Text

Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey Conducted in 2014, Rev. 0, Appendix F, Part 3 of 8
	ML16293A890
Person / Time
Site:	West Valley Demonstration Project, P00M-032
Issue date:	08/22/2016
From:	; MJW Technical Services
To:	; Office of Nuclear Material Safety and Safeguards, State of NY, Energy Research & Development Authority, Office of Nuclear Reactor Regulation
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ML16293A155	List: ML16293A130; ML16293A131; ML16293A132; ML16293A133; ML16293A134; ML16293A135; ML16293A136; ML16293A137; ML16293A139; ML16293A140; ML16293A141; ML16293A142; ML16293A143; ML16293A178; ML16293A179; ML16293A180; ML16293A181; ML16293A182; ML16293A183; ML16293A184; ML16293A185; ML16293A186; ML16293A187; ML16293A278; ML16293A279; ML16293A281; ML16293A282; ML16293A364; ML16293A365; ML16293A366; ML16293A367; ML16293A368; ML16293A389; ML16293A391; ML16293A392; ML16293A393; ML16293A394; ML16293A674; ML16293A675; ML16293A676; ML16293A677; ML16293A678; ML16293A808; ML16293A809; ML16293A810; ML16293A811; ML16293A812; ML16293A843; ML16293A844; ML16293A846; ... further results
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Analytical Results by Area (Area 3)

3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.1 3.1.1.E.2 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP SAMPLE

- Analy;;ed 12/3/2015 12/1/2015 385077 385077 12/3/2015 385077 12/1 /2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077

Parameter Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Antimony-125 Antimony-125 Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40' Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Area3 Fraction Methpd.*.*

R DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R 18.4 0.0105 27.7 0.00 1.04 1.23

-6.76E-05 0.0303 1.40 1.34 14.7 0.634 0.00 1.04 1.09 0.394 0.129 0.00 0.235 0.158 0.00 0.00 1.32 1.34 1.34 0.00585 0.00585

-0.0868

-0.0868 1.26 1.50 16.4 0.00 0.00 1.32 1.32 1.79 1.79 0.367 0.00 0.00 0.0383

- - Uncertainty* GAS" 0.336 14952-40-0 2.52 12587-46-1 0.129 1.76 0.865 0.188 0.144 0.0362 0.155 0.146 0.213 1.64 0.821 0.821 0.188 0.445 0.0939 0.133 0.133 0.298 0.127 0.127 0.810 0.174*

0.124 0.124 0.0524 0.0524 0.139 0.139 0.146 0.221 1.68 0.716 0.716 0.174 0.174 0.335 0.335 0.0904 0.137 0.137 0.392 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14234-35-6 14234-35-6 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14952-40-0

. UnitS PCl/G PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G U

PCl/G U

PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

MDL" 1.00 0.603 2.56 0.235 4.00 1.00 1.72 10.0 1.40 0.147 0.0838 0.100 0.0732 0.304 0.126 0.401 0.880 1.00 1.00 0.147 0.353 0.0724 0.150 0.150 0.586 0.255 0.255 1.41 0.161 0.0758 0.100 0.0758 0.100 0.0881 0.0881 0.235 0.235 0.135 0.146 0.768 0.978 0.978 0.161 0.161 0.277 0.277 0.0713 0.155 0.155 0.707 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5' 20.5 20.5 20.5 20.5 19.4 19.4 19.4 20.5 19.4 20.5 19.4 20.5 19.4 19.4 19.4 19.4 20.5 19.4 20.5 19.4 20.5 19.4 19.4 20.5 19.4 19.4

Sample No. Type Analyzed SDG 3.1.1.E.2 SAMPLE 12/1/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/1/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE*

12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.2 SAMPLE 12/3/2015 385077 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 1/11/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 1/11/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 1/16/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 1/15/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 Parameter ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Americium-241 Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 Europium-154 lodine-129 Lead-212 Lead-212 Lead-214 Lead-214 Area 3 Fraction Method R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE PIASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 13.2

-0.00441 25.7 0.00 1.02 1.94

-0.00321 0.0969 1.44 1.33 17.0 0.00 0.00 1.02 1.18 0.327

-0.00367 0.00701

-0.115 16.3 0.0335

-0.0128 0.0664 23.2 1.32 0.00 0.838 0.754

-0.823 2.12 2.18 0.0125

-0.0565 0.0187 0.0169 0.0304 0.0934

-0.236 0.0709 1.21 1.15 1.05 1.09 Uncertainty GAS Units Lab Qu MDL CRDL Dilution % MoistL 2.26 12587-46-1 PCl/G 2.59 4.00 1.00 19.4 0.158 1.68 0.869 0.241 0.184 0.0508 0.174 0.173 0.230 1.85 1.10 1.10 0.241 0.327 0.0934 0.221 0.251 0.378 2.11 0.0532 0.102 0.138 1.54 0.844 0.995 0.139 0.200 0.792 0.137 0.173 0.0307 0.0527 0.0525 0.0465 0.0521 0.139 0.158 0.139 0.113 0.189 0.168 0.265 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G U

0.291 1.00 19.4 PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G U

1.68 10.0 1.67 0.229 0.0985 0.100 0.0977 0.339 0.153 0.436 0.829 1.28

. 1.28 0.229 0.288 0.108 0.260 0.463 0.645 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 20.6 14952-40-0 14952-40-0 12587-46-1 14596-10-2 14234-35-6 14234-35-6 12587-47-2 PCl/G 1.97 4.00 1.00 19.4 PCl/G PCl/G U

PCl/G U

PCl/G 14913-49-6 PCl/G 14913-49-6 PCl/G UI 14733-03-0 PCl/G 14733-03-0 PCl/G 14762-75-5 PCl/G U

10045-97-3 PCl/G 10045-97-3 PCl/G 10198-40-0 PCl/G U

10198-40-0 PCl/G U

OER-100-93 PCl/G PCl/G U

PCl/G 15585-10-1 PCl/G U

15585-10-1 PCl/G U

15046-84-1 PCl/G U

15092-94-1 PCl/G 15092-94-1 PCl/G 15067-28-4 PCl/G 15067-28-4 PCl/G 0.0736 1.00 0.184 0.266 1.57 10.0 1.00 19.4 1.00 19.4 1.00 20.6 1.00 19.4

0. 726 1.00 19.4 1.46 1.00 20.6 0.124 1.00 19.4 0.191 1.00 20.6 1.38 2.00 1.00 19.4 0.0659 0.100 1.00 19.4 0.0805 0.100 1.00 20.6 0.061 1.00 19.4 0.0595 1.00 20.6 0.056 1.00 1.00 19.4 0.0807 1.00 1.00 19.4 0.0456 1.00 1.00 19.4 0.219 1.00 19.4 0.235 1.00 20.6 0.522 1.00 1.00 19.4 0.104 1.00 19.4 0.165 1.00 20.6 0.126 1.00 19.4 0.181 1.00 20.6

Sample No. Type Analyzed SDG 3.1.1.E.3 SAMPLE 1 /12/2016 388092 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1. 1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 3.1.1.E.3 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 1 /12/2016 388092 1 /12/2016 388092 1 /14/2016 388092 12/29/2015 388092 1 /18/2016 388092 12/29/2015 388092 1 /18/2016 388092 12/29/2015 388092 1/18/2016 388092 12/29/2015 388092 1/18/2016 388092 1 /7/2016 388092 1/19/2016 388092 12/29/2015 388092 1 /18/2016 388092 1/12/2016 388092 1 /12/2016 388092 1/12/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.3 SAMPLE 12/29/2015 388092 3.1.1.E.3 SAMPLE 1/18/2016 388092 3.1.1.E.3 SAMPLE 1/10/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.3 SAMPLE 1/12/2016 388092 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/1/2015 385077 3.1.1.E.4 SAMPLE 12/1/2015 385077 3.1.1.E.4 SAMPLE 1/13/2016 389094 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/1/2015 385077 3.1.1.E.4 SAMPLE 12/1/2015 385077 3.1.1.E.4 SAMPLE 1/13/2016 389094 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 3.1.1.E.4 3.1.1.E.4 SAMPLE 12/3/2015 385077 SAMPLE 12/3/2015 385077 SAMPLE 12/3/2015 385077 Parameter Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tin-126 Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Actinium-227 Actinium-227 ALPHA ALPHA ALPHA

'Antimony-125 Antimony-125 BETA BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Area 3, Fraction Method.

R ASTM C 1476-00 Modified R

DOE EML HASL-300, Pu-11-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Th-01-RC Modified R

R R

R DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 9310/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R

Result 0.126 0.000662

-0.0112

-10.2 14.1 14.5 0.00 0.0605 0.838 0.754 1.07 1.12

-0.219

-0.644 0.429 0.409 0.728

-0.0165 1.20 1.01 0.00 0.00

-1.11

-0.0254 0.906 0.0732 0.779 0.356 0.00 47.8 47.8 14.5 0.0916 0.0916 32.0 32.0 21.6 0.00 1.11 0.315 0.315 0.0439 0.00 Uncertainty CAS Units Lab.Qu MDL CRDL C Dilution % MoistL 0.248 13994-20-2 PCl/G 0.343 1.00 1.00 19.4 0.049 0.0508 7.00

1. 19 1.75 0.806 0.657 0.139 0.200 0.264 0.346 0.842 1.56 0.0742 0.0963 0.509 0.142 0.587 0.537 0.155 0.150 2.39 0.0409 0.238 0.081 0.217 0.453 0.453 3.52 3.52 3.59 0.116 0.116 2.01 2.01 2.76 0.808 0.194 0.0979 0.0979 0.0449 0.0449 13981-16-3 OER-100-70 14119-32-5 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 10098-97-2 14133-76-7 14913-50-9 14913-50-9 14274-82-9 15594-54-4 14269-63-7 PCl/G U

0.109 PCl/G U

0.128 PCl/G U

12.6 PCl/G 0.438 PCl/G 0.834 PCl/G UI 0.802 PCl/G U

1.24 PCl/G 0.124 PCl/G 0.191 PCl/G 0.215 PCl/G 0.285 PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G 1.66 2.77 0.0595 0.0824 0.507 0.329 0.379 1.00 1.00 19.4 1.00 1.00 19.4 15.0 1.00 19.4 1.00 19.4 1.00 20.6 1.00 19.4 1.00 20.6 1.00 19.4 1.00 20.6 1.00 19.4 1.00 20.6 2.00 1.00 19.4 5.00 1.00 20.6 1.00 20.6 1.00 20.6 1.00 1.00 20.6 1.00 1.00 20.6 1.00 1.00 20.6 7440-29-1 PCl/G 0.327 1.00 1.00 20.6 PCl/G U

PCl/G UI 10028-17-8 PCl/G U

14158-29-3 PCl/G U

13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 14952-40-0 14952-40-0 12587-46-1 12587-46-1 12587-46-1 14234-35-6 14234-35-6 12587-47-2 12587-47-2 12587-47-2 14913-49-6 PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI 14733-03-0 PCl/G 10045-97-3 PCl/G 10045-97-3 10198-40-0 10198-40-0 PCl/G PCl/G U

PCl/G UI 0.147 1.00 20.6 0.239 1.00 20.6 4.23 6.00 1.00 20.6 0.130 1.00 1.00 20.6 0.132 1.00 1.00 20.6 0.107 1.00 1.00 20.6 0.0928 1.00 1.00 20.6 0.675 1.00 20.6 0.675 1.00

19. 7 2.23 4.00 1.00 20.6 2.23 4.00 1.00

19. 7 3.92 4.00 1.00

19. 7 0.236 1.00 20.6 0.236 1.00

19. 7 2.14 10.0 1.00 20.6 2.14 10.0 1.00 19.7 2.85 10.0 1.00 19.7 1.59 1.00 19.7 0.147 1.00 19.7 0.0869 0.100 1.00 20.6 0.0869 0.100 1.00 0.103 1.00 0.103 1.00 19.7 19.7 19.7

Sample No. Type Analyzed SDG 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015 385077 3.1.1.E.4 SAMPLE 12/3/2015. 385077 3.1.1.E.4 MSD 1/13/2016 389094 3.1.1.E.4 MSD 1 /13/2016 389094 3.1.1.E.4 MS 1 /14/2016 389094 3.1.1.E.4 MS 1/14/2016 389094 3.1.1.E.4 DUP 1/13/2016 389094 3.1.1.E.4 DUP 1/13/2016 389094 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/1/2015 385077 3.1.1.E.5 SAMPLE 12/1 /2015 385077 3.1.1.E.5 SAMPLE 11/24/2015 385077 3.1.1.E.5 SAMPLE 11/24/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/1/2015 385077 3.1.1.E.5 SAMPLE 12/1/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 11/24/2015 385077 3.1.1.E.5 SAMPLE 11/24/2015 385077 3.1.1.E.5 SAMPLE 11/24/2015 385077 3.1.1.E.5 SAMPLE 11/24/2015 385077 3.1.1.E.5 SAMPLE 11/24/2015 385077 3.1.1.E.5 SAMPLE 11/24/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 3.1.1.E.5 SAMPLE SAMPLE 12/3/2015 385077 12/2/2015 385077 Parameter Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 ALPHA BETA ALPHA BETA ALPHA BETA Actinium-227 Actinium-227 ALPHA ALPHA Americium-241 Americium-241 Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Carbon-14 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-242 Curium-243/244 Curium-243/244 Curium-245/246 Curium-245/246 Europium-154 Europium-154 lodine-129 Area 3 Fraction Method

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

. DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 931 O/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

R R

DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 931 O/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA EERF C-01 Modified EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified Result Uncertainty CAS Units Lab Qu MDL CRDL Dilution % MoistL

-0.0144 1.16 1.07 12.8 0.526 0.00 1.11 1.22 0.373 0.00 107 114 123 105 12.6 20.4 0.285 0.285 16.7 16.7 0.166 15585-10-1 PCl/G U

0.321 1.00 19.7 0.149 15092-94-1 PCl/G 0.134 1.00 19.7 0.219 15067-28-4 PCl/G 0.398 1.00 19.7 1.63 13966-00-2 PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G 0.985 14331-85-2 0.985 14331-85-2 0.194 13982-63-3 0.370 15262-20-1 0.103 14913-50-9 0.177 13.8 12587-46-1

. PCl/G UI 15.6 12587-47-2 16.0 12587-46-1 15.9 12587-47-2 3.39 12587-46-1 PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G 2.73 12587-47-2 0.412 14952-40-0 0.412 14952-40-0 2.60 12587-46-1 2.60 12587-46-1 0.0129 0.0442 0.0129 0.0442

-0.131 0.185

-0.131 0.185 28.1 1.76 28.1 1.76 1.52 1.03 0.858 0.232

-0.754 0.860

-0. 754 0.860 1.25 0.142 1.25 0.142 0.0377 0.0576 0.0377 0.0576

-0.0034 0.0293

-0.00246 0.0369

-0.00246 0.0369 0.0392 0.0565 0.0392 0.0565 0.190 0.174 0.00

-0.00286 0.174 0.364 14596-10-2 PCl/G U

14596-10-2 PCl/G U

14234-35-6 PCl/G U

12587-47-2 PCl/G 12587-47-2 PCl/G 14913-49-6 PCl/G 14733-03-0 PCl/G 14762-75-5 PCl/G U

14762-75-5 PCl/G U

10045-97-3 PCl/G 10045-97-3 PCl/G 10198-40-0 PCl/G U

10198-40-0 PCl/G U

OER-100-93 PCl/G U

PCl/G U

PCl/G 15585-10-1 PCl/G U

15585-10-1 15046-84-1 PCl/G UI PCl/G U

0.979 1.09 1.09 0.147 0.374 0.0747 0.213 5.56 4.38 5.09 3.18 4.09 3.14 0.785 0.785 2.98 2.98 4.00 10.0 4.00 10.0 4.00 10.0 4.00 4.00 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 19.7 1.00 15.6 1.00 19.1 1.00 19.7 1.00 15.6 0.0819 1.00 1.00 15.6 0.0819 1.00 1.00 19.1 0.276 1.00 15.6 0.276 1.00 19.1 1.50 10.0 1.00 15.6 1.50 10.0 1.00 19.1 1.30 1.00 19.1 0.207 1.00 19.1 1.50 2.00 1.00 15.6 1.50 2.00 1.00 19.1 0.111 0.100 1.00 15.6 0.111 0.100 1.00 19.1 0.125 1.00 15.6 0.125 1.00 19.1 0.068 1.00 1.00 15.6 0.068 1.00 1.00 19.1 0.0862 1.00 1.00 15.6 0.0862 1.00 1.00 19.1 0.0682 1.00 1.00 15.6 0.0682 1.00 1.00 19.1 0.382 1.00 15.6 0.382 0.643 1.00 1.00 1.00 19.1 15.6

'\\

Sample No.* Type Analyzed SDG 3.1.1.E.5 SAMPLE 12/2/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 11/23/2015 385077 11/23/2015 385077 11/23/2015 385077 11/23/2015 385077 11/23/2015 385077 11/23/2015 385077 11/25/2015 385077 11/25/2015 385077 3.1.1.E.5 SAMPLE 3.1.1.E.5 SAMPLE 3.1.1.E.5 SAMPLE 3.1.1.E.5 SAMPLE 3.1.1.E.5 SAMPLE 3.1.1.E.5 SAMPLE 3.1.1.E.5 SAMPLE 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 SAMPLE 12/3/2015 385077 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5

'3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 3.1.1.E.5 SAMPLE 12/3/2015 385077 SAMPLE 12/3/2015 385077 SAMPLE 11/29/2015 385077 SAMPLE 11/29/2015 385077 SAMPLE 12/3/2015 385077 SAMPLE 11/24/2015 385077 SAMPLE 11/24/2015 385077 SAMPLE 11/24/2015 385077 SAMPLE 11/24/2015 385077 SAMPLE 11/24/2015 385077 SAMPLE 11/24/2015 385077 SAMPLE 11/24/2015 385077 SAMPLE 11/24/2015 385077 SAMPLE 12/3/2015 385077 SAMPLE 12/3/2015 385077 SAMPLE 12/2/2015 385077 SAMPLE 12/2/2015 385077 SAMPLE 11/25/2015 385077 SAMPLE 11/25/2015 385077 SAMPLE 11/25/2015 385077 SAMPLE 11/25/2015 385077 SAMPLE 11/25/2015 385077 SAMPLE 11/25/2015 385077 SAMPLE 11/25/2015 385077 SAMPLE 11/25/2015 385077 Parameter lodine-129 Lead-212 Lead-214 Neptunium-237 Neptunium-237 Plutonium-238 Plutonium-238 Plutonium-239/240 Plutonium-239/240 Plutonium-241 Plutonium-241 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Strontium-90 Strontium-90 Technetium-99 Technetium-99 Thallium-208 Thorium-228 Thorium-228 Thorium-229 Thorium-229 Thorium-230 Thorium-230 Thorium-232 Thorium-232 Tin-126 Tin-126 Tritium Tritium Uranium-232 Uranium-232 Uranium-233/234 Uranium-233/234 Uranium-235/236 Uranium-235/236 Uranium-238 Uranium-238 Area 3 Fraction Method R

DOE EML HASL-300,1-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

ASTM C 1476-00 Modified R

DOE EML HASL-300, Pu-11-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified DOE EML HASL-300, Tc-02-RC Modified DOE EML HASL-300, Tc-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified Result

-0.00286 1.36 1.15

-0.108

-0.0167

-0.00278

-2.57

-2.57 15.9 0.635 0.635 0.858 0.858 1.19 1.19

-0.0135

-0.0135 1.26 1.26 0.477 1.60 1.60

-0.0396

-0.0396 1.03 1.03 1.28 1.28 0.0421 0.0421 0.912 0.912

-0.02

-0.02 0.995 0.995 0.0427 0.0427 0.849 0.849 Uncertainty GAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.364 15046-84-1 PCl/G U

0.643 1.00 1.00 19.1 0.187 0.274 0.245 0.245 0.0386 0.0386 0.0643 0.0643 5.58 5.58 2.04 0.833 0.833 0.232 0.232 0.351 0.351 0.998 0.998 1.56 1.56 0.110 0.545 0.545 0.134 0.134 0.432 0.432 0.468 0.468 0.158 0.158 1.87 1.87 0.0486 0.0486 0.246 0.246 0.0615 0.0615 0.231 0.231 15092-94-1 15067-28-4 13994-20-2 13994-20-2 13981-16-3 13981-16-3 OER-100-70 OER-100-70 14119-32-5 14119-32-5 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 10098-97-2 10098-97-2 14133-76-7 14133-76-7 14913-50-9 PCl/G 0.161 1.00 19.1 PCl/G 0.222 1.00 19.1 PCl/G U

0.668 1.00 1.00 15.6 PCl/G U

0.668 1.00 1.00 19.1 PCl/G U

0.114 1.00 1.00 15.6 PCl/G U

0.114 1.00 1.00 19.1 PCl/G U

0.145 1.00 1.00 15.6 PCl/G U

0.145 1.00 1.00 19.1 PCl/G U

9.76 15.0 1.00 15.6 PCl/G U

9.76 15.0 1.00 19.1 PCl/G 0.894 1.00 19.1 PCl/G U

1.49 1.00 15.6 PCl/G U

1.49 1.00 19.1 PCl/G 0.207 1.00 15.6 PCl/G 0.207 1.00 19.1 PCl/G 0.390 1.00 15.6 PCl/G 0.390 1.00 19.1 PCl/G U

PCl/G U

PCl/G 1.91 2.00 1.00 1.00 1.00 1.00 1.00 15.6 19.1 15.6 19.1 19.1 1.91 2.00 2.62 5.00 2.62 5.00 0.104 14274-82-9

. PCl/G 0.350 1.00 1.00 15.6 14274-82-9 PCl/G 15594-54-4 PCl/G U

15594-54-4 PCl/G U

14269-63-7 PCl/G 14269-63-7 PCl/G 7440-29-1 PCl/G 7440-29-1 PCl/G 10028-17-8 10028-17-8 14158-29-3 14158-29-3 PCl/G U

PCl/G U

13968-55-3/139( PCl/G 13968-55-3/139( PCl/G 15117-96-1/1391PCl/G U

15117-96-1/1391 PCl/G 7440-61-1 PCl/G 7440-61-1 PCl/G 0.350 1.00 1.00 19.1 0.348 1.00 1.00 15.6 0.348 1.00 1.00 19.1 0.283 1.00 1.00 15.6 0.283 1.00 1.00 19.1 0.128 1.00 1.00 15.6 0.128 1.00 1.00 19.1 0.242 1.00 15.6 0.242 1.00 19.1 3.34 6.00 1.00 15.6 3.34 6.00 1.00 24.4 0.106 1.00 1.00 15.6 0.106 1.00 1.00 24.4 0.0854 1.00 1.00 15.6 0.0854 1.00 1.00 24.4 0.0741 1.00 1.00 15.6 0.0741 1.00 1.00 24.4 0.125 1.00 1.00 15.6 0.125 1.00 1.00 24.4

Sample No. Type 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE 3.1.1.E.6 SAMPLE

Analyzed 12/3/2015 12/3/2015 12/1/2015 SD~

385077 385077 385077 12/1/2015 385077 11/24/2015 385077 11/24/2015 385077 12/312015 385077 12/3/2015 385077 12/1/2015 385077 12/1/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 12/3/2015 385077 12/3/2015 385077 12/2/2015 385077 12/2/2015 385077 12/3/2015 385077 12/3/2015 385077 11/23/2015 385077 11/23/2015 385077 11/23/2015 385077 11/23/2015 385077 11/23/2015 385077 11/23/2015 385077 11/25/2015 385077 11/25/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 12/3/2015 385077 Parameter Actinium-227 Actinium-227 ALPHA ALPHA Americium-241 Americium-241 Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Carbon-14 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-242 Curium-243/244 Curium-243/244 Curium-245/246 Curium-245/246 Europium-154 Europium-154 lodine-129 lodine-129 Lead-212 Lead-214 Neptunium-237 Neptunium-237 Plutonium-238 Plutonium-238 Plutonium-239/240 Plutonium-239/240 Plutonium-241 Plutonium-241 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

R EPA 900.0/SW846 9310/SM 7110B Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA EERF C-01 Modified.

EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified ASTM C 14 76-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga~01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.219 0.219 23.6 23.6 0.0182 0.0182 0.0237 0.0237 29.4 29.4 0.00 0.840

-0.975

-0.975 1.86 1.86

-0.026

-0.026 0.00 0.00

-0.00521

-0.00521 0.137 0.137 0.0489 0.0489 0.162 0.162 1.34 1.23 0.0729 0.0729 0.0278 0.0278

-0.0117

-2.06

-2.06 17.1 0.00 0.00 0.840 0.840

. Uncertainty CAS Units Lab Qu MDL CRDL Dilution % MoistL 0.330 14952-40-0 PCl/G U

0.576 1.00 24.4 0.330 14952-40-0 PCl/G U

0.576 1.00 22.7 2.63 12587-46-1 PCl/G 2.10 4.00 1.00 24.4 2.63 0.0418 0.0418 0.135 0.135 1.83 1.83

0.909 0.203 0.836 0.836 0.164 0.164 0.0457 0.0457 0.0276 0.0276 0.036 0.036 0.0893 0.0893 0.132 0.132 0.310 0.310 0.152 0.229 0.249 0.249 0.0639 0.0639 0.0688 0.0688 6.25 6.25 1.88 1.01 1.01 0.203 0.203 12587-46-1 PCl/G 14596-10-2 PCl/G U

14596-10-2 PCl/G 14234-35-6 PCl/G U

14234-35-6 PCl/G U

12587-47-2 PCl/G 12587-47-2 PCl/G 14Q13-49-6 PCl/G UI 14733-03-0 PCl/G 14762-75-5 PCl/G U

14762-75-5 PCl/G U

10045-97-3 PCl/G 10045-97-3 PCl/G 10198-40-0 PCl/G U

10198-40-0 PCl/G U

OER-100-93 PCl/G U

OER-100-93 PCl/G PCl/G U

PCl/G U

PCl/G X

15585-10-1 PCl/G U

15046-84-1 PCl/G U

15092-94-1 PCl/G 15067-28-4 PCl/G 13994-20-2 PCl/G U

13994-20-2 PCl/G U

13981-16-3 PCl/G U

13981-16-3 PCl/G OER-100-70 PCl/G U

OER-100-70 PCl/G U

14119-32-5 PCl/G U

13966-00-2 PCl/G 14331-85-2 PCl/G UI 14331-85-2 PCl/G UI 13982-63-3 PCl/G 13982-63-3 PCl/G 2.10 4.00 1.00 22.7 0.0663 1.00 1.00 24.4 0.0663 1.00 1.00 22.7 0.255 1.00 24.4 0.255 1.00

22. 7 1.66 10.0 1.00 24.4 1.66 10.0 1.00 22.7 1.49 1.00

22. 7 0.170 1.00 22.7 1.47 2.00 1.00 24.4 1.47 2.00 1.00 22.7 0.0911 0.100 1.00 24.4 0.0911 0.100 1.00

22. 7 0.0821 1.00 24.4 0.0821 1.00 22.7 0.041 1.00 1.00 24.4 0.041 1.00 1.00 22.7 0.0876 1.00 1.00 24.4 0.0876 1.00 1.00 22.7 0.0411 1.00 1.00 24.4 0.0411 1.00 1.00 22.7 0.278 1.00 24.4 0.278 1.00

22. 7 0.601 1.00 1.00 24.4 0.601 1.00 1.00 22.7 0.125 1.00 22.7 0.395 1.00 22.7 0.462 1.00 1.00 24.4 0.462 1.00 1.00

22. 7 0.101 1.00 1.00 24.4 0.101 1.00 1.00 22.7 0.164 1.00 1.00 24.4 0.164 1.00 1.00 22.7 10.9 15.0 1.00 24.4 10.9 15.0 1.00 22.7 0.922 1.00 22.7 1.08 1.00 24.4 1.08 1.00 22.7 0.170 1.00 24.4 0.170 1.00 22.8

Sample No. Type.

3.1. 1.E.6 SAMPLE 3.1. 1.E.6 3.1.1.E.6 3.1.1.E.6

3. 1. 1.E.6

3. 1.1.E.6 3.1.1.E.6 3.1.1.E.6 3.1.1.E.6

3. 1. 1.E.6 3.1.1.E.6 3.1.1.E.6

3. 1. 1.E.6 3.1.1.E.6 3.1.1.E.6 3.1.1.E.6 3.1. 1.E.6 3.1.1.E.6 3.1.1.E.6 3.1.1.E.6 3.1.1.E.6 3.1.1.E.6 3.1.1.E.6 3.1. 1.E.6 3.1.1.E.6 3.1.1.E.6 3.1.1.E.6 3.1.1.E.6 3.1. 1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1. 1.E.7 3.1.1.E.7

' 3.1.1.E.7 3.1.1.E.7 3.1. 1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE DUP DUP DUP SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 12/3/2015 12/3/2015 12/2/2015 12/2/2015 385077 385077 385077 385077 11/29/2015 385077 11/29/2015 385077 12/3/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 11/24/2015 385077 12/3/2015 385077 12/3/2015 385077 12/2/2015 385077 42340 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42340 385077 42340 385077 42340 385077 42341 385077 42341 385077 42339 385077 42339 385077 42332 385077 42332 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42342 385077 Parameter Radium-228 Radium-228 Strontium-90 Strontium-90 Technetium-99 Technetium-99 Thallium-208 Thorium-228 Thorium-228 Thorium-229 Thorium-229 Thorium-230 Thorium-230 Thorium-232 Thorium-232 Tin-126 Tin-126 Tritium Tritium Uranium-232 Uranium-232 Uranium-233/234 Uranium-233/234 Uranium-235/236 Uranium-235/236 Uranium-238 Uranium-238 Strontium-90 Strontium-90 Strontium-90 Actinium-227 Actinium-227 ALPHA

ALPHA Americium-241 Americium-241 Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Carbon-14 Area 3

Fraction Method

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Th-01-RC Modified R

R R

R DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified '

EPA 900.0/SW846 931 O/SM 711 OB Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 711 OB Modified EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA EERF C-01 Modified Result 1.19 1.19

-0.576

-0.576 1.11 1.11 0.430 0.773 0.773

-0.062

-0.062 1.81 1.81 0.998 0.998 0.151 0.00 0.979 0.979 0.0288 0.0288 1.16 1.16 0.0345 0.0345 0.958 0.958 0.0829 0.0829 0.0829 0.193 0.193 10.4 10.4 0.0101 0.0101 0.0443 0.0443 25.0 25.0 2.00 0.912 0.399 Uncertainty GAS Units Lab Qu MDL

. CRDL C Dilution °/o'MoistL 0.438 15262-20-1 PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI 0.285 0.285 0.438 15262-20-1 10098-97-2 1!)098-97-2 14133-76-7 14133-76-7 14913-50-9 14274-82-9 14274-82-9 15594-54-4 15594-54-4 14269-63-7 14269-63-7 7440-29-1 7440-29-1 10028-17-8 PCl/G 10028-17-8 PCl/G 14158-29-3 PCl/G 14158-29-3 PCl/G 13968-55-3/1391 PCl/G 13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 7440-61-1 PCl/G 10098-97-2 PCl/G 10098-97-2 PCl/G 10098-97-2 PCl/G 14952-40-0 PCl/G 14952-40-0 PCl/G 12587-46-1 PCl/G 12587-46-1 PCl/G 14596-10-2 PCl/G 14596-10-2 PCl/G 14234-35-6 PCl/G 14234-35-6 PCl/G 12587-47-2 PCl/G 12587-47-2 PCl/G 14913-49-6 PCl/G 14733-03-0 PCl/G u

1.37 2.00 2.00 5.00 5.00 u

1.37 u

2.99 u

2.99 0.0704 u

1. 11

1. 11 1.00 1.00 1.00 1.00 1.00 1.00 u

0.716 u

u u

u 0.850 0.850 0.617 1.00 0.617 1.00 0.176 0.176 3.29 3.29 0.140 0.140 0.119 6.00 6.00 1.00 1.00 1.00 0.119 1.00 0.0941 1.00 0.0941 1.00 0.0587 1.00 0.0587 1.00 1.52 2.00 1.52 2.00 1.52 2.00 0.648 0.648 2.41

' 4.00 2.41 4.00 0.0888 1.00 0.0888 1.00 0.263 0.263 2.59 10.0 2.59 10.0 0.941 0.177 0.594 0.594 1.76 1.76 0.0867 0.805 0.805 0.274 0.274 1.02 1.02 0.761 0.761 0.127 0.127 1.86 1.86 0.0774 0.0774 0.300 0.300 0.0679 0.0679 0.271 0.271 0.798 0.798 0.798 0.347 0.347 2.05 2.05 0.0454 0.0454 0.139 0.139 2.07 2.07 0.947 0.169 0.897 14762-75-5 PCl/G U

1.52 2.00 1.00 24.4 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 22.8 24.4 22.8 24.4 22.8 22.8 24.4 22.8 24.4 22.8 24.4 22.8 22.7 22.8 22.7 22.8 22.7 22.8 22.7 22.8 22.7 22.8

. 22.7 22.8 22.7 22.8 24.4 22.7 22.8 22.8 23.1 22.8 23.1 22.8 23.1 22.8 23.1 22.8 23.1 23.1 23.1 22.8

Sample No. Type 3.1.1.E.7 SAMPLE 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 3.1.1.E.7 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42342 385077 42341 385077 42341 385077 42341 385077 42341 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332. 385077 42341 385077 42341 385077 42340 385077 42340 385077 42341 385077 42341 385077 42331 385077 42331 385077 42331 385077 42331 385077 42331 385077 42331 385077 42333 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42337 385077 42337 385077 42341 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42341 385077 42340 385077 42340 385077 42332 385077 42332 385077 Parameter Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-242 Curium-243/244 Curium-243/244 Curium-245/246 Curium-245/246 Europium-154 Eurbpium-154 lodine-129 lodine-129 Lead-212 Lead-214 Neptunium-237 Neptunium-237 Plutonium-238 Plutonium-238 Plutonium-239/240 Plutonium-239/240 Plutonium-241 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-228 Strontium-90 Technetium-99 Technetium-99 Thallium-208 Thorium-228 Thorium-229 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tritium Tritium Uranium-232 Uranium-233/234 Area 3 Fraction Method R

EPA EERF C-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300,1-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

R ASTM C 1476-00 Modified ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified DOE EML HASL-300, Tc-02-RC Modified DOE EML HASL-300, Tc-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified Result 0.399 2.58 2.58 0.0335 0.0335 0.00 0.00 0.0125 0.0125 0.101 0.101

-0.128

-0.103

-0.103 1.28 1.26 0.00278 0.00278 0.0414 0.0414

-0.0421

-4.56 15.5 0.870 0.00 0.912 1.27

-0.368 2.21 2.21 0.347 1.38 0.0995 0.0995 0.841 1.15 0.00 1.56 1.56 0.0336 0.747 Uncertainty CAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.897 14762-75-5 u

1.52 PCl/G PCl/G PCl/G PCl/G U

PCl/G U

2.00 1.00 23.1 0.202 0.202 0.0582 0.0582 0.0291 0.0291 0.0352 0.0352 0.0806 0.0806 10045-97-3 10045-97-3 10198-40-0 10198-40-0 OER-100-93 OER-100-93 PCl/G PCl/G U

PCl/G PCl/G X

PCl/G X

0.189 15585-10-1 PCl/G U

0.254 15046-84-1 PCl/G U

0.141 15092-94-1 PCl/G PCl/G 0.178 15067-28-4 0.206 0.206 0.0732 0.0732 0.0719 0.0719 5.95 1.65 0.724 0.724 0.169 0.432 0.522 1.64 1.64 0.111 0.542 0.198 0.198 0.418 0.477 0.093 1.90 1.90 0.105 0.251 13994-20-2 PCl/G U

13994-20~2 PCl/G U

13981-16-3 PCl/G U

13981-16-3 PCl/G OER-100-70 PCl/G U

OER-100-70 PCl/G U

14119-32-5 PCl/G U

13966-00-2 PCl/G 14331-85-2 PCl/G U

14331-85-2 PCl/G UI 13982-63-3 PCl/G 15262-20-1 PCl/G 10098-97-2 PCl/G U

14133-76-7 PCl/G U

14133-76-7 PCl/G 14913-50-9 PCl/G 14274-82-9 PCl/G 15594-54-4 PCl/G U

15594-54-4 PCl/G 14269-63-7 PCl/G 7440-29-1 PCl/G PCl/G UI 10028-17-8 PCl/G U

10028-17-8 PCl/G 14158-29-3 PCl/G u

13968-55-3/1391 PCl/G 0.089 0.100 1.00 22.8 0.089 0.100 1.00 23.1 22.8 23.1 22.8 23.1 22.8 23.1 22.8 23.1 22.8 23.1 22.8 23.1 23.1 23.1 0.109 0.109 0.0434 1.00 0.0434 1.00 0.0376 1.00 0.0376 1.00 0.0435 1.00 0.0435 1.00 0.326 0.326 0.447 1.00 0.447 1.00 0.123 0.192 0.458 1.00 0.458. 1.00 0.111 1.00 0.111 1.00 0.192 1.00 0.192 1.00 10.5 15.0 0.845 0.967 0.967 0.177 0.281 1.12 2.00 2.70 5.00 2.70 5.00 0.0915 0.376 1.00 0.321 1.00 0.321 1.00 0.297 1.00 0.233 1.00 0.122 3.21 3.21 0.196 0.117 6.00 6.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 22.8 1.00 23.1 1.00 22.8 1.00 23.1 1.00 22.8 1.00 23.1 1:00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 23.1 1.00 1.00 1.00 1.00 23.1 23.1 23.1 23.1

Sample No.. Jype Analyzed SDG 3.1.1.E.7 SAMPLE 42332 385077 3.1.1.E.7 SAMPLE 42332 385077 3.1.1.E.7 SAMPLE 42332 385077 3.1.1.E.7 SAMPLE 42332 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42339 385077 3.1.1.E.8 SAMPLE 42339 385077 3.1.1.E.8 SAMPLE 42332 385077 3.1.1.E.8 SAMPLE 42332 385077 3.1.1. E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42339 385077 3.1.1.E.8 SAMPLE 42339 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42342 385077 3.1.1.E.8 SAMPLE 42342 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42332 385077 3.1.1.E.8 SAMPLE 42332 385077 3.1.1.E.8 SAMPLE 42332 385077 3.1.1.E.8 SAMPLE 42332 385077 3.1.1.E.8 SAMPLE 42332 385077 3.1.1.E.8 SAMPLE 42332 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42340 385077 3.1.1.E.8 SAMPLE 42340 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42341 385077 3.1.1.E.8 SAMPLE 42331 385077 3.1.1.E.8 SAMPLE 42331 385077 3.1.1.E.8 SAMPLE 42331 385077 3.1.1.E.8 SAMPLE 42331 385077 3.1.1.E.8 SAMPLE 42331 385077 3.1.1.E.8 SAMPLE 42331 385077 3.1.1.E.8 SAMPLE 42333 385077 3.1.1.E.8 SAMPLE 42333 385077 3.1.1.E.8 SAMPLE 42341 385077 Parameter Uranium-235/236 Uranium-235/236 Uranium-238 Uranium-238 Actinium-227 Actinium-227 ALPHA ALPHA Americium-241 Americium-241 Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Carbon-14 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-242 Curium-243/244 Curium-243/244 Curium-245/246 Curium-245/246 Europium-154 Europium-154 lodine-129 lodine-129 Lead-212 Lead-214 Neptunium-237 Neptunium-237 Plutonium-238 Plutonium-238 Plutonium-239/240 Plutonium-239/240 Plutonium-241 Plutonium-241 Potassium-40 Area 3 Fraction Method R

DOE EML HASL-300, U-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA EERF C-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300,1-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R" R

DOE HASL 300, 4.5.2.3/Ga-01-R R

ASTM C 1476-00 Modified R

ASTM C 14 76-00 Modified R

DOE EML HASL-300, Pu-11-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.159 0.159 0.815 0.815 0.394 0.00 10.7 10.7 0.00914 0.00914 0.00737 0.00737 19.0 19.0 0.533 0.952

-0.847

-0.847 0.315 0.315 0.0063 0.0063 0.00 0.00

-0.0232

-0.0232 0.0702 0.0702 0.119 0.119

-0.243

-0.243 1.12 1.41 0.131 0.131 0.010 0.010 0.00154 0.00154

-4.42

-4.42 13.6 Uncertainty CAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.125 15117-96-1/1391PCl/G 0.117 1.00 1.00 23.1 0.125 0.261 0.261 0.272 0.272 1.91 1.91 0.059 0.059 0.102 0.102 1.50 1.50 0.711 0.176 0.846 0.846 0.083 0.083 0.0346 0.0346 0.0375 0.0375 0.0375 0.0375 0.0828 0.0828 0.132 0.132 0.361 0.361 0.158 0.232 0.257 0.257 0.0556 0.0556 0.0707 0.0707 6.41 6.41 1.60 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 7440-61-1 PCl/G 14952-40-0 PCl/G u

14952-40-0 12587-46-1 12587-46-1 14596-10-2 14596-10-2 14234-35-6 14234-35-6 12587-47-2 12587-47-2 14913-49-6 14733-03-0 14762-75-5 14762-75-5 10045-97-3 10045-97-3 PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G 10198-40-0 PCl/G U

10198-40-0 PCl/G U

OER-100-93 PCl/G U

OER-100-93 PCl/G PCl/G U

PCl/G U

PCl/G 15585-10-1 PCl/G U

15585-10-1 PCl/G U

15046-84-1 PCl/G U

15092-94-1 PCl/G 15067-28-4 PCl/G 13994-20-2 PCl/G U

13994-20-2 PCl/G 13981-16-3 PCl/G U

13981-16-3 PCl/G U

OER-100-70 PCl/G U

14119-32-5 PCl/G U

13966-00-2 PCl/G 0.117 0.101 0.101 0.567 0.567 1.00 1.00 1.00 1.00 1.00 1.00 1.00 23.3 23.1 23.3 23.3 1.00 21.6 2.15 4.00 1.00 23.3 2.15 4.00 1.00 21.6 0.121 1.00 1.00 23.3 0.121 1.00 1.00 21.6 0.193 1.00 23.3 0.193 1.00 21.6 1.50 10.0 1.00 23.3 1.50 10.0 1.00 21.6 1.28 1.00 21.6 0.142 1.00 21.6 1.48 2.00 1.00 23.3 1.48 2.00 1.00 21.6 0.081 0.100 1.00 23.3 0.081 0.100 1.00 21.6 0.0738 0.0738 0.0559 1.00 0.0559 1.00 0.119 1.00 0.119 1.00 0.0895 1.00 0.0895 1.00 0.292 0.292 0.607 1.00 0.607 1.00 0.174 0.389 0.356 1.00 0.356 1.00 0.107 1.00 0.107 1.00 0.155 1.00 0.155 1.00 11.3 15.0 11.3 15.0 0.656 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 1.00 21.6 1.00 21.6 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 1.00 21.6

Sample No. Type 3.1.1.E.8 SAMPLE 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.1.E.8 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.1 O.E.1 3.1.10.E.1 3.1.10.E.1 3.1.1 O.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42337 385077 42337 385077 42341 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42332 385077 42341 385077 42340 385077 42340 385077 42332 385077 42332 385077 42332 385077 42332 385077 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 Parameter Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Strontium-90 Strontium-90 Technetium-99 Technetium-99 Thallium-208 Thorium-228 Thorium-228 Thorium-229 Thorium-229 Thofium-230 Thorium-230

Thorium-232 Thorium-232 Tin-126 Tritium Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

R DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00 0.00 0.952 0.952 0.991 0.991 0.259 0.259 0.991 0.991 0.374 0.973 0.973 0.0786 0.0786 0.960 0.960 1.09 1.09 0.00 1.54 1.54 0.0148 1.12 0.148 0.951

-0.0936 12.8 0.0373 21.5 0.00 1.04 1.16 0.0117

-0.0198 1.07 0.976 14.0 0.00 1.04 1.28 0.308 0.00 Uncertainty GAS Units Lab Qu MDL CRDL Dilution % MoistL 0.788 14331-85-2 UI 1.00 PCl/G PCl/G PCl/G PCJ/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

1.00 23.3 0.788 14331-85-2 UI 1.00 1.00 21.6 0.176 0.176 0.327 0.327 0.510 0.510 1.62 1.62 0.0813 0.445 0.445 0.178 0.178 0.421 0.421 0.444 0.444 0.143 1.91 1.91 0.0869 0.316 0.122 0.288 0.382 3.99 0.153 3.74 0.817 0.222 0.156 0.0593 0.191 0.223 0.295 1.75 0.781 0.222 0.381 0.0992 0.232 0.142 0.142 0.293 0.293 1.00 23.3 1.00 21.6 1.00 23.3 1.00 21.6 13982-63-3 13982-63-3 15262-20-1 15262-20-1 10098-97-2 10098-97-2 14133-76-7 14133-76-7 14913-50-9 14274-82-9 14274-82-9 15594-54-4 15594-54-4 14269-63-7 14269-63-7 7440-29-1 7440-29-1.

u.

