ML090540697

American Radiation Services, Inc. Laboratory Analysis Report No. ARS1-08-01555

ML090540697
Person / Time
Site:	Indian Point
Issue date:	09/15/2008
From:	American Radiation Services
To:	Noggle J NRC Region 1
References
ARS1-08-01555
Download: ML090540697 (15)

Text

2609 North River Road, Port Allen, Louisiana 70767 (800) 401-4277 -- FAX (225) 381-2996 RNA TIONAL American Radiation Services, Inc.

Laboratory Analysis Report ARS1-08-01555 Preparedfor:

/

Nuclear Regulatory Comm'ission (NRC)

James Noggle (

USNRC Region 1 475 Allendale Road King of Prussia, PA 19406 James.Noggle@nrc.gov Phone: 610.337.5063 P~groj~nae eview Management R jew Notes: Amencan Radiation Services, Inc. assumes no liability for the use or interpretation ofany analytical results provided other than the cost of the analysis itself.

Repduclion of this report in less than full requires the written consent of the client.

Contact Person: Questions regarding this analytical report should be addressed to:

Project Manager ProjectManagers@amrad.com Phone: 225.381.2991 Fax; 225.381.2996 LELAP Cert# 30658 NELAP Cert# E87558

.209N1t River Road427PotAlln Louisiana70707 I (BOO) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group: ARS1-08-01555 Request or PO Number: N/A Client Sample XD: MW-67-39-(005)04-22 15:03 ARS Sample ID: ARS1-08-01555-001 Sample Collection Date: 04/22/08 15:03 Date Received: 8/12/2008 Sample Matrix: AQueous Report Date: 09/15/08 09:09 Analysis7Z -h i;i Analyss Analysi nlssAayi " MIX D'C Qual Ar ysyySr Analysis yA Analysis Tracer/Chem DescipIon Resuts

-- Error +/- 25 Units Test Method . Date/me I Technician Recovery M 54 -1.043 0.772 .2410 1 205 I pCi/L ARS-007/EPA 9011 ' 8/19/08 16:32 JLA N/A FE-59 -2.346 3.468 5.060 2.530 pCi/I ARS.007/EPA 901.1 8/19/08 16:32 "LA I N/A CO-58 -0.291 I 0.695 2.340 1 170 1 pCi/L I ARS-007/EPA 901.1 8/19/08 16:32 JLA N/A CO-60 0.314 0.766 2.690 1.345 pCI/L ARS-007/EPA 901.1 8/19/08 16:32 JLA N/A ZN 650092 5.4 460 21 ~ / ARS 007/EPA 901.1 T8/19/08 16:32 JLAN/

/ZR-95  : -0.292 . 1.819 4.210 2105 pCi/IL ARS-007/EPA 901.1 8/19/08 1.6:32 JLA I N/A NS-954 -0.775.34 9 45piI AS07EA 0. /90 63 3LAN/

SR-906908 1350 i pCi/L ARS-007/Ehr90W-1 8/19/08 16:32 J N/A 14.3.6 3090.0910 102.292 .105 pCVL/L ARS-007/EPA 901.1 8/19/08 16:32 BILA N/A CS-34 ,0.9579 2.980 3 1,645

.2905 pCi/L ARS-007/EPA 901.1 8/19/08 16:32 .JSA J N/A CS-3 00902 0.045 2.69 . 1.38 .. ... PCi/L ARS-032/Ehr 901.1 8/26/08 1634 BIS N/A N-140 32.1329 14.2102 107.800 306~/1. ARS-022EP 00.1 18/29/08 09:328 65 /A

. -I.-.-~~... - -.--...-- . .. . . ..-.. . .-.........

LA_14 -0.959__ 0.8 3.9piL __ AS07.P __ _ 63 L /

NOTES: Shipment# 08-152 r--\k -\ r-it1 (3 1\ A Pv Prorc-t Mon8ger Ke j-Notes: American Radiation Services, Inc. assumes no liabiliy for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction ofthis report in less than full requires the written consen: of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A- 2609 North River Road Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 I0NTERNATIONAL ARS Sample Delivery Group: ARSI-08-01555 Request or P0 Number: N/A Client Sample ID: MW-67-105-(005)04-22 15:25 ARS Sample ID: ARS1-08-01555-002 Sample Collection Date: 04/22/08 15:25 Date Received:, 8/12/2008 Sample Matrix: Aqueous Report Date: 09/15/08 09:09 Analysis AnalysIs Analysis Analysis Analysis Analysi Ana~lysis fracer/Chern Decipin Result Erron-.2 MD 10 Qa Units MN-54 0.141l 0.730 2.480 1.240 pCi/L.

