ML23136B289
| ML23136B289 | |
| Person / Time | |
|---|---|
| Site: | 07000398 |
| Issue date: | 05/16/2023 |
| From: | US Dept of Commerce, National Institute of Standards & Technology (NIST) |
| To: | Office of Nuclear Material Safety and Safeguards |
| Shared Package | |
| ML23136B277 | List: |
| References | |
| TAC L32643, EPID L-2022-DFA-0010 | |
| Download: ML23136B289 (1) | |
Text
NIST Scoping Study Scoping Report: 144265-RPT-001, NIST Scoping Study Report Revision: A Appendix Appendix C Liquid Scintillation Results
11/2/2022 3:22:04 PM QuantaSmart (TM) -
4.02 - Serial# 118398 Protocol# 4 -
5 Minute IPA subtract.lsa Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Page 1 User: Default Output Data Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221102 1313 Raw Results Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221102-1313
\\20221102 1313.results Assay File Name: C:\\Packard\\TriCarb\\As,says\\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Sample: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On -
IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions A
B C
LL 0.0 12.0 156.0 Count Corrections UL 18.6 156.0 2000.0 Static Controller: On Colored Samples: Off Coincidence Time (nsec): 18 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=l18398 Cycle 1 Results Bkg Subtract 6.84
- 11. 63 11.02 Luminescence Correction: Off Heterogeneity Monitor: n/a Delay Before Burst (nsec): 75 S#
PID Count Time tSIE CPMA CPMB CPMC DPMl 1
16 5.00 427.76 5
0 0
13 2
16 5.00 427.86 3
0 0
8 3
16 5.00 418.20 10 0
2 28
- rsJL-/
4 16 5.00 425.09 5
0 2
15 5
16 5.00 411. 44 4
0 0
11 6
16 5.00 400.90 6
0 0
18 DPM2 0
0 0
0 0
0 MESSAGES
11/2/2022 3:22:04 PM Quan:taSmart (TM) - 4.02 - Serial# 118398 Page 2 Protocol# 4 -
5 Minute IPA subtract.lsa User: Default 7
16 5.00 407.16 7
2 0
19 2
8 16 5.00 423.77 4
1 0
10 0
9 16 5.00 417.64 9
0 1
26 0
1&-J~-J__ 10 16 5.00 405.62 10 2
0 27 1
11 16 5.00 440.42 3
0 0
9 0
12 16 5.00 434.97 9
0 0
24 0
13 18 5.00 421. 91 7
0 0
20 0
r 14 18 5.00 420.35 7
0 0
20 0
'3'i~
15 18 5.00 426. 82 6
0 1
18 0
--16 18 5.00 428.50 6
0 0
19 0
17 18 5.00 444.77 6
0 0
18 0
18 18 5.00 432.21 6
0 0
17 0
-1~.,,,
19 18 5.00 430.79 7
0 0
20 0
20 18 5.00 422.28 4
0 0
12 0
11/3/2022 9:21:16 AM QuantaSmart (TM) - 4.02 - Serial# 118398 Protocol# 4 -
5 Minute IPA subtract.lsa Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Page 1 User: Default Report Name: Reportl Output Data Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221102 1313 Raw Results Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221102-1313
\\20221102 1313. results Assay File Name: C:\\Packard\\TriCarb\\Assays\\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1
- Vials/Sample: 1 Background Subtract Repeat Sample Count: 1 Calculate%
Reference:
Off Background Subtract: On -
IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions A
B C
LL 0.0 12.0 156.0 Count Corrections UL 18.6 156.0 2000.0 Static Controller: On Colored Samples: Off Coincidence Time (nsec): 18 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=118398 Cycle 1 Results Bkg Subtract 6.84
- 11. 63
- 11. 02 Luminescence Correction: Off Heterogeneity Monitor: n/a Delay Before Burst (nsec): 75
~ S#
PID Count Time tSIE CPMA CPMB CPMC DPMl
~ 1" 16 5.00 427.76 5
0 0
13 2 l"'
16 5.00 427.86 3
0 0
8 3,~ 16
'b cJl 4,~ 16 5.00 418.20 10 0
2 28 5.00 425.09 5
0 2
15 5 '\\,0 16 5.00 411. 44 4
0 0
11 l ""6 16 5.00 400.90 6
0 0
18
'DPM2 0
0 0
0 0
0 MESSAGES
11/3/2022 9:21:16 AM QuantaSmart (TM) -
4.02 - Serial# 118398 Page 2 Protocol# 4 -
5 Minute IPA subtract.lsa User: Default
~~34~;
16 5.00 407.16 7
2 0
19 2
16 5.00 423.77 4
1 0
10 0
9--i 16 5.00 417.64 9
0 1
26 0
10.;
16 5.00 405.62 10 2
0 27 1
i..--
IH 16 5.00 440.42 3
0 0
9 0
l 12, 16 5.00 434.97 9
0 0
24 0
18 5.00 421. 9_1 7
0 0
20 0
14 '\\
18 5.00 420.35 7
0 0
20 0
15 I:)
18 5.00 426. 82 6
0 1
18 0
16 18 5.00 428.50 6
0 0
19 0
4S'17 18 5.00 444.77 6
0 0
18 0
~~ 18 18 5.00 432.21 6
0 0
17 0
19 18 5.00 430.79 7
0 0
20 0
20 18 5.00 422.28 4
0 0
12 0
11/7/2022 1:57:04 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Protocol# 5 -
5 Minute IPA subtract.lsa Assay Definition Assay
Description:
5 min count with IPA. BKG subtract Assay Type: DPM (Dual)
Page 1 User: Default Report Name: Reportl Output Data Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221107 1252 Raw Results Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221107-1252
\\20221107 1252.results Assay File Name: C:\\Packard\\TriCarb\\Assays\\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Sample: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On -
IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions A
B C