0.913 2.00 2.00 5.00 5.00 1.00 23.3 u

0.913 1.00 21.6 u

2.75 1.00 23.3 u

2.75 1.00 21.6 PCl/G PCl/G PCl/G PCl/G PCl/G UJ 10028-17-8 PCl/G 10028-17-8 PCl/G 14158-29-3 PCl/G 13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 14952-40-0 PCl/G 12587-46-1 PCl/G 14234-35-6 PCl/G 12587-47-2 PCl/G 14913-49-6 PCl/G 14733-03-0 PCJ/G 10045-97-3 PCl/G 10198-40-0 PCl/G 15585-10-1 PCl/G 15092-94-1 PCl/G 15067-28-4 PCl/G 13966-00-2 PCl/G 14331-85-2 PCl/G 13982-63-3 PCl/G 15262-20-1 PCl/G 14913-50-9 PCl/G PCl/G u

u u

u UI u

u UJ UI 0.0703 1.00 21.6 0.381 1.00 1.00 0.381 1.00 1.00 0.306 1.00 1.00 0.306 1.00 1.00 0.287 1.00 1.00 0.287 1.00 1.00 0.286 1.00 1.00 0.286

1.00 0.167 3.24 6.00 3.24 6.00 0.173 1.00 0.176 1.00 0.105 1.00 0.121 1.00 0.695 3.97 4.00 0.284 4.48 10.0 1.72 0.180 0.0979 0.100 0.120 0.316 0.171 0.207 0.825 1.46 0.180 0.385 0.112 0.197 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 23.3 21.6 23.3 21.6 23.3 21.6 23.3 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.8 21.8 21.8 21.8 21.8 21.8 21.8 21.8

Sample No. Type 3.1.10.E.1 DUP 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.1 O.E.1 3.1.1 O.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.1 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.1 O.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 3.1.1 O.E.2 3.1.10.E.2 3.1.10.E.2 3.1.10.E.2 DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE' SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 Parameter Actinium-227 Antimony-125 Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4."5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.131 0.0444 0.00 0.978 1.24

-0.024

-0.0451 1.12 1.22 14.7 0.00 0.978 0.957 0.394 0.0594

-0.346

-0.305 9.23 0.0245 0.0514 22.4 0.00 0.00 0.918 0.963 1.28 1.45 0.00583 0.0154

-0.11 0.061 1.24 1.29 1.04 1.08 16.2 15.1 0.00 0.00 0.918 0.963 0.971 1.27 Uncertainty GAS Units

Lab Qu MDL CRDL C Dilution % MoistL 0.407 14952-40-0 PCl/G U

0.669 1.00 21.8 0.158 0.745 0.206 0.147 0.049 0.152 0.182 0.218 1.70 0.931 0.206 0.313 0.0968 0.178 0.350 0.352 3.22 0.154 0.127 2.95 0.774 0.973 0.201 0.178 0.173 0.167 0.0653 0.0581 0.217 0.147 0.155 0.138 0.228 0.205 1.94 1.65 0.913 1.00 0.201 0.178 0.336 0.330 14234-35-6 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G U

PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15092-94-1

PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="15262-20-1" PCl/G 0.287 1.53 1.00 21.8 1.00 21.8 0.145 1.00 21.8 0.101 0.100 1.00 21.8 0.0885 0.283 0.172 0.213 0.745 1.33 0.145 0.328 0.090 0.231 0.597 0.610 3.99 4.00 0.279 0.240 3.27 10.0 1.63 1.49 0.193 0.157 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 21.8 1.00 0

1.00 0

0.112 0.100 1.00 0

0.0872 0.100 1.00 21.8 0.128 1.00 21.8 0.115 1.00 22.9 0.321 1.00 22.9 0.300 1.00 22.9 0.150 1.00 22.9 0.127 1.00 22.9 0.198 1.00 22.9 0.167 1.00 22.9 1.08 1.00 22.9 0.622 1.00 22.9 1.17 1.00 22.9 1.13 1.00 22.9 0.193 1.00 22.9 0.157 1.00 22.9 0.395 1.00 22.9 0.316 1.00 22.9

Sample No. Type 3.1.10.E.2 SAMPLE 3.1.10.E.2 SAMPLE 3.1.10.E.2 SAMPLE 3.1.10.E.2 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.1 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE Analyzed SDG 42387 389296 42405 389296 42387 389296 42405 389296 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070.

42341 385070 42341 385070 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 Parameter Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137.

Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.340 0.400 0.00 0.00 0.167 13.8 0.0531 21.0 1.53 0.946 0.984

-0.0236 0.00 1.29 1.23 16.5 0.00 0.946 1.23 0.364 0.00 0.127

-0.00461 12.4

-0.0984

-0.0709 23.1 0.371 1.07 0.918 1.18 1.44 1.35

-0.0486 0.00937

-0.0346 0.0862 1.41 1.25 0.988 1.17 14.7 15.4 Uncertainty GAS.

Units Lab Qu MDL CRDL 0.107

="14913-50-9" PCl/G 0.0933 0.109

="14913-50-9" PCl/G 0.0826 0.153 PCl/G UI 0.218 0.114 0.254 3.32 0.104 2.81 0.832 0.149 0.0988 0.0349 0.131 0.129 0.191 1.34 0.572 0.149 0.325 0.0786 0.126 0.443 0.300 3.64 0.166 0.134 3.44 0.956 0.710 0.235 0.200 0.183 0.136 0.0489 0.0501 0.174 0.145 0.181 0.134 0.250 0.174 2.43 1.72

="

14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G U

="14913-49-6" PCl/G

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="13966-00-2" PCl/G 0.145 0.482 3.46 4.00 0.197 3.25 10.0 0.628

0.123 0.0738 0.100 0.060 0.255 0.112 0.139 0.455 0.840 0.123 0.266 0.0624 0.135 0.805 0.560 3.93 4.00 0.291 0.232 4.18 1.93 1.05 0.220 0.157 10.0 0.115 0.100 0.0821 0.100 0.0725 0.0994 0.349 0.301 0.163 0.113 0.221 0.171 1.42 0.931 Dilution % MoistL 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.0d 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9

Sample No. rype 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.11.E.2 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 SAMPLE 3.1.12.E.1 MSD 3.1.12.E.1 MSD 3.1.12.E.1 MS 3.1.12.E.1 MS 3.1.12.E.1 DUP 3.1.12.E.1 DUP 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE Analyzed SDG 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 Parameter Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 ALPHA 42341 385070 BETA 42341 385070.

ALPHA 42341 385070 BETA 42340 385070 ALPHA 42340 385070 BETA 42387 389296 Actinium-227 42405 389296 Actinium-227 42395 389296 ALPHA 42387 389296 Antimony-125 42405 389296 Antimony-125 42395 389296 BETA 42387 389296 Bismuth-212 42405 389296 Bismuth-212 42387 389296 Bismuth-214 42405 389296 Bismuth-214 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 7110B Modified R

R R

R' R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00 0.00 0.918 1.18 1.78 1.23 0.316 0.424 0.0695 0.00 0.0126 16.3

-0.107 26.4 0.00 1.06 1.05

-0.0284 0.0371 1.35 1.40 18.3 0.00 1.06 1.41 0.407 0.00 88.7 108 94.7 107 14.7 23.4

-0.203

-0.0241 13.2 0.0615

-0.0245 26.2 0.00 0.00 1.00 1.17 Uncertainty GAS Units

Lab a*u MDL CRDL C Dilution % MoistL 1.16

="14331-85-2" PCl/G UI 1.20 1.00 22.9 0.763

="14331-85-2" PCl/G UI 0.960 1.00 22.9 0.235

="13982-63-3" PCl/G 0.220 1.00 22.9 0.200 0.417 0.388 0.121 0.0832 0.156 0.0899 0.297 3.98 0.111 3.40 0.968 0.187 0.120 0.0415 0.134 0.140 0.182 1.45 0.642 0.187 0.282 0.071 0.133 15.6 17.3 15:2 17.5 4.01 3.49 0.260 0.308 3.71 0.116 0.114 3.18 0.843 0.809 0.174 0.153

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="

14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 12587-46-1 PCl/G U

PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI 12587-47-2 12587-46-1 12587-47-2 12587-46-1 PCl/G 12587-47-2 "PCl/G

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="14733-03-0" PCl/G 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 1.00 22.9 0.157 0.537 0.266 0.115 0.0755 0.233 0.112 0.538 3.95 0.189 4.01 4.00 1.00 22.9 1.00 23.4 10.0 1.00 23.4 1.27 1.00 23.4 0.145 1.00 23.4 0.0736 0.100 1.00 23.4 0.072 1.00 23.4 0.251 1.00 23.4 0.117 1.00 23.4 0.329 1.00 23.4 0.680 1.00 23.4 0.997 1.00 23.4 0.145 1.00 23.4 0.259 1.00 23.4 0.0677 1.00 23.4 0.157 1.00 23.4 7.32 4.00 1.00 23.4 3.78 10.0 1.00 23.4 4.25 4.00 1.00 23.4 4.03 10.0 1.00 23.4 3.86 4.00 1.00 23.4 3.71 10.0 1.00 23.4 0.461 1.00 23.4 0.549 1.00 23.4 3.89 4.00 1.00 23.4 0.223 1.00 23.4 0.203 1.00 23.4 2.87 10.0 1.00 23.4 1.46 1.00 23.4 1.35 1.00 23.4 0.147 1.00 23.4 0.127 1.00 23.4

Sample No. Type 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.12.E.2 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.1 SAMPLE 3.1.13.R.2 SAMPLE 3.1.13.R.2 SAMPLE 3.1.13.R.2 SAMPLE 3.1.13.R.2 SAMPLE Analyzed SDG 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42387 389296 42405 389296 42395 389296 42387 389296 Parameter Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 "Lead-214 Potassium-.40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208

Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 1.35 1.43

-0.0423

-0.0119 0.101

-0.0941 1.28 1.32 1.21 1.15 16.5 16.3 0.00 0.214 1.00 1.17 1.42 1.27 0.466 0.371 0.00 0.0343 0.121 8.17

-0.0425 16.3 1.86 0.964 0.966 0.0291 0.0314 1.04 0.786 10.9 0.00 0.964 0.679 0.385 0.00 0.113 0.172 11.9

-0.000289 Uncertainty GAS Units.

Lab Qu MDL CRDL C Dilution % Moistl 0.141

="10045-97-3" PCl/G 0.0947 0.100 1.00 23.4 0.117

="10045-97-3" PCl/G 0.0674 0.100 1.00 23.4 0.0438 0.039 0.143 0.130 0.131 0.132 0.182 0.210 1.65 1.34 0.805 0.606 0.174 0.153 0.294 0.300

. 0.0933 0.0751 0.0929 0.159 0.266 2.26 0.111 2.09 0.689 0.208 0.126 0.0422 0.136 0.161 0.218 1.55 0.859 0.208 0.385 0.077 0.124 0.345 0.331 3.81 0.143

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G UI

="14331-85-2" PCl/G U

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

0.070 0.0668 0.300 0.222 0.108 0.110 0.355 0.324 0.750 0.641 0.936 1.02 0.147 0.127 0.208 0.261 0.0706 0.074 0.106 0.194 0.537 2.68 4.00 0.201 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 2.47 10.0 1.00 23.4 1.07 1.00 23.4 0.146 1.00 23.4 0.107 0.100 1.00 23.4 0.0935 1.00 23.4 0.273 1.00 23.4 0.137 1.00 23.4 0.159 0.407 0.968 0.146 0.302 0.0737 0.135 0.658 0.631 3.99 4.00 0.264 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4

Sample No. Type Analyzed SDG 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42395 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.13.R.2 SAMPLE 42387 389296 3.1.13.R.2 SAMPLE 42405 389296 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42340 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42340 385070 3.1.14.R.1 SAMPLE.

42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 3.1.14.R.1 SAMPLE 42341 385070 Parameter Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R.

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5:2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE F-iASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result

-0.000515 21.9 0.00 1.52 0.618 0.785 1.10 0.991 0.00

-0.022

-0.0409 0.0246 0.986 1.10 0.994 0.998 11.8 12.0 0.00 0.00 0.618 0.785 1.11 0.00 0.326 0.296 0.00 0.0406

-0.143 9.96

-0.126 20.0 0.00 0.770 1.36

-0.00901 0.00656 1.07 0.817 11.5 0.00 0.770 0.988 Uncertainty GAS Units Lab Qu MDL CRDLC Dilution % Moistt 0.119

="14234-35-6" PCl/G U

0.216 1.00 23.4 2.90 1.21 0.645 0.184 0.179 0.142 0.123 0.0285 0.0518 0.139 0.128 0.148 0.140 0.280 0.204 1.65 1.63 0.622 0.903 0.184 0.179 0.281 0.328 0.104 0.074 0.192 0.114 0.268 3.08 0.101 2.46 0.555 0.161 0.128 0.0442 0.118 0.112 0.194 1.34 0.718 0.161 0.281

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14913-49-6" PCl/G

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G UI

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="15262-20-1" PCl/G UI

="14913-50-9" PCl/G

="14913-50-9" PCl/G 14952-40-0 12587-46-1 14234-35-6 12587-47-2 1'+913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G 2.54 1.65 0.792 0.170 10.0 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 0.171 1.00 22.1 /

0.0823 0.100 1.00 22.1 0.0733 0.100 1.00 22.1 0.0845 1.00 22.1 0.0944 1.00 22.1 0.258 1.00 22.1 0.236 1.00 22.1 0.138 1.00 22.1 0.137 1.00 22.1 0.376 1.00 22.1 0.173 1.00 22.1 0.818 1.00 22.1 0.917 1.00 22.1 1.10 1.00 22.1 1.05 1.00 22.1 0.170 1.00 22.1 0.171 0.271

. 0.650 0.084 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 0.0756 1.00 22.1 0.263 1.00 22.1 0.213 1.00 22.1 0.482 1.00 22.1 3.99 4:00 1.00 22.1 0.173 1.00 22.1 3.06 10.0 1.00 22.1 1.14 1.00 22.1 0.124 1.00 22.1 0.085 0.100 1.00 22.1 0.0833 1.00 22.1 0.232 1.00 22.1 0.101 1.00 22.1 0.137 1.00 22.1 0.743 0.811 0.124 0.244 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1

Sample No. Type 3.1.14.R.1 SAMPLE 3.1.14.R.1 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE.

3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.14.R.2 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE Analyzed SDG 42341 385070 42341 385070 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 Parameter Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 71108 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.277 0.00

-0.0627

-0.172 9.16

-0.0142 0.0178 19.6 1.77 0.00 0.744 0.869 1.37 1.27 0.0227 0.00241

-0.0087

-0.0386

o.942 0.794 0.764 0.915 11.4 11.9 0.00 0.342 0.744 0.869 0.952 1.02 0.200 0.203 0.00 0.00

-0.178 13.1 0.00 21.7 0.00 0.932 1.28 0.0155 0.00314 Uncertainty CAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.0893 14913-50-9 PCl/G 0.0735 1.00 22.1 0.0927 PCl/G UI 0.0936 1.00 22.1 0.280

="14952-40-0" PCl/G u

0.518 1.00 22.1 0.211 3.18 0.117 0.0897 2.47 0.760 0.621 0.173 0.144 0.141 0.0964 0.0403 0.030 0.139 0.0904 0.158 0.104 0.187 0.142 1.46 1.17 0.706 0.443 0.173 0.144 0.265 0.180 0.079 0.0651 0.0993 0.084 0.348 3.19 0.202 2.71 1.11 0.230 0.158 0.0487 0.151

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G UI

="14331-85-2" PCl/G U

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G PCl/G UI 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 PCl/G UI PCl/G U

PCl/G PCl/G UI PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

0.365 3.99 4.00 0.213 0.160 2.29 10.0 0.864 0.663 0.129 0.104 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 0.0746 0.100 1.00 22.1 0.0564 0.100 1.00 22.1 0.0886 1.00 22.1 0.0568 1.00 22.1 0.269 1.00 22.1 0.160 1.00 22.1 0.122 1.00 22.1 0.0986 1.00 22.1 0.148 1.00 22.1 0.234 1.00 22.1 0.591 1.00 22.1 0.428 1.00 22.1 0.953 1.00 22.1

0. 775 1.00 22.1 0.129 1.00 22.1 0.104 1.00 22.1 0.258 1.00 21.5 0.172 1.00 21.5 0.0639 1.00 21.5 0.0563 1.00 21.5 0.175 1.00 21.5 0.126 1.00 21.5 0.605 3.76 4.00 0.246 3.36 10.0 1.55 1.00 1.00 1.00 21.5 21.5 21.5 1.00 21.5 1.00 21.5 0.190 1.00 21.5 0.0961 0.100 1.00 21.5 0.0998 1.00 21.5 0.291 1.00 21.5

. ~ampl~ No.

Type

3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.1 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.1S.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.15.R.2 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE Analyzed SDG 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296.

42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42341 385070 42340 385070 42341 385070 Parameter Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125

. Area 3

. Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

' DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R "R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 1.10 1.16 15.0 0.00 0.932 0.906 0.295 0.0586

-0.0408

-0.053 18.5 0.0275 0.0738 23.7 0.00 2.07 0.828 0.833 1.68 1.72 0.00658 0.0252 0.0103

-0.024 1.20 1.18 0.944 1.26 13.3 15.3 0.00 0.00 0.828 0.833 1.07 1.14 0.301 0.387 0.00 0.00

-0.0964 14.7

-0.0282

.'. Uncertainty GAS*

Units

. lab.Ou MDL 0.154 15092-94-1 PCl/G 0.144 0.224 1.69 0.914 0.230 0.363 0.0794 0.189 0.357 0.283 4.07 0.152 0.121 2.89 0.857 0.966 0.196 0.176 0.183 0.140 0.0551 0.0471 0.135 0.150 0.151 0.129 0.267 0.185 1.65 1.71 0.888 0.996

o.196 0.176 0.376 0.287 0.0966 0.080 0.188 0.112 0.260 3.55 0.112 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14913-49-6" PCl/G

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G 14952-40-0 12587-46-1 14234-35-6 PCl/G UI PCl/G UI PCl/G U

PCl/G PCl/G U

0.173 0.731 1.23 0.190 0.340 0.0849 0.238 0.663 0.489 3.95 0.281 0.231 2.82 1.67 0.966 0.160 0.143 0.108 0.090 0.111 0.0908 0.275 0.244 0.147 0.118 0.204 0.338 0.617 0.730 1.54 0.907 0.160 0.143 0.377 0.282 0.0881 0.0742 0.202 0.124 0.494 3.98 0.206

. CRDL *c Dilution.% Maish 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 4.00 1.00 21.5 1.00 21.5 1.00 21.5 10.0.