TetMtoi ARS 007/EPA 901.1 j Dateffirne 8/21/08 15:02 fechnician ILA Recov~ery N/A FE-59 -0.158 1.471 5 030 2 515 pCO/L ARS-007/EPA 901.1 I 8/21/08 16:02 ILA N/A CO-58 -1.267 1.978 2.220 1.110 pCI/L ARS-007/EPA 901.1 8/21/08 16:02 ILA . N/A CO-60 -0.658 1 022 .. 29 .4-.iL AS07/P o. 8/21/08 18:02 )LA N/A ZN-65 -0.738 4714 6060 3.030 pCi/L ARS-007/EPA 901.1 - 8/21/08 16:02 ,LA . N/A SN-95 0m008 0.680 2.320 1.160 I pC/L ARS 007/EPA 901.1 8/21/08 16:02 N/A

-95 ZR-95_ -0.453

-045

....... 1.177 1.177_ 3.990 3.990_ 1 995 1.995_

pCi/L

__ _0_i ARS-007/EPA

_ __ 901.1

_ _ _-_ 8/21/08

__ 16:02 )LA__ N/A

. _ _r_ .................._._

SC-134 0.753 0.725 2.420 1.210 pCi/L. ARS-007/EPA 901.1 8/21/08 16:02 ILA N/A 0.267 0.824 2.850 1.425 Pi/l ARS-007/EPA 901.1 . 821/08 16:02 J-A N/A BA-140 2.331 ~,. 2.937 9.840 4.920 PC..80I/I..-....--.-JAN/

pClL ARS-007/EPA 901.1 , 8/21/08 16:02 .LA NIA i LA-140' -0.204 107.490 3.380 1.690 1 pCi/L ARS-007/EPA 901.1 j 8/21/08 16:02 )LA N/A t SR-90 1 1.763 0.260 0.591 0.278 i pCI/L ARS-032/Elchrom SRW-01 8/26/08 13:46 8)5 50.00%

