ML23136B287

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Scoping Report 144265-RPT-001, Appendix a - Scoping Survey Calibration Sheets, Rev. a
ML23136B287
Person / Time
Site: 07000398
Issue date: 05/16/2023
From:
US Dept of Commerce, National Institute of Standards & Technology (NIST)
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML23136B277 List:
References
TAC L32643, EPID L-2022-DFA-0010
Download: ML23136B287 (1)
v • d • e


Text

Scoping Report: 144265-RPT-001, NIST Scoping Study Report NIST Scoping Study Revision: A Appendix Appendix A Scoping Survey Calibration Sheets

Safety and Ecology Corporation SEC PROCEDURE# ICAL # 67 Rev o 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 0 ~~====== Calibration Certificate

==

Calibration Certificate for MICRO REM,Seria/ # E050A, Bar Code #,Property# SEC-5378 Date: 04/26/22 Date Last Cal. Expires: 12/10/20 Technician: Jacob Galyon Reason For Calibration: Due for Calibration EQUIPMENT USED DURING CALIBRATION MODEL MP-2 SERIAL#: 314 CAL DUE: 01/11/23 MODEL 87V SERIAL#: 18740384 CAL DUE: 03/01/23 MODEL SERIAL#: CAL DUE:

NIST TRACEABLE SOURCES USED SOURCE ISOTOPE ACTIVITY ASSAY DATE 0300-GY Cs-137 202.897 Ci 2/14/2022 KR-4097 Cs-137 65.94 mCi 2/14/2022 AS FOUND DATA Physical Cond SAT Geotropism: SAT Bat. Check SAT Speaker Check N/A As Found As Left High Voltage High Voltage Indicated in OK Band OK OK

+5 Volt Power Supply (4.5 to 5.5V) 5.086 5.086

-5Volt Power Supply (-3.74 to -5.06 V) -4.27 -4.27 CALIBRATION DATA HVAL Scale Exposure Rate Instrument Reading Percent Error uR/HR _ {MR/HR) ____ f:-s Fou~ ____ As Left As Found

- As Left 0 !______ o_.1_ _ _ _ _5_

r-10

{Pulsed= TO)

(Pulsed = TO)

_5~~--- _

10 5.25

_ _ -~~

-1 5.00 0.00 5.00 0.00

______ 1 15 {Pulsed= TO) , 16 ________ _!~_ __ 6.67 6.67 1 50 (.05) , 52.5 _ _52.5_ -- -~ _ _ ~J~. _ _ 5.00 100 j* (.1) ' 100 . 100 0.00 0.00 L---~-- .. --------~-- .? -

150 ;, (.15) 160 160 6.67 6.67

-- ----------1--- - --------*

10 f 500 (0.5) _ -- ---- 500 -- _ _:i0~- _ - __ 0.00 0.00 1000 (1.0) 950 _ _ _:1__~~- -* -5.00 0.00

_ _ _ _ ___,_ 1500 _ (1.5)_ ----- _ __:1__~00 ________ _,_ 15~0 0.00 3.33 100 5000 (5) 4500 5000 -10.00 0.00 10000 (10) 9250 10000 -7.50 0.00 t 15000 (15) 14000

- 15000 -6.67 0.00

+--- --- -*- -~-- ..... - -* ---

~_ _1_o_oo ____ J 50000 {50) 47500 47500 -5.00 -5.00 100000 (100) 100000 100000 0.00 0.00 Precision -15_0_0_0_0_:_ _..,c..{_15_0_)---,-- 147500 147500___ - *--:f57 **-; ----- - --.

~==~--

Scale

---::::======Exposure Rate

==== As Found Mean Value 3/4Dev

-1.67 X1000 100000 (100) 100000.00 0.00 100000:00 100000.00 0.00 100000.00 0.00 Comments:

~ D.oes Instrument Meet Final Acceptance Criteria? li2I Calibration S ~ r a t l o n o,e Date, ~

Performe~r.-==::f ~ ~ J.,,irr-. Reviewed by: ~ Issue Date: tf ./}-£/,,-r-;)....

Printed rme: j Jacobklalyon ) D All instru~entation11s calib~ated in aclardance with the QAP to meet the criteria of ANSI N323AB-2013 The results~ this,/eport re1J,e only }o' the item calibrated or tested.

Page 1 of 1

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-407 Rev 3 l"JLA 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 calibration 1so11t: ro~s.2~:1

--~~*-**:~:-l!Q Calibration Certific;;,te Calibration Certificate for 44-9,Serial # PR150385, Bar Code #,Property# SEC-5121 Date: 09/28/22 Date Last Cal. Expires: 10/19/22 Technician: Jake Alcorn Reason For Calibration: Due for Calibration Temp: RelHum: BP: Cablelength 5 Ft NIST EQUIPMENT USED DURING CALIBRATION MODEL: 12 SERIAL#: 229284 CAL DUE: 09/28/23 MODEL: SERIAL#: CAL DUE:

NIST TRACEABLE SOURCES USED SOURCE ISOTOPE ACTIVITY 2Tl' ASSAY DATE 5746-06 Tc-99 31899 dpm 19,999 cpm 1/31/2022 5744-06 Sr-90 14539 dpm 10,202 cpm 1/31/2022 Geometry= .in contact with surface unless otherwise specified.

