/09/06 1438 554582 5 Liquid Scint C14, Solid All, FSS Carbon-14 U 0. +/-0.0759 0.0625 +/-0.0759 0.131 pCi/g ATH2 08/09/06 2129 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U --61.9 +/-150 102 +/-150 210 pCi/g MXPI 08/12/06 1949 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0. 0628 +/-0.200 0.165 +/-0.200 0.343 pCi/g EGD1 08/11/06 2338 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified Page 93 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-017F Project: YANKO 1204 Sample ID: 168404013 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 64 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu24 l, Solid-ALL Fý 96 (25%-125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 72 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 73 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 79 (15%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 94 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-001F Proiect: YANKO 1204 Sample ID: 168404014 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 17-MAY-06 Collector: Client Moisture: 27.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0 +/-0.227 0.238 +/-0.227 0.628 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0. +/-0.167 0.00 +/-0.168 0.231 pCi/g Curium-243/244 U 0. +/-0.242 0.241 +/-0.242 0.634 pCi/g Alphaspec Pu, Solid ALL FSS Plutonium-238 U ( +/-0.181 0.143 +/-0.182 0.331 pCi/g BXLI 08/11/06 2250 555697 2 Plutonium-239/240 U -0. +/-0.0865 0.0951 +/-0.0866 0.235 pCi/g Liquid Scint Pu241, Solid ALL FSS Plutonium-241 13.0 +/-6.44 4.78 +/-6.54 10.0 pCi/g BXLI 08/16/06 1553 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0. 0128 +/-0.0141 0.0125 +/-0.0141 0.0262 pCi/g BXF1 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium L 0.548 +/-7.50 6.25 +/-7.50 13.5 pCi/g DFAI 08/09/06 1454 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 L 0.0555 +/-0.0809 0.0655 +/-0.0809 0.137 pCi/g ATH2 08/09/06 2232 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 L -18.1 +/-47.6 32.3 +/-47.6 66.6 pCi/g MXPI 08/12/06 2005 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.134 +/-0.205 0.167 +/-0.205 0.347 pCi/g EGD1 08/11/06 2354 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I 1-RC Modified 3 DOE EML HASL-300, Pu-11 -RC Modified 4 EPA 905.0 Modified Page 95 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-00IF Proiect: YANK01204 Sample ID: 168404014 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 50 (15%-/125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 85 (15°-/125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL F5 99 (25%- 125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 74 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 70 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 96 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-012F Proiect: YANKO 1204 Sample ID: 168404015 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 17-MAY-06 Collector: Client Moisture: 28.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis AIphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.110 +/-0.184 0.140 +/-0.184 0.386 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0.0547 +/-0.141 0.192 +/-0.141 0.544 pCi/g Curium-243/244 U -0.126 +/-0.184 0.245 +/-0.185 0.597 pCi/g AIphaspec Pu, Solid-ALL FSS Plutonium-238 U -( 0.00157 +/-0.126 0.122 +/-0.126 0.291 pCi/g BXLI 08/11/06 2250 555697 2 Plutonium-239/240 U 0.0867 +/-0.0869 0.0406 +/-0.0872 0.128 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 8.31 +/-6.16 4.77 +/-6.21 10.0 pCi/g BXL1 08/16/06 1609 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.0 0771 +/-0.0144 0.0124 +/-0.0144 0.0263 pCi/g BXF1 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid HTD2,ALL FSS Tritium U 01.896 +/-6.17 5.11 +/-6.17 11.0 pCi/g DFAI 08/09/06 1510 554582 5 Liquid Scint C14, SolidAlLFSS Carbon-14 U 0.0162 +/-0.0763 0.0633 +/-0.0763 0.132 pCi/g ATH2 08/09/06 2334 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 23.3 +/-49.3 32.5 +/-49.3 67.0 pCi/g MXPI 08/12/06 2021 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.0577 +/-0.206 0.171 +/-0.206 0.354 pCi/g EGD1 08/12/06 0010 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified Page 97 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-012F Project: YANK01204 Sample ID: 168404015 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 81 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 99 (25%-0125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 68 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 74 (15%-0125/%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-/125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 98 of 105

I~. I QUALITY CONTROL DATA Page 99 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Reoort Date: August 21, 2006 Client: Connecticut Yankee Atomic Power Page 1 of 6 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 168404 PnrmnasmP NA*M S*rnmnle A nil A) C Units RPD% REC% Range Anist Date Time Parmname NOM Sam r le Oual Rad Alpha Spec Batch 555696 QC1201153130 168340011 DUP Americium-241 U -0.000522 U 0.0578 pCi/g 204 (0%- 100%) BXLI 08/11/06 14:34 Uncert: +/-0.0385 +/-0.278 TPU: +/-0.0385 +/-0.279 Curium-242 U 0.00 U -0.0405 pCi/g 200 (0%- 100%)

