ML23136B287

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Scoping Report 144265-RPT-001, Appendix a - Scoping Survey Calibration Sheets, Rev. a
ML23136B287
Person / Time
Site: 07000398
Issue date: 05/16/2023
From:
US Dept of Commerce, National Institute of Standards & Technology (NIST)
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML23136B277 List:
References
TAC L32643, EPID L-2022-DFA-0010
Download: ML23136B287 (1)
v • d • e


Text

NIST Scoping Study Scoping Report: 144265-RPT-001, NIST Scoping Study Report Revision: A Appendix Appendix A Scoping Survey Calibration Sheets

Safety and Ecology Corporation SEC PROCEDURE# ICAL # 67 Rev o 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 0

Calibration Certificate

~~================

Calibration Certificate for MICRO REM,Seria/ # E050A, Bar Code #,Property# SEC-5378 Date: 04/26/22 Date Last Cal. Expires: 12/10/20 Technician:

Jacob Galyon Reason For Calibration:

Due for Calibration EQUIPMENT USED DURING CALIBRATION MODEL MP-2 MODEL 87V MODEL NIST TRACEABLE SOURCES USED SERIAL#: 314 SERIAL#: 18740384 SERIAL#:

SOURCE ISOTOPE 0300-GY KR-4097 Cs-137 Cs-137 CAL DUE: 01/11/23 CAL DUE: 03/01/23 CAL DUE:

ACTIVITY 202.897 Ci 65.94 mCi ASSAY DATE 2/14/2022 2/14/2022 AS FOUND DATA Physical Cond SAT Geotropism:

SAT Bat. Check SAT As Found Speaker Check As Left N/A High Voltage High Voltage Indicated in OK Band OK 5.086

-4.27 OK 5.086

-4.27

+5 Volt Power Supply (4.5 to 5.5V)

-5Volt Power Supply (-3.74 to -5.06 V)

CALIBRATION DATA HVAL 0

Scale Exposure Rate Instrument Reading Percent Error uR/HR

_ {MR/HR) ____ f:-s Fou~ ____

As Left As Found As Left o_.1 _____

5_

{Pulsed= TO)

_5~~--- _

5.25 5.00 5.00 10 (Pulsed = TO) 10

_ _ -~~

0.00 r-

-1 1

15

{Pulsed= TO) 16

________ _!~_

6.67 50

(.05) 52.5 52.5_ -- -~ _ _ ~J~. _ _

1 100 j*

(.1) 100 100 0.00 L---~--

.. --------~--

.? -

150

(.15) 160 160 6.67

-- ----------1---- --------*

10 f

500 (0.5) _ -- ----

500

_:i0~-

0.00 1000 (1.0) 950

_ _ _:1__~~-

-5.00

_____ __,_ 1500 (1.5)_ ----- _ __:1__~00 ________ _,_ 15~0 0.00 5000 (5) 4500 5000 100

-10.00 10000 (10) 9250 10000

-7.50 t 15000 (15) 14000 15000

-6.67 0.00 6.67 5.00 0.00 6.67 0.00 0.00 3.33 0.00 0.00 0.00

+------

-*- -~--

~

1_o_oo ____ J 50000 100000

{50) 47500 47500

-5.00 (100) 100000 100000 0.00

-5.00 0.00 Precision

-15_0_0_0_0_: __

..,c..{_15_0_)---,--

147500 147500 ___ - *--:f57 **-;

~==~-----::::==========

Comments:

Scale X1000 Exposure Rate 100000 (100)

As Found 100000.00 100000:00 100000.00 Mean Value 100000.00 3/4Dev 0.00 0.00 0.00

-1.67

~ D.oes Instrument Meet Final Acceptance Criteria?

Performe~r.-==::f ~ ~

J.,,irr-.

Printed rme: j Jacobklalyon

) D li2I Calibration S~ratlon o,e Date, ~

Reviewed by: ~

Issue Date: tf./}-£/,,-r-;)....

All instru~entation11s calib~ated in aclardance with the QAP to meet the criteria of ANSI N323AB-2013 The results~ this,/eport re1J,e only }o' the item calibrated or tested.

Page 1 of 1

l"JLA calibration 1so11t: ro~s.2~:1

--~~*-**:~:-l!Q Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-407 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Calibration Certific;;,te Calibration Certificate for 44-9,Serial # PR150385, Bar Code #,Property# SEC-5121 Date: 09/28/22 Date Last Cal. Expires: 10/19/22 Technician: Jake Alcorn Cablelength 5 Ft Reason For Calibration: Due for Calibration Temp:

RelHum:

BP:

MODEL: 12 MODEL:

NIST EQUIPMENT USED DURING CALIBRATION SERIAL#: 229284 SERIAL#:

CAL DUE: 09/28/23 CAL DUE:

NIST TRACEABLE SOURCES USED SOURCE ISOTOPE ACTIVITY 2Tl' ASSAY DATE 5746-06 5744-06 Tc-99 Sr-90 31899 dpm 14539 dpm 19,999 cpm 1/31/2022 10,202 cpm 1/31/2022 Geometry=.in contact with surface unless otherwise specified.

PREVIOUS Tc-99 EFFICIENCY: 13.66%

Calibration Voltage:

900V Calibration Threshold:

35mV AS FOUND Instrument Condition:

SAT AS FOUND DATA 1 MINUTE COUNTS (CPM)

AF

Background:

26 Tc-99 Count:

4212 4134 4124 Sr-90 Count:

3294 4 Tl' Efficiencies Tc-99 EFF: [12.9~%

Sr-90 EFF: 12~.48%.