PREVIOUS Tc-99 EFFICIENCY: 13.66% Calibration Voltage: 900V Calibration Threshold: 35mV AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT AS FOUND DATA AS LEFT DATA 1 MINUTE COUNTS (CPM) 1 MINUTE COUNTS (CPM)

AF

Background:

26 AL

Background:

26 AVERAGE AVERAGE Tc-99 Count: 4212 4134 4124 4156.7 Tc-99 Count: 4212 4134 4124 4156.7 Sr-90 Count: 3294 Sr-90 Count: 3294 4 Tl' Efficiencies 4 Tr Efficiencies Tc-99 EFF: [12.9~% Sr-90 EFF: 12~.48%.

"AF" in the AL Efficiency fields means to refer to the AF Efficiencies in the AS FOUND DATA Section

~ Is the AS FOUND efficiency within 20% of efficiency from last calibration?

~ Reproducibility: Are the individual counts within 10% of the average?

~ Does the probe meet final acceptance criteria?

~ Calibration sticker attached?

Comments: Married as a set with: Model: 12 Serial #: 229284 Bar Code#:

by;,0! -'%

Date Instrument is Due For Next Calib~ation: ~:09/2~/23 Perto,med by,~

Printed Name: Jake Alcorn

))e;...L7< - Rovlewed Issue Date: /0 *;l,2

  • 2(

All instrumentation is calibrated in accordance with the QAP to meet the criteria of ANSI N323AB-2013 The results in this report relate only to the item calibrated or tested.

Page 1 of 2

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-404 Rev 3 l'JIA 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Callbratlon

~o;ie: 1:-01s.2:::

.. ~1*-,1-*101-1~1 Calibration Certificate Calibration Certificate for 12,Seria/ # 229284, Bar Code# ,Property# SEC-6278 Date: 09/28/22 Date Last Cal. Expires: 10/19/22 Technician: Jake Alcorn Reason For Calibration: Due for Calibration Temp RelHum: BP:

NIST EQUIPMENT USED DURING CALIBRATION MODEL: 500-2 SERIAL#: 190580 CAL DUE: 06/08/23 MODEL: SERIAL#: CAL DUE:

AS FOUND DATA Geotropism: SAT AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT HIGH VOLTAGE AS FOUND HV AS LEFT HV O New Batteries? Battery Check: SAT Alarm: NIA

(+/-10% tolerance) 500 V: 515 515 AS FOUND Mechanical Zero: 0 AS LEFT Mechanical Zero: 0 1000 V: 990 1000 AS FOUND THRESHOLD: 33.5mV AS LEFT THRESHOLD: 35mV 1500 V: 1475 1480 AS FOUND HV Reading: 900V AS LEFT HV Reading: 900 V HV Range 400-1500V:. SAT RATE MEJER DIGITAL SCALER SCALE RATE CPM AS FOUND % ERROR AS LEFT% ERROR

-- 100 100 t 0.00%

AF 250: 251  % ERR: 0.40% AL250: AF 3/4ERR: 0.40%

x.1 or 100 0.00%

x1

- - - - ~- - -- -- -~--- - - ;,...--- ------ - AF 2500: ,2510 % ERR: 0.40% AL2500: AF  % ERR: 0.40%

250 255 2.00%

250

- 0.00%

~ - --

I x1 or 400 1000 405 1000 J 1.25%

0.00%

400 1000 0.00%

0.00%

I AF25K: 25.1 K % ERR: 0.40% AL25K: AF K % ERR: 0.40%

x10 2500 2550 2.00% 2500 0.00%

l AF 100K: 100.4 K % ERR: 0.40% AL 100K: AF K % ERR: 0.40%

*--*,- ' - ~ Is the As Found Data Within 20% of the Set Point?

-~000 _ ..L 4005 l 0.12% 4000 0.00%

~~- 10K 10 0.00% 10 0.00% -REPRODUCIBILITY x100 25K 25.5 2.00% 25 0.00% x.1 or x1 Scale: 250 250 250 40.5

-r 40 0.00%

~

40K  ! 1.25% I x100 or 100K

-.------- 105  ; 5.00% r 100- . 0.00%

x1 or x10 Scale: 2500 2500 2500 x1000 250K 400K I

I 255 I

i 2.00% i 41.0... ,_ f 2.50% _1_ 400 250 0.00% l 0.00%

x10 or x100 Scale:

x100 or x1000 Scale:

25 K 250 K 25 K 250 K 25 K 250 K

~ Are the Individual Counts Within 10% of the Average?

~ Is the As Found Data Within 20% of the Set Point? ~ Fast/ Slow Response Switch Functions Properly?

Audio Response: SAT Audio Divide: N/A Push Buttons: SAT Lamp:N/A Scaler/Digital: SAT Comments: Married as a set with: Model: 44-9 Serial#: PR150385 Bar Code#:

.~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

~V-..

-~~:u;~;2 Date lnst,F-.u~nt is Due For Next Calibration: [09/28/23 *

,:::;::~: ~ ~ l o o m ~ Re~ewed "?Ill 1<r--9....,,,-- lme Dare, All instrumentation is calibrated in accordance with the OAP to meet the criteria of ANSI N323AB-2013 The results in this report relate only to the item calibrated or tested.