Uncert: +/-0.0756 +/-0.0562 TPU: +/-0.0756 +/-0.0565 Curium-243/244 U -0.0177 U -0.0517 pCi/g 98 (0%- 100%)

Uncert: +/-0.0764 +/-0.257 TPU: +/-0.0765 +/-0.257 QC1201153132 LCS.

Americium-241 12.8 12.8 pCi/g 100 (75%-125%)

Uncert: +/- 1.84 TPU: +/-2.70 Curium-242 U -0.0328 pCi/g Uncert: +/-0.0454 TPU: +/-0.0457 Curium-243/244 15.5 14.3 pCi/g 92 (75%-125%)

Uncert: +/-1.94 TPU: +/-2.92 QC1201153129 MB Americium-241 U 0.0471 pCi/g Uncert: +/-0.157 TPU: +/-0.157 Curium-242 U -0.0469 pCi/g Uncert: +/-0.0459 TPU: +/-0.0464 Curium-243/244 U -0.00385 pCi/g Uncert: +/-0.210 TPU: +/-0.210 QC1201153131 168340011 MS Americium-241 13.3 U -0.000522 12.0 pCi/g 91 (75%-125%)

Uncert: +/-0.0385 +/-1.38 TPU: +/-0.0385 +/-2.08 Curium-242 U 0.00 U 0.0427 pCi/g Uncert: +/-0.0756 +/-0.0837 TPU: +/-0.0756 +/-0.0839 Curium-243/244 16.1 U -0.0177 15.9 pCi/g 99 (75%-125%)

Uncert: +/-0.0764 +/-1.58 TPU: +/-0.0765 +/-2.61 Batch 555697 QC1201153134 168340011. DUP Plutonium-238 U -0.0155 U 0.0237 pCi/g 956 (0%- 100%) BXLI 08/11/06 22:51 Page 100 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 2 of 6 Parmname NOM 5Samnle 011al OC UJnits~ RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 555697 Uncert: +/-0.0215 +/-0.0465 TPU: +/-0.0216 +/-0.0466 Plutonium-239/240 U 0.0414 U -0.0489 pCi/g 2410 (0%- 100%)

Uncert: +/-0.0934 +/-0.124 TPU: +/-0.0935 +/-0.124 QC1201153136 LCS Plutoniurn-238 U 0.155 pCi/g (75%-125%)

Uncert: +/-0.141 TPU: +/-0.142 Plutonium-239/240 11.8 11.5 pCi/g 98 (75%-125%)

Uncert: +/-0.856 TPU: +/-1.32 QC1201153133 MB Plutonium-238 U 0.0552 pCi/g 08/11/06 22:50 Uncert: +/-0.186 TPU: +/-0.186 Plutonium-239/240 U -0.0978 pCi/g Uncert: +/-0.0892 TPU: +/-0.0899 QC1201153135 168340011 MS Plutonium-238 U -0.0155 U 0.0539 pCi/g (75%-125%) 08/11/06 22:51 Uncert: +/-0.0215 +/-0.112 TPU: +/-0.0216 +/-0.112 Plutonium-239/240 12.3 U 0.0414 10.3 pCi/g 84 (75%-125%)

Uncert: +/-0.0934 +/-0.796 TPU: +/-0.0935 +/-I.19 Batch 555698 QC1201153138 168340011 DUP Plutonium-241 U 7.28 U 10.1 pCi/g 0 (0% - 100%) BXL I 08/16/06 16:41 Uncert: +/-6.30 +/-6.39 TPU: +/-6.35 +/-6.46 QC1201153140 LCS Plutonium-241 137 145 pCi/g 106 (75%-125%) 08/16/06 17:14 Uncert: +/-12.5 TPU: +/-19.9 QCI201153137 MB Plutonium-241 U 8.57 pCi/g 08/16/06 16:25 Uncert: +/-6.93 TPU: +/-6.98 QC1201153139 168340011 MS Plutonium-241 138 U 7.28 142 pCi/g 103 (75%-125%) 08/16/06 16:58 Uncert: +/-6.30 +/-12.4 TPU: +/-6.35 +/-19.7 Batch 557837 QC1201158317 168404009 DUP Americium-241 U -0.0851 U 0.167 pCi/g 616 (0%- 100%) BXLI 08/16/06 09:49 Uncert: +/-0.136 +/-0.220 TPU: +/-0.136 +/-0.221 Curium-242 U -0.0253 u 0.241 pCi/g 247 (0%- 100%)

