Text

Request for Partial Release of Humboldt Bay Power Plant Unit 3 Property from the Part 50 Site
	ML16326A004
Person / Time
Site:	Humboldt Bay
Issue date:	11/09/2016
From:	Sharp L; Pacific Gas & Electric Co
To:	; Document Control Desk, Office of Nuclear Material Safety and Safeguards
References
	HBL-16-008
	Download: ML16326A004 (485)
	v • d • e

Loren D. Sharp Humboldt Bay Power Plant Pacific Gas and Senior Director 1000 King Salmon Avenue Electric Company°' Humboldt Bay Nuclear Eureka, CA 95503 707.444.0819 Internal: 375.0819 Fax: 707.444.0871 November 9, 2016 PG&E Letter HBL-16-008 U.S. Nuclear Regulatory Commission ATIN: Document Control Desk Washington, D.C. 20555-0001 Docket No. 50-133, License No. DPR-7 Humboldt Bay Power Plant, Unit 3 Request for Partial Release of Humboldt Bay Power Plant Unit 3 Property from the Part 50 Site *

Dear Commissioners and Staff:

Pacific Gas and Electric Company (PG&E) requests NRG approval to release a portion of the Humboldt Bay Power Plant (HBPP) Unit 3 site in accordance with the HBPP Unit 3 License Termination Plan (LTP). Specifically, PG&E intends to release approximately 30.4 acres, known as the Fisherman's Channel, from the HBPP Unit 3 site to allow for the transfer of this property to the Humboldt Bay Harbor District. contains an assessment that demonstrates that the area can be released for unrestricted use in accordance with LTP criteria. Enclosure 2 contains the Final Status Survey Report for the area to be released. , Figure 1, depicts the current HBPP Unit 3 site property boundary. The land area proposed for release consists of the land and waterway within the site boundary across from King Salmon Avenue (Enclosure 1, Figure 2) and is referred to hereafter as the "Release Area."

HBPP Unit 3 LTP, Section 1.2, describes PG&E's intent to perform this partial site release as part of a phased approach to release the entire site for unrestricted use.

In accordance with LTP, Section 1.2, PG&E has verified that the "Release Area" meets acceptance levels through final status surveys. PG&E also assessed the subject "Release Area" to ensure that this proposed action will have no adverse impact on the ability of the site in the aggregate to meet 10 CFR Part 20, Subpart E, criteria for unrestricted release.

There are no new or revised regulatory commitments (as defined in NEI 99-04) made in this letter.

r'

Document Control Desk PG&E Letter HBL-16-008 November 9, 2016 Page 2 If you have any questions regarding this submittal, please contact Mr. William Barley at (707) 444-0856.

en D. Sharp Senior Director Humboldt Bay Nuclear Enclosures cc: HBPP Humboldt Distribution cc/enc: John B. Hickman, NRC Project Manager Kriss M. Kennedy, NRC Region IV Administrator Gonzalo Perez, California Department of Public Health

Enclosure 1 PG&E Letter HBL-16-008 Humboldt Bay Power Plant Unit 3* "Release Area" Assessment

Enclosure 1 PG&E Letter HBL-16-008 Page 1 of 7 Humboldt Bay Power Plant (HBPP) Unit 3 "Release Area" Assessment

Background:

Humboldt Bay Power Plant (HBPP) Unit 3 commenced commercial operations in 1963 and last operated in July 1976. Unit 3 consisted of a General Electric natural circulation, boiling water reactor, an associated turbine-generator, and the necessary support and auxiliary systems. During its operational period, Unit 3 experienced a variety of operating events (e.g., fuel failures, leaks, spills, and repairs) that have affected decontamination and decommissioning processes. Radiological contamination of the site is found within systems, on components, on structure interiors, and in soil located inside and adjacent to the Unit 3 Restricted Area (RA).

The Atomic Energy Commission (AEC) granted Unit 3 a construction permit on October 17, 1960. The AEC issued Operating License DPR-7 in August 1962, and Unit 3 began commercial operation in August 1963. On May 17, 1976, the NRC issued an order that required satisfactory completion of a seismic design upgrade program and resolution of specified geologic and seismic concerns prior to return to power following the 1976 refueling outage. On July 2, 1976, Pacific Gas and Electric Company (PG&E) shut down Unit 3 for refueling. In December 1980, it became apparent that the cost of completing the required backfits would make it uneconomical to restart the unit. PG&E ultimately concluded that the seismic and other modifications required (i.e., in response to the Three Mile Island accident in 1979) were in fact not economical and in *June 1983

. announced its intention to decommission the unit.

The HBPP Unit 3 reactor was permanently defueled in 1984 and on July 30, 1984,

, PG&E submitted a license amendment request (LAR) to possess fuel for up to 30 years, but no longer operate, and to decommission HBPP Unit 3 using the SAFSTOR method.

On July 16, 1985, the NRC issued License Amendment (LA) 19 to place Unit 3 in a possess-but-not-operate status, and on July 19, 1988, the NRC issued LA 23 approving the Decommissioning Plan and authorizing the decommissioning of Unit 3. PG&E submitted the HBPP Unit 3 Post-Shutdown Decommissioning Activities Report (PSDAR) to the NRC pursuant to 10 CFR 50.82(a)(4)(i) on February 27, 1998. The PSDAR and the Defueled Safety Analysis Report (DSAR) superseded the original Decommissioning Plan and provided the information required by 10 CFR 50.82(a)(4).

By December 2008, all spent fuel had been removed from the HBPP Unit 3 spent fuel pool and transferred to the 10 CFR Part 72-licensed Humboldt Bay Independent Spent Fu~I Storage Installation (HB ISFSI):

In May 2013, PG&E submitted the HBPP Unit 3 License Termination Plan (LTP) in LAR 13-01. In response to the NRC's Requests for Additional Information (RAls),

PG&E submitted Revision 1 to the HBPP Unit 3 LTP on August 13, 2014. The NRC approved the HBPP Unit 3 LTP on May 4, 2016.

Enclosure 1 PG&E Letter HBL-16-008 Page 2 of 7

Purpose:

The purpose of this assessment is to ensure that the requested partial site release will have no adverse impact on the ability of the site, in aggregate, to meet 10 CFR Part 20, Subpart E, criteria for unrestricted release. The Final Status Survey (FSS) Report for the "Release Area" is contained in Enclosure 2.

Site History Related to the "Release Area":

This area of the plant site is nonindustrialized. The 30.4-acre area includes coastal marsh, intertidal areas, and a navigable channel used for recreational boating. The "Release Area,-,, according to the HBPP Historical Site Assessment (2011 Update), was potentially impacted by dry and wet deposition from Unit 3 stack releases. As discussed on page 8 of the FSS Report and Section 2.3 of the LTP, PG&E performed characterization surveys in the area in 1998, and more recently, in 2013. The results of the characterization surveys indicated Cs-137 levels at a small fraction of the derived concentration guideline levels. The FSS of the "Release Area" supports the characterization data. In addition, the FSS of the "Release Area" supports the rejection of the null hypothesis (i.e., the "Release Area" meets the HBPP Unit 3 release criteria) and that the "as low as reasonably achievable" (ALARA) criterion as specified in the LTP was achieved.

Impact of the Release of the Area:

Statement of Dismantling Activities No dismantlement activities are required, orwere performed, in the "Release Area." Since the subject area is impacted, an FSS was performed.

Potential for Cross-Contamination from Subsequent Activities The"Release Area" is bounded on the east by King Salmon Avenue and off-site locations on Jhe north, west and south.

Since the commencement of decommissioning, restrictive controls have been placed on the release of material from radiological controlled areas, which further decreases the probability that the "Release Area" will be impacted from decommissioning activities. These controls include contamination containment, dust control measures, storm water runoff control measures, building demolition controls, and additional evaluations and surveys of material leaving the site.

These radiation protection program requirements for decommissioning activities, as well as the additional protections afforded from FSS isolation and control measures of adjacent site areas, provide strong assurance that the potential for cross-contamination of the "Release Area" is de minimis.

Enclosure 1 PG&E Letter HBL-16-008 Page 3of7 Impact of Releasing the Specific Area on Part 50 Licensing Basis The licensing basis for HBPP Unit 3 includes the maintenance of certain programs to fulfill regulatory requirements and functional responsibilities.

Throughout decommissioning, these programs are modified as necessary and terminated when the applicable concern is no longer relevant. These program changes are implemented using the change processes specified for each type of program. The methodology for releasing land requires a review and assessment of the impact on licensing programs for the site lands remaining within the domain of the Part 50 License. The impact of releasing the "Release Area" on each of the HBPP Unit 3 licensing programs is described below. With this submittal, PG&E is requesting NRC review and concurrence of the changes described herein.

Technical Specifications The Design Features and Administrative Controls, as described in the HBPP Unit 3 Technical Specifications, are not impacted by the release of the "Release Area."

Defueled Safety Analysis Report (DSAR)

A change will be made to the HBPP Unit 3 DSAR, Figure 2-1, to identify the new site boundary reflecting the reduced site area resulting from the release of the "Release Area."

Environmental Report for HBPP Decommissioning LTP Chapter 8 contains the Supplement to the Environmental Report for HBPP Decommissioning, dated July 1984. Neither the Environmental Report nor the

. Supplement is impacted by the release of the "Release Area."

Humboldt Bay Site Emergency Plan This Plan will not be affected by the release of the "Release Area."

Humboldt Bay Quality Assurance Plan This Plan will not be affected by the release of the "Release Area."

Offsite Dose Calculation Manual (ODCM)

This Manual will not be affected by the release of the "Release Area."

Enclosure 1 PG&E Letter HBL-16-008 Page 4of7 Environmental Monitoring Program This Program will not be affected by release of the "Release Area."

Ground Water Monitoring Program The Ground Water Monitoring Program will not be affected by release of the "Release Area." There are no active ground water monitoring wells in the "Release Area." The "Release Area" comprises Humboldt Bay area and tidal-influenced marsh land. Since the area is a considerable distance from areas of potential ground water contamination, there is no need to place ground water wells in the "Release Area." Therefore, there is no need to perform a capture zone analysis and there is no need to add a ground water contribution in the "Release Area."

Fire Protection Program This Program will not be affected by the release of the "Release Area."

Training Program This Program will not be affected by the release of the "Release Area."

Post-Shutdown Decommissioning Activities Report (PSDAR)

This Report will not be affected by the release of the "Release Area."

License Termination Plan (LTP)

Changes will be made to the HBPP Unit 3 LTP in Sections 2.1.8.11 and 8.1.2; Figures 1-2, 2-2, 6-2, and 8-1; and Table 2-3, to reflect the new site boundary and reduced site acreage resulting from the release of the "Release Area."

Additional Areas to be Addressed to Support the Release of the Area PG&E will continue to maintain authority over all activities conducted within the HB ISFSI 10 CFR Part 72 license until such time as the spent fuel is removed from the site and the NRC terminates the 10 CFR Part 72 license.

PG&E will maintain the following records through license termination: (1) a map of the site identifying the facility and site as defined in the original license; (2) a record of the "Release Area" released under this action; and (3) documentation of the radiological conditions of the lands released under this action.

Enclosure 1 PG&E Letter HBL-16-008 Page 5 of 7 Site Release Criteria The site radiological release criteria for the HBPP Unit 3 site correspond to the 10 GFR 20.1402 criteria for unrestricted use. The residual radioactivity, including that from ground water sources that is distinguishable from background, must not cause the total effective dose equivalent (TEDE) to an average member of the critical group to exceed 25 mrem/yr. The residual radioactivity must also be reduced to levels that are ALARA.

Final Status Survey:

HBPP Unit 3 LTP, Section 5, describes the FSS Plan that encompasses the radiological assessment of all affected structures, systems, and land areas for the purpose of quantifying the concentrations of any residual activity that exists following all decontamination activities. An FSS was performed in the "Release Area." The FSS Report determined that the site release criteria was met and is included in Enclosure 2.

==

Conclusion:==

The release of the "Release Area" is part of PG&E's overall effort to terminate License DPR-7 and to achieve unrestricted release of the entire site, with -the exception of the 10 GFR Part 72 portion, in accordance with the criteria in Subpart E of 10 GFR Part 20.

This action is also consistent with the phased approach described in Section 1.2 of the HBPP Unit 3 LTP.

In addition, 10 GFR 50.82(a)(11) establi~hes the following criteria to be used by the NRG for terminating the license of a power reactor facility: (1) dismantlement has been performed in accordance with the approved LTP; and (2) the final radiation survey and associated documentation demonstrate that the facility and site have met the criteria for decommissioning in 10 GFR Part 20, Subpart E. Although no dismantling activities were required for the "Release Area," the FSS supports the release of the "Release Area" by demonstrating that this portion of the site land can be released from the HBPP Unit 3 site.

The FSS Report, along with future reports, provides documentation that decommissioning activities have been performed in accordance with the LTP, and each FSS confirms *that the residual radioactivity in each associated survey unit meets the criteria established in the HBPP Unit 3 LTP. Thus, this action supports the overall license termination process in accordance with NRG regulations.

Enclosure 1 PG&E Letter HBL-16-008 Page 6 of 7 Figure I HBPP Property Boundary 1?

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Enclosure 1 PG&E Letter HBL-16-008 Page 7 of 7 Figure 2 Partial Site Release Boundary PROPERTY BOUNDARY TYP.

FISHERMAN'S CHANN EL

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PARTIAL SITE RELEAS E AREA BOUNDARY PROPERTY BOUNDARY PARTIAL SITE RELEASE AREA TYP.~\ \

Enclosure ~ .-

PG&E Letter HBL-16-008 Humboldt Bay Power Plant Unit 3 "Release Area" Final Status Survey Report

RCP FSS- 17 Attachment 7.2 Rev. I Pacific Gas and HUMBOLDT BAY POWER PLANT Electric Company" FINAL STATUS SURVEY REPORTS HBPP-FSS-OOL 10-11 & HBPP-FSS-OOL 10-12 Final Status Survey Report for Survey Units:

HBPP-FSSP-OOL 10-11 and HBPP-FSSP-OOL 10-12

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Prepared by: Dale Randall, CHP I ) 0i/e l\q 14 ./ql//[,d£;fwi/(Date: 1/--l - It FSS Engineering Supervisor (print/sign)

Reviewed by: Marshall Blake I~

FSS Engineering (print/sign)

Date: I (- ;)- I~

Date: It 1 to FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 1 of 468

Attachments Attachment 1 Survey Plan HBPP-FSSP-OOLl0-11-00 Attachment 2 HTD Assessment data Attachment 3 Laboratory Data for HBPP-FSSP-OOLIO-i 1 &

HBPP-FSSP-OOL 10-12 Attachment 4 . Data Assessment HBPP-FSSP-OOLlO~l l Attachment 5 ALARA Statement Attachment 6 Quality Verification Assessment Report Attachment 7 Survey Plan HBPP-FSSP-OOLl0-12-00 Attachment 8 Data Assessment HBPP-FSSP-OOLl0-12 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 2 of 468

Executive Summary In accordance with the provisions of the Humboldt Bay License Termination Plan, Rev. 1 (LTP), Survey Units HBPP-FSSP-OOLl0-11 and HBPP-FSSP-OOLl0-12 were Final Status Surveyed (FSS) for phased release from the site's 10CFR50 license. This report was prepared to document that the designated survey units satisfy the radiological release criteria.

SurVey Area OOLlO is designated in the LTP as a Class 3 land area with a low likelihood ofradiological contaminants in excess of the derived concentration guideline levels (DCGLs). The total surface area is approximately 235,191 m 2

The two survey units within Survey Area OOLl 0 under consideration for this report consist of site land areas

to the southwest of King Salmon Avenue. It is made up of two survey units, HBPP-FSSP-OOLl0-11 (76,520 m2) and HBPP-FSSP-OOLl0-12 (46,364 m2). Survey Unit HBPP-FSSP-OOLl0-11 (or "OOLl0-11") can be described as the water covered portion of the area that includes Fisherman's Channel, a navigable waterway, and tidal mud flats to the east. Survey Unit HBPP-FSSP-OOLl0-12 (or "OOLI0-12") is the non-tidally influenced land area which includes coastal marshland. The survey units are both designated as Class 3 land areas.

The surveys performed included a total of twenty (20) sediment samples and twenty (20) soil samples. Each of the sample locations was selected based on an approved randomized methodology and the locations were confirmed by a high precision global positioning system (GPS). The sampling included four (4) split-samples and two (2) sample recounts that were taken for quality assurance purposes. The land area (Survey Unit OOLI0-12) was also partially walkover scanned with a gamma sensitive instrument probe. Information for Survey Unit OOLl0-11 is summarized in Executive Summary Table A. Survey Unit OOLl0-12 information is summarized in Executive Summary Table B.

Some minor Quality Assurance (QA) related discrepancies were discovered both by audit and by the failure of one of the six QA sample comparisons performed. These issues were entered into the site's corrective action program, investigated, and evaluated. They are not considered to significantly impact the overall confidence in the results or conclusion.s of the FSS.

The walkover scan survey results found no elevated locations. The sample analysis results indi~ated that the only positively detected plant-derived isotope was Cs-137. Cs-13 7, which also is found in the environment as a result of atmospheric weapons testing fallout, was positively detected in some samples at up to a small fraction of the DCGL.

The maximum hypothetical dose (from all sources, including groundwater) to a future resident farmer was determined to be less than 1. 78 mrem/yr. The report concludes that both survey units have met their FSS data quality objectives and meet the regulatory release criteria of less than or equal to 25 mrem/yr Total Effective Dose Equivalent (TEDE) to the average member of the critical group plus As Low As Reasonably ,

Achievable (ALARA).

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FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 3 of 468

Executive Summary Table A Feature Design Criteria Comment Synopsis of FSS of HBPP-FSSP-OOLl0-11 Survey Unit Land 76,520 m 2 Based on AutoCAD Area Based on the HBPP LTP, Classification Class 3 Rev. 1.

Final Status Survey Plan No. HBPP-FSSP-00110-HBPP Procedure RCP FSS-2 11-00 Grid Spacing 66.5 m Based on triangular grid 7.58 pCi/g Cs-137 Administratively set to DCGL0 p 1 achieve 24 mrem/yr TEDE A variance was taken The L TP requires 1-10% of Scan Survey Area from this area coverage for Class 3 Coverage

2 reqmrement. survey units Number of 15 required 20 Taken on a fixed grid Measurements with random start point Min. Value 5.63E-03 pCi/g Cs-137 Max. Value l.42E-01 pCi/g Cs-137 Mean 7.66E-02 pCi/g Cs-137 Median 7.92E-02 pCi/g Cs-137 Std. Dev. 3.43E-02 pCi/g Cs-137 No. of Bias None NIA Measurements (I) DCGL 0 P is the Operational DCGL; adjusted to conservatively account for potential dose from Hard-to-Detect radionuclides.

(2) The typical approach consisting of walk-over scan surveys using a 2"x2" Nal(Tl) scintillation detector could not be performed due to routine tidal flooding of the inlet.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 4 of 468

Executive Summary Table B Feature Design Criteria Comment Synopsis of FSS of HBPP-FSSP-OOLl0-12 Survey Unit Land 46,364 m 2 Based on AutoCAD Area Based on the HBPP LTP, Classification Class 3 Rev. 1.

Final Status Survey Plan No. HBPP-FSSP-HBPP Procedure RCP FSS-2 OOLl0-12-00 NIA Sample points were randomly Grid Spacing selected.

I 7.58 pCi/g Cs-137 Administratively set to DCGLop achieve 24 mremlyr TEDE The LTP requires 1- 10% of Scan Survey Area Approximately 10% area coverage for Class 3 Coverage survey units Number of 15 required 20 Randomly selected sample Measurements locations were selected Min. Value -1.04E-02 pCilg Cs-137 Max. Value 1.19E+OO pCilg Cs-137 Mean 2.37E-01 pCilg Cs-137 Median 1.68E-01 pCilg Cs-137 Std. Dev. 2.63E-01 pCilg Cs-137 No. of Bias None NIA Measurements Phase 1 Release Area Description The Phase 1 Area for release consists of all site land areas to the south (site west) of King Salmon Avenue. The Phase 1 Area includes two survey units, HBPP-FSSP-OOLl0-11 and HBPP-FSSP-OOLl0-12. This area of the plant site is non-industrialized. The area includes coastal marsh, intertidal areas and a navigable channel used for recreational boating. Figure 1 is an aerial photograph of the area. Figure 2 is a map of the Phase 1 Release area.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 5 of468

Figu re 1. Aerial Photograph of Survey Area HBPP-FSS-OOL 10 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-1 2 Page 6 of 468

Figure 2. Map of the Phase I Release Area & Associated FSS Survey Units PHASE 1 RELEASE AREA HBPP LOCATION MAP rt "-

J PHASE 1 RELEASE

- *- * - AREA BOUNDARY OOL 10-12 LAND ADJACENT TO FISHERMAN'S CHANNEL I OOL 10-11 FISHERMANS CHANNEL

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FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 7 of 468

Survey Unit Designation In accordance with Humboldt Bay Power Plant (HBPP) Procedure RCP FSS-1, Survey Units HBPP-FSSP-OOLl 0-11 and HBPP-FSSP-OOLl 0-12 are designated as Class 3 Survey Units per the HBPP L TP (Ref. 1) and was confirmed by subsequent reviews.

Survey Unit Design Information HBPP-FSSP-OOLl0-11 & HBPP-FSSP-OOLl0-12 Data Quality Objectives (DQOs)

FSS design and planning used the Data Quality Objective (DQO) process as described by the LTP, Procedure RCP FSS-2, "Preparation ofFinal Status Survey Plan," (Ref. 2) and the "Multi-Agency Radiation Survey and Site Investigation Manual" (MARSSIM) (Ref.3). A summary of the main features of the DQO process are provided herein.

The DQO process inc.orporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis.

Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the sul"Vey plan, the underlying assumption (or null hypothesis) assumes residual activity in the survey unit exceeds the release criteria. Rejection of the null hypothesis indicates residual activity within the survey unit does not exceed the release criteria. The primary objective of the FSS plan was to demonstrate that the level ofresidual radioactivity in Survey Units OOLl0-11 & OOLl0-12 did not exceed the*

release criteria specified in the LTP and that the potential dose from residual radioactivity is ALARA.

A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development ofDCGLs. The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil.

The total dose under the LTP criteria is 25 mrem/yr Total Effective Dose Equivalent (TEDE) from all of the potentially present plant derived nuclides. The presence of all radionuclides listed (gamma-emitters, HTD beta-emitters, and TRUs) in the soil (sediment) were evaluated under FSS Survey Plans HBPP-FSSP-OOLl0-11-00 (Attachment 1) and HBPP-FSSP-OOLl0-12-00 (Attachment 7).

DQOs re Nuclide Selection and DCGLs The soil DCGLs determined in the LTP are presented in Table 1, Soil DCGLs and Analysis Lower Limits of Detection.

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 8 of 468

Table 1- Soil DCGLs and Analysis Lower Limits of Detection (LLDs)

Radionuclide (I) Soil DCGL (pCi/g) <2> LLD (pCi/g) <3>

H-3 6.8E+02 6.8E+Ol C-14 6.3E+OO 6.3E-01 Mn-54 l.9E+03 l.9E+02 Fe-55<4> l.OE+04 l.OE+03 Co-60 3.8E+OO 3.8E-01 Ni-63 7.2E+02 7.2E+Ol Sr-90 l.5E+OO 1.5E-01 Nb-94 7.lE+OO 7. lE-01 Tc-99 l.2E+Ol l.2E+OO Cs-137 7.9E+OO 7.58E-01 Eu-152 l.OE+Ol l.OE+OO Eu-154 9.4E+OO 9.4E-01.

Np-237 l.lE+OO l.lE-01 Pu-238 2.9E+Ol 2.9E+OO Pu-239/240 toJ 2.6E+Ol 2.6E+OO Am-241 l!lJ 2.5E+Ol 2.5E+OO Pu-241 8.6E+02 8.6E+Ol Cm-243/244 2.9E+Ol 2.9E+OO Cm-245/246 l.7E+Ol l.7E+OO (1) Bold text indicates radionuclides that are considered Hard to Detect (HTD)

(2) The Soil DCGL(s) are specified by the LTP in Chapter 6 and are equivalent to twenty-five (25) mrern/yr TEDE.

(3) The desired LLD is 10% of the Soil DCGL within an acceptable range of up to 50% of the DCGL.

(4) Generic Screening Value of NUREG 17 57, Vol. 2 (5) Americium-241 can be analyzed by gamma and alpha spectroscopy and is considered to be Easy to Detect (ETD). The preferred result is the alpha spectroscopy's when both analyses are performed.

(6) For radiochemical analyses whose results cannot discern between two isotopes, i.e. Pu-239/240, Cm-243/244 and Cm-245/246, the lower of the two DCGLs was selected from the LTP.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 9 of 468

Nuclide Selection Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration and variability. Based on a review of the samples collected to characterize the environs associated with Survey Area OOLlO, Cs-137 was the only plant-related radionuclide identified consistently in the characterization samples analyzed. Sample results for all other easy-to-detect (ETD) and hard-to-detect nuclides (HTD) were less than the minimum detectable concentration (<MDC) for laboratory analyses of soil samples. This characterization data for Survey Area OOLlO soils was used to formulate the design for Survey Units OOLl0-11 and OOLl0-12. Additional detail on the development of the survey design is provided in Attachment 1, Survey Plan HBPP-FSSP-OOLJ0-11-00 and Attachment 7, Survey Plan for HBPP-FSSP-OOLJ0-12-00.

Based on historical use of the area (Class 3 designation) and review of the existing pre-FSS characterization data, all samples were not analyzed for HTD nuclides. However, any potential dose from HTD nuclides was bounded by directly adding the dose contribution of a representative sample collected from the Reactor Drain Tank (RDT) vault of the Liquid Radioactive Waste Building. This sample had an activity of22 pCi/g and was collected from an area of concentration for all potential plant-related nuclides, including hard-to-detect and transuranic nuclides.

The results of this representative sample were used to bound the dose contribution from HTD nuclides. As shown in Attachment 2, Resultant Dose from Hard-to-Detect Nuclides, the highest potential dose contributed from HTD nuclides is less than 1 mrem/yr. Note that Sr-90 and H-3 were excluded from this bounding estimate, since samples from each survey unit were analyzed on-site for these specific HTD nuclides.

A reduction of 1 mrem/yr to the default Cs-137 DCGL (7.93 pCi/g) was required, since the default DCGL is based on an annual dose of25 mrem/yr (i.e., from both HTD & ETD nuclides). This information and analysis formed the basis for reducing the Cs-137 DCGL by 1 mrem/yr to conservatively account for any potential dose contribution from HTD nuclides.

The limit for the total annual dose for all potential plant-related nuclides is 25 mrem/yr. As previously shown, the only nuclide expected to be present is Cs-137. A reduction of 1 mrem/yr to the default Cs-137 DCGL (7.93 pCi/g) was required, since the default DCGL is based on an annual dose of 25 mrem/yr for all nuclides.

The reduced DCGL for Cs-137, or "Operational DCGL" (DCGL0 p) can be related to the default DCGL (provided in the L TP) using the following principle relationship:

DCGL 0 p DLTP x - - -

DCGLLTP where: DoP = 24 mrem/yr DLrP = 25 mrem/yr DCGLm = 7.93 pCijg FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 10 of 468

This results in a DCGL 0 p of 7.58 pCi/g for Cs-137; scaled to a TEDE of 24 mrem/yr to account for any HTD nuclides that might be present.

In addition to scaling the DCGL for Cs-137, the HBPP Site Closure Laboratory also analyzed all samples from each Sr-90 and H-3 and sent two (2) samples to an independent laboratory for analysis ofHTD nuclides. This methodology and analysis described above was used to account for any potential dose contribution from HTD nuclides present in Survey Units OOLl0-11 & OOLl0-12.

It was also identified during the development of the survey plans that because the expected timing of the Phase 1 release occurs prior to the LTP assumed date 2019, Fe-55 screens into the nuclide suite as a potential nuclide of concern. At present a site specific DCGL for Fe-55 does not exist; however, since Fe-55 has not been detected and would not be expected to be present in detectable concentrations in Class 3 plant areas, the Generic Screening value ofNUREG 1757 Vol. 2 (Ref. 4) was applied as the DCGL for Fe-55 (i.e., 1.0 E+04 pCi/g).

As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. Results reported as less than the Minimum Detectable Concentration (MDC) were not used for FSS. Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty to two (2) standard deviations, data qualifiers, units, and the required and observed MDC.

Survey Unit Description HBPP-FSSP-OOLl0-11 Survey Unit HBPP-FSSP-OOLI0-11 (Fisherman's Channel) is approximately 76,520 square meters of surface area. The unit is completely covered by seawater at high tide, requiring a boat and sample dredge to collect sediment samples for final status survey. The survey unit's boundary abuts both Survey Area HBPP-FSSP-OOLl 0-12 and off-site locations, including residences associated with the King Salmon community. See Figure 2 for detail on survey unit location and adjacent areas.

HSAEvents Within the Historical Site Assessment (HSA), there is no mention of plant related activities occurring within the boundaries of this Survey Unit.

Scoping Surveys Scoping Surveys were not performed in this area based on its assessment as a non-industrialized area.

Characterization Based on a review of the general plant characterization data of the HBPP environs, Cs-137 was the only plant-related radionuclide that was identified consistently in the characterization samples analyzed. Seventy one (71) samples from previous characterization data were used to provide the characterization data for survey area OOLlO. The following data was sufficient to support the planning of Survey Unit HBPP-FSSP-OOLl 0-11.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 1O~12 Page 11 of 468

Cs-137 (51 detects)

Cs-137 was present in 72 % of the characterization samples.

Other HBPP ETD

There were no other easy to detect nuclides identified greater than Minimum Detectable Activity (>MDA).

There were no hard to detect nuclides identified in the four samples analyzed.

A more recent (2013) continuing characterization effort collected and analyzed six (6) randomly located sediment samples which were analyzed by gamma spectroscopy. One (1) sample tested positive for Cs-137, at 0.15 pCi/g. No other plant related isotopes were detected. As a conservative measure the characterization data for OOLlO soils were used to formulate the survey design.

Remedial Action Surveys and Activities No remedial Actions or surveys are known to have been performed in this Survey Unit.

Survey approach/methods The usual survey approach for Class 3 land areas would ordinarily consist of soil collection of statistically random locations and walk-over scanning of biasedly selected areas with a 2" x 2" NaI(Tl) scintillation detector. This approach could not be directly applied as the entire survey unit is normally submerged at high tide. So, the survey approach for the submerged sediment media of Fisherman's Channel was modified to accommodate field conditions.

A boat (See Figure 3) and a specially designed Ekman sample dredge were used to obtain the samples. It was also anticipated that not all sample point locations would be accessible, however all locations were accessed. No means was readily available to perform a gamma scan of submerged sediment media. As a consequence, four compensatory variances from the PSS program were applied:

The investigation level was reduced to 25% (from the required 50%) of the DCGL..

Samples were collected on a triangular grid with a random start point.

The samples were collected with an Ekman sampling dredge designed for collecting sediment.

Twenty (20) samples were collected; an increase from the statistically determined minimum number of fifteen (15).

FSS Report. HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 12 of 468 J

Figure 3 - FSS Survey Crew loads into boat at Fisherman's Channel.

Number samples and measurements The DQO process determined that Cs-137 is the radionuclide of concern in the Survey Unit.

Other radionuclides that were positively identified in concentrations greater than the screening criteria during the performance of this FSS would be evaluated to ensure adequate survey design .

The Sign Test (Ref.12) was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.

The minimum number of soil (sediment) samples for FSS was determined in accordance with Procedure RCP FSS-7, "Determination of the Number and Location of FSS Samples" (Ref.5).

The Lower Bound of the Gray Region (LBGR) was set in accordance with Procedure RCP FSS-7 to achieve a relative shift (f../cr) in the range between 1 and 3. The resulting relative shift was 7.22 pCi/g Cs-137.

A Prospective Power Curve was generated using MARSSIM Power 2000 (Ref. 6). MARSSIM Power 2000 is a software package developed under the sponsorship of the United States Department of Energy Environmental Measurement Laboratory.

The grid pattern and locations of the soil samples were determined using Visual Sample Plan (VSP) in accordance with Procedure RCP FSS-18, "Computer Determination ofNumber and Locations of FSS Samples" (Ref. 7). Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy (Ref. 8). A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate and conservative for a Class 3 area.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 13 of 468

Sample locations were identified using AutoCAD, a commercially available plotting software

package with coordinates consistent with the California State Plane System. These coordinates were integrated with a GPS to locate sample locations in the field. Sample measurement locations for the design are listed with the GPS coordinates in Table 2.

, Table 2 - Sample Measurement Locations with Associated GPS Coordinates (Survey Unit HBPP-FSSP-OOLl0-11)

Desig11cat~on Northing Easting*

OOLl0-11-001-F 5946542.65 2159425.53 OOLl0-11-002-F 5946651.69 2159236.68 OOLl0-11-003-F 5946760.72 2159047.82 OOLl0-11-004-F 5946869.75 2158858.97 OOLl0-11-005-F 5946978.79 2159047.82 OOLl0-11-006-F 5946869.75 2159236.68 OOLl0-11-007-F 5947196.85 2159047.82 OOLl0-11-008-F 5947196.85 2159425.53 OOLl0-11-009-F 5947307.58 2159235.52 OOLl0-11-010-F 5947414.92 2159425.53 OOLl0-11-011-F 5947303.86 2159622.98 OOLl0-11-012-F 5947414.92 2159803.23 OOLl0-11-013-F 5947523.96 2159614.38 OOLl0-11-014-F 5947632.99 2159425.53 OOLl0-11-015-F 5947523.96 2159992.09 OOLl0-11-016-F 5947632.99 2159803.23 OOLl0-11-017-F 5947742.02 2159614.38 OOLl0-11.-018-F 5947960.09 2160369.79 OOLl0-11-019-F 5948178.16 2160369.79 OOLl0-11-020-F 5948505.26 2160180.94 NOTE: See Posting Plot in Attachment 4 for corresponding map of these sample locations.

Procedure RCP FSS-2 specifies that 5% of the samples are required to be selected for HTD analysis. Two (2) soil (sediment) samples or 5% of the number of samples that would be used for non-parametric statistical testing were randomly selected for HTD radionuclide analyses using the Microsoft Excel "RAND" function. Each of the selected samples was sent off-site for a full suite analysis of the HTD radionuclides specified in Table 1.

The LTP requires a minimum of 5% of the samples taken for non-parametric statistical testing be selected for split sample analyses with the off-site laboratory. The implementation of quality control measures as referenced by Procedure RCP FSS-11, "Split Sample Assess~entfor Final Status Survey," (Ref9) included the collection of one (1) soil sample for "split sample" analysis by the off-site laboratory. These locations were selected randomly using the Microsoft Excel "RAND" function. Additionally, Procedure HBAP C-202, "Final Status Survey Quality Assurance Project Plan" (Ref. 10) requires the 5% of the samples taken for non-parametric statistical testing be selected for QC Replicate analyses.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 14 of 468

Table 5-4 of the LTP specifies scanning coverage of"Judgmental" 1-10% for Class 3 areas. A variance from this requirement was taken as noted.

For this Class 3 survey unit, the "Investigation Level" for soil (sediment) sample measurement results is more conservative than that specified in LTP, Table 5-5. Table 3 provides a synopsis of the survey design.

Table 3 - Synopsis of the Survey Design Featllre Design. Criteria ,

Basis Survey Unit Land Area 76,520 m 2 Based on AutoCAD 15 required Type 1 and Type 2 errors were (15 Randomly 0.05, sigma was 0.18 pCi/g, the _

selected)

Number of Measurements LBGR was set at 7.22 pCi/g to 20 Taken on a fixed achieve a Relative Shift in the grid with random start range of 1 and 3 (L1/cr=2.0) point Grid Spacing 66.5m Based on triangular grid 7.58 pCi/g Cs-137 Administratively set to achieve Operational DCGL 24 mrem/yr TEDE (I) 25% of the Operational DCGL Soil (sediment) Investigation 1.90 pCi/g Cs-137 exceeds the L TP criteria for a Level Class 3 survey unit Scan surveys not The LTP requires 1- 10% of Scan Survey Area Coverage applicable; survey unit area coverage for Class 3 is a waterway sutvey units Detectable above background, NIA- Unit is a Scan Investigation Level Per the LTP for Class 3 Survey waterway Units (1) The allowable dose from easy-to-detect nuclides in this survey unit is limited to 24 inrem/yr TEDE as the bounding dose from hard-to-detect nuclides is 1 mrem/yr.

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 15 of 468

Survey Results HBPP-FSSP-OOLl0-11 Sample measurements results All field survey activities were performed on April 28 and April 29, 2014.

The on-site laboratory analyzed the twenty (20) samples collected for non-parametric statistical testing, the associated field splits and one (1) QC replicate sample using gamma spectroscopy.

Gamma spectroscopy analysis was performed to the required MDCs. No plant derived isotopes were positively detected.

Cs-137 was not identified in any of the twenty (20) samples collected for non-parametric statistical testing. A summary of the twenty (20) samples collected for non-parametric statistical testing results is provided in Table 4.

Table 4 - Summary of Gamma Spectroscopy Results for Sediment Samples Compnsmg th e Sta f1sf 1ca I Samp Ie Popu Iaf ion Sample Number Cs-137 pCi/g Percentage of DCGL OOLI0-11-001-F 4.94E-02 6.52E-01 OOLl0-11-002-F 8.63E-02 l.14E+OO OOLI0-11-003-F 3.17E-02 4.18E-01 OOLl0-11-004-F 9.44E-02 l.25E+OO OOLl0-11-005-F 9.30E-02 l.23E+OO OOLI0-11-006-F l.42E-01 l.87E+OO OOLl0-11-007-F 6.44E-02 8.50E-01 OOLl0-11-008-F 6.79E-02 8.96E-01 OOLl0-11-009-F l.03E-01 l.36E+OO OOLI0-11-010-F 2.70E-02 3.56E-01 OOLI0-11-011-F l.33E-01 l.75E+OO OOLI0-11-012-F 9.40E-02 l.24E+OO OOLI0-11-013-F 8.48E-02 l.12E+OO OOLl0-11-014-F l.06E-01 l.40E+OO OOLl0-11-015-F 7.35E-02 9.70E-01 OOLl0-11-016-F 6.24E-02 8.23E-01 OOLl0-11-017-F 4.45E-02 5.87E-01 OOLl0-11-018-F 7.04E-02 9.29E-01 OOLI0-11-019-F 9.92E-02 l.31E+OO OOLl0-11-020-F 5.63E-03 7.43E-02 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 16 of 468

The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories, LLC. The off-site laboratory processed two (2) samples for HTD analyses as required by the sample plan. The requested analyses included alpha spectroscopy, gas proportional counting, and liquid scintillation depending on the radionuclide and the measurement method. All analyses performed met the required minimum MDC. Neither of these results tested positive for Cs.-13 7 or other plant derived nuclides. All laboratory sample results are Included as Attachment 3.

Fixed-point radiation measurements Sediment samples were used as fixed point measurements.

Scan data Scanning was not performed as it was not a feature of the design of this FSS, as noted previously.

Survey Unit Data Assessment HBPP-FSSP-OOLl0-11 Statistical Evaluations The DQO sample design and data were reviewed in accordance with Procedure RCP FSS-14, "Data Quality Assessment" (Ref. 11) for completeness and consistency. The sampling design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed (by inspection) on the data and compared to the original assumptions of the DQOs.

The evaluation of the Sign Test results demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected.

Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 3.

The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). The mean and median values are well below the Operational DCGL. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs. The basic statistical quantities for the statistical sample population are provided below in Table 5.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 17 of 468

Table 5 - Basic Statistical Quantities Cs-137 Statistic Fraction of the DCGL (pCi/~).

DCGLon llJ: 7.58E+OO 1.00E+OO Minimum Value: 5.63E-03 7.43E-04 Maximum Value: l.42E-01 l.87E-02 Mean: 7.66E-02 l.OlE-02 Median: 7.92E-02 l.04E-02 Standard Deviation: 3.43E-02 4.52E-03 1

DCGL0 p is the "operational DCGL" that is adjusted to conservatively account for potential dose from Hard-to-Detect radionuclides.

The range of the data is approximately 4 standard deviations, not a particularly large variation.

The difference between the mean and median was about 0.074 of the standard deviation which indicates very limited skewness in the data. The <;lata was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot indicates a very slight skewness as confirmed by the calculated skew of -0.14.

Graphical Evaluations All data, assessments, and graphical representations are provided in Attachment 3 and Attachment 4.

Survey Unit Investigations and Results HBPP-FSSP-OOLl0-11 No investigations were performed for Survey Unit HBPP-FSS-OOLI0-11.

ALARA Statement HBPP-FSSP-OOLl0-11 A Generic Technically Based Document has been prepared to demonstrate that it is not ALARA to remediate soil to levels below the DCGL. It is provided in Attachment 5.

Changes in Initial Survey Unit Assumptions HBPP-FSSP-OOLl0-11 None of the initial assumptions were changed as a result of information gained in the performance of the FSS survey or in reviewing its results.

Quality Assurance and Corrective Actions HBPP-FSSP-OOLl0-11 Corrective actions While performing the data quality assessment it was determined that the QC recount of Sample HBPP-FSSP-OOLl 0-11-020 and its recount did not achieve an acceptable level of agreement.

The comparison was based onK-40 alone since this was the only isotope detected in the matrix.

The issue was investigated by pulling the archived sample matrix and repeating the recount exercise. Upon reviewing these results it was determined that one count appeared to be an outlier as the initial and second repeat results were in good agreement.

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 18 of 468

The issue was input into site's corrective action tracking system as SAPN No. 1390520. It was concluded that the disagreement detected did not affect the validity or reliability of the balance of the sample results based on the fact that the two other split sample comparisons of this unit were in good agreement and that the nuclide being compared was not a plant derived nuclide. K-40 is ubiquitous in the environment and measurements may be influenced by the detectability of K-40 sources outside the detector shield.

Quality Verification Quality Verification (QV) Assessment# 140830025 defined its scope as follows: "This assessment will verify adequacy of the Survey Plan for the PSS of the Fisherman's Channel.

This particular survey introduces a number of variables that are atypical of a PSS of soils areas.

This assessment will verify that these variables are appropriately addressed in the survey plans.

The QV concluded that while PSS plan number HBPP-FSSP-OOLl0-11-00 (Attachment 1) adequately addresses the unique challenges present by the PSS of the Fisherman's Channel but it also commented that, "When the survey plan was compared against the procedure for the preparation ofFSS survey plans a number of minor discrepancies were identified. Many of the discrepancies were a result of using an uncontrolled copy of the form. Other inconsistencies were noted in the plan. For example at one place in the survey plan, the area was referred to as the "Intake Canal" rather than the "Fisherman's Channel". The identified discrepancies did not affect the performance of an experienced technician. The Data quality is not compromised.

These discrepancies could however affect the quality of records."

The results of this assessment were reviewed with the responsible engineer and appropriate actions are being formulated. The discrepancies identified are addressed in Notification 1388478. QV Assessment# 140830025 is included as Attachment 6.

Survey Unit Description HBPP-FSSP-OOLl0-12 Survey 00110-12 is a part of Survey Area 00110 which consists of the surface area of the remainder of the HBPP land area. The survey unit is made up of coastal marshland that is devoid of plant related structures. It is bordered by Survey Unit 00110-11 over most of its boundary, in addition to off-site locations to plant south and King Salmon A venue to plant east.

It is approximately 46,364 square meters of surface area.

HSAEvents There is no mention of plant related activities occurring within the boundaries of this Survey Unit.

Scoping Surveys Scoping Surveys were not performed in this area.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 19 of 468

Characterization Based on a review of the general plant characterization data of the HBPP environs, Cs-137 was the only plant-related radionuclide that was identified consistently in the characterization samples analyzed. Seventy one (71) samples from previous characterization data were used to provide the characterization data for survey area 00110. The data was sufficient to support the planning of Survey Unit HBPP-FSSP-001I0-12.

Cs-137 (51 detects)

Cs-137 was present in 72 % of the characterization samples.

Other HBPP ETD

There were no other easy to detect nuclides identified >MDA.

There were no hard to detect nuclides identified in the four (4) samples analyzed.

Remedial Action Surveys and Activities No remedial Actions or surveys are known to have been performed in this Survey Unit.

Survey Unit Design Information HBPP-FSSP-OOLl0-12 Data Qualify Objectives (DQOs)

I FSS design and planning used the Data Quality Objective (DQO) process as described by the LTP, Procedure RCP FSS-2, "Preparation of Final Status Survey Plan," and the "Multi-Agency Radiation Survey and Site Investigation Manual" (MARSSIM). A summary of the main features of the DQO process are provided herein.

The DQO process incor.porated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is techniCally known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria.

The primary objective of the FSS plan was to demonstrate that the level ofresidual radioactivity in Survey Unit HBPP-FSSP-00110-12 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development ofDCGLs. The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil.

Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 20 of 468

The total dose under the LTP criteria is 25 mrem/yr Total Effective Dose Equivalent (TEDE) from all of the potentially present plant derived nuclides.

The presence of all radionuclides listed (gamma-emitters, HTD beta-emitters, and TRUs) in the soil (sediment) were evaluated under survey plan HBPP-FSSP-OOLl0-12-00 (Attachment 7).

DQOs re Nuclide Selection and DCGLs As was the case for Survey Unit HBPP-FSSP-QOLl0-11 within Survey Unit BBPP-FSSP-OOLl0-12 no HTD nuclides were expected to be present, the contribution from HTD nuclides (except for H-3 and Sr-90, were measured on-site for each sample) were bounded by directly adding the dose contribution of a sample contaminated to approximately 3 times the DCGL

(~22 pCi/g) for Cs-137. The resultant dose from these HTD nuclides is less than 1 mrem/yr, as shown in Attachment 2.

Also, it was identified that because the expected timing of the Phase 1 release, occurs prior to the current license termination scheduled date 2019, Fe-55 screens into the nuclide suite as a potential nuclide of concern. At present a site specific DCGL for Fe-55 does not exist; however, since Fe-55 has not been detected and would not be expected to be present in detectable concentrations in Class 3 plant areas, the Generic Screening value ofNUREG 1757 Vol. 2 (Ref 4.) was applied as the DCGL. Table 1 presents the Soil DCGLs per the HBPP LTP. Cs-137, the only nuclide expected to be present was scaled to a TEDE of24 mrem/yr to account for any HTD nuclides that might be present.

Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration and variability.

As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. Results reported as less than the Minimum Detectable Concentration (MDC) were not used for FSS. Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty to two (2) standard deviations, laboratory data qualifiers, units, and the required and observed MDC.

Survey approach/methods The survey approach was typical for Class 3 land area survey units and utilized the Sign Test from statistically random locations. Cs-137 was the principal nuclide of concern. Walk-over scanning ofbiasedly selected areas with a 2" x 2" Nal(TI) scintillation detector was also a feature of the survey unit design (See Figure 4). Some quality assurance measures incorporated to the FSS plart included repeat and split sample comparisons in addition to pre-and post-source checks of scanning instruments.

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 21 of 468

Figure 4 - Walkover scan being performed on the opposite shoreline of Fisherman's Channel Number samples and measurements The DQO process determined that Cs-137 is the radionuclide of concern in Survey Unit. Other radionuclides that were positively identified in concentrations greater than the screening criteria during the performance of this FSS would be evaluated to ensure adequate survey design.

The Sign Test (Ref.12) was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.

The minimum number of soi l (sediment) samples for FSS was determined in accordance with Procedure RCP FSS-7, "Determination of the Number and Location of FSS Samples ". The Lower Bound of the Gray Region (LBGR) was set in accordance with Procedure RCP FSS-7 to achieve a relative shift (6./cr) in the range between 1 and 3. The resulting relative shift was 7.22 pCi/g Cs-137.

A Prospective Power Curve was generated using MARS SIM Power 2000. MARSSJM Power 2000 is a software package developed under the sponsorship of the United States Department of Energy Environmental Measurement Laboratory.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 22 of 468

The grid pattern and locations of the soil samples were determined using Visual Sample Plan (VSP) in accordance with Procedure RCP FSS-18, "Computer Determination ofNumber and Locations of FSS Samples." Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy. A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate and conservative for a Class 3 area.

Sample locations were identified using AutoCAD, a commercially available plotting software package with coordinates consistent with the California State Plane System. These coordinates were integrated with a GPS to locate sample locations in the field; Sample measurement locations for the design are listed with the GPS coordinates in Table 6.

Table 6 - Sample Measurement Locations with Associated GPS Coordinates HBPP-FSSP-OOLl0-12 Designation Northing Easting 00110-12-001-F 5947081.59 2159247.24 00110-12-002-F 5947279.91 2159362.50 00110-12-003-F 5947896.89 2159566.82 00110-12-004-F 5947867.51 2159692.56 00110-12-005-F 5947779.37 2159944.03 00110-12-006-F 5948021.76 2159671.60 00110-12-007-F 5947749.99 2160069.77 00110-12-008-F 5947933.62 2159985.94 00110-12-009-F 5948043.79 2159881.16 00110-12-010-F 5948220.07 2159786.86 00110-12-011-F 5947904.24 2160237.42 00110-12-012-F 5948014.41 2160132.64 00110-12-013-F 5948198.04 2160048.81 00110-12-014-F 5948102.55 2160258.37 00110-12-015-F 5948168.66 2160174.55 00110-12-016-F 5948374.32 2159954.51 00110-12-017-F 5948278.83 2160164.07 00110-12-018-F 5948433.08 2160331.72 00110-12-019-F 5948455.11 2160352.68 00110-12-020-F 5948521.22 2160268.85 Procedure RCP FSS-2 specifies that 5% of the samples are required to be selected for HTD analysis. Two (2) soil (sediment) samples or 5% of the number of samples that would be used for non-parametric statistical testing were randomly selected for HTD radionuclide analysis using the Microsoft Excel "RAND" function. Each of the selected samples was sent off-site for a full suite analysis of the HTD radionuclides specified in Table 1.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 23 of 468

The LTP requires a minimum of 5% of the samples taken for non-parametric statistical testing be selected for split sample analyses with the off-site laboratory. The implementation of quality control measures as referenced by Procedure RCP FSS-11, "Split Sample Assessment for Final Status Survey," included the collection of one (1) soil sample for "split sample" analysis by the off-site laboratory. These locations were selected randomly using the Microsoft Excel "RAND" function. Additionally, Procedure HBA.P C-202, "Final Status Survey Quality Assurance Project Plan", requires the 5% of the samples taken for non-parametric statistical testing be selected for QC Replicate analyses.

Table 5-4 of the LTP specifies scanning coverage of"Judgmental" 1-10% for Class 3 areas.

This requirement was conservatively met by performing scan surveys covering approximately ten percent (10%) of the units surface area.

For this Class 3 survey unit, the "Investigation Level" for soil (sediment) sample measurement results is more conservative than that specified in LTP, Table 5-5. Table 7 provides a synopsis of the survey design.

Table 7- Synopsis of the Survey Design HBPP-FSSP-OOLl0-12 Feature Design Criteria Basis 2

Survey Unit Land Area 46,364 m Based on AutoCAD Type 1 and Type 2 errors 15 required were 0.05, sigma was 0.18 pCi/g, the LBGR was set at Number of Measurements (20 Randomly selected 7.22 pCi/g to achieve a were taken) Relative Shift in the range of 1 and 3 (~/cr=2.0)

Sample points were Grid Spacing NIA randomly selected 7.58 pCi/g Cs-137 Administratively set to Operational DCGL achieve 24 mrem/yr TEDE (!)

50% of the Operational 3.79 pCi/g Cs-137 DCGL meets the LTP Soil Investigation Level criteria for a Class 3 survey unit The L TP requires 1- 10% of Scan Survey Area Coverage Approximately 10%. area coverage for Class 3 survey units Detectable above Detectable above Scan Investigation Level background, Per the LTP for background Class 3 Survey Units (1) The allowable dose from easy-to-detect nuclides in this survey unit is limited to 24 mrem/yr TEDE as the bounding dose from hard-to-detect nuclides is 1 mrem/yr.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 24 of 468

Survey Results HBPP-FSSP-OOLl0-12 Sample measurements results All field survey activities were performed on April 30, 2014.

The on-site laboratory analyzed the twenty (20) samples collected for non-parametric statistical testing, the associated field splits and one (1) QC replicate sample using gamma spectroscopy.

Gamma spectroscopy analysis was performed to the required MDCs. Cs-137 was the only plant derived isotope that was positively detected.

Cs-137 was identified in nine (9) of the twenty (20) samples collected for non-parametric statistical testing. A summary of the twenty (20) sample results collected for non-parametric statistical testing results is provided in Table 8.

Table 8 - Summary of Gamma Spectroscopy Results for Surface Soil Samples Compnsmg th e Staf 1s f1caI Samp Ie Popu laf ion HBPP -FSSP -OOLlO -12 Sample Number Cs-137 pCi/g Percentage of DCGL OOLl0-12-001-F 3.lSE-01 4.20E+OO OOLl0-12-002-F l.62E-01 2.14E+OO OOLl0-12-003-F 1.74E-01 2.30E+OO 00L10-12-004-F 3.25E-01 4.29E+OO OOLl0-12-005-F 4.57E-02 6.03E-01 OOLl0-12-006-F -1.04E-02 -l.37E-01 OOLl0-12-007-F 1.24E-01 l.64E+OO OOLl0-12-008-F 2.73E-01 3.60E+OO OOLl0-12-009-F 5.74E-02 7.57E-01 OOLl0-12-010-F l.19E-02 l.57E-01 OOLl0-12-011-F l.56E-01 2.06E+OO OOL 10-12-012-F 3.94E-01 5.20E+OO OOLl0-12-013-F 1.19E+OO l.57E+Ol OOLl0-12-014-F 2.79E-01 3.68E+OO OOLl0-12-015-F 5.17E-01 6.82E+OO OOLl0-12-016-F 2.53E-01 3.34E+OO OOLl0-12-017-F l.95E-01 2.57E+OO OOLl0-12-018-F l.47E-01 l.94E+OO OOLl0-12-019-F 7.23E-02 9.54E-01 OOLl0-12-020-F 5.31E-02 7.0lE-01 NOTE: Bold text indicates results that were greater than laboratory MDC.

The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories, LLC. The off-site laboratory processed two (2) samples for HTD analyses as required by the sample plan. The requested analyses included alpha spectroscopy, gas proportional counting, and liquid scintillation depending on the radionuclide and the measurement method. All analyses performed met the required minimum MDC.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 25 of 468

Neither of these results tested positive for Cs-137 or other plant derived nuclides. All laboratory sample results are included as Attachment 3.

Fixed-point radiation measurements Soil samples were used as fixed point measurements.

Scan data Scanning was performed on greater than 10% of the area, exceeding the coverage minimum called for in the LTP. A portion of the area scanned included a small amount extended into Survey Unit HBPP-FSSP-OOLl0-11 since it became accessible at low tide. The background ranged from approximately 3-4.7 kcpm which compares well with the anticipated range of 3.2 to 5.4 kcpm predicted in the plan. No indications above background were encountered. Field notes related to scanning are included as part of Attachment 3.

Survey Unit Data Assessment HBPP-FSSP-OOLl0-12 Statistical Evaluations The DQO sample design and data were reviewed in accordance with Procedure RCP FSS-14, "Data Quality Assessment, " for completeness and consistency. The sampling design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed (by inspection) on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected.

Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 3.

The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). The mean and median values are well below the Operational DCGL. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs. The basic statistical quantities for the statistical sample population are provided below in Table 9.

Table 9 - Basic Statistical Quantities HBPP-FSSP-OOLl0-12 Cs-137 Statistic Fraction of the DCGL (pCi/g)

DCGLoo llJ: 7.58E+OO l.OOE+OO Minimum Value: -1.04E-02 -l.37E-03 Maximum Value: l.19E+OO l.57E-01 Mean: 2.37E-01 3.13E-02 Median: l.68E-01 2.22E-02 Standard Deviation: 2.63E-01 3.46E-02 1

DCGLop is the "operational" DCGL that is adjusted to conservatively account for potential dose from Hard-to-Detect radionuclides.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 26 of 468

The range of the data is approximately 4.57 standard deviations, not a particularly large variation. The difference between the mean and median was about -0.26 of the standard deviation which indicates some skewness in the data. The data was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot indicates a positive skewness as confirmed by the calculated skew of2.71.

Graphical Evaluations All data, assessments, and graphical representations are provided in Attachment 3 and Attachment 8.

Survey Unit Investigations and Results HBPP-FSSP-OOLl0-12 No investigations were performed for Survey Unit HBPP-FSSP-OOLl0-12.

ALARA Statement HBPP-FSSP-OOLl0-12 A Generic Technically Based Document has been prepared to demonstrate that it is not ALARA to remediate soil to levels below the DCGL. It is provided as Attachment 5.

Changes in Initial Survey Unit Assumptions HBPP-FSSP-OOLl0-12 None of the initial assumptions were changed as a result of information gained in the performance of the FSS survey or in reviewing its results.

Quality Assurance and Corrective Actions HBPP-FSSP-OOLl0-12 Each of the QA related sample comparisons compared favorably against the comparison criteria of Procedure RCP FSS-11, Split Sample Assessment for Final Status Survey. Survey Instruments were verified to be properly calibrated and passed their required pre-survey and post-survey source checks. No anomalies or corrective actions were noted.

Conclusion Survey Units HBPP-FSSP-OOLl0-11 and HBPP-FSSP-OOLl0-12 meet the final DQOs of their respective FSS. The ALARA criterion for soils as specified in the LTP was achieved (Attachment 5). Elevated Measurement Comparison and remediation were not required for either survey unit.

Survey Unit HBPP-FSSP-OOLl0-11 The sample data passed the Sign Test. The null hypothesis was rejected. Graphical representation of data indicates very limited positive skewness. The Retrospective Power Curve generated shows adequate power was achieved. The survey unit was properly designated as Class 3.

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 27 of 468

The hypothetical dose contribution from sediment is 0.25 mrem/yr TEDE based on the average concentration of the samples used for non-parametric statistical sampling.

The average hypothetical total dose from residual radioactivity in this survey unit, including that from HTDs in the sediment, will not exceed 1.25 mrem/yr Total Effective Dose Equivalent (TEDE).

Survey Unit HBPP-FSSP-OOLl0-12 The sample data passed the Sign Test. The null hypothesis was rejected. Graphical representation of data indicates very limited positive skewness. The Retrospective Power Curve generated shows adequate power was achieved. The survey unit was properly designated as Class 3.

The hypothetical dose contribution from sediment is 0.78 mrem/yr TEDE based on the average concentration of the samples used for non-parametric statistical sampling.

The average hypothetical total dose from residual radioactivity in this survey unit, including that from HTDs in the sediment, will not exceed 1.78 mrem/yr Total Effective Dose Equivalent (TEDE).

References 1.0 Humboldt Bay Power Plant License Termination Plan, Rev. 1 Submitted, August, 2014.

2.0 HBPP Procedure RCP FSS-2, "Preparation of Final Status Survey Plan", Rev. OD, September 11, 2013.

3.0 NUREG 1575 Multi Agency Radiation Site Survey and Investigation Manual, (MARSSIM), USNRC Rev. 1 August, 2000.

4.0 NUREG 1757, Vol. 2 Consolidated Decommissioning Guidance "Characterization, Survey, and Determination ofRadiological Criteria",

Rev. 1. USNRC, September, 2006.

5.0 HBPP Procedure RCP FSS-7, "Determination of the Number and Location ofFSS Samples" Rev. OC, September 11, 2013.

6.0 MARS SIM Power 2000 software, V. 1.0.0 Environmental Measurements Laboratory, US Department of Energy, December 2000.

7.0 HBPP Procedure RCP FSS-18, "Computer Determination ofNumber and Locations of FSS Samples, Rev. OC, September 11, 2013.

8.0 VSP Development Team (2014). Visual Sample Plan: A Tool for Design and Analysis of Environmental Sampling. Version 6.2d. Pacific Northwest National Laboratory.

Richland, WA. http://vsp.pnnl.gov.

9.0 HBPP Procedure RCP FSS-11, "Split Sample Assessment for Final Status Survey" Rev.

OC, September 11, 2013.

10.0 HBPP Procedure HBAP C-202, "Final Status Survey Quality Assurance Project Plan" Rev. 3, June 5, 2014.

11.0 HBPP Procedure RCP FSS-14, "Data Quality Assessment" Rev. OC, September 11, 2013.

12.0 HBPP Procedure RCP FSS-15, "Statistical Test" Rev. OC, September 11, 2013.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 28 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOLl0-11-00 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 29 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL 10-11-00 Final Status Survey Planning Worksheet Page 1 of 11 GENERAL SECTION Survey Area No: OOL 10 j Survey Unit No: 11 Survey Unit Name: Fisherman's Channel Final Status Survey Number: HBPP-FSSP-OOL 10-11-00 PREPARATION FOR FINAL STATUS SURVEY ACTIVITIES Check marks in the boxes below signify affirmative responses and completion of the action.

1.1 Files have been established for survey unit FSS records. Yes 0 No 0 N/A D 1.2 ALARA review has. been completed for the survey unit. Yes 0 No D N/A 0 1.3 The survey unit has been turned over for final status survey. Yes 0 No D N/AD 1.4 An initial walkdown has been performed 0 1.5 Activities conducted within area since turnover has been reviewed. 0 Based on reviewed information, subsequent walkdown: 0 not warranted D warranted If warranted, subsequent walkdown has been performed and documented OR The basis has been provided to and accepted for not performing a subsequent walkdown. 0 1.6 A final classification has been performed. 0 Classification: CLASS 1 D CLASS 2 0 CLASS 3 0 DATA QUALITY OBJECTIVES (DQO)

For each survey unit area, an adequate final status survey must be designed to demonstrate compliance with the release criteria per the License termination Plan. That is the Objective of this Plan.

FSS Renart HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Paae 30 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL10-11-00 Final Status Survey Planning Worksheet Page 2of11 1.0 State the problem:

Survey Area OOL-10 consists of the surface area of the remainder of the HBPP land area. Survey Unit OOL-10-11 (Fisherman's Channel) is completely covered by seawater at high tide and will require a boat arid sample dredge to acquire sediment samples for final status survey. It is anticipated that some areas may be inaccessible due to safety and/or access concerns.

The balance of the survey unit's boundary abuts OOL 10 and off-site locations. It is approximately 76;520 square meters of surface area.

The problem as defined by this survey plan is to demonstrate that the years of plant operation did not result in an accumulation of plant-related radioactivity that exceeds the release criteria. PG&E intends to submit a request to the USNRC for an early phase release for this and adjacent Survey Unit OOL 10-12 in accordance with 10CFR20 subpart E. The planned early release causes Fe-55 to screen in as a potential nuclide of concern. At present a site specific DCGL for Fe-55 does not exist.

There is, at present, no readily available means to perform a gamma scan of submerged sediment media. As a consequence, four compensatory variances from the FSS program will be applied:

o The investigation level is reduced to 25% (from the required 50%) of the DCGL.

e Samples will be collected on a triangular grid with a random start point.

o The samples are collected with an Ekman sampling dredge designed for collecting sediment.

e 20 samples will be collected; an increase from the statistically determined minimum number of 15.

The planning team for this effort consists of the Site Closure Manager, FSS Engineers, FSS Foreman and FSS Technicians. The FSS Engineers will make primary decisions with the concurrence of the Site Closure Manager.

2.0 Identify the decision:

Does residual plant-related radioactivity, if present in the survey unit, exceed the release criteria?

Alternative actions may include no action, investigation, resurvey, remediation and reclassification.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 31 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL 10-11-00 ,

Final Status Survey Planning Worksheet Page 3of11 3.0. Identify the inputs to the decision:

Sample media: Sediment Types of measurements: Sediment samples Radionuclides-of-concern: Cs-137 Applicable DCGL: The DCGLs applied under this survey plan correspond to the soil (sediment) dose as determined in the LTP. For Fe-55, the screening level DCGLs ofNUREG 1757 Vol. 2 were applied for interim use until a site specific DCGL is determined.

Nuclide DCGL Nuclide DCGL Nuclide DCGL (pCi/g) (pCi/g) (pCr/g)

H-3 6.8E+02 1-129 4.8E+OO Pu-241 8.6E+02 C-14 6.3E+OO Cs-137 7.9E+OO Am-241 2.5E+01 Ni-59 1.9E+03 Eu-152 1.0E+01 Cm-243 2.9E+01 Co-60 3.8E+OO Eu-154

9.4E+OO Cm-244 4.8E+01 Ni-63 7.2E+02 Np-237 1.1E+OO Cm-245

1.7E+01 Sr-90 1.5E+OO Pu-238 2.9E+01 Cm-246 2.5E+01 Nb-94 7.1E+OO Pu-239 2.6E+01 Fe-55 1.0E+04 Tc-99 1.2E+01 Pu-240 2.6E+01 Based on a review of the general plant characterization data of the HBPP environs, Cs-137 was the only plant-related radionuclide that was identified consistently in the characterization samples analyzed.

Seventy one (71) samples from previous characterization data were used to provide the characterization data for survey area OOL 10. The data is sufficient to support the planning of Survey UnitOOL10-11.

o Cs-137 (51 detects) Cs-137 is present in 72 % of the characterization samples.

o Other HBPP ETD There were no other easy to detect nuclides identified >MDA.

e HBPP HTD There were no hard to detect nuclides identified in the four samples analyzed.

A more recent (2013) continuing characterization effort collected and analyzed six randomly located sediment samples which were analyzed by gamma spectroscopy. One sample tested positive for Cs-137 at 0.15 pCi/g. No other plant related isotopes were detected. As a conservative measure the characterization data for OOL 10 soils were used to formulate the survey design.

The presence of all radionuclides listed in this plan (gamma-emitters, HTD beta-emitters, and TRUs) in the soil (sediment) will be evaluated under this survey plan. Although no HTD nuclides are expected to be present, the contribution from HTD nuclides (except for H-3 and Sr-90, which will be measured on-site for each sample) will be bounded by directly adding the dose contribution of a sample contaminated to a roximatel 3 times the DCGL ~22 Ci/ for Cs-137. The resultant dose from these HTD FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 32 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL10-11-00 Final Status Survey Planning Worksheet Page 4of11 nuclides is less than 1 mrem/y.