Page 1 of 2

~ l'JIA Calibration Safety and Ecology Corporation 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 sEc PROCEDURE# sEc-Is-411 Rev 5

-:sc11~::r;cn12011

.au....i.r-.1....... 107.1.62 Calibration Certificate Calibration Certificate for 43-37,Serial # PR042477, Bar Code #,Property# SEC-5027 Date: 10/17/22 Date Last Cal. Expires: 05/05/23 Technician: Jeffrey Knight Reason For Calibration: Due for Calibration CableLength EQUIPMENT USED DURING CALIBRATION

- - ---- - - -.... ~-~

_______ MODEL: 2360 SERIAL #: ?87589 CAL DUE 10/17/23 NIST TRACEABLE SOURCES USED SOURCE ISOTOPE ACTIVITY 2rr ASSAY DATE L

Efficiencies from last calibration 5747-06 Pu-239 25793 dpm 13,097 cpm 1/31/2022 Pu: 12.10  % 5746-06 Tc-99 31899 dpm 19,999 cpm 1/31/2022 Tc: 17.54  % 5748-06 Th-230 34897 dpm 17,699 cpm 1/31/2022 Th: 7.44 % 5744-06 Sr-90 14539 dpm 10,202 cpm 1/31/2022 SrY: 28.65 %

AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT AS FOUND DATA Calibration Setpoints AS LEFT DATA after repair, HV adjust or Plateau HV: 1750 V Threshold Beta: 4 -- 40 mV Alpha: 120mV HV: 1700 V Back Alpha Beta AF 4 rr Efficiences Alpha Beta AL 4 rr Efficiencies A-BXTLK Back ground: 4 CPM 669 CPM ground: 2 CPM 533 CPM A-BXTLK Pu-239: 4278 CPM 1~~5.7% 10.36%

1112 CPM 19_;$_8~

Pu-239: 3883 CPM 757 CPM t1s;9,s% _ 5.77%

Tc-99: 28 CPM 6916 CPM Tc-99: 13 CPM 7511 CPM  ! ,21~fi:a3/4 -

Th-230: CPM N/A Th-230: 4419 CPM N/A  ;,1:~6~%

SrY-90: N/A CPM SrY-90: N/A 4661 CPM (;~~-~~%~

D Is the As Found Data within 20% of the efficiency from "AF" in the AL Efficiency fields means to refer to the AF the last cal.? Efficiencies in the AS FOUND DATA Section Reproducibility: Isotope: ~ 7468 7383 7330 Average: 7393.7 ~ Are the individual counts within 10% of the average?

j¥ th~-~J'.ounfl_d~fa (eyen af!~r .repair) ts williin'1b_% ofthe: last:cilfi,b,fation.an{lll~ B,l:'. X\alk is,<1 % a~a thEl_/\'B*J,ct~lk is~O%, tl)e_n the t~giniciari in'!Y N/~the:Plilteau D_~fallod "go- direcyy le;> 1 POIJ1.!!]8iJl~_-_'Geome!ryof'sburce='n91\jtbsurfas~c~XC8P.!JJ8§_fi'r.9E<irlional_i:>robes=1/B"ffomsur_faceuniesscitherwisesf)edlied. . - _*: __ "=-- - ~----*--*. ------- -,-. '

PLATEAU DATA Source 1.: Sr-90 Source 2: Pu-239 Response (CPMl Response (CPM} Background (CPMl Net A to B High Voltage A ch. B ch. Net Eff. A ch. B ch. Net Eff. A ch. B ch. Xtalk: <10%

1700 I 9 I 4537 I 21.42% 3987 l 141 l 15.44% 5 I 550 I 4.80%  ;

1720 9 j 4716 I 28.58% 3969 i 882 l 15.36% 7 I 561 1 I 8.10%

1730 r~ 4967 l 30.11% 4194  ; 2813 / 16.26% 0 l 580 I 54.67%

I

'l L l 1 i 1 t

l \

I I i  ! I i l i-------1 l

j 1 1

I I l I l I

~ ~ ~ §rX:!m 2 Pi Efficiencies: [.29,6~%,j I;3~;89.'Vc, I 1-. 24~$.~% V4o~~so/c, Comments: Married as a set with: Model: 2360 Serial #: 287589 Bar Code#:

Calibrated with Teflon spacers installed. New plateau to determine HV setting.

~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration: J:fotWi2.3:;: _",~J All instrumentation is calibrated in accordanc; with the OAP to meet the criteria of ANSI N323AB-2013 lfilrn~mHl~~~~llffl

~---//?7_ v/;, ff Performed by,,,*='""""4,.,!,;,:o....,.,__..,L..L.¢."7---1---- Reviewed by:. _ ___,,,~----~"LL~L-~_lssue Date: /v/lf/})

Printed Name: Page 1 of 2

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-418 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Oak Ridge, TN 37830 Calibration Certificate Calibration Certificate for 2360,Serial # 287589, Bar Code# ,Property# SEC-7426 Date: 10/17/22 Date Last Cal. Expires: 05/05/23 Technician: Jeffrey Knight Reason For Calibration: Due for Calibration NIST EQUIPMENT USED DURING CALIBRATION MODEL: 500-2 SERIAL#: 153622 CAL DUE: 11/16/22 MODEL: SERIAL#: CAL DUE:

- ------- ____ , .......... _ -----~- ---- - -- -------- ----

AS FOUND DATA Geotropism: SAT AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT

~ New Batteries? Battery Check: SAT AS FOUND Mechanical Zero: 0 AS LEFT Mechanical Zero: 0 HIGH VOLTAGE AS FOUND HV AS LEFTHV WINDOW SETTINGS AS FOUND AS LEFT

(+!- 10% tolerance} 500V: 500 V 513 V BT (4 mV +/*. 4 mV): 4 mV AF mV 1000 V: 980 V 1000 V BW (40 mV +/. 4 mV): 41 mV 40 mV 1500 V: 1458 V 1492 V AF HV Setting: 1750 V AL HV Setting: 1700 V AT (120 mV +/-10 mV): 120 mV AF mV SCALE RATE CPM AS F,QUND % ERROR AS LEFT% ERROR H AF 250: 249 D1GffAL,'.$CAl.,.ER