Page 101 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 3 of 6 Pa.rmnnme NOmI '-amnle 012al QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 557837 Uncert: +/-0.0495 +/-0.334 TPU: +/-0.0496 +/-0.335 Curiumn-243/244 U -0.0479 U 0.0761 pCi/g 879 (0%- 100%)

Uncert: +/-0.0542 +/-0.149 TPU: +/-0.0545 +/-0.149 QC1201158319 LCS Americium-241 24.5 25.4 pCi/g 104 (75%-125%)

Uncert: +/-2.47 TPU: +/-4.16 Curium-242 U 0.0477 pCi/g Uncert: +/-0.127 TPU: +/-0.127 Curium-243/244 29.7 27.0 pCi/g 91 (75%-125%)

Uncert: +/-2.54 TPU: +/-4.38 QC1201158316 MB Americium-241 U 0.234 pCi/g Uncert: +/-0.275 TPU: +/-0.277 Curium-242 U 0.00 pCi/g Uncert: +/-0.152 TPU: +/-0.152 Curiumn-243/244 U -0.0551 pCi/g Uncert: +/-0.0624 TPU: +/-0.0628 QC1201158318 168404009 MS Americium-241 26.4 U -0.0851 29.1 pCi/g 110 (75%-125%)

Uncert: +/-0.136 +/-2.97 TPU: +/-0.136 +/-5.01 Curium-242 U -0.0253 U 0.126 pCi/g Uncert: +/-0.0495 +/-0.247 TPU: +/-0.0496 +/-0.248 Curium-243/244 32.4 U -0.0479 31.7 pCi/g 98 (75%-125%)

Uncert: +/-0.0542 +/-3.12 TPU: +/-0.0545 +/-5.39 Rad Gas Flow Batch 556350 QC1201154645 168404003 DUP Strontium-90 U -0.00343 U -0.00637 pCi/g 0 (0% - 100%) BXFI 08/14/06 08:33 Uncert: +/-0.0203 +/-0.0152 TPU: +/-0.0203 +/-0.0152 QC1201154647 LCS Strontium-90 1.56 1.30 pCi/g 83 (75%-125%)

Uncert: +/-0.0563 TPU: +/-0.0881 QC1201154644 MB Strontium-90 U 0.0176 pCi/g Uncert: +/-0.018 TPU: +/-0.018 Page 102 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 4 of 6 Parmname NOM Sample Oual (C Units RPD% REC% Range Anist Date Time Rad Gas Flow Batch 556350 QC1201154646 168404003 MS Strontium-90 1.58 U -0.00343 1.29 pCi/g 82 (75%-125%)