1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 0.100 1.00 21.5 0.100 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 1.00 21.5 4.00 1.00 21.5 1.00 21.5

Sample No. Type 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAl\\APLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.1 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 42340 385070 42341 385070 42341 38507_0 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296

Parameter'.

BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228

Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antiinony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Area 3

. Fraction Method R

EPA 900.0/SW846 931 O/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result.*

21.7 0.00 0.682 1.75 0.00

-0.0232 0.930 0.944 11.7 0.306 0.682 0.716 0.278 0.0837

-0.0361 0.186 8.99

-0.081 0.00 17.0 0.00 0.00 0.475 0.635 2.41 2.48 0.0219

-0.0267

-0.0751

-0.0256 0.829 0.704 0.684 1.07 12.5 12.1

-0.189 0.349 0.475 0.635 0.842 0.663 0.220 Uncertainty GAS

.*Units Lab Ou MDL..

CRDL C Oilution % Moi.stt 2.59 12587-47-2 PCl/G PCl/G UI 0.914 14913-49-6 0.167 0.161 0.0414 0.114 0.129 0.220 1.55 0.558 0.167 0.295 0.0785 0.143 0.247 0.317 3.55 0.107 0.128 2.71 0.503 0.641 0.125 0.180 0.138 0.176 0.0352 0.0439 0.105 0.136 0.108 0.128 0.134 0.214 1.26 1.57 0.462 0.571 0.125 0.180 0.214 0.302 0.0636 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G U

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="14234-35-6" PCl/G UI

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G 2.91 10.0 1.00 21.5 1.23 1.00 21.5 0.139 1.00 21.5 0.0756 0.100 1.00 21.5 0.0968 1.00 21.5 0.191 1.00 21.5 0.163 1.00 21.5 0.149 1.00 21.5 0.702 1.00 21.5 1.12 1.00 21.5 0.139 1.00 21.5 0.279 1.00 21.5 0.0696 1.00 22.5 0.193 1.00 22.5 0.449 0.567 3.91 4.00 1.00 22.5 1.00 22.5 1.00 22.5 0.186 1.00 22.5 0.256 1.00 22.5 2.56 10.0 1.00 22.5 0.988 1.00 22.5 1.11 1.00 22.5 0.117 1.00 22.5 0.146 1.00 22.5 0.063 0.100 1.00 22.5 0.074 0.100 1.00 22.5 0.0715 1.00 22.5 0.0788 1.00 22.5 0.181 1.00 22.5 0.226 1.00 22.5 0.0995 1.00 22.5 0.132 1.00 22.5 0.122 1.00 22.5 0.340 1.00 22.5 0.452 1.00 22.5 0.510 1.00 22.5 0.816 1.00 22.5 1.13 1.00 22.5 0.117 1.00 22.5 0.146 1.00 22.5 0.215 0.242 0.0533 1.00 22.5 1.00 22.5 1.00 22.5

Sample.No. :fYpe 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.2 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.16.R.6 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE

3. 1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.1 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE

3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE SDG""

42387 389296 42405 389296 42325 385070 42340 385070 42325 385070

. 42340 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42367 388092 42387 388092 42381 388092 42381 388092 42367 388092 42387 388092 42381 388092

. Parameter Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Americium-241 Antimony-125 Antimony-125 BETA Area3

Fradion Method.

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA901.1 R

EPA900.0/SW8469310 R

EPA901.1 R

EPA 900.0/SW846 9310 R

EPA901.1 R

EPA 901.1 R

R R

R EPA 901.1 EPA 901.1 EPA 901.1 EPA 901.1 EPA 901.1 EPA901.1 DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 7110B Modified 0.00 0.0248 23.6

-0.489

-8.67

-2.58 31.4

-12.8 0.378 0.318 1.81 0.00

-1.37

-27.9 24.2

-22.7 0.00

-6.8

-0.0672 11.8 0.0605 24.4 0.00 1.05 0.935

-2.82E-05

-0. 112 1.04 1.19 13.0 0.403

. 1.05 1.04 0.426 0.0481

-0.0339 0.0259 10.2 0.0173 0.0422 0.0466 17.9 0.0756

="14913-50-9" PCl/G 0.145 0.173 29.6 1.76 11.0 2.47 54.8 10.9 4.01 4.94 12.7 10.9 11.5 56.9 51.3 22.3 5.92 14.4 0.346 2.94 0.157 2.64 0.727 0.197 0.133 0.0516 0.235 0.154 0.231 1.65 0.712 0.197 0.329 0.0914 0.154 0.182 0.347 3.81 0.0477 0.0675 0.127 3.27 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 14596-10-2 14234-35-6 14234-35-6 12587-47-2 PCl/G UI PCl/G U

PCl/L U

PCl/L UI PCl/L U

PCl/L U

PCl/L UI PCl/L U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G C::RDL c:: Dilut!On.% Moisti.

0.0777 0.140 0.170 55.3 1.00 22.5 1.00 24 1.00 24 1.00 24 3.75 18.0 5.00 1.00 24 1.00 24 4.94 108 5.00 1.00 24 1.00 24 16.5 1.00 24 7.52 9.52 10.0 1.00 24 25.0 12.5 16.9 101 94.5 28.6 6.62 16.0 0.631 3.46 4.00 0.272 3.11 10.0 1.58 0.163 0.0906 0. 100 0.103 0.336 0.142 0.406 0.902 1.23 0.163 0.324 0.0781 0.220 0.336 0.613 3.82 4.00 0.0827 1.00 0.129 0.246 2.92 10.0 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 24 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 24 24 24 24 24 24 24 24 24 24 24 24 24 24 22.8 22.8 22.8 22.8 22.8 22.8 1.00 22.8 1.00

. 22.8 1.00 22.8 1.00 22.8

Saniple No: Type*

3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 3.1.17.R.2 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE Analyzed SDG 42367 388092 42387 388092 42367 388092 42387 388092 42385 388092 42367 388092 42387 388092 42367 388092 42387 388092 42381 388092 42381 388092 42381 388092 42367 388092 42387 388092 42384 388092

,42367 388092 42387 388092 42367 388092 42387 388092 42381 388092 42381 388092 42381 388092 42383 388092 42367 388092 42387 388092 42367 388092 42387 388092 42367 388092 42387 388092 42367 388092 42387 388092 42375 388092 42388 388092 42367 388092 42387 388092 42381 388092 42381 388092 42381 388092 42381 388092 42367 388092 42387 388092 42379 388092 42381 388092

Parameter Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Carbon-14 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 Europium-154 lodine-129 Lead-212 Lead-212 Lead-21,4 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tin-126 Tritium Uranium-232 Area 3 R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA EERF C-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga~01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 905.0 Modified/DOE RP501Rev.1 Modified DOE EML HASL-300, Tc-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified Result 0.00 0.00 0.746 0.814

-0.182 0.773 0.742

-0.000218

-0.00171 0.00 0.0205 0.0155

-0.0157 0.122 0.0568 1.05 1.04 0.841 1.05 0.0424 0.0518 0.031

-6.03 12.5 14.0 0.00 0.00 0.746 0.814 0.965 1.12

-0.298 0.241 0.330 0.293 1.26

-0.0682 1.03 0.848 0.00 0.00 1.27

-0.0392 Uncertainty* CAS 0.624 14913-49-6 1.12 14913-49-6 0.123 0.200 0.783 0.0773 0.107 0.0238 0.0366 0.0385 0.047 0.0436 0.0955 0.136 0.400 0.0862 0.132 0.122 0.215 0.274 0.0673 0.0549 7.26 1.09 1.68 0.411 1.66 0.123 0.200 0.179 0.309 0.841 1.64 0.0473 0.095 0.642 0.158 0.559 0.501 0.0766 0.139 2.46 0.0409 14733-03-0 14733-03-0 14762-75-5 10045-97-3 10045-97-3 10198-40-0 10198-40-0

. OER-100-93 15585-10-1 15585-10-1 15046-84-1 15092-94-1 15092-94-1 15067-28-4 15067-28-4 13994-20-2 13981-16-3 OER-100-70 14119-32-5 13966-00-2 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 10098-97-2 14133-76-7 14913-50-9 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 10028-17-8 14158-29-3 Units Lab,Qu MDL PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G u

0.832 UI 1.27 0.0981 0.162 u

1.34 2.00 0.045 0.100 0.0879 0.100 u

0.0461 u

0.072 PCl/G. U PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G U

PCl/G UI PCl/G U

PCl/G U

0.0573 1.00 0.0745 1.00 0.0465 1.00 0.172 0.293 1.06 1.00 0.0739 0.130 0.0942 0.176 0.560 1.00 0.0957 1.00 0.0832 1.00 12.9 15.0 0.475 0.570 0.710 1.08 0.0981 0.162 0.182 0.293 1.70 2.00 2.84 5.00 0.0465 0.0779 0.449 1.00 0.468 1.00 0.393 1.00 0.212 1.00 0.086 0.165 4.19 6.00 0.142 1.00 D_ilutiori % Moistl 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 22.8 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 22.8 22.8 22.8 22.8 22.8 22.8 22.8 22.8 22.8 22.6 22.8 22.8 22.8 22.8 22.8 22.6 22.8 22.6 22.8 22.6 22.8 22.6 22.8 22.8 22.8 22.6 22.8 22.8 22.8 22.8 22.8 22.6 22.8 22.8

Sample No.* Type*

3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 SAMPLE 3.1.17.R.2 MSD 3.1.17.R.2 MSD 3.1.17.R.2 MS 3.1.17.R.2 MS 3.1.17.R.2 DUP 3.1.17.R.2 DUP 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5. SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE Analyzed SDG 42381 388092 42381 388092 42381 388092 42380 388092 42380 388092 42380 388092 42380 388092 42381 388092 42381 388092 42341 385070 42340 385070 42332 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42332 385070 42332 385070 42332 385070 42341 385070 42340 385070 42341 385070 42341 385070 42331 385070 42331 385070 42331 385070 42333 385070 42341 385070 42341 385070 42341 385070 42341 385070 42340 385070 42337 385070 42341 385070 42332 385070 42332 385070 42332 385070 42332 385070 42341 385070 42340 385070 Parameter Uranium-233/234 Uranium-235/236 Uranium-238 ALPHA BETA ALPHA BETA ALPHA BETA Actinium-227 ALPHA Americium-241 Antimony-125 BETA Bismuth-212 Bismuth-214 Carbon-14 Cesium-137 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 lodine-129 Lead-212 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Protactinium-231 Radium-226 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tritium Area 3 Fraction Method R

DOE EML HASL-300, U-02-RC Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 931 O/SM 7110B Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

R*

R R

R EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL~300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga"01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified DOE EML HASL-300, Tc-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified

Result 0.759 0.0296 0.841 113 118 109 98.6 9.12 16.5

-0.0434 15.2

-0.0175

-0.0629 25.2 0.00 0.800 0.232 1.00 0.00885 0.00 0.0144 0.0417

-0.0489

-0:067 1.10 1.04

-0.0887 0.0726 0.0437

-3.38 13.9 0.00 0.800 0.968

-0.358 1.12 0.352 1.05 0.0144 0.924 1.33 0.00 1.90 Uncertainty GAS Units Lab Qu MDL CRDL "c Dilution % Maish 0.245 13968-55-3/139( PCl/G 0.128 1.00 1.00 22.8 0.0681 0.256 15.4 18.1 11.9 12.6 3.77 2.89 0.269 2.84 0.0406 0.110 2.55 1.09 0.174 0.868 0.114 0.0356 0.0421 0.0647 0.0715 0.137 0.270 0.133 0.183 0.206 0.0919 0.105 6.49 1.52 0.773 0.174 0.302 0.742 1.58 0.073 0.517 0.151 0.439 0.522 0.134 1.91 15117-96-1/139! PCl/G 7440-61-1 PCl/G 12587-46-1 12587-47-2 12587-46-1 12587-47-2 12587-46-1 12587-47-2 14952-40-0 12587-46-1 14596-10-2 14234-35-6 12587-47-2 14913-49-6 14733-03-0 PCl/G PCl/G PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G 14762-75-5 PCl/G U

10045-97-3 PCl/G 10198-40-0 PCl/G U

OER-100-93 PCl/G PCl/G U

PCl/G 15585-10-1 PCl/G U

15046"84-1 PCl/G U

15092-94-1 PCl/G 15067-28-4 PCl/G 13994-20-2 PCl/G U

13981-16-3 PCl/G OER-100-70 PCl/G U

14119-32-5 PCl/G U

13966-00-2 PCl/G.

14331-85-2 PCl/G UI 13982-63-3 PCl/G 15262-20-1 PCl/G 10098-97-2 PCl/G U

14133-76-7 PCl/G U

14913-50-9 PCl/G 14274-82-9 PCl/G 15594-54-4 PCl/G U

14269-63-7 PCl/G 7440-29-1 PCl/G' PCl/G UI 10028-17-8 PCl/G 0.108 0.119 5.40 5.48 4.27 2.65 3.92 2.41 0.489 2.57 0.120 0.199 2.84 0.860 0.126 1.00 1.00 22.8 1.00 1.00 22.8 4.00 1.00 22.6 10.0 1.00 22.6 4.00 1.00 22.6 10.0 1.00 22.6 4.00 1.00 22.6 10.0 1.00 22.6 1.00 22.6 4.00 1.00 22.6 1.00 1.00 22.6 1.00 22.6 10.0 1.00 22.6 1.00 22.6 1.00 22.6 1.48 2.00 1.00 22.6 0.0654 0.100 1.00 22.6 0.0759 1.00 22.6 0.0627 1.00 1.00 22.7 0.126 1.00 1.00 22.7 0.0626 1.00 1.00 22.7 0.255 1.00

22. 7 0.491 1.00 1.00 22.7 0.105 1.00

22. 7 0.341 1.00 22.7 0.609 1.00 1.00

22. 7 0.114 1.00 1.00 22.7 0.190 1.00 1.00 22.7 11.4 15.0 1.00 22.7

0. 732 1.00

22. 7 0.968 1.00 22.7

0.126 1.00 22.7 0.294 1.00

22. 7 1.53 2.00 1.00

22. 7 2.67 5.00 1.00

22. 7 0.0627 1.00 22.7 0.501 1.00 1.00 22.7 0.314 1.00 1.00 22.7 0.154 1.00 1.00 22.7 0.154 1.00 1.00 22.7 0.137 1.00 22.7 3.14 6.00 1.00 22.7

Sample No. Type 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.5 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 SAMPLE 3.1.17.R.6 3.1.17.R.6 3.1.17.R.6 3.1.17.R.6 3.1.17.R.6 3.1.18.R.1 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42332 385070 42332 385070 42332 385070 42332 385070 42341 385070 42340 385070 42332 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42332 385070 42332 385070 42332 385070 42341 385070 42340 385070.

42341 385070 42341 385070 42331 385070 42331 385070 42331 385070 42333 385070 42341 385070 42341 385070 42341 385070 42341 385070 42340 385070 42337 385070 42341 385070 42332 385070 42332 385070 42332 385070 42332 385070 42341 385070 42340 385070 42332 385070 42332 385070 42332 385070 42332 385070 42341 385070 Parameter Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Actinium-227 ALPHA Americium-241 Antimony-125 BETA Bismuth-212 Bismuth-214 Carbon-14 Cesium-137 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246 Europium-154 lodine-129 Lead-212 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Protactinium-231 Radium-226 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Actinium-227 Area 3

Fraction Method R

DOE EML HASL-300, U-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4:5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA EERF C-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300,1-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

R

~

R R

R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified DOE EML HASL-300, Tc-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.0135 1.05 0.0456 0.956 0.0212 12.0

-0.00355

-0.00335 22.6 0.00 0.634

-0.435 0.661

-0.015 0.00 0.000584 0.186

-0.0303

-0.0593 1.13 1.05

-0.181

-0.00502

-0.0301

-3.4 13.6 0.00 0.634 0.00

-0.244 1.73 0.258 1.41

-0.0111 0.773 1.08 0.00

-0.0268 0.0643 1.20 0.110 0.767 0.103 Uncertainty GAS

Units Lab Qu MDL CRDL C Dilution. % MoistL 0.0953 14158-29-3 PCl/G u

0.196 1.00 1.00 22.7 0.329 0.0897 0.312 0.279 3.12 0.0306 0.116 2.41 0.669 0.133 0.836 0.111 0.0369 0.0341 0.0433 0.115 0.122 0.280 0.130 0.194 0.189 0.0433 0.0486 7.08 1.48 0.524 0.133 0.275 0.623 1.69 0.0808 0.530 0.0957 0.385 0.452 0.130 1.65 0.0953 0.361 0.121 0.289 0.301 13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 14952-40-0 12587-46-1 14596-10-2 14234-35-6 12587-47-2 14913-49-6 14733-03-0 14762-75-5 10045-97-3 10198-40-0 OER-100-93 15585-10-1

. 15046-84-1 15092-94-1 15067-28-4 PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G u

u u

UI u

u u

x u

u 13994-20-2 PCl/G U

13981-16-3 PCl/G U

OER-100-70 PCl/G U

14119-32-5 PCl/G U

13966-00-2 PCl/G 14331-85-2 PCl/G UI 13982-63-3 PCl/G 15262-20-1 PCl/G UI 10098-97-2 PCl/G U

14133-76-7 PCl/G 14913-50-9 PCl/G 14274-82-9 PCl/G 15594-54-4 PCl/G U

14269-63-7 PCl/G 7440-29-1 PCl/G PCl/G UI 10028-17-8 PCl/G 14158-29-3 PCl/G 13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 14952-40-0 PCl/G u

u 0.143 0.124 1.00 1.00 22.7 1.00 1.00 22.7 0.0775 1.00 0.529 3.98 4.00 0.0708 1.00 0.187 2.84 10.0 1.30 0.118 1.45 2.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 0.0858 0.100 1.00 22.7 22.7 22.7 22.7 22.7 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 0.0681 1.00 0.0508 1.00 1.00 0.0963 1.00 1.00 0.0507 1.00 1.00 0.229 1.00 0.554 1.00 0.112 0.342 0.656 1.00 0.100 1.00 0.155 1.00 12.4 15.0 0.719 1.09 0.118 0.550 1.31 2.00 2.82 5.00 0.0782 0.336 1.00 0.222 1.00 0.221 1.00 0.255 1.00 0.159 3.19 6.00 0.139 1.00 0.131 1.00 0.0824 1.00 0.0822 1.00 0.588 1.00 1.00 1.00 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 22.4 1.00 1.00 1.00 1.00 1.00 1.00 22.4 22.4 22.4 22.4 22.4 22.4

.:/

Sample No:* Type*

3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.1 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE Analyzed:

SDG ~**

42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 Parameter"

ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Area3 F'raction Method R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3!Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R

.. Result*

7.56 0.00129 23.5 0.00 0.866 1.12 0.00 0.00261 0.773 0.978 11.8 0.367 0.866 1.04 0.291 0.00

-0.253 0.00 11.5 0.0375

-0.0409 17.3 0.00 0.00 0.704 0.799 1.89 1.83

-0.0257 0.019 0.0103

-0.0126 0.948 0.985 0.685 0.923 12.1 11.1 0.385 0.00 0.704 0.799 1.16 Uncertainty. GAS CRDLC Dilution % MoistL 2.42 12587-46-1 PCl/G 3.21 4.00 1.00 22.4 0.121 2.39 0.661 0.181 0.127 0.0372 0.116 0.156 0.184 1.49 0.587 0.181 0.279 0.107 0.244 0.334 0.314 3.28 0.134 0.135 2.52 0.710 0.807 0.181 0.183 0.172 0.160 0.0502 0.0421 0.140 0.129 0.133 0.135 0.205 0.230 1.42 1.54 0.787 0.924 0.181 0.183 0.349 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G PCl/G UI

="14952-40-0" PCl/G U

="14952-40-0" PCl/G UI

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G 0.227 2.63 10.0 1.33 0.167 0.0633 0.100 0.0807 0.229 0.173 0.332 0.717 1.11 0.167 0.306 0.065 0.251 0.569 0.634 3.91 4.00 0.257 0.240 2.77 10.0 1.09 1.43 0.163 0.165 0.0808 0.100 0.0837 0.100 0.0877 0.0844 0.270 0.250 0.133 0.123 0.186 0.187 0.593 0.661 1.29 1.23 0.163 0.165 0.304 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 22.4 22.4 22.4 22.4 22.4 22.4 22.4 22.4 22.4 22.4 22.4 22.4 22.4 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 18.3 19.4 19.4 19.4 19.4 19.4 19.4 19.4 19.4 19.4 19.4 19.4 19.4

~ample No. Type 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.18.R.2 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.1 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2. SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 42387 389296 42405 389296 42387 389296 42405 389296 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42395 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296

\\ Parameter Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Area.3*

~rattion Meth9d.