% ERR: 0.40% AL 250: AF  % ERR: 0.40%

l x.1 or I 100 100 0.00% AF  ! 0.00% I x1 AF 2500: 2494  % ERR: 0.24% AL 2500: AF  % ERR: 0.24%

I 250

- -400-. ' 250 I 0.00% AF I 0.00%

1 AF 25K: 24.94 K % ERR: 0.24% AL 25K: AF K % ERR: 0.24%

 : 400 I 0.00% AF f 0.00%

x1 or 1000 1000 l 0.00%

I AF I 0.00% AF 250K: 249.4 K % ERR: 0.24% AL 250K: AF K % ERR: 0.24%

f x10 f

I 2500 l 2500 I 0.00% AF I 0.00% ~ Is the As Found Data Within 20% of the Set Point?

I 4000 j 1

4000 I 0.00% AF I 0.00% r:.:-*-

R.EPRO'lllJCIB.ILITV 1_  ;

  • x10 or 10K i 10 0.00% AF I 0.00% L - ' - , - -- - - - -- - ... - - - ~ - _, _

__, __ ,j x100 I 25 j l 25K I I 0.00% AF 0.00% x.1 or x1 Scale: 250 250 250 40K 40 0.00% AF ' 0.00%

l x1 or x10 Scale: 2500 2500 2500

!x100 or 100K 100 0.00% AF 0.00%

x1000 x10 or x100 Scale: 25 K 25 K 25 K 250K 250 0.00% AF 0.00%

400K 400 0.00% AF 0.00% x100 or x1000 Scale: 250 K 250 K 250 K

~ Are the Individual Counts Within 10% of the Average?

~ Is the As Found Data Within 20% of the Set Point? Audio Response: SAT Overload Light: SAT Low Battery (2.2V): SAT Comm-ents: Married as a set with: Model: 43-37 Serial #: PR042477 Bar Code#:

~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration: l1Qh7J23 ;;* . *1 Perlo,med by,;,~-~

Printed N a m e : ~ y ight

~L?

Reviewed b y : _ ~ ~ = _ -_ --....,_

-_ " -_.lssue Date:

l (J,1° lf*-v/'}-}-

All instrumentation is calibrated in accordance with the OAP to meet the criteria of ANSI N323AB-2013 The results in this report relate only to the item calibrated or tested.

Page 1 of 1

SEC PROCEDURE# SEC-IS-418 Rev 3 Safety and Ecology Corporation 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Oak Ridge, TN 37830 Calibration Certificate ration Certificate for 2360,Serial # 227394, Bar Code #,Property# SEC-6283 Date: 10/20/22 Date Last Cal. Expires: 06/21/23 Technician: Jeffrey Knight Reason For Calibration: Other (See Comments)

NIST EQUIPMENT USED DURING CALIBRATION MODEL: 500-2 SERIAL#: 153622 CAL DUE: 11/16/22 MODEL: SERIAL#: CAL DUE:

AS FOUND DATA Geotropism: SAT AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT

[g] New Batteries? Battery Check: SAT AS FOUND Mechanical Zero: 0 AS LEFT Mechanical Zero: 0 HIGH VOLTAGE AS FOUND HV AS LEFTHV WINDOW SETTINGS AS FOUND AS LEFT

(+/-10% tolerance) 500V: 509 V AF V BT (4 mV +/- .4 mV): 3.4 mV 4 mV 1000 V: 995 V AF V BW (40 mV +/- 4 mV): 40 mV AF mV 1500 V: 1488 V AF V AF HV Setting: 1800 V AL HV Setting: 1800 V AT (120 mV +/- 1.0 mV): 120 mV AF mV

~-~--__..__._ ~---- '

p DIGITAL

~-~

$_()ALER .'

SCALE RATE CPM AS FOUND  % ERROR AS LEFT% ERROR AF 250: 249  % ERR: 0.40% AL 250: AF  % ERR: 0.40%

\ x.1 or I 100 l 100 0.00% AF I

i 0.00% AF 2500: 2494  % ERR: 0.24% AL 2500: AF  % ERR: 0.24%

x1 t 250 f 250 0.00% AF 0.00%

400 t 400 0.00% AF I 0.00% AF 25K: 24.95 K  % ERR: 0;20% AL 25K: AF K % ERR: 0.20%

l x1 or \ 1000 1000 I 0.00% AF '; 0.00% f AF 250K: 249.9 K  % ERR: 0.04% AL 250K: AF K % ERR: 0.04%

~(j Ll  ! i I 2500 2500 0.00% AF 0.00% ~ Is the As Found Data Within 20% of the Set Point?

4000 '

Il 4000 t 0.00% AF  ! 0.00% ,....-**~-.

- ~ :,._ * ~ r.,.-< ,-*,.--,-,-~-,--*

1

. x10 or I 10K 10 I 0.00% AF 0.00% i REPRODUGIBllllFf

. .' ,, ... .... . ~ ..,

~

I x100  ! 25K i 25 ' 0.00%

AF Ij 0.00% x.1 or x1 Scale: 250 250 250 l 40 40K r 0.00% AF 0.00% x1 or x10 Scale: 2500 2500 2500 I x100 or.! 100K I 100 f 0.00%

j AF 0.00%

x1000 j l x10 or x100 Scale: 25 K 25 K 25 K 250K I 250 1' 0.00% AF 0.00% j I 250 K l

400K I

400 0.00% AF 0.00% x100 or x1000 Scale: 250 K 250 K i I t I

~ Are the Individual Counts Within 10% of the Average?