Uncert: +/-0.0203 +/-0.0535 TPU: +/-0.0203 +/-0.0813 Rad Liquid Scintillation Batch 554580 QC1201150562 168340012 DUP Technetium-99 U 0.0338 U 0.266 pCi/g 0 (0% - 100%) EGDI 08/12/06 00:42 Uncert: +/-0.192 +/-0.226 TPU: +/-0.192 +/-0.226 QC]201150564 LCS Technetium-99 13.1 13.6 pCi/g 103 (75%-125%) 08/12/06 01:14 Uncert: +/-0.496 TPU: +/-0.599 QCI201150561 MB Technetium-99 U 0.0311 pCi/g 08/12/06 00:26 Uncert: +/-0.177 TPU: +/-0.177 QC1201150563 168340012 MS Technetium-99 13.0 U 0.0338 12.0 pCi/g 92 (75%-125%) 08/12/06 00:58 Uncert: +/-0.192 +/-0.523 TPU: +/-0.192 +/-0.602 Batch 554582 QC1201150570 168340011 DUP Tritium U 1.77 U 1.62 pCi/g 0 (0% - 100%) DFA I 08/09/06 15:42 Uncert: +/-8.20 +/-7.47 TPU: +/-8.20 +/-7.47 QC1201150572 LCS Tritium 68.3 76.2 pCi/g 111 (75%-125%) 08/09/06 16:14 Uncert: +/-14.0 TPU: +/-14.1 QC1201150569 MB Tritium U 0.586 pCi/g 08/09/06 15:26 Uncert: +/-8.01 TPU: +/-8.01 QC1201150571 168340011 MS Tritium 61.3 U 1.77 61.8 pCi/g 101 (75%-125%) 08/09/06 15:58 Uncert: +/-8.20 +/-12.2 TPU: +/-8.20 +/-12.3 Batch 554583 QC1201150574 168404003 DUP Carbon- 14 U 0.0937 U 0.0422 pCi/g 0 (0%- 100%) ATH2 08/10/06 01:39 Uncert: +/-0.0813 +/-0.075 TPU: +/-0.0813 +/-0.0751 QC1201150576 LCS Carbon- 14 7.27 7.14 pCi/g 98 (75%-125%) 08/10/06 03:00 Uncert: +/-0.508 TPU: +/-0.520 QC1201150573 MB Page 103 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn QC Summary Workorder: 168404 Page 5 of 6 Parmname NOM Sample Qal QC Units RPD% REC% Range Anist Date Time Rad Liquid Scintillation Batch 554583 Carbon- 14 U -0.0315 pCi/g Uncert: +/-0.0776 TPU: +/-0.0776 QC1201150575 168404003 MS Carbon- 14 15.1 U 0.0937 13.8 pCi/g 92 (75%-125%) 08/10/06 02:43 Uncert: +/-0.0813 +/-1.00 TPU: +/-0.0813 +/-1.03 Batch 555722 QC1201153223 168340012 DUP Iron-55 U -26.5 U 5.83 pCi/g 0 (0% - 100%) vIXPI 08/12/06 20:54 Uncert: +/-65.1 +/-36.9 TPU: +/-65.1 +/-36.9 QC1201153225 LCS Iron-55 641 660 pCi/g 103 (75%-125%) 08/12/06 21:27 Uncert: +/-56.2 TPU: +/-67T2 QCI201153222 MB Iron-55 U 18.2 pCi/g 08/12/06 20:38 Uncert: +/-39.6 TPU: +/-39.6 QC1201153224 168340012 MS Iron-55 717 U -26.5 688 pCi/g 96 (75%-125%) 08/12/06 21:11 Uncert: +/-65.1 +/-60.2 TPU: +/-65.1 +/-71.6 Batch 555723 QC1201153227 168340012 DUP Nickel-63 U 3.79. U 6.68 pCi/g 0 (0% - 100%) vAXPI 08/11/06 11:55 Uncert: +/-5.39 +/-7.43 TPU: +/-5.40 +/-7.43 QC1201153229 LCS Nickel-63 512 479 pCi/g 94 (75%-125%) 08/11/06 12:27 Uncert: +/-22.4 TPU: +/-27.1 QC1201153226 MB Nickel-63 U 15.7 pCi/g 08/11/06 11:38 Uncert: +/-9.92 TPU: +/-9.93 QC1201153228 168340012 MS Nickel-63 530 U 3.79 511 pCi/g 96 (75%-125%) 08/11/06 12:11 Uncert: +/-5.39 +/-23.5 TPU: +/-5.40 +/ -28.7 Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported Result is greater than value reported Page 104 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 6 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 105 of 105

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Attachment 2b Split Sample Assessment Forms (2 Pages)

Comiecticut Yankee Decommissioning Project Health 24265-000-GPR-GGGR-R5124-000 Attachment A Physics Procedure Split Sample Assessment Form Survey Area Survey 0005 Survey Discharge Canal

1. 9106 Unit #: Unit Name:

Sample Plan or WPIR#: 2006-021 SML #: 9106-0005-003 Sample

Description:

Comparison of split samples collected from sample measurement location #03 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The standard sample was 9106-0005-003F the comparison sample was 9106-0005-003FS.

STANDARD COMPARISON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable (Y/N)

Value Error Range Value Error Ratio Cs-137 3.39E-02 1.89E-02 2 NONE- 3.31E-01 2.67E-02 9.76 N/A Co-60 3.15E-01 1.76E-02 18 0.75- 1.33 6.18E-01 3.69E-02 1.96 N Sr-90 1.15E-02 3.23E-03 4 0.50- 2.00 4.13E-03 4.35E-03 0.36 N/A K-40 1.11E+0I 4.20E-01 26 0.75 1.33 1.16E+01 4.38E-01 1.05 Y Comments/Corrective Actions: In consideration of Cs- 137 results, guidance for agreement ranges, obtained from USNRC Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of acceptability for such rations is not appropriate. Since Co-60 has a likelyhood to be present in the sample matrix in particulate form, one would not neccassarily expect it to be Table is provided to show acceptance criteria used homogenuously mixed from processing of the sample-split aliqot. to assess split samples.