LL 0.0 12.0 156.0 Count Corrections UL 18.6 156.0 2000.0 Static Controller: On Colored Samples: Off Coincidence Time (nsec): 18 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=118398 Cycle 1 Results Bkg Subtract 5.96
- 11. 42 10.. 65 Luminescence Correction: Off Heterogeneity Monitor: n/a Delay Before Burst (nsec): 75 S#
PID Count Time tSIE CPMA CPMB CPMC DPMl i-ll')~~c.C, 1 16 5.00 411. 77 5
0 0
14
~\\~
2 16 5.00 417.56 10 1
1 26 3
16 5.00 419.59 10 1
0 27 4
16 5.00 407.61 5
0 0
15 5
16 5.00 404.58 10 6
0 24 FJ.. J'Jf, '?.?.. <-/ 6 16 5.00 411.46 5
1 0
13 A--3of, DPM2 0
0 0
0 6
0 MESSAGES
11/7/2022 1:57:04 PM QuantaSmart (TM) -
4.02 - Serial# 118398 Protocol# 5 -
5 Minute IPA subtract.lsa 16 16 16 16 5.00 5.00 5.00 5.00 405.63 402.43 404.91 412.80 4
5 7
5 1
0 0
0 0
0 0
0 11 13 18 14 1
0 0
0 Page 2 User: Default
11/9/2022 8:59:41 AM QuantaSmart (TM) - 4.02 - Serial# 118398 Protocol# 3 -
5 Minute IPA subtract.lsa Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Page 1 User: Default Report Name: Reportl Output Data Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221109 0821 Raw Results Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221109-0821
\\20221109 0821.results Assay File Name: C:\\Packard\\TriCarb\\Assays\\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1
- Vials/Sample: 1 Background Subtract Background Subtract: On -
IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions A
B C
LL 0.0 12.0 156.0 Count Corrections UL 18.6 156.0 2000.0 Static Controller: On Colored Samples: Off Coincidence Time (nsec): 18 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=ll8398 Cycle 1 Results Repeat Sample Count: 1 Calculate%
Reference:
Off Bkg Subtract 6.43
- 11. 85 10.83 Luminescence ~orrection: Off Heterogeneity.Monitor: n/a Delay Before Burst (nsec): 75 S#
PID Count Time tSIE CPMA CPMB CPMC DPMl 1
12 5.00 391.08 3
1 0
9 2
12 5.00 382.91 4
0 1
12 3
12 5.00 385.83 44 0
0 126 4
12 5.00 398.33 4
2 0
11 5
12 5.00 390.05 5
0 0
15 6
12 5.00 436.93 5
0 0
13 DPM2 1
0 0
2 0
0 MESSAGES eH,,- R.et*uA..+
11/9/2022 5:16:50 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Protocol# 3 -
5 Minute IPA subtract.lsa Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Page 1 User: Default Output Data Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221109 1700 Raw Results Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221109-1700
\\20221109 1700.results Assay File Name: C:\\Packard\\TriCarb\\Assays\\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec):
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal 0.5 2s%
Assay Count Cycles: 1
- Vials/Sample: 1 Repeat Sample Count: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On -
IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions A
B C
LL 0.0 12.0 156.0 Count Corrections UL 18.6 156.0 2000.0 Static Controller: On Colored Samples: Off Coincidence Time (nsec): 18 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=118398 Cycle 1 Results Bkg Subtract
- 6. 43
- 11. 85 10.83 Luminescence Correction: Off Heterogeneity Monitor: n/a Delay Before Burst (nsec): 75 S#
PID Count Time tSIE CPMA CPMB CPMC DPMl 1
12 5.00 389.37 2
0 0
6 Missing vial 2.
3 12 5.00 437.63 3
0 0
10
~;,.'/ Bo 4 '::l DPM2 0
0 Rec.ouo.A-
~ 3 MESSAGES
11/10/2022 12:45:07 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Protocol# 3 -
5 Minute IPA subtract.lsa Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Page 1 User: Default Output Data Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221110 1128 Raw Results Path: C:\\Packard\\Tricarb\\Results\\Default\\5 Minute IPA subtract\\20221110-1128
\\20221110 1128.results Assay File Name: C:\\Packard\\TriCarb\\Assays\\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Sample: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On -
IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions A
B C
LL 0.0 12.0 156.0 Count Corrections UL 18.6 156. 0 2000.0 Static Controller: On Colored Samples: Off Coincidence Time (nsec): 18 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=118398 Cycle 1 Results Bkg Subtract
- 6. 96
- 10. 97
- 11. 00 Luminescence Correction: Off Heterogeneity Monitor: n/a Delay Before Burst (nsec): 75 s#
PID Count Time tSIE CPMA CPMB CPMC DPMl 1
12 5.00 401. 89 2
2 0
4 2
12 5.00 386. 36 12 6
0 29 3
12 5.00 378.98 21 7
0 56 4
12 5.00 380.44 5
0 0
13 5
12 5.00 370.99 6
0 0
18 6
12 5.00 413. 29 7
1 0
19 DPM2 2
6 5
0 0
0 MESSAGES
11/10/2022 12:45:07 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 2 Protocol# 3 -
5 Minute IPA subtract.lsa User: Default 7
12 5.00 377.20 5
0 0
14 0
8 12 5.00 394.38 6
2 0
14 2
9 12 5.00 403. 96 4
0 0
12 0
10 12 5.00 408.58 6
1 0
17 1
11 12 5.00 427.68 6
1 0
14 0
12 12 5.00 430.71 4
0 0
13 0