  • 1 AVERAGE 4156.7 AS LEFT Instrument Condition: SAT AS LEFT DATA 1 MINUTE COUNTS (CPM)

AL

Background:

26 Tc-99 Count:

4212 4134 4124 Sr-90 Count:

3294 4 Tr Efficiencies Tc-99 EFF: r2.95% I Sr-90 EFF: j22.48%

AVERAGE 4156.7 "AF" in the AL Efficiency fields means to refer to the AF Efficiencies in the AS FOUND DATA Section

~ Is the AS FOUND efficiency within 20% of efficiency from last calibration?

~ Reproducibility: Are the individual counts within 10% of the average?

~ Does the probe meet final acceptance criteria?

~ Calibration sticker attached?

Comments: Married as a set with:

Model: 12 Serial #: 229284 Bar Code#:

Date Instrument is Due For Next Calib~ation: ~:09/2~/23 Perto,med by,~ ))e;...L7< -

Rovlewed by;,! -'%

Issue Date: /0 *;l,2

  • 2(

Printed Name:

Jake Alcorn 0

All instrumentation is calibrated in accordance with the QAP to meet the criteria of ANSI N323AB-2013 The results in this report relate only to the item calibrated or tested.

Page 1 of 2

l'JIA Callbratlon

~o;ie: 1:-01s.2:::

.. ~1*-,1-*101-1~1 Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-404 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Calibration Certificate Calibration Certificate for 12,Seria/ # 229284, Bar Code#,Property# SEC-6278 Date: 09/28/22 Date Last Cal. Expires:

10/19/22 Technician: Jake Alcorn Reason For Calibration: Due for Calibration Temp RelHum:

BP:

MODEL: 500-2 MODEL:

NIST EQUIPMENT USED DURING CALIBRATION SERIAL#: 190580 SERIAL#:

CAL DUE: 06/08/23 CAL DUE:

AS FOUND DATA Geotropism:

SAT AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT HIGH VOLTAGE AS FOUND HV AS LEFT HV O New Batteries?

Battery Check: SAT Alarm: NIA

(+/-10% tolerance) 500 V:

515 990 1475 515 1000 1480 AS FOUND Mechanical Zero:

0 AS LEFT Mechanical Zero:

0 I

1000 V:

1500 V:

HV Range 400-1500V:.

SAT RATE MEJER AS FOUND THRESHOLD: 33.5mV AS FOUND HV Reading:

900V AS LEFT THRESHOLD:

35mV AS LEFT HV Reading:

900 V

,. DIGITAL SCALER SCALE RATE CPM AS FOUND % ERROR AS LEFT% ERROR 251

% ERR: 0.40%

AL250:

AF 3/4ERR: 0.40%

x.1 or 100 100 0.00%

100 t

0.00%

AF 250:

x1

~-

-- -~---

250 255 2.00%

250 0.00%

AF 2500:,2510

% ERR: 0.40%

AL2500:

AF

% ERR: 0.40%

J

- ~ - --

400 405 1.25%

400 0.00%

x1 or 1000 1000 0.00%

1000 0.00%

I x10 l

2500 2550 2.00%

2500 0.00%

4005 0.12%

4000 0.00%

AF25K: 25.1 K % ERR: 0.40%

AL25K:

AF K % ERR: 0.40%

AF 100K: 100.4 K % ERR: 0.40%

AL 100K:

AF K % ERR: 0.40%

~ Is the As Found Data Within 20% of the Set Point?

-~000 _..L l

~~-

10K 10 0.00%

10 0.00%

-REPRODUCIBILITY x100 ---- - -***----- -

25K 25.5 40K 40.5 x100 or 100K 105 x1000 250K 255 I

I i

400K I

41.0 f

2.00%

25

-r 1.25%

I 40 5.00% r 100-2.00% i 250.

2.50%

_1_

400 0.00%

~

0.00%

0.00%

0.00%

l 0.00%

x.1 or x1 Scale:

x1 or x10 Scale:

x10 or x100 Scale:

x100 or x1000 Scale:

250 2500 25 K 250 K 250 2500 25 K 250 K 250 2500 25 K 250 K

~ Are the Individual Counts Within 10% of the Average?

~ Is the As Found Data Within 20% of the Set Point?

~ Fast/ Slow Response Switch Functions Properly?

Comments: Married as a set with:

Model:

44-9 Audio Response: SAT Push Buttons: SAT Scaler/Digital: SAT Serial#: PR150385 Audio Divide: N/A Lamp:N/A Bar Code#:

.~ Does Instrument Meet Final Acceptance Criteria?

~ Calibration Sticker Attached?

Date lnst,F-.u~nt is Due For Next Calibration:

[09/28/23 * ~V-..

,:::;::~: ~~loom~

Re~ewed "?Ill 1<r--9....,,,--

lme Dare, -~~:u;~;2 All instrumentation is calibrated in accordance with the OAP to meet the criteria of ANSI N323AB-2013 The results in this report relate only to the item calibrated or tested.