Regarding Sr-90 results, the guidance is primarily intended for use with gamma spectroscopy (Sr-90 was measured using liquid scintillation). Resolution Agreement Range Consequently, a much smaller quantity of media was used for the 4 7 0.50 2.00 analyses from the sample and its split (on the order of 1 gram). A much 8 15 0.60 1.66 higher level of sample homogenization than is routinely performed 16 50 0.75 1.33 would be required to achieve consistent agreement. While the measurement and sample preparation methodology is appropriate for 51 200 0.80 1.25 FSS purposes, the cited guidance considers that the sample > 200 0.85 1.18 methodology may not be well suited for sample analyses by means other than gamma spectroscopy. As K-40 was found to be present in both samples at an acceptable level of agreement, no further action is warranted.

Performed By: Date: Reviewed By: Date:

I WPIR - Work Plan and Inspection Record Z

SML - Sample Measurement Location designation Page I of I

Connecticut Yankee Decommissioning Project Health 24265-000-GPR-GGGR-R5124-000 Attachment A Physics Procedure Split Sample Assessment Form Survey SSurvey 0005 urvey Unit Discharge Canal Area#: 90 it #: Name:

Sample Plan or WPIR#: 2006-0021 SML #: 9106-0005-018 Sample

Description:

Comparison of split samples collected from sample measurement location #18 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The standard sample was 9106-0005-018F, the comparison sample was 9106-0005-018FS.

STANDARD COMPARISON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable (Y/N)

Value Error Range Value Error Ratio Cs-137 3.39E-02 1.54E-02 2 N/A 1.05E-01 3.98E-02 3.10 N/A Co-60 4.19E-02 1.62E-02 3 N/A 0.OOE+00 7.25E-02 0.00 N/A Sr-90 5.37E-02 7.20E-03 8 0.60- 1.66 4.84E-03 4.30E-03 0.09 N/A K-40 1.11E+01 4.20E-01 26 0.75- 1.33 1.16E+01 4.38E-01 1.05 Y C.omments/Corrective Actions: In consideration ot Cs-13'7 and Co-60 results, guidance for agreement ranges, obtained from USNRC Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of acceptability for such rations is 1 4 1 not appropriate. K-40 was found to be present in both samples at an acceptable level of agreement. Regarding Sr-90 results, the guidance Table is provided to show acceptance criteria used is primarily intended for use with gamma spectroscopy (Sr-90 was to assess split samples.

measured using liquid scintillation). Consequently, a much smaller quantity of media was used for the analyses from the sample and its Resolution Agreement Range split (on the order of 1 gram). A much higher level of sample homogenization than is routinely performed would be required to 4 7 0.50 2.00 achieve consistent agreement. While the measurement and sample 8 15 0.60 1.66 preparation methodology is appropriate for FSS purposes, the cited 16 50 0.75 1.33 guidance considers that the sample methodology may not be well suited for sample analyses by means other than gamma spectroscopy. 51 200 0.80 1.25 No further action is warranted. > 200 0.85 1.18 Perfonned By:

,5ý X'Zee' WPIR - Work Plan and Inspection Record /

SML - Sample Measurement Location designation Page I of I

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Attachment 2c Preliminary Data Forms (2 Pages)

Health Physics Procedure GPP-GGGR-R512 1-001 Attachment B, Rev. CY-00 I MAJOR Health Physics Procedure GPP-GGGR-R5121-001 Attachment B, Rev. CY-001 MAJOR Preliminary Data Review Form - Samples for the Sign Test Survey Unit: 9106- 0005 Survey Unit Name: Discharge Canal Classification: 2 Survey Media: Soil Type of Survey: Final Status Survey Type of Measurement: Radionuclide Specific Number of Measurements: 15 Operational DCGL: 1 BASIC STATISTICAL QUANTITIES Cs-137 Co-60 Sr-90 Minimum Value: -2.55E-02 -7.92E-03 -1.93E-03 Maximum Value: 4.73E-01 1.38E+00 5.37E-02 Mean: 1.33E-01 2.49E-01 9.79E-03 Median: 7.09E-02 4.19E-02 6.68E-03 Standard Deviation: 1.34E-01 4.25E-01 1.33E-02 RADIONUCLIDE CONCENTRATION (pCi/g)

NUMBER Cs-137 Co-60 Sr-90 Identified? Identified? Identified?