A consequence of the planned early site release for this area is that the earlier date (Prior to 2019) for site release causes Fe-55 to screen ih as a potential nuclide of concern. The sample will be counted for Fe-55 based on the screening level DCGLs of NUREG 1757 Vol 2. The sample will be retained, per the requirements of the FSS program, in case it is later determined that. a re-analysis for Ee-55 is necessary.

The HBPP Site Closure Laboratory will analyze each soil sample for all listed gamma-emitting nuclides,

$r-90 and Tritium. In addition, 2 FSS soil samples will be sent to an independent laboratory for analyses of gamma-emitters and HTD radionuclides.

Survey Design /Release Criteria Classification: Class 3 Average Cs-137 concentration: 0.38 pCi/g Standard deviation Cs- 137 (a): 0.18 pCi/g .

Surrogate DCGL: NIA (a surrogate DCGL will not be used)

LBGR: Initial= O.SxDCGL = 3.79 pCi/g Cs-137 Adjusted LBGR( set /J./a = 2.0) = 7.22 pCi/g Cs-137 Number of Samples: Calculated = 15 Survey Unit Area: 76,520 m 2 Grid Area (AIN): N/A Class 3 DCGLemo Cs-137: NIA Class 3 Investigation Level for soil samples: > 25% DCGL for Cs-137 = 1.98 pCi/g Cs-137 Gamma scanning Coverage: N/A Investigation Level for SPA-3 Scans: NIA Radionuclides for analysis: All listed nuclides with the focus on Cs-137 The HBPP onsite laboratory will analyze each sediment sample for all listed gamma-emitting nuclides.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 33 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL 10-11-00 Final Status Survey Planning Worksheet Page 5of11 Survey Design /Release Criteria Radionuc/ides for analysis: All listed nuclides with the focus on Cs-137 MDCs for gamma analysis of soil samples: Nuclide 10% to %50 of the DCGL {pCi/g)

Co-60 3.BE-01 to 1.9E+OO Nb-94 7.1E-01 to

3.55E+OO 1-129 4.BE-01 to , 2.4E+OO Cs-137* 7.58E-01 to 3.79E+OO Eu-152 1.0E+OO to 5.0E+OO Eu-154 9.40E-01 to 4.70E+OO Np-237 1.1 E-01 to s:sE~o1 The desired MDCs in the laboratory analyses .of soil samples will be the 10% .DCGL values. If it is impractical to achieve those, the 50% DCGL values must be achieved in the laboratory analyses of the sediment samples.

The DCGL for Cs-137, the only nuclide expected to be present, has bee~ reduced to 24 mrem/y to account for any HTDs that may be present.

MDC's for HTD nuclide:

Nuclide 10% to 50% of the DCGL (pCi/g}

H-3 6.8E+01 3.4E+02 C-14 6.3E-01 3.15E+OO F.e-55 1.0E+03 5.0E+03 Ni-59 1.9E+02 9.5E+02 Ni-63 7.2E+01 3.6E+02 Sr-90 1.5E-01 7.5E-01 Tc-99 1.2E+OO 6.0E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 34 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL 10-11-00 Final Status Survey Planning Worksheet Page 6of11 Pu-238 2.9E+OO 1.45E+01 Pu-239/240 2.6E+OO 1.3E+01 Pu-241 8.6E+01 4.3E+02 Am-241 2.5E+OO 1.25E+01 Cm-243 2.9E+OO 1.45E+01 Cm-244 4.8E+OO 2.4E+01 Cm-245 1.7E+OO 8.5E+OO Cm-246 2.SE+OO 1.25E+01 The MDC values for difficult to detect nuclides will be.

conveyed to the outside laboratory via the sample Chain-Of-Custody form which will accompany the sediment saf!lples.

4.0 Define the boundaries of the survey:

0 Boundaries of Survey Areas are as shown on the attached map. This area is bordered by the Survey Area off-site locations or OOL 10 on all sides.

o The survey will be performed at high tide and under safe marine weather conditions (as defined by instrumentation and/or equipment limitations and human factors). Surveys will be performed during daylight hours.

5.0 Develop a decision rule:

Upon review of the FSS d~ta collected under this survey plan:

(a) If all the sample data show that the sediment concentrations of plant related nuclides. are below the DCGLs and the sum of fractions of nuclides are below unity, then reject the null hypothesis (i.e., Survey Unit OOL 10-11 meets the release criteria).

(b) If the investigation levels are exceeded, then perform an investigation survey.

(c) If the average concentration of any listed nuclide exceeds its respective DCGL or the average sum of fractions for any listed nuclide exceeds one, then accept the null hypothesis (i.e., Survey Unit OOL 10-11 fails to meet the release criteria).

Note: Alternate actions beyond investigations include remediation, reclassification and resurvev.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 35 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL 10-11-00 Final Status Survey Planning Worksheet Page 7of11 6.0 S12ecify tolerable limits on decision errors:

Null hypothesis: Residual plant-related radioactivity in Survey Unit OOL 10-11 exceeds the release criteria.

Probability of type I error: 0.05 Probability of type II error: 0.05 LBGR: Adjusted to 7.22 pCi/g Cs-137 7.0 Optimize Design:

Number and Location of Samples: Twenty (20) sediment samples will be collected at locations based on a triangular grid with a random startpoint.

IGENERAL INSTRUCTIONS

1. Measurement locations will be identified using GPS. Any locations that are not suitable for sediment sampling will be relocated to the nearest suitable location and documented on the survey map.

2. Chain of Custody form will be used for all sediment samples.

3. Alf sediment samples will be received and prepared as directed by the FSS Engineer.

4. The job hazards associated with the Survey described in this package will be addressed in the pre-job brief.

5. All personnel participating in this survey shall be trained in the operation of the -

instrumentation.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 36 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL10-11-00 Final Status Survey Planning Worksheet Page 8of11 ISPECIFIC INSTRUCTIONS

1. All designated measurement locations will be identified by GPS. If a designated sample location is obstructed for any reason, the FSS Engineer or the Lead FSS Technician will select an alternate location within Three meters of the original location. A detailed description of the alternate location will be recorded on the survey form, the survey unit map will be annotated appropriately, and the alternate location will be identified with GPS. GPS coordinates are provided in Table 1 (below).

Table 1 Sample Locations Sample Eastinq* Northinq*

Intake Canal OOL 10-11-001-F 5946542.65 2159425.53 OOL 10-11-002-F 5946651.69 2159236.68 OOL 10-11-003-F 5946760.72 2159047.82 OOL 10-11-004-F 5946869.75 2158858.97 OOL 10-11-005-F 5946978.79 2159047.82 OOL 10-11-006-F 5946869.75 2159236.68 OOL 10-11-007-F 5947196.85 2159047.82 OOL 10-11-008-F 5947196.85 2159425.53 OOL 10-11-009-F 5947307.58 2159235.52 OOL10-11-010-F 5947414.92 2159425.53 OOL 10-11-011-F 5947303.86 2159622.98 OOL 10-11-012-F 5947414.92 2159803.23 OOL10-11-013-F 5947523.96 2159614.38 OOL 10-11-014-F 5947632.99 2159425.53 OOL 10-11-015-F 5947523.96 2159992.09 OOL 10-11-016-F 5947632.99 2159803.23 OOL 10-11-017-F 5947742.02 2159614.38 OOL 10-11-018-F 5947960.09 2160369.79 OOL 10-11-019-F 5948178.16 2160369.79 OOL 10-11-020-F 5948505.26 2160180.94

CA Zone 1 NADB3/NAVD88

2. Sample Requirements:

o Collect twenty (20) 1-liter sediment samples in accordance with the instructions of this plan. Two (2) of the 20 sediment samples will be analyzed as QC split samples and one (1) will be a sample recount to fulfill the QC requirement. The QC split samples will also be anal zed for Hard-to-Detect nuclides.

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 37 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL10-11-00 Final Status Survey Planning Worksheet Page 9of11 e Sediment samples will be collected as follows:

o At the sample location, using a clean drop-dredge implement, deploy the dredge until approximately one liter of sediment material is obtained placing the soil in a sample container. If necessary sample may be decanted to remove excess water.

o Record the number of dredge drops that were required.

o Label the plastic bag with the sample location identifier.

o Transfer the bag of soils to the sample preparation area.

o Clean/decontaminate the dredging tool after each sample is taken.

3. Soil Sample Designation:

Statistical sediment samples: OOL 10-11-001-F through OOL 10-11-020-F corresponding to sample locations 001 through 020.

QC split samples: OOL 10-11-003-F-S and OOL 10-11-016-F-S arei to be designated as QC split samples.

These samples will be sent to the off-site laboratory.

Recount samples: OOL 10-11-020-F-RC is to be counted twice on site. The results will be compared as directed by the FSS Engineer.

4. Sample Analysis:

e Gamma analysis will be performed on all sediment samples. If any of the gamma analyses show that an investigation level has been exceeded an investigation survey will be conducted at that sample location as directed in specific instruction # 5.

o HBPP will analyze OOL 10-11-001-F through OOL 10-11-020-F for gamma-emitting nuclides, H-3 and Sr-90.

I) HBPP will analyze OOL 10-11-020-F as a sample recount. The recounted sample will possess the naming convention OOL 10-11-020-F-RC.

e HBPP will analyze OOL 10-11-003-F-S and OOL 10-11-016-F-S for gamma-emitting nuclides prior to being sent to the off-site laboratory. These samples will be analyzed for gamma emitting nuclides and HTD at the off-site laboratory.

o On-site gamma anal sis of the sam les shall achieve the MDC values stated in the DQO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 38 of 468

Attachment 1 Survey Plan HBPP-FSSP-OOL10-11-00 Final Status Survey Planning Worksheet Page 10of11 section of this plan. The MDC's for off-site analysis will be communicated to the laboratory using an attachment to the Chain-of-Custody form or previous direction that meets specified MDC's of this final status survey plan.

5. If the results of any sample analysis exceed an investigation level, perform a first level investigation as follows:

o Using the GPS establish the investigation sample points at 3m distance in the four compass directions around any confirmed elevated measurement location.

o Obtain a sediment sample at the identified locations. Designate the sample as "OOL 10-11 -xxx-F-1" where "xxx" continues sequentially from the last number assigned to an investigative sample.

o Sediment samples will be collected as follows:

o At the sample location, using a clean drop-dredge implement, deploy the dredge until approximately one liter of sediment material is obtained placing the soil in a sample container. If necessary sample may be decanted to remove excess water.

o Record the number of dredge drops that were required.

o Label the plastic bag with the sample location identifier. .

o Transfer the bag of soils to the s*ample preparation area.

o Clean/decontaminate the dredging tool after each sample is taken.

Prepared by: ------'{)'---'J"-=--~~-~-* . . . . ._____ Date: _...!...tf_--'--'!lo=---*"'_,_/if_.____

FSS Engineer Reviewed by: ~ C k:,,., - Cl '-*

FSS ineer (

Date: --'-1/+-/-'__,7/f--'--'I'-/'-----

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 39 of 468

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Attachment 1 Survey Plan HBPP-FSSP-OOL10-11-00 PROPOSED SURVEY AREA r-**-y ..

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PROPERTY BOUNDARY OOL 10-11 = 76520 SQ. M OOL10-11 OOL 10~11 FISHERMANS CHANNEL N.T.S.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 41 of 468

Attachment 2 Hard-to-Detect (HTD)

Assessment Data FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 42 of 468

Attachment 2: HTD Assessment Data Attachment 2: Resultant Dose from Hard-to-Detect Nuclides Composite Soils - ROT Vault of the Liquid"Radwaste Building Building Surface Results/DCGL Soll Results Results/DCGL DCGL (positive only)

Nuclide (dpm/100 cm 2) DCGL Unity Unity (DC I/al (DC I/al Fraction Fraction Am-241 3.00E+03 2.50E+01 -3.38E-02 -1.4E-03 O.OE+OO C-14 7.00E+06 6.30E+OO -1.65E-01 -2.6E-02 O.OE+OO Cm-243 4.30E+03 2.90E+01 7.53E-02 2.6E-03 2.6E-03 Cm-244 5.50E+03 4.80E+01 7.53E-02 1.6E-03 1.GE-03 Cm-245 2.20E+03 1.70E+01 8.40E-02 4.9E-03 4.9E-03 Cm-246 2.70E+03 2.50E+01 8.40E-02 3.4E-03 3.4E-03 Co-60 1.30E+04 3.80E+OO O.OE+OO O.OE+OO Cs-137 4.60E+04 7.90E+OO O.OE+OO O.OE+OO Eu-152 2.70E+04 1.00E+01 O.OE+OO O.OE+OO Eu-154 2.50E+04 9.40E+OO O.OE+OO O.OE+OO H-3 1.80E+08 6.80E+02 O.OE+OO O.OE+OO 1-129 4.90E+04 4.80E+OO O.OE+OO O.OE+OO Nb-94 1.90E+04 7.10E+OO O.OE+OO O.OE+OO Ni-59 6.30E+07 1.90E+03 O.OE+OO O.OE+OO Ni-63 2.40E+07 7.20E+02 6.81E-01 9.SE-04 9.SE-04 Np-237 2.40E+03 1.10E+OO O.OE+OO O.OE+OO Pu-238 3.40E+03 2.90E+01 O.OE+OO O.OE+OO Pu-239 3.10E+03 2.60E+01 2.81E-01 1.lE-02 1.lE-02 Pu-240 3.10E+03 2.60E+01 2.81E-01 1.lE-02 1.lE-02 Pu-241 1.40E+05 8.60E+02 7.60E-01 8.8E-04 8.8E-04 Sr-90 9.70E+04 1.50E+OO O.OE+OO O.OE+OO Tc-99 9.60E+06 1.20E+01 -5.2E-01 -4.3E-02 O.OE+OO total -3.SE-02 3.6E-02 Total (mrem/y) -8.SE-01 9.0E-01 NOTE: Tritium (H-3) & Strontium-90 (Sr-90) excluded. Both isotopes were measured at on-site lab for each sample.

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 43 of 468

Attachment 2: HTD Assessment Data 311 J Laboratories LLc PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 a member of The GEL Group INC April 11, 2014 www.gel.com Ms. Dee Anderson Pacific Gas and Electric, Humboldt Bay Power Plant 1000 King Salmon Avenue Eureka, California 95503 Re: Final Status Survey Work Order: 345495

Dear Ms. Anderson:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on March 29, 2014. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.

Sincerely, Erin Trent Project Manager Purchase Order: 3500953353, Line item #4 Enclosures FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 44 of 468

Attachment 2: HTD Assessment Data Table of Contents Case Narrative ...................................................................................... I Chain of Custody and Supporting Documentation............................... 3 L*aboratory Certifications ...................................................................... 9 Radiological Analysis ......................................................................... 12 Sample Data Summary ............................................................... 30 Quality Control Data.................................................................. 33 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 45 of 468

Attachment 2: HTD Assessment Data Case Narrative Page 1of47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 46 of 468

Attachment 2: HTD Assessment Data Case Nan:ative for Pacific Gas and Electric Company SDG: 345495 April 11, 2014 Laboratorr Identification:

GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summa1*v Sample Receipt The sample arrived at GEL Laboratories LLC, Charleston, South Carolina on March 29, 2014 for analysis. The sample was delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt.

Sample Identification The laboratory received the following sample:

Laborat01y ID Client ID 345495001 2014~2127a RDT Vault Soil Composite Case Nanative Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL)

Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package.

Data Package The enclosed data package contains the following sections: General Narrative, Chain of Custody and Supporting Documentation, and data from the following fractions: Radiochemistry.

Erin Trent Project Manager Page 2of47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 47 of 468

Attachment 2: HTD Assessment Data Chain of Custody and Supporting Documentation Page 3 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 48 of 468

"Tl PO# :1500953353 Pag~ __l_af _ ! _

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Lab: GEL Chain of Custody and Analytical Request CD

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\V ork Order # 6Li S-l/q '& 7. Excavation Permit II Client Nlllllc: PG & E 707-444-0746 Sample Analysis Requested lSJ (Fill in the number of comainers for *each test)

P~ject/Site Name: llDPP Fm: #:707-441-2671 Should thi$

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Addrcss:1000 King Salmon, Eureka Ca 95503 comidercd: 0 <:;

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1') please call 707-444-0809 SMS-1fl1~00~

Cb,.in of Custody Signatur.cs Sumplc Shipping an<l DcliYcr-y Details Relinquished ny (Signed) Date Time Recoiv]sr d Date rime GEL PM:

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cc CD ~.) l'rmri!li1*e Typt' llA - llydrncl*k*" .~ciu. NI -Xittio Acid. Sii = SodiumHydmxid~. SA= Sulfuric Acid.\.\ -1\<<01hie Aeid, ll.-.:~ "'*""'*~T-Sodnnn Thi~sulfa:e, If 11opr<0<t**ti*oi* .tl.I..!-ko1** Ji;M bl,.d; t c (0 WHITE= LABOR-.\ TORY YELLOW =FILE PIJ';l{=CLTF:NT 0

Ol co Page 4of47

FSS MDAs Attachment 2: HTD Assessment Data

Subject:

FSS M DAs From: "Anderson, Dee" <D1A6@pge.com>

Date: Tue, 2 Oct 2012 15:19:52 +0000 To: Erin Trent <Erin.Trent@gel.com>

CC: "Oliver, Cynthia" <CCOl@pge.com>, "Alderman, Wayne" <WLAB@pge.com>

Good Morning Erin, Attached please find a list of required MDAs to be used for FSS analysis of soils. GEL receives FSS samples for the hard to detect nudides. The MDCs remain the same as previously with the exception that H-3 is now being analyzed onsite.

Thank you for your great work!

D.

Dee Anderson Count Room Supervisor Humboldt Bay Power Plant 1000 King Salmon Eureka, CA 95503 Ph. 707-444-0746 PG&E is committed to protecting our customers' privacy.

To learn more, please visit http://www.pge.com/about/comoanv/privacy/customer/

Content-Description: FSS GEL MDAs.xls FSS GEL MDAs.xls Content-Type: applicationivnd.ms-excel

- ----* ________ JI Content-Encoding: base64 1 ofl 3/31/2014 8:42 AM FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 50 of 468

Attachment 2: HTD Assessment Data Characterization MDCs for GEL. for FSS Sampras Gamma Analysis: 10% to 60% of the DCGL Co-60 3.B2E-01 to 1.91 E+OO pCi/g Nb-94 7.13E-01 to 3.57E+OO pCi/g 1-129 4.83E-01 to 2.42E+OO pCf/g Cs-137 7.93E-01 to 3.97E+OO pCf/g Eu-152 1.01E-t*OO to 5.05E+OO pCllg Eu-154 9.4DE-01 to 4.70E+OO pCi/g Np-237 1.11 E-01 to 5.55E-01 pCl/g Hard to Detect Nucllcfes: 10% to 50% of the DCGL H-3 6.86E+01 to 3.43E+02 pC!ig C-14 6.30E-01 to 3.15E+OO pCi/g Nl-59 1.97E+02 to 9~85E+02 pCi/g Nl-63 7.24t;;+o1

to 3.62E+02 pCllg Sr-90 1.61 E-01 to 7.66E-01 pCi/g Tc-99 1.24E+OO to 6.20E+OO pCl/g Pu-238 2.97E+OO to 1.49E+01 pCl/g Pu-239/240 2.67E+OO to 1.34E+D1 pCflg Pu-241 8.61E+01 to 4.31E+02 pCl/g Am-241 2.58E+OO lo 1.29E+01 pCllg Cm-243 2.90E+OO to 1.45E+01 pCllg Cm-244 4.81 E+OO to 2.41E+01 pCl/g Cm-245 1.78E+OO to e.90E+OO pCl/g Cm-246 2.66E+OO to 1.29E+01 pCJ/g FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 51 of 468 .

Attachment 2: HTD Assessment Data (ij :j ! ILaboratories LLC ;

SAMPLE RECEIPT & REVIEW FORM Clicnl; f Cf..-r?A-h5 v'f> SDG/AR/COC/Worlt Order: ~Sll67S necclvcd B\*: PJ/L- Date Received: 3"~J-.-n -IY

~ 0 *JfNcl Counls > lOOcpm on samples not marked "rmlim1ctivc, contact lhc Rndialion Safety Group ror further Suspected llnznrd Information ;...

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17 invcstigntion.

COCJSnmplC3 marked as rndioaclivc? IMiudmum Net Counts Obscn...;cJ+ (Observed Counts* Arcn DllCksiround Coumsl: r~o Cl~ificd Radiono;livc 11 1.>r Ill bv RSO? ....... IJ:¥ti<. Were swipes taken of sample con1nlincrs < i\Clion le"cls? '

COCJSatnpl.;;t marked con1ainintt PCBs? ,/

Packn3c, COC, and/or Samples marked as ./

bcn*llium or asbestos containinJ?.7 Jf\'C.~. samnlcs are to be S""""'Cnted as Safctv Con:rollcd Smnplcs, nnd opened by the GEL Safet\' Group.

Shipped as a DOT Hnzardous? . / 1-1Jrt1ird Class Shipped: UNll:

Samples identified as Ford~ S~il? /

Sample Receipt Crilerln :!: <

?.:, z 0

Commcn<slQu11Ilficr5 (Required for Non*Couformlng lie ms)

/' Circle 1'.pplicablc:

Shipping containers n:ccivcd intact I ~ Sc:ils brckcn Damtig<..-d canloim:r Lcakil'IJ amtaincr Other (describe) and scaled?

Samp Ics rcqmrmg

' co Id......._, ' /" l're~ation MethOO: Ice bags Blue ice Dry i~~ Other (describe) 2 within (0 :-:; 6 deg.

prcscrva11011 cw* v 1'1 (, *nil tcmpcrnlun:s rn'c rtcorccd in Cc sms Daily chock performed aml passed on v Temperature D<!vlcc Serial 11: f '1,;;;:, f{rZJ* 7//;

2a IR temperature gun'/ ./ S<>:ondory Temporalure Device erial ~ I. f Applicable):

I Chain <lf custody documents l

included with shipment?

Circle Ap~licablc; 4 Sample conlnincrs i11u1c1 nnd scaled? Senls broken D:imagcd ronlaincr Leaking container Other [_describe)

Sample !D's, conlaill<)rS affccled and obS;)n-ed rH:

s Samples requiring chemical _,,,/'

prcscrvalion at proper pH? ...-1lr- -..1.1-1 Inti*.

S:unplc !D's and containers n!Tec!L'tl:

6 VOA \'ials free ofhcadspacc (defined as< 6mm bubble)?

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flfycs, immediately dcliv~r to V<ilatilcs laborntol}')

7 Arc Encore containers present? /

!D's and tcru atTecre~:

Samples rccci\'ed within holding 8

time'/

Sample ID's on COC mulch !D's on Somr-lc !D's and ~ontniners affected:

9 bottles?

Date & time on COC match date & Sample !D's affected:

10 time on bottles?

Number or contnincrs l'eccived match Sample !D's n!Tectcd:

l1 number indicated on COC?

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12 Are sample containers idcnlifiablc as ./"

GEL provided?

CDC form is properly signed in 13 rclinquishcd/n:cciv1..-d sections?

-~ Circle Applicable:

~~ Fcdl>i; Ground UPS Field Services Courier Or her 14 Cnrrier and tracking number. gOY-h /too '7133 Commcnls (U£c Continual.ion Form if llc<!dcd):

PM (ur PMA) .-.::view: lni1fals _ _ _T""""'..S"--'T___ Dutl! ~\?" t'=k P11gc _~_or _l_

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FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 52 of 468

Attachment 2: HTD Assessment Data

Subject:

just a reminder - in case you need it for the package.

From: "Oliver, Cynthia" <CCOl@pge.com>

Date: Fri, 28 Mar 2014 21:16:55 +0000 To: "Erin Trent {Erin.Trent@gel.com)" <Erin.Trent@gel.com>

The soil sample we sent today has the wrong charge line on the CDC - it should be line 4 for FSS Thanks, Cyndi PG&E is committed to protecting our customers' privacy.

To learn more, please visit http://www.pge.com/about/company/privacy/customer/

f~~ 8of47 3/31/20148:49 AM FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 53 of 468

Attachment 2: HTD Assessment Data Laboratory Certifications Page 9 of 47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 54 of 468

Attachment 2: HTD Assessment Data List of current GEL Certifications as of 11 April 2014 State Certification Alaska UST-110 Arkansas 88-0651 CLIA 4200904046 California NELAP 01151CA Colorado .SC00012 Connecticut PH-0169 Delaware SC000122013-10 DoD ELAP/ ISOl 7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-12-00283,P330-12-00284 Georgia SC00012 Georgia SDWA 967 Hawaii SC000122013-10 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky 90129 Louisiana NELAP 03046 (AI33904)

Louisiana SDWA LA130005 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC000122013-10 Nebraska NE-OS-26-13 Nevada SC000122014-l New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 Oklahoma 9904 Pennsylvania NELAP 68-00485 Plant Material Permit PDEP-12-00260 South Carolina Chemistry 10120001 South Carolina GVL 23611001 South Carolina Radiochemi 10120002 Tennessee TN02934 TexasNELAP Tl04704235-14-9 UtahNELAP SC000122013-ll Vermont VT87156 Virginia NELAP 460202 Washington C780-12 Wisconsin 999887790 Page 10 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 55 of 468

Attachment 2: HTD Assessment Data GEL Laboratories LLC problem sofred P.O. Box 30711-C/1orlesto11, S.C. 19417-1040 Samge Road-19407 (8./3)556-8171-Fax(843)766-1178 Invoice for Analytical Services Accounts Payable-PG&E Inrnice #: 285072 Pacific Gas and Electric Company ln\"oice Date: 11-APR-14 Terms: Net30 P.O. Box 7760 Client: Pacific Gas and Electl"ic Company San Francisco, California 94120 Final Status Surrey Descl"iption (Order):

PO: 3500953353, Line item #4 \Yorkorde1*/SDG: 345495 Project: PCGE00606 Project Manager: Elin Trent

-=

GELID:345495001 llfatrll:SOIL Clien!ID: 2014-2127aRDTVault Colletted: 26-MAR-14 Recerred: 29-MAR-14 Test Description Methods TnrnDays Charge GSCGAMMS Gammaspcc, Gamma. Solid (Sbndard DOE HASL 300, 4 5 2 3/G:Hll-R. 14 (Rrceive)

List)

LSC99TCS Llquid Scint Tc99, Solid I 24 pCilg RDL DOE EML HASL-300, Tc--02-R.C Mo 14 (Rrcei\'e)

GSC59NIS Gamma Ni59, Solid 197 pCifg RDL DOER.ESL Ni-I 14 (Rrcei\'e)

=

LSC_14CS Llquid Sein! Cl4, Solid, 0 63 pCifg RDL EPAEERF C--01 Modified 14 (Rrcei\'e)

-=

LSC63NIS liquid Scint Ni63, Solid 72 4 pC"tlg RDL DOE R.ESL NH, Modified 14 (Rrceive)

ASPAMCMS Alphaspcc Am241, Cm, Solid 1 78 pCilg DOE EML HASL-300, Am--05--R.C Mo 14 (Rrcei\'e)

RDL ASP_PUS Alphaspcc Pu, Solid 2 67 pCilg RDL DOE EML HASL-300, Pu-11-R.CMo 14 (Recci\'e)

LSC41PUS Llquid Scint Pu241, Solid 86 I pCilgRDL DOE EML HASL-300, Pu-11-RC Mo 14 (Rrceive)

GFC90SRS GFPC, Si90, soi!O 151 pCilgRDL EPA905 0 Modified 14 (Rrcei\'e)

GSC_J.9IS Gamma 1129, Solid DOE EML HASL-300,I--Ol Modified 14 (Rrcei\'e)

Sample Total:

Miscellaneous Charge Description Charge Invoice Total:

Page 1 ofl Page 11of47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 56 of 468

Attachment 2: HTD Assessment Data Radiological Analysis Page 12 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 57 of 468

Attachment 2: HTD Assessment Data Radiochemish*y Case Narmtive Pacific Gas and Elech'ic Company (PCGE)

SDG345495 Method/Analvsis Information Product: Alphaspec Am241, Cm, Solid 1.78 pCi/g RDL Analytical Method: DOE Elvll.. HASL-300, Am-05-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1377656 Prep Batch Number: 1376446 Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203062540 Method Blank (MB) 1203062541 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203062542 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011REV#24.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Qualitv Conh*ol (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC Information Page 13of47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 58 of 468

Attachment 2: HTD Assessment Data All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed \\ithin the required holding time.

Sample Re-prep/Re-analysis The batch was reprepped due to spectral interference. 111e re-analysis is reported.

Recounts None of the samples in this batch were recounted.

Miscellaneous Information:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may de\iate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG.

l.\ianuallntegration No manual integrations were perfom1ed on data in this batch.

Sample-Specific MDA/l.\'1DC The MDAIMDC reported on the certificate of analysis is a san1ple-specific MDAIMDC.

Additional Comments Additional comments were not required for this sample set.

Qualifie1* Information Manual qualifiers were not required.

l.\iethod/AnalYSis Information Product: Alphaspec Pu, Solid 2.67 pCi/g RDL Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1377658

- Prep Batch Number: 1376446 Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203062543 Method Blank (MB) 1203062544 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203062545 Laboratory Control Sample (LCS)

Page 14of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 59 of 468

Attachment 2: HTD Assessment Data The samples in this SDG were analyzed on a "dry weight" basis.

SOP Refe1*ence Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discnssed in this narrative has been analyzed in accordance with GL-RAD-A-011 REV#24.

Calibmtion lnfo1*mation:

Calibration Information All initial and continuing calibration requirements have been met.

Standards lnfo1*mation Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geometry All counting sources were prepared in the san1e geometry as the calibration standards.

Qnalitv Control (QC) lnfommtion:

Blank Information The blank volume is representative of the san1ple vohune in this batch.

Designated QC The following sample was nsed for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis Sample 345495001 (2014-2127a RDT Vault Soil Composite) was reprepped due to low carrier/tracer yield. The re-analysis is being reported.

Recounts None of the samples in this batch were recounted.

Miscellaneous lnfo1mation:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual docmnents. A data exception report (DER) was not generated for this SDG.

Mannal Integration No manual integrations were perfonned on data in this batch.

Sample-Specific MDAIMDC The MDAIMDC reported on the certificate of analysis is a sample-specific MDAIMDC.

Additional Comments Page 15of47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 60 of 468

Attachment 2: HTD Assessment Data Additional comments *were not required for this sample set.

Qualifier Information Manual qualifiers were not required.

Method/Analvsis Information Prnduct: Gamma 1129, Solid Analytical Method: DOE EML HASL-300,l-01 Modified Analytical Batch Number: 1376494 Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203059635 Method Blank (MB) 1203059636 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203059637 345495001(2014-2127a RDT Vault Soil Composite) Matrix Spike (MS) 1203059638 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

SOP Refe1*ence Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-006 REV# 21.

Calibration Info1*mation:

Calibration Infor*mation All initial and continuing calibration requirements have been met.

Standards Info1*mation Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geometry All connting sources were prepared in the same geometry as the calibration standards.

Qualitv Control (QC) Information:

Blank Information The blank volume is representative of the san1ple volmne in this batch.

Designated QC The following san1ple was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC Information All of the QC samples met the required acceptance linllts.

Page 16of47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 61 of 468

Attachment 2: HTD Assessment Data Technical lnfonnation:

Holding Time All sample procedures for this sample set were performed within the required holding tin1e.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this batch were recounted.

l\'Iiscellnneous Infonnation:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG.

Sample-Specific MD.A/MDC The !\IDA/MDC reported on the certificate of analysis is a sample-specific !\IDA/MDC.

Additional Comments Additional comments were not required for this san1ple set.

Qualifier Information Manual qualifiers were not required.

Method/Analvsis Information Product: Gammaspec, Gamma, Solid (Standard List)

Analytical Method: DOE HASL 300, 4.5.2.3/Ga-Ol-R Prep Method: Dry Soil Prep Analytical Batch Number: 1376566 Prep Batch Number: 1376446 Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203059875 Method Blank (MB) 1203059876 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203059877 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

SOP Refe1*ence Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with Page 17of47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 62 of 468

Attachment 2: HTD Assessment Data GL-RAD-A-013 REV# 25.

Calibration Information All initial and continuing calibration requirements have been met.

Standa1*ds Infm*mation Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batclL Designated QC The following san1ple was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203059876 (2014-2127a RDT Vault Soil Composite) and 345495001 (2014-2127a RDT Vault Soil Composite), did not meet the Ac-228/Ra-228 relative percent difference requirement (0-20%); however, they do meet the relative error ratio requirement (0-3) with value of 1.18.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Sample Re-p1*ep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this batch were recounted.

Miscellaneous Information:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may de\iate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG.

Sample-Specific MDA/MDC The MDAIMDC reported on the certificate of analysis is a sample-specific IvIDAIMDC.

Additional Comments Additional comments wete not required for this sample set.

Qualifier Information Qualifier Reason Analyte Sample Client Sample Page 18 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 63 of 468

Attachment 2: HTD Assessment Data Data rejected due to high 2014-2127a RDT Vault Soil UI Lead-210 1203059876 counting uncertainty. Composite(3454 Data rejected due to low 2014-2127a RDT Vault Soil UI Bismuth-212 345495001 abundance. Composite Data rejected due to no 2014-2127a RDT Vault Soil UI Tuorium-234 1203059876 valid peak. Composite(3454 2014-2127a RDT Vault Soil Uranium-238 1203059876 Composite(3454 Method/Analnis lnfo1*mation Product: Gamma Ni59, Solid 197 pCi/g RDL Analytical Method: DOE RESL Ni-I Prep Method: Tuy Soil Prep Analytical Batch Nmnber: 1376823 Prep Batch Number: 1376446 Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203060558 Method Blauk (MB) 1203060559 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203060560 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a dry weight" basis.

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). Tue data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 16.

Calibration Information:

Calibration Infonnation All initial and continuing calibration requirements have been met.

Standa1*ds Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Page 19of47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 64 of 468

Attachment 2: HTD Assessment Data Quality Contl'ol (QC) Information:

Blank Info1*mation TI1e blank volmne is representative of the sample vohune in this batch.

Designated QC The following sample was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC lnfol'mation All of the QC samples met the required acceptance linllts.

Technical lnfol'mation:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Sample Re-pl'ep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Chemical Recoveries All chemical recoveries meet the required acceptance linllts for this sample set.

Recounts None of the san1ples in this batch were recounted.

Miscellaneous lnfol"mation:

Data Exception (DER) Documentation Data exception reports are generated to docmneut any procedural anomalies that may deviate from referenced SOP or contractual docmnents. A data exception report (DER) was not generated for this SDG.

Sample-Specific MDA/MDC TI1e !'-.IDA/MDC reported on the certificate of analysis is a sample-specific MDAIMDC.

Additional Comments Additional comments were not required for this sample set.

Qualifiel' Infol"mation Manual qualifiers were not required.

Method/Analvsis Information PI"oduct: GFPC, SJ'90, soil 0.151 pCi/g RDL Analytical Method: EPA 905.0 Modified Prep Method: Dry Soil Prep Analytical Batch Nmnber: 1376626 Prep Batch Nmnber: 1376446 Page 20 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 65 of 468

Attachment 2: HTD Assessment Data Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203060080 Method Blank (1v1B) 1203060081 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203060082 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 17.

Calibrntion Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geomeh*y All counting sources were prepared in the same geometry as the calibration standards.

Qualify Cont1*ol (QC) Information:

Blank Information The blank volU111e is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC Info1*mation All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203060081 (2014-2127a RDT Vault Soil Composite) and 345495001 (2014-2127a RDT Vault Soil Composite), did not meet the relative percent difference requirement; however, they do meet the relative error ratio requirement with value of 2.82.

Technical Information:

Holding Time All sample procedures for this sample set were perfonued within the required holding time.

Sample Re-prep/Re-analysis None of the san1ples in this sample set required reprep or reanalysis.

Chelnical Reco,*e1ies All chemical recoveries meet tl1e required acceptance liniits for tllis sample set.

Recounts Samples 1203060081 (2014-2127a RDT Vault Soil Composite) and 345495001 (2014-2127a RDTVault Soil Composite) were recounted due to high relative percent difference/relative error ratio. The recounts are reported.

Page 21of47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 66 of 468

Attachment 2: HTD Assessment Data Miscellaneous Info1*mation:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG.

Sample-Specific MDA/MDC The MDAIMDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments San1ples 1203060081 (2014-2127a RDT Vault Soil Composite) and 345495001 (2014-2127a RDT Vault Soil Composite) \Vere verified by recounting at least five days from the separation date.

Qualifie1* Information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Pu241, Solid 86.1 pCi/g RDL Analytical Method: DOE Eiv!L HASL-300, Pu-11-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1377659 Prep Batch Number: 1376446 Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203062546 Method Blank (MB) 1203062547 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203062548 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

SOP Refei*ence Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 16.

Calibmtion Information:

Calibmtion Information All initial and continuing calibration requirements have been met.

Standards Information Page 22 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 67 of 468

Attachment 2: HTD Assessment Data Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geometry All collllting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Info1*mation The blank volume is representative of the sample volmne in this batch.

Designated QC The following sample *was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-analysis Samples were reprepped due to low carrier/tracer yield. The re-analysis is being reported.

Recounts None of the samples in this batch were recoll!lted.

Miscellaneous Infonnation:

Data Exception (DER) Documentation Data exception reports are generated to doclllllent any procedural anomalies that may deviate from referenced SOP or contractual doclllllents. A data exception report (DER) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Sample-Specific MDA/MDC The .MDAIMDC reported on the certificate of analysis is a san1ple-specific MDAIMDC.

Additional Comments Additional comments were not required for this sample set.

Qualifier Information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Ni63, Solid 72.4 pCi/g RDL Analytical Method: DOE RESL Ni-1, Modified Page 23 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 68 of 468

Attachment 2: HTD Assessment Data Prep Method: Dry Soil Prep Analytical Batch Nmnber: 1376798 Prep Batch Number: 1376446 Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203060483 Method Blank (MB) 1203060484 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203060485 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis.

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022REV#16.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the eJl."]>iration dates.

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Conh*ol (QC) Information:

Blank Information The blank volmne is representative of the sample volmne in this batch.

Designated QC The follmving sample was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC Information All of the QC samples met the required acceptance limits.

Technical Infonnation:

Holding Time All sample procedures for this sample set were performed "I.vi.thin the required holding time.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Recounts Sample 1203060483 (NIB) was recounted due to the quench number being outside the calibration range. The recount is reported.

Page 24 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 69 of 468

Attachment 2: HTD Assessment Data Miscellaneous Information:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG.

Sample-Specific MDAIMDC The MDAIMDC reported on the certificate of analysis is a sample-specific MDAIMDC.

Additional Comments Additional comments were not required for this san1ple set.

Qualifier Information l\'1anual qualifiers were not required.

Method/Analvsis Information Product: Liquid Scint Tc99, Solid 1.24 pCi/g RDL Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 1376803 Sample ID Client ID 345495001 2014-2127a RDT Vault Soil Composite 1203060501 Method Blank (MB) 1203060502 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203060503 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-059 REV# 2.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geometry All cotmting sources were prepared in the same geometry as the calibration standards.

Page 25of47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 70 of 468

Attachment 2: HTD Assessment Data Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volmne in this batch.

Designated QC The following sample was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC Infm*mation All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed "\Vi.thin the required holding time.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Recounts None of the samples in this batch were recounted.

Miscellaneous Infm*mation:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG.

Sample-Specific MD.A/MDC The MDAIMDC reported on the certificate of analysis is a sample-specific MDAIMDC.

Additional Comments Additional comments were not required for this sample set.

Qualifier Information Manual qualifiers were not required.

Method/Analysis Information P1*oduct: Liquid Scint C14, Solid, 0.63 pCi/g RDL Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 1376820 Sample ID Client ID 345495001 2014-2127a RDTVaultSoil Composite 1203060549 Method Blank (MB) 1203060550 345495001(2014-2127a RDT Vault Soil Composite) Sample Duplicate (DUP) 1203060551 345495001(2014-2127a RDT Vault Soil Composite) Matrix Spike (MS)

Page 26 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 71 of 468

Attachment 2: HTD Assessment Data 1203060552 Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on an "as received" basis.

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 15.

Calibrntion Info1*mation:

Calibrntion Information All initial and continuing calibration requirements have been met.

Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates.

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Qualitv Conn*ol (QC) Information:

Blank Info1*mation The blank volume is representative of the sample Yolume in this batch.

Designated QC The following sample was used for QC: 345495001 (2014-2127a RDT Vault Soil Composite).

QC lnfo1*mation All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Sample Re-prep/Re-:malysis None of the san1ples in this sample set required reprep or reanalysis.

Recounts None of the samples in this batch were recounted.

Miscellaneous Information:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced

SOP or contractual documents. A data exception report (DER) was not generated for this SDG.

Sample-Specific l\IDA/MDC The MDAIMDC reported on the certificate of analysis is a san1ple-specific l\IDAIMDC.

Additional Comments Additional comments were not required for this san1ple set.

Page 27of47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 72 of 468

Attachment 2: HTD Assessment Data Qualifiel' Information Manual qualifiers were not required.

Cel'tification Statement Where the analytical method has been perfom1ed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Page 28of47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 73 of 468

Attachment 2: HTD Assessment Data GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Qualifier Definition Report for PCGE006 Pacific Gas and Electric Company Client SDG: 345495 GEL Work Order: 345495 The Qualifiers in this report are defined as follows:

M Result is <LLD and > MDC U Result is < LLD and <MDC UI Uncertain identification for gamma spectroscopy ReviewNalidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package.

The following data validator verified the information presented in this data report:

Signature: ~ Name: Kate Gellatly Date: 14 APR 2014

Title:

Analyst I Page 29 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 74 of 468

Attachment 2: HTD Assessment Data Sample Data Summary Page 30 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 75 of 468

r I

Attachment 2: HTD Assessment Data GEL LABORATORIES LLC Certificate of Analysis 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com GEL Sample ID: 345495001 Client: Pacific Gas and Electric Company Client Sample ID: 2014-2127a RDT Vanlt Soil Composite Collect Date: l\Iarch 26, 2014 Client l\fat:l"ix: Soil Receh-e Date: l\Iarch 29, 2014 Amonnt of Sample Received: Rep01't Date: Ap1il 14, 2014 2Sigma 2 Sigma Isotope Run Date Qualifier Acthity Uncertainty MDC LLD TPU Units C-14 04/03/14 u -1.65E-Ol 2.78E-Ol 4.71E-Ol 6.30E-Ol 2.78E-Ol pCilg Ni-63 04/03/14 u 6.81E-Ol l.49E+ol 2.50E+ol 7.24E+ol 1.49E+ol pCilg Sr-90 04/08/14 4.92E-Ol l.OlE-01 7.89E-02 l.51E-Ol l.36E-01 pCi/g Tc-99 04/08/14 u -5.21E-Ol 5.88E-Ol l.OlE+oO l.24E+o0 5.88£-01 pCilg Pu-241 04/08/14 u 7.60E-Ol 3.32E+ol 5.57E+ol 8.61E+ol 3.32E+ol pCilg Alpha Spec Pu-238 04/05/14 u -8.44E-03 7.28E-02 l.69E-Ol 2.97E+o0 7.29E-02 pCi/g Pu-239/240 04/05/14 u 2.81E-03 l.29E-Ol 2.84E-Ol 2.67E+o0 l.29E-Ol pCi/g Am-241 04/05/14 u -3.38E-02 l.14E-01 2.97E-Ol 2.58E+o0 l.14E-01 pCi/g Cm-243/244 04/05/14 u 7.53E-02 2.56E-Ol 4.82E-Ol 2.90E+OO 2.56E-Ol pCilg Cm-245/246 04/05/14 u 8.40E-02 1.44E-Ol l.26E-Ol l.78E+o0 l.44E-Ol pCi/g Gamma Spec Be-7 04/01/14 u -l.04E-01 3.59E-Ol 6.16E-Ol 3.62E-01 pCi/g Na-22 04/01/14 u 2.14E-02 l.64E-02 3.09E-02 l.91E-02 pCi/g K-40 04/01/14 9.07E+o0 5.97E-Ol l.90E-Ol l.OlE+oO pCi/g Cr-51 04/01114 u -4.87E-02 2.81E-01 4.98E-01 2.82E-Ol pCi/g Mn-54 04/01/14 u -6.62E-03 l.40E-02 2.35E-02 1.43E-02 pCilg Fe-59 04/01114 u -1.21E-02 3.07E-02 5.05E-02 3.12E-02 pCi/g Co-56 04/01114 u 2.23E-02 l.38E-02 2.70E-02 l.73E-02 pCi/g Co-57 04/01114 u -2.48E-03 l.91E-02 3.34E-02 1.91E-02 pCi/g Co-58 04/01/14 u 8.39E-04 l.32E-02 2.32E-02 l.32E-02 pCilg Co-60 04/01/14 M l.02E-Ol 2.04E-02 2.14E-02 3.82E-Ol 2.20E-02 pCilg Ni-59 04/03/14 u -7.28E+ol 5.89E+ol 8.SOE+ol l.97E+02 6.78E+ol pCi/g Zn-65 04/01/14 u 2.llE-06 3.58E-02 5.28E-02 3.58E-02 pCi/g Y-88 04/01/14 u l.48E-02 9.64E-03 2.24E-02 1.lSE-02 pCi/g Zr-95 04/01/14 u l.04E-02 2.64E-02 4.76E-02 2.68E-02 pCi/g Nb-94 04/01/14 u l.34E-02 l.12E-02 2.22E-02 7.13E-Ol l.28E-02 pCi/g Nb-95 04/01/14 u 2.SOE-03 l.57E-02 2.44E-02 l.57E-02 pCi/g Ru-106 04/01/14 u -1.27E-Ol 2.35E-Ol 3.89E-Ol 2.42E-01 pCi/g Ag-llOm 04/01/14 u -1.23E-02 l.85E-02 3.04E-02 l.94E-02 pCifg Sn-113 04/01/14 u l.49E-02 4.63E-02 g.16E-02 4.68E-02 pCilg Sb-124 04/01/14 u -3.64E-03 2.58E-02 4.33E-02 2.59E-02 pCilg Sb-125 04/01/14 u l.79E-02 l.OSE-01 l.88E-Ol l.OSE-01 pCi/g 1-129 04/04/14 u -1.llE-02 2.30E-Ol 3.43E-Ol 5.00E-01 2.30E-Ol pCi/g Cs-134 04/01/14 u l.98E-02 l.62E-02 3.0SE-02 l.86E-02 pCi/g Notes: 1. LLDs are a-priori '"aloes.

2. l\IDCs are calculated a-poste1io1i values.

3. Gamma spectroscopy analysis results are calculated from a measurement using ouly one gamma energy line.

4. Air sample volumes are received in units of ft3. GEL conve11s the units and reports them as m3.

Qualifiers: U. Target isotope was analyzed fo1* but not detected abow the l\IDC and LLD.

UI Uncertain identification for gamma spectroscopy.

X Lab-specific qualifier-please see case narrative, data summary package or contact yonr project manager for details.

M Reported result is less than the LLD and greater than the l\IDC.

Page 31of47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 76 of 468

Attachment 2: HTD Assessment Data GEL LABORATORIES LLC Certificate of Analysis 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com GEL Sample ID: 345495001 Client: Pacific Gas and Electric Company Client Sample ID: 2014-2127a RDT Vault Soil Composite Collect Date: March 26,2014 Client Matrix: Soil Receive Date: March 29,2014 Amount of Sample Received: Report Date: April 14,2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty MDC LLD TPU Units Cs-136 04/01/14 u -l.22E-02 2.46E-02 4.03E-02 2.53E-02 pCi/g Cs-137 04/01/14 2.39E+Ol 2.35E-Ol 4.17E-02 7.93E-01 1.92E+OO pCi/g Ba-133 04/01/14 u -2.61E-02 4.83E-02 7.36E-02 4.97E-02 pCi/g Ba-140 04/01/14 u -1.52E-02 2.0lE-02 2.92E-02 2.13E-02 pCi/g Ce-139 04/01/14 u 5.94E-03 2.32E-02 4.02E-02 2.34E-02 pCi/g Ce-141 04/01/14 u -2.13E-02 4.03E-02 6.91E-02 4.15E-02 pCi/g Ce-144 04/01/14 u -2.33E-02 l.51E-Ol 2.62E-Ol l.51E-Ol pCi/g Nd-147 04/01/14 u -2.00E-01 2.89E-OI 4.84E-Ol 3.03E-Ol pCi/g Pm-144 04/01/14 u -2.83E-03 l.47E-02 2.lOE-02 l.48E-02 pCi/g Pm-146 04/01/14 u -7.lOE-02 5.47E-02 9.24E-02 6.38E-02 pCi/g Eu-152 04/01/14 u 6.63E-02 9.98E-02 1.73E-Ol 1.0lE+OO 1.04E-Ol pCi/g Eu-154 04/01114 u 5.96E-02 4.65E-02 8.77E-02 9.40E-Ol 5.40E-02 pCi/g Eu-155 04/01/14 u 5.16E-02 7.62E-02 l.37E-Ol 7.98E-02 pCi/g Ir-192 04/01/14 u 6.64E-03 3.06E-02 5.47E-02 3.08E-02 pCi/g Hg-203 04/01/14 u 2.62E-02 2.99E-02 5.45E-02 3.22E-02 pCi/g Tl-208 04/01114 l.28E-Ol 4.77E-02 4.58E-02 4.89E-02 pCi/g Pb-210 04/01/14 u -9.12E-Ol 2.37E+OO 4.15E+OO 2.41E+OO pCi/g Pb-212 04/01/14 4.83E-Ol 8.36E-02 9.06E-02 9.43E-02 pCi/g Pb-214 04/01/14 4.54E-Ol l.58E-Ol 1.27E-Ol l.63E-Ol pCi/g Bi-212 04/01/14 UI 4.45E-Ol 3.18E-Ol 4.45E-OI 4.21E-Ol pCi/g Bi-214 04/01/14 3.51E-Ol l.04E-OI 8.79E-02 l.07E-Ol pCi/g Ra-228 04/01/14 5.54E-Ol l.21E-OI 8.65E-02 1.45E-Ol pCi/g Ac-228 04/01/14 5.54E-Ol l.21E-Ol 8.65E-02 l.45E-Ol pCi/g Th-234 04/01/14 u l.31E+OO l.32E+OO l.48E+OO l.36E+OO pCi/g U-235 04/01/14 u -4.84E-03 l.60E-Ol 2.73E-Ol l.60E-Ol pCi/g U-238 04/01/14 u l.31E+OO l.32E+OO 1.48E+OO l.36E+OO pCi/g Np-237 04/01/14 u l.09E-02 6.18E-02 l.lOE-01 l.llE-01 6.20E-02 pCi/g Np-239 04/01/14 u -4.05E-Ol 3.03E-Ol 5.l 7E-Ol 3.56E-Ol pCi/g Am-241 04/01/14 u l.33E-02 l.lOE-01 l.79E-Ol l.lOE-01 pCi/g Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units of ft3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD.

UI Uncertain identification for gamma spectroscopy.

X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.

M Reported result is less than the LLD and greater than th,e MDC.

Page 32 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 77 of 468

Attachment 2: HTD Assessment Data Quality Control Data Page 33 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 78 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: April 14, 2014 Client: Pacific Gas and Electric, Humboldt Bay Power Plant Page 1of14 1000 King Salmon Avenue Eureka, California

Contact:

Ms. Dee Anderson Workorder: 345495 Parmname NOM Sam[!le Qua! QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1377656 QC1203062541 345495001 DUP Americium-241 u -0.0338 u 0.0175 pCilg 0 NIAMXS2 04105/1411 :46 Uncert: +l-0.114 +l-0.113 TPU: +l-0.114 +l-0.113 Curium-2431244 u 0.0753 u 0.00865 pCi/g 0 NIA Un cert: +l-0.256 +l-0.0905 TPU: +l-0.256 +l-0.0905 Curium-2451246 u 0.084 u 0.0272 pCilg 0 NIA Uncert: +l-0.144 +l-0.102 TPU: +l-0.144 +l-0.102 QC1203062542 LCS Americium-241 6.72 7.39 pCilg 110 (75%-125%) MXS2 04105/1411:46 Un cert: +l-1.01 TPU: +l-1.39 Curium-2431244 13.6 13.4 pCi/g 98.4 (75%-125%)

Un cert: +l-1.35 TPU: +l-2.20 Curium-2451246 M 0.236 pCi/g Un cert: +l-0.214 TPU: +l-0.216 QC1203062540 MB Americium-241 u 0.0616 pCilg MXS2' 0410511411 :46 Uncert: +l-0.121 TPU: +l-0.121 Curium-2431244 u -0.0331 pCilg Uncert: +l-0.0768 TPU: +l-0.0769 Curium-2451246 u 0.0401 pCi/g Uncert: +l-0.113 TPU: +l-0.113 Batch 1377658 QCJ203062544 345495001 DUP Plutonium-238 u -0.00844 u 0.0591 pCilg 0 NIAMXS2 0410511411:47 Un cert: +l-0.0728 +l-0.134 TPU: +l-0.0729 +l-0.134 Plutonium-2391240 u 0.00281 u 0.0171 pCi/g 0 NIA Un cert: +l-0.129 +l-0.0948 TPU: +l-0.129 +l-0.0949 QC!203062545 LCS Plutonium-238 u 0.0259 pCi/g (75%-125%) MXS2 04105/1411:47 Un cert: +l-0.167 TPU: +l-0.168 Page 34 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 79 of 468

Attachment 2: HTD Assessment Data GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page 2 of 14 Parmname NOM Sam[!le Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1377658 Plutonium-239/240 9.38 7.58 pCi/g 80.9 (75%-125%)

Un cert: +/-1.17 TPU: +/-1.63 QC1203062543 MB Plutonium-238 u -0.054 pCi/g MXS2 04/05/1411:47 Uncert: +/-0.0871 TPU: +/-0.0873 Plutonium-239/240 u -0.045 pCi/g Uncert: +/-0.0853 TPU: +/-0.0855 Batch 1377659 QCl203062547 345495001 DUP Plutonium-241 u 0.760 u 2.19 pCi/g 0 N/AMXS2 04/08/1408:23 Uncert: +/-33.2 +/-27.1 TPU: +/-33.2 +/-27.l QC1203062548 LCS Plutonium-241 409 346 pCi/g 84.6 (75%-125%) MXS2 04/08/1408:39 Un cert: +/-41.3 TPU: +/-83.6 QC1203062546 MB Plutonium-241 u -8.64 pCi/g MXS2 04/08/1408:07 Uncert: +/-32.5 TPU: +/-32.5 Rad Gamma Spec Batch 1376494 QCl203059636 345495001 DUP Iodine-129 u -0.0111 u -0.049 pCi/g 0 N/AMJHl 04/04/1413:54 Uncert: +/-0.230 +/-0.244 TPU: +/-0.230 +/-0.245 QC1203059638 LCS Iodine-129 9.44 8.61 pCi/g 91.2 (75%-125%) MJHl 04/04/1413:55 Uncert: +/-1.67 TPU: +/-1.88 QC1203059635 MB Iodine-129 u -0.00409 pCi/g MJHI 04/04/1413:54 Un cert: +/-0.158 TPU: +/-0.158 QC1203059637 345495001 MS Iodine-129 9.44 u -0.0111 9.94 pCi/g 105 (75%-125%) MJHl 04/04/1413:55 Uncert: +/-0.230 +/-1.30 TPU: +/-0.230 +/-1.64 Batch 1376566 QC1203059876 345495001 DUP Actinium-228 0.554 0.431 pCi/g 25.l* (0%-20%) MXRl 04/01/1413:35 Uncert: +/-0.121 +/-0.137 Page 35 of 47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 80 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page 3 of 14 Parm name NOM Sam~le Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376566 TPU: +l-0.145 +l-0.146 Americium-241 u 0.0133 u 0.0444 pCilg 0 NIA Uncert: +l-0.110 +l-0.038 TPU: +l-0.110 +l-0.0383 Antimony-124 u -0.00364 u 0.00871 pCilg 0 NIA Uncert: +l-0.0258 +l-0.0276 TPU: +l-0.0259 +l-0.0279 Antimony-125 u 0.0179 u -0.0315 pCilg 0 NIA Uncert: +l-0.108 +l-0.103 TPU: +l-0.108 +l-0.104 Barium-133 u -0.0261 u 0.0213 pCi/g 0 NIA Uncert: +l-0.0483 +l-0.0436 TPU: +l-0.0497 +l-0.0447 Barium-140 u -0.0152 u -0.0201 pCilg 0 NIA Uncert: +l-0.0201 +l-0.0221 TPU: +l-0.0213 +l-0.0239 Beryllium-7 u -0.104 u 0.0692 pCi/g 0 NIA Uncert: +l-0.359 +l-0.344 TPU: +l-0.362 +l-0.345 Bismuth-212 UI 0.00 0.500 pCilg 11.5 (0%- 100%)

Uncert: +l-0.318 +l-0.274 TPU: +l-0.421 +l-0.278 Bismuth-214 0.351 0.419 pCi/g 17.6 (0%-20%)

Uncert: +l-0.104 +l-0.104 TPU: +l-0.107 +l-0.109 Cerium-139 u 0.00594 u 0.00877 pCi/g 0 NIA Uncert: +l-0.0232 +l-0.0191 TPU: +l-0.0234 .+l-0.0196 Cerium-141 u "0.0213 u 0.00945 pCi/g 0 NIA Un cert: +l-0.0403 +/-0.0331 TPU: +l-0.0415 +l-0.0334 Cerium-144 u -0.0233 u 0.144 pCi/g 0 NIA Uncert: +l-0.151 +l-0.121 TPU: +l-0.151 +l-0.138 Cesium-134 u 0.0198 u 7.74E-05 pCi/g 0 NIA Uncert: +l-0.0162 +l-0.0178 TPU: +l-0.0186 +l-0.0178 Cesium-136 u -0.0122 u 0.0197 pCilg 0 NIA Un cert: +l-0.0246 +l-0.0276 TPU: +/-0.0253 +l-0.0291 Cesium-137 23.9 24.6 pCi/g 2.77 (0%-20%)

Uncert: +l-0.235 +l-0.219 TPU: +l-1.92 +/-1.95 Chromium-51 u -0.0487 u 0.134 pCilg 0 NIA Uncert: +l-0.281 +l-0.260 TPU: +l-0.282 +l-0.268 Page 36 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 81 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com QC Summary Workorder: 345495 Page 4 of 14 Parm name NOM Sam~le Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376566 Cobalt-56 u 0.0223 u -0.00238 pCi/g 0 NIA Uncert: +l-0.0138 +l-0.0153 TPU: +l-0.0173 +l-0.0153 Cobalt-57 u -0.00248 u 0.00299 pCilg 0 NIA Uncert: +l-0.0191 +l-0.0151 TPU: +l-0.0191 +l-0.0152 Cobalt-58 u 0.000839 u -0.000717 pCi/g 0 NIA Uncert: +l-0.0132 +l-0.0151 TPU: +l-0.0132 +l-0.0151 Cobalt-60 M 0.102 M 0.110 pCi/g 7.63 (0% - 100%)

Uncert: +l-0.0204 +l-0.0284 TPU: +l-0.022 +/-0.0297 Europium-152 u 0.0663 u -0.0469 pCilg 0 NIA Uncert: +l-0.0998 +l-0.0854 TPU: +l-0.104 +l-0.0881 Europium-154 u 0.0596 u -0.0293 pCi/g 0 NIA Uncert: +l-0.0465 +l-0.0516 TPU: +l-0.054 +l-0.0533 Europium-155 u 0.0516 u 0.0821 pCi/g 0 NIA Un cert: +l-0.0762 +l-0.106 TPU: +l-0.0798 +l-0.106 Iridium-192 u 0.00664 u -0.012 pCi/g 0 NIA Uncert: +l-0.0306 +l-0.0276 TPU: +l-0.0308 +l-0.0281 Iron-59 u -0.0121 u -0.0159 pCi/g 0 NIA Uncert: +/-0.0307 +l-0.0335 TPU: +l-0.0312 +l-0.0343 Lead-210 u -0.912 UI 0.00 pCilg 0 NIA Uncert: +l-2.37 +l-0.690 TPU: +l-2.41 +l-0.693 Lead-212 0.483 0.499 pCi/g 3.24 (0%-20%)

Uncert: +l-0.0836 +l-0.0697 TPU: +l-0.0943 +l-0.086 Lead-214 0.454 0.429 pCilg 5.67 (0% - 100%)

Uncert: +l-0.158 +l-0.110 TPU: +l-0.163 +l-0.117 Manganese-54 u -0.00662 u -0.00453 pCilg 0 NIA Uncert: +l-0.014 +/-0.0157 TPU: +l-0.0143 +l-0.0158 Mercury-203 u 0.0262 u -0.00873 pCilg 0 NIA Uncert: +/-0.0299 +/-0.0264 TPU: +l-0.0322 +l-0.0267 Neodymium-147 u -0.20 u -0.406 pCi/g 0 NIA Uncert: +l-0.289 +l-0.277 TPU: +l-0.303 +l-0.334 Neptunium-237 u 0.0109 u 0.00105 pCilg 0 NIA Page 37 of 47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 82 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page 5 of 14 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec

-Batch 1376566 Un cert: +/-0.0618 +l-0.0545 TPU: +l-0.062 +l-0.0545 Neptunium-239 u -0.405 u 0.286 pCilg 0 NIA Uncert: +l-0.303 +l-0.312 TPU: +l-0.356 +l-0.339 Niobium-94 u 0.0134 u 0.00923 pCi/g 0 NIA Un cert: +/-0.0112 +l-0.0142 TPU: +l-0.0128 +l-0.0149 Niobium-95 u 0.0028 u 0.00172 pCi/g 0 NIA Uncert: +/-0.0157 +/-0.0184 TPU: +l-0.0157 +l-0.0184 Potassium-40 9.07 8.99 pCilg .886 (0%-20%)

Un cert: +l-0.597 +l-0.569 TPU: +l-1.01 +l-0.967 Promethium-144 u -0.00283 u 0.00408 pCilg 0 NIA Un cert: +l-0.0147 +l-0.0148 TPU: +l-0.0148 +l-0.0149 Promethium-146 u -0.071 u -0.0187 pCi/g 0 NIA Un cert: +l-0.0547 +/-0.0527 TPU: +l-0.0638 +l-0.0534 Radium-228 0.554 0.431 pCilg 25.1* (0%-20%)

Un cert: +l-0.121 +l-0.137 TPU: +l-0.145 +l-0.146 Ruthenium-I 06 u -0.127 u 0.170 pCilg 0 NIA Uncert: +l-0.235 . +l-0.214 TPU: +l-0.242 +l-0.228 Silver-llOm u -0.0123 u -0.0159 pCilg 0 NIA Un cert: +l-0.0185 +l-0.0217 TPU: +l-0.0194 +/-0.0229 Sodium-22 u 0.0214 u -0.0103 pCilg 0 NIA Un cert: +l-0.0164 +l-0.0181 TPU: +l-0.0191 +l-0.0187 Thallium-208 0.128 0.142 pCilg 9.86 (0%-100%)

Un cert: +l-0.0477 +l-0.0384 TPU: +l-0.0489 +l-0.0401 Thorium-234 u 1.31 U1 0.00 pCilg 0 NIA Un cert: +l-1.32 +l-0.541 TPU: +l-1.36 +l-0.601 Tin-113 u 0.0149 u -0.0197 pCilg 0 NIA Uncert: +l-0.0463 +/-0.0424 TPU: +l-0.0468 +l-0.0433 Uranium-235 u -0.00484 u 0.0244 pCilg 0 NIA Uncert: +l-0.160 +l-0.151 TPU: +l-0.160 +l-0.151 Uranium-238 u 1.31 U1 0.00 pCilg 0 NIA Un cert: +l-1.32 +l-0.541 Page 38 of 47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 83 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workordcr: 345495 Page 6 of 14 Parmname NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376566 TPU: +l-1.36 +l-0.601 Yttrium-88 u 0.0148 u 0.00421 pCilg 0 NIA Uncert: +l-0.00964 +l-0.0119 TPU: +l-0.0118 +l-0.012 Zinc-65 u 2.1 lE-06 u -0.0505 pCi/g 0 NIA Un cert: +l-0.0358 +l-0.0471 TPU: +l-0.0358 +/-0.0528 Zirconium-95 u 0.0104 u 0.00101 pCi/g 0 NIA Uncert: +l-0.0264 +l-0.0268 TPU: +l-0.0268 +l-0.0268 QC!203059877 LCS Actinium-228 u -2.27 pCi/g MXR.1 04101/1410:36 Uncert: +l-2.20 TPU: +l-2.45 Americium-241 491 585 pCi/g 119 (75%-125%)

Un cert: +l-8.80 TPU: +l-53.3 Antimony-124 u 0.146 pCi/g Uncert: +l-0.430 TPU: +l-0.435 Antimony-125 u 1.26 pCi/g Uncert: +l-1.14 TPU: +l-1.28 Barium-133 u 0.345 pCi/g Uncert: +l-0.458 TPU: +l-0.485 Barium-140 u 0.0731 pCi/g Uncert: +l-0.226 TPU: +l-0.229 Beryllium-7 u 1.42 pCi/g Uncert: +l-3.53 TPU: +l-3.59 Bismuth-212 u -3.61 pCi/g Uncert: +l-6.39 TPU: +l-6.61 Bismuth-214 u -0.386 pCi/g Un cert: +l-0.750 TPU: +l-0.770 Cerium-139 1.10 pCi/g Uncert: +l-0.312 TPU: +/-0.390 Cerium-141 u 0.151 pCi/g Un cert: +l-0.356 TPU: +/-0.362 Cerium-144 u -0.489 pCi/g Uncert: +l-l.72 Page 39 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 84 of 468

Attachment 2: HTD Assessment Data GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page 7 of 14 Parm name NOM SamQle Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376566 TPU: +/-1.73 Cesium-134 u -0.0159 pCi/g Uncert: +/-0.523 TPU: +/-0.523 Cesium-136 u -0.559 pCi/g Un cert: +/-0.731 TPU: +/-0.780 Cesium-137 190 183 pCi/g 96.4 (75%-125%)

Uncert: +/-1.80 TPU: +/-14.5 Chromium-51 u -0.182 pCi/g Un cert: +/-2.67 TPU: +/-2.67 Cobalt-56 u 0.000425 pCi/g Un cert: +/-0.504 TPU: +/-0.504 Cobalt-57 10.4 pCi/g Uncert: +/-0.451 TPU: +/-1.13 Cobalt-58 u 0.0082 pCi/g Uncert: +/-0.467 TPU: +/-0.467 Cobalt-60 223 209 pCi/g 93.8 (75%-125%)

Un cert: +/-2.20 TPU: +/-16.6 Europium-152 u -0.36 pCi/g Uncert: +/-1.03 TPU: +/-1.04 Europium-154 u -0.337 pCi/g Un cert: +/-0.835 TPU: +/-0.850 Europium-155 u -0.0639 pCi/g Un cert: +/-0.875 TPU: +/-0.876 Iridium-192 u 0.141 pCi/g Uncert: +/-0.318 TPU: +/-0.324 Iron-59 u -0.514 pCi/g Uncert: +/-1.09 TPU: +/-1.12 Lead-210 6220 pCi/g Uncert: +/-198 TPU: +/-621 Lead-212 u -0.306 pCi/g Uncert: +/-0.514 TPU: +/-0.533 Page 40 of 47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 85 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page 8 of 14 Parm name NOM Sam11Ie Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376566 Lead-214 u -0.575 pCi/g Uncert: +/-0.790 TPU: +/-0.833 Manganese-54 u -0.104 pCi/g Uncert: +/-0.486 TPU: +/-0.489 Mercury-203 u 0.118 pCi/g Uncert: +/-0.307 TPU: +/-0.311 Neodymium-147 u -0.922 pCi/g Uncert: +/-2.54 TPU: +/-2.57 Neptunium-237 0.294 pCi/g Uncert: +/-0.669 TPU: +/-0.682 Neptunium-239 u 0.947 pCi/g.