H-3 i 1862.953 T 227.626 161.113 79.338 . pCi/L 1 ARS-054/EPA 906.0 9/5/08 14:39 B- S N/A NI-63 4.8492 T- 4.880 1 -- Tý 3.9102 ~. I piLARS-022 08/29/08 13:48 8)5 N/A

~~~~~

.~~~~~~~ .... .............

NOTES: Shipment# 08-152 Pro"ct M aagerwnrr . .. ..

Notes: American Radiation Services, Inc. assumes no Iabillty for the use or Interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group: ARSI-08-01555 Request or PO Number: N/A Client Sample ID: MW-67-173-(005)04-22 15:50 ARS Sample ID: ARS3-08-01555-003 Sample Collection Date: 04/22/08 15:50 Date Received; 8/12/2008 Sample Matrix: ,Aqueous Report Date: 09/15/08 09:09 Analysis Anaysi iracer/Crno Analysis Analysis mp1 g Q1.1 i Analysis Analysis Analysis Analysis Tracer/Chemn Description S Results Error ÷/- Units Test Method DateJTime technildan Recovery

............ 2 2-.........

8.. s

...2.2.550......

... .2S PCi/L , - , ,-

/ ARS-007/EPA 901.1 8/21/08 16:02 JLA N/A MN-54 -0.901 FE-59 0.945 1.420 4.840 2.420 pCi/L ARS-007/EPA 901.1 ,821/08 16:02 *LA N/A CO58 t 0.723 2.450 ...... pCVL ARS-007/EPA 901.1 8/21/08 16:02 ILA N/A C-60-0.004 0.799 2.800 1 400 pCi/, 901.1 8/21/08 8/R5-007/16:02 -LA N/A ZN-65 i 3.609 I 3.226 6.370 I 3.185 pCI/ I ARS-007/EPA901.1 I 8/21/08 16:02 ILA N/A B-*95 .. -o---0.28 2-.722-+ -2.720 1360 ... pi/-- 9*01.1 I 8/21/08 16:02 N/AI

.]

S-95 1

-029 7.670 4.570 2.285 "pCI/L ARS-007/EPA 901.1 6/21/08 16:02 2LA N/A R..5...-........6.

-0.667 2.294

. j ..............

2.970 1.485 5.

70 ...................................

............................ pCVL ARS-007/EPA . .901. .11 .............8/21/08.....

16:02 . .ILA.. . . ..... ........ ......

N-A N/A CS-1374 C11083 -0.204 2.803 2.700 1.4350 1.350 1 1 p ,Ci/I pCI/L  ; ARS 007/EPA 901.1 AP.S-00P/EPA 901.1 8/21/08 8/21/08 16:02 16:02 ILA I LA N/A N/A

..................... L.......... ,f .

BA-140 0.617 3.102 10.600 5.300 pCj/L ARS- 007/EPA 901.1 8/21/08 16:02 . )LA

• N/A LA-140 -0.561 T .1.059 1 3.590 1.795 pCi/L ARS 007/EPA 901.1 6 /21/08 16:02 N/A SR-90 t 0.039 i 0.120 0.415 0.196 pCi/L ARS-032/Eichrom SRW-01 8/26/08 13:46 B)S 66.00%

H-3 1157.880 165.418 263.670 80.597 1 .! pCi/L ARS-054/EPA 906.0 9/5106 18:47 B+85 I- N/A NI-63 23.2552 7.350.7 7.8973 3.8856 pCi/L ARS-022 08/29/08 17:59 8S5 i N/A N .OE. 08-.--- .... ......

NOTES: Shipment# 08-152 p rO-OOctMan+a ge r Re(-ý - . . . .

Notes: American Radiation Services, Inc. assures no liabllity for the use or Interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report In less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate $ E87558

/

2609 North River Roadr Port Allen, Louisiana 70767 I (B00) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group: *AR81-08-01555 Request or PO Number: N/A Client Sample ID: MW-67-219-(005)04-22 12:20 ARS Sample 1D: ARSi-08-01555-004 Sample Collection Date: 04/22/08 12:20 Date Received: 8/12/2008 Sample Matrix: Aqueous Report Date: 09/15/08 09:09 Analysis " Analysis . .. . DLC Qal Analysis AnalystS Analysis Analysis Tracer/Chem 4-.

DesCription ............

. .......Results o.s.... Error r-/-2 s Test Method Date/Time Technician Reco/ery MN-54 0.523 1 0.797 2.690 1.345  ; pC/L i ARS-007/E PA 901.1 8/22/08 16:13 i JLA N/A FE-59 -1.270 1.471 4.960 2.480  :  ! pCVL ARS-007/EPA 901.1 8/22/08 16:13 JLA N/A I CO-58

-0.045 3.376 2.590 1.295 pCr/L ARS-007/EPA 901.1

... . 1 8/22/08 16:13 2LA J L N/A CO-60_ _ 1.112 I 0.761 2.520 1.260 pCi/L ARS-007/EPA 901.1 8/22/08 16:13 i JLA N/A ZN-65 -1.768__ 4.692 6.050 3.025 PCi/L ARS-007/EPA 901.1 8/22/08 16:13 ILA N/A N82R-95 0.3394 300.827 2.800 1 400 ) pCi/L ARS-007/EPA 901.1 8/22/08 16:13 2LA N/A ZR-95 -1.224 30.026 4.980 2.490 1 . ~

p/LARS 007/EPA 901.1

[.8/22/08 16:13 i LA N/A CS-134 ................... .

-0.026 .. ... .1.004

.............. .....-...... ... ... . 3.090

... . . . .. . .....1.545

. ...... ........... ".. PCi/L

....... . . .007/EPA ARS .. ... ... ...901.1