~ Is the As Found Data Within 20% of the Set Point? Audio Response: SAT Overload Light: SAT Low Battery (2.2V): SAT Comments: Married as a set with: Model: 43-37 Serial#: PR037449 Bar Code#:

Calibrated for new customer.

~ Does Instrument Meet Final Acceptance Criteria? .~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration: lf9l20,f23-' .,,,

Performed by:

Printed Name:

td:/,{_,I

'.faf

I/((}

y K~t

/~

Reviewed by:

,/P'.d'://L.,_..-//

~ / Issue Date: fO/}--f/).,:;L All instrumentati n is calibrated in accordance with the QAP to meet the criteria of ANSI N323AB-2013

) The results in this report relate only to the item calibrated or tested.

0 Page 1 of 1

~

Safety and Ecology Corporation sEc PROCEDURE# sEc-Is-411 Revs PJIA 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 C..llbr.1lltJn ISO/lfCl702S:20:1

.:l~<lit.n~11*:C7462 Calibration Certificate Calibration Certificate for 43-37,Seria/ # PR037449, Bar Cod~# ,Property# SEC-5030 Date: 10/20/22 Date Last Cal. Expires: 06/21/23 Technician: Jeffrey Knight Reason For Calibration: Other (See Comments CableLength EQUIPMENT USED DURING CALIBRATION MODEL: 2360 SERIAL#: 227394 CAL DUE 10/20/23 NIST TRACEABLE SOURCES USED SOURCE ISOTOPE ACTIVITY 2TT ASSAY DATE Efficiencies from last calibration 5747-06 Pu-239 25793 dpm 13,097 cpm 1/31/2022 Pu: 13.90  % 5746-06 Tc-99 31899 dpm 19,999 cpm 1/31/2022 Tc: 15.96  % 5744-06 Sr-90 14539 dpm 10,202 cpm 1/31/2022 Th: 11.82 % 5748-06 Th-230 34897 dpm 17,699 cpm 1/31/2022 AK-2579 C-14 23986 dpm 1/31/2022 SrY: 27.61  %

AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT AS FOUND DATA Calibration Set1;1oints AS LEFT DATA after re1;1air, HV adjust or Plateau HV: 1800 V Threshold Beta: 4 - 40 mV Alpha: 120 mV HV: 1725 V Back Al1;1ha Beta AF 4 TT Efficiences Al1;1ha Beta AL 4 TT Efficiencies A-B XTLK Back ground: 20 CPM 712 CPM ground: 3 CPM 582 CPM A-BXTLK 4478 CPM CPM ffT,.28% 9.71%

1145 Pu-239: 3560 CPM 868 CPM r-1~:1~% 8.04%

cs239'.

c-99. 307 CPM 5376 CPM -t 1~.62% 120:4~%.*

r . - , Tc-99: 17 CPM 7117 CPM Th-230: CPM N/A Th-230: 3694 CPM N/A l'.,10:~a%~

SrY-90: N/A CPM l SrY-90: N/A 4836 CPM r 2~:;2'fi3/4 '.

0 Is the As Found Data within 20% of the efficiency from "AF" in the AL Efficiency fields means to refer to the AF the last cal.? Efficiencies in the AS FOUND DATA Section Reproducibility: Isotope: I Sr-90 j 5026 4926 4931 Average: 4961.0 ~ Are the individual counts within 10% of the average?

.,.. -*.--.*.---~* ,. ... ,-,----i- -*;r.-----~.---- _,,..;. ~--.....---.----,---.,_. __ ---~---------~--- ~.,-,.,-._... ~-----,---.--~----*-~ -~~.----~-,-.--.-...,-----1r *,*- *...,.

lfJl_l; ~ *Ffi,L!nd da\;I {O:,V!'O ,after'riepa~),is,wi!hin '10% oflhe lafl calibr":l\<if\~ng ti)~ B:AXtalk )5, :<1% anq tll;.:J'i:B X\a!,k is:<1 o;yc. 11J~n tl)e techniciaifmay N/A:.tha Pl~teau Data.and go \tife9t1y. to j

£omments., 'Geo_l!J:el!)'. of source =*flush to sur:face; except gas_eroport1onal probes= 1/8"-from surface*unless*othe1W1se*s~ _ , ,. ___ ~ . -~- ' __-.!

PLATEAU DATA Source 1: Sr-90 Source 2: Pu-239 Res1;1onse (CPMl Res1;1onse (CPMl Background (CPMl Net A to B High Voltage A ch. B ch. Net Eff. A ch. B ch. Net Eff. Ach. B ch. Xtalk: <10%

1700  ! 7 4442 j 26.76% 3548 i 796 I13.74% 5 I 552 i i 6.89% t 1725 .1 ; 5 4931 I 29.44% 3414 946 j 13.22% 3 650 I I' 8.68%

1150 I I 33 5163 I 30.15% 3717 1070 f 14.40% 3 692 I 10.18%

II I i I

j I I I I  !

~ ~ ~ §rY:fil!

2 Pi Efficiencies: [:;!tAs%*1 l a:2re~o/c{j I, ,20:as$: j I'4f;193/4 ,I Comments: Married as a set with: Model: 2360 Serial #: 227394 Bar Code#:

AF: High background - new plateau to verify HV setting. Calibrated with Teflon spacers installed. C-14 source #AK-2579: 3164 gcpm/23,986 dpm = 10.76% efficiency.