9106-0005-001F 2.88E-02 1.91 E-02 5.10E-03 Y N N 9106-0005-002F 6.60E-02 8.95E-02 8.79E-03 Y Y N 9106-0005-003F 3.09E-01 3.15E-01 1.15E-02 Y Y Y 9106-0005-004F 1.63E-01 2.10E-01 6.21 E-03 Y Y N 9106-0005-005F -2.55E-02 9.87E-03 9.56E-03 N N Y 9106-0005-007F -5.19E-04 -7.92E-03 5.15E-03 N N N 9106-0005-008F 1.86E-01 1.69E-01 -1.56E-03 Y Y N 9106-0005-009F 1.81E-01 2.14E-02 1.30E-02 Y N Y 9106-0005-01OF 2.60E-01 1.38E+00 1.34E-02 Y Y Y 9106-0005-01 IF 5.76E-02 O.OOE+00 1.49E-02 Y N Y 9106-0005-013F 5.31 E-02 1.55E-02 -1.93E-03 Y N N 9106-0005-014F 4.73E-01 1.12E+00 3.27E-03 Y Y N 9106-0005-015F 7.09E-02 2.78E-03 6.68E-03 Y N N 9106-0005-017F 1.39E-01 3.43E-01 -8.59E-04 Y Y N 9106-0005-018F 3.39E-02 4.19E-02 5.37E-02 Y Y Y Performed By: Date: .- 2g-o*

Date: /6-0D(

Health Physics Procedure 24265-000-GPP-GGGR-R5123-000-Rev.CY-000 Attachment B Health Physics Procedure 24265-000-GPP-GGGR-RS 123 -000-Rev.CY-O00 Attachment B Preliminary Data Review Form - Judgemental Samples Survey Unit: 9106- 0005 Survey Unit Name:

Discharge Canal Classification: 2 Survey Media: Soil Type of Survey: Final Status Survey Type of Measurement: Radionuclide Specific Number of Measurements: 1 Operational DCGL: 1 BASIC STATISTICAL QUANTITIES Cs-137 Co-60 Sr-90 Minimum Value: -1.86E-02 2.07E-03 9.07E-04 z

Maximum Value: -1.86E-02 2.07E-03 9.07E-04 Mean: -1.86E-02 2.07E-03 9.07E-04 Median: -1.86E-02 2.07E-03 9.07E-04 Standard Deviation: 1.36E-01 4.55E-02 3.01E-02 RADIONUCLIDE CONCENTRATION (pCi/g)

NUMBER Cs-137 Co-60 Sr-90 Identified?

9106-0005-016F -1.86E-02 2.07E-03 9.07E-04 N N N Performed By: Date: /a - 2, -4ý9 Independent Review: Z,,

_ _.,"_ Date: 6 0

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Attachment 2d Graphical Representation of Data (6 Pages)

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Quantile Plot For Cesium - 137 Survey Unit: 9106-0005 Survey Unit Name: Discharge Canal Mean: 1.33E-01 pCi/g 5.OOE-01 4.OOE-01 L 3.OOE-01 0

2.OOE-01 Q 1.OOE-01 0

o O.OOE+00

-1.OOE-01 Percentage Cs-1 37 Rank Percentage

-2.55E-02 1 3 %

-5.19E-04 2 10 %

2.88E-02 3 17 %

3.39E-02 4 23 %

5.31 E-02 5 30 %

5.76E-02 6 37 %

6.60E-02 7 43 %

7.09E-02 8 50 %

1.39E-01 9 57 %

1.63E-01 10 63 %

1.81E-01 11 70 %

1.86E-01 12 77 %

2.60E-01 13 83 %

3.09E-01 14 90 %

4.73E-01 15 97 %

Prepared By: Date: ,*2-2, - d Reviewed By: f/ i Date:

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Quantile Plot For Cobalt - 60 Survey Unit: 9106-0005 Survey Unit Name: Discharge Canal Mean: 2.49E-01 pCi/g 1.60E+00 1.40E+00 , -

1.20E+00 o 1.OOE+O0 o 8.OOE-01

._ 6.OOE-01 - -

4' 4.OOE-01 o0 2.OOE-01 , -

O.OOE + 0 0 _ 40 0 0-

-2.OOE-01 -- 2--n - 6)80I Percentage Co-60 Rank Percentage

-7.92E-03 1 3 %

0.OOE+00 2 10 %

2.78E-03 3 17 %

9.87E-03 4 23 %

1.55E-02 5 30 %

1.91E-02 6 37 %

2.14E-02 7 43 %

4.19E-02 8 50 %

8.95E-02 9 57 %

1.69E-01 10 63 %

2.10E-01 11 70 %

3.15E-01 12 77 %

3.43E-01 13 83 %

1.12E+00 14 90 %

1.38E+00 15 97 %

Prepared By: z9e-y * ,-'-".