Page 1 of 2

L

~

l'JIA Calibration

-:sc11~::r;cn12011

.au....i.r-.1....... 107.1.62 Safety and Ecology Corporation sEc PROCEDURE#

sEc-Is-411 Rev 5 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Calibration Certificate Calibration Certificate for 43-37,Serial # PR042477, Bar Code #,Property# SEC-5027 Date: 10/17/22 Date Last Cal. Expires: 05/05/23 Technician:

Jeffrey Knight Reason For Calibration:

Due for Calibration CableLength EQUIPMENT USED DURING CALIBRATION MODEL: 2360 SERIAL #: ?87589 CAL DUE 10/17/23

---.... ~-~

NIST TRACEABLE SOURCES USED SOURCE ISOTOPE ACTIVITY 2rr ASSAY DATE Efficiencies from last calibration 5747-06 Pu-239 25793 dpm 13,097 cpm 1/31/2022 Pu:

12.10 %

5746-06 Tc-99 31899 dpm 19,999 cpm 1/31/2022 Tc:

17.54 %

5748-06 Th-230 34897 dpm 17,699 cpm 1/31/2022 Th:

7.44 %

5744-06 Sr-90 14539 dpm 10,202 cpm 1/31/2022 SrY:

28.65 %

AS FOUND Instrument Condition:

SAT AS LEFT Instrument Condition: SAT AS FOUND DAT A Calibration Setpoints AS LEFT DATA after repair, HV adjust or Plateau HV:

1750 V Threshold Beta:

4

-- 40 mV Alpha:

120mV Back Alpha Beta AF 4 rr Efficiences ground:

4 CPM 669 CPM A-BXTLK Pu-239:

4278 CPM 1112 CPM 1~~5.7%

Tc-99:

28 CPM 6916 CPM 19_;$_8~

Th-230:

CPM N/A SrY-90:

N/A CPM D Is the As Found Data within 20% of the efficiency from the last cal.?

10.36%

HV: 1700 V

Back Alpha Beta AL 4 rr Efficiencies ground:

2 CPM 533 CPM A-BXTLK Pu-239:

3883 CPM 757 CPM t1s;9,s% _

5.77%

Tc-99:

13 CPM 7511 CPM !,21~fi:a3/4 -

Th-230:

4419 CPM N/A

,1
~6~%

SrY-90:

N/A 4661 CPM

(;~~-~~%~

"AF" in the AL Efficiency fields means to refer to the AF Efficiencies in the AS FOUND DATA Section Reproducibility: Isotope: ~

7468 7383 7330 Average:

7393.7 ~

Are the individual counts within 10% of the average?

j¥ th~-~J'.ounfl_d~fa (eyen af!~r.repair) ts williin'1b_% ofthe: last:cilfi,b,fation.an{lll~ B,l:'. X\\alk is,<1 % a~a thEl_ /\\'B*J,ct~lk is~O%, tl)e_n the t~giniciari in'!Y N/~the:Plilteau D_~fa llod "go-direcyy le;> 1 POIJ1.!!]8iJl~_-_'Geome!ryof'sburce='n91\\jtbsurfas~c~XC8P.!JJ8§_fi'r.9E<irlional_i:>robes=1/B"ffomsur_faceuniesscitherwisesf)edlied.. -

_*: __ "=-- - ~----*--*.

PLATEAU DATA Source 1.:

Sr-90 Response (CPMl High Voltage A ch.

B ch.

Net Eff.

1700 1720 1730 l

I i-------1 I

9 I 4537 9 j 4716 r~ 4967 L

\\

j l

1 I 21.42%

I 28.58%

l 30.11%

' l I

1 I

Source 2:

Pu-239 Response (CPM}

Background (CPMl Net A to B A ch.

B ch. Net Eff.

A ch.

B ch.

Xtalk: <10%

3987 l 141 l 15.44%

5 I

550 I

4.80%

3969 i 882 l 15.36%

7 I

561 1

8.10%

I 4194 ; 2813 / 16.26%

0 l

580 I

54.67%

I l

1 i

t i

I i

I l

I l

~

2 Pi Efficiencies:

~

[.29,6~%,j I ;3~;89.'Vc, I

~

1-. 24~$.~%

1 l

I.

§rX:!m V4o~~so/c, Comments: Married as a set with:

Model: 2360 Serial #: 287589 Bar Code#:

Calibrated with Teflon spacers installed. New plateau to determine HV setting.

~ Does Instrument Meet Final Acceptance Criteria?

~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration:

J:fotWi2.3:;: _ ", ~J All instrumentation is calibrated in accordanc; with the OAP to meet the criteria of ANSI N323AB-2013 lfilrn~mHl~~~~llffl Performed by,,,* ='""""4,.,!,;,:o....,.,__..,L..L.¢."7---1----

~---//?7_

v/;, ff Reviewed by:. _ ___,,,~----~"LL~L-~_lssue Date: /v/lf/})

Printed Name:

Page 1 of 2

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-418 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Oak Ridge, TN 37830 Calibration Certificate Calibration Certificate for 2360,Serial # 287589, Bar Code#,Property# SEC-7426 Date: 10/17/22 Date Last Cal. Expires: 05/05/23 Technician:

Jeffrey Knight Reason For Calibration:

Due for Calibration NIST EQUIPMENT USED DURING CALIBRATION MODEL: 500-2 MODEL:

- ------- ____,.......... _ -----~-

SERIAL#: 153622 SERIAL#:

CAL DUE: 11/16/22 CAL DUE:

AS FOUND DATA Geotropism: SAT Battery Check: SAT AS FOUND HV AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT

~ New Batteries?

HIGH VOLTAGE

(+!- 10% tolerance}

500V:

500 V 1000 V:

980 V 1500 V:

AF HV Setting:

1458 V 1750 V AL HV Setting:

AS FOUND Mechanical Zero:

0 AS LEFTHV WINDOW SETTINGS 513 V 1000 V BT (4 mV +/ *. 4 mV):

1492 V BW (40 mV +/. 4 mV):

1700 V AT (120 mV +/-10 mV):

AS LEFT Mechanical Zero:

0 AS FOUND 4 mV 41 mV 120 mV AS LEFT AF mV 40 mV AF mV H

D1GffAL,'.$CAl.,.ER SCALE RATE CPM AS F,QUND % ERROR AS LEFT% ERROR AF 250:

249

% ERR: 0.40%

AL 250:

AF

% ERR: 0.40%

l x.1 or 100 100

' 0.00%

AF 0.00% I I

I x1 250 250 I 0.00%

AF I 0.00% 1 I

400 400 0.00%

AF f

0.00% '

AF 2500: 2494

% ERR: 0.24%

AL 2500:

AF

% ERR: 0.24%

AF 25K: 24.94 K % ERR: 0.24%

AL 25K:

AF K % ERR: 0.24%

l x1 or 1000 1000 0.00%

AF 0.00%

f I

I x10 I

2500 l

2500 0.00%

AF I 0.00%

f I

j AF 250K: 249.4 K % ERR: 0.24%

AL 250K:

AF K % ERR: 0.24%

~ Is the As Found Data Within 20% of the Set Point?

