ML23136B289
| ML23136B289 | |
| Person / Time | |
|---|---|
| Site: | 07000398 |
| Issue date: | 05/16/2023 |
| From: | US Dept of Commerce, National Institute of Standards & Technology (NIST) |
| To: | Office of Nuclear Material Safety and Safeguards |
| Shared Package | |
| ML23136B277 | List: |
| References | |
| TAC L32643, EPID L-2022-DFA-0010 | |
| Download: ML23136B289 (1) | |
Text
Scoping Report: 144265-RPT-001, NIST Scoping Study Report NIST Scoping Study Revision: A Appendix Appendix C Liquid Scintillation Results
11/2/2022 3:22:04 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 1 Protocol# 4 - 5 Minute IPA subtract.ls a User: Default Assay Definition Assay Description :
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Output Data Path: C:\Packard\ Tricarb\Res ults\Defaul t\5 Minute IPA subtract\202 21102 1313 Raw Results Path: C:\Packard\ Tricarb\Res ults\Defaul t\5 Minute IPA subtract\202 21102-1313
\20221102 1313.result s Assay File Name: C:\Packard\T riCarb\As,sa ys\5 Minute IPA subtract.ls a Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Samp le: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On - IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions LL UL Bkg Subtract A 0.0 18.6 6.84 B 12.0 156.0 11. 63 C 156.0 2000.0 11.02 Count Corrections Static Controller: On Luminescenc e Correction: Off Colored Samples: Off Heterogenei ty Monitor: n/a Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 Instrument Block Data MODEL=Tri-C arb 3110TR VERSION=2.1 2 SERIAL=l183 98 Cycle 1 Results S# PID Count Time tSIE CPMA CPMB CPMC DPMl DPM2 MESSAGES 1 16 5.00 427.76 5 0 0 13 0 2 16 5.00 427.86 3 0 0 8 0 3 16 5.00 418.20 10 0 2 28 0 4 16
- rsJL-/ 5.00 425.09 5 0 2 15 0 5 16 5.00 411. 44 4 0 0 11 0 6 16 5.00 400.90 6 0 0 18 0
11/2/2022 3:22:04 PM Quan:taSmart (TM) - 4.02 - Serial# 118398 Page 2 Protocol# 4 - 5 Minute IPA subtract.lsa User: Default 7 16 5.00 407.16 7 2 0 19 2 8 16 5.00 423.77 4 1 0 10 0 9 16 5.00 417.64 9 0 1 26 0 1&-J~-J__ 10 16 5.00 405.62 10 2 0 27 1 11 16 5.00 440.42 3 0 0 9 0 12 16 5.00 434.97 9 0 0 24 0 13 18 5.00 421. 91 7 0 0 20 0 r 14 18 5.00 420.35 7 0 0 20 0
'3'i~
--15 16 17 18 18 18 5.00 5.00 5.00 426. 82 428.50 444.77 6
6 6
0 0
0 1
0 0
18 19 18 0
0 0
18 18 5.00 432.21 6 0 0 17 0
-1~.,,, 19 18 5.00 430.79 7 0 0 20 0 20 18 5.00 422.28 4 0 0 12 0
11/3/2022 9:21:16 AM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 1 User: Default Protocol# 4 - 5 Minute IPA subtract.lsa Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Output Data Path: C:\Packard\Tricarb\Re sults\Default\5 Minute IPA subtract\20221102 1313 Raw Results Path: C:\Packard\Tricarb\Re sults\Default\5 Minute IPA subtract\20221102-1313
\20221102 1313. results Assay File Name: C:\Packard\TriCarb\Ass ays\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Sample: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On - IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions LL UL Bkg Subtract A 0.0 18.6 6.84 B 12.0 156.0 11. 63 C 156.0 2000.0 11. 02 Count Corrections Static Controller: On Luminescence Correction: Off Colored Samples: Off Heterogeneity Monitor: n/a Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=118398 Cycle 1 Results