... ....... 8/22/08 16:13 I .LA N/A CS-137 -0.061 1.217 2.930 1.465 1 pCi/L ARS-007/EPA 901.1 8/22108 16:13 ILA N/A BA-140 -0.674 5.234 21.200 1 5.600 1 pCl/L IARS 007/EPA 901.1 I8/22/08 16:13 JLA N/A LA-140 -0.178 1.806 3.230 1.615 pCI/L. ARS-007/EPA 901.1 8/22/08 16:13 ILA N/A SR 8R-90 0.462 0.228 0.730 0.344 pCi/L I ARS-032/Eichrom 8RW-01 8/26/08 13:46 IS 50.00%

H-3 1034.936 154.68 162.273 1 79.909 I pCI1 ARS-054/EPA 906.0 9//s08 N:54 B2S N/A N1-63 4.1121 . 4.7928 778815 3.8778 pCi/L ARS-022 08/29/08 22:11 i BIS N/A I. .........

I NOTES: Shipment# 08-152 Notes: American Radiation Services, Inc. assumes no 11bility for the use or interpretation of any analytical results providediother than the cost of the analysis itself. Reproduction of this report in less than lull requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group: ARS1-08-01555 Request or PO Number: N/A Client Sample ID: MW-67-276-(005)04-22 12:30 ARS Sample ID: ARS-08-01555-005 Sample Collection Date: 04/22/08 12:30 Date Received: 8/12/2008 Sample Matrix: Aqueous Report Date: 09/15/08 09:09

....... A si -*:........

nal .Ly ..... . ;y*V-'---s-* I . .....- MCDLC i..... 1 Analysis Analysis Analysis Analysis Tracer/Chem Analsi Analysis Analysis .

. Description M.: ................

Results ...0-7+/- *2 5 * .................

T6- -* ...Error MDC ...... .........

o..... .. Units Test Method i Date/Time Technician R.co.very I MN5 -0.026 I 0.704 2.52.075 . pCi/L ARS-007/EPA 901.1 8/22/08 16:14 )LA N/A FE-59 S -0.246 1.066 7 3.660 1 1.830 pCi/L ARS-O07/EPA 901.1 8/22/08 16:14 1 )LA

• 1-N/A

• CO-58 -0.314 6.285 2.300 1 1.150 pCi/L ARS-007/EPA 901.1 8/22/08 16:14 1 ILA 8/22/08. 16 :14.........

N/A

..T...7.... 1 CO-60 -0.757 ;25.953 2.430 1.215 1 i pCI/L ILA N/A

"-, -- 4 _______ r *i i 2.875 9.660 4-0.173 4830 I pCi/L ARS-007/EPA 901.1 8/22/08 16:14 I.LA N/A 0.-642-2450312.B758/22/08p'614 NB95 i -1.049 2 .450= 1.225 pCi/L ARS-007/EPA 901.1 8/22/08 16:147 ILA N/A ZR95 0.055 1.14 3.900 1.950 ./L P.i ARS-007/EPA 901.1 8/22/08 16:14 i LA N/A

---

.- .... ....... . . . /

CS-134 -0.189 . 6.287 2m480 1 240 pCi/L 1 ARS-007/EPA 901.1 8/22/08 16:14 T LA N/A CS-137 -0.044 .~0.685 2.330 1.165 pCI/L ARS-007/EPA 901.1 8/22/08 16:14 ILAN/

BA-140 -2.721 9.229 .1 10.200 5 100( pCi/L ARS-007/EPA 901.1 8/22/08 16:14 )LA N/A LA-140 -0.717 7.115 3.430 1.715 pCi/L ARS-007/EPA 901.1 8/22/08 16:14 1 . N/A SR-90 0.919 0.229 0.655 0.309 pCI/L ARS-032/Eichrom SRW-01 8/26/08 13:46 B3 58.00%

1-6 5075 4728 4.25 1 12.13 7.6523 7986 3.765 j

T PCI/ 1 ARS-0541EPA 9060 ARS-022 9/6/08 3:02 t08/30/08 02:22 83J BSN/A j N/

N-3505 -/

,1. ~

. . . .~..... ....................... ......... -------------------

NOTES: Shipment# 08-152 Q J-" "

Proj1ct Manager Notes: American Radiatlon Ser-ices, Inc. assumes no liability for the use or Interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report In less than full requires the written coeent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

A- 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 ARS Sample Delivery Group: ARSI-08-01555 Request or PO Number: N/A Client Sample ID: MW-67-323-(005)04-22 12:56 ARS Sample ID: ARS1-08-01555-006)

Sample Collection Date: 04/22/08 12:56 Date Received: 8/12/2008

• Sample Matrix: Aqueous Report Dater. 09/15/08 09:09 AnalysIs Analysis Analys....s Aas i - ---------

.-- Tracer/Chems Results Error+/-  ; I Analysis Units Analysis Test Method Analysis Date/Time Analysis Techniian Declson Recovery MN-54 0.427 0.750 2.530 ... 26 -. pCi/L ARS-007/EPA 901.1 8/22/08 16:15 A N/A FE-59 0.294 1.290 4.420 2.210 pCi/L ARS-007/EPA 901.1 1 8/22/08 16:15 1 ILA N/A CO-58 -0.583 10.887 - -. ~ 2.230 1.115 PCik ARS-O07/EPA 901.1

--- = -. .............

i 8/22/08 16:15 CO-60 -0.988 8.141 3.260 D 1.630 pCi/L ARS-007/EPA 901.1 8/22/08 16:15 ILA N/A ZN-65 1.092 1.516 5.150 2.575 ARS-007/EPA 901.1 8/22/08 16:15 JLA ICi/L N/A NB-95 -0.394 0.786 2.650 1.325 1 pCV/L ARS-007/EPA901.1 8/22/08 16:15 ILA N/A 1 ZR 95 0.260 1.128 3840 1920D pCi/ ARS-007/EPA 901.1 8/22/08 16:15 JLA N/A CS-134