~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

0 Porio,mod by, Printed Name:

/J¢- ~
~1gh Reviewed by: ~ Issue Date: i(J/Jrf/}J-Page 1 of 2

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-418 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Oak Ridge, TN 37830 Calibration Certificate CJibration Certificate for 2360,Serial # 227402, Bar Code# ,Property# SEC-6214 Date: 09/20/22 Date Last Cal. Expires: 09/20/23 Technician: Noah Kaye Reason For Calibration: Due for Calibration NIST EQUIPMENT USED DURING CALIBRATION MODEL: 500-2 SERIAL#: 171700 CAL DUE: 06/07/23 MODEL:

  • SERIAL#: CAL DUE:

AS FOUND DATA Geotropism: SAT AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT

[] New Batteries? Battery Check: SAT AS FOUND Mechanical Zero: 0 AS LEFT Mechanical Zero: 0

  • 'L HIGH VOLTAGE AS FOUND HV AS LEFT HV WINDOW SETTINGS AS FOUND AS LEFT

(+/- 10% tolerance) 500V: 511 V AF V BT (4 mV +/- .4 mV): 4 mV AF mV 1000 V: 1009 V AF V 1500 V: BW (40 mV +/- 4 mV): 30 mV AF mV 1508 V AF V AF HV Setting: 680 V AL HV Setting: 675 V AT (120 mV +/-10 mV): 121 mV AF mV RATE*METER  :.... *- .. -~_ ... ___ _.,.i.._ _ _ _ ....;:.:,..... Pl~ITA~ SCALER

- >--*- * - ~--- --- t ---- . --~- v ---- -.- ---*L.-

SCALE RATE CPM AS FOUND % ERROR AS LEFT% ERROR AF 250: 250  % ERR: 0.00% AL250: AF  % ERR: 0.00%

x.1 or 100 100 0.00% AF 0.00%

x1 AF 2500: 2514  % ERR: 0.56% AL 2500: AF  % ERR: 0.56%

250 250 0.00% AF 0.00%

400 400 0.00% AF 0.00% AF 25K: 24.9K  % ERR: 0.40% AL25K: AFK % ERR: 0.40%

x1 or 1000 1000 a

0.00% AF 0.00% AF 250K: 249K  % ERR: 0.40% AL 250K: AF K %ERR: 0.40%

10 2500 2500 0.00% AF 0.00% ~ Is the As Found Data Within 20% of the Set Point?

4000 4000 0.00% AF 0.00%

x10 or x100 10K I 10 I 0.00% AF 0.00% ;_, __, --- _._REP'RQDUCIBIL

-- - '*_,,,._...., "_;,. --~_.,...ITY 25K I 25 0.00% AF 0.00% x.1 or x1 Scale: 250 250 250 40K 40 0.00% AF 0.00% '

x1 or x10 Scale: 2500 2500 2500 x100 or 100K 100 0.00% AF 0.00%

x1000 x1 O or x100 Scale: 25 K 25 K 25K 250K 250 0.00% AF 0.00%

400K 400 0.00% AF 0.00% x100 or x1000 Scale: 250 K 250 K 250K

~ Are the Individual Counts Within 10% of the Average?

~ Is the As Found Data Within 20% of the Set Point? Audio Response: SAT Overload Light: rSAT Low Battery (2.2V): SAT Comments: Married as a set with: Model: 43-93 Serial #: PR394086 Bar Code#:

~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration: [Q9/20/?~ .. *~:! I Performed by:

Printed Name:

U Noah Kaye

~z Reviewed bye ~ff Js,ue Dalee q/Jf/J-')---

All instrumentation is calibrated in accordance with the QAP to meet the criteria of-ANSI N323AB-2013 liillOOIMIIJHm The results in this report relate only to the item calibrated or tested.

0 Page 1 of 1

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-420 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Q

l'JLA C,0 C*llb,alion Ca l"b

  • C rt*,&,* t 0

"' ""'*" .:::::.::::.:::':;::::, 1 ration e wca e Calibration Certificate for 43-93,Serial # PR394086, Bar Code #,Property# PFL-354 Date: 09/20/22 Date Last Cal. Expires: 03/30/23 Technician: Noah Kaye Reason For Calibration: Due for Calibration Temp: RelHum: BP: CableLength 5 Ft EQUIPMENT USED DURING CALIBRATION MODEL: 2360 SERIAL#: 227402 CAL DUE 09/20/23 ft..:.*

.,. 1-*

\,, \

NIST TRACEABLE SOURCEs*i:JsED SOURCE ISOTOPE ACTIVITY 2TT ASSAY DATE t..'t

  • \::>\f' Efficiencies from last calibration 4079-02 Pu-239 28991 dpm 14,695 cpm 1/31/2022 Pu: 23.40 % 4072-02 Tc;99 28299 dpm 17,699 cpm 1/31/2022 Tc: 17.24  % 4071-02 Th-230 40296 dpm 20,498 cpm 1/31/2022 Th: 21.63 % 4076-02 ISr-90 9306 dpm 6,529 cpm 1/31/2022 SrY: 35.20 %

AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT AS FOUND DATA Calibration Setpoints AS LEFT DATA after repair, HV adjust or Plateau HV: 675 V Threshold Beta: 4 - 40 mV Alpha: 120mV HV: 675 V Back Alpha Beta AF 4 TT Efficiences Back Alpha Beta AL 4 TT Efficiencies ground: 2 CPM A-B XTLK 143 CPM ground: 2 CPM 143 CPM ~~~ A-B XTLK Pu-239: 6709 CPM 556 CPM i3,1~%- 6.16%

1_1p~_o/o; Pu-239: 6809 CPM 556 CPM '23JIJ,% 6.07%

Tc-99: 3 CPM 5450 CPM 21.fQ"lr/

Tc-99: 3 CPM 5450 cPM 1'ads%'

~ Th-230: 8505 CPM NIA "35J!J%*

Th-230: 8505 CPM NIA 21do%

SrY-90: N/A 3435 CPM SrY-90: NIA 3435 CPM . '3'5:3~'1/6.