~ S# PID Count Time tSIE CPMA CPMB CPMC DPMl 'DPM2 MESSAGES 0 0 13 0
~ 1" 5.00 427.76 5 16 2 l"' 16 5.00 427.86 3 0 0 8 0 3 ,~ 16 5.00 418.20 10 0 2 28 0
'b cJl 4 ,~ 16 5 '\,0 16 5.00 425.09 411. 44 5
4 0
0 2
0 15 11 0
0
.,, 5.00 l ""6 16 5.00 400.90 6 0 0 18 0
QuantaSm art (TM) - 4.02 - Serial# 118398 Page 2 11/3/2022 9:21:16 AM Protocol# 4 - 5 Minute IPA subtract. lsa User: Default 16 5.00 407.16 7 2 0 19 2
~~34~;9--i 16 5.00 423.77 4 1 0
0 1
10 26 0
0 16 5.00 417.64 9 10.; 16 5.00 405.62 10 2 0 27 1 i..--
IH 16 5.00 440.42 3 0 0 9 0 l12, 16 5.00 434.97 9 0 0 24 0 3q3- 14 '\
13~ 18 18 5.00 5.00 421. 9_1 420.35 7
7 0
0 0
0 20 20 0
0 15 I:) 18 5.00 426. 82 6 0 1 18 0 16 18 5.00 428.50 6 0 0 19 0 0 18 0 4S'17 18 5.00 444.77 6 0
~~ 18 19 18 18 5.00 5.00 432.21 430.79 6
7 0
0 0
0 17 20 0
0 20 18 5.00 422.28 4 0 0 12 0
11/7/2022 1:57:04 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 1 Protocol# 5 - 5 Minute IPA subtract.lsa User: Default Assay Definition Assay
Description:
5 min count with IPA. BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Output Data Path: C:\Packard\Tricarb\Results\Default\5 Minute IPA subtract\20221107 1252 Raw Results Path: C:\Packard\Tricarb\Results\Default\5 Minute IPA subtract\20221107-1252
\20221107 1252.results Assay File Name: C:\Packard\TriCarb\Assays\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Sample: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On - IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions LL UL Bkg Subtract A 0.0 18.6 5.96 B 12.0 156.0 11. 42 C 156.0 2000.0 10 .. 65 Count Corrections Static Controller: On Luminescence Correction: Off Colored Samples: Off Heterogeneity Monitor: n/a Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=118398 Cycle 1 Results S# PID Count Time tSIE CPMA CPMB CPMC DPMl DPM2 MESSAGES i-ll')~~c.C, 1 16 5.00 411. 77 5 0 0 14 0 2 16 5.00 417.56 10 1 1 26 0
~\~ 3 16 5.00 419.59 10 1 0 27 0 4 16 5.00 407.61 5 0 0 15 0 5 16 5.00 404.58 10 6 0 24 6 FJ. J'Jf, '?.?..<-/ 6 16 5.00 411.46 5 1 0 13 0 A--3of,
11/7/2022 1:57:04 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 2 Protocol# 5 - 5 Minute IPA subtract.lsa User: Default 16 5.00 405.63 4 1 0 11 1 16 5.00 402.43 5 0 0 13 0 16 5.00 404.91 7 0 0 18 0 16 5.00 412.80 5 0 0 14 0
11/9/2022 8:59:41 AM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 1 Protocol# 3 - 5 Minute IPA subtract.lsa User: Default Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Output Data Path: C:\Packard\Tricarb\Results\Default\5 Minute IPA subtract\20221109 0821 Raw Results Path: C:\Packard\Tricarb\Results\Default\5 Minute IPA subtract\20221109-0821
\20221109 0821.results Assay File Name: C:\Packard\TriCarb\Assays\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Sample: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On - IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions LL UL Bkg Subtract A 0.0 18.6 6.43 B 12.0 156.0 11. 85 C 156.0 2000.0 10.83 Count Corrections Static Controller: On Luminescence ~orrection: Off Colored Samples: Off Heterogeneity .Monitor: n/a Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=ll8398 Cycle 1 Results S# PID Count Time tSIE CPMA CPMB CPMC DPMl DPM2 MESSAGES 1 12 5.00 391.08 3 1 0 9 1 2 12 5.00 382.91 4 0 1 12 0 3 12 5.00 385.83 44 0 0 126 0 eH,,- R.et*uA..+