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R" R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 1.05 0.248 0.333 0.00 0.0199

-0.00874 14.7

-0.0461 19.9 0.00 0.779 1.07

-0.00812 2.92E-05 1.10 0.970 12.9 0.00 0.779 1.02 0.325 0.00

-0.116 0.0926 7.32

-0.00536 0.060 17.8 0.00 0.00 0.849 0.722 1.51 1.46 0.0135

-0.0033

-0.108 0.0518 1.17 0.818 0.967 1.22 14.0 Uncertainty* CP.,S:: *

Lab Ou MDL 0.301

="15262-20-1" 0.0833

="14913-50-9" 0.0799 0.139 0.195 0.244 3.57 0.0992 2.73 0.746 0.132 0.109 0.0401 0.111 0.127 0.202 1.41 0.559 0.132 0.277 0.0871 0.139 0.279 0.307 3.21 0.119 0.138 3.00 0.810 1.19 0.161 0.197 0.129 0.152 0.035 0.0361 0.104 0.163 0.131 0.231 0.186 0.207 1.58

="14913-50-9" PCl/G 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G 0.340 0.088 0.0783 0.192 0.193 0.468 3.83 4.00 0.177 3.13 10.0 1.21 0.111.

0.0739 0.100 0.0765 0.211 0.111 0.137 0.581 0.891 0.111 0.263 0.0669 0.133 0.498 0.597 3.70 4.00 0.214 0.266 2.86 1.29 1.78 0.124 0.175 10.0 0.0771 0.100 0.0917 0.100 0.0755 0.0752 0.166 0.339 0.126 0.157 0.160 0.391 0.710 QJlutiqn % MoistL 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 19.4 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 21.9 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1

sar'npleNo. * :rype 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.19.R.2 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2. E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.1 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42387 389296 42405 389296 42341 385077 42339 385077 42341 385077 42339 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42339 385077 42339 385077 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA

. *Area 3 Frai.:tion Method....

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified Result 13.7 0.00

-0.00463 0.849 0.722 0.898 1.19 0.222 0.335 0.00 0.00

-0.191 17.0

-0.0535 28.1 0.00 0.908 1.29 1.29 0.0116 0.0116 0.0344 0.0344 1.21 1.18 17.0 0.740 0.00 0.908 0.908 1.13 1.13 0.407 0.0958 0.0958

-0.095

-0.095 21.1 21.1

-0.141

-0.141 27.8 27.8 Uncertainty GAS*.

Units l:.aq.Qu MDL 1.74

="13966-00-2" PCl/G 0.721 0.912

="14331-85-2" PCl/G UI 0.923 0.664

="14331-85-2" PCl/G u

1.16 0.161

="13982-63-3" PCl/G 0.197 0.347 0.267 0.0855 0.105 0.120 0.134 0.425 2.33 0.173 1.79 1.19 0.289 0.178 0.178 0.0694 0.0694 0.189 0.189 0.190 0.257 2.32 1.31 1.31 0.289 0.289 0.469 0.469 0.125 0.170 0.170 0.430 0.430 2.71 2.71 0.169 0.169 1.76 1.76

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

=""

14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-.1 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 12587-46-1 14234-35-6 14234-35-6 12587-47-2 12587-47-2 PCl/G UI PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G 0.124 0.175 0.286 0.344 0.0724 0.0929 0.154 0.200 0.725 2.32 0.313 1.65 2.54 0.232 0.140 0.140 0.148 0.148 0.399 0.399

' 0.188 0.481 1.01 1.36 1.36 0.232 0.232 0.550 0.550 0.105 0.240 0.240 0.680 0.680 2.94 2.94 0.277 0.277 1.75 1.75 CRDL C Djli.Jtiori.%. Moistl 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 1.00 22.1 4.00 1.00 22.1 1.00 22.1 10.0 1.00 22.1 1.00 18.1 1.00 18.1 0.100 1.00 22.1 0.100 1.00 18.1 1.00 22.1 1.00 18.1 1.00 22.1 1.00 18.1 1.00 18.1 1.00 18.1 1.00 18.1 1.00 22.1 1.00 18.1 1.00 22.1 1.00 18.1 1.00 22.1 1.00 18.1 1.00 18.1 1.00 22.1 1.00 18.1 1.00 18.1 1.00 16.6 4.00 1.00 18.1 4.00 1.00 16.6 1.00 18.1 1.00 16.6 10.0 1.00 18.1 10.0 1.00 16.6

sample No.

Type,'

3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.2 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2. E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.2.E.4 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE Analyzed

, SDG.

42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077" 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 "42341 385077 42341 385077 42341 385077 42341 385070 42340 385070 Parameter.

Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA

, Area 3 F~actioh f'0ethod* >

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01"R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 7110B Modified Result 2.21 1.22 2.83

-0.0139

-0.131 1.38 1.44 16.9 0.00 1.22 1.31 0.358 0.00 0.0258 0.0258 15.4 15.4 0.0434 0.0434 26.5 26.5 0.00 1.06 0.111 0.00

-0.00513

-0.0586

-0.0586 1.35 1.19 17.5 0.00 0.00 1.06 1.06 1.41 1.41 0.419 0.00 0.00

-0.0414 15.1

. Uncertainty GAS 0.893 14913-49-6 0.231 14733-03-0 0.202 10045-97-3 0.0613 0.183 0.164 0.272 2.05 1.12 0.231 0.373 0.117 0.167 0.374 0.374 2.07 2.07 0.129 0.129 1.88 1.88 0.816 0.188 0.0628 0.0628 0.0445 0.0445 0.159 0.159 0.161 0.210 2.06 1.30 1.30 0.188 0.188 0.325 0.325 0.112 0.184 0.184 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 12587-46-1 14234-35-6 14234-35-6 12587-47-2 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2

14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 0.268 14952-40-0 3.49 12587-46-1 Units PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G U

PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G-U PCl/G CRDL c Dilutiori % Moistt 1.39 1.00 16.6 0.173 1.00 16.6 0.0876 0.100 1.00 16.6 0.116 1.00 16.6 0.318 1.00 16.6 0.159 1.00 16.6 0.223 1.00 16.6 1.16 1.00 16.6 1.32 1.00 16.6 0.173 1.00 16.6 0.363 1.00 16.6 0.0943 1.00 16.6 0.178 1.00 16.6 0.618 1.00 16.6 0.618 1.00 100 2.11 4.00 1.00 16.6 2.11 4.00 1.00 100 0.244 0.244 2.13 10.0 2.13 10.0 1.66 0.170 1.00 1.00 1.00 1.00 1.00 1.00 16.6 100 16.6 100 100 100 0.134 0.100 1.00 16.6 0.134 0.100 1.00 100 0.0869 0.0869 0.289 0.289 0.138 0.178 1.04 1.17 1.17 0.170 0.170 0.315 0.315 0.0828 0.184 0.184 0.502 3.10 4.00 1.00 16.6 1.00 100 1.00 16.6 1.00 100 1.00 100 1.00 100 1.00 100 1.00 16.6 1.00 100 1.00 100 1.00 21 1.00 100 1.00 21 1.00 21 1.00 100 1.00 21 1.00 21 1.00 21

Sample No. Type 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.20.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.1 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE Analyzed

SDG 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070

. 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 Parameter Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL.300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.0855 21.6 0.00 0.833 0.414 0.0164 0.0284 1.02 1.00 12.5 0.326 0.833 1.03 0.309 0.00 0.181 8.73

-0.0507 23.0 0.427 0.649 0.824

-0.00202 0.0258 1.33 0.942 13.0 0.232 0.649 0.857 0.257 0.00

-0.0269

-0.128 13.3 0.0419

-0.127 24.1 0.00 0.00 0.824 0.733 1.02 Uncertainty GAS

Units Lab Qu MDL CRDL C Dilution % MoistL 0.0966 14234-35-6 PCl/G U

0.196 1.00 21 2.76 0.844 0.172 0.089 0.0362 0.128 0.137 0.211 1.39 0.607 0.172 0.249 0.0722 0.123 0.316 2.97 0.113 3.05 0.688 0.195 0.112 0.038 0.163 0.146 0.189 1.41 0.665 0.195 0.408 0.0692 0.127 0.308 0.236 4.01 0.135 0.111 3.57 0.938 0.887 0.185 0.167 0.153 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G 15262-20-1 PCl/G 14913-50-9 PCl/G PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G 3.03 10.0 1.24 0.143 0.0777 0.100 0.078 0.256 0.128 0.326 0.685 0.921 0.143 0.234 0.0634 0.162 0.601 3.65 4.00 0.206 3.31 10.0 1.33 0.161 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 21 21 21 21 21 21 21 21 21 21 20.6 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 0.086 0.100 1.00 20.6 0.0739 0.272 0.125 0.164 0.449 1.09 0.161 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 0.270 1.00 20.6 0.0679 1.00 20.6 0.171 1.00 20.6 0.569 1.00 20.6 0.430 1.00 20.6 3.78 4.00 1.00 20.6 0.254 1.00 20.6 0.181 1.00 20.6 3.40 10.0 1.00 20.6 1.39 1.50 0.166 0.145 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 0.100 0.100 1.00 20.6

Sample No. Type Analyzed SDG 3.1.21.R.2 SAMPLE 42405 389303 3.1.21.R.2 SAMPLE 42387 389303 3.1.21.R.2 SAMPLE 42405 389303 3.1.21.R.2 SAMPLE 42387 389303 3.1.21.R.2 SAMPLE 42405 389303 3.1.21.R.2 SAMPLE 42387 389303 3.1.21.R.2 SAMPLE 42405 389303 3.1.21.R.2 SAMPLE 42387 389303 3.1.21.R.2 SAMPLE 42405 389303 3.1.21.R.2 SAMPLE 42387 389303 3.1.21.R.2 SAMPLE 42405 389303 3.1.21.R.2 SAMPLE 42387 389303 3.1.21.R.2 SAMPLE 42405 389303 3.1.21.R.2 SAMPLE 42387 389303 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2.

SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 SAMPLE 3.1.21.R.2 MSD 3.1.21.R.2 MSD 3.1.21.R.2 MS 3.1.21.R.2 MS 3.1.21.R.2 DUP 3.1.21.R.2 DUP 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 3.1.22.R.1 SAMPLE 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42395 389303 42395 389303 42395 389303 42395 389303 42395 389303 42395 389303 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 Parameter Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 ALPHA BETA ALPHA BETA ALPHA BETA Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 9310/SM 71108 Modified EPA 900.0/SW846 931 O/SM 71108 Modified EPA 900.0/SW846 931 O/SM 71108 Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 71108 Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 71108 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 1.24

-0.026

-0.038

-0.0303 0.0486 0.977 1.07 0.875 0.908 11.8 12.3 0.202 1.05 0.824 0.733 0.769 0.835 0.326 0.309 0.0757 0.00 92.4 114 86.4 113 15.0 23.6

-0.051 14.9 0.0519 25.4 0.00 0.875 1.15

-0.00936

-0.0211 1.02 0.971 11.4 0.00 0.875 0.927 0.293 Uncertainty CAS Units lab Qu MDL CRDL C Dilution % MbistL 0.122

="10045-97-3" PCJ/G 0.0765 0.100 1.00 20.6 0.0503

="10198-40-0" PCl/G u

0.0928 1.00 20.6 0.0351 0.129 0.139 0.134 0.116 0.182 0.148 1.67 1.44 0.680 0.787 0.185 0.167 0.313 0.307 0.0958 0.0688 0.192 0.131 13.5 16.9 14.2 18.1 4.68 3.53 0.245 3.20 0.0931 3.09 0.763 0.143 0.121 0.0338 0.110 0.123 0.194 1.35 0.795 0.143 0.258 0.0704

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCJ/G.

PCJ/G U

PCl/G UI

="12587-46-1"

="12587-47-2"

="12587-46-1"

="12587-47-2"

="12587-46-1" PCl/G

="12587-47-2" PCl/G 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCJ/G PCl/G UI PCl/G PCl/G PCl/G 0.0529 0.251 0.259 0.136 0.100 0.342 0.153 0.701.

0.681 1.14 0.841 0.166 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 1.00 20.6 0.145 1.00 20.6 0.333 1.00 20.6 0.224 1.00 20.6 0.0754 1.00 20.6 0.0771 1.00 20.6 0.232 1.00 20.6 0.113 1.00 20.6 5.74 4.00 1.00 20.6 5.17 10.0 1.00 20.6 7.29.

4.00 1.00 20.6 4.95 10.0 1.00 20.6 3.83 4.00 1.00 20.6 2.89 10.0 0.455 2.53 4.00 0.181 3.20 10.0 1.13 0.117 0.0595 0.100 0.0641 0.180 0.103 0.129 0.618 0.872 0.117 0.245 0.059 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 20.6 21 21 21 21 21 21 21 21 21 21 21 21 21 21 21 21

Sample No. Type 3.1.22.R.1 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 SAMPLE 3.1.22.R.2 MSD 3.1.22.R.2 MSD 3.1.22.R.2 MSD 3.1.22.R.2 MSD 3.1.22.R.2 MS 3.1.22.R.2 MS 3.1.22.R.2 MS 3.1.22.R.2 MS 3.1.22.R.2 DUP 3.1.22.R.2 DUP Analyzed SDG" 42341 385070 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303.

42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42395 389303 42395 389296 42395 389303 42395 389296 42395 389303 42395 389296 42395 389303 42395 389296 42387 389303 42405 389303 Parameter Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 ALPHA ALPHA BETA BETA ALPHA ALPHA BETA BETA Actinium-227 Actinium-227 Area3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

R EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00 0.0982 0.133 16.8

-0.0112

-0.0714 30.8 0.00 0.475 0.529 0.821 1.27 1.37

-0.04 0.0299

-0.0655

-0.0619 0.832 0.891 0.815 0.774 12.9 11.8 0.505 0.00 0.529 0.821 1.14 1.02 0.284 0.359 0.00 0.00 107 107 108 108 103 103 105 105

-0.173 0.0353 Uncertainty CAS Units Lab Qu MDL 0.109 PCl/G UI 0.133 0.337

="14952-40-0" PCl/G U

0.637 0.371

="14952-40-0" PCl/G U

0.693

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14913-49-6" PCl/G U

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" - PCl/G U

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G PCl/G UI PCl/G UI 3.86 0.233 0.277 2.56 1.49 1.83 0.170 0.195 0.101 0.111 0.0861 0.140 0.289 0.285 0.169 0.172 0.195 0.224 0.593 1.21 1.26 1.44 0.170 0.195 0.265 0.319 0.0937 0.0914 0.200 0.186 6.31 6.31 3.72 3.72 5.72 5.72 CRDL C Dilution % MoistL 1.00 21 1.00 21 1.00 21 4.00 1.00 21 1.00 21 1.00 21 10.0 1.00 21 1.00 21 1.00 21 1.00 21 1.00 21 0.100 1.00 21 0.100 1.00 21 1.00 21 1.00 21 1.00 21 1.00 21 1.00 21 1.00 21 1.00 21 1.00 21 1.00 21 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 1.00 20.5 4.00 1.00 19.8 4.00 1.00 19.8 10.0 1.00 19.8 10.0 1.00 19.8 4.00 1.00 19.8 4.00 1.00 19.8 4.32 0.123 0.154 3.49 0.771 1.08 0.192 0.239 0.155 0.178 0.052 0.0619 0.162 0.148 0.174 0.182 0.223 0.230 1.59 1.97 1.05 0.720 0.192 0.239 0.354 0.449 0.0985 0.119 0.143 0.168" 14.2 14.2 14.3 14.3 14.3 14.3 14.9 14.9 0.321 0.293

="12587-46-1"

="12587-47-2"

="12587-46-1"

="12587-47-2"

="14952-40-0" PCl/G U

3.43 10.0 1.00 19.8 3.43 10.0 1.00 19.8 0.566 1.00 20.5 0.539 1.00 20.5

Sample No. Type 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP

3.1.22.R.2 DUP 3.1.22.R.2. DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.22.R.2 DUP 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE Analyzed SDG 42395 389303 42395 389296 42387 389303 42405 389303 42395 389303 42395 389296 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 Parameter ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Fraction Method R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

R R

R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 12.5 12.5 0.00239

-0.16 22.2 22.2 0.00 0.00 0.698 0.639 1.29 1.40

-0.00598 0.011

-0.0667

-0.0101 0.810 0.780 1.07 0.832 13.0 12.7 0.0839 0.00 0.698 0.639 0.876 1.10 0.308 0.232 0.0469 0.00

-0.0379 12.4 0.000438 22.8 1.73 0.855 1.39 0.0434 0.00 1.11 1.16 Uncertainty CAS Units Lab Qu MDL CRDL Dilution % MoistL 3.81

="12587-46-1" PCl/G 3.84 4.00 1.00 19.8 3.81

="12587-46-1" PCl/G 3.84 4.00 1.00 19.8 0.134 0.126 2.90 2.90 0.761 0.646 0.153 0.174 0.142 0.129 0.0353 0.0487 0.167 0.157 0.129 0.144 0.208 0.194 1.62 1.57 0.664 0.753 0.153 0.174 0.265 0.319 0.0785 0.0966 0.165 0.0683 0.295 3.09 0.130 3.44 1.34 0.189 0.155 0.0402 0.168 0.130 0.236

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 PCl/G U

PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G 1.00 20.5 1.00 20.5 0.242 0.210 2.39 10.0 1.00 19.8 2.39 10.0 1.37 1.30 0.143 0.153 0.0835 0.100 0.0786 0.100 0.0704 0.0984 0.255 0.298 0.134 0.153 0.342 0.160 0.568 0.701 1.14 0.943 0.143 0.153 0.238 0.277 0.0623 0.0872 0.182 0.0835 0.556 2.55 4.00 0.250 4.23 10.0 1.05 0.175 0.116 0.100 0.104 0.373 0.120 0.180 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 19.8 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 20.5 19.8 20.5 19.8 20.5 19.8 19.8 19.8 13.6 13.6 13.6 13.6 13.6 13.6 13.6 13.6 13.6

Sample No: Type 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.1 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE

. 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.23.R.2 SAMPLE 3.1.24.R.1 SAMPLE 3.1.24.R.1 SAMPLE 3.1.24.R.1 SAMPLE 3.1.24.R.1 SAMPLE 3.1.24.R.1 SAMPLE 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42341 385070

- 42340 385070 42341 385070 42340 385070 42341 385070 Parameter*

Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimciny-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212

Area 3 Fraction Method<-

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 14.1 0.407 0.855 0.797 0.361 0.00

-0.00968 0.0473 14.4

-0.0441 0.0162 24.2 0.00 0.00 0.727 0.875 1.79 1.64 0.0229 0.00501

-0.0362

-0.0201 0.822 1.03.

0.785 0.958 12.4 13.7 0.394 0.00 0.727 0.875 1.00" 0.921 0.283 0.290 0.00 0.0186 0.200 12.4

-0.0283 21.2 0.809

- Uncertainty CAs: -

1.82 13966-00-2 PCl/G PCl/G U

PCl/G PCl/G PCl/G 0.672 0.189 0.383 0.104 0.0769 0.302 0.305 4.45 0.115 0.118 3.26 0.929 0.793 0.161 0.175 0.152 0.161 0.0394 0.0408 0.119 0.136 0.181 0.136 0.194 0.241 1.42 1.69 0.870 0.851 0.161 0.175 0.279 0.288 0.0923 0.0749 0.116 0.156 0.247 3.69 0.0879 3.25 0.648 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G MDL CRDL c Dilution % MoistL 1.06 1.00 13.6 1.18 0.175 0.355 0.0873 1.00 1.00 1.00 1.00 13.6 13.6 13.6 13.6 0.136 1.00 13.6 0.562 1.00 13.6 0.583 1.00 13.6 3.91 4.00 1.00 13.6 0.204 1.00 13.6 0.222 1.00 13.6 2.30 10.0 1.00 13.6 1.26 1.00 13.6 1.35 1.00 13.6 0.144 1.00 13.6 0.181 1.00 13.6 0.0824 0.100 1.00 13.6 0.0903 0.100 1.00 13.6 0.0864 1.00 13.6 0.086 1.00 13.6 0.222 1.00 13.6 0.265 1.00 13.6 0.157 1.00 13.6 0.131 1.00 19.9 0.324 1.00 19.9 0.356 1.00 19.9

0. 760 J.00 19.9 0.677 1.00 19.9 1.07 1.00 19.9 1:18 1.00 19.9 0.144 1.00 19.9 0.181 1.00 19.9 0.222 1.00 19.9 0.277 1.00 19.9 0.0789 1.00 19.9 0.0767 1.00 19.9 0.0981 1.00 19.9 0.211 1.00 19.9 0.480 1.00 19.9 3.42 4.00 1.00 19.9 0.161 1.00 21 3.39 10.0 1.00 21 0.762 1.00 21

Type.

Analyzed SDG.

SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.1 SAMPLE 42341 385070 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42395 389303

_3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42395 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 3.1.24.R.2 SAMPLE 42405 389303 3.1.24.R.2 SAMPLE 42387 389303 Parameter Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium~231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Area3 Fraction Method*.

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R

.Result 0.939 1.65 0.0239

-0.0407 1.01 1.12 13.7 0.155 0.939 0.868 0.218 0.00 0.108

-0.0852 11.5

-0.0309 0.0205 22.3 0.00 0.402 0.686 0.857 1.53 1.56 0.0154 0.0153 0.0257

-0.0163 0.939 1.04 0.801 1.15 13.2 13.7

-0.0837 0.00 0.686 0.857 0.732 1.24 0.322 0.284 0.00 Uncertaihfy GAS...

tJi)its.