. Uncert: +/-3.83 TPU: +/-3.86 Niobium-94 u -0.0382 pCi/g Uncert: +/-0.372 TPU: +/-0.373 Niobium-95 u -0.0572 pCi/g Uncert: +/-0.421 TPU: +/-0.421 Potassium-40 u -2.17 pCi/g Uncert: +/-1.97 TPU: +/-2.21 Promethium-144 u -0.123 pCi/g Uncert: +/-0.368 TPU: +/-0.372 Promethium-146 u 0.318 pCi/g Uncert: +/-0.572 TPU: +/-0.590 Radium-228 u -2.27 pCi/g Uncert: +/-2.20 TPU: +/-2.45 Ruthenium-106 u -1.99 pCi/g Uncert: +/-3.51 TPU: +/-3.63 Silver-1 IOm u -0.555 pCi/g Uncert: +/-0.775 TPU: +/-0.818 Sodium-22 u -0.0855 pCi/g Un cert: +/-0.292 TPU: +/-0.294 Thallium-208 u 0.0914 pCi/g Page 41of47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 86 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary

"'orkorder: 345495 Page 9 of 14 Parmname NO:M Sample Qual QC Units RPDo/o REC% Range Anlst Date Time Rad G3mma Spec Batch . 1376566 Uncert: +/-0.388 TPU: +/-0.390 Thorium-234 u -42 pCi/g Uncert: +/-18.6 TPU: +/-28.3 Tin-113 u 0.360 pCi/g Uncert: +/-0.571 TPU: +/-0.571 Uranium-235 u 0.530 pCi/g Uncert: +/-1.55 TPU: +/-1.57 Uranium-238 u -42 pCi/g Uncert: +/-18.6 TPU: +/-28.3 Yttrium-88 0.614 pCi/g Uncert: +/-0.394 TPU: +/-0.484 Zinc-65 31.3 pCi/g Uncert: +/-2.00 TPU: +/-5.62 Zirconimn-95 u 0.335 pCi/g Uncert: +/-0.767 TPU: +/-0.783 QC1203059875 MB Actinium-228 u 0.104 pCi/g :MXRl 04/01/1410:35 Uncert: +/-0.104 TPU: +/-0.115 Americiwn-241 u -0.121 pCi/g Uncert: +/-0.0327 TPU: +l-0.065 Antimony-124 u -0.0102 pCi/g Uncert: +/-O.o445 TPU: +/-0.0448 Antimony-125 u -0.00206 pCi/g Uncert: +/-0.052 TPU: +/-0.052 Barium-133 u -0.00627 pCi/g Uncert: +/-0.0235 TPU: +/-0.0237 Barium-140 u -0.00528 pCi/g Uncert: +/-0.0229 TPU: +/-0.0231 Beryllium-7 u 0.0705 pCi/g Uncert: +/-0.173 TPU: +/-0.176 Bismuth-212 u 0.256 pCi/g Page 42 of 47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 87 of 468

Attachment 2: HTD Assessment Data GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page IO of 14 Parm name NOM Sam~le Qua) QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376566 Un cert: +/-0.308 TPU: +/-0.330 Bismuth-214 u 0.067 pCi/g Un cert: +/-0.0646 TPU: +/-0.0716 Cerium-139 u 0.00236 pCi/g Uncert: +/-0.0126 TPU: +/-0.0127 Cerium-141 u 0.00337 pCi/g Un cert: +/-0.0219 TPU: +/-0.0219 Cerium-144 u -0.064 pCi/g Un cert: +/-0.089 TPU: +/-0.0938 Cesium-134 u -0.00831 pCi/g Uncert: +/-0.0253 TPU: +/-0.0256 Cesium-136 u -0.00236 pCi/g Uncert: +/-0.0334 TPU: +/-0.0334 Cesium-137 u 0.00323 pCi/g Uncert: +/-0.0273 TPU: +/-0.0273 Chromium-SI u 0.0505 pCi/g Uncert: +/-0.161 TPU: +/-0.163 Cobalt-56 u 0.000131 pCi/g Un cert: +/-0.0197 TPU: +/-0.0197 Cobalt-57 u -0.00615 pCi/g Uncert: +/-0.011 TPU: +/-0.0113 Cobalt-58 u -0.000878 pCi/g Uncert: +/-0.0206 TPU: +/-0.0206 Cobalt-60 u 0.0105 pCi/g Un cert: +/-0.0206 TPU: +/-0.0212 Europium-152 u 0.00388 pCi/g Un cert: +/-0.0588 TPU: +/-0.0588 Europium-154 u -0.0229 pCi/g Uncert: +/-0.0703 TPU: +/-0.0711 Europium-155 u 0.00814 pCi/g Uncert: +/-0.0435 TPU:

Page 43 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 88 of 468

Attachment 2: HTD Assessment Data GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page 11of14 Parmname , NOM Sam~Ie Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376566

+/-0.0437 Iridium-192 u 0.0182 pCi/g Uncert: +/-0.0274 TPU: +/-0.0286 Iron-59 u 0.000581 pCi/g Uncert: +/-0.0384 TPU: +/-0.0384 Lead-210 u 0.00173 pCi/g Uncert: +/-0.496 TPU: +/-0.496 Lead-212 u 0.0182 pCi/g Un cert: +/-0.0407 TPU: +/-0.0416 Lead-214 u 0.00541 pCi/g Uncert: +/-0.0471 TPU: +/-0.0472 Manganese-54 u -0.00198 pCi/g Uncert: +/-0.0204 TPU: +/-0.0205 Mercury-203 u -0.00656 pCi/g Uncert: +/-0.01.85 TPU: +/-0.0188 Neodymium-147 u -0.0111 pCi/g Uncert: +/-0.127 TPU: +/-0.127 Neptunium-237 u 0.0311 pCi/g Uncert: +/-0.0564 TPU: +/-0.0582 Neptunium-239 u -0.13 pCi/g Uncert: +/-0.176 TPU: +/-0.186 Niobium-94 u 0.0109 pCi/g Uncert: +/-0.0238 TPU: +/-0.0243 Niobium-95 u 0.0117 pCi/g Uncert: +/-0.0205 TPU: +/-0.0212 Potassium-40 u 0.0563 pCi/g Uncert: +/-0.323 TPU: +/-0.323 Promethium-144 u 0.0152 pCi/g Uncert: +/-0.0245 TPU: +/-0.0255 Promethium-146 u 0.00773 pCi/g Uncert: +/-0.0242 TPU: +/-0.0245 Page 44 of 47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 89 of 468

Attachment 2: HTD Assessment Data GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com QC Summat:I

"'orkorde1*: 345495 Page 12 of 14 Parmname NOM Saml!le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376566 Radium-228 u 0.104 pCilg Uncert: +/-0.104 TPU: +/-0.115 Ruthenium-106 u -0.00129 pCi/g Uncert: +/-0.188 TPU: +/-0.188 Silver-11 Om u 0.0234 pCilg Uncert: +/-0.0344 TPU: +/-0.0361 Sodium-22 u -0.0088 pCi/g Uncert: +/-0.024 TPU: +/-0.0243 Thallium-208 u 0.0251 pCi/g Uncert: +/-0.0325 TPU: +/-0.0326 Thorium-234 u -0.0809 pCi/g Uncert: +l-0.350 TPU: +/-0.352 Tin-113 u -0.0128 pCi/g Uncert: +/-0.0232 TPU: +/-0.0239 Uranium-235 u -0.0839 pCi/g Uncert: +/-0.105 TPU: +/-0.112 Uranitun-238 u -0.0809 pCilg Uncert: +/-0.350 TPU: +/-0.352 Yttrium-88 u -0.000317 pCi/g Uncert: +/-0.0227 TPU: +/-0.0227 Zinc-65 u 0.00875 pCi!g Uncert: +/-0.0448 TPU: +/-0.045 Zirconium-9 5 u 0.0193 pCi!g Uncert: +l-0.035 TPU: +/-0.0361 Batch 1376823 QC1203060559 345495001 DUP Nickel-59 u -72.8 u 13.3 pCi'g 0 N/A TYJI 04/03/1409:53 Uncert: +/-58.9 +/-14.6 TPU: +.1-67.8 +/-15.8 QC1203060560 LCS Nickel-59 1670 1420 pCilg 85.3 (75o/o-125%) TYJI 04/03/1409:59 Uncert: +/-202 TPU: +/-246 QC1203060558 MB Page 45 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 90 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page 13 of 14 Parmname NOM Sam[!le Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1376823 Nickel-59 u 1.49 pCi/g TYJl 04/03/1409:33 Uncert: +/-27.0 TPU: +/-27:0 Rad Gas Flow Batch 1376626 QC1203060081 345495001 DUP Strontium-90 0.492 0.850 pCi/g 53.4* (0%-20%) KSDl 04/0811412:01 Uncert: +/-0.101 +/-0.135 TPU: +/-0.136 +!-0.209 QC1203060082 LCS Strontium-90 3.76 4.37 pCi/g 116 (75%-125%) KSDl 04/07/1412: IO Uncert:. +/-0.249 TPU: +/-0.819 QC1203060080 MB Strontium-90 u -0.0173 pCi/g KSDl 04/0711412:10 Uncert: +/-0.0357 TPU: +/-0.0357 Rad Liquid Scintillation Batch 1376798 QC1203060484 345495001 DUP Nickel-63 u 0.681 u 3.04 pCi/g 0 NIA TYJl 04/03/1417:47 Un cert: +/-14.9 +/-11.3 TPU: +/-14.9 +/-11.4 QC1203060485 LCS Nickel-63 586 621 pCi/g 106 (75%-125%) TYJl 04/03/1418:03 Uncert: +/-28.9 TPU: +/-119 QC1203060483 MB Nickel-63 u 0.610 pCi/g TYJl 04/0411419:34 Un cert: +/-12.1 TPU: +/-12.l Batch 1376803 QC1203060502 345495001 DUP Tecbnetium-99 u -0.521 u -0.279 pCi/g 0 N/AMYMl 04/08/1409:16 Uncert: +/-0.588 +/-0.531 TPU: +/-0.588 +/-0.531 QC1203060503 LCS Technetium-99 37.8 36.1 pCi/g 95.5 (75%-125%) MYMl 04/08/1410:20 Uncert: +/-1.06 TPU: +/-4.29 QC1203060501 MB Technetium-99 u -0.331 pCi/g MYMl 04/08/1408: 13 Uncert: +/-0.521 TPU: +/-0.521 Batch 1376820 Page 46 of 47 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 91 of 468

Attachment 2: HTD Assessment Data GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 345495 Page 14 of 14 Parmname NOM Sample Qnal QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1376820 QC1203060550 345495001 DUP Carbon-14 u -0.165 u -0.169 pCi/g 0 NIA BYSl 04/03/1404:50 Un cert: +/-0.278 +/-0.277 TPU: +/-0.278 +/-0.277 QC1203060552 LCS Carbon-14 36.4 33.4 pCi/g 91.8 (75%-125%) BYSl 04/03/1408:04 Uncert: +/-0.802 TPU: +/-2.56 QCl203060549 MB Carbon-14 u -0.0404 pCi/g BYS 1 04/03/1402:49 Un cert: +/-0.279 TPU: +/-0.279 QC120306055! 345495001 MS Carbon-14 36.5 u -0.165 35.3 pCi/g 96.5 (75%-125%) BYSl 04/03/1406:51 Un cert: +/-0.278 +/-0.841 TPU: +/-0.278 +/-2.70 Notes:

TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).

The Qualifiers in this report are defined as follows:

M Result is <LLD and> MDC U Result is <LLD and< MDC Ul Uncertain identification for gamma spectroscopy X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.

NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.

- Indicates analyte is a surrogate/tracer compound.

" The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 47 of 47 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 92 of 468

Attachment 3 Laboratory Data for HBPP-FSSP-OOLl0-11 & HBPP-FSSP-OOLl0-12 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 93 of 468

Att.achment ~ _L,ab Da.ta_for l:J.BPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 3;56:49PM Page 1 of5

--====~ f\pex-Gamma Analysis Report _for FSS-2014-0264 FSSP-OOL 10-11-001-F GAMMA SPECTRUM ANAL YS/S Sample Identification : FSS-2014-0264 Sample Description : FSSP-OOL10-11-001-F Sample Type : 1L Soll Sample Size : 1.604E+03 grams Facility : Default Sample Taken On : 4/28/2014 8:00:00AM Acquisition Started : 4/30/2014 3:46:24PM Procedure : 1L Soil HD Operator : Administrator Detector Name : DET06 Geometry : 1l Marinelli HD live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0,01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 - 4096 Peak Area Range (In channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibrat!on Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli HD Sample Number d : 1596 .r /J ,,....--)

~""' ~ S"-1-!f .!/ti~

PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/30/2014 3:56:31PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 94 of 468

Attachment 3 Lab Data for HBPF'~FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4/30/2014 3:56:49PM Page 2 of5 Analysis Report for FSS-2014-0264 FSSP-OOL 10-11-001-F

. Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. . (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.54 471 - 483 477.05 9.69E+Ol 22.47 l.31E+02 1.56 F 2 609.61 1215 - 1224 1219.21 3.17E+01 12.42 2.22E+Ol 0.76 F 3 1460.74 2914 - 2928 2921.30 l.23E+02 22. 47 7.SOE+OO 2.23 M =First peak in a multrplet region m = Other peak In a multiplet region F ;= Fitted singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl!grams) Uncertainty K-40 0.99 1460.81

10.67 5.87E+OO 1.llE+OO Pb-212 0. 89 238.63

44.60 2,55E-01 6.llE-02 300.09 3.41 Bi-214 0.47 609,31

46.30 1.68E-01 6.66E-02 1120. 29 15.10 1764.49 15.80

=Energy line found In the spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 95 of 468

Attachment 3 Lab Data for HBPP-FSSP~()OL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 3:56:49PM Page 3 of5 Analysis Report for FSS-2014-0264 FSSP-OOL 10-11-001-F

. INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCJ/grams)

K-40 0.999 5.87E+OO 1.llE+OO Pb-212 0.894 2.55E-01 6. llE-02 Bi-214 0.477 1.68E-01 6.66E-02

? nuclide is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy Jines not used in Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 96 of 468

Attachment 3 Lab Data for HBPP~F~SP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 3:56:49PM Page 4 of5 Analysis Report for FSS-2014-0264 FSSP-OOL 10-11-001-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 3:56:31PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide AH peaks were identified.

M = First peak in a multiplet region

=

m Other peak In a multiplet region F = Fltled slnglet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Defaull\Llbrary\HBPP .NLB Nuclide Energy Yield(%) Activity NuclldeMDA Line MDA Name (pCl/grams) {pC//grams) (pCilgrams)

(keV)

+ K-40 1460.81

10.67 5.87E+OO 6.42E-01 6.42E-Ol Co-60 1173.22 100.00 -1.24E-02 9.20E-02 9.78E-02 1332.49 100.00 4.70E-02 9.20E-02 Nb-94 702.63 100.00 -7.94E-03 7.19E-02 7.19E-02 871.10 100.00 -2.24E-02 7.26E-02 Ag-108m 79.20 7.10 -8.63E-01 S.73E-02 1. 30E+OO 433.93 89.90 -l.40E-02 5.73E-02 614.37 90.40 -l.83E-02 1.0BE-01 722. 95 90.50 -l.SSE-02 7.53E-02 Cs-134 569.31 15.43 l.SSE-01 6.54E-02 3.70E-01 604.70 97.60 -3.99E-02 9.48E-02 795.84 85.40 -5.41E-03 6.54E-02 Cs-137 661.65 85.12 4.94E-02 8.4SE-02 8.45E-02 Eu-152 121.78 28.40 5.9SE-03 1.66E-01 l.86E-01 244.69 7.49 3.73E-02 7.16E-01 344.27 26.50 -2.69E-01 l.66E-01 778.89 12.74 2. 72E-Ol 6.04E-01 867.32 4.16 -5,34E-01 1.78E+OO 964. 01 14.40 3.41E-Ol 7.48E-01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 97 of 468

Attachment 3 Li;ib Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 3:56:49PM Page S of5 Analysis Report for FSS-2014-0264 FSSP-OOL 10-11-001-F Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCi/grams) (pC//grams)

(keV)

Eu-152 1085.78 10.00 8. 69.E-02 1.66E-01 8.02E-Ol 1112.02 13.30 5.90E-02 6.15E-Ol 1407.95 20.70 -l.61E-01 3.36E-01 Eu-154 123.07 40.50 -9.78E-02 l.26E-01 l.26E-01 247.94 6.60 -6.54E-Ol 6,74E-01 723.30 19.70 -7.15E-02 3.46E-01 873.19 11. 50 -2.95E-01 6.49E-01 996. 32 10.30 8.56E-02 6.79E-01 1004.76 17.90 1.02E-01 4.20E-01 1274.45 35.50 -2.26E-01 2.23E-01 Eu-155 105.31 20.70 -1.63E-01 2.56E-01 2.56E-01 Pb-206 803.10 100.00 4.20E-03 6.23E-02 6.23E-02 Ac-228 338.32 11.40 4.25E-01 4.D8E-01 5.47E-01 911. 07 27.70 4.04E-01 4.08E-01 969.11 16.60 4.23E-01 6.25E-01 Th-234 63.29 3.80 2.63E+OO 1. 28E+OO 3.79E+OO 92.59 5.41 8,28E-01 l.28E+OO U-235 143.76 10.50 -7.47E-02 l.OOE-01 4.51E-01 163.35 4.70 4.92E-01 9.48E-Ol 185.72 54.00 2.96E-02 1.00E-01 205.31 4.70 6.31E-Ol l.06E+OO Np-237 311.98 38.60 -7,21E-03 1.lOE-01 1. lOE-01 Am-241 59.54 35.90 -2.99E-01 4.25E-01 4.25E-01

+ = Nuclide Identified during the nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able lo perform the decay correction

? = CAUTION: MDA value is inconsistent with Currie MDA al 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 98 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:11 :50PM Pagel of5 Apex-Gamma Analysis Report for FSS-2014-0265 FSSP-OOL 10-11-002-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-.0265 Sample Description : FSSP-OOL10-11-002-F Sample Type : 1LSoil Sample Size : 1.049E+03 grams Facility : Default Sample Taken On : 4/28/2014 8:10:00AM Acquisition Started : 4/30/2014 4:01:25PM Procedure : 1LSoil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : O.Q1 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) ; 100 -4096 Peak Area Range (In channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/2212012 Efficiency Calibration Used Done On : 4/27,/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Nu~!1er

t.---. ,

PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/30/2014 4:11:32PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 99 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:11:50PM Page 2 of5 Analysis Report for FSS-2014-0265 FSSP-OOL 10-11-002-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV} start end Centroid Area Uncertainty Counts (keV)

F 1 238.41 470 - 482 476.78 9.47E+Ol 22.99 l.46E+02 1. 23 F 2 295.26 585 - 594 590.48 4.llE+Ol 14.73 4.33E+Ol 1.12 F 3 1460.81 2915 - 2929 2921.45 1.80E+02 26.93 3.25E+OO 2.20 M = First peak In a multiplet region m =Other peak in a multlpfet region F =Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : c:\Canberra\Apex\Root\Default\Library\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1. 00 1460,81

10.67 1.23E+Ol 1.96E+OO Pb-212 0,88 238.63

44. 60 3.50E-01 8.74E-02 300.09 3.41

= Energy line found in the spectrum.

- =Manuaffy added nuclide.

? = Manually ed.iled nuclide.

@ =Energy line not used for Welghted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 100 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4/30/2014 4:11 :50PM Page3 of5 Analysis Report for FSS-2014-0265 FSSP-OOL 10-11-002-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

K-40 1. 000 1. 23E+Ol l.96E+OO Pb-212 0,888 3.SOE-01 8.74E-02

? nuclide is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 101 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:11:50PM Page 4 of5 Analysis Report for FSS-2014-0265 FSSP-OOL 10-11*002-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 4:11:32PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 295.26 6.84689E-02 17.92 Tol.

=

M First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted al 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCJ/grams) (pCJ/grams) (pCi/grams) *

(keV)

+ K-40 1460.81

10. 67 l.23E+Ol 6.50E-01 6.SOE-01 Co-60 1173.22 100.00 -l.18E-01 l.13E-01 l.43E-01 1332.49 100.00 3. 4 6E-02 l.13E-01 Nb-94 702.63 100.00 -l.97E-02 8.66E-02 8.66E-02 871.10 100.00 -4.46E-02 1.0lE-01 Ag-108m 79.20 7.10 l.48E+OO 9.98E-02 1.76E+OO 433.93 89.90 7.06E-02 9.98E-02 614.37 90.40 1. 91E-01 1.62E-01 722. 95 90.50 9.52E-02 l.26E-01 Cs-134 569.31 15.43 1.0lE-01 1. 21E-01 5.89E-01 604.70 97.60 1.34E-Ol 1.46E-01 795.84 85.40 5.84E-02 1. 21E-01 Cs-137 661,65 85.12 8.63E-02 l.32E-01 l.32E-01 Eu-152 121. 78 28.40 -8.04E-02 2.26E-01 2.36E-01 244.69 7.49 l.31E-01 1.13E+OO 344.27 26.50 -4.55E-Ol 2.26E-01 778.89 12.74 -8.0lE-02 8. 31E-01 867.32 . 4 .16 3.0lE-01 2.95E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 102 of 468

Attachment 3 Lab Data for HBPP-FS~f'-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:11:50PM Page 5 of5 Analysis Report for FSS-2014-0265 FSSP-OOL 10-11-002-F Nuclide Energy Yield(%) Activity Nuc/ideMDA L/neMDA Name (pCi/grams) (pCl/grams) (pCi!grams)

(keV)

Eu-152 964.01 14.40 l.20E+OO 2.26E-01 1.20E+OO 1085.78 10.00 -9.57E-02 l.25E+OO 1112.02 13.30 -1.32E+OO 8.81E-01 1407.95 20.70 -8.55E-03 5.14E-01 Eu-154 123.07 40.50 -1.17E-02 1.69E-01 1.69E-01 247.94 6.60 -1.14E+OO 9.96E-01 723.30 19.70 4.38E-01 5.80E-01 873.19 11. 50 -2.86E-01 8.31E-01 996. 32 10.30 -4.45E-01 1.00E+OO 1004.76 17.90 4.52E-Ol 7.18E-01 1274.45 35.50 -2.56E-01 3.34E-Ol Eu-155 105.31 20,70 -6,34E-02 3.25E-01 3.25E-01 Pb-206 803.10 100.00 1. 71E-02 1.06E-01 l.06E-01 Ac-228 338.32 11. 40 5,73E-01 5:7BE-01 7.33E-01 911.07 27.70 5.61E-01 5.78E-01 969 .11 16.60 B.71E-01 1.04E+OO Th-234 63.29 3.80 3,03E+OO l.87E+OO 4.30E+OO 92.59 5.41 1.45E+OO 1.87E+OO U-235 143.76 10.50 3.45E-01 1. 35E-Ol 6,55E-01 163.35 4.70 5.SOE-01 l.SlE+OO 185. 72 54.00 4.63E-02 l.35E-01 205.31 4.70 -l.25E+OO 1.38E+OO Np-237 311.98 38.60 -1.13E-01 1.64E-01 l.64E-01 Am-241 59.54 35.90 6.87E-02 4.93E-Ol 4.93E-01

+ = Nuclide Identified during the nuclide ldentiflcatlon

= Energy line found fn the spectrum

> MDA value not calculated

@ Haff-life too short to be able to perform the decay correction

? CAUTION: MDA value is Inconsistent wflh Currie MDA at 95% confidence level

.r HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 103 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/1/2014 12:01 :51 PM Pagel ofS

---== ~pex-Gamma Analysis Report for FSS-2014-0266 FSSP-OOL 10-11-003-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0266 Sample Description : FSSP-OOL 10-11-003-F Sample Type : 1L Soi!

Sample Size : 1.14BE+03 grams Facility : Defaull Sample Taken On : 4/28/2014 8:20:00AM Acquisilion Started : 4/30/2014 4:16:26PM Procedure : 1LSollMD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time ; 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100-4096 Peak Area Range (In channels) : 100. 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Callbrallon Used Done On : 4/27/2011 Efficiency Calibralion Description : 1L Marinelli MD Sample Number : 1608 /J u~.2

>/

k~ S--f-1'/ .s--?-tf PEAK ANAL YS/S REPORT Peak Analysis Performed on : 5/1/2014 12:01:33PM Peak Analysis From Channel : 100 Peak Analysis To Channel ; 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 104 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/1/2014 12:01:51PM Page 2 of5 Analysis Report for FSS-2014-0266 FSSP-OOL10-11-003-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.54 472 - 482 477.04 1.25E+02 26.52 l.75E+02 1.19 F 2 351.92 698 - 710 703.79 7. 71E+01 19.91 8.60E+Ol 1. 38 F 3 609.45 1214 - 1225 1218.88 6.24E+Ol 16.77 2.54E+Ol 1. 41 F 4 1460.89 2915 - 2928 2921.60 1.91E+02 27.64 3.68E+OO 2.02

=

M First peak In a multiplet region m =Other peak In a mulUplet region F = Fitted singlet Errors quoted al 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Library\HBPP .NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity . Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.81

10.67 l.19E+Ol l.84E+OO Pb-212 0.89 238.63

44.60 4.22E-01 9.29E-02 300.09 3.41 Bi-214 0.48 609,31

46.30 4.32E-01 l.19E-01 1120.29 15.10 1764.49 15.80

= Energy line found In !he spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted a! 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 105 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/1/2014 12:01:51PM Page 3 of5 Analysis Report for FSS-2014-0266 FSSP-OOL10-11-003-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.999 l.19E+01 l.84E+00 Pb-212 0.894 4.22E-01 9.29E-02 Bi-214 0.485 4.32E-01 l.19E-01

? nuclide is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used !n Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 106 of 468

Attachm.ent 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/1/2014 12:01:51PM Page 4 of5 Analysis Report for FSS-2014-0266 FSSP-OOL 10-11-003-F UNIDENTIFIED PEAKS Peak Locale Performed on : 5/1/2014 12:01 :33PM Peak Locale From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351.92 1.28488E-01 12.92 Tol.

~§ft>

M = First peak in a multiplet region

=

m Other peak In a mullfplet region

=

F Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Apex\Roo!\Defaull\Library\HBPP.NLB Nuclide Energy Yield(%) Activity NucfideMDA Line MDA Name (pCi/grams) (pCi/grams) (pCf/grams)

(keV)

+ K-40 1460.81

10.67 l.19E+Ol 6.39E-01 6.39E-01 Co-60 1173.22 100.00 -l.21E-01 1.03E-01 1. 28E-01 1332. 49 100.00 1.08E-02 1. 03E-01 Nb-94 702.63 100.00 -4.15E-03 9. 71E-02 9.71E-02 871. 10 100.00 -2.08E-02 l.02E-01 Ag-108m 79.20 7.10 l.73E-01 6.59E-02 1. 72E+OO 433.93 89.90 -3.14E-02 6.59E-02 614.37 90.40 -1. 87E-02 1.61E-01 722. 95 90.50 -5.53E-03 l.22E-01 Cs-134 569.31 15.43 1.18E-01 8.86E-02 5.46E-01 604.70 97.60 -4.77E-02 1. 52E-01 795.84 85.40 -3.75E-02 8.86E-D2 Cs-137 661.65 85.12 3.17E-02 l.15E-01 1.lSE-01 Eu-152 121. 78 28.40 -5.21E-02 2.23E-01 2.23E-01 244.69 7.49 -8.93E-02 l.03E+OO 344.27 26.50 -l.84E-01 2.64E-01 778.89 12.74 1.0lE-01 8.03E-01 867.32 4.16 4.41E-01 2.59E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 107 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/1/2014 12:01:51 PM Page 5 of5 Analysis Report for FSS-2014-0266 FSSP-OOL 10-11-003-F Nuclide Energy Yield(%) Activity Nucl/deMDA LineMDA Name (pCl!grams) (pCi/grams) (pCl!grams)

(keV)

Eu-152 964.01 14.40 2.18E-Ol 2.23E-01 9.37E-01 1085.78 10.00 -5.17E-01 l.17E+OO 1112.02 13.30 -2.70E-Ol 8.76E-01 1407.95 20. 70 2.34E-02 4.96E-01 Eu-154 123.07 40,50 -7.13E-02 1.58E-01 l.58E-01 247.94 6.60 -l.73E+OO 9' 51E-01 723 '30 19.70 -2.54E-02 5.61E-01 873.19 11. 50 5.48E-02 9.07E-01 996.32 10.30 4.34E-01 l.08E+OO 1004.76 17.90 -l.02E-01 6.13E-01 1274.45 35.50 -2. 96E-02 3.68E-01 Eu-155 105.31 20.70 -l.67E-01 3.0lE-01 3.0lE-01 Pb-206 803.10. 100. 00 -5.96E-02 7.88E-02 7.88E-02 Ac-228 338.32 11. 40 5.lOE-01 5.56E-01 7.34E-01 911. 07 27.70 3,87E-01 5.56E"-01 969. 11 16.60 6.66E-01 8,74E-01 Th-234 63.29 3.80 -3,03E-01 l.58E+OO 3.88E+OO 92.59 5.41 -4.65E-01 l.58E+OO U-235 143.76 10.50 -3.27E-Ol l.31E-01 6.14E-Ol 163.35 4.70 5.44E-01 1. 35E+OO 185.72 54.00 2. 86E-02 l.31E-Ol 205.31 4.70 -7.86E-01 l.40E+OO Np-237 311. 98 38.60 7.97E-03 l.64E-01 l.64E-01 Am-241 59.54 35.90 -1.30E-02 4.77E-01 4.77E-01

+ = Nucl!de identified during the nuclide Identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 108 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:14:06PM Page I of5

_f\pex-Gamma Analysis Report for FSS-2014-0267 FSSP-OOL 10-11-004-F GAMMA SPECTRUM ANAL YS/S Sample Identification : FSS-2014-0267 Sample Descrlpllon : FSSP-OOL10-11-004-F Sample Type : 1L Soil Sample Size : 1.264E+03 grams Facility : Default Sample Taken On : 4/28/2014 6:40:00AM Acquisition Started : 4/29/2014 1:03:41PM Procedure : 1LSoil HD Operator : Administrator Detector Name : DET06 Geometry .: 1L Marinelll HD Live Time : 600.0 seconds Real Time. : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (In channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli HD Sample Numb~

PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/29/2014 1:13:48PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 109 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 4/29/2014 1:14:06PM Page 2 of5 Analysis Report for FSS-2014-0267 FSSP-OOL 10-11-004-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM N_o. (keV) start. end Centroid Area Uncertainty counts (keV)*

F 1 76.99 148 - 159 153.97 1.11E+02 24.98 2.27E+02 1. 64 F 2 238.54 471 - 483 477.05 1.07E+02 24.65 1.95E+02 1. 05 F 3 351.86 697 - 710 703.68 1.07E+02 21.13 4.22E+Ol 1. 73 F 4 583.09 1160 - 1172 1166 .18 5.50E+Ol 15.95 3.00E+Ol 1. 63 F 5 609.47 1214 - 1226 1218.93 6.82E+Ol 17 .11 l.90E+Ol 1. 75 F 6 1460.98 2916 - 2929 2921. 79 l.77E+02 26.87 4.lOE+OO 2.07 M =First peak In a mulllplel region

- m = Other peak In a mulliplet region

=

F Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canbarra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nucf/de Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty Bi-xRay 0.54 77'11

100.00 2.18E-01 5 .15E-02 87.20 36.00 K-40 0.99 1460.81

10.67 1.05E+01 l.69E+OO Tl-208 0.69 277.35 6.80 583.14

84.20 1. 93E-01 5.72E-02 860.37 12. 46 Pb-212 0.89 238.63

44.60 3.54E-Ol 8.37E-02 300.09 3.41 Bi-214 0.48 609.31

46,30 4.52E-01 l.16E-01 1120. 29 15.10 1764.49 15.80 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 11 O of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:14:06PM Page 3 of5

. Analysis Report for FSS-2014-0267 FSSP-OOL 10-11-004-F

= Energy line found in Iha spectrum.

=Manually added nuclide.

7 =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV

=

Nuclide conndence index threshold 0.40 Errors quoted al 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

Bi-xRay 0.541 2.18E-01 5.lSE-02 K-40 0.995 1.0SE+Ol 1.69E+00 Tl-208 0. 696 l.93E-01 5. 72E-02 Pb-212 0.894 3.54E-01 8.37E-02 Bi-214 0.483 4.52E-01 l.16E-01 7 nuclide is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted al 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 111 of468

Attachment 3 Lab Data for HBPP-FSSP.:OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:14:06PM Page 4 of5 Analysis Report for FSS-2014-0267 FSSP-0 OL 10-11-004-F UNIDENTIFIED PEAKS Peak Locate Pe normed* on : 412912014 1 :13:4BPM Peak Locale Fro'm Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size {CPS} Uncertainty Type Nuclide F 3 351.86 1.77778E-01 9.90 Tol.

c~~

M4 q-z.9-t M= First peak In a multiplel region m = other peak In a mulliplet region F =Filled singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Default\Library\HBPP.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCl/grams) (pCl/grams) (pCilgrams)

(keV)

+ ~-40 1460.81

10.67 1.05E+Ol 6.50E-01 6.50E-01 Co-60 1173,22 100.00 -9.68E-02 8.31E-02 1.22E-01 1332.49 100.00 -7.15E-02 8.31E-02 Nb-94 702.63 100.00 -3.79E-02 8.65E-02 8.65E-02 871. 10 100.00 -3.73E-02 8.83E-02 Ag-108m 79.20 7.10 -6.77E-01 7.38E-02 2.08E+OO 433.93 89.90 3,33E-04 7.38E-02 614.37 90.40 . -7, 23E-04 1. 57E-01 722. 95 90.50 1. 54E-02 1.18E-01 Cs-134 569.31 15.43 2,34E-01 1.06E-01 6.45E-01 604.70 97.60 -7.33E-02 1.41E-01 795.84 85.40 5.lBE-02 1.06E-01 Cs-137 661. 65 85.12 9.44E-02 l.27E-01 1.27E-01 Eu-152 121. 78 28.40 -4.36E-02 2.25E-01 2.58E-01 244.69 7.49 -9.59E-01 l.lOE+OO 344.27 26.50 -3.26E-01 2.25E-01 778.89 12.74 9.62E-02 7.54E-01 867.32 4.16 -9.19E-01 2.28E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 112 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL1 oc12 412912014 1:14:06PM Page 5 of5

. Analysis Report for FSS-2014-0267 FSSP-OOL 10-11-004-F Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pGl/grams) (pGi/grams) (pCi/grams)

(keV)

Eu-152 964.01 14.40 9.30E-01 2.25E-01 9.22E-01 1085.78 10.00 -8 .16E-Ol 9.04E-01 1112. 02 13.30 -2. 72E-Ol 8.37E-01 1407.95 20.70 -l.21E-01 4.72E-01 Eu-154 123.07 40.50 -1.40E-01 1.78E-Ol l.78E-01 247.94 6.60 -1.31E+OO 1.08E+OO 723. 30 19.70 7.07E-02 5.44E-01 873.19 11.50 4.93E-01 8.49E-Ol 996,32 10.30 -l.46E-01 l.13E+OO 1004.76 17.90 3.09E-01 6.13E-01 1274.45 35.50 1. 72E-01 3.60E-01 Eu-155 105.31 20.70 1.38E-Ol 3.68E-01 3.68E-01 Pb-206 803.10 100.00 2.54E-03 8.24E-02 8.24E-02 Ac-228 338.32 11. 40 O.OOE+OO 5.82E-01 6.30E-01 911.07 27.70 5.80E-01 5.82E-01 969 .11 16. 60 3.50E-01 8.56E-01 Th-234 63.29 3,80 2.00E+OO 1.77E+OO 5.33Et00 92.59 5.41 -8.90E-Ol 1.77E+OO U-235 143.76 10.50 9,73E-02 1'.38E-01 6.88E-01 163.35 4.70 -3.65E-01 l.38E+OO 185.72 54.00 9.25E-02 1. 38E-01 205.31 4.70 6,54E-01 1. 61E+OO Np-237 311. 98 38.60 -5.92E-02 l.55E-Ol 1. 55E-01 Am-241 59.54 35.90 -5,41E-01 6.38E-01 6.38E-01

+ = Nuclide identified during the nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value is lnconsis~ent wilh Currie MDA al 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 113 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:29:08PM Page I of5 1\pex-Gamma Analysis Report for FSS-2014-0268 FSSP-OOL 10-11-005-F GAMMA SPECTRUM ANAL YS/S Sample Identification : FSS-2014-0268 Sample Description : FSSP-OOL10-11-005-F Sample Type : 1LSoil Sample Size : 1.211E+03 grams Facility : Default Sample Taken On : 4/28/2014 8:50:00AM Acquisition Started : 4/29/2014 1:18:43PM Procedure : 1LSoilMD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 - 4096 Peak Area Range (in channels) : 100 -4096 Identification Energy Tolerance : 1.000keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Number : 1586

~~<.-( Lf-> C,-1'/

PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/29/2014 1:28:50PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 114 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:29:08PM Page 2 of5 Analysis Report for FSS"2014*0268 FSSP-OOL 10-11-005-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 77.00 148 - 159 153.98 7.34E+Ol 22.50 2.32E+02 0.93 F 2 238.57 471 - 483 477.09 1.19E+02 .25. 73 *1.98E+02 1. 22 F 3 351.81 697 - 710 703.58 8.25E+Ol 20.03 7.SOE+Ol 1. 21 F 4 609.28 1212 - 1224 1218.55 6.13E+Ol 16.87 3.23E+Ol 1. 44 F 5 1460.87 2915 - 2928 2921.56 1.87E+02 27.52 7.40E+OO 1. 95

=

M First paak in a mul!ipla! region m =Other peak in a multiplet region

=

F Fitted singlet Errors quoted al 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide library Used : C:\Canberra\Apex\Root\Defaull\Ubrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty Bi-xRay 0.54 77 .11

100.00 1.19E-01 3.75E-02 87.20 36.00 K-40 0.99 1460.81

10. 67 l.llE+Ol 1.74E+OO Pb-212 0.89 238.63

44.60 3.BlE-01 8.53E-02 300.09 3.41 Bi-214 0.48 609.31

46.30 4.03E-01 1.13E-01 1120. 29 15.10 1764,49 15.80

/

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 115 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:29:08PM Page 3 of5 Analysis Report for FSS-2014-0268 FSSP-OOL 10-11-005-F

=Energy line found In the spectrum.

- = Manually added nuclide.

? =Manually e-dlted nuclide.

=

@ Energy line not used for Weighted Mean Activity E_nergy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nucllde Nuclide Wt mean Wt mean Comments Name Id Activity Activity Conf{dence Uncertainty (pCl!grams)

Bi-xRay 0.547 1.19E-01 3.75E-02 K-40 0.999 1. llE+Ol 1.74E+OO Pb-212 0. 895 3.81E-01 8.53E-02 Bi-214 0. 486 4.03E-01 l.13E-01

? nuclide is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted al 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 116 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:29:0BPM Page 4 of5 Analysis Report for FSS-2014-0268 FSSP-OOL 10*11-005-F UNIDENTIFIED PEAKS Peak Locate Performed on : 412912014 1:28:50PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 3 351.81 1.37506E-01 12.14 Tol.

~

1114- '/*Z~-l'f M = First peak In a multiplet region

=

m Other peak In a multiplet.region

=

F Fitted singlet Errors quoted al 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB Nucf/de Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pC//grams) (pCl/grams) (pCi!grams)

(keV)

+ K-40 1460.81

10.67 1. llE+Ol 7.95E-01 7.95E-01 Co-60 1173.22 100.00 8.98E-03 l.21E-01 1.SlE-01 1332.49 100.00 2.93E-03 l.21E-01 Nb-94 702.63 100.00 -1.54E-02 8.SlE-02 9.SlE-02 871.10 100.00 -7.81E-02 8.51E-02 Ag-108m 79.20 7.10 -2.47E-01 B.28E-02 1.67E+OO 433.93 89.90 -5.64E-02 8.28E-02 614. 37 90.40 -7.53E-02 1. 59E-01 722.95 90.50 5.43E-02 1.16E-01 Cs-134 569.31 15.43 2.63E-01 1.33E-01 5.99E-01 604.70 97.60 l.20E-02 l.40E-01 795.84 85.40 4.0lE-02 1. 33E-01 Cs-137 661.65 85.12 9.30E-02 1.26E-01 1. 26E-01 Eu-152 121. 78 28.40 -1.60E-02 2.33E-Ol 2.33E-01 244.69 7.49 -8.57E-01 1.02E+00 344.27 26. 50 -4.93E-Ol 2.35E-01 778.89 12.74 3.75E-02 7.62E-01 867.32 4.16 -5.90E-01 2.26E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 117 of 468

Attachment

. 3 Lab Data for .HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 '

4/29/2014 1:29:08PM Page 5 of5 Analysis Report for FSS-2014-0268 FSSP-OOL 10-11-005-F Nuclide Energy Yield(%) Activity NucfideMDA LineMDA Name (pCilgrams) (pCf/grams) (pCilgrams)

(keVJ Eu-152 964.01 14. 40 l,16E+OO 2.33E-01 1. llE+OO 1085.78 10.00 4.89E-01 1.16E+OO 1112. 02 13.30 -1.63E+OO 7.14E-01 1407.95 20.70 2.67E-01 4.93E-01 Eu-154 123.07 40.50 -9.26E-02 l.62E-01 1.62E-01 247.94 6.60 -2.62E+OO 8.95E-01 723.30 19.70 2.49E-01 5.32E-01 873.19 11. 50 3.39E-Ol 8.60E-01 996. 32 10.30 1. 48E-01 8.40E-01 1004.76 17.90 6.lOE-02 5.20E-01 1274.45 35.50 6.Q8E-02 2.89E-Ol Eu-155 105.31 20.70 7.74E-02 3.23E-01 3.23E-01 Pb-206 803.10 100.00 -1.26E-01 9.40E-02 9.40E-02 Ac-228 338.32 11. 40 5.41E-01 4.83E-01 6.73E-'-01 911. 07 27.70 1.45E-01 4.83E-01 969.11 16.60 7.22E-01 9.54E-Ol Th-234 63.29 3.80 1.45E+OO 1.63E+OO 4.04E+OO 92.59 5.41 7.40E-01 l.63E+OO U-235 143.76 10.50 -1.57E-01 1. 34E-01 5 .. BSE-01 163.35 4.70 -7.14E-01 1.34E+OO 185. 72 54.00 1.28E-01 1.34E-01 205.31 4.70 6. 72E-01 1.43E+OO Np-237 311.98 38.60 -6.67E-02 1.47E-Ol 1. 4 7E-01 Am-241 59.54 35.90 -4.76E-Ol 4.63E-01 4.63E-Ol

+ = Nuclide ldentifie~ during the nuclide identification

= Energy line found in the spectrum

> MDA value not calculated

@ Half-life loo short to be able to perform the decay correction

? CAUTION: MDA value is Inconsistent wilh Currie MDA al 95% confidence level FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 118 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:44:10PM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0269 FSSP-OOL10-11-006-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0269 Sample Description : FSSP-OOL 10-11-006-F Sample Type : 1L Soll Sample Size : 1.161E+03 grams Facility : Default Sample Taken On : 4/28/2014 9:20:00AM Acquisition Started : 4/29/2014 1:33:44PM Procedure : 1L Soil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 212212012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD sample Num~w

/C-"' .4~ ,, lf *fl1-li PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/29/2014 1:43:51PM Peak Analysis From Channel : 100 Peak Analysis.To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 119 of 468

Attachment 3 Lab Data for HBPP~_FS~P-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1 :44:1 OPM Page.2 of5 Analysis Report for FSS-2014-0269 FSSP-OOL 10-11-006-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.51 472 - 480 476.99 l .11E+02 24.99 l.19E+02 1.15 F 2 351.85 700 - 708 703.67 8 .11E+Ol 18.88 2.40E+Ol 1.54 F 3 609.43 1214 - 1225 1218.86 4.79E+Ol 15.20 2.59E+Ol 1. 45 F 4 1460. 96 2914 - 2928 2921.74 1.57E+02 25.14 7.68E+OO 2.21 M = First peak in a multiple! region

=

m Other peak In a multiplet region

=

F Filled singlet Errors quoted al 2.000sigma No background subtract performed on .this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB IDENTIFIED NUCUDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 146.0. 81

10.67 9.67E+00 1.64E+OO Pb-212 0.89 238.63

44.60 3.71E-01 8.62E-02 300.09 3.41 Bi-214 0.48 609.31

46.30 3.28E-01 1.06E-01 1120. 29 15.10 1764.49 15.80

=Energy line found in the .spectrum.

- = Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 120 of 468

Attachment 3 Lab Data for HBPP~F$SP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:44:1 OPM Page 3 of5 Analysis Report for FSS-2014-0269 FSSP-OOL 10-11-006-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl!grams)

K-40 0,997 9.67E+OO l.64E+OO Pb-212 0.893 3.71E-01 8.62E-02 Bi-214 0.485 3.28E-01 l,06E-01

? nuclide is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used In Weighted Mean Aclivity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 121 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10~11 & HBPP-FSSP-OOL10-12 4/29/2014 1:44:10PM Page 4 of5 Analysis Report for FSS-2014-0269 FSSP-OOL 10-11-006-F UNIDENTIFIED PEAKS Peak Locale Performed on : 4/29/2014 1:43:51PM Peak Locale From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nu cl/de F 2 351.85 1.35236E-01 11. 64 Tol.

~

AJk 'I* 'Z <?~I

=

M First peak in a mulllplet region m =other peak in a mulllplst region

=

F Fitted singlet Errors quoted al 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbsrra\Apex\Rool\Defaull\Ubrary\HBPP.NLB Nuclide Energy Yield(%) Activity NucfideMDA Line MDA Name (pCi/grams) (pCl/grams) (pCi/grams)

(keV)

+ K-40 1460.81

10.67 9.67E+OO 8.49E-01 8.49E-01 Co-60 1173.22 100.00 2.31E-02 8.62E-02 l,43E-01 1332.49 100.00 1.63E-02 8.62E-02 Nb-94 702. 63 100.00 7.77E-02 9.61E-02 9.76E-02 871.10 100.00 3.92E-03 9.61E-02 Ag-108m 79.20 7.10 -4.48E-01 7.38E-02 l.53E+00 433.93 89.90 -5.25E-02 7.38E-02 614.37 90.40 -l.75E-02 l.51E-01 722. 95 90.50 6.17E-02 1.17E-01 Cs-134 569.31 15. 43 2.15E-01 1. 09E-01 5.SOE-01 604.70 97.60 -2.06E-02 1.29E-01 795.84 85,40 6.28E-02 l.09E-01 Cs-137 661.65 85.12 1.42E-Ol 1.34E-01 l.34E-01 Eu-152 121. 78 28.40 -7.20E-02 2.22E-01 2.24E-01 244.69 7.49 -1.29E+OO 9.93E-01 344.27 26.50 -4.35E-01 2.22E-01 778.89 12.74 -l.88E-01 6.34E-01 867.32 4.16 -6.48E-01 2.46E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 122 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:44:10PM Page 5 of5 Analysis Report for FSS-2o1'4-0269 FSSP-OOL 10-11-006-F Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pCl/grams) (pCl/grams) (pCi/grams)

(keV)

Eu-152 964.01 14.40 O.OOE+OO 2.22E-0.1 8.41E-01 1085.78 10.00 -2.35E-Ol 9.35E-01 1112.02 13.30 -4.65E-01 9.50E-01 1407.95 20.70 -3.86E-02 4.36E-01 Eu-154 123.07 40.50 -3.16E-02 1.60E-01 1.60E-Ol 247.94 6. 60 -l.92E+OO 9.20E-01 723. 30 19. 70 2,84E-01 5.39E-01 873.19 11. 50 -6.95E-02 8,77E-01 996.32 10.30 2.68E-01 8.76E-01 1004.76 17.90 -2.25E-01 5.43E-01 1274.45 35.50 1.92E-01 4.07E-01 Eu-155 105.31 20.70 2.05E-01 3.13E-Ol 3.13E-01 Pb-206 803.10 100.00 -6.00E-03 8.75E-02 8.75E-02 Ac-228 338.32 11. 40 4.78E-01 5.55E-01 7. llE-01 911. 07 27.70 4.16E-01 ?.55E-01 969.11 16. 60 4.94E-01 7,59E-01 Th-234 63.29 3.80 -3.90E-01 1.57E+OO 3.69E+OO 92.59 5.41 1.69E-Ol l.57E+OO U-235 143.76 10.50 l.78E-Ol 1. 25E-01 6.16E-01 163,35 4.70 -4.59E-Ol 1.25E+OO 185. 72 54.00 6,57E-02 1.25E-01 205.31 4.70 9.87E-01 l.40E+OO Np-237 311. 98 38.60 7.29E-03 1.57E-01 1.57E-01 Am-241 59.54 35.90 -1.78E-01 4.78E-01 4.78E-01

+ = Nuclide identified during the nuc!lde identification

= Energy line found in the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value Is inconsistent wilh Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 123 of 468

Attachment 3 Lab Datl:J.for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:41 :52PM Page l of5

'l\pex-Gamma Analysis Report for FSS-2014-0270 FSSP-OOL 10-11-007-F GAMMA SPECTRUM ANALYSIS Sample ldentiflcallon : FSS-2014-0270 Sample Description : FSSP-OOL10-11-007-F Sample Type : 1LSoil Sample Size : 1.209E+03 grams Facility : Default Sample Taken On : 4/28/2014 9:00:00AM Acquisition Started : 4/30/2014 4:31 :28PM Procedure : 1LSoil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD live Time : 600.0 seconds Real Time : 600.1 seconds Dead.Time : O.Q1 %

Peak Locate Threshold : 4.00 Peak Locale Range (In channels) : 100-4096 Peak Area Range (in channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibralion Used Done On : 4/27/2011 Efficiency Calibration Description : 1l Marinelli MD Sample Number : 1599 ,./J

&.,e{}~t s--1-1r fl/;d~

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 4/30/2014 4:41:34PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 124 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:41:52PM Page 2 of5 Analysis Report for FSS-2014-0270 FSSP-OOL 10-11-007-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238,54 471- 482 477.03 1. 28E+02 26. 46 l.76E+02 1. 50 F 2 295.12 586 - 595 590.20 4.35E+Ol 15.19 4.36E+Ol 1. 24 F 3 351.82 698 - 709 703.61 8.97E+Ol 20.36 5.45E+Ol 1. 41 F 4 609.40 1213 - 1225 1218.79 7.48E+01 18.36 3.32E+Ol 1. 55 F 5 1460.81 2914 - 2929 2921. 4 6 1. 88E+02 . 27.74 1.17E+Ol 1. 88 M = First peak in a multiplet region m =Other peak in a multiplet region F = Fitted singlet Errors quoted al 2.000slgma No background subtract performed on this spectrum.

NUCLIDE !DENT/FICA TJON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl/grams) Uncertainty K-40 1. 00 1460.81

10.67 1. llE+Ol l.75E+OO Pb-212 0.89 238.63

44.60 4. llE-01 8.82E-02 300.09 3. 41 Bi-214 0.48 609.31

46.30 4.92E-01 1. 24E-01 1120.29 15.10 1764.49 15.80 Pb-214 0. 79 241. 98 7.49 295.21

19.20 3.80E-01 1.34E-01 351. 92

37.20 4.66E-01 l.OBE-01 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 125 of 468

_f\ttachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/3012014 4:41:52PM Page 3 of5 Analysis Report for FSS-2014-0270 FSSP-OOL 10-11-007-F

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold= 0.40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 1. 000 l. llE+Ol l.75E+OO Pb-212 0.894 4. llE-01 8.82E-02 Bi-214 0.486 4.92E-01 l.24E-01 Pb-214 0.790 4.32E-01 8.44E-02

? nuclide is part of an undetermined solution X

nuclide rejecled by the interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sfgma FSS Report HBPP-FSSP-OOL 1U-11 & HBPP-FSSP-OOL10-12 Page 126 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4{30/2014 4:41:52PM Page 4 of5 Analysis Report for FSS-2014-0270 FSSP-OOL 10-11-007-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 4:41:34PM Peak [ocate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak In a multiplet region m = Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2,000sigma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Apex\Root\Defauit\Library\HBPP.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pC//grams) (pCl/grams)

(keV)

+ K-40 1460.81

10.67 l. llE+Ol 9.73E-01 9.73E-01 Co-60 1173.22 100.00 3.13E-02 1.07E-01 l.44E-01 1332.49 100.00 -3.08E-02 1.07E-01 Nb-94 702.63 100.00 -2.64E-03 7.46E-02 8.91E-02 871. lb 100.00 -4.24E-02 7.46E-02 Ag-108m 79.20 7.10 2. 31E-01 7.41E-02 l,57E+OO 433.93 89.90 2.06E-02 7. 41E-02 614.37 90.40 5.09E-03 1.68E-01 722.95 90.50 9 .13E-02 1.19E-01 Cs-134 569.31 15.43 2.80E-01 1. 26E-01 5.86E-01 604.70 97. 60 -1. 71E-02 l.47E-01 795.84 85.40 6.27E-02 l.26E-01 Cs-137 661.65 85.12 6. 44E-02 l. lOE-01 1.lOE-01 Eu-152 121.78 28.40 2.77E-03 2.14E-01 2.17E-01 244.69 7.49 5.71E-01 9.58E-01 344.27 26.50 -4.61E-01 2.14E-01 778.89 12.74 -2.68E-01 6.26E-01 867.32 4.16 -9.97E-01 1.98E+OO 964.01 14.40 4.95E-Ol 9.88E-01' FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 127 of 468 -

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:41:52PM Page 5 of5 Analysis Report for FSS-2014-0270 FSSP-OOL 10-11-007-F Nuclide , -Energy Yield(%) Activity NuclideMDA LlneMDA Name (pCi/grams) (pCifgrams) (pC/fgrams)

(keV)

Eu-152 1085.78 10.00 -1.07E+OO 2.14E-01 9. 96E-01 1112. 02 13.30 -l.21E+OO 8.lOE-01 1407. 95 20.70 2.05E-01 5.38E-01 Eu-154 123.07 40.50 -3.91E-02 1.52E-01 1.52E-01 247.94 6.60 -8.90E-01 9.59E-01 723. 30 19.70 4.20E-01 5.47E-01 873.19 11. 50 -2.BOE-01 6.50E-01 996. 32 10.30 4.24E-01 1.00E+OO 1004.76 17,90 -l.96E-01 5.37E-01 1274.45 35.50 5.58E-02 3,58E-01 Eu-155 105.31 20.70 -1.62E-01 3.12E-01 3.12E-01 Pb-206 803.10 100.00 -2.55E-02 1. OlE-01 l*. OlE-01 Ac-228 338.32 11. 40 6.64E-01 5.54E-01 6.74E-01 911. 07 27.70 7,38E-01 5.54E-01 969 .11 16.60 9.42E-01 8.81E-Ol Th-234 63.29 3.80 -l.03E+OO l.67E+OO 3.85E+OO

92. 59 5.41 -3.73E-01 1.67E+OO U-235 143.76 10.50 -9.29E-02 1. 36E-Ol 6.17E-01 163.35 4.70 4.58E-01 1.38E+OO 185. 72 54.00 2.llE-02 1. 36E-01 205.31 4.70 -5,65E-01 1. 43E+OO Np-237 311.98 38.60 -3,83E-02 l.60E-01 1.60E-01 Am-241 59.54 35.90 -8.87E-02 4.62E-01 4.62E-01

+ = Nuclide identified during the nuclide Identification

= Energy line found Jn the spectrum

> MDA value not calculated

@ Half-life too short lo be able to perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA at 95% conf!dence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 128 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:59:11PM Page l of5

~f\pex-Gamma Analysis Report for FSS-2014-0271 FSSP-OOL 10-11-008-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0271 Sample Description : FSSP-OOL10-11-008-F Sample Type : 1L Soil Sample Size : 1.143E+03 grams Facility : Defaull Sample Taken On : 4/28/2014 9:45:00AM Acquisition Started : 4/29/2014 1:48:46PM Procedure : 1l Soil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : O.o1 %

Peak locate Threshold : 4.00 Peak Locate Range (In channels) : 100 -4096 Peak Area Range (in channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Callbrallon Used Done On : 4/27/2011 Efficiency Calibration Description : 1l Marinelli MD Sample Number : 1588

,tfrn. 4~ '(-J. "1-1'{

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 4/29/2014 1:58:53PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 129 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:59:11PM Page 2 ofS Analysis Report for FSS-2014-0271 FSSP-OOL 10-11-008-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.48 473 - 482 476.91 7.49E+Ol 21.59 l.38E+02 1. 22 F 2 295.26 585 - 595 590.48 3.98E+Ol 15.97 7.84E+Ol 1.19 F 3 1460.87 2914 - 2928 2921. 56 l.76E+02 26.61 3.75E+OO 2.23

=

M First peak in a multiplet region m = Other peak in a multiple! region

=

F Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield{%) Actfvity Activity Name Confidence (keV} (pCi!grams) Uncertainty K-40 0.99 1460.81

10.67 1.lOE+Ol 1.77E+OO Pb-212 0.89 238.63

44.60 2.54E-01 7.48E-02 300.09 3.41

=Energy line found in the spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 130 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4/29/2014 1:59:11 PM Page 3 ofS Analysis Report for FSS-2014-0271 FSSP-OOL 10-11-008-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.999 1.lOE+Ol 1. 77E+OO Pb-212 0.892 2.54E-01 7.48E-02

? nuclide is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 131 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/2~/2014 1:59:11PM Page 4 of5 Analysis Report for FSS-2014-0271 FSSP-OOl 10-11-008-F UNIDENTIFIED PEAKS Peak locate Performed on : 4/29/2014 1 :58:53PM Peak locate From Channel : 100 Peak locate To Channel : 4096 Peak CPS(%) Peak *Tolerance Peak No. Energy (keV} Peak Size (CPS) Uncertainty Type Nuclide F 2 295.26 '-- 6.63513E-02 20.06 Tol.

~

t '{~ z (./'{

=

M First peak in a multiplet region m = other peak In a multiplet region

=

F Filled single!

Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NlB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCi/grams) (pCi!grams)

(keV)

I

+ K-40 1460.81

10.67 l.lOE+Ol 6.SOE-01 6.50E-01 Co-60 1173. 22 100.00 -6.92E-03 1.08E-01 1.34E-01 1332.49 100. 00 6.21E-02 1.08E-01 Nb-94 702.63 100.00 4.54E-02 8.75E-02 9.43E-02 871.10 100.00 -3.26E-02 8.75E-02 Ag-108m 79.20 7.10 4.92E-01 7.14E-02 1.67E+OO 433.93 89.90 -7.00E-02 7.14E-02 614.37 90.40 1.61E-01 l.40E-01 722.95 90.50 4.58E-02 9.87E-02 Cs-134 569.31 15.43 3.09E-01 1.29E-Ol 7.16E-01 604.70 97.60 1. 41E-01 1.36E-01 795,84 85.40 8.73E-02 1. 298-01 Cs-137 661.65 85.12 6.79E-02 1.21E-01 1. 21E-01 Eu-152 121.78 28.40 1.41E-01 2.28E-01 2.28E-01 244.69 7.49 -1.16E-01 1.02E+OO 344.27 26.50 -1.37E-01 2.38E-01 778.89 12.74 -5.0lE-02 7.31E-01 867.32 4.16 -1. 89E+OO 2.28E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 132 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 1:59:11PM Page S of5 Analysis Report for FSS-2014-0271 FSSP-OOL10-11-008-F Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pC//grams) (pCl/grams) (pCl/grams)

(keV)

Eu-152 964.01 14.40 4.36E-Ol 2.28E-01 1.05E+OO 1085.78 10.00 -6.SlE-01 1.15E+OO 1112.02 13.30 -7.35E-01 7.83E-01 1407.95 20.70 3.45E-Ol 5. 69E-01 Eu-154 123.07 40.50 -7.67E-02 l.56E-01 1.56E-01 247.94 6,60 -1.0SE+OO 9.76E-01 723.30 19.70 2.lOE-01 4.54E-01 873.19 11. so 2.28E-01 7.86E-01 996.32 10.30 1.18E-02 1. 09E+OO 1004.76 17.90 -5.73E-02 6.45E-01 1274.45 35,50 -7.70E-02 3.60E-01 Eu-155 105.31 20.70 -7,05E-02 3.13E-Ol 3.13E-01 Pb-206 803.10 100.00 1.70E-02 l.02E-01 l.02E-01 Ac-228 338.32 11. 40 9.74E-02 4.93E-Ol 6.35E-01 911.07 27.70 3.12E-Ol 4.93E-01 969 .11 16.60 1.00E+OO 9.83E-01 Th-234 63.29 3.80 3.41E+OO l.60E+OO 3. 96E+OO 92.59 5.41 8.31E-Ol l.60E+OO U-235 143.76 10.50 2.21E-01 l.28E-01 5.96E-01 163.35 4.70 7.37E-02 1.34E+OO 185.72 54.00 7,66E-02 l.28E-Ol 205.31 4.70 -2.52E-Ol 1.36E+OO Np-237 311. 98 38.60 -4.17E-02 1.58E-01 1.58E-01 Am-241 59.54 35.90 -l.17E-01 4.74E-01 4.74E-Ol

+ = Nuclide identified during lhe nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too sh9rt lo be able to perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 133 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:56:53PM Page 1 of5 f\pex-Gamma Analysis Report for FSS-2014-0272 FSSP-OOL 10-11-009-F GAMMA SPECTRUM ANAL YS/S Sample Identification : FSS-2014-0272 Sample Description : FSSP-OOL10-11-009-F Sample Type ; 1L Soil Sample Size : 1.195E+03grams Facility : Default Sample Taken On : 4/29/2014 9:50:00AM Acquisition Started : 4/30/2014 4:46:29PM Procedure : 1LSoil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time ; 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 - 4096 Peak Area Range (In channels) ; 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2122/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibratlon Description : 1L Marinelli MD Sample Number ~ : 1600 / ;J )

,£-., If~ s*-1-1r tf/;A~ S-- ?-/t(

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 4/30/2014 4:56:35PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 &*HBPP-FSSP-OOL10-12 Page 134 of 468

Attachment 3 Lab Dal? for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL fci-12 4/30/2014 4;56;53PM Pnge 2 of5 Analysis Report for FSS-2014-0272 FSSP-OOL 10-11-009-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid* *Area Uncertainty Counts (keV)

F 1 238.45 470 - 483 476. 86 l.30E+02 25.48 1.62E+02 1. 61 F 2 295.06 586 - 596 590.07 4.03E+Ol 15.94 7.95E+Ol 1.15 F 3 351.69 699 - 708 703.34 7.84E+Ol 19.82 5.84E+Ol 1. 30 F 4 609.38 1215 __, 1223 1218,76 3.44E+01 13.08 2.06E+Ol 1.32 F 5 1461.03 2914 - 2929 2921. 88 l.94E+02 27.90 3.87E+OO 2.16 M " First peak In a multiplet region m " Other peak in a multiple! region F " Filled singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used ; C:\Canberra\Apex\Root\Default\llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activlfy Activity Name Confidence (keV) (pCl/grams) Uncertainty K-40 0.99 1460.81

10.67 l.16E+Ol l.79E+OO Pb-212 0.89 238.63

44.60 4.23E-01 8.63E-02 300.09 3.41 Bi-214 0.48 609.31

46.30 2.29E-01 8.81E-02 1120.29 15.10 1764.49 15.80 Pb-214 0.78 241. 98 7.49 295.21

19.20 3.56E-Ol 1. 42E-01 351.92

37.20 4.12E-01 l.06E-01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 135 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 4/30/2014 4:56:53PM Page 3 of5 Analysis Report for FSS-2014-0272 FSSP-OOU0-11-009-F

=Energy line found in the spectrum.

=Manually added nuclide.

? = Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl!grams)

K-40 0.993 l.16E+Ol l.79E+OO Pb-212 0.890 4.23E-Ol B.63E-02 Bi-214 0. 486 2.29E-01 8.BlE-02 Pb-214 0.786 3.92E-01 8.SlE-02

? nuclide Is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used fn Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 136 of 468

Attachment 3 Lab Data. for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:56:53PM Page 4 of5 Analysis Report for FSS-2014-0272 FSSP-OOL 10-11-009-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 4:56:35PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were idenlified.