.......... 1.167 0.802 2.650 1 1.325 I...............................

pCl/L ARS-007/EPA 901.1 -

I./.........,...........

..... 2.0......

8/22/08 16:15 ILA N/A CS-137 . -1.936 2.601 2.910 1.455 pCL ARS-007/EPA 9011/2181:1 L i.....

BA100.326 - 2.691 9 160 4.580 PCi/L ARS 007/EPA 901. 1/2D 61 L /

LA-140 0.176 , 0.940 3.280 1.640 PC/iL ARS-007/EPA 901.1 8/22/08 16:15 JLA N/A SR-90 -0.044 . 0471 0.0.134 0223 pCi/L ARS-032/Eichrom SRW-01 8/26/08 13:46 BJS 58.00%

H-3 356.340 107.279 161.183 79.372 pCi/L ARS-054/EPA 906.0 9/6/08 7:09 B1S1 N/A N1-63 -0.6756 4.4686 7.6404 3.7592 pCi/L I ARS-022 08/30/08 06:26 B)S N/A

... .. 08-1......... .....

NOTES: Shipment# 08-152 Pro~d 1 Manager 2ý1 Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this repon fl lesS than full resuires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 INTERNATIONAL ARS Sample Delivery Group: ARS1-08-01555 Request or PO Number: N/A Client Sample ID: MW-67-340-(005) 04-22 12:50 ARS Sample ID: ARS1-08-01555-007 Sample Collection Date: 04/22/08 12:50 Date Received: 8/12/2008 Sample Matrix: Aqueous Report Date: 09/15/08 09:09

- nlyi Anaysi, Analysis 1 Analysis j Analysi i D I LC Qua Analysis Analysis Analysisre Analysis Tracer/Chem i Desc~pt~n .1 2Rsuls UitsTest Method MN-54. 1.130

.Erro 0 .738 S.

2.440 . 1.22D 3Ci/L AR-0/A91.

... /-'2*

/

2/;81 :5

/Date/816:15 Technician

.L............... . Recovery N/........

N/A P8-59 -1.022 35.013 4.880 2.440 pi/AR-0EP90. i 8/22/08 16:15 1 ILA N/A I C0-58 -0,236 0.742 2.500 1 1.250 i pCi/L -D7EA91 901.1 ARS007/EPA /20 8/22/08 16.15 IL N/A C0-60 -1,219 8.301 3.12D 1. 560 pCi/L ARS-007/EPA 901.1 ' 8/22/08 16:15 ILA N/A ZN-65 -3.539 3.367 6.580 3.290 1 pCi/L ARS-007/EPA 901.1 8/22/08 16:15 ILA N/A NB09 -D.398 , .8 1 2.520 126 t pci/L ARS 07E 9 8/22/0816:15 ;L N/A zR-g. -1.796  : 12.149 4 490 2.245 pCi/L ARS-007/EPA 901.1 1 8/22/08 16:15 ILA /

S 134 ACS134 -1.212

-1.212 92143 9.573 2.920 1.2460 1.460 pCi/L pCI/L I ARS-007/EPA 901.1 ARS-007/EPA 901.1 8/22/08 16:15 8/22/08- 16:15 IL "

ILA 1 ...

N/A N/A BA-140 -1.511 8.255 10.700 5.350 i pCI/L ARS-007/EPA 901.1 8/22/08 16:15 ILA N/A LA-140 -0.119 . 0.923 3.180 1.590 pCl/L ARS 007/EPA 901.1 ) 8/22/08 16:15 ILA N/A SR-90 0.141 D.150 " 0.506 0.238 pCi/L ARS-032/Eichrom SRW-01 8/26/08 13:46 1 BS2 58.00%

.3 I 489.197 114.108 1 160o136 I 76i8857 pCi/L ARS 054/EPA 9060 i 9/6/08 11:17 :1 1 /A I-63 3.3699 4.8795 8 1082 I 3.9893 pCI/L ARS022 08/30/08 10:32 r 825 - -N/A 1 I..--.- I

. NO....... S.......n

-5 NOTES: Shipment# 08-152

(-77'ý-A YV()lA) ~ I J -- )-

Project Manage Re "

Notes: American Radiaiion Services, Inc. assumes no liability for the use or Interpretation of any analytical results provided other than the Costof the analysis Itself. Reproductlon of this report In less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

PAGE 1 of 2 NRC FORM 301 U.S. NUCLEAR REGULATORY COMMISSION LABORATORY USE ONLY CONTROL NUMBER S rFO ANALYSIS AND L. -41N Oi CUSTODY LABORATORY:

SAMPLE LOCATION (LICENSEE) LICENSEE NUMBER DOCKET NO.

INDIAN POINT ENERGY CENTER SAMPLE SUBMITTED

1. TOTAL TYPE VOLUME WEIGHT DATE SAMPLES SUBMITTED PRIORITY 2 Kg ROUTINE 1 GROUND WATER 2000 ML .- ] URGENT TMONTH SAMPLE COLLECTION INTERVAL

______________ _____________ DAY YEAR TIME INSPECTOR RESPONSIBLE TELEPHONE NUMBER Jim Noggle (USNRC), (610) 337-5063 STOP 1

LIST DESIRED LIST DESIRED ANALYSIS TO BE PERFORMED LLD (Optional) OTHER TYPE OF ANALYSIS (Specify) LLD (Optional)

D GROSS ALPHA (GA) _ STRONTIUM-90(Sr90)

D GROSS BETA (GB) NICKEL-63(Ni63)

GAMMASPEC(GS) -

TRITIUM (H3) D D CARBON-14 (C14) D 0--i IODINE-125 (1125) D RELENOUISHED BY RECEIVED BY DATE TIME REASON FOR CHANGE OF CUSTODY.

FEE RECOVERABLE D NO YES TAC NUMBER REMARKS:

Inspection Report: 1007005

'NOTE: SAMPLES WILL BE DISCARDED AFTER ANALYSIS UNLESS REASON ARE NOTED IN REMARKS ABOVE.