I 4000 4000 I 0.00%

AF I 0.00%

1

  • x10 or 10K i

10 0.00%

AF 0.00%

r:.:-*-

R.EPRO'lllJCIB.ILITV 1_

I x100 25K I

25 I 0.00%

AF j 0.00%

I 40K 40 0.00%

AF 0.00%

!x100 or l

100K 100 0.00%

AF 0.00%

x1000 250K 250 0.00%

AF 0.00%

400K 400 0.00%

AF 0.00%

~ Is the As Found Data Within 20% of the Set Point?

Comm-ents: Married as a set with:

Model:

43-37

~ Does Instrument Meet Final Acceptance Criteria?

l L

~ -

x.1 or x1 Scale:

250 250 250 x1 or x10 Scale:

2500 2500 2500 x10 or x100 Scale:

25 K 25 K 25 K x100 or x1000 Scale:

250 K 250 K 250 K

~ Are the Individual Counts Within 10% of the Average?

Audio Response:

SAT Overload Light:

SAT Low Battery (2.2V):

SAT Serial #: PR042477 Bar Code#:

~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration:

l1Qh7J23 ;;*. *1 Perlo,med by,;,~-~

Printed Name:~y ight

~L?

l (J,1° /'}-

Reviewed by:_~~=----"-

.lssue Date:

lf*-v }-

All instrumentation is calibrated in accordance with the OAP to meet the criteria of ANSI N323AB-2013 The results in this report relate only to the item calibrated or tested.

_, _ __, __,j Page 1 of 1

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-418 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Oak Ridge, TN 37830 Calibration Certificate ration Certificate for 2360,Serial # 227394, Bar Code #,Property# SEC-6283 Date: 10/20/22 Date Last Cal. Expires: 06/21/23 Technician:

Jeffrey Knight Reason For Calibration:

Other (See Comments)

MODEL: 500-2 MODEL:

NIST EQUIPMENT USED DURING CALIBRATION SERIAL#: 153622 SERIAL#:

CAL DUE: 11/16/22 CAL DUE:

AS FOUND DATA Geotropism: SAT Battery Check: SAT AS FOUND HV AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT

[g] New Batteries?

AS FOUND Mechanical Zero:

0 AS LEFT Mechanical Zero:

0 HIGH VOLTAGE AS LEFTHV

(+/-10% tolerance) 500V:

1000 V:

1500 V:

AF HV Setting:

509 V 995 V 1488 V 1800 V AL HV Setting:

~-~--__..__._ ~----

SCALE RATE CPM AS FOUND % ERROR AS LEFT% ERROR

\\ x.1 or I 100 l

100 0.00%

AF I

0.00%

i x1 t

250 f

250 0.00%

AF 0.00%

400 t

400 0.00%

AF I 0.00%

l x1 or

\\

1000 1000 I 0.00%

AF 0.00%

~(j l 2500 2500 i 0.00%

AF I 0.00%

L 4000 4000 t 0.00%

AF ! 0.00%

I

. x10 or I 10K l

10 I 0.00%

AF 0.00%

I x100 !

25K i

25 0.00%

AF I

0.00%

j 40K l

40 r 0.00%

AF 0.00%

I x100 or.!

100K I

100 f 0.00%

AF 0.00%

j x1000 j 250K 250

' 0.00%

AF 0.00%

I 1

I l

400K I

400 0.00%

AF 0.00%

i I

t I

~ Is the As Found Data Within 20% of the Set Point?

Comments: Married as a set with:

Model:

43-37 Calibrated for new customer.

~ Does Instrument Meet Final Acceptance Criteria?

WINDOW SETTINGS AS FOUND AS LEFT AF V 3.4 mV 4

BT (4 mV +/-.4 mV):

mV AF V AF V BW (40 mV +/- 4 mV):

40 mV AF mV 1800 V AT (120 mV +/- 1.0 mV):

120 mV AF mV p

DIGITAL $_()ALER

~-~

AF 250:

249

% ERR: 0.40%

AL 250:

AF

% ERR: 0.40%

AF 2500: 2494

% ERR: 0.24%

AL 2500:

AF

% ERR: 0.24%

AF 25K: 24.95 K % ERR: 0;20%

AL 25K:

AF K % ERR: 0.20%

f AF 250K: 249.9 K % ERR: 0.04%

AL 250K:

AF K % ERR: 0.04%

~ Is the As Found Data Within 20% of the Set Point?

,....-**~-.

~

  • ~

r.,.-<

,-*,.--,-,-~-,--* 1

' i l

j REPRODUGIBllllFf..

..~ ~,

x.1 or x1 Scale:

250 250 250 x1 or x10 Scale:

2500 2500 2500 x10 or x100 Scale:

25 K 25 K 25 K x100 or x1000 Scale:

250 K 250 K 250 K

~ Are the Individual Counts Within 10% of the Average?