=

M First peak in a multiplet region'

=

m other peak in a multiple! region F = Filled singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaullllibrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nucl/deMDA LineMDA Name (pCl/grams) (pCi/grams) (pCJ!grams)

(keV)

+ K-40 1460.81

10.67 1.16E+Ol .6. 33E-01 6.33E-01 Co-60 1173.22 100.00 5. 92E-02 9.90E-02 1.39E-01 1332.49 100.00 l,65E-02 9.90E-02 Nb-94 702.63 100.00 l.27E-02 9.34E-02 9.64E-02 871.10 100.00 -3.12E-03 9.34E-02 Ag-108m 79.20 7 .10 3.96E-Ol 7.SOE-02 1.64E+OO 433.93 89.90 -2.58E-02 7.50E-02 614.37 90.40 -3.04E-02 1. 35E-01 722.95 90.50 4.13E-03 1. llE-01 Cs-134 569.31 15.43 l,44E-01 9.64E-02 6.14E-01 604.70 97.60 -1.23E-01 l.20E-01 795.84 85.40 -l.07E-02 9.64E-02 Cs-137 661. 65 85.12 l,03E-01 1.22E-01 1.22E-01 Eu-152 121.78 28. 40 1.44E-01 2.15E-01 2.15E-01 244.69 7.49 -4.SSE-01 l.04E+OO 344.27 26.50 -2. 4 4E-01 2.43E-01 778.89 12.74 -3.88E-01 5.39E-01 867.32 4.16 1.85E-01 2.39E+OO 964.01 14.40 2.20E-Ol 8.87E-01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 137 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 4:56:53PM Page 5 of5 Analysis Report for FSS-2014*0272 FSSP-OOL10-11-009-F Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams)' (pC!lgrams) (pC/lgrams)

(keV)

Eu-152 1085.78 10.00 -3.99E-01 2.15E-01 1.04E+OO 1112. 02 13.30 -1.76E+OO 8.19E-01 1407.95 20.70 2.39E-01 5.23E-01 Eu-154 123.07 40.50 -5.99E-02 1.51E-01 1.51E-01 247.94 6.60 -8.0SE-01 9.64E-01 723.30 19.70 1.90E-02 5.09E-01 873.19 11. 50 2.86E-03 8.34E-01 996.32 10.30 l.90E-01 1.02E+OO 1004.76 17.90 3.07E-01 6.17E-01 1274.45 35.50 5.65E-02 3,62E-01 Eu-155 105.31 20.70 -9. 78E-02 3.14E-01 3.14E-01 Pb-206 803 .10 100.00 -6.31E-02 8.05E-02 8.05E-02 Ac-228 338.32 11.40 7.33E-01 5.40E-Ol 7.53E-01 911. 07 27,70 2,94E-01 5,40E-01 969.11 16.60 7.88E-01 7. 96E-01 Th-234 63.29 3.80 2.36E-01 1.53E+OO 3.76E+OO 92.59 5.41 -3.07E-01 1.53E+OO U-235 143.76 10.50 5.00E-02 1. 27E-Ol 5.86E-01 163.35 4.70 2.lOE+OO 1.36E+OO 185. 72 54.00 9. 43E-02 1.27E-01 205.31 4.70 7.87E-Ol 1.40E+OO Np-237 311.98 38.60 9, 71E-02 1. 72E-Ol 1. 72E-01 Am-241 59.54 35.90 1.16E-01 4.53E-01 4.53E-01

+ = Nuclide Identified during the nuclide idenlificallon

= Energy line found in the spectrum

> MDA value not calculated

@ Half-life too short lo be able to perform the decay correction

? CAUTION: MDA value ls Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 138 of 468

AttachrnE!llt} Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/1/2014 4:08:25PM Page l of5 jl\pex~Gamma Analysis Report for FSS-2014-0273 FSSP-OOL 10-11-010-F GAMMA SPECTRUM ANALYSIS Sample Jdenlificalion : FSS-2014-0273 Sample Description : FSSP-OOL10-11-010-F Sample Type : 1L Soil Sample Size : 1.352E+03 grams Faclllty : Default Sample Taken On : 4/29/2014 9:25:00AM Acqulslt!on Started : 5/1/2014 3:57:59PM Procedure : 1LSollHD Operator : Administrator Detector Name : DET06 Geometry : 1L Marlnefli HD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 -4096 Peak Area Range (Jn channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1 L Marlnelll HD Sample Number /J

&.IL~

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 5/1/2014 4:08;06PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 139 of 468

Attachment 3 Lab Data for H_BPp_-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/1/2.014 4:08:2.5PM Page 2 of5 Analysis Report for FSS-2014-0273 FSSP-OOL 10-11-010-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.54 472 - 483 477.04 l.28E+02 25.66 l.47E+02 1.35 F 2 351.97 699 - 709 703.89 7.49E+Ol 18.00 2.BOE+Ol 1. 77 F 3 583.17 1162 - 1171 1166.33 4.88E+Ol 15.42 2.75E+Ol 1. 47 F 4 609.36 1213 - 1222 1218.71 7.37E+Ol 18.44 3.00E+Ol 1. 53 F 5 1460.87 2915 - 2929 2921.56 1.71E+02 26.36 7.50E+OO 2.08 M = First peak in a multiplet region m = Other peak Jn a multiplet region F = Filled singlet Errors quoted al 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.81

10.67 9.63E+OO l.58E+OO Tl-208 0.69 277.35 6.80 583.14

84.20 l.63E-Ol 5.23E-02 860.37 12.46 Pb-212 0.89 238.63

44.60 4.0lE-01 8.36E-02 300.09 3.41 Bi-214 0. 48 609.31

46.30 4.64E-01 1.19E-01 1120. 29 15.10 1764.49 15.80 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 140 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HB.PP-FSSP-OOL10-12 5/1/2014 4:08:25PM Page 3 of5 Analysis Report for FSS-2014-0273 FSSP-OOL 10-11-010-F

=Energy line found in the spectrum.

= Manually added nuclide.

? =Manually edited nuclide,

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.QOO keV Nuclide confidence index threshold = 0.40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.999 9.63E+OO 1.58E+OO Tl-208 0' 696 1.63E-01 5.23E-02 Pb-212 0.893 4.0lE-01 8.36E-02 Bi-214 0.485 4.64E-Ol 1.19E-01

? nuclide Is part of an undetermined soluflon X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 141 of468

Attachment 3 Lab Data for HBPP-FSSP-00~10-.11 & HBPP-FSSP-OOL10-12 5/1/2014 4:08:25PM Page4 of5 Analysis Report for FSS-2014-0273 FSSP-OOL 10-11-010-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/1/2014 4:08:06PM Peak locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351.97 1.24868E-01 12.01 Tol.

M = First peak Jn a mulliplet region

=

m other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Apex\Root\Default\llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCilgrams) (pCl/grams) (pCl!grams)

(keV}

+ K-40 1460.81

10. 67 9.63E+OO 7.65E-01 7, 65E-0,1 Co-60 1173.22 100.00 2.lOE-02 9.33E-02 l.42E-01 1332.49 100.00 -1.15E-01 9.33E-02 Nb-94 ,702. 63 100.00 -1.67E-02 7,91E-02 8.37E-02 871.10 100.00 -1.0BE-01 7.91E-02 Ag-108m 79.20 7.10 -4.23E-01 7.69E-02 l.89E+OO 433.93 89.90 -4.81E-02 7.69E-02 614.37 90.40 -2.68E-01 1.60E-01 722. 95 90.50 -3.39E-03 9.30E-02 Cs-134 569.31 15.43 1.88E-01 1. 03E-01 4.81E-01 604.70 97. 60 -4.76E-02 1.39E-01 795.84 85.40 2.45E-02 1.03E-01 Cs-137 661.65 85.12 2.70E-02 1.09E-01 1.09E-01 Eu-152 121.78 28.40 -l.15E-01 2.36E-01 2.37E-01 244.69 7.49 -2.86E-02 1.03E+OO 344.27 26.50 -1.71E-Ol 2.36E-01 778.89 12.74 -7.57E-02 5.48E-01 867.32 4.16 3.30E-02 2.22E+00 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 142 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/1/2014 4:08:25PM Page5ofS Analysis Report for FSS-2014-0273 FSSP-OOU0-11-010-F Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pCi/grams) (pCi/grams) (pCilgrams)

(keV)

Eu-152 964.01 14.40 4.98E-Ol 2.36E-01 8.88E-01 1085.78 10.00 -4.33E-01 1.09E+OO 1112.02 13,30 -7.25E-01 5.45E-01 1407.95 20.70 l.OlE-01 4.48E-01 Eu-154 123.07 40.50 1.49E-02 l.70E-01 l.70E-01 247.94 6.60 -1.0lE-01 1.04E+OO 723. 30 19.70 -l.56E-02 4.27E-01 873.19 11. 50 -2.57E-02 7.70E-01 996. 32 10.30 2.40E-01 8. 86E-01 1004.76 17.90 3.06E-02 5.42E-01 1274.45 35.50 -7.23E-02 3.33E-01 Eu-155 105. 31 20.70 -8.78E-02 3.38E-01 3.38E-01 Pb-206 803.10 100,00 -6.37E-02 7.61E-02 7.61E-02 Ac-228 338.32 11. 40 4.22E-01 5.89E-01 6.62E-01 911. 07 27.70 7.59E-01 5.89E-01 969 .11 16.60 5.57E-01 8.13E-01 Th-234 63.29 3.80 -3.76E-01 l.82E+OO 4.53E+OO 92.59 5.41 1.04E+OO 1.82E+OO U-235 143.76 10.50 4.03E-02 1.43E-Ol 6.21E-Ol 163.35 4.70 -6,54E-01 l.34E+OO 185.72 54.00 4.31E-02 l.43E-01 205.31 4.70 8.14E-02 1.44E+OO Np-237 311. 98 38.60 -6,60E-03 1.56E-01 l.56E-01 Am-241 59.54 35.90 -2.77E-02 5.80E-Ol 5.80E-Ol

+ = Nuclide Identified during the nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value ls Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 143 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 2:14:14PM Page I of5 f\pex-Gamma Analysis Report for FSS-2014-0274 FSSP-OOL 10-11-011-F GAMMA SPECTRUM ANALYSIS

. Sample ldentlflcal!on : FSS-2014-0274 Sample Description : FSSP-OOU0-11-011-F Sample Type : 1L Soll

.Sample Size : 1.131E+03grams Facility . : Default Sample Taken On : 4/28/2014 9:25:00AM Acquisition Started : 4/29/2014 2:03:48PM Procedure : 1LSollMD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0,01 %

Peak Locate Threshold : 4.00 ,

Peak Locate Range (in channels) : 100-4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2{22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample ~umber

/ . . d~

PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/29/2014 2:13:55PM Peak Analysis From Channel : 100 Peak Analysis To Channel ; 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV}

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 144 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4/29/2014 2:14:14PM Page 2 of5 Analysis Report for FSS-2014-0274 FSSP-OOL 10-11-011-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.63 471 - 483 477.22 1;13E+02 24.36 l.56E+02 1. 50

.F 2 351. 81 697 - 708 703.58 7.58E+Ol 18.64 4.33E+Ol 1. 71 F 3 583.01 1161- 1171 1166.01 5.84E+Ol 16.24 1.94E+Ol 1. 56 F 4 609.36 1212 - 1223 1218.71 6.54E+Ol 16.80 1.76E+Ol 1 :83 F 5 1460. 96 2915 - 2929 2921.74 2.06E+02 29.07 1.50E+Ol 1. 97

=

M First peak in a multiplet region m = Other peak In a multiplet region

=

F Fitted single!

Errors quoted al 2.000slgma No background subtract performed on this spectrum.

NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Defaull\Ubrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty_

K-40 0.99 1460.81

10.67 1. 30E+Ol 1.97E+OO Tl-208 0.69 277.35 6.80 583.14

84.20 2.18E-01 6.18E-02 860.37 12.46 Pb-212 0,89 238.63

44.60 3.87E-01 8.65E-02 300.09 3.41 Bi-214 0.48 609.31

46,30 4.59E-01 l.21E-01 1120.29 15.10 1764.49 15.80 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 145 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 2:14:14PM Pnge 3 of5 Analysis Report for FSS-2014-0274 FSSP-OOL 10-11-011-F

= Energy line found in the speclrum.

- = Manually added nucllde.

? = Manually ediled nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0,40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.997 1.30E+Ol 1.97E+OO Tl-208 0.693 2.18E-01 6.lBE-02 Pb-212 0.895 3.87E-01 8.65E-02 Bi-214 0. 486 4.59E-01 l.21E-01

? nuclide is part of an undetermined solution X nuclide rejected. by the interference analysis

@ . nuclide contains energy lines no! use<;! in Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 146 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/29/2014 2:14:14PM Page 4 of 5 Analysis Report for FSS-2014-0274 FSSP-OOL 10-11-011-F

.UNIDENTIFIED PEAKS Peak Locate Performed on : 4/29/2014 2:13:55PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide E' 2 351.81 l.26351E-01 12.30 Tol. ~-

lf/4- i(-ZN1 M= First peak in a mulUplet region m = Other peak in a multiplet region F =fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Library\HBPP .NLB Nuclide Energy Yield(%) Activity Nuclide MDA UneMDA Name (pCi/grams) (pCl/grams) (pCi/grams)

(keV)

+ K-40 1460.81

10,67 1. 30E+Ol 1.14E+OO l.14E+OO Co-60 1173.22 100.00 5.37E-02 l.22E-01 1.44E-Ol 1332.49 100.00 4.30E-02 1.22E-01 Nb-94 702.63 100.00 3.20E-02 9.35E-02 9.35E-02 871.10 100.00 9.95E-03 9.86E-02 Ag-108m 79.20 7.10 4.28E-01 '8.46E-02 1.70E+OO 433.93 89.90 -l.43E-02 8.46E-02 614.37 90.40 -1.86E-01 l,64E-01 722. 95 90.50 2.28E-02 1. lOE-01 Cs-134 569.31 15.43 3.30E-01 1.48E-01 5,95E-01 604.70 97.60 -5.64E-02 1.48E-01 795.84 85.40 4.42E-02 1.48E-01 Cs-137 661.65 85.12 1.33E-01 1. 42E-01 l.42E-01 Eu-152 121.78 28.40 -1.09E-02 2.40E-01 2.43E-01 244.69 7.49 -1.84E-01 1. 09E+OO 344.27 26. 50 -4.14E-01 2, 40E-01 778.89 12.74 -3.19E-01 6. 51E-01 867.32 4.16 -2.82E+OO 2.18E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 147 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4/29/2014 2:14:14PM Page 5 of5 Analysis Report for FSS-2014-0274 FSSP-OOL 10-11-011-F Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name (pC/lgrams) (pCilgrams) (pCilgrams)

(keV)

Eu-152 964.01 14.40 8.07E-01 2.40E-01 1.06E+OO 1085.78 10.00 -2.30E-01 1.24E+OO 1112.02 13.30 -9.96E-Ol 8.17E-01 1407.95 20.70 -1.46E-01 4.76E-01 Eu-154 123.07 40.50 -l.08E-Ol l.70E-01 l.70E-01 247.94 6.60 -1.44E+00 1.02E+OO 723. 30 19.70 1.05B-01 5.b4E-01 873,19 11. 50 1.66E-01 8.39E-01 996.32 10.30 5. 96E-01 1. 31E+OO 1004.76 17.90 3.92E-01 6. 51E-01 1274.45 35.50 4.26E-03 4.18E-01 Eu-155 105.31 20.70 2.56E-02 3.13E-01 3.13E-01 Pb-206 803.10 100.00 5.22E-02 1.12E-01 1.12E-01 Ac-228 338.32 11. 40 4.02E-Ol 6.13E-01 7.87E-Ol 911.07 27.70 6. 4.9E-Ol 6.13E-01 969.11 16.60 1.60E-01 9.41E-01

rh-234 63.29 3.80 -8.0SE-01 1.74E+OO 3.99E+OO 92.59 5.41 -2.13E-01 1. 74E+OO U-235 143.76 10.50 -1.0lE-01 1.42E-Ol 6.47E-Ol 163.35 4.70 -1.40E-01 l.34E+OO 185. 72 54.00 9.43E-02 l.42E-01 205.31 4.70 -5.27E-01 1.43E+OO Np-237 311. 98 38.60 -4.64E-02 1.61E-01 1.61E-01 Am-241 59.54 35.90 -1.48E-01 4.67E-01 4.67E-01

+ = Nuclide identified during the nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correclion 7 CAUTION: MDA value is inconsistent with Currie MDA at 95~ confidence level FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 148 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12

-~Apex-Gamma Analysis Report for FSS-2014-0275 5/9/2014 12:49:28PM Page I of5

(

FSSP-OOL10-11-012-F GAMMA SPECTRUM ANAL YS/S Sample Identification : FSS-2014-0275 Sample Description : FSSP-OOL 10-11-012-F Sample Type : 1L Soil Sample Size : 1.256E+03 grams Facility : Default Sample Taken On : 4/28/2014 10:30:00AM Acquisition Started : 4/29/2014 12:48:41PM Procedure : 1L Soil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelll MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locale Range (in channels) : 100 -4096 Peak Area Range (In channels) : 100 - 4096 ldentlflcallon Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibratlon Description : 1L Marinelli MD Sample Number : 1672

?.#~ t-1-rr PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/9/2014 12:49:09PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy RD/ ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 149 of 468

Atl?.C:hrnent 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/9/2014 12:49:28PM Page 2 of5 Analysis Report for FSS-2014-0275 FSSP-OOL 10-11-012-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.52 148 - 157 153.03 1.01E+02 23.22 1.63E+02 2.56 F 2 238.52 471 - 483 477.00 1. 34E+02 25.52 1.31E+02 1.37 F 3 351.81 698 - 709 703.58 7.62E+01 19.88 7.93E+Ol 1. 61 F 4 583.26 1161 - 1172 1166.52 5.18E+Ol 15.80 3.44E+01 1.39 F 5 609.29 1214 - 1225 1218.58 5.69E+Ol 16.73 3.60E+Ol 1. 62 F 6 1460.84 2914 - 2928 2921.50 1.57E+02 25.42 1. 50E+Ol 2.05 M =First peak in a multiplet region m =Other peak In a mul!lplet region F = Filled singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum ..

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Ubrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty Bi-xRay 0.50 77.11

100.00 1. 59E-01 3.86E-02 87.20 36.00 K-40 1. 00 1460.81

10.67 8.93E+OO 1.53E+OO Tl-208 0.69 277. 35 6.80 583.14

84.20 1.74E-01 5,40E-02 pJ):..:.2i2" ..

8§9 .:n 12 .. 46 0.89 238. 63

44.60 4.13E-01 8.24E-02 300,09 3.41 Bi-214 0.48 609,31

46.30 3.60E-01 l.08E-01 1120.29 15.10 1764.49 15.80 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 150 of 468 FSS Report

Attachment 3 Lab Data for..~BPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12

.5/9/2014 12:49:28PM Page 3 of5 Analysis Report for FSS-2014-0275 FSSP-OOL10-11-012-F

= Energy line found In the spectrum.

-= Manually added nuclide.

? = Manually edlled nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold= 0.40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

Bi-xRay 0.508 1.59E-01 3.86E-02 K-40 1.000 8.93E+OO 1.53E+OO Tl-208 0,693 1.74E-01 5.40E-02 Pb-212 0.893 4.13E-01 8.24E-02

Bi-214 0.486 3.60E-01 l.08E-01

? nuclide Is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000s!gma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 151 of 468 FSS Report

Attachment 3 Lab Data for HBPP-F$.§P-OOL 10-11 & HBPP-FSSP-OOL10-12 5/9/2014 12:49:2BPM Page 4 of5 Analysis Report for FSS-2014-0275 FSSP-OOL 10-11-012-F UNIDENTIFIED PEAKS Peak Locale Performed on : 5/9/2014 12:49:09PM Peak Locale From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak* Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type N_y_c;Jlde__ _

F 3 351.81 1.27024E-01 13.04 Tol.

=

M First peak in a multiple! region m = Other peak in a mulflpJel region F = Filled sJngle!

Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Llbrary Used : C:\Canberra\Apex\Root\Defaull\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCJ/grams) (pCI/grams) (pCi/grams)

(keV)

+ K-40 1460.81

10.67 8.93E+00 1. 03E+OO 1.03E+OO Co-60 1173.22 100.00 -3.lOE-02 6.79E-02 1.37E-01 1332.49 100.00 -l.OOE-01 6.79E-02 Nb-94 702.63 100.00 -4.65E-03 8.lOE-02 8.lOE-02 871.10 100.00 -3. 41E-02 9.31E-02 Ag-108m 79.20 7.10 -7.17E-01 6.60E-02 1.58E+OO 433.93 89.90 -6.31E-02 6.60E-02 614.37 90.40 -2.76E-02 1.48E-01 722. 95 90.50 1. 04E-02 l.12E-Ol Cs-134 569.31 15.43 3.19E-01 9.16E-02 5.97E-01 604.70 97.60 -5.73E-02 1.29E-01

.795,.94 .. 85*;40* 1 .18E~02 * . ***9 .T6E.::02 Cs-137 661.65 85.12 9. 40E-02 1. 25E-01 l.25E-Ol Eu-152 121.78 28.40 -1.47E-01 2.13E-01 2 .13E-01 244.69 7.49 -3.38E-01 8.64E-01 344.27 26.50 -3.28E-01 2.45E-01 778.89 12.74 -6.64E-01 6.65E-01 867.32 4.16 -8.73E-01 2.18E+OO HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 152 of 468 FSS Report

Attachment 3 L;:!b Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/9/2014 12:49:28PM Page 5 of5 Analysis Report for FSS-2014-0275 FSSP*OOL 10-11-012-F Nucllde Energy Yield{%) Activity Nuc/ideMDA LlneMDA Name (pC//grams) (pC//grams) (pCl/grams)

(keV)

Eu-152 964.01 14.40 8,75E-01 2 .13E-Ol 1.07E+OO 1085.78 10.00 -1.26E+OO 9.59E-01 1112. 02 13.30 -6.96E-01 7.58E-Ol 1407.95 20.70 1.26E-01 5.37E-01 Eu-154 123.07 40.50 -7.37E-02 1. 51E-Ol 1.51E-01 247.94 6,60 -5.34E-01 9.23E-Ol 723. 30 19.70 4.79E-02 5.13E-Ol 873.19 11. 50 -l.13E-01 8.80E-01 996.32 10.30 -2.96E-01 8.lOE-01 1004,76 17.90 4.17E-01 5.87E-01 1274.45 35,50 -5.72E-02 3.69E-01 Eu-155 105.31 20.70 l.02E-02 2.94E-01 2.94E-01 Pb-206 803.10 100.00 -5. llE-02 7.20E-02 7.20E-02 Ac-228 338.32 11.40 5.19E-01 4.77E-01 7.24E-01 911. 07 27.70 3.65E-01 4.77E-01 969 .11 16.60 7.17E-01 9.29E-01 Th-234 63.29 3.80 2.27E+OO 1.48E+OO 3.83E+OO 92 .59 5.41 -1. 05E-Ol l.48E+OO U-235 143.76 10.50 -3.28E-01 1. 21E-01 5.80E-01 163.35 4.70 9.86E-01 1.29E+OO 185. 72 54.00 3.74E-02 1. 21E-01 205.31 4.70 l,08E-02 1.37E+OO Np-237 311. 98 38.60 3.59E-02 l.54E-01 1.54E-01 Am-241 59.54 35.90 -1.69E-01 4.50E-01 4.50E-01

+ = Nuclide Identified during the nuclide Identification

= Energy line found in the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value Is inconsistent with Currie MDA at 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 153 of 468 FSS Report

Attachment 3 Lab Data for HBPP-F~~P~Q0~10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:11 :54PM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0276 FSSP-OOL 10-11-013-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0276 Sample Description : FSSP-OOL 10-11-013-F Sample Type : 1LSoi)

Sample Size : 1.366E+03 grams Facllity : Default Sample Taken On : 4/29/2014 9:40:00AM Acquisition Started : 4/30/2014 5:01:29PM Procedure : 1L Soil HD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli HD Live Time : 600.0 seconds ReaiTime : 600.1 seconds Dead Time : 0,01 %

_peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 -4096 Peak Area Range (In channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli HD

1601 S"-/-1'!

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 4/30/2014 5:11 :36PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 154 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11. & l:JBPP:F.SSP-OOL 10-12 4/30/2014 5:11:54PM Page 2 of5 Analysis Report for FSS-2014-0276 FSSP-OOL 10-11-013-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV} start end Centroid Area Uncertainty Counts (keV)

F 1 77. 07 148- 159 1511.13 6.112E+Ol 21. 41 2.22E+02 1. 05 F 2 238.52 471 - 1183 1177.00 1. 2 9E+02 26.011 l.77E+02 1. 05 F 3 351.87 699 - 710 703.70 8,65E+Ol 19.89 ll.98E+Ol 1. 53 F 4 583.28 1160 - 1171 1166. 54 5.14E+Ol 16.06 4.03E+Ol 1. 50 F 5 609.52 1213 - 1223 1219.03 4.64E+Ol 15.54 3.85E+Ol 1.42 F 6 1460. 72 2913 - 2928 2921.27 l.70E+02 26. 05 3.90E+OO 2.22 M " First peak in a multiplet region m " Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pC/!grams) Uncertainty Bi-xRay 0.54 77 .11

100.00 l.18E-01 4.02E-02 87.20 36.00 K-40 0.99 1460.81

10.67 9.46E+OO l.54E+OO Tl-208 0.69 277.35 6.80 583.14

84.20 l.70E-01 5.40E-02 860.37 12.46 Pb-212 0.89 238.63

44.60 3.99E-01 8.39E-02 300.09 3.41 Bi-214 0.48 609.31

46.30 2.89E-Ol 9.83E-02 1120.29 15.10 1764.49 15.80 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 155 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:11 :54PM Page 3 of5 Analysis Report for FSS-2014-0276 FSSP-OOL 10-11-013-F

=Energy line found In the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line no! used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted al 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

Bi-xRay 0.543 l.lBE-01 4.02E-02 K-40 0.999 9. 46E+OO l.54E+00 Tl-208 0.694 l.70E-01 S.40E-02 Pb-212 0.893 3.99E-01 8.39E-02 Bi-214 0.481 2.89E-01 9. 83E ? nuclide Is part of an undetermined solulion X - nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted al 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 156 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:11 :54PM Page 4 of5 Analysis Report for FSS-2014-0276 FSSP-OOL 10-11-013-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 5:11:36PM Peak Locate From Channel : 100 Peak Locate To Channel ; 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide

_,...----~

F 3 351. 87 l.44096E-01 11. 50 Tol.

~

1<<4- S'- ?-/'(

=

M First peak in a multiplet region m = Other peak Jn a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA Line MDA Name (pCl!grams) (pCl/grams) (pCi!grams)

(keV)

+ K-40 1460.81

10.67 9.46E+OO S.93E-01 S.93E-01 Co-60 1173 .22 100. 00 -9.16E-03 9.65E-02 l.34E-01 1332.49 100.00 3.52E-02 9.65E-02 Nb-94 702.63 100.00 -2.83E-02 7.81E-02 7.SlE-02 871.10 100.00 -3.llE-02 8.52E-02 Ag-108m 79.20 7.10 -4.33E-01 6.73E-02 l.81E+OO 433.93 89.90 2.75E-02 6.73E-02 614.37 90.40 -5.41E-02 1.42E-01 722.95 90.50 3.56E-02 1.lOE-01 Cs-134 569.31 15.43 3.19E-01 9.72E-02 5.94E-01 604.70 97.60 6.19E-03 1. 24E-01 795.84 85.40 -4.lOE-02 9.72E-02 Cs-137 661. 65 85.12 8.48E-02 1.05E-01 1. 05E-01 Eu-152 121. 78 28.40 1.27E-01 2.22E-01 2.37E-01 244.69 7.49 -1.82E-02 9.70E-01 344.27 26.50 -2.47E-01 2.22E-01 778.89 12.74 1.13E-01 8.07E-01 867.32 4.16 l.38E+OO 2.38E+OO FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 157 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPf'-FSSP-OOL 10-12 4/30/2014 5:11:54PM Page 5 of5 Analysis Report for FSS-2014-0276 FSSP-OOL 10-11-013-F Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCi!grams) (pGf/grams} (pCl/grams}

(keV)

Eu-152 964.01 14.40 9.SOE-02 2.22E-01 8.42E-01 1085.78 10.00 -3.19E-01 l.08E+OO 1112.02 13.30 -6.75E-01 8.26E-01 1407.95 20.70 2.27E-02 4.44E-01 Eu-154 123.07 40.50 -1. 28E-02 1.64E-01 l.64E-01 247.94 6.60 -1.12E+OO 8.51E-01 723.30 19.70 l.64E-01 5,04E-01 873.19 11. 50 -2.55E-02 7.62E-01 996.32 10.30 -5.llE-01 9.02E-Ol 1004.76 17.90 -7.68E-02 5.08E-01 1274.45 35.50 -5.08E-02 3.03E-Ol Eu-155 105.31 20.70 2.25E-02 3.llE-01 3. llE-01 Pb-206 803.10 100.00 -1.15E-02 8.55E-02 8.55E-02 Ac-228 338.32 11. 40 l.91E-Ol 4.53E-01 6.34E-01 911. 07 27.70 3.61E-01 4.53E-01 969 .11 16.60 3.48E-01 7.45E-01 Th-234 63.29 3.80 4.62E-01 1. 72E+OO 4.55E+00 92.59 5.41 l.24E+OO 1. 72E+OO U-235 143.76 10.50 4. 61E-Ol 1. 28E-01 6.76E-01 163.35 4.70 -2.lOE-01 1.22E+OO 185. 72 54.00 1.04E-01 1. 28E-01 205.31 4.70 9.65E-01 l.43E+OO Np-237 311.98 38.60 4.59E-03 l.49E-01 l.49E-01 Am-241 59.54 35.90 -9.20E-02 5 ,'4lE-01 5.41E-01

+ = Nuclide identified during Iha nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Haff-life loo short lo be able lo perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA al 95% confidence level FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 158 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12

~Apex-Gamma Analysis Report for FSS-2014-0277 4/30/2014 5:26:58PM Page I of5 FSSP-OOL 10-11-014-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0277 Sample Description : FSSP-OOL 10-11-014-F Sample Type : 1L Soll Sample Size : 1.118E+03 grams Facility : Default Sample Taken On : 4/29/2014 10:05:00AM Acquisition Started : 4/30/2014 5:16:31 PM Procedure : 1LSoil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels} : 100 -4096 Peak Area Range (In channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Number

,t?- ~( ,

PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/30/2014 5:26:38PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 159 of 468

Attac;hrnE!nt} L?~ PC!ta for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4/30/2014 5:26:5BPM Page 2 of5 Analysis Report for FSS-2014-0277 FSSP-OOL 10-11-014-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.57 471 - 483 4 77. 09 1.30E+02 25.33 1.47E+02 1.59 F 2 351. 81 697 - 708 703.59 8.07E+Ol 19.94 7.25E+Ol 1.35 F 3 609.39 1215 - 1224 1218. 77 5. 45E+Ol 17.13 4.20E+Ol 1.67 F 4 14(i0.85 2916 - 2928 2921.52 2.09E+02 29,30 6.50E+OO 2.17 M = First peak In a multiple! region m = other peak In a multiplet region F =Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Dafault\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1. 00 1460.81

10. 67 l.34E+Ol 2.0lE+OO Pb-212 0.89 238.63

44.60 4.50E-01 9.17E-02 300.09 3.41 Bi-214 0. 48 609.31

46. 30 3.88E-01 l.24E-01 1120. 29 15.10 1764.49 15.80

=Energy line found In the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 160 of 468

Attachment 3 Lab Data f9r HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:26:58PM Page 3 of5 Analysis Report for FSS-2014-0277 FSSP*OOL 10-11-014-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCJ/grams)

K-40 1. 000 1.34E+Ol 2.0lE+OO Pb-212 0.895 4.SOE-01 9.17E-02 Bi-214 0.486 3.88E-01 1.24E-01

? nuclide Is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy !Ines not used In Weighted Mean Activity Errors quoted at 2,000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 161 of468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:26:58PM Page 4 of 5 Analysis Report for FSS-2014-0277 FSSP-OOL 10-11-014-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 5:26:3BPM Peak Locate From Channel : 100 Peak Locate*To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) , Peak Size (CPS) Uncertainty Type Nuclide F 2 351.81 1.34575E-01 12.35 Tol.

M = First peak in a multiple! region

=

m Other peak In a multiplet region

=

F Fllfed singlet Errors quoted al 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\H8PP.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pC//grams) (pCi!grams) (pCJ!grams)

(keV)

+ K-40 1460.81

10.67 1. 34E+Ol 7.94E-01 7.94E-Ol Co-60 1173.22 100.00 -1.85E-02 1. llE-01 1.40E-01 1332.49 100.00 1.75E-02 1. llE-01 Nb-94 702.63 100.00 3.69E-02 8.37E-02 1. OBE-01 871.10 100.00 3.92E-02 8.37E-02 Ag-108rn 79.20 7.10 -3.25E-01 8.66E-02 1.76E+00 433.93 89.90 2.02E-02 B.66E-02 614.37 90.40 -2,98E-02 1.73E-01 722.95 90,50 -5.83E-02 1.27E-01 Cs-134 569.31 15.43 2.35E-01 l.16E-01 6.85E-01 604.70 97.60 -1.64E-01 1.48E-01 795.84 85.40 2.64E-02 1.16E-01 Cs-137 661.65 85.12 1.06E-01 1.42E-Ol l.42E-01 Eu-152 121.78 28.40 9.57E-02 2.SOE-01 2.50E-01 244.69 7.49 -7.28E-01 l.12E+OO 344.27 26.50 -3.75E-01 2.65E-01 778.89 12.74 -3,57E-01 7.47E-01 867,32 4.16 -5.59E-01 2.07E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 162 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:26:58PM Page 5 of5 Analysis Report for FSS-2014-0277 FSSP-OOL 10-11-014-F Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCl!grams) (pCl/grams) (pCilgrams)

(keV)

Eu-152 964.01 14.40 8.07E-Ol 2.50E-01 9.76E-01 1085,78 10.00 5.49E-01 1.49E+OO 1112.02 13.30 *-5. 03E-Ol 8.99E-01 1407.95 20.70 1.60E-Ol 6.25E-01 Eu-154 123.07 40.50 -_2. 4 6E-01 l.65E-01 l,65E-01 247.94 6.60 -6.lBE-01 1.12E+OO 723.30 19.70 -2.68E-01 5.84E-01 873.19 11. 50 -1.lOE-01 7.03E-01 996.32 10.30 -1.14E+OO 9.73E-Ol 1004.76 17.90 2.61E-Ol 7-. 41E-01 1274.45 35,50 6.44E-02 4.79E-01 Eu-155 105.31 20,70 -1.66E-01 3.46E-Ol 3.46E-01 Pb-206 803.10 100.00 -3,16E-02 9.54E-02 9.54E-02 Ac-228 338.32 11. 40 2.17E-01 6.lSE-01 7,34E-01 911. 07 27.70 3.29E-Ol 6.15E-01 969 .11 16.60 9.0lE-01 9.09E-Ol

rh-234 63.29 3.80 -2.32E-01 1.82E+OO 4.23E+OO 92.59 5.41 7.70E-03 l.82E+OO U-235 143.76- 10.50 1. 86E-01 1.42E-01 7.15E-01 163.35 4.70 8.03E-01 l.54E+OO 185. 72 54.00 4.29E-02 1.42E-01 205.31 4,70 4.12E-01 1.53E+OO Np-237 311. 98 38.60 -1.55E-02 1. 78E-01 1.78E-Ol Am-241 59.54 35.90 -3.37E-Ol 5.04E-01 5.04E-Ol

+ = Nuclide Identified during the nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA al 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 163 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 413012014 5:41:59PM PBge I of5 Apex-Gamma Analysis Report for FSS-2014-0278 FSSP-OOL10-11-015-F GAMMA SPECTRUM ANALYSIS Sampfe !denlificalion : FSS-2014-0278 Sample Description : FSSP-OOL 10-11-015-F Sample Type : 1LSoli Sample Size : 1.262E+03 grams Facility : Default Sample Taken On : 412812014 8:20:30PM Acqulslllon Started : 4130/2014 5:31:33PM Procedure : 1L Soil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (Jn channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV "Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used. Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Number

£n !}~

PEAK ANAL YSJS REPORT Peak Analysis Performed on : 4/3012014 5:41:39PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 164 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12

\.

4/30/2014 5:41:59PM Page 2 of5 Analysis Report for FSS-2014-0278 FSSP-OOL 10-11-015-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.52 472 - 481 476.99 l.22E+02 27.21 1.86E+02 1. 20 F 2 351.84 697 - 709 703.63 7.49E+Ol 18.49 4.77E+Ol 1. 59 F 3 609.37 1212 - 1224 1218.74 6.0lE+Ol 16. 45 2.27E+Ol 1. 57 F 4 1460.83 2915 - 2928 2921. 48 1.84E+02 27.21 3.23E+OO 2.12

=

M First peak In a mul\iplet region

=

m Olher peak In a mulliplet region F :: Filled singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1. 00 1460.81

10. 67 1.05E+01 1.65E+OO Pb-212 0.89 238.63

44.60 3.75E-01 8.64E-02 300.09 3.41 Bi-214 0.48 609.31

46.30 3.79E-01 1.06E-01 1120. 29 15.10 1764.49 15.80

= Energy line found in the speclrum.

- =Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold= 0.40 Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 165 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:41 :59PM Page 3 of5 Analysis Report for FSS-2014-0278 FSSP-OOL 10-11-015-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 1. 000 1.0SE+Ol 1.65E+OO Pb-212 0.893 3.75E-01 8.64E-02 Bi-214 0.486 3.79E-01 1.06E-01

? nuclide is part or an undelermlned solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 166 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-09L 10-12 4/30/2014 5:41:59PM Page 4 of5 Analysis Report for FSS-2014-0278 FSSP-OOL 10-11-015-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 5:41:39PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (ke V) Peak Size (CPS) Uncertainty Type Nuclide F 2 351.84 1.24824E-01 12.34 Tol.

~~=-~

Ml- s~?~I'{

=

M First peak in a multiplet region

=

m Olher peak In a multlplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Ubrary\HBPP.NLB Nucl/de Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCl/grams) (pCl/grams) (pCi/grams)

(keV)

+ K-40 1460.81

10.67 1.0SE+Ol 5.39E-01 5.39E-01 Co-60 1173.22 100.00 -1. 41E-02 9.38E-02 1.29E-Ol 1332.49 100.00 -4.78E-02 9,38E-02 Nb-94 702.63 100.00 1.86E-02 8.38E-02 8.38E-02 871. 10 100.00 4.24E-02 8.62E-02 Ag-108m 79.20 7.10 7.44E-Ol 6.24E-02 1.60E+OO 433.93 89.90 2.45E-02 6.24E-02 614.37 90.40 -4.54E-02 l.38E-Ol 722. 95 90.50 2.80E-02 1.08E-Dl Cs-134 569.31 15.43 7.22E-Ol i.OlE-01 6.77E-01 604.70 97.60 4.30E-03 1.33E-Ol 795.84 85.40 -7.87E-03 1. OlE-01 Cs-137 661.65 85.12 7.35E-02 l.22E-01 1. 22E-01 Eu-152 121.78 28.40 3.19E-03 2.20E-01 2.20E-01 244.69 7.49 -l.73E-01 9.93E-01 344.27 26.50 -3.SOE-01 2.33E-Ol 778. 89 12.74 3.29E-02 7.31E-01 867.32 4.16 -2.0lE+OO 1.84E+OO FSS Report 'HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 167 of 468

Attachment 3 Lab Data for HBPP-FSSf'-OOL 10-11 & HBPP-FSSP-OOL10-12

_)

4/30/2014 5:41:59PM Page 5 ofS Analysis Report for FSS-2014-0278 FSSP-OOL 10-11-015-F Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCl!grams) (pCi/grams) (pCl!grams)

(keV)

Eu-152 964.01 14.40 8.79E-01 2.20E-01 9.79E-01 1085,78 10.00 2.97E-02 1.06E+OO 1112. 02 13.30 -8.46E-01 7.76E-01 1407.95 20.70 -9.24E-02 3.41E-Ol Eu-154 123. 07 40.50 2.82E-02 l.57E-01 l.57E-01 247.94 6.60 -9.67E-01 9.53E-01 723. 30 19.70 1. 29E-01 4.97E-01 873.19 11. 50 -2.63E-Ol 6.91E-01 996. 32 10.30 -5.03E-01 8.35E-01 1004.76 17.90 -4.02E-02 5.44E-01 1274.45 35.50 4.16E-02 3.34E-Ol Eu-155 105.31 20.70 -l.21E-01 3.05E-01 3.0SE-01 Pb-206 803.10 100.00 -2.02E-02 8.65E-02 8.65E-02 Ac-228 338.32 11. 40 4.68E-01 4.91E-01 7.25E-Ol 911. 07 27.70 4.12E-Ol 4,91E-01 969.11 16. 60 6.66E-Ol 8.0SE-01 Th-234 63 .29 3.80 1.68E+OO l.53E+OO 3.82E+OO 92.59 5.41 2.43E-01 l.53E+OO U-235 143.76 10.50 2 .16E-Ol 1. 23E-01 5.82E-01 163.35 4.70 5.53E-01 l.32E+OO 185. 72 54.00 4.61E-02 -l.23E-01 205.31 4.70 3.67E-Ol 1.41E+OO Np-237 311.98 38.60 -6,47E-02 1.52E-01 1.52E-01 Am-241 59.54 35.90 -2.18E-01 4.45E-01 4.45E-01

+ = Nuclide identified during the nuclide identification

= Energy line found in the spectrum

> MDA value not calculated

@ HalF-life too short to be able to perform !he decay correction

? CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 168 of 468

Attachment 3 Lab Data for HBPf"~FS_SP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/1/2014 4:23:26PM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0279 FSSP-OOL 10-11-016-F-S GAMMA SPECTRUM ANAL YS/S Sample Identification : FSS-2014-0279 Sample Description : FSSP-OOL10-11-016-F-S Sample Type : 1L Soll Sample Size : 1.020E+03 grams Facility : Default Sample Taken On : 4/29/2014 9:30:00AM Acquisition Started : 5/1/2014 4:13:01PM Procedure : 1L Soil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : om%

Peak Locate Threshold : 4.QO Peak Locale Range (In channels) : 100. 4096 Peak Area Range (In channels) : 100. 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Callbralfon Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Number : 1613

,L ~ s-1-1y PEAK ANAL YS/S REPORT Peak Analysis Performed on : 5/1/2014 4:23:07PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM.

No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 169 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/1/2014 4:23:26PM Page 2 of5 Analysis Report for FSS-2014-0279 FSSP-OOL 10-11-016-F-S Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 77.17 152 - 159 154.32 4.46E+Ol 29.93 l.74E+02 0.67 F 2 238.25 470 - 482 476.46 l.01E+02 23.70 1.63E+02 1. 48 F 3 351.78 696 - 709 703.53 9.08E+Ol 18.93 2.36E+Ol 1.77 F 4 1460.75 2915 - 2927 2921.32 1.33E+02 23.37 6.63E+OO 1. 97 M = First peak in a multiple! region

=

m Other peak In a multiplet region

=

F Filled singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C;\Canberra\Apex\Root\Default\Library\HBPP.NLB IDENTIFIED NUCLIDES Nuc:/lde Id Energy Yield(%} Ac:tivlty Activity Name Confidenc:e (keV} (pCi!grams) Unc:ertalnty Bi-x:Ray 0.54 77 .11

100.00 8.55E-02 5.77E-02 87.20 36.00 K-40 0.99 1460.81

10.67 9.33E+OO l.72E+OO Pb-212 0.87 238.63

44. 60 3.82E-01 9.28E-02 300.09 3.41

=Energy line found In the spectrum.

- = Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 170 of 468

Attachment 3 Lab _Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/1/2014 4:23:26PM Page 3 of5 Analysis Report for FSS-2014-0279 FSSP-OOL 10-11-016-F-S INTERFERENCE CORRECTED REPORT Nuclide Nuclfde Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

Bi-xRay 0.548 8.SSE-02 5.77E-02 K-40 0.999 9.33E+OO 1. 72E+OO Pb-212 0.874 3.82E-01 9.28E-02

? nuclide is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used In Welghted Mean Activity Errors quoted al 2.000sigma HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 171 of 468 FSS Report

Attachment 3 Lab Data fo_r HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/1/2014 4:23:26PM Page 4 of5 Analysis Report for FSS-2014-0279 FSSP-OOL 10-11-016-F-S UNIDENTIFIED PEAKS Peak Locate Performed on' : 5/1/2014 4:23:07PM Peak Locate From Channel : 100 Peak Locate,To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No_ Energy (keV) Peak Size {CPS} Uncertainty Type Nuclide F 3 351.78 1.51355E-01 10.42 Tol.

=

M First peak in a multiplet region m = Other peak In a multlptef region

=

F Fitted single!

Errors quoted al 2,000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

+ K-40 1460.81

10. 67 9.33E+OO 8.SOE-01 8.80E-Ol Co-60 1173.22 100.00 8.24E-02 l.OSE-01 l.63E-01 1332.49 100.00 4.97E-04 1.05E-01 Nb-94 702.63 100.00 6.17E-02 9.SOE-02 9.77E-02 871.10 100.00 -7.48E-02 9.SOE-02 Ag-108m 79.20 7.10 8.58E-01 9.lSE-02 1.85E+OO 433.93 89.90 8.47E-02 9.lSE-02 614.37 90.40 9.94E-02 1. 44E-01 722. 95 90.50 5.23E-04 1.13E-01 Cs-134 569.31 15.43 2.0lE-01 1. 22E-01 6.87E-01 604.70 97.60 1. 28E-01 1.43E-01 795.84 85.40 5.07E-02 1. 22E-01 Cs-137 661.65 85.12 6.24E-02 l.24E-01 l.24E-01 Eu-152 121.78 28. 40 3.74E-03 2.43E-01 2.43E-01 244.69 7. 49 -5.15E-02 1. 06E+OO 344.27 26. 50 -3.72E-01 2.67E-01 778.89 12.74 1.13E-01 8.54E-01 867.32 4.16 -2.04E-01 2.56E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 172 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/1/2014 4:23:26PM Page 5 of5 Analysis Report for FSS-2014-0279 FSSP-OOL 10-11-016-F-S Nuc/fde Energy Yield(%) Activity Nuc/ideMDA LfneMDA Name (pCi!grams) (pCl!grams) (pCl/grams)

(keV)

Eu-152 964.01 14.40 8.92E-01 2.43E-01 1. lOE+OO 1085.78 10.00 -8.99E-01 1.14E+OO 1112. 02 13.30 -8.73E-01 9.06E-01 1407.95 20.70 2.46E-01 5.28E-01 Eu-154 123.07 40.50 -5.12E-02 1.69E-01 l.69E-01 247.94 6.60 -2.23E+OO 9.84E-01 723.30 19.70 2.41E-03 5.19E-01 873.19 11. 50 -4.82E-02 8. 81E-01 996. 32 10.30 1.73E-01 l.03E+OO 1004.76 17.90 -1.88E-02 6.90E-01 1274.45 35.50 1.28E-01 3.80E-01 Eu-155 105.31 20.70 1.92E-01 3.55E-01 3.55E-01 Pb-206 803.10 100.00 -7.23E-02 I

1.14E-01 1.14E-01 Ac-228 338.32 11. 40 9.07E-01 5.07E-01 8.05E-01 911.07 27.70 l.30E-01 5. 07E-01~,

969 .11 16.60 7.87E-01 9.96E-01 Th-234 63.29 3.80 4.56E-01 1.79E+OO 3.86E+OO 92.59 5. 41 1.03E+OO 1. 79E+OO U-235 143.76 10.50 5.24E-02 l.35E-01 6.68E-01 163.35 4.70 -6.87E-01 l.45E+OO 185. 72 54.00 5,98E-02 l.35E-01 205.31 4.70 -4.26E-01 1.59E+OO Np-237 311. 98 38.60 -2.15E:._02 1.61E-01 l.61E-Ol Am-241 59.54 35.90 2. 43E-01 5.14E-01 5.14E-01

+ = Nuclide Identified during the nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-fife too short lo be able to perform the decay correction

? CAUTION: MDAvalue Is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 173 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:57:01PM Pagel of5

~pex-Gamma Analysis Report for FSS-2014-0280 FSSP-OOL 10-11-017-F GAMMA SPECTRUM ANAL YS/S Sample ldenlification : FSS-2014-0280 Sample Description , : FSSP-OOL10-11-017-F Sample Type : 1LSoil Sample Size : 1.195E+03 grams Facility : Default Sample Taken On : 4/29/2014 11:00:00AM Acquisition Started : 4/30/2014 5:46:35PM Procedure : 1LSoil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4,00 Peak Locate Range (in channels) : 100 -4096 Peak Area Range (In channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD d : 1604 /12/ /J ----

Sample Number

& Ld&<<d -~-1-1r ,,w/d~

r PEAK ANAL YS/S REPORT Peak Analysis Performed on : 4/30/2014 5:56:42PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 174 of 468

Attachment 3..Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:57:01PM Page 2 of5 Analysis Report for FSS-2014-0280 FSSP-OOL10-11-017-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.52 470 - 483 477.00 l.16E+02 24.99 l.81E+02 1. 43 F 2 338.08 673 - 679 676.11 3.17E+Ol 13.65 3.31E+Ol 1.12 F 3 351.70 699 - 709 703.35 7.92E+Ol 19.56 5.65E+Ol 1. 33 F 4 609.27 1213 - 1223 1218.53 5.81E+Ol 17.09 3.81E+Ol 1. 64 F 5 1460.85 2914 - 2928 2921. 53 l.96E+02 28.24 l.12E+Ol 2.18

=

M First peak In a mulliplet region

=

m Other peak in a mulllplel region

=

F Fitted singlet Errors quoted at 2.000sigrna No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Roo!\Default\Library\HBPP .NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1. 00 1460,81

10.67 1.18E+Ol l.81E+OO Pb-212 0.89 238.63

44.60 3.75E-01 8. 40E-02 300.09 3.41 Bi-214 0.48 609.31

46.30 3.87E-01 l.16E-01 1120.29 15.10 1764.49 15.80 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 175 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 5:57:01PM Page 3 of5 Analysis Report for FSS-2014-0280 FSSP-OOL10-11-017-F

= Energy line found in_ the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Acllvlly Energy Tolerance : 1.000 keV Nuclide confidence index threshold= 0.40 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl!grams)

K-40 1 :000 1.18E+Ol 1.81E+OO Pb-212 0.893 3.75E-01 8.40E-02 Bi-214 0.486 3.87E-01 l.16E-01

? nuclide is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 176 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4/30/2014 5:57:01PM Page 4 of5 Analysis Report for FSS-2014-0280 FSSP-OOL 10-11-017-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 5:56:42PM Peak Locate From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%} Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 338.08 5.28347E-02 21.53 Tol. c&_:~28')

F 3 351.70 l.31994E-01 12.35 Tol. ('lib~~

~ >-'!-/'(

=

M Firs! peak In a multiplet region

=

m Olher peak in a multiplet region F = Filled singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canbarra\Apax\Root\Defaull\Llbrary\HBPP.NLB NucJlde Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCJ/grams) (pCilgrams) (pCl/grams)

(keV)

+ K-40 1460.81

10.67 l.18E+Ol 9.56E-01 9.56E-01 Co-60 1173.22 100.00 -6.27E-02 9.43E-02 1. 04E-01 1332.49 100.00 -l.62E-02 9.43E-02 Nb-94 702.63 100.00 O.OOE+OO 8.87E-02 9.93E-02 871.10 100.00 -l!.41E-02 8.87E-02 Ag-108rn 79.20 7.10 3.67E-01 7.39E-02 1.64E+OO 433.93 89.90 -7.27E-02 7.39E-02 614.37 90.40 -9.29E-02 1.59E-01 722. 95 90.50 6.78E-02 1. 20E-01 Cs-131! 569.31 15.43 l.45E-01 l.19E-01 6.47E-01 604.70 97.60 -9. llE-03 1. 41E-01 795.84 85.40 6.lOE-02 1.19E-01 Cs-137 661.65 85.12 4.45E-02 1.25E-01 l.25E-01 Eu-152 121.78 28. 40 -6. 14E-02 2.14E-Ol 2.14E-01 244.69 7.49 1.75E-04 1.02E+OO 344.27 26' 50 -9.40E-02 2.41E-01 778.89 12.74 3,65E-01 7. 72E-01 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 177 .of 468

Attachment 3 Lab Da.ta.for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 4/30/2014 5:57:01PM Page 5 of5 Analysis Report for FSS-2014-0280 FSSP-OOL 10-11-017-F Nuclide Energy Yield(%) Activity Nuc/JdeMDA LineMDA Name (pC//grams) (pCl/grams) (pCl/grams)

(keV)

Eu-152 8 67. 32 4.16 -2.60E-01 2.14E-01 2.39E+OO 964. 01 14.40 6.56E-01 1.03E+OO 1085.78 10.00 -3.88E-01 9.09E-01 1112.02 13.30 -2.02E+00 l.02E+00 1407.95 20.70 1.05E-01 5.23E-01 Eu-154 123.07 40.50 2.23E-02 1.SlE-01 l.51E-01 247.94 6.60 -2.05E+OO 9.0lE-01 723.30 19.70 3.12E-01 5.53E-01 873.19 11.50 -2.30E-01 7.73E-01 996. 32 10.30 -4.23E-01 l.15E+OO 1004.76 17.90 8.16E-02 6.81E-01 1274.45 35.50 9.88E-02 4.llE-01 Eu-155 105.31 20.70 -l.03E-01 3.18E-01 3.18E-01 Pb-206 803.10 100.00 3.93E-02 1. 06E-Ol l.06E-Ol Ac-228 338.32 11.40 5.91E-01 5.29E-01 7.57E-01 911. 07 27.70 6.02E-01 5.29E-01 969 .11 16. 60 7.62E-01 8,50E-01 Th-234 63.29 3.80 1.70E+OO 1.69E+OO 4.0lE+OO 92.59 5.41 7.38E-01 l.69E+OO U-235 143.76 10.50 4.17E-01 l.33E-Ol 5.99E-01 163.35 4.70 6.46E-01 1. 40E+OO 185. 72 54.00 2.03E-02 l.33E-01 205.31 4.70 -3.18E-01 1.46E+OO Np-237 311. 98 38.60 1. 24E-01 l.77E-01 l.77E-01 Am-241 59.54 35.90 4.45E-02 4.66E-01 4.66E-01

+ = Nuclide identified during the nuclide Identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life loo short to be able lo perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 178 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:12:03PM Page 1 of5

~pex-Gamma Analysis Report for FSS-2014-0281 FSSP-OOL 10-11-018-F GAMMA SPECTRUM ANAL YS/S Sample ldenlificalion : FSS-2014-0281 Sample Description : FSSP-OOL10-11-018-F Sample Type : 1L Soil Sample Size : 1.069E+03 grams Facility : Default Sample Taken On : 4/28/2014 12:00:00PM Acquisition Started : 4/30/2014 6:01:36PM Procedure : 1LSol! MD Operator : Administrator Detector Name : DET06 Geometry ; 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : O.o1 %

Peak Locate Threshold : 4.00 Peak Locale Range (In channels) : 100 - 4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/2212012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Cal!bratlon Description : 1L Marinelli MD Sample Number : 1605 ~

,? l~ud s--1-d 7

~

PEAK ANAL YSJS REPORT Peak Analysis Performed on : 4/30/2014 6:11:43PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 179 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:12:03PM Pngc2 of5 Analysis Report for FSS-2014-0281 FSSP-OOL 10-11-018-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 186.02 367 - 377 372. 00 4.08E+Ol 16.43 1.06E+02 1. 02 F 2 238.61 471 - 480 477.17 1.12E+02 25.22 1.33E+02 1. 39 F 3 351.97 699 - 707 703.90 8.19E+Ol 19.17 3.00E+Ol 1. 41 F 4 609.40 1212 - 1225 1218.80 6.0BE+Ol 15.90 1.61E+Ol 1.67 F 5 1460.91 2915 - 2929 2921.65 l.72E+02 26.26 O.OOE+OO 2.12 M = First peak in a multiplet region m =Other peak in a multlplet region F =Fllted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Library\HBPP.NL8 IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.81

10.67 1.15E+Ol l.87E+OO Pb-212 0.89 238.63

44.60 4.08E-Ol 9.46E-02 300.09 3.41 Bi-214 0.48 609.31

46,30 4.53E-01 1.21E-01 1120. 29 15.10 1764.49 15.80 U-235 0.55 143.76 10.50 163.35 4.70 185. 72

54.00 1.0SE-01 4.26E-02 205.31 4.70 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 180 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 4/30/2014 6:12:03PM Pogc 3 of5 Analysis Report for FSS-2014-0281 FSSP-OOU0-11-018-F

= Energy line found in the spectrum.

- = Manually added nuclide.

=

? Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV

=

Nuclide confidence index threshold 0.40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.998 1.lSE+Ol 1.87E+OO Pb-212 0,895 4.08E-01 9.46E-02 Bi-214 0.486 4.53E-01 1.21E-01 U-235/~,;t.) c,, 0.550 1.0SE-01 4.26E-02

? nuclide ls pari of an undetermined solution X nucl!de rejected by the interference analysis

.@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 181 of468

Attachment 3 Lab .Qata for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:12;03PM Page 4 of 5 Analysis Report for FSS-2014-0281 FSSP-OOL 10-11-018-F UNIDENTJFIED PEAKS Peak Locate Performed on : 4/30/2014 6:11 :43PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS} Uncertainty Type Nuclide F 3 351.97 1.36514E-01 11.70 Tol.

,.et4- 544 WkS*7*1tf 5'. '1,1'(

=

M First peak in a multiplet region m = Other peak in a multiplet region F =Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB Nuclide Energy Yield(%) Activity Nucl/deMDA Lfne MDA Name (pCf/grams) (pCl/grams) (pCilgrams)

(keV)

+ K-40 1460.81

10.67 1.15E+Ol l.81E-Dl 1.81E-01 Co-60 1173.22 100.00 -4.49E-03 1.0SE-01 1.44E-01 1332.49 100.00 -1.39E-02 1.05E-01 Nb-94 702.63 100.00 -2.72E-02 8.04E-02 8.04E-02 871.10 100.00 -6.98E-03, 8.44E-02 Ag-108m 79.20 7.10 -4.lSE-01 9.06E-02 1. 71E+OO 433.93 89.90 -3.18E-02 9.06E-02 614.37 90.40 -1. 06E-02 1.63E-01 722. 95 90.50 5.16E-02 l.18E-01 Cs-134 569.31 15.43 -2.58E-02 l.14E-01 6.94E-01 604.70 97.60 -4.03E-02 1.52E-01 795.84 85.40 2.29E-02 1.14E~Ol Cs-137 661.65 85.12 7.04E-02 1. 42E-01 1.42E-01 Eu-152 121. 78 28.40 -3,34E-02 2.52E-01 2.52E-01 244.69 7.49 -2.41E+OO 1.02E+OO 344.27 26.50 -7.05E-02 2.99E-01 778.89 12.74 -4.06E-01 7.64E-01 867.32 4.16 -9.19E-01 2.37E+OO HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 182 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:12:03PM Page 5 ofS Analysis Report for FSS-2014-0281 FSSP*OOL10-11-018-F Nuclide Energy Yield(%) Activity Nucl/de MDA LineMDA Name (pC//grams) (pCl/grams) (pCl/grams)

(keV)

Eu-152 964.01 14.40 -l.16E-Ol 2.52E-Ol l.04E+OO 1085.78 10.00 9.43E-Ol l.48E+OO 1112.02 13.30 -8.59E-01 l.12E+OO 1407.95 20.70 2.52E-02 5.32E-01 Eu-154 123.07 40.50 8.22E-02 1.80E-01 1.80E-01 247.94 6.60 -1.55E+OO 9.70E-01 723.30 19.70 2.37E-01 5.43E-01 873.19 11. 50 -3,89E-02 7.63E-01 996.32 10.30 l,46E-01 1.22E+OO 1004.76 17.90 3 .- 44E-01 8.0lE-01 1274.45 35.50 2.28E-02 4.24E-Ol Eu-155 105.31 20.70 -9.89E-02 3.36E-01 3,36E-01 Pb-206 803.10 100,00 -7.14E-02 8.74E-02 8.74E-02 Ac-228 338.32 11. 40 4.81E-01 5.54E-01 7.73E-01 911.07 27.70 2.93E-01 5.54E-01 969 .11 16.60 8.53E-Ol 9.51E-01 Th-234 63.29 3.80 8,30E-01 l.79E+OO 4.31E+OO 92.59 5.41 -1. 72E-01 l.79E+OO

+ U-235 143.76 10.50 3.91E-01 1. llE-01 6.53E-01 163.35 4.70 -1. 03E-02 1.55E+OO 185.72

54.00 1.05E-Ol 1. llE-01 205.31 4.70 1.BlE-01 1.56E+OO Np-237 311. 98 38.60 -l.19E-01 1. 71E-01 l.71E-01 Am-241 59.54 35.90 -7.21E-02 5.21E-Ol 5.21E-01

+ = Nuclide identified during the nuclide Identification

= Energy line found ln the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 183 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:27:03PM Page l of5

/\pex-Gamma Analysis Report for FSS-2014-0282 FSSP-OOL 10-11-019-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0282 Sample Description : FSSP-OOL 10-11-019-F Sample Type : 1LSoll Sample Size : 1.107E+03 grams Facility : Default Sample Taken On : 4/28/2014 11:30:00AM Acquisition Started : 4/30/2014 6:16:38PM Procedure : 1L Soil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locale Range (in channels) : 100 -4096 Peak Area Range (In channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Nu'3)er : 1606

~~

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 4/30/2014 6:26:45PM Peak Analysis From Channel : 100 PeakAnalysls To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 184 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:27:03PM Page 2 of 5 Analysis Report for FSS-2014-0282 FSSP-OOL 10-11-019-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.49 471- 481 476.93 9.58E+Ol 24.00 1. 48E+02 1. 34 F 2 1460.84 2914 - 2929 2921. 52 2.02E+02 28.43 4.22E+OO 2.14 M = First peak In a mulfiplet region .

m = other peak in a mulliplel region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 1. 00 1460.81

10.67 l.31E+Ol l.97E+OO Pb-212 0.89 238.63

44.60 3.36E-01 8.63E-02 300.09 3.41

=Energy line found In !he spectrum.

=Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.40 .

Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 185 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:27:03PM Pagc3 of5 Analysis Report for FSS-2014-0282 FSSP-OOL 10-11-019-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 1.000 1.31E+Ol 1.97E+OO Pb-212 0.892 3.36E-01 8.63E-02

? nucllde is part of an undetermined solulion X nucllde rejected by the interference analysis

@ nuclide contains energy lines not used in Weighted Mean Aclivity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 186 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:27:03PM Pagc4 of5 Analysis Report for FSS-2014-0282 FSSP-OOL 10-11-019-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 6;26:45PM Peak Locate From Channel : 100 Peak locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Llbrary\HBPP .NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCilgrams) (pCl/grams) (pCi/grams)

(keV)

+ K-40 1460.81

10.67 1.31E+Ol 7.22E-01 7.22E-01 Co-60 1173.22 100.00 -2.84E-02 7.71E-02 1.23E-01 1332.49 100.00 -8.18E-02 7.71E-02 Nb-94 702.63 100.00 J.47E-02 9.57E-02 l.02E-01 871.10 100.00 5.12E-03 9.57E-02

Ag-lOBm 79.20 7.10 l.40E+00 7.98E-02 1.76E+OO 433.93 89.90 l.87E-02 7.98E-02 614.37 90.40 2.14E-01 l.73E-01 722. 95 90.50 -2.80E-02 l.16E-01 Cs-134 569.31 15.43 -2.73E-01 1.15E-01 5.75E-01 604.70 97. 60 1. 89E-01 l.51E-01 795.84 85.40 7.08E 1.15E-01 Cs-137 661.65 85.12 9.92E-02 l.33E-01 1.33E-01 Eu-152 121.78 28.40 5.28E-02 2.36E-01 2.36E-01 244.69 7.49 -3.05E-01 1.03E+OO 344.27 26.50 -2.20E-01 2.65E-01 778.89 12.74 -2.32E-01 7.55E-01 867.32 4.16 -7.75E-01 2.53E+OO 964.01 14.40 9.95E-01 l.OlE+OO FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 187 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:27:03PM Page 5 of5 Analysis Report for FSS-2014-0282 FSSP-OOL 10-11-019-F Nuclide Energy* Yield(%) Activity Nuc/ldeMDA LineMDA Name {pCl/grams) (pC/lgrams) (pCl!grams)

{keV)

Eu-152 1085.78 10.00 -4.99E-01 2.36E-01 l.12E+OO 1112. 02 13.30 -9.25E-01 1. 02E+OO 1407.95 20.70 -7.83E-02 4.57E-Ol Eu-154 123.07 40.50 -5.38E-03 l.71E-01 l.71E-01 247.94 6.60 -l.32E+OO 9.66E-01 723. 30 19.70 -l.29E-01 5,33E-01 873.19 11. 50 -3.15E-01 7.63E-01 996. 32 10.30 4.08E-Ol l.lOE+OO 1004.76 17.90 -2,41E-02 5.87E-Ol 1274.45 35,50 2.12E-02 3.61E-01 Eu-155 105.31 20.70 -2.48E-02 3.18E-01 3.18E-01 Pb-206 803.10 100.00 -7.63E-02 8.94E-02 8.94E-02 Ac-228 338.32 11. 40 5.llE-01 5.02E-01 7.00E-01 911. 07 27.70 2.47E-Ol 5.02E-01 969 .11 16.60 7.13E-Ol 8. 71E-Ol Th-234. 63.29 3.80 2.02E+OO l.68E+OO 4.24E+OO 92.59 5.41 -3.03E-01 l.68E+OO U-235 143.76 10.50 -3.64E-02 l.41E-01 6.56E-01 163,35 4.70 2.22E-01 l.43E+OO 185.72 54.00 1. 44E-01 1. 41E-01 205.31 4.70 -7.0lE-01 l.47E+OO Np-237 311. 98 38.60 l.28E-02 l.77E-01 l.77E-01 Am-241 59.54 35.90 -8.99E-02 5.llE-01 5. llE-01

+ Nuclide identified during !he nuclide Identification

" Energy line found in the spectrum

> MDA value not calculated

@ Half-life too short lo be able to perform the decay correction

? CAUTION: MDA value is inconsistent wilh Currie MDA at 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 188 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 413012014 3:41:47PM Pagel of5

~=~pex-Gamma Analysis Report for FSS-2014-0283 FSSP-OOL 10-11-020-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0283 Sample Description : FSSP-OOL10-11-020-F Sample Type * : 1L Soil Sample Size : 1.110E+03grams Facility : Default Sample Taken On : 4128/2014 11:05:00AM Acquislllon Started : 4/30/2014 3:31:22PM Procedure : 1LSollMD Operator : Administrator Detector Name : DET06 Geomelry : 1L Marinelli MD UveTime : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locale Threshold : 4.00 Peak Locale Range (In channels) : 100 -4096 Peak Area Range (In channels) : 100. 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2122/2012 Efficiency Calibration Used Done On : 4/2712011 Efficiency Callbratlon Description : 1L Marinelli MD

1595 /,/' *----..

s-1-1y :Jl;At~ s--2-1r PEAK ANALYSIS REPORT Peak Analysis Performed on : 4/30/2014 3:41:29PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 189 of 468

Attachment 3 Lab Dat<,i.for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 4/30/2014 3:41:47PM Page 2 of5 Analysis Report for FSS-2014-0283 FSSP-OOL 10-11-020-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.49 473 - 482 476.93 1.52E+02 27.85 1.44E+02 1. 43 F 2 295.24 586 - 595 590.43 4.52E+Ol 16.13 6.92E+Ol 1. 00 F 3 351. 72 697 - 709 703.40 8.44E+Ol 19. 71 5.65E+Ol 1. 50 F 4 609.56 1213 - 1226 1219 .11 5,90E+Ol 16.15 2.56E+Ol 1. 72 F 5 1461.02 2916 - 2929 2921. 87 1.64E+02 26.11 l.69E+Ol 2.03

=

M First peak in a mullipfet region m"' Other peak In a multiplet region F = Filled singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty K-40 0.99 1460 .81

10. 67 1.06E+Ol l.78E+OO Pb-212 0.89 238.63

44.60 5.33E-01 1.02E-01 300.09 3.41 Bi-214 0.48 609.31

46.30 4.23E-01 1.18E-01 1120.29 15.10 1764.49 15.80 Pb-214 0.78 241. 98 7.49 295.21

19.20 4.30E-01 l.55E-01 351.92

37.20 4.77E-01 l.14E-01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 190 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 3:41 :47PM Pnge 3 of5 Analysis Report for FSS-2014-0283 FSSP-OOL10-11-020-F

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV

=

Nuclide confidence index threshold 0.40 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.993 1.06E+Ol 1.78E+OO Pb-212 0.892 5.33E-01 1.02E-01 Bi-214 0.480 4.23E-01 1.18E-01 Pb-214 0,788 4.61E-01 9.20E-02

? nuclide is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 191 of46S

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 3:41 :47PM Page 4 of 5 Analysis Report for FSS-2014-0283 FSSP-OOL 10-11-020-F UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 3:41:29PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size {CPS) Uncertainty Type Nuclide All peaks were idenfified.