0.133 14733-03-0 PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G 0.120 10045-97-3 0.031 10198-40-0 0.110 15585-10-1 0.121 15092-94-1 0.168 1.25 0.552 0.133 0.242.

0.0745 0.134 0.363 0.315 3.78 0.142 0.128 3.36 0.788 0.772 0.211 0.198

.0.168 0.170 0.0505 0.053 0.135 0.130 0.144 0.144 0.258 0.213 1.56 1.64 0.838 0.607 0.211 0.198 0.301 0.353 0.0872 0.109 0.213 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14913-49-6" PCl/G U

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

=""

PCl/G UI CRDL C Dilution %. MoisU 0.115 1.00 21 0.0529 0.100 1.00 21 0.0651 1.00 21 0.194 1.00 21 0.0984 1.00 21 0.121 1.00 21 0.562 1.00 21 0.897 1.00 21 0.115 1.00 21 0.205 1.00 21 0.063 1.00 21 0.128 1.00 21 0.655 1.00 21 0.579 1.00 21 3.87 4.00 1.00 21 0.257 1.00 21 0.239 1.00 21 3.35 10.0 1.00 21 1.44 1.00 21 1.36 1.00 21 0.162 1.00 21 0.151 1.00 21 0.100 0.100 1.00 21 0.096 0.100 1.00 21 0.0934 1.00 21 0.108 1.00 21 0.273 0.252 0.144 0.126 0.180 0.373 0.740 0.392 1.33 1.16 0.162 0.151 0.306 0.339 0.0821 0.0776 0.215 1.00 21 1.00 21 1.00 21 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4 1.00 23.4

Sample No.* Type 3.1.24.R.2 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.24.R.6 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.1 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 3.1.3.E.2 3.1.3.E.2 3.1.3.E.2 SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42405 389303

. 42325 385070 42341 385070 42325 385070 42341 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42341 385077 42339 385077 42341 385077 42339 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42339 385077 42341 385077 42339 385077 42341 385077 42341 385077 Parameter Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactiniumc231 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Area 3

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 901.1 R

EPA 900.0/SW846 9310 R

EPA901.1 R

EPA 900.0/SW846 9310 R

EPA901.1 R

EPA 901.1 R

EPA901.1 R

EPA 901.1 R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

R R

R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.0515

-10.6

-1.8 0.696 0.222 44.1 0.00

-1.85 3.35

-5.74 6.17 0.00

-46.1 27.1

-16.5 0.00 4.94

-0.199 14.3

-0.0166 22.1 0.00 1.04 1.24 0.00584

-0.084 1.31 1.20 15.1 0.908 0.00 1.04 1.20.

1.20 0.383 0.0841 0.00

-0.187 18.0

-0.016 28.5 0.00 1.05 Uncertainty CAS 0.135 26.8 14952-40-0 1.22 12587-46-1 10.5 14234-35-6 2.57 12587-47-2 63.5 14913-49-6 16.8 14733-03-0 4.78 10045-97-3 4.73 10198-40-0 11.7 15585-10-1 9.46 15092-94-1 12.9 15067-28-4 57.9 13966-00-2 51.0 14331-85-2 20.6 15262-20-1 7.38 14913-50-9 11.4 0.287 14952-40-0 2.07 12587-46-1 0.119 14234-35-6 1.44 12587-47-2 0.763 0.174 0.122 0.0434 0.147 0.135 0.189 1.53 0.773 0.773 0.174 0.265 0.265 0.0777 0.131 0.131 0.402 2.24 0.140 2.05 0.996 0.224 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 Units Lab Qu MDL CRDL C Dilution % Moistl PCl/G U

0.206 1.00 23.4 PCl/L U

47.1 1.00 23.4 PCl/L U

3.58 5.00 1.00 23.4 PCl/L U

19.0 1.00 23.4 PCl/L U

4.69 5.00 1.00 23.4 PCl/L U

108 1.00 23.4 PCl/L UI 17.1 1.00 23.4 PCl/L U

7.89 10.0 1.00 23.4 PCl/L U

9.47 1.00 23.4 PCl/L U

19.6 1.00 23.4 PCl/L U

13.5 1.00 23.4 PCl/L UI 15.2 1.00 23.4 PCl/L U

89.9 1.00 23.4 PCl/L U

94.5 1.00 23.4 PCl/L U

29.9 1.00 22.6 PCl/L UI 6.70 1.00 22.6 PCl/L U

19.4 1.00 22.6 PCl/G U

0.513 1.00 22.6 PCl/G 2.38 4.00 1.00 22.6 PCl/G U

0.215 1.00 22.6 PCl/G 1.20 10.0 1.00 22.6 PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G 1.39 1.00 22.6 0.155 1.00 22.6 0.0719. 0.100 1.00 22.6 0.0865 1.00 22.6 0.259 1.00 22.6 0.117 1.00 22.6 0.162 1.00 22.6 0.471 1.00 22.6 0.975 1.00 22.6 0.975 1.00 22.6 0.155 1.00 22.6 0.230 1.00*

22.6 0.230 1.00 28.2 0.0737 1.00 28.2 0.140 1.00 22.6 0.140 1.00 28.2 0.623 1.00 28.2 2.30 4.00 1.00 28.2 0.255 1.00 28.2 2.51 10.0 1.00 28.2 1.71 1.00 28.2 0.171 1.00 28.2

Sample No. Type 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 "SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.2 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 3.1.3.E.4 3.1.3.E.4 3.1.3.E.4 SAMPLE SAMPLE SAMPLE SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 SAMPLE 3.1.3.E.4 MSD 3.1.3.E.4 MSD Analyzed SDG 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42339 385077 42339 385077 Parameter Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 ALPHA ALPHA Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 9310/SM 71108 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 931 O/SM 7110B Modified Result 1.54 0:013

-0.0145 1.42 1.23 14.7 0.543 1.05 1.33 1.33 0.406 0.00723 0.00723

-0.0286

-0.0286 12.8 12.8

-0.0962

-0.0962 26.0 26.0 0.00 0.904 0.178 0.178

-0.0268

-0.0528

-0.0528 1 :16 1.07 16.2 0.00 0.00 0.904 0.904 1.14 1.14 0.281 0.111 0.00 122 122 Uncertainty CAS 0.159 10045-97-3 0.0499 0.151 0.164 0.249 1.69 0.790 0.224 0.358 0.358 0.124 0.193 0.193 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 15262-20-1 14913-50-9 0.359 14952-40-0 0.359 14952-40-0 1.84 12587-46-1 1.84 12587-46-1 0.141 0.141 1.75 1.75 0.990 0.230 0.091 0.091 0.0478 0.0478 0.167 0.167 0.146 0.254 2.02 0.719 0.719 0.230 0.230 0.351 0.351 0.115 0.172 0.172 5.99 5.99 14234-35-6 14234-35-6 12587-47-2 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262"20-1 15262-20-1 14913-50-9 12587-46-1 12587-46-1 Units Lab Qu MDL CRDL C Dilution % MoistL PCl/G 0.121 0.100 1.00 28.2 PCl/G U

0.101 1.00 28.2 PCl/G U

0.287 1.00 28.2 PCl/G 0.153 1.00 28.2 PCl/G 0.435 1.00 28.2 PCl/G 0.866 1.00 28.2 PCl/G U

1.36 1.00 28.2 PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI 0.171 0.334 0.334 0.0998 0.279 0.279 0.669 0.669 1.79 1.79 0.241 0.241 1.00 28.2 1.00 28.2 1.00 17.1 1.00 17.1 1.00 28.2 1.00 17.1 1.00 17.1 1.00 19.5 4.00 1.00 17.1 4.00 1.00 19.5 1.76 10.0 1.00 1.00 1.00 17.1 19.5 17.1 19.5 1.76 10.0 1.00 1.69 1.00 19.5 0.183 1.00 19.5 0.0874 0.100 1.00 17.1 0.087 4 0.100 1.00 19.5 0.0858 1.00 17.1 0.0858 1.00 19.5 0.310 1.00 17.1 0.310 1.00 19.5 0.132 1.00 19.5 0.160 1.00 19.5 1.13 1.00 19.5 0.873 1.00 17.1 0.873 1.00 19.5 0.183 1.00 17.1 0.183 1.00 19.5 0.286 1.00 17.1 0.286 1.00 19 0.0769 1.00 19 0.194 1.00 17.1 0.194 1.00 19 2.58 4.00 1.00 19.5 2.58 4.00 1.00 19

Sample No. Type*

3.1.3.E.4 MSD 3.1.3.E.4 MSD 3.1.3.E.4 3.1.3.E.4 3.1.3.E.4 3.1.3.E.4 3.1.3.E.4 3.1.3.E.4 3.1.3.E.4 3.1.3.E.4 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R 1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R 1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.1 3.1.4.R.2 3.1.4.R.2 3.1.4.R.2 3.1.4.R.2 3.1.4.R.2 MS MS MS MS DUP DUP DUP DUP SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42339 385077 42339 385077 42339 385077 42339 385077 42339 385077 42339 385077 42339 385077 42339 385077 42339 385077 42339 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 Parameter BETA BETA ALPHA ALPHA BETA BETA ALPHA ALPHA BETA BETA Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-2'26 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Area 3 Fraction Method R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

R EPA 900.0/SW846 931 O/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R Result..

111 111 108 108 106 106 13.4 13.4 22.0 22.0

-0.09

-0.09 11.5 11.5 0.0478 0.0478 20.8 20.8 0.520 0.728 0.762 0.762 0.0209 0.0209

-0.0107

-0.0107 0.942 1.19 10.9 0.363 0.363 0.728 0.728 0.871 0.871 0.280 0.00 0.00

-0.115

-0.115 14.7 14.7

-0.0339 Uncertainty CAS 6.33 12587-47-2 6.33 5.71 5.71 6.31 6.31 2.36 2.36 1.71 1.71 0.281 0.281 1.87 1.87 0.0998 0.0998 1.99 1.99 0.726 0.192 0.0927 0.0927 0.0434 0.0434 0.105 0.105 0.158 0.181 1.39 0.832 0.832 0.192 0.192 0.277 0.277 0.0734 0.201 0.201 0.277 0.277 2.08 2.08 0.106 12587-47-2 12587-46-1 12587-46-1 12587-47-2 12587-47-2 12587-46-1 12587-46-1 12587-47-2 12587-47-2 14952-40-0 14952-40-0 12587-46-1 12587-46-1 14234-35-6 14234-35-6 12587-47-2 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 14952-40-0 14952-40-0 12587-46-1 12587-46-1 14234-35-6 Units Lab Qu MDL 1.81 1.81 2.82 2.82 2.13 2.13 PCl/G 2.88 PCl/G 2.88 PCl/G 1.86 PCl/G 1.86 PCl/G U

0.522 PCl/G U

0.522 PCl/G 2.13 PCl/G 2.13 PCl/G U

0.194 PCl/G U

0.194 PCl/G 2.65 CRDL C Dilution % MoistL 10.0 1.00 19.5 10.0 1.00 19 4.00 1.00 17.1 4.00 1.00 19 10.0 1.00 19.5 10.0 1.00 19 4.00 1.00 17.1 4.00 1.00 19 10.0 1.00 17.1 10.0 1.00 19 4.00 4.00 10.0 1.00 19 1.00 19.4 1.00 1.00 1.00 19 19.4 19 1.00 19.4 PCl/G PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PClfG* U PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

2.65 10.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 19 21.9 21.9 21.9 19 21.9 19 21.9 19 21.9 21.9 21.9 21.9 19 21.9 19.4 21.9 19.4 21.9 21.9 19.4 21.9 21.9 18 21.9 18 21.9 1.27 0.135 0.0697 0.100 0.0697 0.100 0.0901 0.0901 0.204 0.204 0.163 0.339 0.760 0.835 0.835 0.135 0.135 0.275 0.275 0.0732 0.164 0.164 0.490 0.490 2.16 4.00 2.16 4.00 0.189

I I L Sample No. Type Analyzed SDG 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42339 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3.1.4.R.2 SAMPLE 42341 385077 3".1.4.R.2 SAMPLE 42341 385077 3.1.4.R.4 SAMPLE 42341 385077 3.1.4.R.4 SAMPLE 42341 385077 3.1.4.R.4 SAMPLE 42339 385077 3.1.4.R.4 SAMPLE 42339 385077 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 3.1.4.R.4 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 Parameter Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-228 Thallium-208 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HAS!:. 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result

-0.0339 22.7 0.00 0.810 1.13 0.00591

-0.0405 1.07 1.06 14.7 0.754 0.00 0.810 0.810 1.07 1.07 0.301 0.00 0.00 0.00799 0.00799 13.1 13.1

-0.0256

-0.0256 20.2 20.2 0.00 0.792 0.821 0.821

-0.0101

-0.0101 0.0182 0.0182 1.13 1.13 13.0 0.492 0.00 0.792 0.752 0.290 Uncertainty CAS 0.106 14234-35-6 1.71 0.527 0.159 0.120 0.0347 0.107 0.115 0.175 1.20 0.767 0.767 0.159 0.159 0.241 0.241 0.0761 0.124 0.124 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 0.257 14952-40-0 0.257 14952-40-0 1.89 12587-46-1 1.89 12587-46-1 0.0984 0.0984 1.42 1.42 0.607 0.145 0.0951 0.0951 0.0312 0.0312 0.122 0.122 0.123 0.184 1.37 0.496 0.496 0.145 0.322 0.086 14234-35-6 14234-35-6 12587-47-2 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 Units Lab Qu MDL CRDL C Dilution % MoistL PCl/G U

0.189 1.00 18 PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G 1.82 1.09 10.0 1.00 1.00 18 18 0.128 1.00 18 0.0632 0.100 1.00 18 0.0673 1.00 18 0.194 1.00 18 0.0972 1.00 100 0.301 1.00 100 0.591 1.00 100 0.787 1.00 18 0.787 1.00 100 0.128 1.00 18 0.128 1.00 100 0.223 1.00 18 0.223 1.00 100 0.058 1.00 100 0.140 1.00 18 0.140 1.00 100 0.482 1.00 100 0.482 1.00 22.3 2.05 4.00 1.00 100 2.05 4.00 1.00 22.3 0.176 1.00 0.176 1.00 1.35 10.0 1.00 1.35 10.0 1.00 1.17 1.00 0.141 1.00 0.064 0.100 1.00 0.064 0.100 1.00 0.0591 1.00 0.0591 1.00 0.213 1.00 0.213 1.00 0.106 1.00 0.141 1.00 0.531 1.00 0.981 1.00 0.981 1.00 0.141 1.00 0.202 1.00 0.0647 1.00 100 22.3 100 22.3 22.3 22.3 100 22.3 100 22.3 100 22.3 22.3 22.3 22.3 100 22.3 22.3 22.3 22.3

Sample No. Type,,

3.1.4.R.4 SAMPLE 3.1.5.R.1 3.1.5.R.1 3, 1,5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3:1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.1 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 3.1.5.R.2 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42341 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42339 385077 42339 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 Parameter Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Area 3 '

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R, DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900".0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.00

-0.259

-0.259 12.5 12.5 0.0106 0.0106 20.5 20.5 0.00 0.795 1.11 1.11

-0.00027

-0.00027 0.0226 0.0226 1.11 1.10 13.3 0.296 0.296 0.795 0.992 0.329 0.121 0.00 0.061

-0.212 13.4

-0.00818 0.0975 25.8 0.00 0.00 0.699 0.817 0.978 0.940 0.00 0.0112

-0.0832

-0.0645 Uncertainty GAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.111 PCl/G UI 0.118 1.00 22.3 0.351 14952-40-0 PCl/G U

0.614 1.00 22.3 0.351 14952-40-0 PCl/G U

0.614 1.00 22.4 1.91 12587-46-1 PCl/G 2.08 4.00 1.00 22.3 1.91 12587-46-1 PCl/G 2.08 4.00 1.00 22.4 0.114 0.114 1.65 1.65 0.882 0.155 0.124 0.124 0.0429 0.0429 0.125 0.125 0.138 0.189 1.54 0.650 0.650 0.155 0.301 0.0898 0.142 0.142 0.240 0.336 4.47 0.120.

0.120 3.69 0.561 0.852 0.153 0.160 0.0991 0.140 0.0351 0.0396 0.118 0.119 14234-35-6 14234-35-6 12587-47-2 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G UI

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

0.210 0.210 1.82 10.0 1.82 10.0 1.36 0.140 0.0731 0.100 0.0731 0.100 0.0851 0.0851 0.253 0.253 0.127 0.350 0.476 1.19 1.19 0.140 0.239 0.0621 0.201 0.201 0.446 0.522 3.86 4.00 0.189 0.245 2.84 10.0 1.13 1.42 0.130 0.139 0.0759 0.100 0.0887 0.100 0.0747 0.0874 0.203 0.224 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 22.3 22.4 22.3 22.4 22.4 22.4 22.3 22.4 22.3 22.4 22.3 22.4 22.4 22.4 22.4 22.3 22.4 22.4 22.4 22.4 22.4 22.4 22.4 22.4 22.4.

22.4 22.4 22.4 22.4 22.4 23 23 23 23 23 23 23 23

Sample No. Type 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1 :5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.2 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6.

SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.5.R.6 SAMPLE 3.1.6.R.1 3.1.6.R.1 3.1.6.R.1 3.1.6.R.1 3.1.6.R.1 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE Analyzed SDG 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42325 385077 42340 385077 42325 385077 42340 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42341 385077 42340 385077 42341 385077 42340 385077 42341 385077 Parameter Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium~137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Area 3 Fractiori Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 901.1 R

EPA 900.0/SW846 9310 R

R R

EPA 901.1 EPA 900.0/SW846 9310 EPA 901.1 EPA 901.1 EPA 901.1 EPA 901.1 EPA901.1 EPA901.1 EPA 901.1 EPA 901.1 EPA 901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA 901.1 EPA 901.1 EPA 901.1 DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.840 0.858 0.600 0.765 12.4 10.5 0.00 0.206 0.699 0.817 0.679 0.944 0.236 0.246 0.00 0.00

-4.01

-1.45 3.43 1.44 29.7 0.00

-0.0607

-0.0607 1.75 1.75

-5.67 "5.67 0.00 5.84

-72.3

-13.1

-8.91

-8.91 0.00

-8.53

-0.13 10.8

-0.0274 15.3 0.00 Uncertainty CAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.133

="15092-94-1" PCl/G 0.127 0.133

="15092-94-1" PCl/G 0.123

="15067-28-4" PCl/G

=" 13966-00-2" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G UI

="14331-85-2" PCl/G U

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G PCl/G UI PCl/G UI PCl/L U

1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 1.0Q 23 1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 0.143 0.205 1.32 1.57 0.605 0.631 0.153 0.160 0.219 0.283 0.0672 0.0759 0.107 0.164 28.1 1.49 9.89" 2.10 64.9 12.0 4.50 4.50 4.04 4.04 11.5 11.5 10.0 10.2 52.1 54.3 54.3 19.5 19.5 7.47 10.7 10.7 0.243 4.44 0.0904 3.82 0.750 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 15262-20-1 15262-20-1 14913-50-9 PCl/L U

0.129 0.154 0.461 1.02 1.04 1.10 0.130 0.139 0.248 0.278 0.0567 0.0807 0.118 0.177 50.1 4.10 18.1 5.00 1.00 23 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 PCl/L. U PCl/L U

PCl/L U

PCl/L UI PCl/L U

PCl/L U

PCl/L UI PCl/L U

PCl/L U

PCl/L UI PCl/L U

PCl/L U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI 3.60 5.00 113 17.8 7.34 10.0 7.34 10.0 8.20 8.20 20.3 20.3 15.5 17.2 87.6 88.1 88.1 27.6 27.6 5.79 15.9 15.9 0.438 3.79 4.00 0.165 4.05 10.0 1.08 1.00 23 1.00 23 1.00 23 1.00 23 1.00 23 1.00 21.4 1.00 23 1.00 21.4 1.00 23 1.00 21.4 1.00 21.4 1.00 21.4 1.00 21.4 1.00 23 1.00 21.4 1.00 23 1.00 21.4 1.00 21.4 1.00 23 1.00 21.4 1.00 21.4 1.00 21.4 1.00 21.4 1.00 21.4 1.00 21.4

Sample No. Type Analyzea SDG 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6. R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.1 SAMPLE 42341 385077 3.1.6.R.2 SAMPLE 42387 389303 3.1.6.R.2 SAMPLE 42405 389303 3.1.6.R.2 SAMPLE 42395 389303 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2

.3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 3.1.6.R.2 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 Parameter Bismuth-214 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

R.