Audio Response:

SAT Overload Light:

SAT Low Battery (2.2V):

SAT Serial#: PR037449 Bar Code#:

.~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration:

lf9l20,f23-'

/~

,/P'.d':// L.,_..-//

Performed by: td:/,{_,I :I/((}

Reviewed by: ~ / Issue Date: f O/}--f/).,:;L Printed Name:

'.faf y K~t All instrumentati n is calibrated in accordance with the QAP to meet the criteria of ANSI N323AB-2013

)

The results in this report relate only to the item calibrated or tested.

0 Page 1 of 1

~

Safety and Ecology Corporation sEc PROCEDURE#

sEc-Is-411 Revs PJIA C..llbr.1lltJn ISO/lfCl702S:20:1

.:l~<lit.n~11*:C7462 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Calibration Certificate Calibration Certificate for 43-37,Seria/ # PR037449, Bar Cod~#,Property# SEC-5030 Date: 10/20/22 Date Last Cal. Expires: 06/21/23 Technician:

Jeffrey Knight Reason For Calibration:

Other (See Comments CableLength EQUIPMENT USED DURING CALIBRATION MODEL: 2360 SERIAL#: 227394 CAL DUE 10/20/23 NIST TRACEABLE SOURCES USED SOURCE ISOTOPE ACTIVITY 2TT ASSAY DATE Efficiencies from last calibration 5747-06 Pu-239 25793 dpm 13,097 cpm 1/31/2022 Pu:

13.90 %

5746-06 Tc-99 31899 dpm 19,999 cpm 1/31/2022 Tc:

15.96 5744-06 Sr-90 14539 dpm 10,202 cpm 1/31/2022 Th:

11.82 %

5748-06 Th-230 34897 dpm 17,699 cpm 1/31/2022 AK-2579 C-14 23986 dpm 1/31/2022 SrY:

27.61 AS FOUND Instrument Condition:

SAT AS LEFT Instrument Condition: SAT AS FOUND DATA Calibration Set1;1oints AS LEFT DATA after re1;1air, HV adjust or Plateau HV:

1800 V Threshold Beta:

4

- 40 mV Alpha:

120 mV HV: 1725 V

Al1;1ha Beta AF 4 TT Efficiences Beta Back ground:

20 CPM 712 CPM A-B XTLK Back Al1;1ha AL 4 TT Efficiencies 3

CPM 582 CPM A-BXTLK cs239'.

4478 CPM 1145 CPM ffT,.28%

c-99.

307 CPM 5376 CPM -t 1~.62%

Th-230:

CPM N/A r. -,

SrY-90:

N/A CPM l 0 Is the As Found Data within 20% of the efficiency from the last cal.?

9.71%

ground:

Pu-239:

3560 CPM 868 CPM r-1~:1~%

8.04%

Tc-99:

17 CPM 7117 CPM 120:4~%.*

Th-230:

3694 CPM N/A l'.,10:~a%~

SrY-90:

N/A 4836 CPM r 2~:;2'fi3/4 '.

"AF" in the AL Efficiency fields means to refer to the AF Efficiencies in the AS FOUND DATA Section Reproducibility: Isotope: I Sr-90 j 5026 4926 4931 Average:

4961.0 ~ Are the individual counts within 10% of the average?

.,.. -*.--.*.---~*,....,-,----i- -*;r.-----~.---- _,,..;. ~--.....---.----,---.,_. __ ---~---------~--- ~.,-,.,-._... ~-----,---.--~----*-~ -~~.----~-,-.--.-...,-----1r *,*- *...,.

lfJl_l; ~

  • Ffi,L!nd da\\;I {O:,V!'O,after'riepa~),is,wi!hin '10% oflhe lafl calibr":l\\<if\\~ng ti)~ B:AXtalk )5, :<1% anq tll;.:J'i:B X\\a!,k is:<1 o;yc. 11J~n tl)e techniciaifmay N/A:.tha Pl~teau Data.and go \\tife9t1y. to j

£omments., 'Geo_l!J:el!)'. of source =*flush to sur:face; except gas_eroport1onal probes= 1/8"-from surface*unless*othe1W1se*s~ _

~

. -~-

PLATEAU DATA Source 1: Sr-90 Res1;1onse (CPMl High Voltage A ch.

B ch.

Net Eff.

1700 7

4442 j 26.76%

1725

.1 ;

5 4931 I 29.44%

1150 I I 33 5163 I 30.15%

I I I

j I

I I

Source 2:

Pu-239 Res1;1onse (CPMl A ch.

B ch. Net Eff.

3548 i 796 I 13.74%

3414 946 j 13.22%

3717 1070 f 14.40%

2 Pi Efficiencies:

~

[:;!tAs%*1 Background (CPMl Ach.

B ch.

5 I

552 i

i 3

650

' I I 3

692 I

i I

I

~

l a:2re~o/c{j Net A to B Xtalk: <10%

6.89%

8.68%

10.18%

~

I,,20:as$: j t

§rY:fil!

I '4f ;193/4,I Comments: Married as a set with:

Model: 2360 Serial #: 227394 Bar Code#:

AF: High background - new plateau to verify HV setting. Calibrated with Teflon spacers installed. C-14 source #AK-2579: 3164 gcpm/23,986 dpm = 10.76% efficiency.

0

~ Does Instrument Meet Final Acceptance Criteria?

~ Calibration Sticker Attached?