NRC FORM303 (4-2004) PRINTED ON RECYCLED PAPE

a PAGE 2 of 2 NRC FORM 303 U.S. NUCLEAR REGULATORY QOMMIS'"N LABORATORY USE ONLY (4-2004) CONTROL NUMBER SAMPLE RECORD - Continued LABORATORY:

SAMPLE SAMPLE NAME COLLECTION REMARKS, PRESERVATIVE NUMBER AND DESCRIPTION DATEITIME ANALYSIS REQUESTED, ETC.

MW-67-39-(005) Ground Water Split Sample of MW-67-39-(005) Sample is unfiltered & unpreserved. Analyze o*

22 5 Gamma Spec. H3, Sr90, Ni63 MW-67-105-(005) Ground Water Split Sample of MW-67-105-(005) . - Sample is unfiltered & unpreserved. Analyze fo

-1 ' 1.52:5 Gamma Spec, H3, Sr90, Ni63 MW-67-173-(005) Ground Water Split Sample of MW-67-173-(005) I Sample is unfiltered & unpreserved. Analyze to MW-67-219-(005) r a2 CoA . Gamma Spec, H3, Sr90, N163 MW-67-219005). Ground Water Split Sample of MW-67-21 9-(005) Sample is unfiltered & unpreserved. Analyze fo MW_67_27___005)_ GroundWate__Sp__tSmpeoMW-67-276-(005) ~ 4 22 1 i 22 Gamma Spec, H3, sr90, Ni63 MW-67-276-(005) Ground Water Split Sample of MW-67-276-(005) Sample is unfiltered & unpreserved. Analyze for 4122 15 )-l Gamma Spec, H3, sr90, Ni63 MW-67-323-(005) Ground Water Split Sample of MW-67-323-(005) - Sample is unfiltered & unpreserved. Analyze fo

_______________________________ 122,10 ic~ 2-5k Gamma Spec, H3, Sr9a, Ni63 MW-67-340-(005) Ground Water Split Sample of M-730(5)-

4W-67-30-(o-3)212051 Sample is unfiltered & unpreserved. Analyze for Gamma Spec, H3, 5rS0, Ni63

.0f NR .OMO (-204 RN.DO EYCE AE NRC FORM303 (4-2004) PRINTED ON RECYCLED PAPER

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 SERVICES, INC.

QC Results Report Sample.Delivery Group: ARSI-08-01555 Date Received: 8/12/2008 Laboratory Control Samp le Evaluation Analysis Batdh N/A -

QC Type LCS Anelyte Ni-63 JResults Analysis 210.12 u (1 8) 48.8 jU MDC 8.0357 Expected Value 204.49 Report Units pCi/L Analysis Test Method ARS-022 Analysis Date/Tine 8/28/08 20:51 Anayllysis Technidan 8J5 Percent Recosery (%)

103 L

AccepteIce 75%-125%

Blank Evaluation Anlyi' Analysis I Expected Qiul Report Analysil Analysis Analysis Batch Type Results value . Units Teat Method Date/Time Technican N/A MBL Ni-63 -0.141 4.68 7.9878 NA U pCi/L ARS-022 8/29/08 5:17 BJS RER Duplicate Evaluation Anlalysis QO Analysis Anlss RR A~pacRR hol s ReAals utlatI CSU 1 (16) Result 2 csU 2 15) QulAayis Anaelysis Analysis Analysis RR Acetne Batch Type Description I I I Units Test Method Date/Time Technicien is' N/A LCSD Ni-63 . 210.12 48.8 219.354 50,926 pCi/L ARS-022 8/29/08 1:05 BS 0.09 1 DER Duplicate. Evaluation atch QC Analysis Result 1 OSU 1(1-) Result 2 CSU 2 Analysis Analysis Analysis Analysis DER E R Altch Typ Description U nisJ Test Method [ Date/Time Tc.hnician DER AcceptanceR N/A LCSD Ni-63 210.12 48.8 219.354 50.926 pCi/L ARS-022 8/29/08 1:05 81S 0.26 < 3 SPr-oj* -iManager R~f_ --

Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reprodution Of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (8003 401-4277 FAX (225) 381-2996 QOR MERAN RAhDIATION SERVICES, INC.

QC Results Report Sample Delivery Group: ARS1-08-01555 Date Received: 8/12/2008 Laboratory Control Sampl Evaluation s U1 Mac Expected Report Analysia Analysis An.yi Percent LC Analys is Betch Type ReSlts Val..e Unit. Test Method Dat./Time Technician Recove=ry (%) Acceptance ARSl-BDB-02293 ICS H3 1136.06 161.4 158.48416 1270.45 PCVL' ARS-O54/FPA 906.0 .9/4/08 18:01 . BIS 89 75%-125%

Blank Evaluation Anlysis tch I QC Typo Analyte Analysis CSU 1 (1 s) M4C Expected i Report Analysts Analysis Analysis Results V UnitsT____thod/TTestchnician ARS1-808-02293 MBL H3 67.923 94.439817 158.41962 NA U pCI/L APS-054/EPA.906.0 9/5/08 2:16 BJS RER Duplicate Evaluation Analysis QC Analysis [ 1 Analysis Analysis Analysis Analysis RER 1 B ItchType Description RIsult 1 ESU 1(1 a) ISURsult 2 2(ls) QIel Units Test Method [ Deta/Time Technician RER Acc'ptencei ARS1-808-02293 LCSD H3 1 1136.06 161.4 1143,2572 161.96361 1 pCI/LI ARS-054/EPA 906.0[ 9/4/08 22:09 BJS 0.02 DER Duplicate Evaluation An Batch y Q Type r Oescrption A-uIt 1 CSU 1 (1s) Result 2 CSU 2 (Is) Qual IF Ant. eEn