M = First peak in a multiplet region m = Other peak In a multiplet region F = Fitted singlet Errors quoted al 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Llbrary\HBPP .NLB Nuclide Energy Yield(%) Activity Nuc/ldeMDA LlneMDA Name (pCJ!gra.ms) (pCi/gra.ms) (pCi/grams)

(keV)

+ K-40 1460.81

10.67 1.06E+Ol l.20E+OO 1.20E+OO Co-60 1173.22 100.00 -5.32E-03 l.25E-01 1.44E-01 1332.49 100.00 -9.60E-03 1.25E-01 Nb-94 702.63 100.00 -5.84E-03 8.79E-02 8.79E-02 871.10 100.00 -1.34E-02 1.lOE-01 Ag-108m 79.20 7.10 7,79E-01 7.84E-02 1.85E+OO 433.93 89.90 -1.32E-02 7.84E-02 614.37 90.40 1.93E-02 l.62E-01 722. 95 90.50 3.22E-02 l.16E-01 Cs-134 569.31 15.43 -1. 50E-02 l.15E-01 6.39E-01 604.70 97.60 -2.53E-02 1.45E-01 795.84 85.40 5.83E-02 l.15E-01 Cs-137 661.65 85.12 5.63E-03 l .14E-01 1.14E-01 Eu-152 121.78 28. 40 1. 42E-01 2.37E-01 2.37E-01 244.69 7.49 -3.73E-01 1.lOE+OO 344.27 26.50 -3.19E-01 2.73E-01 778.89 12.74 -2.JOE-01 7.36E-01 867.32 4.16 -7.63E-01 2.63E+OO 964.01 14.40 6.61E-01 9.84E-01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 192 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 3:41:47PM Page 5 of5 Analysis Report for FSS-2014-0283 .

FSSP-OOL 10-11-020-F Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name' {pCilgrams) (pCi/grams) (pCilgrams)

(keV)

Eu-152 1085.78 10.00 3,08E-01 2.37E-01 l.50E+OO 1112. 02 13.30 -l.77E-Ol 8.82E-Ol 1407.95 20.70 -2.31E-03 4.85E-01 Eu-154 123.07 40.50 -8.06E-02 l.61E-01 1.61E-01 247.94 6.60 -1.27E+OO 1.04E+OO 723.30 19.70 l.48E-01 5.32E-01 873.19 11. 50 3.89E-Ol 9.77E-01 996.32 10.30 5.58E-Ol l.20E+OO 1004.76 17.90 -2.40E-01 7.59E-01 1274.45 35.50 1.85E-02 3.70E-01 Eu-155 105.31 20.70 -l.78E-01 3.39E-01 3.39E-01 Pb-206 803.10 100.00 -1.09E-Ol 7.87E-02 7 :87E-02 Ac-228 338.32 11.40 -2.28E-02 6.04E-01 6.87E-Ol 911. 07 27.70 7.00E-01 6.04E-01 969 .11 16.60 4.99E-01 8.45E-01 Th-234 63. 29 3.80 3.53E+OO 1.71E+OO 4.47E+OO 92.59 5.41 2. 72E-01 1. 71E+OO U-235 143.76 10.50 -3.12E-01 l.44E-01 6.43E-01 163.35 4.70 l.27E+OO 1.51E+OO 185. 72 54,00 1.59E-01 1.44E-01 205,31 4.70 -1.20E-01 l.54E+OO Np-237 311.98 38.60 -7.49E-02 l.42E-01 1.42E-01 Am-241 59.54 35.90 -3.50E-01 4.98E-01 4.98E-Ol

+ = Nuclide identified during the nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 193 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:42:03PM Page 1 of5 Apex-Gamma Analysis Report for FSS-2014-0283rc FSSP-OOL 10-11-020-F-RC GAMMA SPECTRUM ANAL YS/S Sample ldentificallon : FSS-2014-0283rc Sample Description : FSSP-OOL10-11-020-F-RC Sample Type : 1LSoil Sample Size : 1.110E+03 grams Facility : Default Sample Taken On : 4/28/2014 11:05:00AM Acquisition Started : 4/30/2014 6:31:39PM Procedure : 1LSoil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.00 %

Peak Locate Threshold : 4.00 Peak Locale Range (in channels) : 100 - 4096 Peak Area Range (in channels} : 100. 4096 Identification Energy Tolerance : 1.000 keV Energy Callbralion Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Number . : 1607

f~ ,~-t s-1-1'1 7

S-* I? -If PEAK ANALYSIS REPORT P~ak Analysis Performed on : 4/30/2014 6:41:46PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 194 of 468

Attac;hment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:42:03PM Page 2 of5 Analysis Report for FSS-2014-0283rc FSSP-OOL 10-11-020-F-RC Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV)

start end Centroid Area Uncertainty Counts (keV)

F 1 77.05 152 - 159 154.09 2.31E+Ol 13.15 8.64E+Ol 0.69 F 2 238.59 473 - 481 4 77. 14 4.04E+Ol 16.18 7.90E+Ol 0.98 F 3 1460.68 2916 - 2927 2921. 20 7.32E+Ol 17.34 2.60E+OO 2.05 M = First peak In a multiple! region

=

m Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence {keV) (pCilgrams) Uncertainty Bi-xRay 0.54 77 .11

100,00 4.09E-02 2.34E-02 87.20 36.00 K-40 0.99 1460.81

10.67 4.73E+OO l.15E+00 Pb-212 0.89 238,63

44.60 1.41E-01 5.72E-02 300.09 3.41

= Energy line found in the speclrum.

- = Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Acllvlty Energy Tolerance: 1.000 keV Nuclide confidence index threshold= 0.40 Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 195 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:42:03PM Page 3 of5 Analysis Report for FSS-2014-0283rc FSSP-OOL 10-11-020-F-RC INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pC//grams)

Bi-xRay 0.548 4.09E-02 2.34E-02 K-40 0.997 4.73E+OO 1.15E+OO Pb-212 0.895 1.41E-01 5. 72E-02

? nuclide is part of an undetermined solulion X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 196 of 468 FSS Report

Attachment 3 Lab Data for HB.PP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 4/30/2014 6:42:03PM Page 4 of5 Analysls Report for FSS-2014-0283rc FSSP-OOL 10-11*020*F-RC UNIDENTIFIED PEAKS Peak Locate Performed on : 4/30/2014 6:41:46PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

M = First peak In a multiplet region

=

m Other peak In a mulUplet region F = Filled singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP .NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pC//grams) (pCi!grams)

(keV)

+ K-40 1460.81

10.67 4.73E+OO 5.45E-01 5.45E-01 Co-60 1173.22 100.00 -3.89E-02 8.65E-02 8.65E-02 1332.49 100.00 2.58E-02 l.02E-01 Nb-94 702.63 100.00 8.57E-03 7.04E-02 7.04E-02 871.10 100.00 2.13E-02 8.13E-02 Ag-108m 79.20 7.10 -4.75E-02 5.59E-02 l.16E+OO 433.93 89.90 -7.79E-02 5.59E-02 614.37 90.40 7.95E-02 l.09E-01 722.95 90.50 l.79E-02 9.73E-02 Cs-134 569.31 15.43 -6.79E-03 8.12E-02 4.22E-01 604.70 97.60 7.28E-02 9. 96E-02 795.84 85.40 -2.88E-02 8.12E-02 Cs-137 661. 65 85.12 l.83E-02 8.90E-02 8.90E-02 Eu-152 121. 78 28.40 l.78E-02 l.78E-01 l.78E-01 244.69 7.49 -2.56E-01 7.34E-01 344.27 26. 50 -2.55E-01 2.20E-01 778.89 12.74 2.83E-Ol 6.03E-01 867.32 4.16 l.40E+OO 2.09E+OO 964.01 14.40 8.75E-01 9.26E-01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 197 of 468

Attachment 3 Lab Data for HBPP-FSSP~_()OL 10-11 & HBPP-FSSP-OOL10-12 4130/2014 6:42:03PM Page 5 of5 Analysis Report for FSS-2014-0283rc FSSP-OOL 10-11-020-F-RC Nuclide Energy Yield{%) Activity Nuc/ldeMDA LineMDA Name (pCl/grams) (pCi/grams) (pCl/grams)

(keV)

Eu-152 1085.78 10.00 -1.21E-01 1.78E-Ol 9.79E-Ol 1112.02 13.30 -1.41E-01 8.82E-Ol 1407.95 20.70 2.26E-01 4.85E-01 Eu-154 123.07 40.50 -5.73E-03 l.25E-01 l.25E-01 247.94 6.60 -9.44E-02 7.53E-01 723. 30 19.70 8.22E-02 4.47E-01 873.19 11,50 -9.31E-01 5.51E-01 996. 32 10.30 -l.05E-01 B.84E-01 1004.76 17.90 -6.50E-02 4.92E-01 1274.45 35.50 1. 04E-01 2. 45E-01 Eu-155 105.31 20.70 7. llE-02 2.31E-01 2.31E-Ol Pb-206 803.10 100,00 -3.79E-02 6.28E-02 6.28E-02 Ac-228 338.32 11. 40 -2,00E-02 4.12E-01 5.75E-01 911.07 27.70 3.21E:-01 4.12E-01 969 .11 16.60 6.40E-01 7.53E-Ol Th-234 63.29 3.80 -1. 71E-01 1.24E+OO 2.58E+OO 92.59 5.41 5.15E-01 l.24E+OO U-235 143.76 10.50 l.28E-Ol 8.87E-02 4.64E-01 163.35 4.70 2.55E-04 l.llE+OO 185.72 54.00 -1.43E-02 8.87E-02 205.31 4.70 8.74E-01 1.25E+OO Np-237 311. 98 38.60 3.02E-02 1.35E-01 l.35E-01 Am-241 59.54 35.90 -2.83E-01 2.85E-01 2.85E-01

+ = Nuclide Identified during the nuclide identificallon

= Enargy line found in the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 198 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL.19.~.11 & H.BPP-FSSP-OOL10-12 5/8/2014 11:26:06AM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0284 FSSP-OOL 10-12-001-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0284 Sample Description : FSSP-OOL 10-12-001-F Sample Type : 1LSo!I Sample Size : 8.616E+02 grams Facility : Default Sample Taken On : 4/28/2014 9:05:00AM Acquisilion Started : 5/8/2014 11:15:41AM Procedure : 1L Soil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : O.o1 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels} : 100 - 4096 Peak Area Range (In channels} : 100 -4096 ldenlific'lllon Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2122/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 11:25:48AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuc1m FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 199 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11:26:06AM Page 2 of5 Analysis Report for FSS-2014-0284 FSSP-OOL 10-12-001-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 661. 77 1318 - 1329 1323.55 S.90E+Ol 16.18 1.80E+Ol 1. 72 F 2 1460.86 2915 - 2927 2921. 54 8.91E+Ol 19.23 6.45E+OO 1. 82

=

M First peak In a multiplet region m =Other peak in a multiple! region F =Fitted singlet .

Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Defaul!\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1. 00 1460.81

10.67 7.41E+OO 1.65E+OO Cs-137 0,99 661.65

85.12 3.18E-01 8.89E-02

= Energy line found In the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 200 of 468

Attachment 3 Lab Data for_lj_BPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11 :26:06AM Page 3 of5 Analysis Report for FSS-2014-0284 FSSP-OOL 10-12-001-F INTERFERENCE CORRECTED REPORT Nuclide Nuc/lde Wt mean Wt mean Comments Name

Id Activity Activity Confidence Uncertainty (pCJ!grams)

K-40 1.000 7.41E+OO 1.65E+OO v/Cs-137 0.998 3.18E-01 8.89E-02

? nuclide Is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted al 2.000sigma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 201 of 468 FSS Report

Attachmen.! .3. ..Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11 :26:06AM Page 4 of5 Analysis Report for FSS-2014-0284 FSSP-OOL 10-12-001-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 11 :25:48AM Peak locate From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were ldenti!led.

M = Firs! peak in a rnul!lplet region

=

m Other peak In a mulllple! region

=

F Fitted singlet Errors quoted al 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : G:\Canberra\Apex\Root\Defaul!\Llbrary\HBPP.NLB Nuclide Energy Yield{%) Activity Nuc/ideMDA LineMDA Name (pCi/grams) (pCl/grams) (pCl/grams)

(keV)

+ K-40 1460.81

10.67 7.41E+OO l.03E+OO l.03E+OO Co-60 1173.22 100.00 -3.72E-03 1.24E-01 1.50E-01 1332.49 100.00 -l.22E-01 1.24E-Ol Nb-94 702.63 100.00 -1.44E-02 8.39E-02 8.39E-02 871.10 100.00 -1.59E-02 9.62E-02 Ag-108m 79.20 7.10 6.62E-01 8.42E-02 1.66E+OO 433.93 89.90 8.36E-03 8. 42E-02 614.37 90.40 2.00E-02 1. 26E-Ol 722. 95 90,50 6.74E-02 1.49E-01 Cs-134 569.31 15.43 5.88E-01 l.lOE-01 8.09E-01 604.70 97.60 -3.76E-02 1.20E-01 795.84 85.40 2.37E-02 1.lOE-01

+ Cs-137 661.65

85.12 3.18E-Ol 9.88E-02 9.88E-02 Eu-152 121.78 28.40 -2.20E-01 2.34E-01 2.34E-01 244.69 7.49 -2. 47E+OO 1.06E+OO 344.27 26.50 -3.99E-Ol 2.57E-Ol 778.89 12.74 -6.55E-01 8.04E-01 867.32 4.16 1.26E-Ol 2.51E+OO 964.01 14.40 7.19E-01 1.14E+OO FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 202 of 468

Attachment 3 _!:.a.ti.Pata for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11:26:06AM Page 5 of5 Analysis Report for FSS-2014-0284 FSSP-OOL 10-12-001-F Nuclide Energy Yield(%) Activity NuclideMDA UneMDA Name (pCl/grams) (pCl/grams) (pCl!grams)

(keV)

Eu-152 1085.78 10.00 -5.86E-01 2.34E-01 7.49E-01 1112.02 13.30 -5.41E-01 8.0lE-01 1407.95 20.70 2.SOE-01 5.88E-01 Eu-154 123.07 40.50 -3.74E-02 1.70E-01 l.70E-01 247.94 6.60 -l.28E+00 9.96E-01 723.30 19.70 3.lOE-01 6.86E-01 873.19 11. 50 3.78E-02 8.78E-01 996.32 10.30 -2.54E-01 9.44E-01 1004.76 17.90 1.50E-01 5.47E-01 1274.45 35.50 -2.62E-02 3.16E-01 Eu-155 105.31 20.70 -l.26E-01 3.26E-01 3.26E-01 Pb-206 803.10 100.00 -l.02E-01 7.06E-02 7, 0 6E-02 Ac-228 338.32 11. 40 l.27E-01 6.59E-Ol 6.59E-01 911. 07 27.70 7.50E-01 6,79E-01 969 .11 16.60 8.BlE-01 l,OlE+OO Th-234 63.29 3.80 -4.19E-01 . 1. 82E+OO 4 .13E+OO 92.59 5.41 1.04E+OO 1.82E+OO U-235 143.76 10. 50 1.16E-01 1.50E-01 6.96E-01 163.35 4.70 3.88E-Ol 1.41E+OO 185. 72 54.00 l.38E-01 l.50E-01 205.31 I 4,70 -3.56E-01 l.39E+OO I

Np-237 311. 98 38.60 -2.41E-02 1.43E-01 1. 43E-Ol Am-241 59.54 35.90 IJ.75E-02 5.29E-01 5.29E-01

+ "" Nuclide Identified during the nuclide Identification

"" Energy line found in the speclrµm

> MDA value not calculated

@ Half-life too short lo be able to perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 203 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11:41:07AM Page 1 of5

_==E~~pex-Gamma Analysis Report for FSS-2014-0285 FSSP-OOL 10-12-002-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0285 Sample Description : FSSP-OOL 10-12-002-F Sample Type : 1LSoil Sample Size : 9.294E+02 grams Facility : Defaull Sample Taken On : 4/28/2014 9:10:00AM Acqulslllon Started : 5/8/2014 11:30:42AM Procedure : 1L Soll MD Operator : Administrator Detector Name : DE.T06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (In channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibratio.n Description : 1 L Marinelli MD PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 11:40:49AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 204 of 468

Attachment 3 Lab Data for HBPP-F.~~>.P-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11:41:07AM Page 2 of5 Analysis Report for FSS-2014-0285 FSSP-OOL 10-12-002-F Peak Energy ROJ ROJ Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.57 471 - 483 477 .11 l.22E+02 24 .*41 1.25E+02 1. 49 F 2 351 .. 87 699 - 708 703.70 5.40E+Ol 16.27 3.63E+Ol 1.19 F 3 1460.97 2916 - 2929 2921. 78 l,34E+02 23.36 2.93E+OO 2.09

=

M First peak In a mulllplet region m = Other peak in a multiple! region

=

F Filled singlet Errors quoted at 2.000s!gma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty K-40 0.99 1460.81

10. 67 1. 03E+Ol l.89E+OO Pb-212 0,89 238.63

44. 60 5.09E-Ol 1.06E-01 300.09 3.41

= Energy line found in the spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV

=

Nuclide confidence Index threshold 0.40 Errors quoted at 2.000sigma HBPP-FSSP-OOL10:11 & HBPP-FSSP-OOL 10-12 Page 205 of 468 FSS Report

..... ***-*** *-***** _Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11 :41 :07AM Page 3 of5 Analysis Report for FSS-2014-0285 FSSP-OOL 10-12-002-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.996 1.03E+Ol 1.89E+OO Pb-212 0.895 5.09E-01 l.06E-01

? nuclide Is part of an undetermined solution X nuclide rejected by !he Interference analysis

@ nuclide contains energy llnes not used In Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 206 of 468

Attachment 3 Lab Data..for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 11:41:07AM Page 4 of 5 Analysis Report for FSS-2014-0285 FSSP-OOL 10-12-002-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 11 :40:49AM Peak Locale From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351.87 9.00031E-02 15.06 Tol.

M = First peak In a multiplet region

=

m Olher peak In a multiplet region F = Filled singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclfde Library Used : C:\Canberra\Apex\Root\Defaull\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi!grams) (pCl/grams) (pCilgrams)

(keV)

+ K-40 1460.81

10.67 l,03E+Ol 6.93E-01 6.93E-01 Co-60 1173.22 100.00 -5.49E-02 1.08E-01 1.39E-01 1332.49 100.00 -6.51E-02 1. 08E-01 Nb-94 702.63 100.00 4.89E-02 9.32E-02 l.07E-01 871. 10 100.00 -5.96E-02 9.32E-02 Ag-108m 79.20 7.10 -9.28E-01 1.00E-01 l.86E+OO 433.93 89.90 8.00E-02 l.OOE-01 614.37 90.40 2.34E-01 1. 91E-01 722. 95 90.50 3.42E-02 l.40E-01 Cs-134 569.31 15.43 3.49E-01 l.38E-01 7. 96E-01 604.70 97. 60 l.05E-01 1.65E-01 795.84 85.40 4,28E-02 l.38E-01 Cs-137 661.65 85.12 l.62E-01 l,73E-01 1.73E-01 Eu-152 121.78 28.40 -7.35E-02 2.34E-01 2.34E-01 244.69 7.49 -4.82E-Ol 1.24.E+OO 344.27 26.50 -6.SOE-01 3.lOE-01 778.89 12.74 -2.87E-Ol 7.20E-01 867.32 4.16 -9.47E-01 2.33E+OO HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 207 of 468 FSS Report

Attachment 3 Lab Data fo_r ljBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11:41:07AM Pages of5 Analysis Report for FSS-2014-0285 FSSP-OOL 10-12-002-F Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name (pCJ!grams) (pCl/grams) (pC/!grams)

(keV)

Eu-152 964.01 14.40 1.0lE+OO 2.34E-Ol 1.19E+OO 1085.78 10.00 9,03E-02 1.52E+OO 1112. 02 13.30 -B.86E-Ol 6.49E-01 1407.95 20.70 6.96E-02 5.07E-01 Eu-154 123.07 40.50 -5.70E-03 1.69E-Ol 1.69E-01 247.94 6.60 -l.59E+OO 1.20E+OO 723. 30 19.70 l,57E-Ol 6.46E-01 873.19 11. 50 4.41E-Ol 8.79E-01 996.32 10.30 5.24E-Ol 1.31E+OO 1004.76 17.90 3.98E-02 6.80E-01 1274.45 35.50 -l.45E-01 4.18E-01 Eu-155 105.31 20.70 -5.96E-02 3.33E-01 3.33E-01 Pb-206 803.10 100.00 -4.46E-02 l.25E-01 1.25E-Ol Ac-228 338,32 11. 40 8,55E-01 5.48E-01 9.52E-01 911. 07 27.70 5.62E-01 5.48E-01 969 .11 16.60 5,88E-01 1.0lE+OO Th-234 63.29 3.80 2.24E+OO l.90E+OO 4.45E+OO 92.59 5.41 5.91E-01 1.90E+OO U-235 143.76 10.50 -9.29E-02 l.52E-01 6.28E-01 163.35 4.70 -7.85E-01 1.41E+OO 185. 72 54.00 l.38E-Ol l.52E-01 205,31 4.70 -5.14E-01 1.65E+OO Np-237 311.98 38.60 -3.68E-02 1.92E-Ol 1.92E-01 Am-241 59.54 35.90 -5.65E-02 5.28E-01 5.28E-Ol

+ = Nuclide identified during !he nuclide ldentiflcaflon

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short lo be able lo perform the decay correction 7 CAUTION: MDA value ls inconsistent with Currie MDA at 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 208 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11:56:09AM Page 1 of5 1\pex-Gamma Analysis Report for FSS-2014-0286 FSSP-OOL 10-12-003-F GAMMA SPECTRUM ANALYSIS Sample ldentiflcalion : FSS-2014-0286 Sample Description : FSSP-OOU0-12-003-F Sample Type : 1LSoil Sample Size : 1.372E+03 grams Faclllly : Default Sample Taken On : 4/30/2014 1:15:00PM Acquisition Started : 5/8/2014 11:45:43AM Procedure : 1L Soll HD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli HD live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time ; 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 -4096 Peak Area Range (In channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli HD Peak Analysis Performed on : 5/8/2014 11 :55:50AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start *end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 209 of 468

Attachment .3.Lab.Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 11:56:09AM Page 2 of5 Analysis Report for FSS-2014-0286 FSSP-OOL10-12-003-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.47 470 - 483 476.90 l.19E+02 23.87 l.09E+02 1.30 F 2 351.68 697 - 707 703.31 5.51E+Ol 16.45 3.05E+Ol 1. 47 F 3 609.34 1214 - 1225 1218.67 4.66E+Ol 14.97 2.89E+Ol 1. 39 F 4 661.84 1318 - 1330 1323.68 4.82E+Ol 14.95 2.39E+Ol 1. 63 F 5 1460.93 2914 - 2928 2921.69 1.15E+02 21.67 7.56E+OO 2.19

=

M First peak in a mulllplet region

=

m Olher peak In a multiplet region F = Fitted singlet Errors quoted at 2.000slgma No background subtract performed on this speo!rum.

NUCLIDE /DENT/FICA T!ON REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl!grams) Uncertainty K-40 0.99 1460.81

10.67 6.39E+OO l.25E+OO Cs-137 0.99 661.65

85.12 1.74E-01 5.SOE-02 Pb-212 0.89 238.63

44. 60 3.68E-01 7.66E-02 300.09 3.41 Bi-214 0.48 609.31

4 6. 30 2.89E-01 9.44E-02 1120.29 15.10 1764.49 15.80 HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 210 of 468 FSS Report

Attachment 3 Lab Data for HBf'l_F-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/~/2014 11 :56:09AM Page 3 of5 Analysis Report for FSS-2014-0286 FSSP-OOL10-12-003-F

=Energy llne found Jn the spectrum.

=Manually added nuclide,

? =Manually edited nucllde.

@ = Energy Jlne not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold= 0.40 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty

{pCf!grams)

K-40 0.998 6.39E+OO 1. 25E+OO v Cs-137 0.994 1.74E-01 5.SOE-02 Pb-212 0,891 3.68E-01 7.66E-02 Bi-214 0.485 2.89E-01 9.44E-02

? nuclide is part of an undetermined solution X nuclide rejected by the Interference analysts

@ nuclide contains energy Jines not used in Weighted Mean Activity Errors quoted at 2.000sJgma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 211 of 468 FSS Report

Attachment 3 Lab Data.Jar HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/8/2014 11 :56:09AM Page 4 of5 Analysis Report for FSS-2014-0266 FSSP-OOL 10-12-003-F UNIDENTIFIED PEAKS Peak locate Performed on : 5/6/2014 11:55:50AM Peak locale From Channel : 100 Peak locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS} Uncertainty Type Nuclide F 2 351.68 9.18327E-02 14.92 Tol.

=

M First peak in a mulllplet region

=

m Other peak In a mulliplet region

=

F Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Defaull\Library\HBPP.Nl8 Nuclide Energy Yield(%) Activity Nuc/ideMDA Line MDA Name (pCilgrams) (pCilgrams) (pCl/grams)

(keV)

+ K-40 1460.81

10.67 6.39E+OO 7.59E-01 7.59E-01 Co-60 1173.22 100.00 -6. 42E-03 9. 71E-02 9.71E-02 1332. 49 100.00 -2.00E-02 1.08E-Ol Nb-94 702,63 100.00 -2. 48E-02 7.94E-02 7.94E-02 871.10 100.00 4.BlE-02 9.51E-02 Ag-lOBm 79.20 7.10 -2.66E-01 6,59E-02 l.58E+OO 433.93 89.90 2.67E-02 6.59E-02 614.37 90.40 1. 45E-02 1.32E-01 722. 95 90.50 4.89E-02 1.00E-01 Cs-134 569.31 15.43 1.88E-01 9.51E-02 4.43E-01 604.70 97.60 -2.55E-02 1.25E-01 795.84 85,40 -p.12E-03 9.51E-02

+ Cs-137 661.65

85.12 1.74E-01 7.82E-02 7.82E-02 Eu-152 121.78 28.40 -1. 43E-01 1.77E-01 2.12E-01 244.69 7.49 -5.87E-02 9.15E-Ol 344.27 26.50 -2.79E-01 1.77E-01 778.89 12.74 -9.53E-02 5.91E-01 867.32 4.16 -4.32E-01 2.28E+OO HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 212 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 11:56:09AM Page 5 of5 Analysis Report for FSS-2014-0286 FSSP-OOL 10-12-003-F Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pC!lgrams) (pCl/grams) (pC/lgrams)

(keV)

Eu-152 964,01 14.40 3.04E-01 l.77E-Ol 8.39E-01 1085.78 10.00 -l.OlE-01 9.39E-01 1112.02 13.30 -6.47E-01 6.74E-01 1407.95 20.70 l.66E-01 4.42E-01 Eu-154 123.07 40.50 -l.03E-Ol 1.51E-01 1.51E-01 247.94 6.60 -5.84E-Ol 8.54E-01 723. 30 19.70 2.25E-01 4.61E-01 873.19 11. 50 -2.87E-01 7.96E-01 996.32 10.30 -2. 4 6E-01 9.00E-01 1004.76 17.90 -l.65E-01 4.60E-01 1274.45 35.50 -8.40E-02 2.92E-01 Eu-155 105.31 20.70 8.82E-02 3.08E-01 3.08E-01 Pb-206 803.10 100.00 2.88E-03 7.72E-02 7.72E-02 Ac-228 338.32 11.40 3.00E-01 4.88E-01 5,75E-01 911.07 27.70 4.17E-01 4.88E-Ol 969 .11 16.60 7.64E-Ol 7.52E-01 Th-234 63.29 3.80 -4.36E-01 l.52E+OO 4.20E+OO 92.59 5.41 -2.77E-01 l.52E+OO U-235 143.76 10.50 8.09E-02 l.15E-01 5.84E-01 163.35 4.70 1.45E-03 1.28E+OO 185.72 54.00 2.51E-02 1.15E-Ol 205.31 4.70 1.55E+OO 1.44E+OO Np-237 311.98 38.60 3. 91E-03 l.42E-01 1.428-01 Am-241 59.54 35.90 -2.43E-01 4.95E-Ol 4.95E-Ol

+ :: Nuclide idenlifled during the nuclide Identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able lo perform the decay correction 7 CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 213 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:11:11PM Pagel of5

~pex-Gamma Analysis Report for FSS-2014-0287 FSSP-OOL 10-12-004-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0287 Sample Description : FSSP-OOL 10-12-004-F Sample Type : 1LSoil Sample Size : 8.810E+02 grams Facility : Default Sample Taken On : 4/30/2014 1:25:00PM Acquisition Started : 5/8/2014 12:00:44PM Procedure : 1LSoilMD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : O.o1 %

Peak Locate Threshold : 4.00 Peak Locate Range {In channels) : 100 - 4og6 Peak Area Range (In channels) : 100 -4096 Identification Energy Tolerance : 1,000 keV Energy Callbratlon Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marlnelll MD Sample Number

~.2'.;:Ak -;+c(,

PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 12:10:51 PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096

(

Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 214 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 12:11:11PM Page 2 of5 Analysis Report for FSS-2014-0287 FSSP-OOL 10-12-004-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.58 471 - 483 4 77 .11 9.85E+Ol 22.57 1.22E+02 1. 29 F 2 351. 96 699 - 708 703.88 3.70E+Ol 14.23 4.34E+Ol 1. 01 F 3 661.64 1318 - 1329 1323.28 6.17E+Ol 16.54 2.13E+Ol 1. 60 F 4 1460.87 2914 - 2928 2921.57 1.46E+02 24.04 O.OOE+OO 2.27

=

M First peak in a multiplet region

=

m Olher peak in a multiplet region F = Filled singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\library\HBPP.NLB IDENTIFIED NUCLJDES Nuclide Id Energy Yield{%) Activity Activity Name Confidence (keV) (pCl!grams) Uncertainty K-40 0.99 1460.81

10.67 l.19E+Ol 2.06E+OO Cs-137 1. 00 661.65

85.12 3.25E-01 8.89E-02 Pb-212 0.89 238.63

44.60 4.34E-01 1. 03E-01 300.09 3.41

= Energy line found in the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

=

- @ Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000sigma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 215 of 468 FSS Report

Attachment 3 Lab Data for HBPP-F_SSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:11:11PM Page 3 of5 Analysis Report for FSS-2014-0287 FSSP-OOL 10*12-004-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl!grams)

K-40 0.999 1.19E+Ol 2.06E+OO v Cs-137 1. 000 3.25E-01 8.89E-02 Pb-212 0.895 4.34E-01 1. 03E-01

? nuclide is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 216 of 468

Attachment 3 Lab Data for HBPP-f$.SP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 12:11:11PM Page 4 of5 Analysis Report for FSS-2014-0287 FSSP-OOL 10-12-004-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 12:10:51PM Peak Locate From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351. 96 6.17489E-02 19.20 Tol.

M = First peak Jn a mulliplet region m =Other peak in a mulliplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Ubrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuc/ldeMDA Line MDA Name (pC/lgrams) (pCl/grams) (pCilgrams)

(keV)

+ K-40 1460.81

10.67 l.19E+Ol 2.20E-01 2.20E-01 Co-60 1173.22 100.00 l.45E-02 1. 21E-Ol l.32E-01 1332' 49 100.00 2.54E-02 1.21E-01 Nb-94 702.63 100.00 4.45E-02 l.17E-01 l.22E-01 871.10 100.00 2.74E-02 1.17E-Ol Ag-108m 79.20 7.10 1 .14E+OO 1.00E-01 2.0SE+OO 433.93 89.90 -2.28E-02 1.00E-01 614.37 90.40 l.84E-Dl 1. 72E-01 722. 95 90.50 7,45E-02 1. 23E-01 Cs-131J 569.31 15.43 2.81E-01 l.55E-01 6.32E-01 604.70 97.60 l.54E-Ol 1.55E-01 795.84 85.40 7.30E-02 1. 71E-01

+ Cs-137 661.65

85.12 3.25E-01 l.04E-01 1.04E-01 Eu-152 121.78 28.40 -5.79E-02 2.59E-01 2.59E-01 244.69 7.49 -3,73E-01 1.21E+OO 344.27 26.50 -8.81E-02 3.47E-01 778.89 12.74 -3,51E-01 7.03E-01 867.32 4.16 l.05E+OO 2.88E+OO HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 217 of 468 FSS Report

Attach.r:nent -~ ~ab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:11:11PM Page 5 of5 Analysis Report tor FSS-2014-0287 FSSP-OOL 10-12-004-F Nuc/fde Energy Yield(%) Activity Nuc/fdeMDA LineMDA Name (pCi/grams) (pCi/grams) {pCl/grams)

(keV}

Eu-152 964.01 14.40 5.22E-01 2.59E-01 l.19E+OO 1085.78 10.00 -2.75E-02 1.33E+OO 1112.02 13 .30 -1.12E+OO 1.02E+OO 1407.95 20.70 3.05E-01 7.lOE-01 Eu-154 123.07 40.50 4.84E-02 1.89E-01 1. 89E-01 247.94 6.60 -l.55E+OO l.12E+OO 723. 30 19.70 3.43E-01 S.64E-Oi 873.19 11.50 1.89E-01 9.60E-01 996.32 10.30 -1.30E-01 1.31E+OO 1004.76 17. 90 1.25E-01 7.59E-01 1274.45 35.50 7.79E-02 4.41E-01 Eu-155 105.31 20.70 -9.26E-02 3.39E-01 3.39E-01 Pb-206 803.10 100.00 -l.80E-01 1.09E-01 l.09E-Ol Ac-228 338.32 11. 40 6.23E-Ol 5.49E-01 8.24E-01 911. 07 27.70 2.55E-01 5.49E-01 969.11 16.60 5.19E-01 1.05E+OO Th-234 63.29 3.80 -1.21E+OO 1.99E+OO 4.42E+OO 92.59 5.41 3.37E-01 1.99E+OO U-235 143.76 10.50 5.71E-Ol l.54E-01 7.35E-01 163.35 4.70 -3.52E-01 1.51E+OO 185.72 54.00 8.84E-02 1.54E-01 205.31 4.70 4.19E-01 1. 83E+OO Np-237 311. 98 38.60 -1.19E-02 1. 98E-01 1.98E-01 Am-241 59.54 35.90 -2.81E-01 S.43E-01 5.43E-01

+ = Nuclide Identified during Iha nuclide Identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too shorl to be able lo perform the decay correction

? CAUTION: MDA value is Inconsistent wi!h Currie MDA at 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 218 of 468 FSS Report

Atta.c_h.ment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:26:10PM Pnge l of5 Analysis Report for FSS-2014-0288 FSSP-OOL10-12-005-F GAMMA SPECTRUM ANALYSIS Sample lden!ific:atlon : FSS-2014-0288 Sample Description ; FSSP-OOL 10-12-005-F Sample Type : 1L Soll Sample Size : 9.561E+02 grams Facility ; Default Sample Taken On : 4/30/2014 1:30;00PM Acquisition Started : 5/8/2014 12:15:46PM Procedure : 1LSollMD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Liva Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 - 4096 Peak Area Range (in channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibralfon Used Done On : 2122/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 12:25:52PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 219 of 468

Attachment 3 _~ab._9.§Jafor HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 12:26:10PM Page 2 of5 Analysis Report for FSS-2014-0288 FSSP-OOL 10-12-005-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.37 472 - 482 476.70 7.63E+Ol 20.63 1.08E+02 1. 30 F 2 351.91 698 - 709 703.78 4.86E+Ol 14.95 2.76E+Ol 1. 35 F 3 609.49 1214 - 1224 1218.97 5.50E+Ol 15.59 1. 84E+01 1. 50 F 4 1461. 04 2915 - 2929 2921. 90 l.16E+02 21.71 3.45E+OO 2.18 M =First peak In a mufliplet region m = Other peak In a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C;\Canberra\Apex\Rool\Default\Library\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty K-40 0.99 1460.81

10.67 8. 71E+OO 1.69E+OO Pb-212 0.88 238,63

44.60 3.lOE-01 8.56E-02 300.09 3.41 Bi-214 0.48 609.31

46.30 4.57E-01 l.32E-01 1120.29 15.10 1764.49 15.80

=Energy line found In the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide conndence Index threshold = 0.40 Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 220 of 468

Attachment 3 Lab Data for.J:J.13PP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 12:26:10PM Page 3 of5 Analysis Report for FSS-2014-0288 FSSP-OOL 10-12-005-F INTERFERENCE CORRECTED REPORT Nuclide Nuc/lde Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0,992 B.71E+OO l.69E+OO Pb-212 0.885 3.lOE-01 8.56E-02 Bi-214 0.483 4.57E-01 1.32E-01

? nucl!de is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used Jn Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 221 of 468

Attachment 3 Laq_p;;,itcifor HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:26:10PM Page 4 of 5 Analysis Report for FSS-2014-0288 FSSP-OOL 10-12-005-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 12:25:52PM Peak Locate From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS} Uncertainty Type Nuclide F 2 351.91 8.10677E-02 15.37 Tol.

=

M First peak in a multiplet region

=

m Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Ubrary\HBPP.NLB Nuclide Energy Yield(%) Activity NuclideMDA LfneMDA Name (pCl/grams) (pCilgrams) (pCl!grams)

(keV)

+ K-40 1460.81

10.67 8. 71E+OO 7.40E-Ol 7.40E-01 Co-60 1173.22 100.00 7.20E-02 9.76E-02 1.50E-01 1332.49 100.00 3.72E-02 9,76E-02 Nb-94 702.63 100.00 2.39E-02 9.74E-02 9.74E-02 871 .10 100.00 1. 21E-02 9,79E-02 Ag-108m 79.20 7.10 3.82E-01 9.SOE-02 1.76E+OO 433.93 89.90 3.87E-02 9,SOE-02 614.37 90.40 -7.64E-02 l.74E-01 722. 95 90.50 5.43E-02 l.30E-01 Cs-134 569.31 15.43 4.42E-01 l. 37E-01 7.54E-Ol 604.70 97.60 -4.84E-02 l.60E-01 795.84 85.40 6,75E-02 1.37E-01 Cs-137 661.65 85.12 4.57E-02 l. l 9E-01 1.19E-01 Eu-152 121.78 28.40 2 .17E-01 2.51E-01 2.51E-01 244.69 7.49 -5,39E-01 1.03E+OO 344.27 26.50 -1.61E-01 3.04E-01 778.89 12.74 1.77E-01 6.74E-01 867.32 4.16 2.05E-Ol 2.51E+OO 0

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 222 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:26:10PM Page 5 of5 Analysis Report for FSS-2014-0288 FSSP-OOL 10-12*005-F Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pC//grams) (pCi/grams) (pCJ!grams)

(keV)

Eu-152 964. 01 14.40 7.27E-01 2.51E-01 1.00E+OO 1085.78 10.00 6.29E-01 1.30E+OO 1112. 02 13.30 -6.62E-01 8.0lE-01 1407.95 20.70 3,76E-02 2.76E-01 Eu-154 123.07 40.50 -9.0lE-02 1.71E-01 1. 71E-01 247.94 6.60 -1.12E+OO 1.02E+OO 723.30 19.70 2.50E-01 5.98E-01 873.19 11. 50 4.60E-01 9.13E-01 996.32 10.30 -5.42E-01 1.07E+OO 1004.76 17.90 -1.77E-01 6.60E-01 1274.45 35.50 -l.51E-01 3.03E-01 Eu-155 105.31 20.70 -1. 46E-01 3.32E-Ol 3.32E-01 Pb-206 803,10 100.00 -4.35E-02 l.OlE-01 1.0lE-01 Ac-228 338.32 11. 40 4.64E-Ol 5.58E-01 7.72E-01 911. 07 27.70 1.12E-01 5.58E-01 969 .11 16.60 6.86E-01 8.06E-01 Th-234 63.29 3.80 l.OBE+OO 1.63E+OO 4.07E+OO 92.59 5.41 -9,58E-01 1.63E+OO U-235 143.76 10.50 3.69E-01 1.27E-01 6.53E-01 163.35 4.70 -9.83E-01 1.29E+OO 185.72 54.00 7. 4 6E-02 1. 27E-01 205.31 4.70 1.63E-01 l.43E+OO Np-237 311. 98 38.60 7.34E-02 1.87E-01 1. 87E-Ol Am-241 59.54 35.90 -8. 96E-02 4.98E-01 4.98E-01

+ = Nuclide identified during !he nuclide identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 223 of 468

.. A.tt?,chment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/812014 12:41:12PM Pagel ofS Analysis Report for FSS-2014-0289 FSSP-OOL 10-12-006-F GAMMA SPECTRUM ANAL YS/S Sample Identification : FSS-2014-0289 Sample Description : FSSP-OOL10-12-006-F Sample Type : 1L Soil Sample Size : 1.486E+03 grams Facility : Default Sample Taken On : 4/30/2014 1:17:00PM Acquisition Started : 5/8/2014 12:30:47PM Procedure : 1L Soll HD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli HD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (!n channels) : 100 -4096 Peak Area Range (in channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2122/2012 Efficiency Calibration Used Done On : 4127/2011 Efficiency Calibration DescripUon : 1L Marinelli HD Sample Numbe~

~;-

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 518/2014 12:40:54PM Peak Analysls From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 224 of 468

Attachment 3 La9 Data for HBPP-FSSP-OOL10-11 & HBP_P-FSSP-OOL10-12 5/8/2014 12:41:12PM Page 2 of5 Analysis Report for FSS-2014-0289 FSSP-OOL10-12-006-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 338.50 671 - 682 676.95 3.39E+Ol 13.85 5.96E+Ol 1. 02 F 2 351. 87 697 - 709 703. 71 5.66E+Ol 16.75 5.63E+Ol 1. 50 F 3 583.32 1162 - 1171 1166.62 3.09E+Ol 11. 95 l.33E+Ol 1.13 F 4 609,31 1213 - 1224 1218.62 4.85E+Ol 15.10 2.69E+Ol 1. 45 F 5 1461. 06 2915 - 2928 2921.94 1.52E+02 24.65 3.45E+OO 2.43 M :: First peak in a murtrplet region

=

m Other peak In a multiplet region F == Fitted singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB IDENTIFIED NUCLIDES

\

Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty K-40 0.99 1460.81

10' 67 7.78E+OO 1.33E+OO Tl-208 0.69 277.35 6.80 583.14

84.20 9.38E-02 3.67E-02 860.37 12. 46 Bi-214 0.48 609.31

46.30 2.77E-01 8.79E-02 1120. 29 15.10 1764.49 15.80 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 225 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/812014 12:41 :12PM Pagc3 of5 Analysis Report ror FSS-2014-0289 FSSP-OOL10-12-006-F

= Energy Jlne found in the spectrum.

- = Manually added nuclide.

? =Manually edlled nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.990 7,78E+OO l.33E+OO Tl-208 0,692 9.38E-02 3.67E-02 Bi-214 0,485 2.77E-01 8.79E-02

? nuclide is part of an undetermined solution X nucllde rejected by the Interference analysis

@ nuclide contains energy lines not used in Weighted Mean Aclivity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 226 of 468

Attachment 3 Lab Data for HBPP~i:':§.§p-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:41 :12PM Page 4 of5 Analysis Report for FSS-2014-0289 FSSP-OOL 10-12-006-F UNIDENTIFIED PEAKS Peak Locale Performed ori : 5/8/2014 12:40:54PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty N~c~

Type F . 1 338.50 5.64743E-02 20.44 Tol. Ac-228 F 2 351.87 9.42738E-02 14.81 Tol. Pb-2~

-~--

=

M First peak in a multiplet region m "'Other peak in a mul!iplet region

=

F Filled singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apsx\Root\Default\library\HBPP .NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pCl!grams) (pCl/grams) (pCi/grams)

(keV}

+ K-40 1460.81

10.67 7.78E+OO 5.0SE-01 5.0SE-01 Co-60 1173.22 100.00 4.06E-03 9.26E-02 1.06E-01 1332.49 100.00 2.SlE-02 9.26E'--02 Nb-94 702.63 100.00 -3.31E-02 7.02E-02 7.02E-02 871.10 100.00 2.07E-02 7.83E-02 Ag-108m 79.20 7.10 7.37E-Ol 6.37E-02 l.64E+OO 433.93 89.90 -l.57E-02 6.37E-02 614.37 90.40 -7.38E-04 l.21E-01 722. 95 90.50 6.62E-02 9.53E-02 Cs-134 569.31 15.43 1.13E-Ol 9.78E-02 4.47E-01 604.70 97.60 2.15E-02 1.15E-01 795.84 85.40 -8.97E-03 9.78E-02 Cs-137 661.65 85.12 -1.04E-02 8.35E-02 8.35E-02 Eu-152 121. 78 28.40 -5.07E-02 1.99E-01 1.99E-01 244.69 7.49 -1.31E+OO 8.84E-01 344.27 26.50 -5.54E-02 2.0BE-01 778.89 12.71] -3.15E-01 4.98E-01 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 227 of 468 FSS Report

Attachme.!lJ) Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 12:41:12PM Page 5 of5 Analysis Report for FSS-2014-0289 FSSP-OOL 10-12-006-F Nuclide Energy Yield(%) Activity NuclldeMDA Line MDA Name (pCJ/grams) (pC//grams) (pCi/grams)

(keV)

Eu-152 867.32 4.16 -2.21E+OO l.99E-Ol l.67E+OO 964.01 14. 40 6.09E-02 6. 51E-01 1085.78 10.00 3.68E-01 8.93E-01 1112.02 13.30 -l.53E-01 7.04E-01 1407.95 20.70 5.25E-02 3.63E-01 Eu-154 123.07 40.50 -9.48E-02 1. 41E-01 1.41E-01 24 7. 94 6.60 -l,30E+OO 8.llE-01 723.30 19.70 3.05E-01 4.39E-01 873.19 11. 50 3.09E-01 7.18E-01 996. 32 10.30 l.27E-02 7.59E-01 1004 .. 76 17.90 3.05E-02 4.68E-01 1274.45 35.50 3. 46E-02 3.03E-01 Eu-155 105.31 20.70 -7.96E-02 2.91E-01 2.91E-01 Pb-206 803.10 100.00 -3.28E-02 7.85E-02 7,85E-02 Ac-228 338.32 11.40 6.94E-01 4.31E-Ol 6.59E-01 911.07 27.70 4. 96E-01 4.31E-01 969 .11 16.60 3.85E-01 5.54E-01 Th-234 63.29 3.80 -8.82E-01 l.49E+OO 3.81E+OO 92.59 5.41 1.19E+OO 1. 4 9E+OO U-235 143.76 10.50 4.09E-01 1.08E-Ol 5,63E-01 163.35 4.70 -9.56E-02 l.16E+00 185. 72 54.00 l.70E-02 l.08E-01 205.31 4.70 -2.82E-01 l.17E+OO Np-237 311. 98 38.60 -7.22E-02 1.30E-01 l.30E-01 Am-241 59.54 35.90 -9.59E-02 4.59E-Ol 4.59E-Ol

+ = Nuclide identified during the nuclide Identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform Iha decay correction

? CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 228 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:56: 12PM Page 1 of5

~pex-Gamma Analysis Report for FSS-2014-0290 FSSP-OOL 10-12-007-F GAMMA SPECTRUM ANAL YS/S Sample Identification* : FSS-2014-0290 Sample Description : FSSP-OOL 10-12-007-F Sample Type : 1L Soll Sample Size : 5,960E+02 grams Facility : Default Sample Taken On : 4/30/2014 1:50:00PM Acquisition Started : 5/8/2014 12:45:48PM Procedure : 1LSoil LO Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli LO Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.01 %

Peak Locale Threshold : 4.00 Peak locate Range (In channels) : 100- 4096 Peak Area Range (In channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli LO Sample Number

~

~-':=J-.--. a:=:s PEAK ANAL YS/S REPORT Peak Analysis Performed on : 5/8/2014 12:55:54PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 229 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:56:12PM Page 2 of5 Analysis Report for FSS-2014-0290 FSSP-OOL 10-12-007-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.51 472 - 480 476.97 4.60E+Ol 16.68 6.82E+Ol 0.99 F 2 351.97 700 - 709 703.89 3.42E+Ol 12.95 2.28E+Ol 1. 25 F 3 1460;96 2916 - 2928 2921. 75 6.55E+Ol 16.50 2.86E+OO 1. 69

=

M First peak in a mul!iplet region

=

m Other peak In a multlplel region F = Fitted singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.81

10.67 7.36E+OO l.90E+OO Pb-212 0.89 238.63

44.60 2.66E-Ol 9.76E-02 300.09 3.41

= Energy line found in the spectrum.

- =Manually added nucllde.

? =Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000sfgma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 230 of 468

Attachrr.i_ent ~ l.:?..b Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 12:56:12PM Page 3 of5 Analysis Report for FSS-2014-0290 FSSP-OOL 10-12-007-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pC//grams)

K-40 0.996 7.36E+OO 1.90E+OO Pb-212 0.893 2.66E-01 9.76E-02

? nuclide fs part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 231 of 468

Attachment 3 Lab 0..ci~a for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:56;12PM Page 4 of5 Analysis Report for FSS-2014-0290 FSSP-OOL 10-12-007-F UNIDENTIFIED PEAKS Peak Locale Performed on : 5/8/2014 12:55:54PM Peak Locale From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351.97 5.70779E-02 18.91 Tol.

M =First peak In a rnulllplet region m =Other peak In a multiplet region F =Filled singlet Errors quoted at 2.000s!gma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB Nuclide Energy Yield{%) Activity NuclldeMDA LlneMDA Name (pCl/grams) (pCl/grams) {pCi/grams)

(keV)

+ K-40 1460.81

10.67 7.36E+OO 9.98E-01 9.98E-01 Co-60 1173.22 100.00 4.44E-02 1.67E-01 l.74E-01 1332.49 100.00 2. llE-02 l.67E-01 Nb-94 702.63 100.00 -4.36E-04 l.09E-01 1.16E-01 871.10 100 .00 2.02E-02 1.09E-01 Ag-108m 79.20 7.10 1.0lE-01 9.72E-02 l.88E+OO 433.93 89,90 7.03E-02 9, 72E-02 614.37 90.40 4.02E-02 1.SlE-01 722.95 90.50 -2.95E-02 l.21E-01 Cs-134 569' 31 15.43 l.92E-01 l.64E-01 7.99E-01 604.70 97.60 l.13E-01 l.66E-01 795.84 85.40 3.lSE-02 l.64E-01 Cs-137 661.65 85.12 l.24E-Ol 2.24E-01 2.24E-01 Eu-152 121. 78 28.40 -4.48E-03 2.26E-01 2.26E-Ol 244,69 7.49 -5.77E-01 l.18E+00 344.27 26.50 -1.lSE-01 3.21E-01 778.89 12.74 -1.37E-02 7.74E-01 867,32 4.16 -4,61E-02 2.60E+OO HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 232 of 468 FSS Report

A!!9chment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 12:56:12PM Page 5 of5 Analysis Report for FSS-2014-0290 FSSP-OOL 10-12-007-F Nuclide Energy Yield{%) Activity Nuc/ideMDA LlneMDA Name (pCJ/grams) (pCl/grams) (pC//grams)

(keV)

Eu-152 964. 01 14. 40 9.78E-01 2.26E-01 1. 46E+OO 1085.78 10.00 -3.26E-01 1. 22E+OO 1112. 02 13 .30 -9.52E-01 9,38E-01 1407.95 20.70 1. 90E-01 7.93E-01 Eu-154 123.07 40,50 -l.27E-01 1.53E-01 1. 53E-01 247.94 6.60 -1.08E+OO 1.20E+OO 723.30 19.70 -1.36E-01 5.55E-01 873.19 11. so -2.46E-01 9.47E-01 996.32 10.30 -2.36E-02 1.33E+OO 1004.76 17.90 -2.92E-01 5.25E-01 1274.45 35.50 -3.24E-01 3.62E-Ol Eu-155 105.31 20.70 -1.42E-01 3.39E-01 3.39E-01 Pb-206 803.10 100.00 7.68E-03 1.44E-01 l.44E-Ol Ac-228 338.32 11. 40 4.90E-01 5.44E-Ol 9.SOE-01 911.07 27.70 1.09E-01 5.44E-01 969 .11 16.60 7.88E-Ol 1.20E+OO Th-234 63.29 3.80 -5.97E-01 1.85E+OO 4.19E+OO 92.59 5.41 -1.0SE+OO l.85E+OO U-235 143.76 10.50 l.27E-01 1. 51E-01 6.30E-01 163.35 4.70 7.42E-01 l,63E+OO 185. 72 54.00 8.09E-02 l,51E-Ol 205.31 4.70 1. 09E-01 1.69E+OO Np-237 311.98 38.60 -6.46E-02 1.90E-01 1.90E-01 Am-241 59.54 35.90 -5.04E-01 4.93E-Ol 4.93E70l

+ = Nuclide identified during the nuclide Identification

= Energy lfne found In the spectrum

> MDA value not calculated

@ Half-life too short to be able lo perform the decay correction

? CAUTION; MDA value Is inconsistent with Currie MDA at 95% confidence level HBPP-FSSP-OOL10-11 & HBPP"FSSP-OOL 10-12 Page 233 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/9/2014 9:11 :53AM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0290RC FSSP-OOL10-12-007-F-RC GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0290RC Sample Description : FSSP-OOL 10-12-007-F-RC Sample Type : 1L Soll Sample Size : 5.960E+02 grams Facility : Default Sample Taken On : 4/30/2014 1:50:00PM Acquisition Started : 5/8/2014 4:16:12PM Procedure : 1LSolfLD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli LO Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0,01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100- 4096 Peak Area Range (ln channels) : 100- 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marlnelll LD Sample Number lf~--*

PEAK ANALYSIS REPORT Peak Analysls Performed on : 5/9/2014 9:11:35AM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 234 of 468

Attachment 3 Lab Data for .H.§P.P-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/9/2014 9;11:53AM Page 2 of5 Analysis Report for FSS-2014-0290RC FSSP-OOL10-12-007-F-RC Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 1461.05 2917 - 2926 2921.93 5.61E+Ol 15.70 5.lOE+OO 1. 88 M =First peak In a multiplet region m =Other peak In a multiple! region

=

F Filled singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Ubrary\HBPP.NLB IDENTIFIED NUCUDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty K-40 0.99 1460.81

10.67 6.30E+OO 1.80E+OO

= Energy line found In the spectrum.

- =Manually added nuclide.

? = Manually edited nuclide.

@ =Energy line no! used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 235 of 468

Attachment 3 Lab Data for HBPP:F'?SP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/9/2014 9:11:53AM Page 3 of5 Analysis Report for FSS-2014-0290RC FSSP-OOL 10*12-007-F-RC INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

K-40 0.991 6.30E+OO l.80E+OO

? nuclide Is part of an undetermined solution X nuclide rejected by lhe Interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted al 2.000slgma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 236 of 468 FSS Report

Attachment 3 Lab [)9t?__fc:Jr_f:lBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/9/2014 9:11 :53AM Page 4 of5 Analysis Report for FSS-2014-0290RC FSSP-OOL 10-12-007-F*RC UNIDENTIFIED PEAKS Peak locate Performed on : 5/9/2014 9:11:35AM Peak Locale From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were Identified.

=

M Firs! peak in a multiplet region

=

m Other peak in a multiple! region F = Fitted singlet Errors quoted al 2.000slgma NUCLIDE MDA REPORT Nuclide library Used : C:\Canberra\Apex\Rool\Default\library\HBPP.NLB Nuclide Energy Yield(%) Activity NuclideMDA LlneMDA Name {pC//grams) (pCi!grams) (pCilgrams)

{keV)

+ K-40 1460.81 10.67 6.30E+OO 1.20E+OO l.20E+OO Co-60 1173.22 100.00 -4,44E-02 1.67E-Ol 1.95E-01 1332.49 100.00 7.79E-02 1.67E-01 Nb-94 702,63 100.00 2.87E-02 l.28E-01 l,40E-01 871. 10 100.00 4.64E-02 l.28E-01 Ag-108m 79.20 7.10 7.47E-01 1. 08E-01 l.79E+OO 433.93 89.90 4.30E-02 1.0BE-01 614.37 90.40 1. 07E-01 l.69E-01 722. 95 90.50 8.lBE-02 1.66E-01 Cs-134 569.31 15.43 3,83E-01 1. 50E-01 6.31E-01 604.70 97.60 3,37E-02 1. SOE-01 795.84 85.40 1.19E-02 1.SBE-01 Cs-137 661.65 85.12 l.78E-01 2.21E-01 2.21E-01 Eu-152 121. 78 28.40 -1.07E-01 2.47E-01 2.47E-01 244.69 7.49 -2.65E+OO l.lOE+OO 344.27 26.50 -l.95E-01 2.63E-01 778.89 12.74 -2.54E-01 8.71E-01 867.32 4.16 -2.68E+OO 2.93E+OO 964.01 14.40 8.62E-01 1.40E+00 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 237 of 468

Attachment 3 Lab Data for HE?.P.P-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/9/2014 9:11:53AM Page 5 of5 Analysis Report for FSS-2014*0290RC FSSP-OOL 10*12-007-F-RC Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCilgrams) (pCi/grams) (pCl/grams)

(keV}

Eu-152 1085.78 10.00 5,44E-02 2.47E-Ol 1.31E+OO 1112. 02 13.30 -5.40E-01 l.25E+OO 1407.95 20.70 1.12E-Ol 5.22E-01 Eu-154 123.07 40.50 -8.18E-02 1.81E-01 1. 81E-01 247.94 6.60 -8.69E-01 l.12E+OO 723.30 19.70 3.76E-01 7.66E-01 873.19 11. 50 l.85E-01 1.12E+OO 996.32 10.30 8.41E-01 l,46E+OO 1004-. 76 17.90 -4.96E-Ol 7.32E-01 1274.45 35.50 4.22E-01 6.07E-01 Eu-155 105.31 20.70 -l.55E-Ol 3.42E-Ol 3.42E-01 Pb-206 803.10 100.00 -2.56E-04 l.44E-01 1.44E-01 Ac-228 338.32 11. 40 4.59E-01 7.23E-01 8.17E-01 911.07 27.70 4.53E-Ol 7.23E-01 969 .11 16.60 6.48E-Ol l.17E+OO Th-234 63.29 3.80 4.45E-01 2.02E+OO 4. 23E+OO, 92.59 5.41 l.56E+OO 2.02E+OO U-235 143.76 10.50 5,64E-01 l.63E-01 7.22E-01 163.35 4.70 -7.64E-01 ~ 1. 40E+OO 185. 72 54.00 1.35E-Ol 1.63E-01 205.31 4.70 9.44E-02 1.53E+OO Np-237 311.98 38,60 3.08E-02 1.94E-01 1.94E-01 Am-241 59.54 35.90 l,56E-01 5.34E-01 5.34E-01

+ = Nuclide identified during the nuclide Identification

= Energy line found In lhe spectrum

> MDA value not calculated

@ Half-life too short to be able lo perform the decay correction

? CAUTION: MDA value Is inconsistent with Currie MDA al 95% confidence level HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 238 of 468 FSS Report

Attachment 3 Lab Data for HE!J='P-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:11:13PM Pagel of5 Analysis Report for FSS-2014-0291 FSSP-OOL 10-12-008-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0291 Sample Description : FSSP-OOL 10-12-008-F Sample Type : 1L Soll Sample Size : 9,306E+02 grams Facility : Default Sample Taken On : 4/30/2014 2:10:00PM Acquisition Started : 5/8/2014 1:00:49PM Procedure : 1L Soi! MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelll MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0,01 %

Peak Locate Threshold : 4,00 Peak Locate Range (In channels} : 100 - 4096 Peak Area Range (In channels) : 100- 4096 ldentlficatlon Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibralion Used Done On : 4/27/2011 Efficiency Calibration Description : 1 L Marinelli MD Sample Number : 1653

/ *~-=- -:::.:;...(?,,[ y Hd~ 5'-9-1'/

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 5/8/2014 1:10:56PM Peak Analysis From Channel : 100 Peak Analysfs To Channel : 4096 Peak En orgy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 239 of 468

Attachment 3 Lab Data for HBPP-FSSP-OQ~.!.0.~ 11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:11:13PM Page 2 ofS Analysis Report for FSS-2014-0291 FSSP-OOL 10-12-008-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.53 472 - 483 477.02 8.97E+Ol 21.62 l.10E+02 1.18 F 2 609.43 1213 - 1223 1218.85 4.45E+Ol 14.34 1.93E+Ol 1. 40 F 3 661.79 1319 - 1330 1323.57 5.49E+Ol 15.32 l.08E+Ol 1. 69 F 4 1461. 03 2915 - 2927 2921.88 1.17E+02 21.67 O.OOE+OO 1. 89 M =First peak in a mulllplet region m =other peak in a mulllplet region F = Fitted singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE IDENTIFICATION REPORT

Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460,81

10' 67 8.98E+OO 1.74E+OO Cs-137 0,99 661.65

85.12 2.73E-01 7.79E-02 Pb-212 0,89 238.63

44. 60 3.74E-01 9.27E-02 300;09 3.41 Bi-214 o.48 609.31

46.30 3.BOE-01 1.24E-01 1120.29 15.10 1764.49 15.80 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 240 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP_-OOL 10-12 5/8/2014 1 :11 :13PM Page 3 ofS Analysis Report for FSS-2014-0291 FSSP-OOL 10-12-008-F

=Energy line found In the spectrum.

- = Manually added nuclide.

? = Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence Index threshold= 0.40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nucl/de Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pC//grams)

K-40 0.993 8.98E+OO 1.74E+OO

,_.,/ Cs-137 0.997 2.73E-01 7.79E-02 Pb-212 0.894 3.74E-01 9.27E-02 Bi-214 0.485 3.80E-01 1.24E-01

? nuclide Is part of an undetermined solution X nuclide rejected by !he interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12

Page 241 of 468

Attachment 3 Lab Data for HBPf.'~f.~SP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:11 :13PM Page 4 of5 Analysis Report for FSS-2014-0291 FSSP-OOL 10-12-008-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 1:10:56PM Peak Locate From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were Identified, M = Firs! peak in a multiplet region

=

m Other peak In a multiplet region

=

F Fitted singlet

Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LineMDA Name (pC/lgrams) (pCl/grams) (pCi!grams)

(keV)

+ K-40 1460.81

10.67 8.98E+OO 2.08E-01 2.08E-01 Co-60 1173.22 100.00 2.41E-02 l.49E-Ol 1.54E-Ol 1332.49 100.00 l.63E-02 l.49E-01 Nb-94 702.63 100.00 4,68E-02 l_l2E-Ol 1.12E-01 871.10 100.00 2.18E-02 l.28E-01 Ag-l08m 79.20 7.10 1.44E+OO 9.35E-02 1.93E+OO 433.93 89.90 -l.72E-02 9.35E-02 614. 37 90.40 -6.63E-02 1.75E-01 722. 95 90.50 9.76E-02 1.38E-01 Cs-134 569.31 15.43 l.59E-01 1.24E-01 7.28E-01 604.70 97.60 7.38E-04 1.56E-01 795.84 85.40 3.lOE-03 1.24E-01

+ Cs-137 661.65

85.12 2.73E-01 7.30E-02 7.30E-02 Eu-152 121.78 28.40 -2.51E-02 2.53E-01 2.53E-01 244.69 7.49 -2.29E-01 1.lOE+OO 344.27 26.50 -5.91E-Ol 2.66E-01 778.89 12.74 -2.22E-01 8.36E-01 867.32 4. 16 -2.19E+OO 2.80E+OO 964.01 14.40 6.99E-02 1.19E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 242 of 468

Attachment 3 Lab Data f()rr,IB,PP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 1:11:13PM Page 5 ofS Analysis Report for FSS-2014-0291 FSSP-OOL 10-12-008-F Nuclide Energy Yield(%) Activity Nuciide.MDA LlneMDA Name (pCf/grams) (pC!/grams) (pC//grams)

(keV)

Eu-152 1085.78 10.00 l.36E-02 2.53E-01 1.25E+OO 1112. 02 13.30 -8.57E-01 1. 05E+OO 1407.95 20.70 -2.30E-01 5.06E-01 Eu-154 123.07 40.50 -3.07E-02 1.74E-01 1.74E-01 247.94 6.60 -2.03E+OO 9.84E-Ol 723. 30 19.70 4.49E-01 6.35E-01 873.19 11. 50 3.74E-Ol 1.12E+OO 996.32 10.30 5.28E-01 1.31E+OO 1004.76 17.90 -5.92E-01 6.35E-01 1274.45 35.50 9.53E-02 4.42E-01 Eu-155 105.31 20.70 4,26E-02 3.79E-01 3,79E-01 Pb-206 803.10 100.00 -3.78E-02 1. 09E-01 l.09E-01 Ac-228 338.32 11. 40 3.92E-Ol 5.73E-01 8.39E-01 911. 07 27.70 2,98E-01 5.73E-01 969 .11 16.60 1.21E+OO l. llE+OO Th-234 63 .29 3.80 8.83E-01 1.90E+OO 4.38E+DO 92.59 5.41 1.29E+OO l.90E+00 U-235 143.76 10.50 -9.66E-01 l.57E-01 6.47E-01 163.35 4.70 -9.02E-01 1.52E+OO 185.72 54.00 l.06E-01 1.57E-01 205,31 4.70 4.12E-01 1.62E+00 Np-237 311.98 38.60 4,93E-02 1.BlE-01 l.81E-01 Am-241 59.54 35.90 4.78E-02 5.58E-01 5.58E-01

+ = Nuclide identified during the nucllde Identification

= Energy line found in the speclrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value Is inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 243 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8{2014 1:26:15PM Page 1 of5

~pex-Gamma Analysis Report for FSS-2014-0292 FSSP-OOL 10-12-009-F GAMMA SPECTRUM ANAL YSJS Sample ldentificalion : FSS-2014-0292 Sample Description : FSSP-OOL10-12-009-F Sample Type : 1LSoil Sample Slw : 9.243E+02 grams Facility : Default Sample Taken On : 4/30/2014 2:00:00PM Acquisition Started : 5{8/2014 1:15:50PM Procedure : 1LSolJMD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.01 %

Peak locate Threshold : 4.00 Peak Locale Range (in channels) : 100 - 4096 Peak Area Range (in channels) : 100 -4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2122(2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibrallon Description : 1L Marlnelll MD Sample Number P?-z::* 5'- r-1'/

PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 1:25:57PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 244 of 468

Attachment

..... 3 Lab .Data

.. -........ .for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/8/2014 1:26:15PM Page 2 of5 Analysis Report for FSS-2014-0292 FSSP*OOL 10-12-009-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 76.99 148 - 157 153. 96 6.24E+Ol 21.14 1. 71E+02 1.10 F 2 185.90 369 - 377 371. 77 3.82E+Ol 17.20 l.19E+02 0.98 F 3 238.56 472 - 481 477.08 l,27E+02 26.02 1.29E+02 1.13 F 4 351. 96 697 - 710 703.89 5. 72E+Ol 16.26 4.20E+Ol 1. 45 F 5 1460.95 2914 - 2929 2921. 74 1.45E+02 24.23 8.00E+OO 2.22 M= First peak in a mulllplet region m =-Other peak In a multiplet region F = Fitted singlet Errors quoted at 2,000slgma No background subtract performed on this spectrum.

NUCLIDE !DENT/FICA TION REPORT Nuclide Library lJsed : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl/grams) Uncertainty Bi-xRay 0,54 77 .11

100.00 l.32E-01 4.60E-02 87.20 36.00 K-40 0.99 1460.81

10.67 1.12E+Ol 1.97E+OO Pb-212 0.89 238.63

44.60 5.32E-Ol 1.13E-01 300.09 3.41 U-235 0.55 143.76 10.50 163.35 4.70 185. 72

54.00 l.13E-01 5.14E-02 205,31 4.70 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 245 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & H.f.3.P.P-FSSP-OOL 10-12 5/8/2014 1:26:15PM Page 3 of5 Analysis Report for FSS-2014-0292 FSSP-OOL 10*12-009-F

= Energy llne found in the spectrum.

- =Manually added nucllde.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Act!Vity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity ActiVity Confidence. Uncertainty (pCi!grams)

Bi-xRay 0.547 l.32E-01 4.60E-02 K-40 0.997 l.12E+Ol 1.97E+OO Pb-212 0.894 5.32E-01 l .13E-01 U-235/k *ZZ~ 0.557 l.l3E-01 5.14E-02

? nuclide is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines ~ot used In Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 246 of 468

Attachment 3 Lab Data for HBPP-f..§.~W-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:26:15PM Page 4 of5 Analysis Report for FSS-2014-0292 FSSP-OOL10*12-009-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8i2014 1;25:57PM Peak Locate From Channel : 100 Peak locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 4 351.96 9.52886E-02 14.22 Tol. ((~/

JM S*'1-I'/

M=First peak in a multiplet region m =,other peak in a multlpiel region F = Fitted singlet Errors quoted at 2,000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LlneMDA Name (pCilgrams) (pCl/grams) (pCl/grams)

(keV)

+ K-40 .1460.81

10.67 l.12E+Ol l.09E+00 l.09E+OO

Co-60 1173.22 100.00 -l.33E-01 1.16E-01 1.52E-01 1332.49 100.00 -3.35E-02 l.16E-01 Nb-94 702.63 100.00 2.84E-02 1.18E-01 1.19E-01 871.10 100.00 4.90E-03 l.18E-01 Ag-108m 79.20 7.10 -7.70E-01 8.83E-02 2.04E+OO 433.93 89.90 2.08E-02 8.83E-02 614.37 90.40 1.19E-01 1.76E-01 722. 95 90,50 9.95E-02 1. 39E-01 Cs-134 569.31 15.43 3.03E-01 1.44E-01 8.07E-01 604.70 97.60 1.68E-01 1.67E-01 795.84 85.40 3,94E-02 1.44E-01 Cs-137 661.65 85.12 5.74E-02 1.44E-01 1.44E-01 Eu-152 121. 78 28.40 -1.96E-01 2.62E-01 2.62E-01 244.69 7.49 -1.40E-01 l.19E+OO 344.27 26.50 -2.96E-01 3. llE-01 778.89 12.74 2. llE-01 8.84E-01 867.32 4.16 -5.37E-02 2.89E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 247 of 468

Attachment 3 Lab Data for HBPP-FSSP-O()L10-11 & HBPP-FSSP-OOL 10-12 5(8(2014 1:26:15PM Page 5 of5 Analysis Report for FSS-2014-0292 FSSP-OOL 10*12-009-F Nuclide Energy Yield{%) Activity Nuclide MDA LineMDA Name (pCl/grams) (pCi/grams) (pCi/grams)

(keV)

Eu-152 964.01 14.40 7.97E-01 2.62E-01 l.15E+OO 1085.78 10.00 -2.34E-Dl 1.49E+OO 1112.02 13.30 2.56E-Dl l.OOE+OO 1407.95 20.70 2.33E-01 5.48E-01 Eu-154 123.07 40.50 -l.85E-Ol 1.89E-Ol l.89E-01 247.94 6.60 -2.50E:+OO l.09E+OO 723. 30 19.70 4.58E-Dl 6.39E-01 873.19 11. 50 -1.77E-01 l.05E+OO 996.32 10.30 3,06E-01 l.06E+OO 1004.76 17.90 -3.77E-01 5.lOE-01 1274.45 35.50 3.60E-02 4. 91E-01 Eu-155 105.31 20.70 -2,38E-04 3.83E-01 3.83E-01 Pb-206 803.10 100.00 -5.42E-02 9.78E-02 9.78E-02 Ac-228 338.32 11. 40 4.82E-01 6.55E-01 8,57E-01 911. 07 27.70 5.15E-01 6.55E-01 969 .11 16. 60 4.09E-01 9.99E-01 Th-234 63.29 3.80 4.30E+OO 2.09E+OO 4.98E+OO 92.59 5.41 -2.77E-02 2.09E+OO

+ U-235 143. 7 6 10.50 -4.0lE-02 1. 28E-01 7.43E-01 163.35 4.70 6.42E-Ol l,69E+OO 185. 72

54.00 1.13E-01 1. 28E-01 205,31 4.70 -2.73E-Ol 1. 58E+OO Np-237 311.98 38.60 -9. OOE-03 1. 75E-01 1.75E-01 Am-241 59.54 35;90 -l.33E-Ol S.62E-01 5.62E-01

+ = Nuclide identified during !he nuclide identification

= Energy line found in the spectrum

> MDA value no! calculated \

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 248 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:41:15PM Page l of5

====== f\pex-Gamma Analysis Report for FSS-2014-0293 FSSP-OOL 10-12-010-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0293 Sample Description : FSSP-OOL 10-12-010-F Sample Type : 1L Soil Sample Size : 1.307E+03 grams Facility : Defaull Sample Taken On : 4/30/2014 1:05:00PM Acquisition Started : 5/8/2014 1:30:52PM Procedure : 1LSol!HD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli HD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100. 4096 Peak Area Range (In channels} : 100-4096 ldentifk;allon Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Callbra!!on Description : 1L Marinelli HD I

PEAK ANAL YS/S REPORT Peak Analysis Performed on : 5/8/2014 1 :40:58PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 249 of 468

Attachment 3 Lab Data for rt~f"P-FSSP-OOL 10~11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:41:15PM Page 2 of5 Analysis Report for FSS-2014-0293 FSSP-OOL 10-12-010-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.55 472 - 483 477.06 1.40E+02 26.23 l.39E+02 1. 48 F 2 351.92 699 - 709 703.79 8.61E+Ol 19.69 3.98E+Ol 1. 43 F 3 583.14 1160 - 1170 1166.26 3.44E+Ol 13.44 2.64E+Ol 1. 25 F 4 609. 39 1213 - 1225 1218.77 6.0lE+Ol 16.65 3.0lE+Ol 1. 53 F 5 1461.06 2914 - 2930 2921.96 l.14E+02 21.38 O.OOE+OO 1. 95 M = First peak in a multiplet region m = Other peak In a multiplet region

=

F Fitted singlet Errors quoted at 2.000slgma No background subtract performed on !his spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl/grams) Uncertainty K-40 0.99 1460.81 '* 10.67 6.66E+00 1.30E+OO Tl-208 0.69 277.35 6.80 583.14

84.20 1.19E-01 4.69E-02 860.37 12.46 Pb-212 0.89 238.63

44.60 4.52E-01 8.BBE-02 300.09 3.41 Bi-214 0.48 609.31

46.30 3.91E-01 1. llE-01 1120.29 15.10 1764.49 15.80 HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 250 of 468 FSS Report

Attachment 3 Lab Data for HEl.E'.P.-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 1:41 :15PM Page 3 of5 Analysis Report for FSS-2014-0293 FSSP-OOL10-12*010-F

=Energy line found In the speolrum.

- = Manually added nuolide.

? =Manually edited nuclide.

=

@ Energy line not used for Weighted Mean Activity Energy Tolerance : 1,000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCilgrams)

K-40 0.990 6.66E+OO 1.30E+OO Tl-208 0.696 1.19E-01 4.69E-02 Pb-212 0. 894 4.52E-01 8.88E-02 Bi-214 0.485 3.91E-01 1.llE-01

? nuclide Is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy line~ not used In Weighted Mean Activity Errors quoted al 2.000slgma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 251 of 468 FSS Report

Attachment 3 Lab Data for HB.PP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12

. 5/8/2014 1:41:15PM Page 4 of5 Analysis Report for FSS-2014-0293 FSSP-DOL 10-12-010-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 1:40:5BPM Peak locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak Na. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351.92 l.43442E-Ol 11.44 Tol.

=

M First peak in a multiplet region m = other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Ubrary\HBPP.NLB Nuclide Energy Yield(%) Activity NuclideMDA LineMDA Name . (pC!/grams) (pCi/grams) (pCilgrams)

(keV)

+ K-40 1460.81

10. 67 6.66E+OO l.58E-01 l.58E-01 Co-60 1173.22 100.00 -5. 91E-02 1.02E-01 l.02E-01 1332.49 100.00 2.18E-02 1.05E-01 Nb-94 702.63 100.00 2.02E-02 6.78E-02 8.65E-02 871 .10 100.00 -4.37E-02 6.78E-02 Ag-108m 79.20 7.10 -3.26E-Ol 6.33E-02 1.88E+OO 433.93 89.90 -8.33E-03 6.33E-02 614.37 90.40 -2.77E-02 l.53E-01 722. 95 90,50 2.56E-02 9.98E-02 Cs-134 569.31 15.43 1.46E-01 8.94E-02 6.43E-01 604.70 97.60 -2.19E-02 1.35E-01 795.84 85.40 -2.06E-02 8.94E-02 Cs-137 661.65 85.12 1. l 9E-02 9.49E-02 9. 4 9E-02 Eu-152 121. 78 28. 40 -5.07E-02 2.40E-01 2.50E-Ol 244.69 7. 49 . -5.06E-02 9.83E-Ol 344.27 26.50 -5.31E-01 2.40E-01 778.89 12.74 2.40E-01 7.82E-Ol 867.32 4.16 O.OOE+OO 1.70E+OO HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 252 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:41:15PM Page 5 of5 Analysis Report for FSS-2014-0293 FSSP-OOL 10-12-010-F Nuclide Energy Yield(%) Activity Nucl/deMDA LineMDA Name (pCi/grams) (pCi/grams) (pCl/grams)

(keV)

Eu-152 964.01 14.40 7.28E-01 2.40E-01 9.66E-Ol 1085.78 10.00 7.88E-01 l.13E+DO 1112. 02 13.30 -l.D8E+OO 5.96E-01 1407.95 20.70 2.34E-Ol 4.64E-01 Eu-154 123.07 40.50 -2.74E-02 1. 73E-01 1.73E-01 247.94 6.60 -7,81E-01 9.47E-01 723. 30 19.70 1. lBE-01 4.59E-01 873.19 11. 50 -3. llE-01 6.18E-01 996.32 10.30 2.77E-Ol 1.04E+OO 1004.76 17.90 4.55E-Dl 6.54E-01 1274.45 35.50 1.52E-01 3.17E-01 Eu-155 105.31 20.70 l.30E-01 3.29E-01 3.29E-Ol Pb-206 803.10 100.00 -1.97E-02 7.64E-02 7.64E-02 Ac-228 338.32 11. 40 6. 45E-Ol 4.61E-01 6.98E-Dl 911. 07 27.70 2.93E-01 4.61E-01 969 .11 16. 60 6.15E-Ol 8.61E-01 Th-234 63.29 3.80 7.22E-01 l.66E+OO 4.82E+OO 92.59 5.41 -6.87E-02 1.66E+OO U-235 143.76 10.50 l.60E-01 1. 32E-Ol 6.0lE-01 163:35 4.70 2.BlE-01 1.31E+OO 185. 72 54.00 1.04E-Ol l.32E-01 205.31 4.70 l,37E+OO l.47E+OO Np-237 311.98 38.60 4.33E-02 1.47E-01 l.47E-01 Am-241 59.54 35.90 -1.25E-Ol 5.91E-01 5.91E-Ol

+ = Nuclide ldenlifled during the nuclide Identification

= Energy Hne found In the spectrum

> MDA value not calculated

@ Hair-lire too short to be able to perform the decay correction

? CAUTION: MDA value Is inconsistent with Currie MDA at 95% confidence level HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 253 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:56:18PM Page I of5

~=~pex-Gamma Analysls Report for FSS-2014-0294 FSSP-OOL10-12-011-F GAMMA SPECTRUM ANALYSIS Sample Jdentlflcallon : FSS-2014-0294 Sample Description : FSSP-OOL10-12-011-F Sample Type : 1L Soll Samplf! Size : 9.662E+02 grams Faclllty : Default Sample Taken On : 4/30/2014 1:40:00PM Acquisllion Started : 5/8/2014 1:45:53PM Procedure : 1LSoilMD Operator : Administrator Detector Name : DET06 Geomelry : 1L Marlnelll MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Tiine : O.Q1 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (In channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On ; 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Number

~--""'),~ s~._,l

1656 lf PEAK ANAL YS/S REPORT Peak Analysis Performed on : 5/8/2014 1:56:00PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts {keV)

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 254 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:56:18PM Page 2 of5 Analysis Report for FSS-2014-0294 FSSP-00l10-12-011*F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.61 473 - 483 477.18 9.93E+Ol 24.30 1.78E+02 1.22 F 2 351. 74 698 - 709 703.45 5.06E+Ol 15.73 4.38E+Ol 0.92 F 3 583.55 1163 - 1170 1167.08 3.30E+Ol 13.19 2.62E+Ol 1.11 F 4 609.48 1214 - 1223 1218.96 4.29E+Ol 15.19 . 3. 73E+Ol 1.38 F 5 911. 65 1817 - 1828 1823.34 3.00E+Ol 11. 56 1. 21E+01 1. 30 F 6 1460.99 2915 - 2927 2921.80 l.45E+02 24.60 9.61E+OO 2.01 M = First peak in a muHlplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Ubrary\H8PP.Nl8 IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCf/grams) Uncertainty K-40 0.99 1460.81

10.67 l.OBE+Ol l.92E+OO Tl-208 0. 67 277.35 6.80 583.14

84,20 1.44E-01 5.82E-02 860.37 12.46 Pb-212 0.89 238.63

44.60 3.99E-01 1. OOE-01 300.09 3.41 Bi-214 0.48 609.31

46.30 3.53E-01 l.27E-01.

1120. 29 15.10 1764.49 15.80 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 255 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/8/2014 1:56:18PM Page 3 of 5 Analysis Report for FSS-2014-0294 FSSP-OOL 10-12-011-F

=Energy line found ln the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0-40 Errors quoted at 2.000slgma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.995 l.08E+Ol 1.92E+OO Tl-208 0.674 l.44E-Ol 5.82E-02 Pb-212 0.895 3.99E-01 1.00E-01 Bi-214 0.484 3.53E-01 l.27E-01

? nuclide Is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used in Weighted Mean Aclivity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 256 of 468

Attachment 3 Lab Data for HBPP-F~Sif.'-90L 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:56:1BPM Page 4 of5 Analysis Report for FSS-2014-0294 FSSP-OOL 10-12-011-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 1:56:00PM Peak Locate From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351. 74 8.44012E-02 15.53 Tol.

F 5 911.65 5.00027E-02 19.26 Tol.

p.IA-- .>~9~/tf

=

M First peak in a multiplet region m = Other peak in a muJUp!et region F = Filled sfnglet Errors quoted at 2.000sfgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB Nuclide Energy Yield{%) Activity NuclideMDA LineMDA Name (pCi/grams) (pCi/grams) (pCilgrams)

(keV)

+ K-40 1460.81

10.67 1.08E+Ol l.06E+OO 1.06E+OO Co-60 1173.22 100.00 3.69E-02 l.41E-01 l.41E-01 1332.49 100.00 -1.37E-02 1. 44E-01 Nb-94 702.63 100.00 4.87E-02 1. OOE-01 1.17E-01 871.10 100.00 l.94E-02 1.00E-01 Ag-108m 79.20 7.10 3.99E-01 8.44E-02 1.82E+OO 433.93 89.90 -1.56E-02 8.44E-02 614.37 90.40 -9.31E-02 1.73E-01 722. 95 90.50 7.43E-02 l.24E-01 Cs-134 569.31 15.43 3 .13E-02 1.20E-01 6.82E-01 604.70 97.60 -4.68E-02 1.65E-Ol 795.84 85,40 7.38E-02 l.20E-Ol

cs-137 661.65 85.12 l,56E-01 1.61E-01 1.61E-01 Eu-152 121.78 28.40 3,25E-03 2.42E-01 2.42E-01 244.69 7.49 -4.74E-01 1.27E+OO 344.27 26.50 -IJ.15E-01 2.88E-01 778.89 12.74 5.68E-01 9.56E-01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 257 of 468

r Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 1:56:18PM Page 5 of5 Analysis Report for FSS-2014-0294 FSSP-OOL 10-12-011-F Nuc/lde Energy Yield(%) Activity NuclideMDA LineMDA Name {pCl!grams) (pCl/grams) (pCUgrams)

(keV)

Eu-152 867.32 4.16 -l.16E+OO 2.42E-01 2.32E+OO 964.01 14.40 9.28E-01 l.16E+OO 1085.78 10.00 -l.89E-01 l.43E+OO 1112. 02 13.30 -1,07E+OO 1.09E+OO 1407.95 20.70 -8.36E-02 5.90E-01 Eu-154 123.07 40.50 7.17E-02 1.77E-01 1.77E-01 247.94 6.60 -3.07E+OO 9.95E-01 723.30 19.70 3.42E-01 5.71E-01

873 .19 11. 50 -6.59E-Ol 8.45E-01 996.32 10.30 3.64E-01 1.29E+OO 1004.76 17.90 l.46E-01 7,llE-01 1274.45 35.50 1.32E-01 4.37E-01 Eu-155 105.31 20.70 7.00E-02 3.46E-Ol 3.46E-01 Pb-206 803.10 100.00 -4.93E-02 9.04E-02 9.04E-02 Ac-228 338.32 11. 40 3.61E-01 6.48E-01 8.72E-01 911. 07 27.70 5.49E-01 6.48E-01 969 .11 16. 60 7.40E-01 9.98E-01 Th-234 63.29 3.80 2.88E+00 1.94E+OO 4.61E+OO 92.59 5.41 l.45E+OO 1. 94E+o*o U-235 143.76 10.50 -2.08E-Ol 1. 59E-01 6.70E-01 163.35 4.70 4.91E-01 l.59E+00 185. 72 54.00 1. l 9E-01 1.59E-01 205.31 4.70 -2.63E-Ol l.56E+OO Np-237 311. 98 38.60 3.22E-02 1.95E-01 1.95E-01 Am-241 59.54 35.90 -9,88E-02 5.28E-01 5.28E-01

' + = Nuclide Identified during the nuclide Identification

= Energy fine found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 258 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:11 :19PM Page I of5

~=~pex-Gamma Analysis Report for FSS-2014-0295 FSSP-OOL10-12-012-F GAMMA SPECTRUM ANAL YS/S Sample ldentmcation : FSS-2014-0295 Sample Description : FSSP-OOL10-12-012-F Sample Type : 1L Soil Sample Size : 7.275E+02 grams Facility : Default Sample Taken On : 4/30/2014 2:15:00PM Acquisition Started : 5/8/2014 2:00:54PM Procedure : 1LSoilMD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time ; 0.01 %

Peak Locale Threshold : 4.00 Peak Locate Range (in channels) : 100. 4096 Peak Area Range (In channels) : 100 -4090 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 2:11:01PM Peak Analysis From Channel : 100 Peak Analysis To Channel ; 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 259 of 468

Attachment 3 Lab Data for HBPP-F.~SP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 2:11:19PM Page 2 of5 Analysis Report for FSS-2014-0295 FSSP-OOL 10-12-012-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.66 474 - 481 477.28 8.04E+Ol 22.45 1.18E+02 1. 21 F 2 351.75 697 - 710 703.47 6.70E+Ol 16.76 2.80E+Ol 1.82 F 3 583.15 1161 - 1169 1166.28 2.67E+Ol 11.52 1.46E+Ol 1.17 F 4 661.80 1318 - 1328 1323.61 6.18E+Ol 16.65 1.93E+Ol 1. 51 F 5 1460,86 2914 - 2928 2921.55 1.17E+02 21.69 3.75E+OO 2.37 M = First peak In a mulliplet region m = Olher peak In a multlp!et region

=

F Filled singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP .NLB IDENTIFIED NUCUDES Nuc:lide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCl/grams) Uncertainty K-40 1. 00 1460.81

10.67 1.15E+Ol 2.23E+OO Cs-137 0,99 661.65

85.12 3.94E-01 1.08E-01 Tl-208 0.69 277.35 6.80 583.14

84.20 1.SSE-01 6.74E-02 860.37 12.46 Pb-212 0.89 238.63

44.60 4.29E-01 1. 22E-01 300.09 3.41 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 260 of 468

Attachment 3 Lab Data for HBPP-FSS.J:-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:11 :19PM Page 3 of5 Analysis Report for FSS-2014-0295 FSSP-OOL 10-12-012-F

= Energy line found In the spectrum.

- =Manually added nuclide.

? =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold= 0.40 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 1.000 1.15E+Ol 2.23E+OO V' Cs-137 0. 996 3.94E-01 1.08E-01 Tl-208 0,695 l.55E-01 6.74E-02 Pb-212 0.895 4.29E-01 l.22E-01

? nuclide is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nucllde contains energy lines not used In Weighted Mean Activity Errors quoted al 2.000sigma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 261 of 468 FSS Report

Attachment 3 Lab Data for HBPP.~f~.SP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:11:19PM Page 4 of5 Analysis Report for FSS-2014-0295 FSSP-OOL 10-12-012-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 2:11 :01PM Peak Locate From Channel : 100 Peak Locale To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS} Uncertainty Type Nuclide F 2 351. 75 l .11685E-01 12.51 Tol.

M = First peak In a multiple! region m =Other peak in a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Defauil\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuc/ldeMDA LineMDA Name (pCi/grams) (pCl/grams) (pCl!grams)

(keV)

+ K-40 1460.81

10.67 l.15E+Ol 1.02E+OO l.02E+OO Co-60 1173.22 100.00 l.67E-02 1.47E-01 2.12E-01 1332.49 100.00 3.35E-02 l.47E-01 Nb-94 702.63 100.00 2.52E-02 l.33E-01 l.34E-01 871.10 100.00 -9.73E-03 1. 33E-01 Ag-108m 79.20 7.10 4.22E-Ol l.16E-01 2.36E+00 433.93 89.90 -l.33E-02 l.16E-01 614.37 90.40 1. 56E-01 l.91E-Ol 722. 95 90.50 -3.59E-02 1.22E-Ol Cs-134 569.31 15.43 3.62E-Ol 1. 50E-01 9. 31E-01 604.70 97.60 5.33E-02 l.59E-01 795.84 85,40 s*. 28E-02 1.50E-01

+ Cs-137 661.65

85.12 3.94E-01 l.lBE-01 1.18E-01 Eu-152 121.78 28.40 2.44E-01 3,43E-01 3.43E-01 244.69 7.49 -1. 84E-01 1.46E+OO 344.27 26.50 -l.39E-01 3.78E-01 778.89 12.74 -2.03E-01 1.07E+OO 867.32 4.16 -1. 71E+OO 3.19E+OO HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 262 of 468 FSS Report

Attachment 3 Lab Datci.J.9r. .HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/8/2014 2:11:19PM Page S of5 Analysis Report for FSS-2014-0295 FSSP-OOL 10-12-012-F Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCl!grams) (pCl!grams) (pCilgrams)

(keV)

Eu-152 964.01 14.40 9.79E-Ol 3.43E-01 1. 44.E+OO 1085.78 10.00 4.12E-02 1.60E+OO 1112.02 13.30 6.88E-01 1.49E+OO 1407.95 20.70 4. 44E-Ol 8.22E-01 Eu-154 123.07 40.50 -8.76E-03 2.41E-01 2.41E-01 247.94 6.60 -1.83E+OO 1.30E+OO 723.30 19.70 -1.65E-01 5.59E-01 873.19 11. 50 4.76E-01 1.31E+OO 996.32 10.30 -4.79E-Ol l.18E+OO 1004.76 17.90 2.57E-01 8.40E-01 1274.45 35,50 -9. 45E-02 4.21E-01 Eu-155 105.31 20.70 -1.43E-01 4.34E-01 4.34E-01 Pb-206 803.10 100.00 -7.02E-02 l.06E-01 1.06E-01 Ac-228 338.32 11. 40 9.08E-01 7.44E-01 1.lOE+OO 911.07 27.70 5.83E-01 7.44E-01 969.11 16.60 l.03E+OO 1.31E+OO Th-234 63.29 3.80 -1.99E+OO 2.39E+OO 5.51E+OO 92.59 5.41 1. 21E+OO 2.39E+OO U-235 143.76 10.50 3.79E-01 1. 73E-01 8,45E-01 163.35 4.70 4.76E-01 1. 88E+OO 185. 72 54.00 l. llE-01 1.73E-01 205.31 4.70 1. 08E-02 2.02E+OO Np-237 311. 98 38.60 8.62E-02 2.22E-01 2.22E-01 Am-241 59.54 35.90 3,42E-Ol 7.0lE-01 7.0lE-01

+ = Nuclide identified during the nuclide Identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value is inconsistent wi!h Currie MDA at95% confidence level HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 263 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:26:20PM Page I ofS

~pex-Gamma Analysis Report for FSS-2014-0296 FSSP-OOL 10-12-013-F GAMMA SPECTRUM ANAL YS/S Sample ldentlficatlon : FSS-2014-0296 Sample Description : FSSP-OOL10-12-013-F Sample Type : 1L Soll Sample Size : 6.940E+02 grams Facility : Default Sample Taken On : 4/30/2014 2:14:00PM Acquisition Started : 5/8/2014 2:15:55PM Procedure : 1LSoil MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 -4096 Peak Area Range (in channels) : 100 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Number

,py;c;s.~s;. .

1658

)1-}

yy

/J,/ , / I J

I J'Vf-:.J~ 9 1/

s----1 .,_

PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 2:26:02PM Peak Analysis From Channel ; 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 264 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5(8(2014 2:26:20PM Page 2 of5 Analysis Report for FSS-2014-0296 FSSP-OOL10-12-013-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.73 472 - 483 477.41 7.66E+Ol 19.98 9.18E+Ol 1. 34 F 2 661. 81 1318 - 1330 1323.62 l.79E+02 26.84 2.03E+Ol 1. 75 F 3 1460.98 2916 - 2928 2921.78 9.25E+Ol 19.36 O.OOE+OO 2.21

=

M First peak in a mulliplet region m =Other peak In a mulliplel region

=

F Filled singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.99 1460.81

10. 67 9.55E+OO 2.06E+OO Cs-137 0.99 661.65

85.12 l.19E+OO 1.92E-01 Pb-212 0.89 238.63

44.60 4.29E-01 1.14E-01 300.09 3. 41

=Energy line found In the spectrum.

- =Manually added nuclide.

? =Manually edited nuclfda.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 265 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL1Q~1J .. & HBPP-FSSP-OOL 10-12 5/8/2014 2:26:20PM Page3 of5 Analysis Report for FSS-2014-0296 FSSP-OOL 10-12-013-F INTERFERENCE CORRECTED REPORT Nu cf/de Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

K-40 0.996 9.55E+OO 2.06E+OO v Cs-137 0.996 1.19E+OO l.92E-01 Pb-212 0,894 4.29E-01 1.14E-01

? nuclide Is part of an undetermined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 266 of 468

Attachment 3 Lab Data for HBPP-FSSP~.OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 2:26:20PM Page 4 of5 Analysis Report for FSS-2014-0296 FSSP-OOL 10-12-013-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 2:26:02PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were idenlilied.

=

M First peak in a mulflplet region m =Other peak In a mulliplel region F =Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCi/grams) (pCi/grams) (pCi/grams)

(keV)

+ K-40 1460.81

10.67 9.55E+OO 2.79E-01 2.79E-01 Co-60 1173.22 100,00 7.lSE-02 1.54E-01 1.91E-01 1332.49 100.00 -2.93E-02 l.54E-01 Nb-94 702.63 100.00 -6.22E-02 1.27E-01 1.27E-01 871.10 100.00 -6.35E-02 1.40E-01 Ag-108m 79.20 7.10 -1.llE+OO 1.22E-01 2.23E+OO 433.93 89.90 3. llE-02 1. 22E-01 614.37 90.40 1.72E-01 1. 72E-Ol 722. 95 90.50 7.73E-03 1.36E-01 Cs-134 569.31 15.43 4.19E-01 1.56E-Ol 8.80E-01 604.70 97.60 6.76E-03 1.56E-01 795.84 85.40 1. 06E-01 1. 71E-01

+ Cs-137 661.65

85.12 1.19E+OO l.33E-01 1.33E-01 Eu-152 121. 78 28.40 5.97E-02 2.88E-01 2.88E-01 244.69 7.49 -6,98E-02 1.27E+OO 344.27 26.50 -4.lOE-01 3.63E-01 778.89 12.74 -5,64E-01 7.22E-01 867.32 4.16 -1.47E+OO 3.35E+00 964.01 14.40 1.08E+OO l.53E+OO HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 267 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:26:20PM Page 5 of5 Analysfs Report for FSS-2014-0296 FSSP-OOL 10-12-013-F Nuclide Energy Yield(%) Activity Nuc/JdeMDA Line MDA Name (pGl!grams) (pG//grams) (pGi/grams)

(keV)

Eu-152 1085.78 10.00 l.40E-01 2.88E-01 1.37E+OO 1112.02 13.30 -6.81E-Dl 1.05E+OO 1407.95 20.70 -1.81E-01 4.8DE-01 Eu-154 123.07 40.50 3.55E-02 2.07E-01 2.07E-01 247.94 6.60 -l.82E+OD 1. 21E+OO 723. 30 19.70 3.56E-02 6.27E-01 873.19 11.50 -l.60E-01 1.33E+00 996.32 10.30 2.38E-01 1.36E+OO 1004.76 17.90 1.28E-01 7.54E-01 1274.45 35.50 2.23E-01 4.41E-01 Eu-155 . 105.31 20.70 2.47E-02 4.31E-Ol 4.31E-01 Pb-206 803.10 100.00 -5.43E-02 1. llE-01 l. llE-01 Ac-228 338.32 11. 40 -2.12E-01 7.22E-01 1.02E+00 911.07 27.70 4.71E-01 7.22E-01 969.11 16.60 3.90E-01 1. 27E+OO Th-234 63.29 3.80 4.97E+OO 2.36E+OO 5.91E+OO 92.59 5.41 5.21E-Ol 2.36E+OO U-235 143.76 10.50 9.94E-02 2.llE-01 9.74E-01 163.35 4.70 -1.09E+OO 1.77E+OO 185. 72 54.00 7.50E-02 2. llE-01 205.31 4.70 1.69E-01 2,08E+OD Np-237 311. 98 38.60 -9.41E-02 2.39E-01 2.39E-01 Am-241 59.54 35.90 -6.43B-01 6.52E-01 6.52E-01

+ " Nuclide Identified during !he nuclide identification

" Energy line found in the spectrum

> MDA value not calculated -

@ Half-life too short to be able to perform the d!Jcay correction

? CAUTION: MDA value is inconsistent wi!h Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 268 of 468

_J

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:41:21PM Page 1 of5 Analysls Report for FSS-2014-0297 FSSP-OOL 10-12-014-F GAMMA SPECTRUM ANAL YS/S Sample Identification : FSS-2014-0297 Sample Descrlplion : FSSP-OOL10-12-014-F Sample Type : 1LSo11 Sample Size : 9.091E+02 grams Facility : Default Sample Taken On ; 4/30/2014 2:11:00PM Acquisition Started : 5/8/2014 2:30:56PM Procedure : 1L Soll MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 -4096 Peak Area Range (in channels) : 100 - 4096 ldentiflcation Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Samp!eNum~* ~ ~ ~

. ~S-9~) . ~

. '1659 PEAK A '.AL YSIS REPORT Peak Analysis Performed on : 5/8/2014 2:41:02PM Peak Analysis From Channel : 100 Peak Analysis To Channel . : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 269 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:41:21PM Page 2 ors Analysis Report tor FSS-2014-0297 FSSP-OOL10-12-014-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts {keV)

F 1 238.57 471 - 482 477 .11 l.lOEf-02 24.45 1.48E+02 1.15 F 2 661.63 1318 - 1330 1323.27 5.47E+Ol 15.18 l.03E+Ol 1. 47 F 3 1460.87 2914 - 2929 2921. 57 l.70E+02 26.01 O.OOE+OO 2.19 M = First peak in a mul!ip!et region

=

m Other peak Jn a multiplet region

=

F FiUed singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Ubrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.81

10.67 1. 34E+Ol 2.17E+OO Cs-137 1. 00 661.65

85.12 2.79E-01 7.90E-02 '-'

Pb-212 0.89 238.63

44.60 4.69E-01 l,08E-01 300.09 3. 41

=Energy line found In !he spectrum.

- =Manually added nuclide.

7 =Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 270 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 2:41 :21PM Page 3 of5 Analysis Report for FSS-2014-0297 FSSP-OOL10-12-014-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

K-40 0.999 1.34E+Ol 2.17E+OO v Cs-137 1.000 2.79E-01 7.90E-02 Pb-212 0,895 4.69E-01 1.08E-01

? nuclfde Is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines nol used In Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 271 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12

*>* *H*** 0 5/8/2014 2:41:21PM Page 4 of 5 Analysis Report for FSS-2014-0297 FSSP-OOL 10-12-014-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 2:41:02PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS{%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were Identified.

M=First peak in a mulllplet region m =Other peak In a multiplet region F =Fit!ed singlet Errors quoted at 2.000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB Nuclide energy Yield(%) Activity Nur:fideMDA LineMDA Name (pCi/grams) (pCi!grams) (pCilgrams)

(keV)

+ K-40 1460.81

10. 67 l.34E+Ol 2.13E-01 2.13E-01 Co-60 1173.22 100.00 -5.28E-02 l.03E-01 1.83E-01 1332.49 100.00 -5.83E-02 l.03E-01 Nb-94 702.63 100.00 4.15E-02 l.07E-01 1.19E-01 871. 10 100,00 -4.64E-02 l.07E-01 Ag-108m 79.20 7.10 2.19E-01 8.97E-02 l.98E+OO 433.93 89.90 -6.03E-02 8.97E-02 614.37 90.40 1. 80E-01 l.73E-01 722. 95 90,50 5.42E-02 1.29E-01 Cs-134 569.31 15. 43 2.57E-01 1.31E-01 7.35E-01 604.70 97.60 3.77E-02 1. 32E-.01 795,84 85.40 4.65E-02 l.31E-01

+ Cs-137 661.65

85.12 2.79E-01 7.68E-02 7.68E-02 Eu-152 121. 78 28.40 -6,02E-02 2.81E-01 2.81E-01 244.69 7.49 8.74E-02 l.22E+OO 344.27 26. 50 -5.66E-01 3.06E-01 778.89 12.74 -3.00E-01 8. llE-01 867.32 4.16 -2.0SE-02 2.79E+OO 964. 01 14.40 3.88E-01 1.20E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 272 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 2:41:21PM Page 5 of 5 Analysis Report for FSS-2014-0297 FSSP-OOL 10-12-014-F Nuc/fde Energy Yield(%} Activity Nuclide MDA LlneMDA Name (pCJ/grams) (pCl/grams} (pCllgrams)

(keV}

Eu-152 1085. 78 10.00 -4.20E-01 2.81E-01 1.24E+OO 1112. 02 13.30 3,79E-02 1.24E+OO 1407.95 20.70 2.76E-Ol 5.93E-01 Eu-154 123.07 40.50 1. 72E-01 2.07E-01 2.07E-Ol 247.94 6.60 -1.39E+OO 1.18E+OO 723. 30 19.70 2.50E-01 5.95E-01 873.19 11. 50 2.34E-01 9.60E-01 996.32 10.30 2.43E-01 1.30E+OO 1004,76 17.90 1.55E-01 7.56E-01 1274.45 35.50 5.20E-02 4.40E-01 Eu-155 105.31 20.70 8.74E-03 3.62E-01 3.62E-01 Pb-206 803.10 100.00 -3.50E-02 1.06E-01 1. 06E-01 Ac-228 338.32 11. 40 9.99E-02 6.74E-01 8.46E-01 911. 07 27.70 4.51E-01 6.74E-01 969.11 16.60 3.84E-01 1.03E+OO Th-234 63.29 3.80 3.27E+OO 1.94E+OO 5.lOE+OO 92.59 5.41 2.78E-01 1.94E+OO U-235 143.76 10.50 -3.93E-02 1.60E-01 6.86E-Ol 163.35 4.70 1.92E-01 1.61E+OO 185.72 54.00 5.76E-02 1.60E-01 205.31 4.70 9.69E-02 1.66E+OO Np-237 311. 98 38.60 -3.79E-02 1 .,85E-01 l.85E-01 Am-241 59.54 35.90 7.92E-02 5.98E-01 5.98E-01

+ = Nuclide Identified during the nuclfde Identification

= Energy fine found in the speclrum

> MDA value not calculated

@ Half-life too short to be able to perform the decay correction

? CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 273 of 468

At1~1:!.11J~!lt_3_ Lab Data for HBPP-FSSP-.OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:56:23PM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0298 FSSP-OOL10-12-015-F GAMMA SPECTRUM ANAL YS/S Sample Identification ; FSS-2014-0298 Sample Description : FSSP-OOL10-12-015-F sample Type : 1L Soll Sample Size : 6.067E+02 grams Facility : Default Sample Taken On : 4/3012014 2:20:00PM Acquisition Started : 5/8/2014 2:45:57PM Procedure : 1L son LD Operator : Administrator Detector Name : DET06 Geometry : 1L MarineHi LD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.o1 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 -4096 Peak Area Range (In channels) : 100 -4096 ldentlficatlon Energy Tolerance : 1.000 keV Energy Callbrat!on Used Done On : 2/22/2012 Efficiency Callbrallon Used Done On : 4/2712011 Efficiency Calibralion Description : 1L Marinelli LO PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 2:56:04PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 274 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:56:23PM Page 2 of 5 Analysis Report for FSS-2014-0298 FSSP-OOL 10-12-015-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.47 471 - 482 476.90 7.68E+Ol 19.88 8.80E+Ol 1. 48 F 2 661. 75 1318 - 1328 1323. 50 7.38E+Ol 17 .26 5.SOE+OO 1.60 F 3 1460.99 2916 - 2928 2921. 80 1.16E+02 21.53 O.OOE+OO 2.14 M = First peak in a mult!plel region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yfe/d(%) Activity Activity Name Confidence (keV) (pCJ/grams) Uncertainty K-40 0.99 1460.81

10. 67 1.28E+Ol 2.47E+OO Cs-137 0.99 661.65

85.12 5.17E-01 1.24E-01 Pb-212 0.89 238,63.

44.60 4.36E-01 1.16E-01 300.09 3.41

= Energy line found In the spectrum.

- =Manually added nuclide.

? = Manually edited nucllde.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence Index threshold= 0.40 Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 275 of 468

Attachment 3 Lab Data for HBPP-FSSP-OQ.L1.0-11./lt HBPP-FSSP-OOL10-12 5/8/2014 2:56:23PM Page 3 of5 Analysis Report for FSS-2014-0298 FSSP-OOL 10-12-015-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)

K-40 0.995 1.28E+Ol 2.47E+00 v Cs-137 0.998 5.17E-Ol 1.24E-01 Pb-212 0.892 4.36E-01 l,16E-01

? nuclide is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuc!Jde contains energy lines not used in Weighted Mean Activity Errors quoted at 2.. ooOslgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 276 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 2:56:23PM Page 4 of5 Analysis Report for FSS-2014-0298 FSSP-OOL 10-12-015-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 2:56:04PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were Identified.

M = First peak in a multiplet region m =Other peak in a multiplet region F = Filled singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB Nuclide Energy Yfe/d(%) Activity NuclideMDA LineMDA Name (keV) (pC//grams} (pCl/grams) (pCl/grams)

+ K-40 1460.81

10.67 1. 28E+Ol 2.99E-01 2.99E-01 Co-60 1173.22 100.00 -7.44E-02 1.54E-01 2.20E-01 1332.49 100.00 3.28E-02 1. 54E-01 Nb-94 702.63 100. OD -6.26E-02 1.18E-Dl 1.18E-01 871.10 100.00 -8.32E-02 1.26E-01 Ag-108m 79.20 7.10 -9.95E-01 l.13E-01 2.29E+00 433.93 89.90 -7.75E-03 1.13E-01 614.37 90.40 2.77E-01 2.20E-01 722. 95 90.50 6. llE-02 1.52E-Ol Cs-134 569.31 15.43 3.08E-Ol l.66E-01 8.55E-01 604.70 97.60 l.49E-Ol 1.97E-01 795.84 85.40 3.'27E-02 1.66E-01

+ Cs-137 661. 65

85.12 S.17E-01 7.78E-02 7.78E-02 Eu-152 121.78 28.40 -5.31E-02 2.94E-01 2.94E-01 244.69 7.49 -1.84E-02 l.26E+00 344.27 26.50 -4.SOE-01 3.34E-01 778.89 12.74 -6.99E-Dl 1.0lE+OO 867.32 4.16 2.71E+DD 3.97E+OO 964.01 14.40 -l.64E-01 l.35E+DO FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 277 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 2:56:23PM Page 5 of5 Analysis Report for FSS-2014-0298 FSSP-OOL 10-12-015-F Nuc/fde Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCJ!grams) (pCl!grams) (pCl/grams)

(ke\.1 Eu-152 1085.78 10.00 3.93E-02 2.94E-01 1.84E+OO 1112.02 13.30 -1.33E+OO 1. 28E+OO 1407.95 20.70 -1.43E-01 7.79E-01 Eu-154 123.07 40.50 -8,18E-02 2.04E-01 2.04E-01 247.94 6.60 -1.17E+OO 1.20E+OO 723. 30 19.70 2.81E-01 6.97E-01 873.19 11. 50 -3.17E-01 1.lOE+OO 996. 32 10.30 3.51E-01 1.66E+OO 1004.76 17.90 -9.81E-02 8.34E-01 1274.45 35.50 l.85E-03 5.58E-01 Eu-155 105.31 20.70 -l,88E-01 4. 13E-01 4.13E-Ol Pb-206 803.10 100.00 -4.76E-02 1. 33E-01 l.33E-01 Ac-228 338.32 11. 40 6.34E-01 7.88E-01 1.13E+OO 911. 07 27.70 4.68E-01 7.88E-01 969 .11 16.60 1.09E+OO 1. 30E+OO Th-234 63.29 3,80 -1,56E+OO 2.55E+00 5.21E+OO 92.59 5.41 1.28E+OO 2.55E+OO U-235 143.76 10.50 7.97E-03 1. 99E-01 8.22E-01 163.35 4.70 4.64E-01 1.81E+OO 185. 72 54.00 2.02E-01 1.99E-01 205.31 4.70 -3.02E-02 2.lOE+OO Np-237 311. 98 38.60 3.78E-02 2.29E-01 2.29E-01 Am-241 59.54 35.90 2.82E-01 6.76E-01 6.76E-01

+ " Nuclide ldentined during the nuclide Identification

" Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short to be able lo perform the decay correction

? CAUTION: MDA value rs Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 278 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:11:31PM Pagel of5

~pex-Gamma Analysis Report for FSS-2014-0299 FSSP-OOL 10-12-016-F GAMMA SPECTRUM ANAL YS/S Sample ldenllficalion : FSS-2014-0299 Sample Description : FSSP-OOL10-12-016-F Sample Type : 1L Soil Sample Size : 9.240E+02 grams Facility : Default Sample Taken On : 4/30/2014 1:10:00PM Acquisition Started : 5/8/2014 3:01 :07PM Procedure ; 1LSoll MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.0 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (in channels) : 100 - 4096 Peak Area Range (In channels) : 100. 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marlnelll MD

,/J,/ Al/)

-* s~&-J

1661 1{,

~a:;/ s-r-1'1 Peak Analysls Performed on : 5/8/2014 3:11:13PM Peak Analysls From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts {keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 279 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FS~.P-OOL 10-12 5/8/2014 3:11:31PM Page 2 of5 Analysis Report for FSS-2014-0299 FSSP-OOL 10-12*016-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.40 472 - 482 476.76 9.87E+Ol 24.41 l.85E+02 1.15 F 2 351.73 698 - 709 703.42 5.79E+Ol 15.67 2.05E+Ol 1. 64 F 3 661.78 1319 - 1328 1323.56 5.04E+Ol 15.44 2.09E+Ol 1. 57 F 4 1461.01 2915 - 2928 2921.85 l.60E+02 25.22 O.OOE+OO 2.26 M = First peak in a multiplet region m = Other peak ln a mufliplat region

=

F Filled singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA T/ON REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Ubrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty K-40 0,99 1460.81

10.67 1. 24E+Ol ,2.07E+OO Cs-137 0.99 661.65

85.12 2.53E-01 7.88E-02 Pb-212 0.88 238.63

44.60 4.14E-01 l.OSE-01 300.09 3.41

=Energy line found in the spectrum.

- =Manually added nucllde.

? =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.40 Errors quoted at 2.000sigma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 280 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 3:11:31PM Page 3 of5 Analysis Report for FSS-2014-0299 FSSP-OOL10-12-016-F INTERFERENCE CORRECTED REPORT Nuclide Nuc:/lde Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl/grams)

K-40 0.994 1.24E+Ol 2.07E+OO v Cs-137 0.997 2,53E-01 7.88E-02 Pb-212 0.887 4.14E-01 1.0SE-01

? nuclide is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 281 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 _& HBPP~FSSP-OOL 10-12 5/8/2014 3:11 :31 PM Pagc4 of5 Analysis Report for FSS-2014-0299 FSSP-OOL 10-12-016-F UNIDENTIFIED PEAKS Peak Locate Performed on : 518/2014 3:11 :13PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size {CPS) Uncertainty Type Nuclide F 2 351.73 9.65650E-02 13.52 Tol.

M = Firs! peak in a multiplet region m =Other peak in a murtrplet region

=

F Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuc/idaMDA LineMDA Name (pCl/grams) (pC//grams) (pCJ/grams)

(kaV)

+ K-40 1460.81

10.67 1.24E+Ol 2.lOE-01 2.lOE-01 Co-60 1173.22 100.00 l.27E-02 l.45E-01 1.63E-01 1332.49 100.00 9.63E-04 1. 45E-01 Nb-94 702.63 100.00 1.70E-02 1.18E-01 1.23E-01 871.10 100.00 5.94E-02 1.18E-01 Ag-108m 79.20 7.10 4.50E-01 9.27E-02 1.94E+OO 433.93 89.90 -6.87E-03 9.27E-02 614.37 90. 40 2.30E-01 1.82E-01 722. 95 90.50 1.14E-01 1.43E-01 Cs-134 569.31 15.43 5.74E-02 l.55E-01 7.23E-01 604.70 97.60 1.75E-Ol 1.64E-Ol 795.84 85. 40 1. 03E-01 1.55E-01

+ Cs-137 661.65

85.12 2.53E-Ol 9.56E-02 9.56E-02 Eu-152 121.78 28.40 -1.70E-03 2.64E-01 2.65E-01 244.69 7. 49 1. 60E-01 1.24E+OO 344.27 26.50 -4.60E-01 2.64E-01 778.89 12.74 -5. 43E-01 9.25E-01 867.32 4.16 -4.08E+OO 2.34E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 282 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:11:31PM Page 5 of5 Analysis Report for FSS-2014-0299 FSSP-OOL 10-12-016-F Nuclide Energy Yield(%) Activity NuclldeMDA LineMDA Name (pCJ/grams) (pCl/grams) (pCl/grams)

(keV)

Eu-152 964. 01 14.40 1. llE+OO 2.64E-Ol 1.28E+OO 1085.78 10.00 -5.25E-01 l.30E+00 1112.02 13.30 -7.55E-01 7.47E-01 1407.95 20.70 3.llE-01 6.16E-01 Eu-154 123.07 40.50 -8.31E-02 1.85E-01 1.85E-01 247.94 6.60 -1.84E+OO l.13E+OO 723.30 19.70 5.23E-01 6,60E-01 873.19 11,50 5,99E-01 1. 08E+OO 996.32 10.30 1.47E-01 1. 21E+OO 1004.76 17.90 O,OOE+OO 6.83E-01 1274.45 35,50 -1.94E-01 4.57E-01 Eu-155 105.31 20.70 9.58E-02 3.92E-01 3.92E-01 Pb-206 803.10 100.00 -8.79E-03 1.lOE-01 1.lOE-01 Ac-228 338.32 11. 40 4.0lE-01 6.lOE-01 7.85E-01 911. 07 27.70 4.54E-01 6.lOE-01 969.11 16.60 8.55E-01 1.13E+OO Th-234 63.29 3.80 6.75E-01 2.05E+OO 4.64E+OO 92.59 5.41 -2.31E-01 2.05E+QO U-235 143.76 10.50 2.31E-01 1.55E-01 6.79E-01 163.35 4.70 4.21E-01 1.48E+OO 185. 72 54.00 6. lOE-02 l,55E-01 205.31 4.70 -3.81E-01 1. 72E+OO Np-237 311. 98 38.60 2. 77E-02 1.68E-01 1.68E-01 Am-241 59.54 35.90 -2.21E-02 5.89E-0:L 5.89E-01

+ = Nuclide identified during the nuclide !denlifica!ion

= Energy line found in the spectrum

> MDA value not calculated

@ Half-life loo shorl lo be able to perform the decay correction

? CAUTION: MDA value is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 283 of 468

Attachment 3 Lab Data for H.BP.P.-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:26:34PM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0300 FSSP-OOL 10-12-017-F GAMMA SPECTRUM ANALYSIS Sample Jdentiflcation : FSS-2014-0300 Sample Description : FSSP-OOL10-12-017-F Sample Type : 1LSol!

Sample Size : 9.562E+02 grams Facility : Default Sample Taken On : 4/30/2014 2:25:00PM Acquls!Uon Started : 5/8/2014 3:16:08PM Procedure : 1LSoll MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0,01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 -4096 Peak Area Range (Jn channels) : 100 - 4096 ldenliflcatlon Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Peak Analysis Performed on : 5/8/2014 3:26:14PM PeakAnalysls From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts {keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 284 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:26:34PM Page 2 of 5 Analysls Report for FSS-2014-0300 FSSP-OOL10-12-017-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 77.13 149 - 158 154.25 6.21E+01 21.11 l.60E+02 0.85 F 2 238.56 473 - 480 477.09 9.67E+Ol 23.48 l.09E+02 1. 06 F 3 295.09 586 - 594 590.15 4.30E+Ol 15.60 4.74E+Ol 1.17 F 4 351. 85 698 - 709 703.65 5.05E+Ol 15.95 4.80E+Ol 1.21 F 5 1461.01 2914 - 2929 2921.84 1.40E+02 23.51 O.OOE+OO 2.33 M " First peak in a mulliplet region m == Other peak In a multiplet region F == Fitted singlet Errors quoted at 2.000slgma No background subtract performed on this spectrum.

NUCLIDE !DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi!grams) Uncertainty Bi-xRay 0.54 77 .11

100.00 1.27E-01 4.42E-02 87.20 36.00 K-40 0.99 1460.81

10.67 1.0SE+Ol l.85E+OO Pb-212 0.89 238.63

44.60 3.92E-01 9.79E-0.2 300.09 3.41 Pb-214 0.79 241. 98 7.49 295.21

19.20 4.75E-01 l.74E-01 351. 92

37.20 3.31E-01 1. 06E-01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 285 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/8/2014 3:26:34PM Page 3 of5 Analysis Report for FSS-2014-0300 FSSP-OOL 10*12*017-F

= Energy line found In the spectrum.

= Manually added nuclide.

? = Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold= 0.40 Errors quoted at 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nucl/de Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

Bi-xRay 0.548 1.27E-Ol 4.42E-02 K-40 0.994 1.0SE+Ol l,85E+OO Pb-212 0.894 3. 92E-01 9.79E-02 Pb-214 0.790 3.70E-01 9.06E-02

? nuclide is part of an undetennined solution X nuclide rejected by the interference analysis

@ nuclide contains energy lines no! used Jn Weighted Mean Activity Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 286 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 3:26:34PM Page 4 of5 Analysis Report for FSS-2014-0300 FSSP-OOL 10-12-017-F UNIDENTIFIED PEAKS Peak Locate Performed on ; 5/8/2014 3:26:14PM Peak Locate From Channel ; 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.

=

M First peak in a multiplet region

=

m Other peak In a multiplet region F = Fitted singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP .NLB Nuclide Energy Yield(%} Activity Nuclide MDA LlneMDA Name (pCJ/grams) (pCl/grams) (pC//grams)

(keV)

+ K-40 1460.81 10.67 l.05E+Ol 2.03E-01 2.03E-01 Co-60 1173.22 100.00 4.53E-02 1. 35E-0'1 1. 50E-01 1332.49 100.00 3.89E-02 l.35E-01 Nb-94 702.63 100.00 l.09E-01 1.0lE-01 l.19E-01 871.10 100.00 -6.24E-02 1.0lE-01 Ag-108m 79.20 7.10 -l.BlE-01 1.00E-01 1.95E+OO 433.93 89.90 2.23E-02 1.00E-01 614.37 90:40 1. 84E-01 1. 71E-01 722.95 90.50 -2.19E-02 1. 32E-01 Cs-134 569.31 15.43 6.47E-01 l.39E-01 8.69E-01 604.70 97.60 1. 48E-01 1.53E-01 795.84 85.40 7.12E-02 l.39E-01 Cs-137 661.65 85 .12 l.95E-01 l.94E-01 1. 94E-01 Eu-152 121. 78 28.40 -5.74E-02 2.38E-01 2.38E-01 244.69 7.49 -1.76E+OO 1. llE+OO 344.27 26.50 -3.98E-01 3.26E-01 778.89 12.74 -3.95E-01 8.3SE-01 867.32 4.16 -1.30E+00 2.66E+OO 964.01 14.40 6.36E-01 l. llE+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 287 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/8/2014 3:26:34PM Pagc5 ofS Analysis Report for FSS-2014-0300 FSSP-OOL 10-12-017-F Nuclide Energy Yield(%) Activity Nuc/ldeMDA LlneMDA Name (pC/lgrams) (pCl/grams} (pC/lgrams}

{keV)

Eu-152 1085.78 10.00 3.99E-01 2.38E-01 l.30E+OO 1112. 02 13. 30 -4.33E-01 1'. 02E+OO 1407.95 20.70 l,13E-01 4.04E-Ol Eu-154 123.07 40.50 -l.07E-01 l.67E-01 1.67E-01 247.94 6.60 -6,86E-01 l.16E+OO 723. 30 19.70 -1.0lE-01 6.08E-01 873.19 11. 50 -l.15E-01 9.13E-01 996. 32 10.30 2.50E-01 l.07E+OO 1004.76 17.90 -7.70E-02 6.39E-01 1274.45 35.50 6,88E-02 3:66E-01 Eu-155

105.31 20.70 -5.94E-03 3.67E-01 3,67E-01 Pb-206 803.10 100.00 -7.16E-02 l.09E-01 1.09E-01 Ac-228 338.32 11. 40 -6.92E-03 6.41E-01 8.22E-01 911.07 27.70 5,76E-01 6.41E-01 969.11 16,60 7.00E-01 8.90E-01 Th-234 63.29 3.80 3.45E-01 1.96E+OO 4.66E+OO 92.59 5.41 2.91E-01 1. 96E+OO U-235 143.76 10.50 8.41E-03 l.66E-Ol 7.0lE-01 163.35 4.70 9.17E-01 l.52E+OO 185.72 54.00 l.69E-01 1.66E-01 205.31 4.70 1.34E+OO l.62E+OO Np-237 311. 98 38. 60 -4.74E-02 1.97E-01 1.97E-01 Arn-241 59.54 35.90 2.04E-02 5.60E-Ol 5.60E-01

+ = Nuclide identified during the nuclide identificalion

= Energy line found In the spectrum

> MDA value not calculated

@ Half-life too short lo be able to perform !he decay correction

? CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 288 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:41:36PM Page 1 of5

~pex-Gamma Analysis Report for FSS-2014-0301 FSSP-OOL 10-12-018-F GAMMA SPECTRUM ANALYSIS Sample Identification : FSS-2014-0301 Sample Descrlptlon : FSSP-OOL 10-12-018-F Sample Type : 1LSoil Sample Size : 8,375E+02 grams Facility : Default Sample Taken On : 4/30/2014 2:31:00PM Acquisition Started : 5/8/2014 3:31:09PM Procedure : 1LSoUMD Operator : Administrator Detector Name ; DET06 Geometry : 1L Marinelli MD Live Time : 1600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100 -4096 Peak Area Range (In channels) : 100-4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Callbrallon Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marinelli MD Sample Number : 1663 /}

p-.ree-~~ S- gvj +/-' -~~

11 s---r-11 PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 3:41:16PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 289 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 51812014 3:41:36PM Page 2 of5 Arialysls Report for FSS-2014-0301 FSSP-OOL 10-12-018-F Peak Energy ROI ROI Peak Net Peak NetArea Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.56 472- 483 477.07 l.19E+02 25.12 l.62E+02 1. 05 F 2 1461. 07 2916 - 2928 2921.97 l.46E+02 24.21 O.OOE+OO 1. 94 M = First peak In a mul!lplet region m = Other peak In a mulliplet region F = Flfted singlet Errors quoted at 2.000sigma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Ubrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCilgrams) Uncertainty K-40 0.98 1460.81

10.67 1.25E+Ol 2.18E+OO Pb-212 0.89 238.63

44.60 5.52E-01 l.21E-01 300.09 3.41

= Energy line found In the spectrum.

- =Manually added nuclide.

7 =Manually edited nuclide.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 290 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:41:36PM Page 3 ofS Analysis Report for FSS-2014-0301 FSSP-OOL 10-12-018-F INTERFERENCE CORRECTED REPORT Nuclide Nucl/de Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCl!grams)

K-40. 0.989 1.25E+Ol 2.18E+OO Pb-212 0.894 5.52E-01 l.21E-01

? nuclide Is part of an undetermined solution X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000sigma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 291 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:41 :36PM Page 4 of5 Analysis Report for FSS-2014-0301 FSSP-OOL 10-12-018-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 3:41:16PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were Identified.

M =First peak In a multiplet region m = Other peak In a muIUplet region F =Filled singlet Errors quoted at 2.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Defaull\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuc/ideMDA LlneMDA Name (pCl/grams) (pCllgrams) (pCi/grams)

(keV)

+ K-40 1460.81

10. 67 1. 25E+Ol 2.32E-01 2.32E-01 Co-60 1173.22 100.00 6.59E-02 l.02E-01 l.76E-01 1332.49 100.00 -2.97E-02 1.02E-01 Nb-94 702.63 100. 00 -2.64E-03 l.03E-01 1. 03E-01 871.10 100.00 -4.50E-02 l.12E-01 Ag-108m 79.20 7,10 -9.86E-02 1.02E-01 2.lOE+OO 433.93 89.90 1. 60E-02 1. 02E-01 614.37 90.40 1.53E-01 2.00E-01 722.95 90.50 5.78E-02 1. 51E-01 Cs-134 569.31 15.43 -2.26E-01 l.42E-01 7.29E-01 604.70 97.60 1. 26E-01 1.77E-01 795.84 85.40 6.98E-02 1.42E-01 Cs-137 661.65 85.12 1. 4 7E-01 l.84E-01 l.84E-01 Eu-152 121.78 28.40 9.88E-02 2.86E-01 2.86E-01 244.69 7.49 -6.62E-Ol 1.31E+OO 344.27 26. 50 -3.0lE-01 3.21E-01 778.89 12.74 -6.42E-01 7.70E-01 867.32 4.16 -1.78E-01 3.19E+OO 964.01 14.40 7.80E-01 l.23E+OO FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 292 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 5/8/2014 3:41:36PM Page 5 of5 Analysis Report for FSS-2014-0301 FSSP-OOL 10-12-018-F Nuclide Energy Yield{%) Activity Nuc/ideMDA LineMDA Name (pCl/grams) (pCl/grams) (pC//grams)

(keV)

Eu-152 1085.78 10.00 6.71E-01 2.86E-01 1. 53E+OO 1112. 02 13 .30 -4.SlE-02 1.lOE+OO 1407.95 20.70 -6.19E-02 7.14E-01 Eu-154 123.07 40.50 -7.51E-02 1. 95E-01 1.95E-01 247.94 6,60 -1.0lE+OO 1.20E+OO 723. 30 19.70 2.66E-01 6.94E-01 873. 19 11. 50 -3.37E-01 9.75E-01 996. 32 10.30 -9.42E-01 1.38E+OO 1004.76 17.90 3.64E-01 8.41E-01 1274.45 35.50 3.03E-01 5.05E-01 Eu-155 105.31 20.70 1.22E-02 4.13E-01 4.13E-01 Pb-206 803.10 100.00 -6.51E-02 8.32E-02 8.32E-02 Ac-228 338.32 11. 40 9.05E-01 6.64E-01 9.18E-01 911.07* 27.70 2.17E-Ol 6.64E-01 969. 11 16.60 2.26E-Ol l.07E+OO Th-234 63.29 3.80 1.97E+OO 2.00E+OO 4.91E+OO 92.59 5.41 -1.06E-01 2.00E+OO U-235 143.76 10.50 9.60E-01 1.69E-01 8.49E-01 163.35 4.70 -2.62E-Ol 1.55E+OO 185. 72 54.00 6.35E-02 1.69E-01 205.31 4.70 l.99E-01 l.71E+OO Np-237 311. 98 38.60 5.09E-02 2.0lE-01 2.0lE-01 Am-241 59.54 35.90 9.22E-03 5.71E-01 5. 71E-01

+ Nuclide Identified during the nuclide identification

" Energy line found In the spectrum

> MDA value not calculated

@ Half-fife loo short to be able lo perform the decay correction

? CAUTION: MDA value is inconsistent with Currie MDA al 95% confidence level FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 293 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/B/2014 3:56:36PM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0302 FSSP-OOL 10-12-019-F GAMMA SPECTRUM ANAL YS/S Sample ldentlficallon : FSS-2014-0302 Sample Description : FSSP-OOL 10-12-019-F Sample Type : 1L Soll Sample Size : 1.112E+03grams Facility : Default Sample Taken On : 4/30/2014 2:28:00PM Acquisition Started : 5/8/2014 3:46:10PM Procedure : 1LSoll MD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli MD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4.00 Peak Locate Range (In channels) : 100. 4096 Peak Area Range (In channels) : 100. 4096 ldentlnca!lon Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2/22/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency Calibration Description : 1L Marlnelll MD Sample Number~~~~ ~ #t)L 2 PEAK A~AL YSIS REPORT Peak Analysis Performed on : 5/8/2014 3:56;16PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 294 of 468

Attachment 3 Lab Data for HBPP-F.~S.P:OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 3:56:36PM Page 2 of5 Analysis Report for FSS-2014-0302 FSSP-OOL 10-12-019-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. {keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238,50 470 - 483 476.97 1.42E+02 26.60 1.66E+02 1. 37 F 2 351.90 699 - 709 703.77 7.02E+Ol 17.74 3.02E+Ol 1. 45 F 3 1460,99 2915 - 2929 2921. 80 1.68E+02 26.03 3.42E+OO 2.13 M = First peak in a mulliplet region m =Other peak In a multiplet region F = Filled singlet Errors quoted al 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Rool\Defauil\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pC/lgrams) Uncertainty K-40 0.99 1460.81

10,67 1.08E+Ol 1.78E+OO Pb-212 0.89 238.63

44.60 4.94E-01 9. 71E-02 300.09 3.41

= Energy line found In the spectrum.