Porio,mod by, ;/J ¢-

Printed Name:

~:~1gh Reviewed by: ~

Issue Date: i(J/Jrf/}J-Page 1 of 2

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-418 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Oak Ridge, TN 37830 Calibration Certificate CJibration Certificate for 2360,Serial # 227402, Bar Code#,Property# SEC-6214 Date: 09/20/22 Date Last Cal. Expires: 09/20/23 Technician:

Noah Kaye Reason For Calibration:

Due for Calibration MODEL: 500-2 MODEL:

NIST EQUIPMENT USED DURING CALIBRATION SERIAL#: 171700

  • SERIAL#:

CAL DUE: 06/07/23 CAL DUE:

AS FOUND DATA Geotropism: SAT Battery Check: SAT AS FOUND HV AS FOUND Instrument Condition: SAT AS LEFT Instrument Condition: SAT

[] New Batteries?

AS FOUND Mechanical Zero:

0 AS LEFT Mechanical Zero:

0 HIGH VOLTAGE AS LEFT HV

(+/- 10% tolerance) 500V:

1000 V:

1500 V:

AF HV Setting:

511 V 1009 V 1508 V 680 V AL HV Setting:

RATE*METER

~---

t ----

SCALE RATE CPM AS FOUND % ERROR AS LEFT% ERROR x.1 or 100 100 0.00%

AF 0.00%

x1 250 250 0.00%

AF 0.00%

400 400 0.00%

AF 0.00%

x1 or 1000 1000 0.00%

AF 0.00%

AF V AF V AF V 675 V

.... *-.. -~_... ___

AF 250:

AF 2500:

AF 25K:

AF 250K:

'L WINDOW SETTINGS AS FOUND AS LEFT BT (4 mV +/-.4 mV):

4 mV AF mV BW (40 mV +/- 4 mV):

30 mV AF mV AT (120 mV +/-10 mV):

121 mV AF mV

_.,.i.._ ___....;:.:,..... Pl~ITA~ SCALER

. --~ -v ----

---*L.-

250

% ERR: 0.00%

AL250:

AF

% ERR: 0.00%

2514

% ERR: 0.56%

AL 2500:

AF

% ERR: 0.56%

24.9K % ERR: 0.40%

AL25K:

AFK % ERR: 0.40%

249K % ERR: 0.40%

AL 250K:

AF K %ERR: 0.40%

a 10 2500 2500 0.00%

AF 0.00%

~ Is the As Found Data Within 20% of the Set Point?

4000 4000 x10 or 10K I

10 x100 25K I

25 40K 40 x100 or 100K 100 x1000 250K 250 400K 400 0.00%

AF 0.00%

I 0.00%

AF 0.00%

0.00%

AF 0.00%

0.00%

AF 0.00%

0.00%

AF 0.00%

0.00%

AF 0.00%

0.00%

AF 0.00%

REP'RQDUCIBILITY

'*_,,,._...., "_;,. --~_.,... __,.._....

x.1 or x1 Scale:

x1 or x10 Scale:

x1 O or x100 Scale:

x100 or x1000 Scale:

250 2500 25 K 250 K 250 2500 25 K 250 K 250 2500 25K 250K

~ Are the Individual Counts Within 10% of the Average?

~ Is the As Found Data Within 20% of the Set Point?

Audio Response:

SAT Overload Light: rSAT Low Battery (2.2V):

SAT Comments: Married as a set with:

Model:

43-93 Serial #: PR394086 Bar Code#:

~ Does Instrument Meet Final Acceptance Criteria?

~ Calibration Sticker Attached?

Performed by: U Printed Name:

Noah Kaye Date Instrument is Due For Next Calibration:

[Q9/20/?~.. *~:! I

~z Reviewed bye ~ff Js,ue Dalee q/Jf /J-')---

liillOOIMIIJHm All instrumentation is calibrated in accordance with the QAP to meet the criteria of-ANSI N323AB-2013 The results in this report relate only to the item calibrated or tested.

0 Page 1 of 1

Safety and Ecology Corporation SEC PROCEDURE#

SEC-IS-420 Rev 3 l'JLA 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 C,

C*llb,alion C l"b C rt*,&,*

t Q

0 0 ""'*"

a 1 ration e wca e Calibration Certificate for 43-93,Serial # PR394086, Bar Code #,Property# PFL-354 Date: 09/20/22 Date Last Cal. Expires: 03/30/23 Technician:

Noah Kaye Reason For Calibration:

Due for Calibration Temp:

RelHum:

BP:

CableLength 5 Ft EQUIPMENT USED DURING CALIBRATION MODEL: 2360 SERIAL#: 227402 CAL DUE 09/20/23 ft..:.*

.,. 1-*

\\,, \\

NIST TRACEABLE SOURCEs*i:JsED SOURCE ISOTOPE ACTIVITY 2TT ASSAY DATE t..'t

  • \\::>\\f' Efficiencies from last calibration 4079-02 Pu-239 28991 dpm 14,695 cpm 1/31/2022 Pu:

23.40 %

4072-02 Tc;99 28299 dpm 17,699 cpm 1/31/2022 Tc:

17.24 %

4071-02 Th-230 40296 dpm 20,498 cpm 1/31/2022 Th:

21.63 %

4076-02 ISr-90 9306 dpm 6,529 cpm 1/31/2022 SrY:

35.20 %

AS FOUND Instrument Condition:

SAT AS LEFT Instrument Condition: SAT AS FOUND DAT A Calibration Setpoints AS LEFT DATA after repair, HV adjust or Plateau HV:

675 V Threshold Beta:

4 40 mV Alpha:

120mV HV: 675 V

Alpha Beta AF 4 TT Efficiences Beta AL 4 TT Efficiencies Back ground:

2 CPM 143 Back Alpha A-B XTLK CPM 2

CPM 143 CPM

~~~

A-B XTLK Pu-239:

6709 CPM 556 CPM i3,1~%-

Tc-99:

3 CPM 5450

~

Th-230:

8505 CPM NIA SrY-90:

N/A 3435 CPM 1_1p~_o/o; 21.fQ"lr/

CPM "35J!J%*

~ Is the As Found Data within 20% of the efficiency from the last cal.?

6.16%

ground:

Pu-239:

6809 CPM 556 CPM

'23JIJ,%

6.07%

Tc-99:

3 CPM 5450 cPM 1'ads%'

Th-230:

8505 CPM NIA 21do%

SrY-90:

NIA 3435 CPM

. '3'5:3~'1/6.

"AF" in the AL Efficiency fields means to refer to the AF Efficiencies in the AS FOUND DATA Section Reproducibility: Isotope: I Sr-90 I 3555 3515 3532 Average:

3534.0 ~ Are the individual counts within 10% of the average?

"itu,e ~ Found ~ata ( even~~fter rep~ir) is williin 10% of llieiait calititation and ihe B'.A Xtaik.i!i <1 % ~rid the A::s xialk is :;,10%:* iiieq the fech~iclan inay N[ A ihe'Piateau o;ta and go directly to

£9nifii_~2t~:~Ge£_inetiyo(,;_c,_~rce = fllish"\\o _s.ilrf§~,~x~pt 9!!~prcjpprtjopal pr!]bes=Jf.8"fr.9m:s.'Jrf~~ aJirii_stetii!'~e,_sj)Jgifi~i:!:_:' Jc, ____ - - --

PLATEAU DATA Source 1:

Tc-99 Response (CPM)

/I High Voltage A ch.

B ch.

Net Eff.

N/A Source 2:

Th-230 Response (CPM)

Background {CPM)

Net A to B A ch.

B ch. Net Eff.

A ch.

B ch.

Xtalk: <10%

I N/A I

N/A N/A N/A N/A I

N/A

~ ~

./

2 Pi Efficiencies:

F4~;~?%J b~s~~s~J Comm.e"nts: Married as a set with:

~.c.

Model: 2360 Serial#: 227402 Bar Code#:

~ Does Instrument MeetFinal Acceptance Criteria?

~ Calibration Sticker Attached?

Date Instrument is Due For Next Calibration:

lo~12Qfg~ :.,-~-.. J 8 All instrumentation is calibrated in accordance with the OAP to meet the criteria of ANSI N323AB-2013 Perto,med by,~~,6:z Reviewed by, ~

Printed Name:

Noah Kaye Issue Date:

Page 1 of 2

Safety and Ecology Corporation SEC PROCEDURE# SEC-IS-418 Rev 3 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Oak Ridge, TN 37830 Calibration Certificate Calibration Certificate for 2360,Serial # 184947, Bar Code #,Property # SEC-5549 Date: 10/14/22 Date Last Cal. Expires: 06/07/23 Technician:

Jeffrey Knight Reason For Calibration:

Repair NIST EQUIPMENT USED DURING CALIBRATION MODEL: 500-2 MODEL:

SERIAL#: 153622 SERIAL#:

CAL DUE: 11/16/22 CAL DUE:

AS FOUND DATA Geotropism: SAT AS FOUND Instrument Condition: UNSAT AS LEFT Instrument Condition: SAT Q] New Batteries?

HIGH VOLTAGE

{+/- 10% tolerance}

Battery Check: SAT AS FOUND HV 500 V:

1000 V:

1500 V:

AF HV Setting:

496 V 984 V 1473 V 650 V AL HV Setting:

AS FOUND Mechanical Zero:

0 AS LEFTHV WINDOW SETTINGS 502 V 1000 V BT (4 mV +/-.4 mV):

1489 V BW (40 mV +/- 4 mV):

650 V AT (120 mV +/-10 mV):

AS LEFT Mechanical Zero:

0 AS FOUND AS LEFT 3.1 mV 4 mV 28 mV 40 mV 120 mV 123 mV

.___._~-*........

~te MET~R,

. H~: ~----*o_*

.1~G_t1~:*,A~.L~.s_:e_* A_L_E_R_:. ___ _

SCALE RATE CPM AS FOUND % ERROR AS LEFT% ERROR

x.1 or L 100 1

100

' 0.00%

AF l

0.00%

I I

l x1

~

250 250 0.00%

AF l 0.00%

~Qr7-- 1:

0 0°0 - ~

400 I 0.00%

AF I

0.00%

I 1000

[

0.00%

AF

! 0.00%

f x10 l

2500 I

2500 I

0.00%

AF I

0.00%

I I

I I

I 4000 f

4000 0.00%

AF I

0.00%

x10 or I

10K l

10 0.00%

AF 1 0.00%

I x100 '

25K I

25

! 0.00%

AF

  • )

0.00%

t 1

40K 40

' 0.00%

AF I

0.00%

I f

l I

'x100 or 1 100K I

100 j

0.00%

AF l 0.00%

x1000 250K l

250 1 0.00%

AF I

0.00%

1 t

I 0.00%

1 400K 400 I

0.00%

AF l

~ Is the As Found Data Within 20% of the Set Point?

Comments: Married as a set with:

Model:

43-93 AF: Broken HV/Reset switch - replaced switch.

~ Does Instrument Meet Final Acceptance Criteria?

l l

I I

l I

AF 250:

250

% ERR: p.00%

AL250:

AF

% ERR: 0.00%

AF 2500: 2494

% ERR: 0.24%

AL 2500:

AF

% ERR: 0.24%

AF 25K: 24.94 K % ERR: 0.24%

AL 25K:

AF K % ERR: 0.24%

AF 250K: 249.4 K % ERR: 0.24%

AL 250K:

AF K % ERR: 0.24%