" Anysis 1 . 1 D DER 1 Unyis AnhMethod s Dina/Time Achnicisn AccatnR ARS1-B08-02293 LCSD I H3 1 1136.06 161.4'1 1143.2572 161.9536 pCi/L ARS-054/EPA 906.0 1 9/4/08 22:09 1J $S 0.06 < 3 Matrix Spike "

AnalysIs QC A Analysis CSU I spiked p Report Analysis Analysis Analysis Percent LCS Batch Type 623 U1 (21) SUv pike conQ Unit. TeSt Mthod Data/Tim Technican Rovery( %) Acceptance A 2R 3A i 8 8 0 ay e R a su lts 1429i 035 t e t e h dD it / h n T c n ca R a nge ARS--B08-02293 MS H3 137S5.623 1429.035 1862.953 13970.11 pCI/iL ARS-054/EPA 906.0 9/5/08 6:24 WS .85 60%-140%

Pro) ct Manage r

Notes: American Radiatlon Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Certificate# 30658. NELAP Certificate # E87558

2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 j

V4AMEýCRADIATION SERVICES, INC.

QC Results Report Sample Delivery Group: ARS1-08-01555 Date Received: 08/12/08 Laboratory Control Sample Evaluation Analytis QC Analysis CSU ( ) MDC Epeted Report Analysis Analysis Analysis .LcS Pecent Type Results / Value Units Test Method Date/Time Technician Reco~very (,%) Acceptance ARSI-BO8-02219 LCS Sr-90 21.729 1.699 0.531 21.34 pCi/L ARS-032/EPA 905.0 8/26/08 13:46 BIS 102 75%-125%

Blank Evaluation Anatysi [ ye [ Axslt lysis eut aa I E t Value Units Analysis Test Method Analysis DowTue/ir Analysis Technician Ratch Type Re sul 1(t)sC O~tdqi eOt AaysAayi ARS1-808-02219 MBL Sr-90 -0.200 0.202 0.729 NA U pCVL ARS-032/EPA 905.0 8/26/08 13:46 B3S RER Duplicate Evaluation Analysis QC Analysis Analysis Analysis Analysis RER lytch Typ Dsrpon Result 2 cSU 1 (2 s) Result 2 CSU 2 (1.) Qua, Analysis .t1TiRER

• AcceptacaR

.*~ ypj ~icpi Units Test Method Dt/Tm

. Technician _arms ARS1-B08-02219 LCSD Sr-90 21.729 1.699 23.673 1.862 pCi/L ARS-032/EPA 905 0 8/26/08 13:46 3S 0.55 <1 DER Duplicate Evaluation 1 1

[

Analyais QC A..as sult 1 CSU I () Result 2 CSU 2 (is) Aalys Analysis Analysis Analysis D DLR Batch Type esscription 1 1 Units Test Method Date/Time Technician OER AeptanceR ARS1-B08-02219 LCSD Sr-90 21.729 1.699 23.673 1.862 [ pCi/L ARS-032/EPA 905.0 1 8/26/08 13:46 BJS 1.54 33 Prjyt M anagear Notes; American Radiation Services, Inc. assume no liability for the use or interpretation of any analytial results provided other than the cost of the analysis itself. Reproductionnof this report In less than full requires the written consent of the client.

LELAP Certificate# 30658 NELAP Certificate # E87558

/

'4.

-A- RS INTERNATIONAL 2609 North River Road, Port Allen, Louisiana 70767 1 (800) 401-4277 FAX (225) 381-2996 QC Results Report Sample Delivery Group: ARSI-08-01555 Date Received: 08/12/08 Laboratory Control Sample Evaluation Analyss TAnalysis QC CSU L (1) M " Expected Report Analysis Analysis Analysis Percent LCS Acceptance Batch Type. vResult.

vlue Units. Test Method Date Technician Recovery (%) Range ARS1-B08-02203 LCS CO-60 25281.00 495.35 210.80 25315.22 pCO/g EPA901.1 08/19/08 )LA 100 75%-125%

ARS1-B08-02203 LCS CS-137 15370.00 345.75 130.00 15285.98 pCVg EPA901.1 08/19/08 JLA 101 75%-125%

ARSI-608-02203 LCS AM-241 34109.00 1251.70 288.40 34794.33 PCVQg EPA901.1 08/19/08 JLA 98 75%-125%

B la n k Ev a lu a tio n L..__-

Analysis QOC Analyse Analysis CSU I (1I) MDC Expected Report Analysix Analysis Analysis Batch Type Results Value Unite Test Method DOate Technician ARS1-B08-02203 MBL CO-60 0.001 0.001 0.004 NA U pCi/g EPA901.1 08/19/08 iLA ARS1-B08-02203 [MBL CS-137 0.001 0.001 0.004 NA U pCi/g EPA901.1 08/19/08 JLA ARS1-B08-02203 MBL AM-241 0.000 0.003 0.007 NA U PCi/g EPA901.1 08/19/08 ILA RER Duplicate Evaluation Analylis QC Analysis sult 1 CSU 1 (1 Rut 2 CSU 2 (is) Quni Analysis Analysis Analysis RIB BatchR Type Description U nit Test Method Oato Technician B ptainceIlta ARS1-B08-02203 LCSD CO-60 25281.00 495.35 24786.00 496.33 pCO/g EPA901.1 