- =Manually added nuclide.

=

? Manually edited nuclide.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence Index threshold = 0.40 Errors quoted at 2.000slgma FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 295 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:56:36PM Page 3 of5 Analysls Report for FSS-2014-0302 FSSP-OOL 10-12-019-F INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

K-40 0.995 l.OBE+Ol l.78E+OO Pb-212 0.893 4-94E-01 9. 71E-02

? nuclide Is part of an undetermined solullon X nuclide rejected by the Interference analysis

@ nuclide contains energy lines not used In Weighted Mean Activity Errors quoted at 2.000slgma HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 296 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:56:36PM Page 4 of5 Analysis Report for FSS-2014-0302 FSSP-OOL 10-12-019-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 3:56:16PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide F 2 351.90 l.17049E-01 12.63 Tol.

M = First peak in a multiplet region m = Other peak In a multiplet region

=

F Fitted singlet Errors quoted at 2,000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\HBPP .NLB Nuclide Energy Yield(%) Activity Nuc/ldeMDA LlneMDA Name (pCl/grams) (pCi/grams) (pCl!grams)

(keV)

+ K-40 1460.81

10.67 1.08E+Ol 6.32E-01 6.32E-01 Co-60 1173.22 100.00 2.96E-02 8.39E-02 1.60E-01 1332.49 100.00 3.20E-02 8.39E-02 Nb-94 702.63 100.00 -7.81E-02 8.58E-02 8.58E-02 871.10 100.00 l.51E-02 l.lOE-01 Ag-108m 79.20 7.10 4.06E-01 6.53E-02 l.74E+OO 433.93 89.90 -3.15E-02 6.53E-02 614.37 90.40 l,14E-01 l,45E-01 722. 95 90,50 -3,88E-03 1.26E-01 Cs-134 569.31 15.43 4.29E-01 l.17E-01 6.86E-01 604.70 97. 60 6.71E-02 1.33E-01 795.84 85.40 -4.0lE-03 1.17E-01 Cs-137 661.65 85.12 *7.23E-02 1.18E-01 1.18E-01 Eu-152 121. 78 28.40 l.80E-02 2.25E-01 2.25E-01 244.69 7.49 -9.57E-01 1.04E+OO 344.27 26.50 -3.47E-01 2.85E-01 778,89 12.74 -2.88E-01 7.68E-01 867.32 4.16 -1.66E+OO 2.63E+00 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSPDOL10-12 Page 297 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 3:56:36PM Page 5 of5 Analysis Report for

FSS-2014-0302 FSSP-OOL10-12-019-F Nuol/de Energy Yield(%) Activity Nuol/deMDA LlneMDA Name (pC//grams) (pC/lgrams) (pCl/grams)

(keV)

Eu-152 964.01 14.40 6.27E-01 2.25E-01 l.15E+OO 1085.78 10.00 5.49E-01 l.24E+OO lll2.02 13.30 -l.61E+OO 7.78E-01 1407.95 20.70 2.02E-01 6.29E-01 Eu-154 123,07 40.50 -9.14E-02 l.59E-01 1. 59E-cil 21J7.94 6.60 -2.12E+OO 9.55E-01 723. 30 19.70 -1. 79E-02 S.80E-01 873,19 11.50 7.37E-Ol 1. OlE+OO 996. 32 10.30 -9.33E-02 l.OlE+OO 1004.76 17.90 l.06E-01 4.92E-01 1274.45 35.50 l.22E-Ol 3.02E-Ol Eu-155 105,31 20.70 l.OOE-01 3.40E-Ol 3.40E-01 Pb-206 803.10 100.00 -3.76E-02 B.90E-02 8.90E-02 Ac-228 338.32 11. 40 4.26E-Ol 5.86E-01 7.53E-01 911. 07 27.70 5.42E-01 5.86E-01 969. ll 16.60 6.85E-01 9.68E-01 Th-234 63.29 3.80 3.26E-Ol l.62E+OO 4.18E+OO 92.59 5.41 -2.38E-01 1.62E+OO U-235 143.76 10.50 2.06E-02 l.41E-01 6.22E-01 163,35 4.70 -2,22E-02 1.43E+OO 185. 72 54.00 1. 09E-01 1.41E-01 205.31 4.70 2.36E-01 l.45E+OO Np-237 311. 98 38.60 l.30E-01 1. 88E-01 1. 88E-01 Am-241 59.54 35.90 -7.13E-02 4.95E-01 4.95E-01

+ " Nuclide Identified during the nuclide Identification

= Energy line found In the spectrum

> MDA value not calculated

@ Half-llfe too short to be able lo perform !he decay correction

? CAUTION: MDA value Is lnconsislenl with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 298 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 5/8/2014 4:11:39PM Page I of5

~pex-Gamma Analysis Report for FSS-2014-0303 FSSP-OOL 10-12-020-F GAMMA SPECTRUM ANALYSIS Sample ldentiflcaUon : FSS-2014-0303 Sample Description : FSSP-OOL 10-12-020-F Sample Type : 1LSoll Sample Size : 1.286E+03 grams Facility : Default Sample Taken On : 4/30/2014 2:40:00PM Acquisition Started : 5/8/2014 4:01 :11 PM Procedure : 1L Soil HD Operator : Administrator Detector Name : DET06 Geometry : 1L Marinelli HD Live Time : 600.0 seconds Real Time : 600.1 seconds Dead Time : 0.01 %

Peak Locate Threshold : 4,00 Peak Locale Range (in channels) : 100 - 4096 Peak Area Range (fn channels} : 100. 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 2122/2012 Efficiency Calibration Used Done On : 4/27/2011 Efficiency CallbraUon Description : 1L Marinelli HD Sample Number PEAK ANALYSIS REPORT Peak Analysis Performed on : 5/8/2014 4:11:18PM Peak Analysis From Channel : 100 Peak Analysis To Channel : 4096 Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 299 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 4:11:39PM Page 2 of 5 Analysis Report for FSS-2014-0303 FSSP-OOL 10-12-020-F Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV)

F 1 238.55 472 - 482 477.05 l.50E+02 27.52 l.45E+02 1. 29 F 2 295.14 585 - 594 590.24 4.60E+Ol 15.85 5.33E+01 1,16 F 3 351.80 698 - 710 703.57 7.62E+Ol 18.34 3.78E+Ol 1. 50 F 4 583.42 1162 - 1170 1166.83 3.16E+Ol 12.56 1.80E+Ol 1. 26 F 5 609.49 1214 - 1224 1218.98 6.39E+Ol 17.11 2.70E+Ol 1. 33 F 6 1461.01 2917 - 2927 2921.85 1.54E+02 25.18 8.56E+OO 1. 75

=

M First peak in a multiplet region

=

m other peak In a multiplet region

=

F Fitted singlet Errors quoted al 2.000slgma No background subtract performed on this spectrum.

NUCLIDE /DENT/FICA TION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pC//grams) Uncertafnty K-40 0.99 1460. 811

10.67 9.lOE+OO 1.57E+OO Tl-208 0.68 277.35 6.80 583.14

84.20 1. llE-01 4.46E-02 860.37 12. 46 Pb-212 0.89 238,63

44.60 4.92E-01 9.49E-02 300,09 3.41 Bi-214 0.48 609,31

46.30 4.23E-01 1.16E-01 1120.29 15 ..10 1764.49 15.80 Pb-214 0.79 241.98 7.49 295.21

19.20 4.08E-01 1.43E-01 351.92

37.20 4.00E-01 9.86E-02 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 300 of 468

Attachment 3 Lab D§t? for HBPP-FSSP-OOL 10-11 & HBPP-FSSP~OOL 10-12 5/8/2014 4:11:39PM Page 3 of5 Analysis Report for FSS-2014-0303 FSSP-OOL 10-12-020-F

= Energy line found In the spectrum.

- =Manually added nuclide.

? = Manually edited nucllde.

@ =Energy line not used for Weighted Mean Activity Energy Tolerance: 1.000 keV Nuclide confidence index threshold= 0.40 Errors quoted al 2.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi!grams)

K-40 0.993 9.lOE+OO l.57E+OO Tl-208 0.686 l. llE-01 4.46E-02 Pb-212 0.894 4.92E-01 9.49E-02 Bi-214 0.482 4.23E-01 1.16E-01 Pb-214 0,791 4.03E-01 8.llE-02

? nuclide is part of an undetennined solution X huc!Jde rejected. by the Interference analysis

@ nuclide contains energy lines not used in Weighted Mean Activity Errors quoted al 2.000slgma FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 301 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 5/8/2014 4:11:39PM Page 4 of5 Analysis Report for FSS-2014-0303 FSSP-OOL 10-12-020-F UNIDENTIFIED PEAKS Peak Locate Performed on : 5/8/2014 4:11:18PM Peak Locate From Channel : 100 Peak Locate To Channel : 4096 Peak CPS(%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were Identified.

=

M First peak In a multiplet region

=

m Other peak in a multiplet region

=

F Fitted singlet Errors quoted at 2,000slgma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Llbrary\HBPP.NLB Nuclide Energy Yield(%) Activity Nuc/JdeMDA LineMDA Name (pCl/grams) (pCi!grams) {pCf!grams)

(keV)

+ K-40 1460.81

10,67 9,lDE+OO 7.92E-01 7.92E-01 Co-60 1173.22 100.00 2.42E-04 9.65E-02 9.65E-02 1332.49 100.00 l,03E-02 9.83E-02 Nb-94 702.63 100.00 -l.30E-02 9.SBE-02 9.58E-02 871.10 100.00 3.48E-02 9.72E-02 Ag-108m 79.20 7.10 1.56E+OO 7.68E-02 l.92E+OO 433.93 89,90 -8.15E-02 7.68E-02 614.37 90.40 -5.19E-02 1.58E-01 722. 95 90.50 -2,54E-02 1.12E-01 Cs-134 569.31 15,43 2.63E-01 l.13E-01 5.72E-01 604.70 97,60 -4.20E-02 l.37E-01 795.84 85,40 3.52E-02 1.13E-01 Cs-137 661.65 85.12 5. 31E-02 l.lOE-01 1.lOE-01 Eu-152 121. 78 28.40 -4.76E-02 2.37E-01 2.37E-01 244.69 7.49 1. 9BE-01 9.14E-01 344.27 26.50 -4.81E-01 2.63E-01 778. 89 12.74 -2.57E-01 7.95E-01 867.32 4.16 -2.19E+OO 1.BOE+OO 964.01 14 .40 8.27E-01 8.96E-01 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 302 of 468

Attachment 3 Lab Data for HBPP-FSSP_-O_(JL10J 1 & HBPP-FSSP-OOL 10-12 5/8/2014 4:11:39PM Page 5 of5 Analysis Report for FSS-2014-0303 FSSP-OOL 10-12-020-F Nuclide Energy Yield(%) Activity Nuclide MDA LineMDA Name (pCJ!grams) (pCl/grams) (pCl!grams)

(keV)

Eu-152 1085.78 10.00 1.58E-01 2.37E-01 1.17E+OO 1112.02 13.30 -l.27E+OO 6.65E-01 1407.95 20.70 4.21E-02 4.95E-01 Eu-154 123.07 40.50 -6.70E-02 1.69E-Ol 1.69E-01 247.94 6.60 -9,21E-01 8.91E-01 723. 30 19.70 -1.17E-01 5.15E-01 873.19 11. 50 3.56E-01 9,03E-01 996.32 10.30 -2.48E-01 1.0lE+OO 1004.76 17.90 -l.05E-01 5.0BE-01 1274.45 35,50 1. 96E-01 3,93E-01 Eu-155 105.31 20.70 -2.65E-02 3.40E-01 3.40E-Ol Pb-206 803.10 100.00 -6.52E-02 7.27E-02 7.27E-02 Ac-228 338.32 11.40 5.30E-01 4.75E-01 7.62E-01 911.07 27.70 3,13E-01 4,75E-01 969.11 16.60 5.52E-01 8.13E-01 Th-234 63.29 3.80 1. 40E+OO 1. 66E+OO 4.76E+OO 92.59 5.41 -1. 65E+OO 1.66E+OO U-235 143,76 10,50 4.23E-02 l.43E-01 6.55E-01 163.35 4.70 -3.70E-01 1.39E+OO 185. 72 54.00 4.61E-02 1.43E-01 205.31 4.70 2.38E-01 1.40E+OO Np-237 311. 98 38.60 8.57E-02 1.59E-01 1. 59E-01 Am-241 59.54 35.90 -1. 02E-01 5.67E-01 5.67E-01

+ = Nuclide identified during the nuclide Identification

= Energy line found In the spectrum

> MDA value not calculated

@ Haff-life too short lo be able lo perform the decay correction

? CAUTION: MDA value Is Inconsistent with Currie MDA at 95% confidence level FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 303 of 468

Att!"chment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontiumw90 Analysis Sheet Sample Number: 2014

0264 Gen~ral Information .

Sample

Description:

FSSP-OOL 10-11-001-F Fishermans Channel Sample Collection Datemme: __4_12_8_!1_4_8_:o_o_

Counting Instrument: _ _P_r_o_te_an __ S/N: 7109 Calibration Due Date: 10/16/2014

sr Recovery i Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 . "1.00 0.0961 o.1q11 57.96 Sample blank 1(-0*.*t.; 0.00 Net Recovery 57.96 Caunting Information Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/time 3.01 60.00 60.00 5/8/14 9:47 4.99E-01 5/8/14 18:30 Count Data *11 R.~suits 1 Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.63 3.17 0.241 0.342 0.577 0.277 Comments: Batch: OOL10-11-Sr-2 Performed By~ Date :Hz.ti Reviewed By: ~~

,- Date .:"-1.:J./t/

2014-0264.xls V and V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 304 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0265 General Information :

Sample

Description:

FSSP-OOL 10-.11-002-F Fisherman's Channer Sample Collection Dateffime: __ 4/_2_81_1_4_8_:1_0_

Counting Instrument: _ _P_r_ot_e_an_ _ S/N: 7108 Calibration Due Date: 10/29/2014 Sr Carrier Sr Recovery mglml g g (%)

Sample ... 5.12 0.0960 0.1042 95.05 Sample blank 0.00 Net Recovery 95.05 Counting Information '.

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Daternme Factor dateltlme 3.00 60.00 60.00 5/1/14 14:48 9.55E-01 5/1/20 19:52 Count Data II . Results .

Gross Sample Background sr-90 Activily 2o Error MDA Le (cpm) {cpm) pCl/g pCilg pCi/g pCi/g 3.90 4.07 -0.028 0.118 0.208 0.100 Comments: Batch: OOL10-11-Sr-1 PerformedBy~ Date S:J.Lt Reviewed By:

2014-0265.xls V and V Date 11/14/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 305 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 1O~12 Strontium~90 Analysis Sheet Sample Number: 2014 - 0266 Sample

Description:

FSSP-OOL10-11-0003-F Fisherman's Channel Sample Collection DatefTime: __ 4/_2_81_1_4_8_:2_0_

Counting Instrument: _ _P_r_ot_e_an_ _ SIN:- -7109 ---

Calibration Due Date: 10/16/2014 g g Sample 0.0948 0.1009 Sample blank 0.00 Net Recovery 70.71

.. *, ., :::* .:f ~ 'r*

~: ~ ~~:

.. - ll,*

~*"' ~ -~.

~ *

.;:. _ii.;

~

. *couniin9;into.~rfl*att0~ *;~;~*:<:,~** ,. . \-:*::** . ~~ ~::,:;:1 ::": .... '

- - ,J!:'1

." ~!

Sample Volume Sample Cnt Time Bkg CntTlme Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (mln) Date/Time Factor date/time 3.02 60.00 . 60.00 5/14/14 10:27 4.82E-01 5/14/14 15:46 I

~)~?C

<>.~ilt;i

faia/ ;-;;}"

;

-

;>'II *

~.;~~~ r~< ~~.=:~=;~~ ;!.~: ~ ~:}\-:~=;~. ~:t:::;~~~}~*.-:~R,~~:-~i~S.~:!~ *:~ ~~}:~:;=:~~~*~ -~~:~~~~: .~~~..;*~~* ~-~- : \; ._; *;_~I Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCl/g pCi/g pCl/g pCi/g 3.68 3.85 -0.073 0.304 0.536 0.258 Comments: Batch: OOL10-11-Sr-3 eorto*m" By~o.* .S:Zi l~ " Reviewed By:

d-~ Date <--9.f-/t{

2014--0266.xls V and V Date 11/14113 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 306 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium"90 Analysis Sheet Sample Number: 2014 - 0267 General Information Sample

Description:

FSSP-OOL 10-11-004-F Fisherman's Channel Sample Collection Dateffime: __ 4_12_8/_1_4_8_:4_0_

Counting lnstrument: _ _P_r_o_te_a_n_ _ SIN: 7108 Calfbration Due Date: __1_0_12_9_:_/2_:_0_:_1_:_4_

g Sample 0.0959 0.1039 Sample blank 0.00 Net Recovery 92.73 Counting Information Sample Volume Sample Cnt Time Bkg Cn!Time Y-90 Extraction Ingrowth-Efficiency Sample Mld-Cnt Time '

g (min) (min) Datemme Faclor date/time 3.01 . 60.00 60.00 5/1 /14 15:03 9.55E-01 5/1/20 20:52 Count Data II Ftesults 1 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.55 4.07 -0.087 0.118 0.213 0.103 Comments: Batch: OOL10*11-Sr-1 PerformadB~ Date 5.::J 11' Reviewed By:

r

~~ Date ,:;-.-'] ~ H 2014-02si.x1s V and V Date 11f14f13 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 307 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: \ 2014 - 0268 General Information :

Sample

Description:

FSSP-OOL10-11-005-F Fisherman's Channel Sample Collection Dateffime: __ 41_2_81_1_4_8_:5_0_

Counting Instrument:* Protean S/N: 7108 Calibration Due Date: 10/29/2014 g g Sample 0.0958 0.1036 Sample blank 0.00 Net Recovery 90.42 Counting Information l Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/time 3.02 60.00 . 60.00 5/1/14 14:45 4.95E-01 5/1/14 21 :53 Count Data II Results :

Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.37 4.07 -0.233 0.230 0.418 0.202 Comments: Batch: OOL10-11-Sr-1

'°""m""'~ Date 5_.:J_ l~ RevlewedBy: ~ Date ~fJ-N 2014-0268.xfs V and V Date 11/14/13 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 308 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 StrontiumM90 Analysis Sheet Samplo Number: 2014 - 0269 General Information i Sample

Description:

FSSP-OOL10-11-006-F Fisherman's Channel Sample Collection Datefflme: __ 41_2_81_1_4_9_:2_0_

Counting lnstrument: _ _P_r_ot_e_an_ _ 10/29/2014 S/N:

- -7108

--- Calibration Due Date:

Sr Carrier Filter Tare Wt. Filler Gross Wt Sr Recovery mgfml ml g g (%)

Sample 5.12 1.00 0.0959 0.1032 84.62 Sample blank 0.00 Net Recovery 84.62 Counting Information i Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction tngrowth-Etriciency Sample Mid-Cnt Time g (min) (min) Date!Time Factor date/time 3.01 60.00 60.00 . 5/1 /14 15:30 4.97E-01 5/1/14 22:53 Co_unt Data II Re~mlts Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm} (cpm) pC!/g pCi/g pC!/g pCl/g 3.47 4.07 -0.214 0.247 0.448 0.216 Comments: Balch: OOU0-11-Sr-1 Performed B~ Date '5.].l4 Reviewed By: ~1fJ&i~ Date .<"~I)-;#

2014-0269.XIS V and V Dale 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 309 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0270 Sample Descript!on: FSSP-OO_L 10-11-0007-F Fisherman's Channel Sample Collection Date/Time: __ 4/_2_81_1_4_9_:0_0_

Counting Instrument: _ _P_r_o_te_a_n_ _ SIN:

- -7109

--- Calibration Due Date: 10/16/2014

-_,** .. : ., ... '* .-* .. " . . S R .. . . . .. . . . .- *'1

. . .. *:. ... .. ...,.:* * . .r e~qv_ery

_ - , ***

Sr Carrier Sr Carrier Added Filler Tare Wt. Filler Gross Wt Sr Recovery mg/ml ml g g (%}

Sample 5.12 1.00 0.0959 0.1022 73.Q3 Sample blank ... '"

I\\",\L:i . 0.00 Net Recovery 73.03

" .... * .. * * .. ._ :_ * :*.-.*.* ,* '_ .Coti'11tj,ng Information _"': _.- ,: ~ * . . -. . . . . .. .. : . * . c.,-.

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mld-Cnt Time 9 (min) (min) DatefTime Factor date/time 3.01 60.00 60.00 5/14/14 10:27 4.87E-01 5/14114 16:46 Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) {cpm) pCi/g pCifg pCi/g pCl/g 4.05 3.85 0.084 0.299 0.515 0.249 Comments: Balch: OOL10-11-Sr-3 Reviewed By:

~~Date e-,.,1~1tf 2014-0270.l<ls V and V Dale 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 310 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Strontium~90 Analysis Sheet Sample Number: 2014 - 0271

. Genera'! lnformatlan 1 Sample

Description:

FSSP-OOL 10-11-008-F Fisherman's Channel Sample Collection DatefTime: __4_12_8_11_4_9_:4_5_

Counting Instrument: _ _P_r_ot_e_an

__ SIN:- -7108 Calibration Due Date: 10/29/2014 Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 .. 0.0952 0.1020 78.82 Sample blank 0.00 Net Recovery 78.82

counii!lg Information '

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnl Time g (min) (min) Dateffime Factor date/time 3.00 60.00 60.00 5/1/14 15:20 5.03E-01 5/1/14 23:54 I

Count Data II Results I Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCifg pCi/g pCi/g 3.23 4.07 -0.316 0.259 0.476 0.230 Comments: Balch: OOU0-11-Sr-1 /

PerformedB~ Date c;;.J.l~ Reviewed By: ,. f/fd..~~ Date S-? 2014-0271. xis Vand V Date 11/14113 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 311 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0272

(

Sample

Description:

FSSP-OOL 10-11-0009-F Fisherman's Channel Sample Collection Date(Time: . 4/29/14 9:50 Counting lns!rument: _ _P_r_o_le_an __ S/N:

- -7109

--- Calibralipn Due Date: __1_0_11_6_12_0_1_4_

g g Sample 0.0949 0.1025 Sample blank Net Recovery 88.10

:*: ... *:-, *.**~~*

.;.. ~*,; ,., .,<. *":~ :.,:: .ou11t!119.**!"11,orma.t~on

...:,: *. ...,. _, -: " \*:*. -*:"*<~"1:*;":"'0*'.'\'0:. ...... ** ..... **: .;

.. ~ ~,. *,'.;_\Z

-..~ : ;, :!' ""1 * :.

- ."" ":. ~*' ~+; -~.- .;_: -::1 Sample Volume, Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mld-Cnl Time g (min) (min) Date!Time Factor date/lime 3.00 60.00 60.00 5/14/14 1.0:27 4.92E-01 5/14/1417:47

'*"~:~/-"'.-' . **-:Q:<?lin(b,~f~**.* ~:-*Jl:** ':i~ll~~ t-2~:!:~~;~>:~,:*;:~~~:r~i'.:;:*.:::*"' ?-~ :~tR~~-µi(s. ;* ::*~-~f ,;,~::~:;: :~*<>:i~: *:.*_~4;.r ~*:::

Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCl/g 3.28 3.85 -0.197 0.234 0.424 0.205 Comments: Batch: OOL10-11-Sr-3

,,...~.,~ Date K.:z I.*!~ Reviewed By: ~~ Date s; '?-f ~ I Lf 2014--0272.Xls Vand V Date 11/14/13 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 312 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0273 Sample

Description:

FSSP-OOL 10-11-010-F Fisherman's Channel Sample Collection DatefTime: __4_12_9_11_4_9_:2_5_

SIN: Calibration Due Date: 10116/2014 Counting Instrument: _ _P_r_o_le_a_n__

- -7109

.g Sample 0.0955 0.1031 Sample blank Net Recovery Sample Volume Sample Cnt Time Bkg CntTlme Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) DatefTime Factor dateftime 3.04 60.00 60.00 5/8/14 14:02 5.36E-01 5/9/14 6:35 Gross Sample Background Sr-90 Activity 2o Error MDA Le

{cpm) (cpm) pCl/g pCifg pCi/g pCifg 3.42 3.17 0.079 0.204 0.350 0.168 Comments: Batch: OOL10-11-Sr-2

' ~* .

Performed B~~ Dale 5.2( \4- Reviewed By:

2014-0273.xls V and V Dale 11/14/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 313 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014

0274

General Information ,;'

Sample

Description:

FSSP-OOL 10-11-011-F Fisherman's Channel Sample Collection Date/rime: __4_12_8_11_4_9_:5_5_

Counting lnstrumenl: _ _P_r_ot_e_an_ _ S/N: 7108 Calibration Due Date: 10/29/2014 Sr Recovery j Sr Carrier Sr Carrier Added Filter Tare WI. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample :.5.12 *'.'1.00 0.0960 0.1035 86.94 Sample blank 0.00 Net Recovery 86.94 Co_unting Information l Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Dale/Time Factor date/time 3.04 60.00 60.00 5/1/1415:45 5.05E-01 5/2/14 0:54 Ceunt Da~a II Results Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCitg pCifg pCifg pCl/g 3.62 4.07 -0.152 0.236 0.423 0.204 Comments: Balch: OOL10-11-Sr-1 Performed By~ Date '5:*:114- Revlewed By: .fl/dL~ Date \-9-/i/

2014-0274.xls V and V Dale 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 314 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0275 General Information i Sample

Description:

FSSP-OOL 10-11-012-F Fishermans Channel Sample Co!leclion Date!Time: 4/28/14 10:30 Counting Instrument: _ _P_r'-.ot_e_an_ _ S/N:

- -7109

--- Calibration Due Date: 10/16/2014 Sr Recovery i Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0967 0.1038 82.30 Sample blank 0.00 Net Recovery 82.30 Counting Information .l Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Da!e!Time Factor date/time 3.01 60.00 60.00 5/8/14 9:47 5.04E-01 518114 19:31

.. ... ,, ~ .. ~-~ . ..

Count Data Results I Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) {cpm) pCi/g pCl/g pCl/g pCi/g 3.48 3.17 0.114 0.236 0.402 0.193 Comments: Balch: OOL10-11-Sr-2 Pe~ormedBy~ Date l>'*l"Z..l 1:_ Reviewed By: JU~ Date $"-/;1~11 20144l275.xls V and V Date 11/14/13 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 315 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0276 Sample

Description:

FSSP-OOL10-11-013-F Fisherman's Channel Sample CollecUon DatefTime: __4_12_91_1_4_9_:4_0_

Counting Instrument: _ _P_r_o_te_a_n_ _ SIN: 10/16/2014

- -7109

--- Calibration Due Date:

Sample Sample blank Net Recovery 83.46

.*.: z'. **, ~~~-~ *. ;~ :~.** *;*.._: ~...: .. *.:: * : - t* >:-:[_: ;,;:_co.untfn9~1Q"{prmaHor:i ,,:* :.-. . . . . .':~<: ~. '.":-- *. ** .... ~.*:.:~= * *;* }: . ~.: :_: *:~:.'-**.~l Sample Volume Sample Cnt Time Bkg Cn!Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Datemme Factor dale/lime 3.01 .. 60.00 60.00 5/14/14 10:27 4.97E-01 5/14/14 18:47

"*' >*:**.:*;,.~~e*9):~*iif ~at~*L.:>:/:.:1t*:-:~;(..::**~,:=:;;;*~:~;,.:;*:. ;.*'.~; *:: ~-:~: <.~::::~/.~eslJ~t~-:.-.,:;:::'~*{" *;'f:~*::._.. :*:::~:-:~*:;:..~~:,t:::/ "::;

Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpin) . pC!lg pCi/g pCi/g pCi/g 3.37 3.85 -0.174 0.245 0.442 0.213 Comments: Batch: OOL10-11-Sr-3

'"'°'mod Syd~ Pate fi.2.l.l~ Reviewed By: ;:JM.~ Date C:-.:2{-(I/

2014-0276.xls V and V Date 11/14/13 HBPP-FSSP-OOL 10-11 & HBP,P-FSSP-OOL10-12 Page 316 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet

.. Sample Number: 2014 - 0277 Sample

Description:

FSSP-OOL10-11-014-F Fisherman's Channel Sample Collection Date/Time: 4/29/14 10:05 Counting Instrument:

- -Protean---- S/N: 7109 Calibration Due Date: 10/16/2014 g

Sample 0.1023 Sample blank 0.00 Net Recovery 73.03

~*.:. :*:: =.. ->. :* >>"~'.,:,: '*..:<=::.-*:-.:-:::_ . ::*:*c.Q.~~-~ihg-:ir~~*r_iil'atfo:p~*--**"* ,. ~-~,. *:**;* _::_, :**>*:**:*. _. <. -~- )-~~->-.:' *.;::

Sample Volume Sample Cnt Time Bkg CntTlme Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor dale/lime 3.00 60.00 60.00 5/14/14 10:31 5.02E-01 5/14/14 19:47 c::.'.:. ~~-- .:* i;ci_.~il_ti_{:>~!~.-- -~ *:<>:;f-* *,:'.*)~;~ ;<}: ( ~-$.7:~~'-:-t::,;S:;;/ ?~,~~~_lt~i<*,~ ~'.}*:*.: :!{.>::* **<<,;::*:: <*\;'\. \>:,j 0

Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCl/g pC!/g pCl/g pCi/g 3.53 3.85 -0.130 0.282 0.502 0.242 Comments: Batch: OOL10-11-Sr-3

""~"*~ Date f;it.~JJ4- Reviewed By: ~~Date

,,-- s-;11-ttl 2014-0277J<ls Vand V Date 11/14113 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 317 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0278 General Information .,

Sample

Description:

FSSP-OOL 10-11-015-F Fishermans Channel Sample Collection Date/Time: __ 4_12_8!_1_4_8_:2_0_

Counting Instrument: _ _P_r_ot_e_an_ _ S/N: 7109 Calibration Due Dale: 10/16/2014 Sr Recovery Sr Carrier Sr Carrier Added Filter Tare Wt. Filler Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 . 1,00 0.0955 0.1004 56.80 Sample blank ...*. 0.00 Net Recovery 56.80 Counting. Information Sample Volume Sample Cnt Time Bkg Cnt Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/time 2.99 60.00 60.00 5/8/14 9:47 5.09E-01 5/8/14 20:31

.. II ....* . .. ..

'.)-'*: *coqn't data

~ ~: *~*

*. *.":1~.e~~ii1is ~"'., '

Gross Sample Background Sr-90 Activity 2o Error MDA le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.83 3.17 0.347 0.349 0.581 0.279 Comments: Batch: OOL10-11-Sr-2 Performed By~ Date 'S'. l.Z...lt Reviewed By: ~~ Date S-1.7-l'f 2014-0278.Xls Vand V Dale 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 318 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0279 -

General Information J Sample

Description:

FSSP-OOL10-11-016-F Flshermans Channel Sample Collection DatefTime: 4/29/14 9:30 Counting Instrument: SIN: 7109

- -Protean

Calibration Due Date: 10/16/2014 g g Sam le 0.0957 0.1020 Sample blank 0.00 Net Recovery 73.03

' '

Counting i'nformation ,

Sample Volume Sample Cnt Time Bkg CntTfme Y-90 Extraction Ingrowth-Efficiency Sample Mld-Cnt Time g {min) {min) DatefTime Factor date/time 3.01 60.00 60.00 5/8/14 14:02 5.24E-01 5/9/14 4:05 Gross Sample Background Sr-90 Activity 2cr Error MDA Le (cpm) {cpm) pCi/g pCifg. pCi/g pCi/g 3.88 3.17 0.280 0.263 0.436 0.209 Comments: Batch: OOL10-11-Sr-2 Performed By~ Date '5".l2.l4 Reviewed By: -~~~ Date .<;'~/tJ-/t/

2014-0279.xls Vand V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 319 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0280

* * - General Information * ;

Sample

Description:

FSSP-OOL 10-11-017-F Fishermans Channel Sample Collection Date/Time: 4/29/14 11 :00 Counting Instrument: Protean S/N: 7109 Calibration Due Dale: 10/16/2014 ml g Sample 1.00 0.1015 Sample blank 0.00 Net Recovery 62.60

. ~*'. '

Counting Information i Sample Volume Sample Cnt Time Bkg Cn!Tlme Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Datemme Factor date/time 3.02 60.00 60.00 5/8114 14:02 5.26E-01 5/9/14 4:34

=*. . . _ . . ., *. .. .... *:1

~

count Data . ~i.'.*,*11 *:'};*. ",:*-'.'":*.;' -\; . ,. * - '* :~:* ;R~sults " ~ ~" ~ ~ ,,: ' -:. ~.

Gross Sample Background Sr-90 Ac!ivily 2o Error MDA Le (cpm) (cpm) pCl/g pC!/g pCi/g pCi/g 2.95 3.17 -0.098 0.283 0.505 0.242 Comments: Batch: OOL10-11-Sr-2 Performed By:~~ Dale ~.L::l. Reviewed By:

,~~- Date ,t;'~/;1../1/

2014-0280,xls Vand V Date 11114113 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 320 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Strontium"90 Analysis Sheet Sample Number: 2014 - 0281

** General Information l Sample

Description:

FSSP-OOL 10-11-018-F Fishermans Channel Sample Collection DatefTime: 4/28/14 12:00 Counting Instrument: Protean S/N: 7109 Calibration Due Date: 10/16/2014 ml g g Sample 1.00 0.0956 0.0994 Sample blank Net Recovery 44.05 Counting Information i Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction lng!owth-Efficiency Sample Mid-Cnt Time g (min) (min) Date!Time Factor date/time 3.05 60.00 60.00 5/8/1414:02 5.31E-01 5/9/14 5:34

.. * *coun.t"oata ~- -.. **," , II ,... * .;. ** . :* -: .. :~ . .. **Results *... *<<,..~~" : :, . ~ .

- 1

Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCl/g pCi/g pCi/g 3.13 3.17 -0.021 0.401 0.704 0.338 Comments: Batch: OOL10-11-Sr-2

!Pe~ormed By~ Date 5.!2.!4 Reviewed By: w~

,.- Date .>--/P~llf 2014-0281.xls Vand V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 321 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0282

General Information :

Sample

Description:

FSSP-OOL 10-11-019-F Flshermans Channel Sample Collection Date/Time: 4/28/14 11 :30 Counting Instrument: _ _P_r_o_te_a_n__ S/N:

- -7109

--- Calibration Due Date: 10/16/2014 Sr Re9overy i

' Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0961 0.1014. 61..44 Sample blank 0.00 Net Recovery 61.44 Counting Information !

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mld-Cnt Time g (min) (min) Date/Time Factor date/time 3.01 60.00 60.00 5/8/14 14:02 5.22E-01 5/9/14 3:33

, ****,.Count Data

11 * * * *Res Li its '

Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) {cpm) pCi/g pCi/g pCi/g pCl/g 3.63 3.17 0.218 0.308 0.520 0.250 Comments: Batch: OOL10-11-Sr-2 Performed By:~ Date S:-IZ*I~ Reviewed By:~~ Date S"'-tP.-1 r/

2014-0282.xls Vand V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 322 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014

0283

General Information

Sample

Description:

FSSP-OOL 10-11-020-F Rshermans Channel Sample Collection DatefTime: 4/28/14 11:05 Counting lnstrument: _ _P_r_ot_e_an_ _ S/N:

- -7109

--- Calibration Due Date:

10/16/2014 g g Sample 0.0964 0.1028 Sample blank Net Recovery Counting Information '

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) DatefTime Factor date/time 3.02 60.00 60.00 5/8/14 14:02 4.67E-01 5/8/14 16:28

.. *;;;;*,: ., '* '. .:11 * .. .,., ...... .. ~* ~ .*. ** .. , .,

Count Data Re'sli1is .: '"<;: r Gross Sample Background Sr-90 Activity 2cr Error MDA Le (cpm) (cpm} pCVg pCi/g pCi/g pCl/g 3.38 3.17 0.093 0.279 0.480 0.230 Comments: Balch: OOU0-11-Sr-2 PerionnedBy~ Date S. ( 2.~1: Reviewed By: f?l1t,d.'-:J Date <"'~/;J~/ t/

2014-0283.>ls V and V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 323 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0283 RC

'Genei:al Information : :* * '

Sample

Description:

FSSP-OOL10-11-020-F Flshermans Channel Sample Collectlon Date!Tlme: 4/28/14 11 :05 Counting Instrument: _ _P_r_ot_e_an_ _ S/N: 7109 Calibration Due Date: 10/16/2014 Sr Recovery 1 j

Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross WI Sr Recovery mg/ml ml g g (%)

Sample 5.12 .. 1.00 0.0964 0.1028 74.19 Sample blank 0.00 Net Recovery 74.19 j

. Counting lnformati'orJ Sample Volume Sample Cnt Time Bkg Cn!Time Y-90 Extract!on Ingrowth-Efficiency Sample Mld-Cn! Time g (min) (min) Date/Time Factor date/time 3.02 60.00 60.00 5/8/14 14:02 4.73E-01 5/8/14 17:30

' ' ., ~ - . *11****,*,;*.**.-.. ... * ""a:**;~*~ \\ ,,.w"c,,' *" .. .. ' ~

~ ~ ~ .'

Co\f nt .Data .. . . ~e~1.ilts '

Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCl/g pCi/g pCi/g 3.67 3.17 0.213 0.282 0.474 0.228

,Comments: Batch: OOU0-11-Sr-2 Performed By:~ Data '5'*l?..l1::: Reviewed By: .-Ud~ Data S'-f;l*/t/

2014-0283 RC.xis Vand V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 324 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Strontium-90 Analysis Sheet Sample Number: 2014

0284 General Information :

Sample

Description:

FSSP-OOL10-12-001-F Land Adj. to Fisherman's Channel Sample Collection Datemme: 4/28/14 9:05 Counting Instrument: Protean S/N: 7109 Calibration Due Date: 10/16/2014 g g Sample 0.0970 0.1032 Sample blank Net Recovery 71.87 Counting Information

~ample Volume Sample Cnt Time Bkg Cnt Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/time 3.04 60.00 60.00 5/12/1410:10 4.90E-01 5/12114 17:04

**cou~~t.bata * : *.-*,. ,.,/II .'! '. *' *:*~.:. *.'~ . ;

. .. ~ ;

Results

.. * .*.. ~ . !: *.

Gross Sample Background Sr-90 Activity 2cr Error MDA Le (cpm) (cpm) pCi/g pCi/g pCJ/g pCi/g 3.75 3.50 0.105 0.287 0.492 0.237 Comments: Balch: OOL10-12-Sr-1 PerformedB~ Date s.1'3.I~ Reviewed By; ~~

7-Date s~Jtf-/'/

2014-0284.xls Vand V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 325 of 468

Attachment 3*Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0285

. General Information ;

Sample

Description:

FSSP-OOL10-12-002-F Land Adj. to Fisherman's Channel Sample Collection Dateffime: __ 41_2_81_1_4_9_:1_0_

Counting lnstrument: _ _P_ro_t_e_an_ _ S/N:

- -7109

--- Calibration Due Date: 10/16/2014

.. Sr Recovery j Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0963 0.1039 88.10 Sample blank -~ '>***

0.00 Net Recovery 88.10 Counting Information '

Sample Volume Sample Cnt Time Bkg CntTfme Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date!Time Factor date/time 3.00 60.00 60.00 5/12/1410:10 4.95E-01 5/12114 18:05

",, ~ ~" .. :

Cou*nt Data .. II : "<< *Results

II Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCl/g pCi/g pCi/g pCi/g 3.23 3.50 -0.092 0.226 0.403 0.194

~

Comments: Batch: OOL10-12-Sr-1 Perfo~med By~,) Date s:.13.1~ Reviewed By: .~@~ Date s~/'{~!t/

2014-0265.xls Vand V Date 11/14/13 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 326 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0286 Sample

Description:

FSSP-OOL 10-12-003-F Land Adj. to Fisherman's Channel Sample Collection Date/Time: 4/30114 13:15 Counting Instrument: Protean S/N: 7109 Calibration Due Date: 10/16/2014 g g Sample 0.0965 0.1030 Sample blank Net Recovery 75.35

.::-.;, 'J* :* _.,~- ..... -<* :.:-.',' *.*:::-;,; *. **::. ,:,:**~*.; :*

pqq_1.friti*ri9~1nfqriJiaii9*it: :,--."~_*::. ;~:: -_*--:* -*: :':"' ::~ .~: . . ~-~:-:::--~:,.:* >-.:~,_:

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (m!n) (min) Date/Time Factor dateltime 3.01 60.00 60.00 5115/14 10:27 4.88E-01 5/15/14 16:56 s;_; ~~>*"~.:~¢.-9!.i~fo~t-~ :-:::*:*:*: ~:~:*11::~t*:;*~:.":.;_~}~::;.' ;~:-/::::~ .~ _.-"';:,~J~~~~uJt~: **~~'-* ::::*:;lt;:**_::.\* >:. :~-~"=:.~':. ".;'.*[~i Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.40 3.20 0.081 0.265 0.456 0.219 Comments: Batch: OOL10-12-Sr-3

""'=***~ Date £°,21.I~ Reviewed By: flffj~

Date S:-::Z I-le/

2014-0288.xls Vand V Date 11f14/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 327 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0267 General Information " i Sample

Description:

FSSP-OOL 10-12-004-F Land Adj. to Fisherman's Channel Sample Collection Date!Tfme: 4/30/1413:25 Counting Instrument: _ _P_r_ot_e_an_ _ SIN: 7109 Callbration Due Date: 10/16/2014 Sr.Recovery ; l Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0961 0.1035 85.78 Sample blank 0.00 Net Recovery 85.78

]

Counting !~formation Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g {min) (min) Date/Time Factor date/tline 3.00 60.00 60.00 5/12114 10:10 5.05E-01 5/12114 20:06

.count Data .. ., '***... II *'-' "" .*. .. .;""~. ~-: _._

"*":* Resuits *~. "o.\ ..

Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) {cpm) pCi/g pCl/g pCi/g pCl/g 4.32 3.50 0.283 0.245 0.406 0.195 Comments: Batch: OOL10-12-Sr-1 PertonnedBy~ Date S. !;3.L~ Reviewed By: .fl:!fL~ Date .S-1'/-/ r/

2014-028].xls Vand V Dale 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 328 of 468 L___

.Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0288

General Information ~

Sample

Description:

FSSP-OOL10-12-005-F Land Adj. to Fisherman's Channel Sample CollecUon Dateffime: 4/30/14 13:30 Counting Instrument: Protean S/N: 7109 Calibration Due Date: 10/16/2014 g g Sample 0.0950 0.1033 Sample blank Net Recovery Counting Information '

Sample Volume Sample Cnt Time . Bkg Cn!Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/time 3.02 60.00 60.00 5/12/14 10:10 5.10E-01 5/12/14 21 :06 count riata *, ,, :*<**11

~ ~

'i~-~. ~ ...... ~.: : * ~ ...* "'~ ~ ~* ~. *~

~ ;_,

~ ~

Results ....

Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 4.27 3.50 0.233 0.215 0.356 0.171 Comments: Balch: OOL10-12-Sr-1 Performed By~ Date 'S.1;3,1~ Reviewed By: J?J'~ Date ~*l'ld'f 2014-0288.xls V and V Date 11/14/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 329 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0289

General lnfor.mati'on ;

Sample

Description:

FSSP-OOL 10-12-006-F Land Adj. to Fisherman's Channel Sample Collection DalefTime: 4/30/14 13:17 Counting Instrument: _ _P_r_ol_e_an_ _ S/N:

- -7109

--- Calibration Due Date: 10/16/2014 g

Sample 0.1042 Sample blank 0.00 Net Recovery 93.89

Cour:itinQ _Information __ ;

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/lime 2.99 60.00 60.00 5/12114 10:10 5.15E-01 5/12/14 22:07 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCifg pCi/g pCi/g pCifg 3.93 3.50 0.135 0.215 0.365 0.176 Comments: Batch: OOU0-12-Sr-1 Performed By:~ Date 5.1"3.l4 Reviewed By: ,~Date .SV'?*lr/

2014-0289.xfs V and V Date 11/14(13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 330 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0290 Sample

Description:

FSSP-OOL 10-12-007-F Land Adj. to Fisherman's Channel Sample Collection Da!efTime: 4/30/14 13:50 Counting Instrument: _ _P_ro_te_a_n_ _ S/N: 7109 Calibration Due Date: 10/16/2014 Sr Carrier Sr Carrier Added Filter Tare WI. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0952 0.1019 . 77.67 Sample blank *'" ..... ..., 0.00 Net Recovery 77.67 Sample Volume Sample Cnt Time Bkg Cn!Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cn! Time g (min) (min) Daterrime Factor date/time 3.01 60.00 60.00 5/15/14 10:31 4.77E-01 5/15/14 14:50 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCi/g pCilg pCi/g 3.50 3.20 0.121 0.265 0.453 0.218 Comments: Balch: OOL10-12-Sr-3 Date '$.2..l. l4=

2014-0290.>ls Vand V Date 11/14/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 331 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0290 RC Sample

Description:

FSSP-OOL10-12-007-F Land Adj. to Fisherman's Channel (Recount)

Sample Colleci!on DatefTime: 4/30/14 13:50 Counting lnstrument: _ _P_r_o_te_a_n__ S/N: 7109 Calibration Due Date: 10/16/2014 Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0952 0.1019 77.67 Sample blank ..*. :i,;f:\\ .,,, ..* 0.00 Net Recovery 77.67 Sample Volume Sample Cnt Time . Bkg Cnt Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/time 3.01 60.00 60.00 5/15/14 10:31 4.83E-01 5/15/1415:56 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.32 3.20 0.047 0.258 0.447 0.215 Comments: Batch: oouo-12-sr-3 Reviewed By: ffJ:!l}l~ Date t';'-:JCJ-llf 2014-0290 Recounlxls Vand V Date 11114/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 332 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium"90 Analysis Sheet Sample Number: 2014 - 0291 General Information !

Sample

Description:

FSSP-OOL 10-12-008-F Land Adj. to Fisherman's Channel Sample Collection Date!Time: 4/30/14 14:10 Counting Instrument: _ _P_r_ot_e_an_ _ SIN: 7109 Calibration Due Date: 10/16/2014 Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mgfml ml g g (%)

Sample . 5.12 1.00 0.0964 0.1045 93.89 Sample blank 0.00 Net Recovery 93.89 Counting Information '

Sample Volume Sample Cnl Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) DatefTime Factor dale/time 3.03 60.00 60.00 5/12/14 10:10 5.24E-01 5/13/14 0:07

.: * * :C9urit Data ** : *<:**::II "".: \. ' *'. ~:. ' ~ *,. ... ::: .....~ . * *:** .: ..;: .:Results =~ *::.-:

Gross Sample Background I Sr-90 Activity 2o Error MDA I le (cpm) (cpm) pCi/g pCi/g pCl/g pCl/g 3.53 3.50 0.010 0.203 0.354 0.170 Comments: Batch: OOL10-12-Sr-1 Performed B~ Date '£.C?. li Reviewed By: ,~Date .S-:-/'l* l'f 2014-0291.xls V and V Date 11/14/13 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 333 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Strontium~90 Analysis Sheet Sample Number: 2014 - 0292 Sample

Description:

FSSP-OOL 10-12-009-F Land Adj. to Fisherman's Channel Sample Collecllon Dateffime: 4/30/14 14:00 Counting Instrument: Protean S/N: 7109 Calibration Due Date: 10/16/2014 g

Sample 0.1021 Sample blank 0.00 Net Recovery 75.35

.* . q<i'a0,Hn9 1r1tormation ** * ..

~ * : ~ **.~~~"!'~:s*. * ~.*>;

.. .. ;-." . ~~

:*. : ~:

,.. ....: ~ . ..

" ' : "' \ *.:. < -* :.:: ' * "

I Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Dateffime Factor date/time 3.00 60.00 60.00 5/15/14 10:30 4.98E-01 5/15/14 18:57

<:-;~:~,>~ ~t.oiJn(b~Ja_: *:;~: . . *: :*-. ~"11-.:;~t: *. .,<)~?rt: ~:.:*~:<.~,::\*}~~:~. ~~~.f!)Js' . :'Y*:ii~::.:~:r} *i~ ?' **: *. *-:*:;:/**';*;.\~~I Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCifg pCl/g pCi/g 3.20 3.20 0.000 0.257 0.449 0.216 Comments: Batch: OOL10-12-Sr-3 Performed B~ Date '£.2£>,J4-- Reviewed By: ~~ Dale 5-2~--(</

2014-0292.>ls V and V Dale 11114/13 HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 334 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Strontiumw90 Analysis Sheet Sample Number: 2014 - 0293 Sample

Description:

FSSP-OOL10-12-010-F Land Adj. to Fisherman's Channel Sample Co!lectlon DatefTime: 4/30/14 13:05 Counting Instrument: Protean S/N: 7109 Calibration Due Date: 10/16/2014 g g Sample 0.0959 0.1029 Sample blank Net Recovery 81.14

\:' >* -.t*; :'~:-':- ::': ...,. _*;, :-'~~-:,;_,/:{".::**co'unting.. Jnt:orrrlati_9~.\-'. -': :--* v* _: ~ .- .:'-f. ;: ~.,. ..'7***. "~5., *~_"":"**.

I

~

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Datemme Factor date/time 3.03. 60.00 60.00 5/15/1410:33 5.02E-01 5/15/14 19:57 x**:.:~}'.-'.*::~:c.9\Ji:i'fPa!? **\:?;*~*:*111':~~;.:~\~::*~ . ;: . ::.-:\;*:::*.::::~,_?:.'p1~"--~;~~ii~'.it~;~?f~':;;:;;*-~:y.'::: ':'*:*t~r;~:::)t*;*~;;.*-::.~1 Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCl/g 3.37 3.20 0.061 0.237 0.409 0.196 Comments: Balch: OOL10-12-Sr-3 PerformedBy~Date '5W!.:1: Reviewed By: ,1'Ld~Pr;_~ Date S-::iO-(t/

2014-0293.xls V and V Date 11/14/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 335 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium"90 Analysis Sheet Sample Number: 2014 - 0294 Sample

Description:

FSSP-OOL 10-12-011-F Land Adj. to Fisherman's Channel Sample Collection Datefflme: 4/30/14 13:05 Counting lnstrumenl: _ _P_ro_te_a_n_ _ SIN: 7109 Callbralion Due Date: 10/16/2014 Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0962 0.1025 73.03 Sample blank 0.00 Net Recovery 73.03 Sample Volume Sample Cnt Time Bkg Cn!Time Y-90 Extraction Ingrowth-Efficiency Sample Mld-Cnt Time g (min) (min) Daterrime Factor date/lime 3.00 60.00 60.00 5/15/14 10:28 5.08E-01 5/15/14 20:58 Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCl/g 3.38 3.20 0.074 0.263 0.454 0.218 Comments: Batch: OOL10-12-Sr-3 Pelformed By~ Dale .5.20.l4 Reviewed By:

2014-0294.xls V and V Date 11/14/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 336 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0295 Sample

Description:

FSSP-OOL 10-12-012-F Land Adj. to Fisherman's Channel Sample Collect!on DatelTime: 4130/1414:15 Counting Instrument: _ _P_r_o_le_a_n_ _ SIN: 7109 Calibration Due Date: 10/16/2014 Sr Carrier Sr Carrier Added Filler Tare Wt. Fi!ter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0960 0.1020 69.55 Sample blank ' .\£;, 0.00 Net Recovery 69.55 Sample Volume Sample Cnt Time Bkg CntTlme Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor dale/time 3.00 60.00 60.00 5/15/1410:37 5.12E-01 5/15/14 21 :58 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.23 3.20 0.014 0.271 0.473 0.227 Comments: Batch: OOU0-12-Sr-3 Performed By~ Date z 2f) 14 2014-0295.xls Vand V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 337 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0296 Sample

Description:

FSSP-OOL10-12-013-F Land Adj. to Fisherman's Channel Sample Collection Date/Time: 4/30/14 14:14 Counting Instrument: _ _P_r_o_te_a_n_ _ SIN: 7109 Calibration Due Date: 10/16/2014 g g Sample 0.0960 0.1017.

Sample blank 0.00 Net Recovery 66.07

-:*, * , , *:.::.-;*;l **, ::<~*:.:,\*:x*:-:. * ".:*:q:\ *:::'c.<>ii6tiilg 1ilf'9rm~lti9n *. . t:/:-.~:r*:*'~**':: '.: *:-.,:;--~~:;r' \-.* _,,. *-~* '"*" ~<.::_* ";~1 Sample Volume Sample Cnl Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) DatefTlme Factor date/time 3.00 60.00 60.00 5/15/14 10:38 5.16E-01 5/15/14 22:59

(:~?::~ ;} *,:~¢9~\l:fP,-~t~i\.'. *. ';;:*'.tJI ~~'~'.:*:>~';_:>._: t:~:::.;;.:~;\~?~~~** -~\'.')* ~ ~is.4!j$J: ~):~t*~~t~i?*':~~-,~~(;C-.~< :;,<;~<:~*;;;~!

Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g pCl/g pCl/g pCi/g 3.47 3.20 0.118 0.288 0.493 0.237 Comments: Batch: OOL10-12-Sr-3 Performed B~ Date 5.Ul.l4 Reviewed By: ,~A?/1,~ Date S-,;<o* (</

1014-0296.xls V and V Date 11/14113 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 338 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0297 Sample

Description:

FSSP-OOU0-12-014-F Land Adj. to Fisherman's Channel Sample Collection Dateffime: 4/30/1414:11 Counting Instrument: Protean S/N: 7109 Calibration Due Date: 10/16/2014 9

Sample 0.1034 Sample blank Net Recovery Sample Volume Sample Cnt Time Bkg Cn!Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Datemme Factor date/time 3.02 60.00 60.00 5!15/14 12:51 5.15E-01 5/16114 0:59 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCilg pCi!g pCi/g 3.78 3.20 0.224 0.257 0.431 0.207 Comments: Batch: ooL10-12-Sr-3 Performed B~ Date :5.Zt>.14:

2014-0297.xls V and V Dale 11114113 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 339 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Strontium-90 Analysis Sheet Sample Number: 2014

0298 Sample

Description:

FSSP-OOL 10-12-015-F land Adj. lo Fisherman's Channel

Sample Collection Date/Time; 4/30/14 14;20 SIN: 10/16/2014 Counting Instrument: ___ P_ro_te_a_n_ _

- -7109

--- Calibration Due Date:

Sr Carrier Sr Carrier Added Filler Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12

1.00 0.0953 0.1012 68.39 Sample blank 0.00 Net Recovery 68.39 Sample Volume Sample Cnt Time Bkg Cnt Time Y-90 Extractron Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/time 3.02 60.00 60.00 5/15/14 10:35 5.21E-01 5/15/14 23:59 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.55 3.20 0.147 0.275 0.469 0.225

\

Comments; Balch: OOU0-12-Sr-3 Date 'Z>.20,/ 4 Reviewed By: ~Date S~.:101/f/

2014-0298.xls V and V Date 11114113 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 340 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Strontium~90 Analysis Sheet Sample Number: 2014 - 0299 Sample

Description:

FSSP-OOU0-12-016-F Land Adj. to Fisherman's Channel Sample Collection DatefTime: 4/30/14 14:20 Counting Instrument: ___ P_ro_le_a_n_ _ S/N: 7109 Calibration Due Date: 10/16/2014 g g Sample 0.0960 0.1030 Sample blank 0.00 Net Recovery 81.14 Sample Volume Sample Cnt Time Bkg Cn!Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) DatefTime Factor date/lime 3.00 60.00 60.00 5/15/14 10:32 5.31E-01 5/16/14 2:00 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm) (cpm) pCi/g pCi/g pCi/g pCi/g 3.63 3.20 0.151 0.231 0.391 0.188 Comments: Batch: OOL10-12-Sr-3 Performed By:~. Date 'S.21> 14 Reviewed By: , /lf2;4~~ Date S.:1.61/</

2014*0299.x!S V and V Dale 11/14/13 HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 341 of 468 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014 - 0300 Gene~al lnformatfon ;

Sample

Description:

FSSP-OOL10-12-017-F Land Adi. to Fisherman's Channel Sample Collection DatefTim_e: 4/30/14 14:25 Counting Instrument:

- -Protean

S/N: 7109 Calibration Due Date: 10/16/2014 g g Samp!e 0.0947 0.1020 Sample blank Net Recovery

Cpunting ,lnform~tion J Sample Volume Sample Cnt Time Bkg Cn!Time Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min} Date/Time Factor dale/time 3.02 60.00 '60.00 5/14/14 10: 29 5.12E-01 5/14/14 21 :48 Gross Sample Background Sr-90 Activity 2o Error MDA Le (cpm} (cpm) pCi/g pCi/g pCi/g pCi/g 3.73 3.85 -0.040 0.240 0.422 0.204 Comments: Batch: OOL10-12-Sr-2 Reviewed By: Date 5-'*:5'-/

2014-0300.xls Vand V Date 11/14/13 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 342 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Strontium-90 Analysis Sheet Sample Number: 2014

0301

General Information ~

Sample

Description:

FSSP-OOL10-12-018-F Land Adi. to Fisherman's Channel Sample Collection DatefTime: 4/30/14 14:31 Counting Instrument: _ _P_r_ot_e_an_ _ S/N:

- -7109

--- Calibration Due Date: 10/16/2014 g g Sample 0.0951 0.1022 Sample blank 0.00 Net Recovery 82.30 Counting Information Sample Volume Sample Cnt Time Bkg CntTlme Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date/Time Factor date/time 3.01 60.00 60.00 5/14/14 10:29 5.16E-01 5/14/14 22:49

.. '":>~

Count Data II "Results Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pC!/g pCi/g pCi/g pCi/g 3.23 3.85 -0.217 0.237 0.431 0.208 Comments: Batch: OOL10-12-Sr-2

'"""mod"'~ Date S-IS.\~ Reviewed By: fd'd~ Date S-!S--/t(

2014-0301.xls VandVDate 11/14/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 343 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Strontium"90 Analysis She et Sample Number; 2014 - 0302 General Information Sample

Description:

FSSP-OOL 10-12-019-F Land Adj. to Fisherman's Channel Sample Collection Date/Time: 4/30/14 14:31 Counting lnstrument: _ _P_r_ot_ea_n_ _ SIN: 7109 Calibration Due Date: 10/16/2014 Sr Recovery Sr Carrier Sr Carrier Added Filter Tare Wt. Filter Gross Wt Sr Recovery mg/ml ml g g (%)

Sample 5.12 1.00 0.0964 0 .1032 78.82 Sample blank 0.00 Net Recovery 78.82 Counting Information Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction lngrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Dale/Time Factor date/time 3.01 60.00 60.00 5114/1410:29 5. 21E-01 5/14/14 23:49

~:_-- Count Data II .* * * -

Resul ts '

Gross Sample Background Sr-90 Activity 2cr Error MDA Le (cpm) (cpm) pCi/g pCi/g pCl/g pCl/g 3.22 3.85 -0.231 0.245 0 .446 0.215 Comments; Saleh: OOL10-12-Sr-2 Reviewed By: ~'d~oate s--1.s--1tf 2014-0302.xls Vand V Date 11114/13 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-1 2 Page 344 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 StrontiumM90 Analysis Sheet Sample Number: 2014 - 0303

. G_eneral Information ;

Sample

Description:

FSSP-OOL 10-12-020-F Land Adj. to Fisherman's Channel Sample Collection DatefTime: 4130/14 14:40 Counting Instrument: _ _P_r_o_te_a_n__ SIN: 7109 Calibration Due Date: 10/16/2014 ml Sample 1.00 Sample blank 0.00 Net Recovery 83.46 Counting Information ]

Sample Volume Sample Cnt Time Bkg CntTime Y-90 Extraction Ingrowth-Efficiency Sample Mid-Cnt Time g (min) (min) Date!Time Factor date/time 3.02 60.00 60.00 5/14/14 10:31 5.25E-01 5/15/14 0:49 Count .Cata II *

Results *. * :

Gross Sample Background Sr-90 Activity 2a Error MDA Le (cpm) (cpm) pCi/g. pCi/g pCi/g pCl/g 3.52 3.85 -0.113 0.234 0.417 0.201 Comments: Balch: OOL10-12-Sr-2

""""""' 'Y~ "'"' \;.IC:.14 Reviewed By: ,itjJ~ Date S'""-1~~;.

2014-03-03.xls V and V Date 11/14113 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 345 of 468

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Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12

          #111 ILaboratories LLc a member of The GEL Group INC                                                            PO Box 30712   Charleston, SC 29417 2040 Savage Road   Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gel.com May30, 2014 Ms. Dee Anderson Pacific Gas and Electric, Humboldt Bay Power Plant 1000 King Salmon Avenue Eureka; California 95503 Re: Final Status Survey Work Order: 348598

Dear Ms. Anderson:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on May 13, 2014. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504. Sincerely, Erin Trent Project Manager Purchase Order: 3500953353, Line item #4 Enclosures FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 356 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Table of Contents I l Case Narrative ...................................................................................... 1 Chain of Custody and Supporting Documentation............................... 3 Laboratory Certifications .................................................................... 10 Radiological Analysis ............... ~ ......................................................... 14 Sample Data Summary ............................................................... 34 Quality Control Data.................................................................. 43 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 357 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Case Narrative ( Page 1of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 358 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Case NmTative fol' Pacific Gas and Electlic Company SDG: 348598 May30,2014 Labo1*atorv Identificntion: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summn1y Sample Receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on May 13, 2014 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any 'lrisible signs of tampering or breakage. Please see attached email regarding required analyses and MDCs. Sample ldentificntion The laboratory received the following samples: Labomton* ID Client ID 348598001 FSS 0294 OOLlO 12 011 F S 348598002 FSS-0302 OOLI0-12-019-F-S 348598003 FSS 0266 OOLlO 11 003 F S 348598004 FSS-0279 OOLl0-11-016-F-S Case Nal'mtive Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package Dntn Package The enclosed data package contains the following sections General Narrative, Chain of Custody and Supporting Documentation, and data from the following fractions Radiochemistry Erin Trent Project Manager Page2 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 359 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Chain of Custody and Supporting Documentation Page 3 of 58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 360 of 468

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                 \i'orl: Order#                                                                                                                                                                                                                                                  EXC..'.l\'3tion Permit ;j' Cllem N~nie: PG & F.                                                                                                     707-444-0746                                                            Sam11lc Anals*i* Requested j5) (fill in the nunibcr of contai11e1s for each tt::il)

Project/Site Name: HBPP Fa~ #:707-441-2671 Slioald 1l1i> i.'.! <- l'r~m-,-01i,*c Typo (6) f--~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~--~~~~-1..,mplobe Aclcln.-,,;::1000 King Salmon. E~reka. Ca 95503 coasidor<d:

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FSS-0294 I OOLJ 0-12-011-F-S 4130l2-0l4 N so x x x OJ 13:40 N 2 LJ LJ fSS-0302 (J) (J) OOLl 0-12-019-F-S 4/3012014 14:2g N N so x 2 x x LJ 6 FSS-0266 ~ ru 0 0

  ~              OOL 10-11-003-F-S                                                                                        41281201-1                   S:2~      N           N         so          x                    2     x x                                                                                                                      ::::r 3

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w Qo OOLI0-11-016-F-S 412912014 9:30 N N so 1-'--=-"--~--"~..;;_~~~~~~~~~~-'--"-;;;;..;.;""-'--'--,..-~--'~~'------'-...;::._;:-1.-'-'C~-~r-::---L...:..:.....L.;:.:.....1~-'-~'---'"~....I------'-~"'---'~~~~~~----~ x 2 x x r I ru TATRequ~ted:Normnl: IFa~Results: J.e,d~ OJ c-Rush: Snecif\': tSubiml<*Smmm'<l Yes I No Cin:ldMi**crah!c: r:orA ! <X:Summar.* 1 Ltwl I I Level2 I IBeD 1 LJ LJ oru Remnrli<J: Are there crny known hazards applicahll! to tlr~e .mmp!P.s 7 If so, please list tire lummls. Tflu11kyou PG&E (Samples c011 he discarded npproprial<!{J~ ill case of emergency ill (J) plea.fe t:all 707-444-0/:.'09 *HA11alyze for uttucl1ed list of 1mclides as listed 111 /etter a11uclledfro111 FSS e11;:il1eer. SOIL FOR GAMM1t ANAL J'SJS HAS AlRJ:."rlDY Bl:."EN (J) LJ PROCESSED/DRIED, Pl.EASE COUNT JN Tl!E CONFIGURT/ON AS SENT TO YOU. **"* ~ I 6 OJ 0 Chain or Custody Signalure.* Sample Shipping and Delim-:i* Details LJ

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Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 JFisherm:ms Channel :md Adjacent Lano Arca SplH Snmpfos The following samples were collected for split sample analyses between HBPP and the NRC: o Two samples of sediment from the Fishennans Chaimel o Three samples from the OJJen land area adjacent to the channel The split samples will be analyzed at the HBPP CounLroom for the following radionuclides to the MD C's; Nuclide 10% of DCGL MDC (vCi/g) 50% oflilCGL MDC (1>Ci/g) Co-60 3.BE-01 1.9E+OO Nb-94 7.1 E-01 3.55E+OO 1-129 ' 4.SE-01 2.4E+OO Cs-137" 7.58E-01 3.79E+OO Eu-152 1.0E+OO 5.0E+OO Eu-154 9.40E-01 4.70E+OO

                       'Np-237                                1.1E-01                              5.5E-01 H-3                                6.8E+01                               3.4E+02 Sr-90                                1.5E-01                              7.5E-01

The DCGL for Cs-137, the only nuclide expected to be present has beea ~duced to 24 mrem/y to account for any HTDs that might be present.