~ Is the As Found Data within 20% of the efficiency from "AF" in the AL Efficiency fields means to refer to the AF the last cal.?

Efficiencies in the AS FOUND DATA Section Reproducibility: Isotope: I Sr-90 I 3555 3515 3532 Average: 3534.0 ~ Are the individual counts within 10% of the average?

"itu,e ~ Found ~ata (even~~fter rep~ir) is williin 10% of llieiait calititation and ihe B'.A Xtaik.i!i <1 %~rid the A::s xialk is :;,10%:* iiieq the fech~iclan inay N[Aihe'Piateau o;ta and go directly to

£9nifii_~2t~:~Ge£_inetiyo(,;_c,_~rce =fllish"\o _s.ilrf§~,~x~pt 9!!~prcjpprtjopal pr!]bes=Jf.8"fr.9m:s.'Jrf~~ aJirii_stetii!'~e,_sj)Jgifi~i:!:_:' Jc,____ - - -- . . --- **- _ *.

PLATEAU DATA Source 1: Tc-99 Source 2: Th-230 Response (CPM) Response (CPM) Background {CPM) Net A to B

/I High Voltage N/A A ch. B ch. Net Eff. A ch. B ch. Net Eff. A ch. B ch.

I Xtalk: <10%

N/A I N/A N/A N/A N/A

.. I N/A

~ ~ ./

2 Pi Efficiencies: F4~;~?%J b~s~~s~J Comm.e"nts: ~ .c. Married as a set with: Model: 2360 Serial#: 227402 Bar Code#:

~ Does Instrument MeetFinal Acceptance Criteria? ~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration: lo~12Qfg~ :.,-~-.. J 8 All instrumentation is calibrated in accordance with the OAP to meet the criteria of ANSI N323AB-2013 Perto,med b y , ~ ~

Printed Name: Noah Kaye

,6:z Reviewed by, ~ Issue Date:

Page 1 of 2

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-418 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Oak Ridge, TN 37830 Calibration Certificate Calibration Certificate for 2360,Serial # 184947, Bar Code # ,Property # SEC-5549 Date: 10/14/22 Date Last Cal. Expires: 06/07/23 Technician: Jeffrey Knight Reason For Calibration: Repair NIST EQUIPMENT USED DURING CALIBRATION MODEL: 500-2 SERIAL#: 153622 CAL DUE: 11/16/22 MODEL: SERIAL#: CAL DUE:

AS FOUND DATA Geotropism: SAT AS FOUND Instrument Condition: UNSAT AS LEFT Instrument Condition: SAT Q] New Batteries? Battery Check: SAT AS FOUND Mechanical Zero: 0 AS LEFT Mechanical Zero: 0 HIGH VOLTAGE AS FOUND HV AS LEFTHV WINDOW SETTINGS AS FOUND AS LEFT

{+/- 10% tolerance} 500 V: 496 V 502 V BT (4 mV +/- .4 mV): 3.1 mV 4 mV 1000 V: 984 V 1000 V BW (40 mV +/- 4 mV): 28 mV 40 mV 1500 V: 1473 V 1489 V AF HV Setting: 650 V AL HV Setting: 650 V AT (120 mV +/-10 mV): 120 mV 123 mV

.___._~-*. . . . ~te MET~R, . H~: ~----*o_*.1~G_t1~:*,A~.L~.s_:e_*A_L_E_R_:._ _ __

SCALE RATE CPM AS FOUND % ERROR AS LEFT% ERROR AF 250: 250  % ERR: p.00% AL250: AF  % ERR: 0.00%

I' 0.00%

l

x.1 or L 100 1 100 AF I 0.00% l AF 2500
2494  % ERR: 0.24% AL 2500: AF  % ERR: 0.24%

l x1 ~ 250  ! 250 0.00% AF l 0.00% l

~Qr7-- ~ I 0 400 0.00% AF I

I AF 25K: 24.94 K % ERR: 0.24% AL 25K: AF K % ERR: 0.24%

I 0.00%

1:0°0 - 1000 [ 0.00% AF  ! 0.00% I AF 250K: 249.4 K % ERR: 0.24% AL 250K: AF K % ERR: 0.24%

f x10 2500 I I

l 2500 I I 0.00% AF I 0.00% ~ Is the As Found Data Within 20% of the Set Point?

I I 4000 f 4000 0.00% AF I

I 0.00% ,---*--------,-- - 7

x10 or I

10K l 10 0.00% AF 1 0.00% i

ijEPR@_IDJ.lGIBltity l I x100 ' 25K I 25 AF
  • )

! 0.00% t 0.00% x.1 or x1 Scale: 250 250 250 I 1 40K f 40 'l 0.00% AF I I 0.00% l x1 or x10 Scale: 2500 2500 2500 1 j .,

'x100 or x1000 100K I 100 0.00% AF lI 0.00%

x10 or x100 Scale: 25 K 25 K 25 K t

250K lI 250 1 0.00% AF 1 0.00%

x100 or x1000 Scale
250 K 250 K 250 K 1 400K 400 I 0.00% AF l 0.00% I

-~ Are the Individual Counts Within 10% of the Average?