~ Is the As Found Data Within 20% of the Set Point?

-;ijEPR@_IDJ.lGIBltity 7 l i,_ ____ ------*.

x.1 or x1 Scale:

250 250 250 x1 or x10 Scale:

2500 2500 2500 x10 or x100 Scale:

25 K 25 K 25 K x100 or x1000 Scale:

250 K 250 K 250 K

-~ Are the Individual Counts Within 10% of the Average?

Audio Response:

SAT Overload Light:

SAT Low Battery (2.2V):

SAT Serial#: PR293983 Bar Code#:

~ Calibration Sticker Attached?

te Instrument is Due For Next Calibration:

Performed by:.....,,,_........,;A.,<--+---4..£+4------

Reviewed by: ~r7 Issue Date: {(//{ VJ-')

Printed Name:

O nstrumentation is calibrated in accordance with the OAP to meet the criteria of ANSI N323AB-2013

~ e results in this report relate only to the item calibrated or tested.

m~m111moo11 Page 1 of 1

~

Safety and Ecology Corporation SEC PROCEDURE#

sEc-1s-420 Rev 3 PJIA

~llbr.atlon iso,m:111;2s:20!1

~.....tr..-t-Cll"tC7"61 10512 Lexington Drive, Suite 200, Knoxville, TN 37932 Calibration Certificate Calibration Certificate for 43-93,Seria/ # PR293983, Bar Code#,Property# SEC-7164 Date: 10114122 Date Last Cal. Expires: 06107123 Technician:

Jeffrey Knight Reason For Calibration:

Married Inst Needed R Temp: 75 F _ ~~Hum: 26 % __ __§~~ ?J~19 in!-i~

EQUIPMENT USED DURING CALIBRATION CableLength 5 Ft MODEL: 2360 SERIAL #: 184947 CAL DUE 10114123 NIST TRACEABLE SOURCES USED SOURCE Efficiencies from last calibration 4079-02 Pu:

21.74 %

4072-02 Tc:

16.77 4071-02 Th:

18.95 %

4076-02 SrY:

34.27 %

ISOTOPE Pu-239 Tc-99 Th-230 Sr-90 AS FOUND Instrument Condition:

SAT AS FOUND DATA Calibration Setpoints HV:

650 V Threshold Beta:

4

- 40 mV Alpha:

120 mV Alpha Beta AF 4 rr Efficiences Back A-BXTLK ground:

1 CPM 195 CPM Pu-239:

6415 CPM 516 CPM

[ 22~12'1/4

[19.53%

Tc-99:

1 CPM 5721 CPM ch-230:

(20:38%

8215 CPM NIA I ~s.3_8o/~

SrY-90:

NIA 3487 CPM

~ Is the As Found Data within 20% of the efficiency from the last cal.?

5.00%

Back ground:

Pu-239:

Tc-99:

Th-230:

SrY-90:

ACTIVITY 28991 dpm 28299dpm 40296 dpm 9306 dpm 2rr 14,695 cpm 17,699 cpm 20,498 cpm 6,529 cpm ASSAY DATE 113112022 113112022 113112022 113112022 AS LEFT Instrument Condition: SAT AS LEFT DATA after repair, HV adjust or Plateau HV: 650 V

Alpha Beta AL 4 rr Efficiencies 1

CPM 195 CPM A-BXTLK 6415 CPM CPM

_,2?~,12%_

-3.02%

1 CPM 5721 CPM 1"9,;§33/4-,

8215 CPM NIA

~-~°'3-~%,--

NIA 3487 CPM

35:38_% -

"AF" in the AL Efficiency fields means to refer to the AF Efficiencies in the AS FOUND DATA Section Reproducibility: Isotope: l Sr-90 l 3470 3412 3427 Average:

3436.3 ~ Are the individual counts within 10% of the average?

  • --~-

jiJ!ieisioi,m~d~\\E!(even'.~M~~pair) Js.\\¥(lhin,1.0.%ofitierasJ c;alibr~tiorfa~d the :s-A,~ta!k}~ <1~~fi}ie '°f!{XlE!l_ki~,<1Q~:thefy.theJteclinici"!ll m~ NIA ttieJ'late~u Data_fuid go'.djre.ctlyto~

f;OJ!l_ments. 'Geornetry'ofsource*= flush. to surface~el-Q!!;Ll1roeortronal probes ='1/8" from surface unless*othefW!se. specrfieq,>

______. ____ 1 PLATEAU DATA Source 1: Tc-99 Source 2:

Th-230 Response (CPM)

Response (CPM)

Background (CPM)

Net A to B High Voltage A ch.

B ch.

Net Eff.

A ch.

B ch. Net Eff.

A ch.

B ch.

Xtalk: <10%

NIA I

j 1

l I

I I

j l

I l

I l

' l j

I I

j 2 Pi Efficiencies:

Comments: Married as a set with:

Model: 2360 l

i I I I

)

~

I ~3-El$:.~,, I Serial#: 184947 l

1 :

l I

l i

l I

1

-I I I

1 1

~

I 31,2?;%~ j NIA i

NIA I

NIA I

NIA l

NIA t

NIA t'

I Ih:lli.

[ 4.Q:Ci.'V1/4c, j Bar Code#:

~

1* 5_0.'42%

~ Does Instrument Meet Final Acceptance Criteria?

~ Calibration Sticker Attached?

Q Date Instrument is Due For Next Calibration:

[10/14/?3:,*

  • J Alli;~;,;;~;~ i:ii?f oo Mfu the OAP to mret ::.::.: :.AN~

11m~1H1m~1~1m~~~

Issue Date:

/ rJ /I q/),).,

Page 1 of 2

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