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.731 1.04 0.0352 0.00 0.117 0.00 0.992 0.937 13.3 0.00 0.00 0.731 0.731 0.685 0.685 0.241 0.135 0.00

-0.0238

-0.211 10.8 0.074

-0.03 30.2 1.16 1.06 0.573 0.718 2.74 2.52 0.0276

-0.0168

-0.0267

-0.053 0.967 0.938 0.752 0.899 12.2 11.8 0.00 0.00 0.573 Uncertainty-CAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.168 14733-03-0 PCl/G PCl/G 0.092 10045-97-3 0.033 0.033 0.115 0.115 0.120 0.167 1.13 0.743 0.743 0.168 0.168 0.290 0.290 0.0711 0.146 0.146 0.303 0.335 3.83 0.107 0.152 3.66 0.744 0.658 0.214 0.206 0.174 0.190 0.0326 0.043 0.087 0.103 0.128 0.139 0.186 0.266 1.31 1.49 0.812 1.05 0.214 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 PCl/G U

PCl/G UI PCl/G U

PCl/G UI PCl/G PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G PCl/G PCl/G PCl/G PCl/G U

PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G UI

="14331-85-2". PCl/G UI

="13982-63-3" PCl/G 0.121 1.00 21.4 0.0633 0.100 1.00 21.4 0.071 0.071 0.212 0.212 0.104 0.257 0.380 0.764 0.764 0.121 0.121 0.237 0.237 0.052 0.168 0.168 1.00 21.4 1.00 21.6 1.00 21.4 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.4 1.00 21.6 1.00 21.4 1.00 21.6 1.00 21.4 1.00 21.6 1.00 21.6 1.00 21.4 1.00 21.6 0.555 1.00 21.6 0.605 1.00 21.6 3.85 4.00 1.00 21.6 0.208 1.00 0.277 1.00 2.21 10.0 1.00 0.890 1.00 1.02 1.00 0.126 1.00 0.154 1.00 0.0702 0.100 1.00 0.0834 0.100 1.00 0.0754 1.00 0.079 1.00 0.167 1.00 0.186 1.00 0.117 1.00 0.140 1.00 0.168 1.00 0.190 1.00 0.564 1.00 0.747 1.00 0.918 1.00 1.19 1.00 0.126 1.00 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6 21.6

. 21.6 21.6 21.6 21.6

Sample No. Type 3.1.6.R.2 SAMPLE 3.1.6.R.2 SAMPLE 3.1.6.R.2 SAMPLE 3.1.6'.R.2 SAMPLE 3.1.6.R.2 SAMPLE 3.1.6.R.2 SAMPLE 3.1.6.R.2 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1. 7.R.1

.SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3:1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.1 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE 3.1.7.R.2 SAMPLE Analyzed SDG 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42341 385077 42340 385077 42341 385077 42340 385077 42340 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 Parameter Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 ALPHA Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Area 3 Fraction Method *.

R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R

.R DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.718 0.551 0.916 0.206 0.202 0.00 0.0902 0.0425 10.1 0.0725' 25.2 25.2 0.00 0.942 1.17 1.17

-0.000285

-0.0842

-0.0842 1.17 1.12 16.0 0.938 0.00 0.942 0.942 0.00 0.00 0.357 0.138 0.00 0.200

-0.0459 19.5

-0.000137

-0.0724 25.7 0.00 0.00 0.965 1.02 0.998 Uncertainty CAS Units Lab Qu MDL' 0.206

="13982-63-3" PCl/G

0. 154 0.340

="15262-20-1" PCl/G 0.227 0.327 0.0722 0.0999 0.104 0.210 0.316 3.56 0.144 3.50 3.50 0.753 0.208 0.175 0.175 0.0565 0.0565 0.154 0.154 0.150 0.206 1.93 0.752 0.752 0.208 0.208 0.380 0.380 0.0877 0.154 0.154 0.325 0.384 6.16 0.137 0.166 4.32 2.11 1.02 0.217 0.201 0.139

="15262-20-1" PCl/G

="14913-50-9" PCl/G

=""

14952-40-0 12587-46-1 14234-35-6 12587-47-2 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 13982-63-3 15262-20-1 15262-20-1 14913-50-9 PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G UI PCl/G PCl/G PCl/G UI PCl/G UI PCl/G PCl/G U

PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G 0.369 0.0576 0.0903 0.121 0.232 0.610 3.48 0.275 2.93 2.93 1.64 0.181 0.103 0.103 0.109 0.109 0.269 0.269 0.136 0.179 0.874 1.13 1.13 0.181 0.181 0.697 0.697 0.0897 0.196 0.196 0.634 0.706 3.54 0.261 0.289 2.98 2.33 1.76 0.169 0.185 0.120 CRDL C Dilution % Moistl 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 1.00 21.6 4.00 1.00 21.6 1.00 21.6 10.0 1.00 21.6 10.0 1.00 20 1.00 20 1.00 20 0.100 1.00 21.6 0.100 1.00 20 1.00 21.6 1.00 20 1.00 21.6 1.00 20 1.00 20 1.00 20 1.00 20 1.00 21.6 1.00 20 1.00 21.6 1.00 20 1.00 21.6 1.00 20 1.00 20 1.00 21.6 1.00 20 1.00 20 1.00 20 4.00.

1.00 20 1.00 20 1.00 20 10.0 1.00 20 1.00 20 1.00 20 1.00 20 1.00 20 0.100 1.00 20

Sample No. Type Analyzed SDG 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1. 7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.7.R.2 SAMPLE 42387 389303 3.1.7.R.2 SAMPLE 42405 389303 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42340 385077 3.1.8.R.1 SAMPLE 42340 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42340 385077 3.1.8.R.1 SAMPLE 42340 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE.

42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 3.1.8.R.1 3.1.8.R.1 SAMPLE SAMPLE SAMPLE 42341 385077 42341 385077 42341 385077 Parameter..

Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40

Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactini um-231 Radium-226 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.869

-0.0154 0.00 0.0277 0.0647 1.13 1.24 1.34 1.21 15.4 18.7 0.316 0.00 0.965 1.02 0.00 1.30 0.449 0.481 0.00 0.00

-0.078

-0.078 10.1 10.1 0.0462 0.0462 21.3 21.3 0.00 1.14 0.952 0.952 3.29E-05 3.29E-05 0.179 0.179 1.27 1.09 13.9 0.529 0.529 1.14 Uncertainty GAS Units Lab Qu MDL CRDL C Dilution % Moistt 0.142

="10045-97-3" PCl/G 0.0688

="10198-40-0" PCl/G u

UI 0.0633 0.351 0.211 0.168 0.215 0.240 0.233 2.20 2.13 0.692 0.904 0.217 0.201 0.378 0.394 0.126 0.101 0.093 0.204 0.285 0.285 3.17 3.17 0.131 0.131 3.21 3.21 0.876 0.210 0.137 0.137 0.0705 0.0705 0.184 0.184 0.141 0.235 1.94 0.632 0.632 0.210

="10198-40-0" PCl/G

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G UI

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G 14952-40-0 14952-40-0 12587-46-1 12587-46-1 14234-35-6 14234-35-6 12587-47-2 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 10198-40-0 15585-10-1 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 14331-85-2 13982-63-3 PCl/G UI PCl/G UI PCl/G U

PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G 0.0946 0.100 1.00 20 0.131 0.134 0.570 0.418 0.153 0.233 0.452 0.209 0.699 0.882 1.31 1.24 0.169 0.185 0.901 0.305 0.120 0.0966 0.115 0.230 0.530 0.530 1.00 20 1.00 20 3.60 4.00 3.60 4.00 0.260 0.260 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 3.97 10.0 1.00 3.97 10.0 1.00 1.69 1.00 0.167 1.00 0.105 0.100 1.00 0.105 0.100 1.00 0.137 1.00 0.137 1.00 0.412 1.00 0.412 0.118 0.165 1.29 1.14 1.14 0.167 1.00 1.00 1.00 1.00 1.00 1.00 1.00 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 18.4 100 18.4 100 18.4 100 18.4 18.4 18.4 100 18.4 100 18.4 100 18.4 18.4 18.4 18.4 100 18.4 18.4

Sample No. Type Analyzed SDG 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.1 SAMPLE 42341 385077 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42395 389303 3.1.8.R.2.

SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42395 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.2 SAMPLE 42387 389303 3.1.8.R.2 SAMPLE 42405 389303 3.1.8.R.6 SAMPLE 42325 385077 3.1.8.R.6 SAMPLE 42325 385077 3.1.8.R.6 SAMPLE 42340 385077 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 42340 385077 42325 385077 42325 385077 42340 385077 42340 385077 Parameter Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA Bismuth-212 Bismuth-212.

Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactini um-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-~1-R R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA901.1 R

EPA 900.0/SW846 9310 R

R R

EPA 900.0/SW846 9310 EPA 901.1 EPA901.1 EPA 900.0/SW846 931 O EPA 900.0/SW846 9310 Result 0.961 0.420 0.00 0.0509

-0.115 17.8

-0.0439 0.0577 27.8 1.48 0.00 0.781 0.981 0.850 0.972 0.00527

-0.052 0.0161

-0.126 0.963 1.16 0.830 0.927 14.6 14.8 0.0933 0.00 0.781 0.981 0.937 1.14 0.273 0.334 0.00 0.00

-7.35

-0.394

-0.394 8.29 8.29

-1.74

-1.74 Uncertainty CAS Units Lab Qu MDL CRDL C Dilution % Moistt 0.351 15262-20-1 PCl/G PCl/G 0.0846 14913-50-9 0.0975 0.338 0.295 4.94 0.123 0.119 4.00 0.799 1.49 0.194 0.184 0.128 0.117 0.0459 0.0493 0.169 0.147 0.162 0.133 0.231 0.217 1.78 1.70 0.678 0.566 0.194 0.184 0.300 0.321 0.0878 0.0856 0.167 0.0946 31.7 31.7 1.37 1.37 12.4 12.4 2.37 2.37 PCl/G UI

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G

="14913-49-6" PCl/G

="14913-49-6" PCl/G UI

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G 14952-40-0 14952-40-0 12587-46-1 12587-46-1 14234-35-6 14234-35-6 12587-47-2 12587-47-2 PCl/G UI PCl/G UI PCl/L U

PCl/L U

0.434 0.0906 1.00 18.4 1.00 18.4 0.111 1.00 18.4 0.643 1.00 18.4 0.538 1.00 18.4 3.88 4.00 1.00 18.4 0.220 1.00 18.4 0.228 1.00 18.4 3.97 10.0 1.00 18.4 1.11 1.00 18.4 1.53 1.00 18.4 0.176 1.00 24.2 0.135 1.00 24.2 0.100 0.100 1.00 24.2 0.0796 0.100 1.00 24.2 0.0961 1.00 24.2 0.0775 1.00 24.2 0.332 1.00 24.2 0.244 0.140 0.115 0.377 0.167 0.864 0.815 1.28 1.05 0.176 0.135 0.277 0.320 0.0999 0.0717 0.222 0.189 54.9 54.9 3.12 5.00 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 24.2 1.00 22.3 1.00 24.2 3.12 5.00 1.00 22.3 18.6 1.00 24.2 18.6 1.00 22.3 4.71 5.00 1.00 24.2

4. 71 5.00 1.00 22.3

3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.8.R.6 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1.

SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.1 SAMPLE 3.1.9.E.2 SAMPLE 3.1.9.E.2 SAMPLE 3.1.9.E.2 SAMPLE 3.1.9.E.2 SAMPLE 3.1.9.E.2 SAMPLE 3.1.9.E.2 SAMPLE Analyzed

. SDG 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42341 385077 42341 385077 42340 385077 42340 385077 42341 385077 42341 385077 42340 385077 42340 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42341 385077 42387 389303 42405 389303 42395 389303 42387 389303 42405 389303 42395 389303 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA ALPHA Antimony-125 Antimony-125 BETA BETA Bismuth-212 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 Antimony-125 BETA

Area 3.

Eracti6r:t Method*.*

R EPA901.1 R

EPA901.1 R

R R

R EPA901.1 EPA901.1 EPA 901.1 EPA 901.1 EPA 901.1 EPA 901.1 EPA901.1 EPA 901.1 EPA901.1 EPA901.1 DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified

ResulL 3.83 1.15 4.62 14.5 7.04 0.00 7.04

-0.837 4.13

-1.9 13.0 0.176 11.4 3.31 14.5

-82.5 68.0

-3.47 60.2 0.00 23.7 0.00 5.64 1.41 13.8

-0.0975 0.329

-0.0975 0.329 14.9 4.08 14.9 4.08 0.0871 0.106 0.0871 0.106 11.6 2.53 11.6 2.53 2.21 0.853 0.883 0.203 1.36 0.157 1.36 0.157 0.0466 0.0506 0.0466 0.0506

-0.113 0.130 1.19 0.151 1.21

. 0.233 15.7 1.72 1.18 0.829 0.00 0.829 0.883 0.203 1.26 0.361 0.398 0.104 0.109 0.122 0.0559 0.302 0.262 0.399 16.8 4.88 0.0655 0.127 0.0925 0.121 28.2 4.16 Units

Lab.Ou MDL, **. CRDL C Dilutii:iri %.MoistL 14913-49-6 14733-03-0 10045-97-3 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 15262-20-1 14913-50-9 PCl/L PCl/L PCl/L u

121 1.00 22.3 u

16.0 1.00 22.3 u

PCl/L UI PCl/L U

PCl/L U

PCl/L UI PCl/L UI PCl/L U

14952-40-0 PCl/G U

12587-46-1 PCl/G 12587-46-1 PCl/G 14234-35-6 PCl/G U

14234-35-6 PCl/G U

12587-47-2 PCl/G 12587-47-2 PCl/G 14913-49-6 PCl/G 14733-03-0 PCl/G 10045-97-3

PCl/G 10045-97-3 PCl/G 10198-40-0 PCl/G U

10198-40-0 PCl/G U

15585-10-1 PCl/G U

15092-94-1 PCl/G 15067-28-4 PCl/G 13966-00-2 PCl/G 14331-85-2 PCl/G U

. 14331-85-2 PCl/G UI 13982-63-3 PCl/G 15262-20-1 PCl/G 14913-50-9 PCl/G PCl/G U

="14952-40-0" PCl/G U

="12587-46-1" PCl/G

="14234-35-6" PCl/G U

="12587-47-2" PCl/G 7.68 10.0 1.00 22.3 7.68 10.0 1.00 22.3 6.41 1.00 22.3 23.7 1.00 22.3 14.2 1.00 22.3 18.0 1.00 22.3 112 1.00 22.3 105 1.00 22.3 24.8 1.00 22.3 9.62 1.00 22.3 16.6 1.00 22.3 0.608 1.00 22.3 0.608 1.00 100 3.69 4.00 1.00 22.3 3.69 4.00 1.00 1 OD 0.218 1.00 22.3 0.218 1.00 100 2.58 10.0 1.00 22.3 2.58 10.0 1.00 100 1.16 1.00 100 0.148 1.00 100 0.105 O: 1 DO 1.00 22.3 0.105 0.100 1.00 100 0.114 1.00 22.3 0.114 1.00 100 0.219 1.00 100 0.148 1.00 100 0.417 1.00 100 0.607 1.00 1 OD 1.24 1.00 100 1.24 1.00 100 0.148 1.00 100 0.319 1.00 100 0.0853 1.00 1 OD 0.236 1.00 1 DO 0.574 1.00 100 0.740 1.00 100 3.80 4.00 1.00 1 DO 0.244 1.00 1 OD 0.302 1.00 22.1 3.88 10.0 1.00 22.1

3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.2 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 3.1.9.E.6 Type SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 3.1.9.E.6 SAMPLE 3.1.9.E.6 SAMPLE 3.1.9.E.6 SAMPLE 3.1.9.E.6 SAMPLE 3.1.9.E.6 SAMPLE 3.1.9.E.6 SAMPLE Analyzed SDG 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42387 389303 42405 389303 42325 385077 42325 385077 42340 385077 42325 385077 42340 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 42325 385077 Paramete.r Bismuth-212 Bismuth-212 Bismuth-214 Bismuth-214 Cesium-137 Cesium-137 Cobalt-60 Cobalt-60 Europium-154 Europium-154 Lead-212 Lead-212 Lead-214 Lead-214 Potassium-40 Potassium-40 Protactinium-231 Protactinium-231 Radium-226 Radium-226 Radium-228 Radium-228 Thallium-208 Thallium-208 Tin-126 Tin-126 Actinium-227 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-228 Thallium-208 Tin-126

. Area 3.

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA901.1 R

EPA 900.0/SW846 9310 R

EPA901.1 R

EPA 900.0/SW846 9310 R

EPA901.1 R

EPA 901.1 R

EPA901.1 R

EPA 901.1 R

EPA901.1 R

R R

R EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA901.1 Result 0.00 0.00 0.829 1.21 1.93 1.85

-0.023

-0.0121 0.0206

. 0.0468 1.32 1.35 1.05 1.09 14.1 15.3 0.320 0.00 0.829 1.21 1.10 1.23 0.341 0.305 0.00 0.00 27.4 0.00

-1.65

-2.19

-0.673

-25 4.82 1.37 0.608

-8.62 0.00

-1.34

-43

-68.4 0.986

-5.06

-7.98 Uncertainty* CAS

Units

L.ab.Q1:l' MQl, CRDL c Dilution, % MoistL 0.708

="14913-49-6" PCl/G UI 1.45 1.00 22.1 1.86

="14913-49-6" PCl/G U I 1.68 1.00 22.1 0.186 0.196 0.157 0.178 0.0511 0.0506 0.131 0.187 0.140 0.171 0.194 0.259 1.60 1.71 0.791 0.896 0.186 0.196 0.271 0.339 0.0967 0.116 0.140 0.152 29.8 29.8 1.19 9.90 1.72 64.8 14.4 4.00 4.26 11.1 12.7 10.1 52.8 57.1 21.4 5.07 11.7

=" 14 733-03-0" PCl/G

="14733-03-0" PCl/G

="10045-97-3" PCl/G

="10198-40-0" PCl/G U

="15585-10-1" PCl/G U

="15092-94-1" PCl/G

="15067-28-4" PCl/G

="13966-00-2" PCl/G

="14331-85-2" PCl/G U

="14331-85-2" PCl/G UI

="13982-63-3" PCl/G

="15262-20-1" PCl/G

="14913-50-9" PCl/G

="14913-50-9" PCl/G 14952-40-0 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 15262-20-1 14913-50-9 PCl/G UI PCl/G UI PCl/L U

PCl/L UI PCl/L U

PCl/L U

PCl/L UI PCl/L U

PCl/L U

0.165 1.00 22.1 0.210 1.00 22.1 0.0947 0.100 1.00 22.1 0.113 0.100 1.00 22.1 0.076 1.00 22.1 0.0933 1.00 22.1 0.255 1.00 22.1 0.320 1.00 22.1 0.126 1.00 22.1 0.162 1.00 22.1 0.353 1.00 22.1 0.221 1.00 22.1 0.970 1.00 22.1 0.853 1.00 22.1 1.15 1.00 22.1 1.31 1.00 22.1 0.165 1.00 22.1 0.210 1.00 22.1 0.253 1.00 22.1 0.329 1.00 22.1 0.0729 1.00 22.1 0.104 1.00 22.1 0.144 0.196 1.00 22.1 1.00 22.1 54.8 1.00 54.8 1.00 3.74 5.00 1.00 17.7 1.00 3.58 5.00 1.00 100 1.00 12.9 1.00 7.47 10.0 1.00 8.12 1.00 18.5 1.00 11.1 1.00 100 100 100 100 100 100 100 100 100 100 100 15.9 88.5 90.0 28.5 8.21 17.6 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00.

100

Sample No. Type 3.2.1.R.1 SAMPLE 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.1 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1".R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 3.2.1.R.5 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 3.2.1.R.5 SAMPLE Analyzed SDG 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42340 385070 42332 385070 42341 385070 42340 385070 42341 385070 42341 385070 42342 385070 42341 385070 42341 385070 42332 385070 42332 385070 42332 385070 42341 385070 42340 385070 42341 385070 42341 385070 42331 385070 42331 385070 42331 385070 42333 385070 42341 385070 42341 385070 42341 385070 42341 385070 42340 385070 Parameter Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Americium-241 Antimony-125 BETA Bismuth-212 Bismuth-214 Carbon-14 Cesium-137 Cobalt-60 Curium-242 Curium-243/244 Curium-245/246

Europium-154 lodine-129 Lead-212 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Protactini um-231 Radium-226 Radium-228 Strontium-90 Area~

Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

R R

DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE EML HASL-300,l-01Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R ASTM C 1476-00 Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Result

-0.125 14.7 0.0292 22.9 0.723 0.641 0.468 0.00212

-0.00831 1.21 0.983 14.3 0.00 0.641 0.856 0.343 0.00

-0.16 13.7

-0.0163

-0.00147 22.9 0.00 0.886

-0.282 0.543 0.0104

-0.0152 0.00697 0.0775

. -0.0576

-0.109 0.986 0.997

-0.083 0.0398

-0.0223

-0.504 13.8 0.00 0.886 0.664

-0.702 Uncertainty CAS 0.289 14952-40-0 4.11 12587-46-1 0.120 3.59 1.05 0.190 0.126 0.0502 0.157 0.144 0.215 1.80 0.585 0.190 0.261 0.109 0.177 0.283 4.03 0.0308 0.105 2.95 0.889 0.155 0.648 0.0972 0.0271 0.0351 0.0387 0.0748 0.136 0.287 0.129 0.167 0.157 0.0682 0.076 6.04 1.49 0.607 0.155 0.346 0.599 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14596-10-2 14234-35-6 12587-47-2 14913-49-6 14733-03-0 14762-75-5 10045-97-3 10198-40-0 OER-100-93 15585-10-1 15046-84-1 15092-94-1 15067-28-4 13994-20-2 13981-16-3 OER-100-70 14119-32-5 13966-00-2 14331-85-2 13982-63-3 15262-20-1 10098-97-2 Units Lab Qu MDL CRDL.C Dilution % MoistL PCl/G U

0.536 1.00 26.1 PCl/G 3.45 4.00 1.00 26.1 PCl/G U

PCl/G PCl/G U

PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G X

PCl/G U

PCl/G PCl/G PCl/G U

PCl/G PCl/G U

PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

0.229 3.73 10.0 1.65 0.166 0.0895 0.100 0.099 0.300 0.126 0.173 0.609 1.19 0.166 0.377 0.074 0.189 0.488 3.88 4.00 0.0951 1.00 0.198 2.20 10.0 1.48 0.149.