~ Is the As Found Data Within 20% of the Set Point? Audio Response: SAT Overload Light: SAT Low Battery (2.2V): SAT Comments: Married as a set with: Model: 43-93 Serial#: PR293983 Bar Code#:

AF: Broken HV/Reset switch - replaced switch.

~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

te Instrument is Due For Next Calibration:

Performed by:.....,,,_........,;A.,<--+---4..£+4------ Reviewed by: ~r7 Issue Date: {(//{ VJ-')

Printed Name:

m~m111moo11 O~

nstrumentation is calibrated in accordance with the OAP to meet the criteria of ANSI N323AB-2013 e results in this report relate only to the item calibrated or tested.

Page 1 of 1

~ PJIA

~llbr.atlon Safety and Ecology Corporation 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 SEC PROCEDURE# sEc-1s-420 Rev 3 iso,m:111;2s:20!1

~.....tr..-t-Cll"tC7"61 Calibration Certificate Calibration Certificate for 43-93,Seria/ # PR293983, Bar Code# ,Property# SEC-7164 Date: 10114122 Date Last Cal. Expires: 06107123 Technician: Jeffrey Knight Reason For Calibration: Married Inst Needed R Temp: 75 F _ ~~Hum: 26 %__ __§~~ ?J~19 in!-i~ CableLength 5 Ft EQUIPMENT USED DURING CALIBRATION MODEL: 2360 SERIAL #: 184947 CAL DUE 10114123 NIST TRACEABLE SOURCES USED SOURCE ISOTOPE ACTIVITY 2rr ASSAY DATE Efficiencies from last calibration 4079-02 Pu-239 28991 dpm 14,695 cpm 113112022 Pu: 21.74  % 4072-02 Tc-99 28299dpm 17,699 cpm 113112022 Tc: 16.77  % 4071-02 Th-230 40296 dpm 20,498 cpm 113112022 Th: 18.95 % 4076-02 Sr-90 9306 dpm 6,529 cpm 113112022 SrY: 34.27 %

AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT AS FOUND DATA Calibration Setpoints AS LEFT DATA after repair, HV adjust or Plateau HV: 650 V Threshold Beta: 4 - 40 mV Alpha: 120 mV HV: 650 V Back Alpha Beta AF 4 rr Efficiences Back Alpha Beta AL 4 rr Efficiencies ground: 1 CPM A-BXTLK 195 CPM ground: 1 CPM 195 CPM A-BXTLK Pu-239: 6415 CPM 516 CPM [ 22~12'1/4 5.00%

Pu-239: 6415 CPM CPM _,2?~,12%_ -3.02%

Tc-99: 1 CPM 5721 CPM [19.53%

(20:38%

Tc-99: 1 CPM 5721 CPM 1"9,;§33/4-,

ch-230: 8215 CPM NIA Th-230: 8215 CPM NIA ~-~°'3-~%,--

SrY-90: NIA 3487 CPM I~s.3_8o/~ SrY-90: 3487 :35:38_% -

NIA CPM

~ Is the As Found Data within 20% of the efficiency from "AF" in the AL Efficiency fields means to refer to the AF the last cal.?

Efficiencies in the AS FOUND DATA Section Reproducibility: Isotope: l Sr-90 l 3470 3436.3 ~ Are the individual counts within 10% of the average?

  • --~- 3412 3427 Average:

jiJ!ieisioi,m~d~\E!(even'.~M~~pair) Js.\¥(lhin,1.0.%ofitierasJ c;alibr~tiorfa~d the:s-A,~ta!k}~ <1~~fi}ie '°f!{XlE!l_ki~ ,<1Q~:thefy.theJteclinici" f;OJ!l_ments. 'Geornetry'ofsource*= flush. to surface~el-Q!!;Ll1roeortronal probes ='1/8" from surface unless*othefW!se. specrfieq,> .-, __ __ ___ _!ll m~

NIA ttieJ'late~u Data_fuid go'.djre.ctlyto~

_ . . ______ . ____ 1 PLATEAU DATA Source 1: Tc-99 Source 2: Th-230 Response (CPM) Response (CPM) Background (CPM) Net A to B High Voltage A ch. B ch. Net Eff. A ch. B ch. Net Eff. A ch. B ch. Xtalk: <10%

NIA I j 1 l l l 1

NIA i I  !

j I  ! i l I NIA I I

l I

I l l i NIA I

' l I I l I NIA l l j '

-I

! 1 I NIA t I I j )

I I 1 1

NIA t' I

~ ~ Ih:lli. ~

2 Pi Efficiencies : I~3-El$:.~,, I I 31,2?;%~ j [ 4.Q:Ci.'V1/4c, j 1* 5_0.'42%

Comments: Married as a set with: Model: 2360 Serial#: 184947 Bar Code#:

~ Does Instrument Meet Final Acceptance Criteria? ~ Calibration Sticker Attached?

Q i:ii?f Date Instrument is Due For Next Calibration: [10/14/?3:,*

  • J Alli;~;,;;~;~ oo Mfu the OAP to mret ::.::.:  :.AN~ 11m~1H1m~1~1m~~~

Issue Date: / rJ/I q/),).,

Page 1 of 2

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