-- A Date: la- 2e-01=,

Reviewed By: Date: / -0*.*z ld V

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Quantile Plot For Strontium - 90 Survey Unit: 9106-0005 Survey Unit Name: Discharge Canal Mean: 9.79E-03 pCi/g 6.OOE-02 5.OOE-02 4.OOE-02

0. S3.00E-02 t.,- 2.OOE-02 -

C 1.OOE-02 -- - -

0.00E+O00,,,8* I 2jýj 8 iO

-1.OOE-02 Percentage Sr-90 Rank Percentage

-1.93E-03 1 3 %

-1.56E-03 2 10 %

-8.59E-04 3 17 %

3.27E-03 4 23 %

5.10E-03 5 30 %

5.15E-03 6 37 %

6.21E-03 7 43 %

6.68E-03 8 50 %

8.79E-03 9 57 %

9.56E-03 10 63 %

1.15E-02 11 70 %

1.30E-02 12 77 %

1.34E-02 13 83 %

1.49E-02 14 90 %

5.37E-02 15 97 %

Prepared By:- Date: /2-Reviewed By: Date: 4/2 --,e6O0

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Cobalt-60 Survey Unit: 9106-0005 Survey Unit Name: Discharge Canal Mean: 0.249 pCi/g 10 8-I 6 t Cr 4 0) .

.1 I¸ L.

L.

2 0 -I 0.00 0.25 0.50 0.75 1.00 1.25 1.50 Upper End Value (pCilg)

Upper End Observation Observation %

Value Frequency Frequency 0.00 2 13%

0.25 9 60%

0.50 2 13%

0.75 0 0%

1.00 0 0%

1.25 1 7%

1.50 1 7%

Total 15 100%

Prepared By: Date: /0- 30-601 Reviewed By: Date: / 4)- 3-0 -6 6,

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Cs - 137 Survey Unit: 9106-0005 Survey Unit Name: Discharge Canal Mean: 0.133 pCi/g Upper End Observation Observation %

Value Frequency Frequency 0.10 8 53%

0.20 4 27%

0.30 1 7%

0.40 1 7%

0.50 1 7%

Total 15 100%

Prepared By: Date: /10-30Q-Q)

/0- -7 Reviewed By: Date:

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Sr -90 Survey Unit: 9106-0005 Survey Unit Name: Discharge Canal Mean: 0.010 pCi/g 12 10-S6-

"m4 U-2-

0.01 0.02 0.03 0.04 0.05 0.06 Upper End Value (pCi/g)

Upper End Observation Observation %

Value Frequency Frequency 0.01 10 67%

0.02 4 27%

0.03 0 0%

0.04 0 0%

0.05 0 0%

0.06 1 7%

Total 15 100%

Prepared By: ,rý, Date:

Reviewed By: Date: {oi .

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Attachment 2e Sign Test Calculation (1 Page)

Health Physics Procedure GPP-GGGR-R512 1-000 Attachment A, Rev. CY-00 I MAJOR Sign Test Calculation Sheet For Multiple Radionuclisdes Survey Unit Number: 9106-0005 Survey Unit Name: Discharge Canal WP&IR#: 2006-021 Classification : 2 I TYPE I (c error):0.05 TYPE I (3 error):0.051 Radionuclides: Cs-137 Co-60 Survey Design DCGL (pCi/g): 6.0116 2.8956 Results Cs-137 Results Co-60 Weighted Sum (W,) DCGL-Result Sign 2.88E-02 1.91E-02 1.57E-02 9.84E-01 I 6.60E-02 8.95E-02 4.93E-02 9.5 1E-01 3.09E-01 3.15E-01 1.70E-0 1 8.30E-01 1.63E-01 2.1 OE-0 I 1.05E-01 8.95E-01

-2.55E-02 9.87E-03 7.28E-03 9.93E-01

-5.19E-04 -7.92E-03 1.55E-03 9.98E-01 1 1.86E-01 1.69E-0 I 8.80E-02 9.12E-01 1.81E-01 2.14E-02 4.85E-02 9.5 1E-01 2.60E-01 1.38E+00 5.3 1E-0I 4.69E-0 I 1 5.76E-02 0.OOE+00 2.22E-02 9.78E-01 5.3 1E-02 1.55E-02 1.25E-02 9.87E-0 I 4.73E-01 1.12E+00 4.68E-01 5.32E-01 7.09E-02 2.78E-03 1.84E-02 9.82E-01 1.39E-01 3.43E-01 1.41 E-01 8.59E-01 3.39E-02 4.19E-02 6.57E-02 9.34E-0 I Number of Positive Differences (S+): 15 Critical Value: 11 Survey Unit: Meets Acceptance Criterion Performed By: Date:

Independent Review: Date: />v -'v&---O*

Page 1 of 1

DISCHARGE CANAL SURVEY UNIT 9106-0005 RELEASE RECORD Attachment 2f COMPASS DQA Surface Soil Report with Retrospective Power Curve (3 Pages)

DQA Surface Soil Report Assessment Summary Site: 9106-0005 (19 mrem/yr)

Planner(s): Dale Randall Survey Unit Name: 9106-0005 Report Number: 1 Survey Unit Samples: 15 Reference Area Samples: 0 Test Performed: Sign Test Result: Not Performed Judgmental Samples: 0 EMC Result: Not Performed Assessment

Conclusion:

Reject Null Hypothesis (Survey Unit PASSES)

Retrospective Power Curve 1

0.9 -1 I1. ______

______ _____ ~ZZE g

.4- 0.8 U

I.

I-

~

0.7 I.'

-I -!

-v I ______ -I-ziz21 0.6 _

______ 4i 0.5 ___ ______ -~-- -: I

= 0.4

'S ______ _____ -k-i ______

0.3 0.2 1~

L

.1 0.1 _ -A 0 = ~zzi ______ ______ ______ ______

0.0 0.2 0.4 0.6 0.8 1.0 1.2 Unity Rule Sum-of-Rados, including backgruund

- - Prospective Power U 1-beta .... Actual Power

- LBGR - - Estimated Power DCGL ---- Retrospective Power COMPASS vl.0.0 110131112006 Page 1

DQA Surface Soil Report Survey Unit Data NOTE: Type = "S" indicates survey unit sample.

Type = "R" indicates reference area sample.

Sample Number Typesample.sample,Co-60 (pCi/g) Cs-137 (pCi/g) SrY-90 (pCilg)

= Unit "S"

"R" Type 9106-0005-001 F Type NOTE: survey unitarea reference indicates

=indicates 9106-0005-002F Data Survey S S

0.02 0.09 0.03 0.07 0.01 0.01 9106-0005-003F S 0.32 0.31 0.01 9106-0005-004F S 0.21 0.16 0.01 9106-0005-005F S 0.01 -0.03 0.01 9106-0005-007F S -0.01 0 0.01 9106-0005-008F S 0.17 0.19 0 9106-0005-009F S 0.02 0.18 0.01 9106-0005-01OF S 1.38 0.26 0.01 9106-0005-011 F S 0 0.06 0.01 9106-0005-013F S 0.02 0.05 0 9106-0005-014F S 1.12 0.47 0 9106-0005-015F S 0 0.07 0.01 9106-0005-017F S 0.34 0.14 0 9106-0005-018F S 0.04 0.03 0.05 Modified Data (Unity Rule SOR)

NOTE: Type = "S" indicates survey unit sample.

Type = "R" indicates reference area sample.

Sample Number Type Sum-of-Ratios (SOR) 9106-0005-001 F NOTE:

Type sample.

"S" indicates

=="R" Type Modified Rule (Unity sample.

unit area SOR) survey reference Data S 0.02 9106-0005-002F S 0.05 9106-0005-003F S 0.17 9106-0005-004F S 0.1 9106-0005-005F S 0.01 9106-0005-007F S 0 9106-0005-008F S 0.09 9106-0005-009F S 0.05 9106-0005-01OF S 0.53 9106-0005-011 F S 0.02 9106-0005-013F S 0.01 9106-0005-014F S 0.47 9106-0005-015F S 0.02 9106-0005-017F S 0.14 9106-0005-018F S 0.07 COMPASS vI.0.0 10131/2006 Page 2

IDQA Surface Soil Report Basic Statistical Quantities Summary Statistic Survey Unit Background DQO Results Sample Number 15 N/A N=13 Mean (SOR) 0.12 N/A 0.17 Median (SOR) 0.05 N/A N/A Std Dev (SOR) 0.16 N/A 0.06 High Value (SOR) 0.53 N/A N/A Low Value (SOR) 0.00 N/A N/A COMPASS vl.O.0.P 10/3112006 Page 3