4 12 5.00 398.33 4 2 0 11 2 5 12 5.00 390.05 5 0 0 15 0 6 12 5.00 436.93 5 0 0 13 0
11/9/2022 5:16:50 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 1 Protocol# 3 - 5 Minute IPA subtract.lsa User: Default Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Output Data Path: C:\Packard\Tricarb\Re sults\Default\5 Minute IPA subtract\20221109 1700 Raw Results Path: C:\Packard\Tricarb\Re sults\Default\5 Minute IPA subtract\20221109-1700
\20221109 1700.results Assay File Name: C:\Packard\TriCarb\Ass ays\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Sample: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On - IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off
~;,.'/ Bo 4 '::l Regions LL UL Bkg Subtract A 0.0 18.6 6. 43 B 12.0 156.0 156.0 11. 85 Rec.ouo.A-C 2000.0 10.83
~ 3 Count Corrections Static Controller: On Luminescence Correction: Off Colored Samples: Off Heterogeneity Monitor: n/a Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=118398 Cycle 1 Results S# PID Count Time tSIE CPMA CPMB CPMC DPMl DPM2 MESSAGES 1 12 5.00 389.37 2 0 0 6 0 Missing vial 2.
3 12 5.00 437.63 3 0 0 10 0
11/10/2022 12:45:07 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 1 Protocol# 3 - 5 Minute IPA subtract.lsa User: Default Assay Definition Assay
Description:
5 min count with IPA BKG subtract Assay Type: DPM (Dual)
Report Name: Reportl Output Data Path: C:\Packard\Tricarb\Results\Default\5 Minute IPA subtract\20221110 1128 Raw Results Path: C:\Packard\Tricarb\Results\Default\5 Minute IPA subtract\20221110-1128
\20221110 1128.results Assay File Name: C:\Packard\TriCarb\Assays\5 Minute IPA subtract.lsa Count Conditions Nuclide: 3H 14C Open Quench Indicator: tSIE/AEC External Std Terminator (sec): 0.5 2s%
Pre-Count Delay (min): 0.00 Quench Sets:
Low Energy: H-3 UG 16-0108A Mid Energy: C-14 UG 16-0108B Count Time (min): 5.00 Count Mode: Normal Assay Count Cycles: 1 Repeat Sample Count: 1
- Vials/Sample: 1 Calculate%
Reference:
Off Background Subtract Background Subtract: On - IPA Low CPM Threshold: Off 2 Sigma% Terminator: Off Regions LL UL Bkg Subtract A 0.0 18.6 6. 96 B 12.0 156. 0 10. 97 C 156.0 2000.0 11. 00 Count Corrections Static Controller: On Luminescence Correction: Off Colored Samples: Off Heterogeneity Monitor: n/a Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 Instrument Block Data MODEL=Tri-Carb 3110TR VERSION=2.12 SERIAL=118398 Cycle 1 Results s# PID Count Time tSIE CPMA CPMB CPMC DPMl DPM2 MESSAGES 1 12 5.00 401. 89 2 2 0 4 2 2 12 5.00 386. 36 12 6 0 29 6 3 12 5.00 378.98 21 7 0 56 5 4 12 5.00 380.44 5 0 0 13 0 5 12 5.00 370.99 6 0 0 18 0 6 12 5.00 413. 29 7 1 0 19 0
11/10/2022 12:45:07 PM QuantaSmart (TM) - 4.02 - Serial# 118398 Page 2 Protocol# 3 - 5 Minute IPA subtract.lsa User: Default 7 12 5.00 377.20 5 0 0 14 0 8 12 5.00 394.38 6 2 0 14 2 9 12 5.00 403. 96 4 0 0 12 0 10 12 5.00 408.58 6 1 0 17 1 11 12 5.00 427.68 6 1 0 14 0 12 12 5.00 430.71 4 0 0 13 0