1.11 2.00 0.0808 0.100 0.0653 0.104 1.00 0.0743 1.00 0.0465 1.00 0.242 0.447 1.00 0.114 0.154 0.485 1.00 0.0597 1.00 0.188 1.00 10.5 15.0 0.603 1.10 0.149 0.272 1.38 2.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 26.1 1.00 26.1

l Sample No. Type 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.5 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 SAMPLE 3.2.1.R.6 3.2.1.R.6 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 3.2.2.R.1 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE

. Analyzed SDG 42337 385070 42341 385070 42332 385070 42332 385070 42332 385070 42332 385070 42341 385070 Parameter Technetium-99 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 42340 385070 Tritium 42332 385070 Uranium-232 42332 385070 Uranium-233/234 42~32 385070 Uranium-235/236 42332 385070 Uranium-238 42325 385070 Actinium-227 42340 385070 ALPHA 42325 385070 Antimony-125 42340 385070 BETA 42325 385070 1 Bismuth-212 42325 385070 Bismuth-214 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42325 385070 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Area 3

Fraction Method R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

R R

,R R

R R

DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 906.0 Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified DOE EML HASL-300, U-02-RC Modified EPA901.1 EPA 900.0/SW846 9310 EPA901.1 EPA 900.0/SW846 9310 EPA901.1 EPA901.1 EPA901.1 EPA901.1 EPA 901.1 EPA901.1 EPA 901.1 EPA 901.1 EPA 901.1 EPA 901.1 EPA901.1 EPA901.1 DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 1.88 0.303 0.992

-0.0684 1.16 0.663 0.064 1.88

-0.0077 0.738 0.159 1.09 6.77

-0.452

-4.08 2.79 8.13 0.00 2.65

-2.49

-7.84 4.34 0.00

-25 30.0 13.2 0.00

-6.92 0.128 12.6 0.0566 18.5 0.00 0.964 0.597

-0.0062 0.0739 0.992 1.13 14.5 0.00 0.964 1.00 Uncertainty GAS Units Lab Qu MDL CBDL C Dilution % Mbistt 1.70 14133-76-7 PCl/G PCl/G PCl/G PCl/G U

0.0876 0.587 0.279 0.606 0.431 0.128 2.06 0.0532 0.260 0.127 0.312 23.6 1.39 8.38 2.91 46.7 12.9 3.72 3.56 11.2 9.59 12.2 44.4 57.5 23.9 4.65 8.98 0.281 3.79 0.112 2.88 1.30 0.175 0.0934 0.0496 0.163 0.161 0.191 1.67 0.728 0.175 0.332 14913-50-9 14274-82-9 15594-54-4 14269-63-7 7440-29-1 10028-17-8 14158-29-3 PCl/G PCl/G PCl/G U

PCl/G PCl/G U

13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 14952-40-0 12587-46-1 14234-35-6 PCl/L U

PCl/L U

12587-47-2 PCl/L 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 PCl/L U

PCl/L UI PCl/L U.

PCl/L U

PCl/L UI PCl/L U

PCl/L U

PCl/L UI PCl/L U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G 2.83 5.00 1.00 26.1 0.0665 1.00 26.1 0.663 1.00 0.659 1.00 0.629 1.00 0.349 1.00 0.162 3.43 6.00 0.129 1.00 0.126 1.00 0.0683 1.00 0.0681 1.00 43.6 3.15 5.00 14.3 4.83 5.00 88.3 12.1 7.33 6.15 16.2 11.8 15.3 79.5 80.4 31.1 5.82 12.5 0.532 10.0 3.83 4.00 0.219 2.64 10.0 1.38 0.136 0.0888 0.100 0.0942 0.327 0.158 0.165 0.518 0.939 0.136 0.293 1.00 26.1 1.00 26.1 1.00 26.1 1.00 26.1 1.00 26.1 1.00 26.1 1.00 26.1 1.00 26.1' 1.00 26.1 1.00 26.1 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 100 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 100 100 100 100 100 24.3 24.3 24.3 24.3 24.3 24.3 24.3 24.3 24.3 24.3 24.3 24.3 24.3 24.3 24.3

Sample No. Type 3.2.2.R.1 SAMPLE 3.2.2.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.3.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.1 3.2.4.R.3 3.2.4.R.3 3.2.4.R.3 3.2.4.R.3 3.2.4.R.3 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE 3.2.4.R.3 SAMPLE 3.2.4.R.3 SAMPLE Analyzed SDG 42341 385070 42341 385070 42341 385070 42340 385070 42341 385070 42340 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385070 42341 385068 42340 385068 42341 385068 42340 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42340 385068 42341 385068 42340 385068 42341 385068 42341 385068 42341 385068 Parameter Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226

Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Area'3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 7110B Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 7110B Modified R

R R

R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 7110B Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result 0.301 0.00 0.0642 15.1

-0.0231 15.0 0.00 0.780 0.527 0.00422

-0.0114 1.07 0.898 14.1 0.00 0.780 0.886 0.276 0.00 0.159 10.3 0.0132 19.1 0.00 0.743 0.556 0.0158 0.0443 0.962 0.896 12.4 0.400 0.743 0.757 0.233 0.00 0.162 11.5 0.0327 19.4 0.00 1.05 0.129 Uncertainty GAS

0.105 14913-50-9 0.171 0.286 4.45 0.109 3.82 1.09 0.148 0.0938 0.0399 0.112 0.125 0.165 1.50 0.815 0.148 0.277 0.0868 0.102 0.229 3.60 0.101 3.10 0.616 0.148 0.0885 0.035 0.0665 0.118 0.184 1.44 0.647 0.148 0.237 0.0763 0.104 0.331 3.65 0.123 3.13 0.925 0.214 0.0839 14952-40-0 12587-46-1 14234-35:6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 Units, Lab Qu MDL CRDL C Dilution % MoistL PCl/G 0.0761 1.00 24.3 PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G PCl/G PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G 0.122 0.546 3.90 4.00 0.196 4.91 10.0 1.52 1.00 24.3 1.00 27.1 1.00 27.1 1.00 27.1 1.00 27.1 1.00 27.1 0.152 1.00 27.1 0.0788 0.100 1.00 27.1 0.0806 1.00 27.1 0.219 1.00 27.1 0.109 1.00 27.1 0.141 1.00 27.1 0.488 1.00 27.1 0.933 1.00 27.1 0.152 1.00 27.1 0.315 1.00 27.1 0.0744 1.00 27.1 0.127 1.00 27.1 0.438 3.90 4.00 0.191 2.93 10.0 1.16 0.112 0.0692 0.100 0.0737 0.187 0.0972 0.304 0.639 0.953 0.112 0.288 0.0664 0.129 0.667 3.82 4.00 0.241 3.13 10.0 1.98 1.00 25.8 1.00 25.8 1.00 1.00 1~00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 0.129 1.00 25.8 25.8 25.8 25.8 25.8 25.8 25.8 25.8 25.8 25.8 25.8 25.8 25.8 25.8 25.8 18 18 18 18 18 18 18 0.105 0.100 1.00

Sample No:_ Type Analyied SDG 3.2.4.R.3 SAMPLE 42341 385068 3.2.4.R.3 SAMPLE 42341 385068 3.2.4.R.3 SAMPLE 42341 385068 3.2.4.R.3 SAMPLE 42341 385068 3.2.4.R.3 SAMPLE.

42341 385068 3.2.4.R.3 SAMPLE 42341 385068 3.2.4.R.3 SAMPLE 42341 385068 3.2.4.R.3 SAMPLE 42341 385068 3.2.4.R.3 SAMPLE 42341 385068 3.2.4.R.3 SAMPLE.

42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42340 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42340 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 SAMPLE 42341 385068 3.2.4.R.4 MSD 42340 385068 3.2.4.R.4 MSD 42340 385068 3.2.4.R.4 MS 42340 385068 3.2.4.R.4 MS 42340 385068 3.2.4.R.4 DUP 42340 385068 3.2.4.R.4 DUP 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 42340 385068 42341 385068 42340 385068 42332 385068 42341 385068 42340 385068 42341 38\\)068 42341 385068 42341 385068 42341 385068 42341 385068 Parameter Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 Actinium-227 ALPHA Antimony-125 BETA Bismuth-212 Bismuth-214 Cesium-137 Cobalt-60 Europium-154 Lead-212 Lead-214 Potassium-40 Protactinium-231 Radium-226 Radium-228 Thallium-208 Tin-126 ALPHA BETA ALPHA BETA ALPHA BETA Actinium-227 ALPHA Americium-241 Antimony-125 BETA Bismuth-212 Bismuth-214 Carbon-14 Cesium-137 Cobalt-60 Area 3 Fraction Method R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 900.0/SW846 9310/SM 711 OB Modified R

EPA 900.0/SW846 9310/SM 7110B Modified R

EPA 900.0/SW846 931 O/SM 711 OB Modified R

EPA 900.0/SW846 931 O/SM 7110B Modified R

R R

EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 711 OB Modified DOE EML HASL-300, Am-05-RC Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 931 O/SM 711 OB Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R EPA EERF C-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R DOE HASL 300, 4.5.2.3/Ga-01-R Result

-0.0185

-0.000223 1.19 0.882 15.9 0.00 1.05 1.02 0.321 0.0598 0.0585 7.79 0.00225 22.1 0.00 0.774 0.0806

-0.0334 0.0196 1.10 0.989 15.5 0.00 0.774 0.644 0.349 0.00 98.6 99.5 114 99.2 10.8 17.8

-0.042 14.3 0.0114 0.0101 22.3 1.93 0.650

-0.897 0.0821 0.0119 UnQertainty GAS Units Lab Qu MDL CRDL C Dilution %.*MoistL 0.0575 10198-40-0 PCl/G U

0.108 1.00 18 0.173 15585-10-1 0.17 4 15092-94-1 0.221 15067-28-4 1.99 13966-00-2 0.901 14331-85-2 0.214 13982-63-3 0.350 15262-20-1 0.115 14913-50-9 0.141 0.289 3.14 0.112 3.13 0.754 0.174 0.0521 0.0537 0.152 0.143 0.206 1.67 0.760 0.174 0.326 0.0761 0.170 15.0 16.6 15.4 15.4 3.38 14952-40-0 12587-46-1 14234-35-6 12587-47-2 14913-49-6 14733-03-0 10045-97-3 10198-40-0 15585-10-1 15092-94-1 15067-28-4 13966-00-2 14331-85-2 13982-63-3 15262-20-1 14913-50-9 12587-46-1 12587-47-2 12587-46-1 12587-47-2 12587-46-1 PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G U

PCl/G U

PCl/G PCl/G U

PCl/G PCl/G UI PCl/G PCl/G PCl/G U

- PCl/G U

PCl/G PCl/G PCl/G PCl/G UI PCl/G PCl/G PCl/G PCl/G UI PCl/G 2.57 0.264 4.06 0.080 0.106 3.26 1.06 0.197 0.756 0.0612 0.0448 12587-47-2 PCl/G 14952-40-0

. PCl/G U

12587-46-1 PCl/G 14596-10-2 PCl/G U

14234-35-6 PCl/G U

12587-47-2 PCl/G 14913-49-6 PCl/G 14733-03-0 PCl/G 14762-75-5 10045-97-3 10198-40-0 PCl/G U

PCl/G PCl/G U

0.342 0.129 0.215 0.950 1.16 0.129 0.334 0.0949 0.175 0.545 3.84 4.00 0.205 3.06 10.0 1.00 18 1.00 18 1.00 18 1.00 18 1.00 18 1.00 18 1.00 18 1.00 18 1.00 18 1.00 8.9 1.00 8.9 1.00 8.9 1.00 8.9 1.46 1.00 8.9 0.149 1.00 8.9 0.0878 0.100 1.00 8.9 0.0943 1.00 8.9 0.298 1.00 8.9 0.128 1.00 8.9 0.171 1.00 8.9 0.775 1.00 8.9 0.952 1.00 8.9 0.149 1.00 8.9 0.315 1.00 8.9 0.0697 1.00 8.9 0.211 1.00 8.9 6.33 4.00 1.00 8.9 4.16 10.0 1.00 8.9 6.11 4.00 1.00 8.9 3.82 10.0 1.00 8.9 3.63 4.00 1.00 8.9 2.14 10.0 1.00 8.9 0.500 1.00 9.87 3.97 4.00 1.00 9.87 0.164 1.00 1.00 9.87 0.200 1.00 9.87 3.20 10.0 1.00 9.87 0.957 1.00 9.87 0.142 1.00 9.87 1.33 2.00 1.00 9.87 0.0811 0.100 1.00 9.87 0.0924 1.00 9.87

Sample No. Type 3.2.4.R.5 SAMPLE 3.2.4.R.5 SAMPLE 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 3.2.4.R.5 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MS DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP DUP Analyzed SDG,

42332 385068 42332 385068 42332 385068 42341 385068 42340 385068 42341 385068 42341 385068 42331 385068 42331 385068 42331 385068 42333 385068 42341 385068 42341 385068 42341 385068 42341 385068 42341 385068 42337 385068 42341 385068 42332 385068 42332 385068 42332 385068 42332 385068 42341 385068 42340 385068 42332 385068 42332 385068 42332 385068 42332 385068 42341 385068 42332 385068 42332 385068 42332 385068 42332 385068 42332 385068 42332 385068 42331 385068 42331 385068 42331 385068 42331 385068 42331 385068 42334 385068 42332 385068 42332 385068 Parameter Curium-242 Curium-243/244 Curium-245/246 Europium-154 lodine-129 Lead-212 Lead-214 Neptunium-237 Plutonium-238 Plutonium-239/240 Plutonium-241 Potassium-40 Protactinium-231 Radium-226 Radium-228 Strontium-90 Technetium-99 Thallium-208 Thorium-228 Thorium-229 Thorium-230 Thorium-232 Tin-126 Tritium Uranium-232 Uranium-233/234 Uranium-235/236 Uranium-238 Tritium Americium-241 Americium-241 Curium-242 Curium-242 Curium-243/244 Curium-245/246 Neptunium-237 Plutonium-238 Plutonium-238 Plutonium-239/240 Plutonium-239/240 Plutonium-241 Thorium-228 Thorium-229 Area 3 Fract.ion Method R

DOE EML HASL-300, Am-05-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300,1-01 Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

ASTM C 14 76-00 Modified R

DOE EML HASL-300, Pu-11-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 905.0 Modified/DOE RP501 Rev. 1 Modified R

DOE EML HASL-300, Tc-02-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

DOE EML HASL-300, Th-01-RC Modified R

DOE HASL 300, 4.5.2.3/Ga-01-R R

EPA 906.0 Modified R

DOE EML HASL-300, U-02-RC Modified R

EPA 906.0 Modified R

DOE EML HASL-300, Am-05-RC Modified R

ASTM C 1476-00 Modified R

DOE EML HASL-300, Pu-11-RC Modified R

R R

R DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Th-01-RC Modified Result 0.00 0.021 0.0494 0.0149

-0.0408 1.13 0.999

-0.0331

-0.00459 0.00153

-1.12 14.5 0.00 0.650 0.740

-0.149 1.61 0.348 0.416 0.161 0.796 1.14 0.0509 1.83 0.0125 0.940 0.0897 0.769 91.4 0.0397 0.0397 0.00 0.00

-0.00374

-0.00433

-0.0348 0.00 0.00 0.0333 0.0333

-1.32 1.15

-0.0399 Uncertainty CAS Units Lab Qu MDL CRDL C Dilution % MoistL 0.044 OER-100-93 PCl/G 0.133 PCl/G u

0.0874 0.130 0.283 0.137 0.167 0.146 0.0396 0.0702 6.25 1.64 0.529 0.197 0.344 0.410 1.50 0.080 0.459 0.261 0.424 0.501 0.118 1.74 0.0672 0.258 0.0866 0.233 7.47 0.0631 0.0631 0.0366 0.0366 0.0323 0.0373 0.154 0.033 0.033 0.0663 0.0663 5.37 0.748 0.275 PCl/G 15585-10-1 PCl/G 15046-84-1 PCl/G 15092-94-1 PCl/G 15067-28-4 PCl/G 13994-20-2 PCl/G 13981-16-3 PCl/G OER-100-70 PCl/G 14119-32-5 PCl/G 13966-00-2 PCl/G 14331-85-2 PCl/G 13982-63-3 PCl/G 15262-20-1 PCl/G 10098-97-2 PCl/G 14133-76-7 PCl/G 14913-50-9 PCl/G 14274-82-9 PCl/G 15594-54-4 PCl/G 14269-63-7 PCl/G 7440-29-1 PCl/G PCl/G 10028-17-8 PCl/G 14158-29-3 PCl/G 13968-55-3/1391 PCl/G 15117-96-1/1391 PCl/G 7440-61-1 PCl/G 10028-17-8 14596-10-2 PCl/G 14596-10-2 PCl/G OER-100-93 PCl/G OER-100-93 PCl/G 13994-20-2 13981-16-3 PCl/G PCl/G PCl/G PCl/G u

u u

u UI u

u u

u 13981-16-3 PCl/G U

OER-100-70 PCl/G OER-100-70 PCl/G U

14119-32-5 PCl/G U

14274-82-9 PCl/G 15594-54-4 PCl/G U

0.0654 1.00 1.00 9.87 0.261 1.00 0.132 1.00 0.261 0.496 1.00 0.107 0.154 0.382 1.00 0.0917 1.00 0.154 1.00 10.8 15.0 0.577 1.08 0.142 0.254 0.857 2.00 2.50 5.00 0.064 0.725 1.00 0.421 1.00 0.318 1.00 0.342 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 0.136 2.83 1.00 6.00

. 1.00 0.126 1.00 0.0991 1.00 0.0538 1.00 0.0537 1.00 4.52 6.00 0.0873 1.00 0.0873 1.00 0.0544 1.00

. 0.0544 1.00 0.0748 1.00 0.0865 1.00 0.402 1.00 0.0491 1.00 0.0491 1.00 0.108 1.00 0.108 1.00 9.33 15.0 0.842 1.00 0.670 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87 9.87

Area3 Sample No. Type.

Analyzed SDG Parameter Fraction Method

Result Uncertainty. CAS Units Lab Qu MDL CRDL C Dilution % Moi.stL

-*~ l 3.2.4.R.5 DUP 42332 385068 Thorium-230 R

DOE EML HASL-300, Th-01-RC Modified 0.861 0.592 14269-63-7 PCl/G 0.501 1.00 1.00 9.87 3.2.4.R.5 DUP 42332 385068 Thorium-232 R

DOE EML HASL-300, Th-01-RC Modified 0.339 0.400 7440-29-1 PCl/G 0.432 1.00 1.00 9.87 3.2.4.R.5 DUP 42332 385068 Thorium-232 R

DOE EML HASL-300, Th-01-RC Modified 0.339 0.400 7440-29-1 PCl/G u

0.432 1.00 1.00 9.87 3.2.4.R.5 DUP 42341 385068 Tritium R

EPA 906.0 Modified

. 2.00 1.74 10028-17-8 PCl/G 2.80 6.00 1.00 9.87 3.2.4.R.5 DUP 42341 385068 Tritium R

EPA 906.0 Modified 2.00 1.74 10028-17-8 PCl/G u 2.80 6.00 1.00 9.87 3.2.4.R.5 DUP 42332 385068 Uranium-232 R

DOE EML HASL-300, U-02-RC Modified

-0.0225 0.0732 14158-29-3 PCl/G u 0.172 1.00 1.00 9.87 3.2.4.R.5 DUP 42332 385068 Uranium-233/234 R

DOE EML HASL-300, U-02-RC Modified 0.758 0.250 13968-55-3/1391 PCl/G 0.141 1.00 1.00 9.87 3.2.4.R.5 DUP 42332 385068 Uranium-235/236 R

DOE EML HASL-300, U-02-RC Modified 0.0201 0.0566 15117-96-1/1391 PCl/G 0.0604 1.00 1.00 9.87 3.2.4.R.5 DUP 42332 385068 Uranium-235/236 R

DOE EML HASL-300, U-02-RC Modified 0.0201 0.0566 15117-96-1/1391 PCl/G u 0.0604 1.00 1.00 9.87 3.2.4.R.5 DUP 42332 385068 Uranium-238 R

DOE EML HASL-300, U-02-RC Modified 0.903 0.267 7440-61-1

. PCl/G 0.0602 1.00 1.00 9.87

ML16293A890

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