08/19/08- JLA 0.50 < 1 AR51-B08-02203 LCSD CS-137 15370.00 345.75 14809.00 374.51 pCI/g EPA901.1 08/19/08 ILA 0.78 < I ARS1-808-02203 LCSD AM-241 34109.00 1251.70 34780.00 1262.00 pCl/g EPA901.1 08/19/08 ILA 0.27 < 1 DER Duplicate Evaluation Analysis Bnatchi TpQC Analysis Anptlys RRAnalsis CSU I (I Resul 2 Analysis Analysis AnalysisI OR Test Method Date Technidcan R AcceptancsRange ARS1-B08-02203 LCSD CO-60 25281.00 495,35 24786.00 496.33 pCi/g EPA 901.1 08/19/08 JLA 1.41 <3 ARSI-B08-02203 LCSD CS-137 15370.00 345.75 14809.00 374.51 pCi/g EPA 901.1 08/19/08 ILA 2.20 <3 ARS1-508-02203 LCSD AM-241 34109.00 1251.70 34780.00 1262.00 pCl/g EPA 901.1 08/19/08 JLA 0.76 <3

-- Quaill Assurance Notes: American Radiation Services, lnc. assumnes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis Itself. Reproduction of this report In less than hfll requires the written consent of the client.

LELAP Certificate* 306SB NELAP Certificate # E87558

2609. North River Road Port Allen, Louisiana 70767 O AMOV t1N 1 (800) 401-4277 FAX (225) 381-2996

• I'AMERICAN RADIATION SERVCESS, INC.

Notes:

Comments:

1.0), Soil and Sludge analysis are reported on a wet basis or an as received basis unless otherwise indicated.

2.0) The data in this report are within the limits of uncertainty specified in the reference method unless specified.

3.0). Modified analysis procedures are procedures that are modified to meet the certain specifications. An example may be the use of a water method to analyze a solid matrix due to the lack of an officially recognized procedijre for the analysis of the solid matrix.

4.0) Derived Air Concentrations and Effluent Release Concentrations are obtained from 10 CFR 20 Appendix B.

5.0) Total activity is actually total gamma activity and is determined utilizing the prominent gamma emitters from the naturally occurring radioactive decay chains and other prominent radioactive nuclides. Total activity may be lower than the actual total activity due to the extent of secular equilibrium achieved in the various decay chains at the time of analysis. The total activity is riot representative of nuclides that emit solely alpha or beta particles.

6.0) Ra-228 is determined via secular equilibrium with its daughter, Actinium 228. (Gamma Spectroscopy only).

7.0) U-238 is determined via secular equilibrium with its daughter, Thorium 234. (Gamma Spectroscopy only).

8.0) All gamma spectroscopy was performed utilizing high purity germanium detectors (HPGe).

9.0) ARS makes every attempt to match sample density to calibrated density; however, in some cases, it is not practical or possible to do so and data results may be affected.

Method

References:

1.0) EPA 600/4-80-032, Prescribed Procedures for the Measurements of Radioactivity in Drinking Water, August 1980.

2.0) Standard Methods for Examination of Water and Waste Water, 18'h, 1992.

3.0) EPA SW-846, Test Methods for Evaluating Solid Waste, Third Edition, (9/86).. (Updated through 1995).

4.0) EPA 600/4/79-020, Methods for Chemical Analysis of Water and Waste, March 1983.

5.0) HASL 300 Definitions:

1.0) BDL Analyte not detected because the value was below the detection limit.

2.0) ND Not detected above the detection limit.

3.0) Detection Limit The minimum amount of the analyte that ARS can detect utilizing the specific analysis.

4.0) B Method Blank 5.0) D . Method Duplicate 6.0) MS Matrix Spike 7.0) S Spike 8.0) RS Reference Spike 9.0) *SC Subcontracted out to another qualified laboratory 10.0) NR . Not Referenced

11. 0) N/A . Not Applicable 12.0) Reported as a calculated value 13.0) False Positive due to interference from Bi-214 Notes: American Radiation Services, Inc. assumes no liability for the use or interpretation of any analytical results provided other than the cost of the analysis itself. Reproduction of this report in less than full requires the written consent of the client.

LELAP Cert-# 30658 NELAP Cert'# E87558