The desfrecl MDCs in the laboratory analyses of soil samples will be tlw 10% DCGL values. Tf it is impractical to achieve those, the 50% DCGL values must be achieved in the laboratory analyses of the samples.

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p.. Page 362 of 468 HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 FSS Report

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Characterization MDCs for GEL for FSS Samples Gamma Analysis: 10% to 50% of the DCGI,. Co-60 3.B2E*01 to 1.91E*t00 pCl/g Nb-94 7.13E-01 lo 3.57E+OO pCl/g 1-129 4.83E-01 lo 2.42E+OO pCJ/g Cs-137 7.93E-Oi to 3.97E+OO pCVg Eu-152 1.01E+OO lo 5.05E+OO pCJ/g Eu-154 9.40E-01 to 4.70E+OO pCi/g Np-237 1.11E--01 to 5.55E-01 pCi/g Hard to Detect Nuclldes: 10% to 50% of the DCGL H-3 6.ll('IE+01 to 3.43E+02 pCVg C-14 6.30E-01 to 3,15E+OO pCi/g Nl-59 1.97E+O~ to 9.!l5E+02 pCi/g Ni-63 7.24E+01 io **.3.62E+02 pClfg Sr-90 1.S1E~o1* to . i55E-01 pCifg Tc-99 1.24E+OO to 6.20E+OO pCl/g Pu-238 2.97E+OD to 1.49E+01 pCifg Pu-239/240 2.67E+OO to 1.34E+01 pClfg Pu-241 6.61E+01 to 4.31E+02 pCi/g Am-241 2.56E+OO to 1.29E+01 pCl/g Cm-.243 2.90E+OO to 1.45E+01 pCllg Om-244 4.81E+OO. to 2.41E+01 pCl!g Cm-245 1.78E+OO to 8,90E+OO pCIJg Cm-246 2.68E+OO to 1.29E+01 pCJ/g FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 363 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12

              ~I Laboratories LLC                                              SAMPLE RECEIPT & REVIEW FORM CHcnl:                                                             SDG/All/COC/Worl< Ortlcr:                        '.S'-/'i$'51'i)

Hcccivctl lly: 111f- 011lr Umimt: .::-~ /3-///- l'.l 0 *If Net Co1mts > IOCcp:n en san:pk::;'.101 nir.rkcd "rndior.cti*;c, conlncl the Radiation SalCl)' Group fer I'.1r~1cr Susprcletl llnz11r1l lnformnlio11

                                                          ;.. [;t* invcs1iga:ion.

COCISrunnl:s rnnrk~tl ns mdioacti'.. c? ,/ ~,-:Gtxirm1m Net Coullls Observed" (Ollscr;cci Count:; - /\rcn 13nckgrnund Counts): (: /11.--,_:;;. Classified Radioncti\*c II or iii bv RSO? / I~~. Were swipes 1nkt:n ofsmnpic contmi11ers < nclion level~'? COCISmnplcs rnnrkcd contniniri;:: PCBs? Package, CCC, and/or S;>mp!cs marked ns bc1vlli11111 or as\:1.-'5los cnntninin~? I/_, ffYcs;*snrn1Jlcs arc to be sc;!.rCl!oa\cc as S;ifct~* Conu*QJlcd Samnlcs. nnd cmcncd bv lhc GEL Snfctv Gro1111. Shiml<:d as DDOT Hazartlous7 V Jl:liilftl Class Shlp1>cd: Ul\11: Sam11lcs idcnliflctl ru Fllrdun Seil~* / Snm11k Uccdpt Criterin Cn111111mts/Qu11lincrs (l~c11u!rctl for Nun-Conforming ltm1s) Circl* /,ppticoM: 1 Shipping containers received intact and scalcxl'I I/ Dumug.c:d C1..)llttiini;r Li::.a\:i11g co:u.:af1u':1' O'htr (d~.s(rjUc) Samples rc-.iuiring cold prcservalion v i'ccior"*lion Method: kc \.'"1lJ!i Blue ice D;ylt'~ Kron" _Jbthcr (tlcscrib~) 2 { *111I ternpcrat11rc'3 ore rc<:ord:d i'l1-cr..'--mus within (0:;; 6 deg. C)?* Daily check pcrfornml and passed on' / ' TcmFcralurc Dcl'i;c Scrrnl 11: J :7 0 5?:. 77{.. Socondnry Tcmpcmllirc [)'"ice S~rial II (If A:l.;ifo.£bic): 2o lR tc111rcrnturc gun? I/ Chain of custody doct:mcms 3 included with shipment? * ,.

                                                                      ~--t-~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~----

c; rcI; Applicable: 4 Snmplc con miners inlact nnd scaled? .-- s..11, i>rokcn I:*nug::J cunminor Lcal:ing container 5 Samples requiring chemical I/ v- Sample ID"s, contnit1ors *lfr<ld """ olw:r>od pll: p:eservntion m proper pH? / "D..,....... "" "*'*'-' 1 __ ,,.. VOA vials free ofhcadspac.: &un1>lc JD's nud cun:nir.crs affoct<d: 6 (defined ns < 6111111 bubble)'.' 7 1\rc E."lcorc container~ present? Sumplcs received within ho:ditlg ID's r:nd lc>IS nfli:ctcJ: 8 time? / Somplc :o*s untl contoin-;rs an:,ctcd: Sample !D's cm COC mctch llYs an 9 b\1ttlcs? Dale & lim~ on COC ma:ch date & 10 t:m.: o:i bottles? s~mplc !D's olfcc1.:d: Number of containers rccch*cd match tl numb.:r intliculcd on COC? Arc sample containers idcnlifiahlc as 12 GEL pro*;idccl? COC lbrm is properly signed in 13 rclinquishcd/rcceivcd sections? Cirl!l<: Applicnbl.:::

                                                                           .  ,,/~')                                FedEx Ground              UPS           Fie!\! Scr*;ic.;;s      Gonrier         Oilier
                                                                      //                   ~
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14 Cmricr un~ tracking numb~'T. Cmrun~nts (Us~ C*.mtilwation Form if needed): PM (or l'MA) review: lniH~l~--~U,~~T~--- Datc _ _~r;~_,_/1~3~1-'-/J~r./_*__ l'ngc_/_or_J__ I I FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 364 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 FW:FW:

Subject:

FW: FW: From: "Oliver, Cynthia" <CCOl@pge.com> Date: Tue, 13 May 201415:14:44 +0000 To: "Erin Trent (Erin.Trent@gel.com)" <Erin.Trent@gel.com> CC: "Anderson, Dee" <D1A6@pge.com>, "Alderman, Wayne" <WLAB@pge.com> Erin - I am sorry the Engineer made a mistake in that letter - he did not include the nu elides you have listed below. Yes we need them analyzed for those nuclides also at the MDC's stated in the original letter from Dee. If this needs "more clarification -we will have him type up a new letter with exactly what he wants, please let me know. Thanks, Cyndi From: Erin Trent [1] Sent: Tuesday, May 13, 2014 8:10 AM To: Oliver, Cynthia

Subject:

Re: PN: Thanks. So we DON'T need to do the analyses below? Ni-63 Tc-99 C-14 Am/Cm Pu-238,329/240,241 Ni-59 Erin Trent Project Manager GEL Laboratories, LLC 2040 savage Road Charleston, SC (USA) 29407 Direct: 843.769.7374 Main: 843.556.8171 Fax: 843.766.1178 Email: Erin.Trent@gel.com Web: www.gel.com On 5/13/2014 11:06 AM, Oliver, Cynthia wrote: Here is the attached letter from the FSS engineer - please apply this to the samples received today from Fisherman's Channel Thanks, Cyndi From: Oliver, Cynthia Sent: Tuesday, May 13, 2014 8:05 AM To: Oliver, Cynthia

Subject:

r~2 8 of58

                 ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~-

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 365 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 FW:FW: To learn more, please visit http://www.pge.com/about/company/privacy/customer/ CONFIDENTIALITY NOTICE: This e-mail and any files transmitted with it are the property of The GEL Group, Inc. and its affiliates. All rights, including without limitation copyright, are reserved. The proprietary information contained in this e-mail message, and any files transmitted with it, is intended for the use of the recipient(s) named above. If the reader of this e-mail is not the intended recipient, you are hereby notified that you have received this e-mail in error and that any review, distribution or copying of this e-mail or any files transmitted with it is strictly prohibited. If you have received this e-mail in error, please notify the sender immediately and delete the original message and any files transmitted. The unauthorized use of this e-mail or any files transmitted with it is prohibited and disclaimed by The GEL Group, Inc. and its affiliates. PG&E is committed to protecting our customers' privacy. To learn more, please visit http://www.pge.com/about/company/privacy/customer/ p~g~ 9of58 5/13/201411:58 A~ FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 366 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Laboratory Certifications Page 10of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 367 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 List of current GEL Certifications as of 30 May 2014 State Certification Alaska UST-110 Arkansas 88-0651 CLIA 42D0904046 California NELAP 01151CA Colorado SC00012 Connecticut PH-0169 Delaware SC000122013-10 DoD ELAP/ ISOl 7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-12-00283,P330-12-00284 Georgia SC00012 Georgia SDWA 967 Hawaii SC000122013-10 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky 90129 Louisiana NELAP 03046 (AI33904) Louisiana SDWA LA130005 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC000122013-10 Nebraska NE-OS-26-13 Nevada SC000122014-l New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 Oklahoma 9904 Pennsylvania NELAP 68-00485 Plant Material Permit PDEP-12-00260 South Carolina Chemistry 10120001 South Carolina GVL 23611001 South Carolina Radiochemi 10120002 Tennessee TN 02934 TexasNELAP T104704235-14-9 UtahNELAP SC000122013-11 Vermont VT87156 Virginia NELAP 460202 Washington C780-12 Wisconsin 999887790 Page 11of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 368 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 GEL Laboratories LLC problem solved P.O. Box 30712-Clzarleston, S.C. 29417-2040 Savage Road-29407 (843)556-8171-Fax(843) 766-1178 Invoice for Analytical Services Accounts Payable-PG&E Invoice#: 288063 Pacific Gas and Electric Company Invoice Date: 30-MAY-14 Terms: Net 30 P.O. Box 7760 Client: Pacific Gas and Electric Company San Francisco, California 94120 Description (Order): Final Status Survey PO: 3500953353, Line item #4 Workorder/SDG: 348598 Project: PCGE00606 Project Manager: Erin Trent GELID:34859800l Matrix: SOIL Client!D: FSS-0294 OOLl0 Collected: 30-APR-14 Received: 13-MAY-14 Test Description Methods Turn Days Charge GSCGAMMS Gammaspec, Gamma, dried soil, Direct DOE HASL 300, 4 5 2 3/Ga-01-R 21 (Receive) $73 46 Count LSC99TCS Liquid Scint Tc99, Solid I 24 pCi/g RDL DOE EML HASL-300, Tc-02-RC Mo* 21 (Receive) $106 25 GSC59NIS Gamma Ni59, Solid 197 pCi/g RDL DOE RESL Ni-l 21 (Receive) $110 50 LSC_l4CS Liquid Scint Cl4, Solid, 0 63 pCi/g RDL EPA EERF C-01 Modified 21 (Receive) $110 50 LSC63NIS Liquid Scint Ni63, Solid 72 4 pCi/g RDL DOE RESL Ni-l, Modified 21 (Receive) $130 22 ASPAMCMS Alphaspec Am241, Cm, Solid I 78 pCi/g DOE EML HASL-300, Am-05-RC M1 21 (Receive) $140 25 RDL ASP_PUS Alphaspec Pu, Solid 2 67 pCi/g RDL DOE EML HASL-300, Pu-11-RC Mo* 2l (Receive) $140 25 LSC4IPUS Liquid Scint Pu24l, Solid 86 1 pCi/g RDL DOE EML HASL-300, Pu-11-RC Mo* 21 (Receive) $140 25 GFC90SRS GFPC, Sr90, soil 0 151 pCi/g RDL EPA 905 0 Modified 21 (Receive) Sl66 95 GSC_29IS Gamma Il29, Solid DOE EML HASL-300,1-01 Modified 2l (Receive) $236 25 Sample Total: $1,354.88 GELID:348598002 Matrix:SOIL Client!D: FSS-0302 OOLl0 Collected: 30-APR-14 Received: 13-MAY-14 Tcst Description Methods Turn Days Charge GSCGAMMS Gammaspcc, Gamma, dried soil, Direct DOE HASL 300, 4 5 2 3/Ga-01-R 21 (Receive) $73 46 Count LSC99TCS Liquid Scint Tc99, Solid l 24 pCi/g RDL DOE EML HASL-300, Tc-02-RC Mo* 21 (Receive) $106 25 GSC59NlS Gamma Ni59, Solid 197 pCi/g RDL DOE RESL Ni-l 21 (Receive) $110 50 LSC_l4CS Liquid Scint Cl4, Solid, 0 63 pCi/g RDL EPA EERF C-01 Modified 21 (Receive) Sl 10 50 LSC63NlS Liquid Scint Ni63, Solid 72 4 pCi/g RDL DOE RESL Ni-1, Modified 21 (Receive) $130 22 ASPAMCMS Alphaspec Am241, Cm, Solid 1 78 pCi/g DOE EML HASL-300, Am-05-RC M1 21 (Receive) $140 25 RDL ASP_PUS Alphaspec Pu, Solid 2 67 pCi/g RDL DOE EML HASL-300, Pu-11-RC Mo* 21 (Receive) $140 25 LSC41PUS Liquid Scint Pu24l, Solid 86 I pCi/g RDL DOE EML HASL-300, Pu-11-RC Mo< 21 (Receive) $140 25 GFC90SRS GFPC, Sr90, soil 0 l 5 l pCi/g RDL EPA 905 0 Modified 21 (Receive) $166 95 GSC_29IS Gamma Il29, Solid DOE EML HASL-300,1-01 Modified 21 (Receive) $236 25 Sample Total: $1,354.88 GELID:348598003 Matrix: SOIL Client!D: FSS-0266 OOLlO-ll- Collected: 28-APR-14 Received: 13-MAY-14 Tcst Description Methods 'Turn Days Charge GSCGAMMS Gammaspec, Gamma, dried soil, Direct DOE HASL 300, 4 5 2 3/Ga-01-R 21 (Receive) $73 46 Count LSC99TCS Liquid Scint Tc99, Solid I 24 pCi/g RDL DOE EML HASL-300, Tc-02-RC Mo* 2l (Receive) $106 25 GSC59NlS Gamma Ni59, Solid 197 pCi/g RDL DOE.RESL Ni-1 21 (Receive) $110 50 LSC_l4CS Liquid Scint Cl4, Solid, 0 63 pCi/g RDL EPA EERF C-01 Modified 21 (Receive) $110 50 LSC63NlS Liquid Scint Ni63, Solid 72 4 pCi/g RDL DOE RESL Ni-l, Modified 2l (Receive) $130 22 ASP AM CMS Alphaspec Am241, Cm, Solid 1 78 pCi/g DOE EML HASL-300, Am-05-RC M1

2l (Receive) $140 25 RDL ASP_PUS Alphaspcc Pu, Solid 2 67 pCi/g RDL DOE EML HASL-300, Pu-I I-RC Mo* 21 (Receive) $140 25 LSC4lPUS Liquid Scint Pu241, Solid 86 l pCi/g RDL DOE EML HASL-300, Pu-11-RC Mo* 2l (Receive) $140 25 GFC90SRS GFPC, Sr90, soil 0 151 pCi/g RDL EPA 905 0 Modified 21 (Receive) $166 95 GSC_291S Gamma Il29, Solid DOE EML HASL-300,1-01 Modified 2l (Receive) $236 25

                                                                                                                                                          $1,354.88 Page 12of58                                                                          Page 1 of2 FSS Report                                                  HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12                                                     Page 369 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10.-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 GEL Laboratories LLC problem sofred Accounts Payable-PG&E Jnyoice #: 288063 Inrnice Date: 30-::\IAY-14 Description (Order): Final Statns Snn*ey PO: 3500953353, Line item #4 GELID:348598004 lllalrix: SOIL ClientJD: fSS-0279 OOLl0 Collected: 29-APR-14 Receiyed: 13-MAY-14 Test 'Descripdon 1\Iethods Turn Days Charge GSCGAMMS Gammaspec, Gamma, dried soil, Direct DOE HASL 300, 4 5 2 3/Ga-ol-R 21 (Receive) $7346 Count LSC99TCS Liquid Sein! Tc99, Solid 1 24 pCi/g RDL DOE EML HASL-300, Tc--02-RC Mo. 21 (Receive) $10625 GSC59NIS Gamma Ni59, Solid 197 pCi/g RDL DOE RESL Ni-I 21 (Receive) $110 50 LSC_l4CS Liquid Sein! Cl4, Solid, 0 63 pCi/g RDL EPA EERf C-01 Modified 21 (Recci\'C) Sl!O 50 LSC63NIS Liquid Scint Ni63, Solid 724 pCi/g RDL DOE RESL Ni-I, Modified 21 (Receive) $13022 ASPAMCMS Alpbaspec Am'.!41, Cm, Solid I 78 pCi/g DOE*EML HASL-300, Am--05-RC Mt 21 (Receive) $14025 RDL ASP_PUS Alpbaspec Pu, Solid 2 67 pCi/g RDL DOE EML HASL-300, Pu-11-RC Mo. 21 (Recci\'C) Sl4025 LSC41PUS Liquid Sein! Pu241, Solid 86 1 pCi/g RDL DOE EML HASL-300, Pu-11-RC Moo 21 (Recci\'C) Sl4025 GFC90SRS GfPC, SI90,soil 0 151 pCi/gRDL EPA905 OModlfied 21 (Recci\'<) $16695 GSC_29IS Gamma Il29, Solid DOE EML HASL-300,I-OI Modified 21 (Recci\'C) $23625 Sample Total: Sl,35-1.88 Miscellaneous Charge Descripdon Charge Inrnice Total: S5419.52 Page2of2 Page 13 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 370 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Radiological Analysis Page 14 of 58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 371 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Radiochemistry Case Nal'l'atin Pacific Gas and Elechic Company (PCGE) SDG348598 Method/Analysis Information Product: Alphaspec Am241, Cm, Solid 1.78 pCi/g RDL Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Dcy Soil Prep Analytical Batch Number: 1387983 Prep Batch Number: 1387637 Sample ID Client ID 348598001 FSS-0294 OOLl 0-12-011-F-S 348598003 FSS-0266 OOLl0-11-003-F-S 348598004 FSS-0279 OOLI0-11-016-F-S 1203088580 Method Blank (MB) 1203088581 34859800l(FSS-0294 OOLl0-12-011-F-S) Sample Duplicate (DUP) 1203088582 Laboratocy Control Sample (LCS) The samples in this SDG were analyzed on a "dcy weight" basis. SOP Referenre Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011 REV#24. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Gt>omeh-y All coU11ting sources were prepared in the same geometry as the calibration standards. Quality Conh*ol (QC) Information: Blank Infonnation The blank volmne is representative of the sample volmnes in this batch. Designated QC The following sample was used for QC: 348598001 (FSS-0294 OOLl0-12-011-F-S). Page 15 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 372 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 QC lnfol'mation All of the QC samples met the required acceptance limits. Technical lnfol'mation: Holding Time All sample procedures for this sample set were perfom1ed within the required holding time. Sample Re-pl'ep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Recounts Samples 1203088580 (MB), 1203088581 (FSS-0294 OOLl0-12-011-F-S) and 348598004 (FSS-0279 OOLlO-l l-016-F-S) were recounted due to a suspected false positive. The recotlnts are reported. Miscellaneous lnfol'mation: Data Exception (DER) Documentation Data exception reports are generated to doclllllent any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) :was not generated for this SDG. Manual Integmtion No manual integrations were performed on data in this batch. Sample-Specific MDAIMDC The l\IDAIMDC reported on the certificate of analysis is a sample-specific l\IDAIMDC. Additional Comments Additional comments were not required for this sample set. Qnalifiel' Infol'mation Manual qualifiers were not required. Method/Analvsis Infol'mation P1*oduct: Alphaspec Pu, Solid 2.67 pCi/g RDL Anal;1ical Method: DOE EML HASL-300, Pn-11-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1387984 Prep Batch Number: 1387637 Sample ID Client ID 348598001 FSS-0294 OOLl0-12-011-F-S 348598002 FSS-0302 OOLI0-12-019-F-S 348598003 FSS-0266 OOLIO-l l-003-F-S Page 16 of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 373 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 348598004 FSS-0279 OOLl0-11-016-F-S 1203088587 Method Blank (lvffi) 1203088588 34859800l(FSS-0294 OOLl0-12-011-F-S) Sample Duplicate (DUP) 1203088589 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Refe1*em:e Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011 REV# 24. ~ Calibration Information: Calibmtion Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Qualitv Control {QC) Information: Blank Information The blank volume is representative of the sample volUllle in this batch. Designated QC The following sample was used for QC: 348598001 (FSS-0294 OOLl0-12-011-F-S). QC Information All of the QC samples met the required acceptance lin1its. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this saniple set required reprep or reanalysis. Recounts None of the samples in this batch were recounted.

Miscellaneous Information:

D~ta Exception (DER) Documentation Data exception reports are generated to docUlllent any procedural anomalies that may deviate from referenced SOP or contractual docUlllents. A data exception report (DER) was not generated for this SDG. Manual Integration No manual integrations were performed on data in this batch. Page 17 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 374 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Sample-Specific MDA/MDC The MDAIMDC reported on the certificate of analysis is a sample-specific MDAIMDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/Analysis Information

Product: Alphasper Am241, Cm, Solid 1.78 pCi/g RDL Analytical Method: DOE EML HASL-300, A.m-05-RC Modified Prep Method: Dry Soil Prep Analytical Batch Nmnber: 1390686 Prep Batch Number: 1387637 Sample ID Client ID 348598002 FSS-0302 OOLI0-12-019-F-S 1203095525 Method Blank (MB) 1203095526 348598002(FSS-0302 OOLl0-12-019-F-S) Sample Duplicate (DUP) 1203095527 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure, for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-011 REV# 24. Calibration Information: Calibrntion Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control (QC) Information: Blank Info1*mation Page 18 of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 375 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 The blank volume is representative of the sample vohune in this batch. Designated QC Tue following sample was used for QC: 348598002 (FSS-0302 OOLl0-12-019-F-S). QC Infol'mation All of the QC samples met the required acceptance limits. Tedmical Information: Holding Time All sample procedures for this sample set were perfonned within the required holding time. Sample Re-p1*ep/Re-analysis Sample 348598002 (FSS-0302 OOLI0-12-019-F-S) was reprepped to verify activity. The re-analysis is reported. Recounts Sample 1203095527 (LCS) was recounted due to high recovery. The reconnt is reported. Samples 1203095526 (FSS-0302 OOLI0-12-019-F-S) and 348598002 (FSS-0302 OOLI0-12-019-F-S) were recounted due to a suspected false positive. The recounts are reported. Miscell:m"ous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual docun1ents. A data exception report (DER) was not generated for this SDG. Manual Integration No manual integrations were performed on data in this batch. Sample-Specific MDAJMDC The MDA!MDC reported on the certificate of analysis is a sample-specific MDA!MDC. Additional Comments Additional comments were not required for this san1ple set. Qualifier Information Manual qualifiers were not required. Method/Analvsis Information Prnduct: Gamma Ni59, Solid 197 pCi/g RDL Analytical Method: DOE RESL Ni-I Prep Method: Dry Soil Prep Analytical Batch Number: 1387640 Prep Batch Number: 1387637 Page 19 of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 376 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Sample ID Client ID 348598001 FSS-0294 OOLl0-12-011-F-S 348598002 FSS-0302 OOLl0-12-019-F-S 348598003 FSS-0266 OOLl0-11-003-F-S 348598004 FSS-0279 OOLl0-11-016-F-S 1203087730 Method Blank (MB) 1203087731 348598003(FSS-0266 OOLI0-11-003-F-S) Sample Duplicate (DUP) 1203087732 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of anal}'tical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 16. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards lnfo1*mation Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Quality Control (QC) Information: Blank Infm*mation The blank volume is representative of the sample volun1e in this batch. Designated QC The following sample was used for QC: 348598003 (FSS-0266 OOLl0-11-003-F-S). QC Information All of the QC samples met the required acceptance lin1its. Technical Information: Holding Time All sample procedures for this sample set were perfonned within the required holding time. Sample Re-p1*ep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical Recove1ies All chemical recoveries meet the required acceptance linllts for this sample set. Recounts None of the san1ples in this batch were recounted. Page 20 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 377 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Mi~l"ellaneous Infonnatiou: Data Exception (DER) Documentation Data exception reports are generated to docmnent any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) -..vas not generated for this SDG. Sample-Spedfic l\'IDA/MDC 111e MDAIMDC reported on the certificate of analysis is a sample-specific MDAIMDC. Additional Comments Additional comments were not required for this saniple set. Qualifiel' Infol'mation Manual qualifiers were not required. Method/Analysis Information Product: Gammaspec, Gamma, d1ied soil, Direct Count Analytical Method: DOE HASL 300, 4.5.2.3/Ga-Ol-R Analytical Batch Nmnber: 1387698 Sample ID Client ID 348598001 FSS-0294 OOLl0-12-011-F-S 348598002 FSS-0302 OOLl0-12-019-F-S 348598003 FSS-0266 OOLl0-11-003-F-S 348598004 FSS-0279 OOLl0-11-016-F-S -- 1203087897 Method Blank (MB) 1203087898 348598001(FSS-0294 OOLl0-12-011-F-S) Saniple Duplicate (DUP) 1203087899 Laboratory Control Saniple (LCS) The saniples in this SDG were analyzed 011 an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data.discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 25. Calibmtion Information: Calibration Infol'mation All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the e11.-piration dates. Sample Geometi*y Page 21 of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 378 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 All counting sources were prepared in the same geometry as the calibration standards. Qualitv Control (QC) Information: Blank Information The blank volun1e is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 348598001 (FSS-0294 OOLl0-12-011-F-S). QC Information All of the QC samples meet the required acceptance linrits with the following exceptions: The san1ple and the duplicate, 1263087898 (FSS-0294 OOLl0-12-011-F-S) and 348598001 (FSS-0294 OOLI0-12-0ll-F-S), did not meet the relative percent difference requirement for Cs-13 7; however, they do meet the relative error ratio requirement with value of 1.23. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Recounts None of the samples in this batch were recounted. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDAJMDC

                     ?1e MDAIMDC reported on the certificate of analysis is a sample-specific MDA/MDC.

Additional Comments Additional comments were not required for this.sample set. Qu:difier Information Qualifier Reason Anal)1e Sample Client Sample Data rejected due to high FSS-0279 UI Cerimn-141 348598004 peak-width. OOLI0-11-016-F-S FSS-0279 Uranium-235 348598004 OOLIO-ll-016-F-S Data rejected due to low FSS-0302 UI Bismuth-212 348598002 abundance. OOLI0-12-019-F-S FSS-0294 Cesium-134 348598001 OOLI0-12-011-F-S Page 22 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 379 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 FSS-0302 348598002 OOLl0-12-019-F-S FSS-0266 348598003 OOLl0-11-003-F-S FSS-0294 Cesium-136 348598001 OOLl0-12-011-F-S FSS-0279 Niobium-95 348598004 OOLl0-11-016-F-S Method/Analysis Information Prnduct: Gamma 1129, Solid Analytical Method: DOE EML HASL-300,1-01 Modified Analytical Batch Number: 1387906 Sample ID Client ID 348598001 FSS-0294 OOLl0-12-011-F-S 348598002 FSS-0302 OOLI0-12-019-F-S 348598003 FSS-0266 OOLl0-11-003-F-S 348598004 FSS-0279 OOLl0-11-016-F-S 1203088381 Method Blank (MB) 1203088382 34859800l(FSS-0294 OOLl0-12-011-F-S) Sample Duplicate (DUP) 1203088383 34859800l(FSS-0294 OOLl0-12-011-F-S) Matri.'> Spike (MS) 1203088384 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GJ~L Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-006 REV# 21. Calibration Information: Calibrntion Information All initial and continuing calibration requirements have been met. Standards lnfo1*mation Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Page 23 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 380 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Qualitv Contml (QC) Information: Blank Info1*matiou The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 348598001 (FSS-0294 OOLI 0-12-011-F-S). QC Information All of the QC samples met the required acceptance limits. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Recounts Sample 1203088383 (FSS-0294 OOLl0-12-011-F-S) was recounted due to low recovery. The recount is reported. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific !\'IDA/MDC The MDAIMDC reported on the certificate of analysis is a sample-specific MDAIMDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/Analvsis Information Product: GFPC, Sr90, soil 0.151 pCi/g RDL Analytical Method: EPA 905.0 Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1391080 Prep Batch Number: 1387637 Page24 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 381 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Sample ID Client ID 348598001 FSS-0294 OOLl0-12-011-F-S 348598002 FSS-0302 OOLl0-12-019-F-S 348598003 FSS-0266 OOLl 0-11-003-F-S 348598004 FSS-0279 OOLl0-11-016-F-S 1203096526 Method Blank (MB) 1203096527 348598001(FSS-0294 OOLl0-12-011-F-S) Sample Duplicate (DUP) 1203096528 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 17. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. Qunlity Contl'ol (QC) Infol'mation: Blank Info1*mation The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 348598001 (FSS-0294 OOLl0-12-011-F-S). QC Information All of the QC san1ples met the required acceptance limits. Technical Information: Holding Time All sample procedures for this sample set were performed within the required holding tinie. Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Chemical RecoYelies All chemical recoveries meet the reqUired acceptance limits for this sample set. Recounts Saniple 348598004 (FSS-0279OOLl0-11-016-F-S) was recounted due to a suspected false positive. The recount is reported. Page 25 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 382 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Miscell:meous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDAJMDC The tvIDAIMDC reported on the certificate of analysis is a sample-specific rvIDA/MDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information Manual qualifiers were not required. Method/Analysis Information Prnduct: Liquid Sdnt Pu241, Solid 86.1 pCi/g RDL Analytical Method: DOE EML HASL-300, Pu-II-RC Modified Prep Method: Dry Soil Prep Analytical Batch Number: 1387985 Prep Batch Number: 1387637 Sample ID Client ID 348598001 FSS-0294 OOLI0-12-011-F-S 348598002 FSS-0302 OOLl0-12-019-F-S 348598003 FSS-0266 OOLI0-11-003-F-S 348598004 FSS-0279 OOLI0-11-016-F-S 1203088590 Method Blank (MB) 1203088591 348598001(FSS-0294 OOLI0-12-011-F-S) Sample Duplicate (DUP) 1203088592 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 16. Calibration Information: Calibration Information All initial and continuing calibration requirements have been met. Standa1*ds Information Page26 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 383 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geomeh*y All counting sources were prepared in the same geometry as the calibration standards. Quality Control (QC) Information: Blank Info1*mation The blank volume is representative of the sample volUllle in this batch. Designated QC The following sample was used for QC: 348598001 (FSS-0294 OOLI0-12-011-F-S). QC Information All of the QC samples met the required acceptance limits. Technicallnformation: Holding Time All sample procedures for this sample set were performed within the required holding time. Sample Re-p1*ep/Re-analysis None of the samples in this sample set required reprep or reanalysis. Recounts None of the samples in this batch were recounted.

                     ~Iiscellaneous  Info1"1Ilation:

Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual docun1ents. A data exception report (DER) was not generated for this SDG. l\Ianual Integration No manual integrations were performed on data in this batch. Sample-Specific MDA/MDC The :MD.A/l'vIDC reported on the certificate of analysis is a sample-specific MD.A/l'vIDC. Additional Comments Additional comments were not required for this sample set. Qualifier Information

Manual qualifiers were not required.

Method/Analvsis Information Product: Liquid Scint Ni63, Solid 72.4 pCi/g RDL Analytical Method: DOE RESL Ni-I, Modified Page 27 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 384 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Prep Method: Dry Soil Prep Analytical Batch Number: 1387641 Prep Batch Number: 1387637 Sample ID Client ID 348598001 FSS-0294 OOLl0-12-011-F-S 348598002 FSS-0302 OOLl0-12-019-F-S 348598003 FSS-0266 OOLl0-11-003-F-S 348598004 FSS-0279 OOLl0-11-016-F-S 1203087733 Method Blank (MB) 1203087734 348598003(FSS-0266 OOLl0-11-003-F-S) Sample Duplicate (DUP) 1203087735 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. SOP Reference Procedure for preparation, analysis and reporting of anal)'1ical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 16. Calibrntion Info1*mation: Calibrntion Information All initial and continuing calibration requirements have been met. Standards Information Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources were prepared in the san1e geometry as the calibration standards. Quality Control (QC) Information: Blank lnfm*mation The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 348598003 (FSS-0266 OOLI0-11-003-F-S). QC lnfo1*mation All of the QC san1ples met the required acceptance linlits. Technkal Information: Holding Time All sample procedures for this sample set were performed *witllin the required holding tin1e. Sample Re-prep/Re-analysis None of the samples in tllis sample set required reprep or reanalysis. Page 28 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 385 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Recounts None of the samples in this batch were recounted. Miscellaneous lnfol'mation: Data Exception (DER) Documentation Data exception reports are generated to docmnent any procedural anomalies that may deviate from referenced SOP or contractual doctunents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDAJMDC The MDAIMDC reported on the certificate of analysis is a sample-specific MDAIMDC. Additional Comments Additional comments were not required for this sample set. Qualifiel' Infol'mation Manual qualifiers were not required. Method/Analysis Infol'mation Prnduct: Liquid Scint Tc99, Solid 1.24 pCi/g RDL Analytical Method: DOE E:rv1L HASL-300, Tc-02-RC Modified Analytical Batch Number: 1387681 Sample ID Client ID 348598001 FSS-0294 OOLl0-12-011-F-S 348598002 FSS-0302 OOLl0-12-019-F-S 348598003 FSS-0266 OOLl0-11-003-F-S 348598004 FSS-0279 OOLl0-11-016-F-S 1203087837 Method Blank (MB) 1203087838 348598001(FSS-0294 OOLI0-12-011-F-S) Sample Duplicate (DUP) 1203087839 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. SOP Refel'ence Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). Tue data discussed in this nam1tive has been analyzed in accordance with GL-RAD-A-059 REV# 2. Calibrntion Info1*mation: Calibrntion lnfol'mation All initial and continuing calibration requirements have been met. Standm*ds Infot'lllation Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used Page29 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 386 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 before the expiration dates. Sample Geomet1'Y All counting sources were prepared in the same geometry as the calibration standards. Qualitv Conti*ol (QC) Information: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 348598001 (FSS-0294 OOLl0-12-011-F-S). QC Information All of the QC samples met the required acceptance limits. Technical Information: Holding Time All sample procedures for this sample set were perfom1ed within the required holding tinie. Sample Re-p1*ep/Re-analysis None of the san1ples in this sample set required reprep or reanalysis. Recounts None of the san1ples in this batch were recounted. Miscellaneous Information: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MDA/MDC The MDAJMDC reported on the ce11ificate of analysis is a sample-specific MDAJMDC. Additional Comments Additional collllllents were not required for this sample set. Qualifier* Information Manual q~alifiers were not required. Method/Analvsis Infonnation Product: Liquid Scint C14, Solid, 0.63 pCi/g RDL Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 1388352 Page 30 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 387 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Sample ID Client ID 348598001 FSS-0294 OOLl0-12-011-F-S 348598002 FSS-0302 OOLl0-12-019-F-S 348598003 FSS-0266 OOLl0-11-003-F-S 348598004 FSS-0279 OOLl0-11-016-F-S 1203089505 Method Blank (MB) 1203089506 34859800l(FSS-0294 OOLl0-12-011-F-S) Sample Duplicate (DUP) 1203089507 34859800l(FSS-0294 OOLl0-12-011-F-S) Matrix Spike (MS) 1203089508 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on au "as received" basis. SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by GEL Laboratories LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 15. Calibration Information: Calibmtion Information All initial and continuing calibration requirements have been met. Standards lnfo1*mation Standard solutions for these analysis are NIST traceable or verified with a NIST traceable standard and used before the expiration dates. Sample Geometry All counting sources *were prepared in the same geometry as the calibration standards. Qualitv Control (QC) Info1*mation: Blank Information The blank volume is representative of the sample volume in this batch. Designated QC The following sample was used for QC: 348598001 (FSS-0294 OOLl0-12-011-F-S). QC Information All of the QC san1ples met the required acceptance linlits. Technical Infonnation: Holding Time All san1ple procedures for this sample set were performed witllin the required holding time. Sample Re-prep/Re-analysis None of t11e san1ples in tllis san1ple set required reprep or reanalysis. Recounts Samples 348598001 (FSS-0294 OOLl0-12-011-F-S) and 348598002 (FSS-0302 OOLl0-12-019-F-S) were recounted due to the quench number being outside tlie calibration rauge. The recotu1ts are reported. Sauiples 1203089506 (FSS-0294 OOLl 0-12-011-F-S) and 348598004 (FSS-0279 OOLI0-11-016-F-S) were recounted due to a suspected false positive. The recounts are reported. Sample 348598003 (FSS-0266 OOLl0-11-003-F-S) was recounted due to the quench number being outside the calibration rauge and then recounted due to results more negative than the three sigma TPU. The third count is reported. Page 31 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 388 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Miscelfaneous lnfonnatiou: Data Exception (DER) Documentation Data exception reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A data exception report (DER) was not generated for this SDG. Sample-Specific MD.A/MDC The MDAIMDC reported on the certificate of analysis is a sample-specific MDA&IDC. Additional Comments Additional comments were not required for this sample set. Qualifier Info1*mation Manual qualifiers were not required. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard tmless otherwise noted in the analytical case narrative. Page 32 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 389 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Qualifier Definition Report for PCGE006 Pacific Gas and Electric Company Client SDG: 348598 GEL Work Order: 348598 The Qualifiers in this report are defined as follows: M Result is < LLD and > MDC U Result is <LLD and <MDC UI Uncertain identification for gamma spectroscopy ReviewNalidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: ....._"JA,u~~ ~ Name: Theresa Austin Date: 02 JUN 2014

Title:

Group Leader Page 33of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 390 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Sample Data Summary Page 34of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 391 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis GEL Sample ID: 348598001 Client: Pacific Gas and Electric Company Client Sample ID: FSS-0294 OOLl0-12-011-F-S Collect Date: April 30, 2014 Client Matrix: Soil Receive Date: May 13, 2014 Amount of Sample Received: Report Date: June 02, 2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty MDC LLD TPU Units C-14 05/22/14 u -2.98E-Ol 3.40E-Ol 5.79E-Ol 6.30E-Ol 3.40E-Ol pCi/g Ni-63 05/22/14 u -8.50E+OO 2.55E+Ol 4.33E+Ol 7.24E+Ol 2.55E+Ol pCi/g Sr-90 05/29/14 u l.67E-02 5.41E-02 8.67E-02 l.51E-Ol 5.42E-02 pCi/g Tc-99 05/25/14 u 4.24E-04 4.69E-Ol 7.87E-Ol l.24E+OO 4.69E-Ol pCi/g Pu-241 05/27/14 u -l.71E+Ol 3.07E+Ol 5.31E+Ol 8.61E+Ol 3.07E+Ol pCi/g Alpha Spec Pu-238 05/21/14 u -2.33E-02 l.61E-Ol 3.92E-Ol 2.97E+OO l.61E-Ol pCi/g Pu-239/240 05/21/14 u 1.48E-Ol 2.40E-Ol 3.71E-Ol 2.67E+OO 2.41E-Ol pCi/g Am-241 05/21/14 u 9.43E-02 l.86E-Ol 3.15E-Ol 2.58E+OO l.87E-Ol pCi/g Cm-243/244 05/21/14 u 3.21E-02 2.58E-Ol 5.15E-Ol 2.90E+OO 2.58E-Ol pCi/g Cm-245/246 05/21/14 u l.28E-Ol l.85E-Ol 2.23E-Ol l.78E+OO l.86E-Ol pCi/g Gamma Spec Be-7 05/14/14 u 9.47E-02 l.32E-Ol 2.34E-Ol l.39E-Ol pCi/g Na-22 05/14/14 u -8.06E-03 l.69E-02 2.67E-02 l.73E-02 pCi/g K-40 05/14/14 l.24E+Ol 7.03E-Ol l.82E-Ol l.26E+OO pCi/g Cr-51 05/14/14 u -l.23E-Ol l.57E-Ol 2.59E-Ol l.67E-Ol pCi/g Mn-54 05/14/14 u -5.73E-03 l.46E-02 2.42E-02 l.49E-02 pCi/g Fe-59 05/14/14 u -5.95E-03 3.53E-02 5.84E-02 3.54E-02 pCi/g Co-56 05/14/14 u 8.96E-04 l.46E-02 2.50E-02 l.46E-02 pCi/g Co-57 05/14/14 u 2.85E-03 l.29E-02 2.19E-02 l.29E-02 pCi/g Co-58 05/14/14 u 9.64E-03 l.59E-02 2.86E-02 l.65E-02 pCi/g Co-60 05/14/14 u l.lOE-02 l.56E-02 2.80E-02 3.82E-Ol l.63E-02 pCi/g Ni-59 05/21/14 u -3.19E+Ol l.49E+Ol 2.0IE+Ol l.97E+02 2.09E+Ol pCi/g Zn-65 05/14/14 u -2.59E-02 4.35E-02 5.79E-02 4.52E-02 pCi/g Y-88 05/14/14 u -3.49E-03 l.04E-02 l.60E-02 l.05E-02 pCi/g Zr-95 05/14/14 u 2.49E-02 2.92E-02 5.16E-02 3.14E-02 pGi/g Nb-94 05/14/14 u -8.88E-03 1.42E-02 2.22E-02 7.13E-Ol 1.48E-02 pCi/g Nb-95 05/14/14 u 2.12E-02 1.87E-02 3.0IE-02 2.l IE-02 pCi/g Ru-106 05/14/14 u -6.80E-02 l.24E-Ol l.97E-Ol l.28E-Ol pCi/g Ag-llOm 05/14/14 u -9.17E-03 l.87E-02 3.04E-02 l.92E-02 pCi/g Sn-113 05/14/14 u l.OOE-02 l.87E-02 3.30E-02 l.93E-02 pCi/g Sb-124 05/14/14 u 1.42E-02 2.05E-02 4.04E-02 2.15E-02 pCi/g Sb-125 05/14/14 u l.70E-02 3.85E-02 6.72E-02 3.93E-02 pCi/g I-129 05/27/14 u 3.03E-Ol 3.35E-Ol 4.63E-Ol 5.00E-01 3.63E-Ol pCi/g Cs-134 05/14/14 UI 3.57E-02 2.25E-02 3.57E-02 3.26E-02 pCi/g Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units offt3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD. UI Uncertain identification for gamma spectroscopy. x Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. M Reported result is less than the LLD and greater than the MDC. Page 35 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 392 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis GEL Sample ID: 348598001 Client: Pacific Gas and Electric Company Client Sample ID: FSS-0294 OOLl0-12-011-F-S Collect Date: April 30, 2014 Client Matrix: Soil Receive Date: May 13, 2014 Amount of Sample Received: Report Date: Jone 02, 2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty MDC LLD TPU Units Cs-136 05/14/14 UI 6.99E-02 4.77E-02 6.99E-02 6.04E-02 pCi/g Cs-137 05/14/14 M l.llE-01 3.08E-02 2.49E-02 7.58E-Ol 3.20E-02 pCi/g Ba-133 05/14/14 u 3.07E-03 2.02E-02 3.05E-02 2.03E-02 pCi/g Ba-140 05/14/14 u -9.62E-03 2.42E-02 3.38E-02 2.46E-02 pCi/g Ce-139 05/14/14 u 7.21E-03 l.63E-02 2.45E-02 l.67E-02 pCi/g Ce-141 05/14/14 u l.23E-02 3.22E-02 5.49E-02 3.27E-02 pCi/g Ce-144 05114114 u -9.97E-03 9.84E-02 l.65E-01 9.86E-02 pCi/g Nd-147 05/14/14 u 4.97E-03 2.14E-01 3.59E-01 2.14E-Ol pCi/g Pm-144 05/14/14 u l.07E-03 1.43E-02 2.38E-02 l.43E-02 pCi/g Pm-146 05/14/14 u -l.27E-03 l.63E-02 2.74E-02 l.63E-02 pCi/g Eu-152 05/14/14 u -1.83E-02 4.96E-02 6.74E-02 I.OlE+OO 5.03E-02 pCi/g Eu-154 05/14/14 u -l.64E-02 4.75E-02 7.61E-02 9.40E-Ol 4.81E-02 pCi/g Eu-155 05/14/14 u 7.40E-02 5.61E-02 9.98E-02 6.56E-02 pCi/g Ir-192 05/14/14 u -4.63E-03 l.50E-02 2.54E-02 l.51E-02 pCi/g Hg-203 05/14/14 u l.57E-02 2.0lE-02 3.0SE-02 2.13E-02 pCi/g Tl-208 05/14/14 l.79E-01 2.38E-02 2.28E-02 2.79E-02 pCi/g Pb-210 05/14/14 u l.39E+OO 2.77E+OO 4.88E+OO 2.85E+OO pCi/g Pb-212 05/14/14 5.94E-01 4.62E-02 4.63E-02 6.77E-02 pCi/g Pb-214 05/14/14 5.37E-01 6.78E-02 5.67E-02 8.06E-02 pCi/g Bi-212 05/14/14 6.88E-01 2.93E-Ol 3.21E-Ol 3.00E-01 pCi/g Bi-214 05/14/14 4.73E-Ol 6.26E-02 4.83E-02 7.33E-02 pCi/g Ra-228 05/14/14 6.05E-Ol l.l lE-01 9.21E-02 l.34E-Ol pCi/g Ac-228 05/14/14 6.05E-OI 1.1 lE-01 9.21E-02 l.34E-Ol pCi/g Th-234 05/14/14 u l.19E+OO l.19E+OO l.38E+OO l.22E+OO pCi/g U-235 05/14/14 u -3.30E-02 l.08E-Ol I.78E-Ol l.08E-01 pCi/g U-238 05/14/14 u l.19E+OO l.19E+OO l.38E+OO l.22E+OO pCi/g Np-237 05/14/14 u l.50E-02 2.77E-02 "4.90E-02 l.llE-01 2.85E-02 pCi/g Np-239 05/14/14 u -3.92E-02 2.12E-Ol 3.57E-Ol 2.13E-01 pCi/g Am-241 05/14/14 u 5.31E-02 l.09E-Ol l.69E-Ol l.l lE-01 pCi/g Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units offt3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD. UI Uncertain identification for gamma spectroscopy. X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. M Reported result is less than the LLD and greater than the MDC. Page 36 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 393 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis GEL Sample ID: 348598002 Client: Pacific Gas and Electric Company Client Sample ID: FSS-0302 OOLl0-12-019-F-S Collect Date: April 30, 2014 Client Matrix: Soil Receive Date: May 13, 2014 Amount of Sample Received: Report Date: June 02, 2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty MDC LLD TPU Units C-14 05/22/14 u -4.06E-01 3.35E-01 5.73E-01 6.30E-01 3.35E-01 pCi/g Ni-63 05/22/14 u -l.55E+Ol 1.77E+Ol 3.06E+Ol 7.24E+Ol l.77E+ol pCi/g Sr-90 05/29114 u 4.62E-02 6.18E-02 9.22E-02 1.51E-01 6.23E-02 pCi/g Tc-99 05/25/14 u 2.49E-Ol 4.85E-01 8.02E-01 1.24E+OO 4.86E-01 pCi/g Pu-241 05/27/14 u -2.64E+Ol 2.31E+Ol 4.llE+Ol 8.61E+Ol 2.30E+Ol pCi/g Alpha Spec Pu-238 05/21114 u 2.99E-02 l.12E-01 l.88E-01 . 2.97E+OO 1.12E-Ol pCi/g Pu-239/240 05/21114 u 2.04E-02 1.14E-01 2.18E-Ol 2.67E+OO 1.14E-Ol pCi/g Am-241 05/29/14 u -4.78E-02 1.44E-01 4.05E-Ol 2.58E+OO 1.45E-01 pCi/g Cm-243/244 05/29/14 u l.84E-02 l.92E-01 4.0lE-01 2.90E+OO l.92E-Ol pCi/g Cm-245/246 05/29/14 u 5.77E-02 2.l 7E-01 3.64E-Ol l.78E+OO 2.17E-01 pCi/g Gamma Spec Be-7 05/14/14 u 9.36E-03 1.03E-01 1.78E-01 l.03E-01 pCi/g Na-22 05/14/14 u 7.75E-03 l.67E-02

2.57E-02 l.71E-02 pCi/g K-40 05/14/14 l.33E+Ol 6.67E-01 l.82E-01 l.31E+OO pCi/g Cr-51 05/14/14 u -3.50E-02 1.29E-01 2.lOE-01 lJOE-01 pCi/g Mn-54 05/14/14 u l.85E-03 1.46E-02 2.12E-02 l.47E-02 pCi/g Fe-59 05/14/14 u l.06E-02 3.09E-02 5.39E-02 3.13E-02 pCi/g Co-56 05/14/14 u -7.78E-03 1.30E-02 l.78E-02 1.35E-02 pCi/g Co-57 05/14/14 u -7.75E-03 l.22E-02 l.92E-02 1.27E-02 pCi/g Co-58 05/14/14 u l.45E-02 l.73E-02 2.06E-02 1.86E-02 pCi/g Co-60 05/14/14 u -1.39E-03 1.44E-02 2;03E-02 3.82E-01 1.45E-02 pCi/g Ni-59 05/21114 u 6.17E+OO 1.52E+Ol 2.85E+Ol 1.97E+02 l.55E+ol pCi/g Zn-65 05/14/14 u -1.39E-03 3.60E-02 5.22E-02 3.60E-p2 pCi/g Y-88 05/14/14 u 9.87E-03 1.03E-02 2.03E-02 1.12E-02 pCi/g Zr-95 05/14/14 u 3.79E-02 2.44E-02 4.57E-02 3.00E-02 pCi/g Nb-94 05/14/14 u 2.58E-03 1.09E-02 l.85E-02 7.13E-01 1.09E-02 pCi/g Nb-95 05/14/14 u 2.31E-02 1.68E-02 2.76E-02 l.99E-02 pCi/g Ru-106 05/14/14 u 2.27E-02 l.05E-01 1.SOE-01 l.05E-01 pCi/g Ag-llOm 05/14/14 u 6.80E-03 1.56E-02 2.75E-02 l.59E-02 pCi/g Sn-113 05/14/14 u 1.24E-02 1.61E-02 2.79E-02 l.71E-02 pCi/g Sb-124 05/14/14 u -6.46E-03 2.36E-02 3.82E-02 2.38E-02 pCi/g Sb-125 05/14/14 u l.28E-02 3.44E-02 5.76E-02 3.49E-02 pCi/g I-129 05/27/14 u l.43E-03 9.80E-02 l.70E-Ol 5.00E-01 9.80E-02 pCi/g Cs-134 05/14/14 UI 2.65E-02 2.16E-02 2.65E-02 2.51E-02 pCi/g Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units offt3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD. m- Uncertain identification for gamma spectroscopy. x Lab-specific qualifier-please sec case narrative, data summary package or contact your project manager for details. M Reported result is less than the LLD and greater than the MDC. Page 37 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 394 of 468 l__

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis GEL Sample ID: 348598002 Client: Pacific Gas and Electric Company Client Sample ID: FSS-0302 OOLI0-12-019-F-S Collect Date: April 30,2014 Client Matrix: Soil Receive Date: M~y 13,2014 Amount of Sample Received: Report Date: June 02,2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty l\IDC LLD TPU Units Cs-136 05/14114 u -2.94E-03 3.32E-02 5.61E-02 3.32E-02 pCi/g Cs-137 05/14/14 M 3.19E-02 l.96E-02 2.24E-02 7.58E-Ol l.97E-02 pCi/g Ba-133 05/14114 u 7.48E-03 1.56E-02 2.36E-02 l.60E-02 pCi/g Ba-140 05/14/14 u 2.54E-02 4.06E-02 4.67E-02 4.22E-02 pCi/g Ce-139 05/14114 u 2.27E-03 1.27E-02 2.19E-02 l.27E-02 pCi/g Ce-141 05/14114 u. 7.78E-03 4.32E-02 4.71E-02 4.33E-02 pCi/g Ce-144 05/14/14 u -4.13E-02 8.66E-02 1.48E-Ol 8.87E-02 pCi/g Nd-147 05/14114 u -3.72E-02 1.73E-01 2.90E-Ol 1.74E-01 pCi/g Pm-144 05/14114 u l.04E-02 l.06E-02 l.92E-02 l.16E-02 pCi/g Pm-146 05/14/14 u 8.59E-03 1.84E-02 2.46E-02 l.88E-02 pCi/g Eu-152 05/14114 u -9.05E-03 4.22E-02 5.99E-02 1.0!E+OO 4.24E-02 pCi/g Eu-154 05/14/14 u -1.47E-03 5.05E-02 7.23E-02 9.40E-01 5.05E-02 pCi/g Eu-155 05/14/14 u 3.9!E-02 6.69E-02 8.76E-02 6.70E-02 pCi/g Ir-192 05/14/14 u 5.31E-03 1.25E-02 2.13E-Or l.27E-02 pCi/g Hg-203 05/14/14 u 2.08E-02 2.93E-02 2.36E-02 2.94E-02 pCi/g Tl-208 05/14114 l.60E-01 2.70E-02 1.93E-02 3.00E-02 pCi/g Pb-210 05/14/14 u -4.14E+OO 3.13E+OO 4.94E+OO 3.66E+OO pCi/g Pb-212 05/14/14 6.22E-01 4.45E-02 3.74E-02 7.12E-02 pCi/g Pb-214 05/14114 5.53E-01 5.92E-02 4.52E-02 7.52E-02 pCi/g Bi-212 05/14/14 UI 3.86E-01 3.20E-Ol 3.86E-Ol 4.33E-01 pCi/g Bi-214 05/14114 4.04E-Ol 6.30E-02 3.91E-02 7.12E-02 pCi/g Ra-228 05/14/14 5.23E-Ol l.03E-Ol 7.73E-02 l.24E-01 pCi/g Ac-228 05/14/14 5.23E-01 l.03E-Ol 7.73E-02 1.24E-Ol pCi/g Th-234 05/14/14 u 9.79E-Ol 9.29E-Ol 1.40E+OO 9.58E-Ol pCi/g U-235 05/14/14 u 2.55E-02 l.41E-01 1.49E-01 1.42E-Ol pCi/g U-238 05/14/14 u 9.79E-Ol 9.29E-Ol l.40E+OO 9.58E-01 pCi/g Np-237 05/14/14 u -1.04E-02 2.46E-02 4.00E-02 l.l !E-01 2.51E-02 pCi/g Np-239 05/14/14 u -3.3!E-02 1.93E-Ol 3.llE-01 l.94E-Ol pCi/g Am-241 05/14/14 u 1.49E-Ol l.llE-01 l.77E-Ol l.3 !E-01 pCi/g Notes: 1. LLDs are a-priori values.

2. l\IDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units offt3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD. UI Uncertain identification for gamma spectroscopy. X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. M Reported result is less than the LLD and greater than the l\IDC. Page 38 of 58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 395 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis GEL Sample ID: 348598003 Client: Pacific Gas and Electric Company Client Sample ID: FSS-0266 OOLl0-11-003-F-S Coliect Date: April 28, 2014 Client Matrix: Soil Receive Date: May 13, 2014 Amount of Sample Received: Report Date: June 02, 2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty MDC LLD TPU Units C-14 05/23/14 u -3.00E-01 3.31E-Ol 5.64E-Ol 6.30E-Ol 3.3 IE-01 pCi/g Ni-63 05/22/14 u -2.49E+OO 2.43E+ol 4.09E+Ol 7.24E+Ol 2.43E+Ol pCi/g Sr-90 05/29/14 u l.14E-02 4.20E-02 6.68E-02 l.51E-Ol 4.20E-02 pCi/g Tc-99 05/25114 u 3.32E-02 4.38E-Ol 7.34E-Ol 1.24E+OO 4.38E-Ol pCi/g Pu-241 05/27/14 u -l.70E+OO 2.35E+Ol 3.97E+Ol 8.61E+Ol 2.35E+Ol pCi/g Alpha Spec Pu-238 05/21/14 u -l.87E-02 8.26E-02 2.16E-Ol 2.97E+OO 8.28E-02 pCi/g Pu-239/240 05/21/14 u l.40E-02 l.65E-Ol 3.48E-Ol 2.67E+OO l.65E-Ol pCi/g Am-241 05/21/14 u -5.47E-02 7.71E-02 2.52E-Ol 2.58E+OO 7.72E-02 pCi/g Cm-243/244 05/21/14 u 8.88E-02 l.28E-Ol l.54E-Ol 2.90E+OO l.28E-Ol pCi/g Cm-245/246 05/21/14 u -1.79E-02 7.91E-02 2.06E-Ol l.78E+OO 7.92E-02 pCi/g Gamma Spec Be-7 05/14/14 u 9.29E-02 1.38E-O1 2. l 7E-Ol l.38E-Ol pCi/g Na-22 05/14/14 u -8.0IE-03 l.69E-02 2.67E-02 l.73E-02 pCi/g K-40 05/14/14 l.22E+O 1 6. 6 !E-0 1 l.28E-Ol 1.23E+OO pCi/g Cr-51 05/14/14 u l.49E-O 1 l.48E-O 1 2.64E-Ol l.63E-Ol pCi/g Mn-54 05/14/14 u 5.18E-03 l.42E-02 2.41E-02 l.44E-02 pCi/g Fe-59 05/14/14 u 5.32E-03 3 .74E-02 6.38E-02 3.75E-02 pCi/g Co-56 05/14/14 u -1.14 E-02 I. 51 E-02 2.31E-02 l.60E-02 pCi/g Co-57 05/14/14 u l.02E-02 l.l 5E-02 2.00E-02 l.24E-02 pCi/g Co-58 05/14/14 u -1.93E-03 l.40E-02 2.29E-02 l.40E-02 pCi/g Co-60 05/14/14 u 1.21E-02 l.39E-02 2.55E-02 3.82E-Ol l.50E-02 pCi/g Ni-59 05/21/14 u -2.84E+OO 4.85E+OO 5.34E+OO 1.97E+02 5.03E+OO pCi/g Zn-65 05/14/14 u l.6 lE-02 4.l 8E-02 6.31E-02 4.25E-02 pCi/g Y-88 05/14/14 u 2.68E-03 l.04E-02 l.82E-02 l.04E-02 pCi/g Zr-95 05/14/14 u l.94E-03 2.81E-02 4.70E-02 2.81E-02 pCi/g Nb-94 05/14/14 u l.02E-02 l.28E-02 2.27E-02 7.13E-Ol l.36E-02 pCi/g Nb-95 05/14/14 u l.55E-02 2. l lE-02 3.25E-02 2.23E-02 pCi/g Ru-106 05/14/14 u 4.57E-02 l.13E-01 l.97E-Ol 1.15E-Ol pCi/g Ag-llOm 05/14/14 u 6.00E-03 l.6 IE-02 2.87E-02 1.64E-02 pCi/g Sn-113 05/14/14 u 2.18E-03 l.73E-02 2.90E-02 l.73E-02 pCi/g Sb-124 05/14/14 u 2.08E-02 2.61E-02 4.96E-02 2.77E-02 pCi/g Sb-125 05/14/14 u l.59E-02 3.46E-02 5.89E-02 3.54E-02 pCi/g I-129 05/27/14 u -2.12E-02 1.49E-Ol 2.llE-01 5.00E-01 l.50E-Ol pCi/g Cs-134 05/14/14 UI 3.09?-02 2.28E-02 3.09E-02 2.91E-02 pCi/g Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units offt3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD. UI Uncertain identification for gamma spectroscopy. X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. M Reported result is less than the LLD and greater than the MDC. Page 39 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 396 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis GEL Sample ID: 348598003 Client: Pacific Gas and Electric Company Client Sample ID: FSS-0266 OOLI0-11-003-F-S Collect Date: April 28,2014 Client Matrix: Soil Receive Date: May 13,2014 Amount of Sample Received: Report Date: June 02,2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty MDC LLD TPU Units Cs-136 05/14/14 u 3.28E-02 4.37E-02 7.86E-02 4.64E-02 pCi/g Cs-137 05114114 M 5.74E-02 2.16E-02 2.29E-02 7.58E-Ol 2.21E-02 pCi/g Ba-133 05/14/14 u -4.78E-03 l.83E-02 2.62E-02 l.84E-02 pCi/g Ba-140 05/14/14 u 3.36E-02 2.78E-02 5.25E-02 3.18E-02 pCi/g Ce-139 05/14/14 u -l.33E-02 l.29E-02 2.0lE-02 l.45E-02 pCi/g Ce-141 05/14/14 u 2.0lE-02 3.03E-02 4.65E-02 3.17E-02 pCi/g Ce-144 05/14/14 u 8.86E-02 1.0lE-01 l.57E-Ol l.09E-Ol pCi/g Nd-147 05/14/14 u 8.85E-02 2.19E-Ol 3.86E-Ol 2.23E-Ol pCi/g Pm-144 05/14/14 u 8.82E-04 1.25E-02 2.lOE-02 l.25E-02 pCi/g Pm-146 05/14114 u -3.70E-03 l.55E-02 2.50E-02 l.56E-02 pCi/g Eu-152 05/14/14 u 2.16E-02 3.77E-02 6.12E-02 l.OlE+OO 3.90E-02 pCi/g Eu-154 05/14/14 u -3.26E-02 4.90E-02 7.58E-02 9.40E-Ol 5.12E-02 pCi/g Eu-155 05/14/14 u l.38E-02 4.74E-02 8.l lE-02 4.78E-02 pCi/g Ir-192 05/14/14 u -4.74E-03 l.38E-02 2.28E-02 l.39E-02 pCi/g Hg-203 05/14/14 u 7.43E-03 l.71E-02 2.64E-02 l.75E-02 pCi/g Tl-208 05/14/14 l.64E-Ol 3.05E-02 2.23E-02 3.33E-02 pCi/g Pb-210 05/14/14 u -l.57E+OO 3.33E+OO 5.17E+o0 3.41E+OO pCi/g Pb-212 05/14/14 5.58E-Ol 4.24E-02 3.70E-02 6.35E-02 pCi/g Pb-214 05/14/14 5.94E-Ol 6.39E-02 4.47E-02 8.05E-02 pCi/g Bi-212 05/14114 7.90E-Ol 3.58E-Ol 2.58E-Ol 3.65E-Ol pCi/g Bi-214 05/14/14 5.00E-01 5.75E-02 3.78E-02 7.07E-02 pCi/g Ra-228 05/14114 4.94E-Ol l.17E-Ol 9.13E-02 l.32E-Ol pCi/g Ac-228 05/14114 4.94E-Ol l.17E-Ol 9.13E-02 l.32E-Ol pCi/g Th-234 05/14/14 u l.02E+OO 1.21E+OO l.31E+OO l.23E+OO pCi/g U-235 05/14/14 u l.17E-Ol l.15E-Ol 1.42E-Ol l.16E-Ol pCi/g U-238 05/14/14 u l.02E+OO l.21E+OO 1.3 lE+OO 1.23E+o0 pCi/g Np-237 05/14114 u -3.21E-03 2.44E-02 4.09E-02 l.l lE-01 2.44E-02 - pCi/g Np-239 05/14/14 u 3.35E-02 l.78E-Ol 3.02E-Ol l.79E-Ol pCi/g Am-241 05/14/14 u 4.69E-02 l.06E-Ol 1.70E-Ol l.08E-Ol pCi/g Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units offt3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD. UI Uncertain identification for gamma spectroscopy. X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. M Reported result is less than the LLD and greater than the MDC. Page 40 o{58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 397 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis GEL Sample ID: 348598004 Client: Pacific Gas and Electric Company Client Sample ID: FSS-0279 OOLI0-11-016-F-S Collect Date: April 29,2014 Client Matrix: Soil Receive Date: May 13,2014 Amount of Sample Received: Report Date: June 02,2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty MDC LLD TPU Units C-14 05/23/14 u -1.72E-01 3.46E-01 5.85E-01 6.30E-01 3.46E-01 pCi/g Ni-63 05/22/14 u 3.02E+OO 2.45E+Ol 4.IOE+Ol 7.24E+Ol 2.45E+Ol pCi/g Sr-90 05/30/14 u 4.45E-02 4.39E-02 6.16E-02 1.51E-01 4.47E-02 pCi/g Tc-99 05/25/14 u -2.79E-01 4.79E-01 8.18E-01 1.24E+OO 4.79E-01 pCi/g Pu-241 05/27/14 u -9.53E+OO 2.60E+Ol 4.45E+Ol 8.61E+Ol 2.60E+Ol pCi/g Alpha Spec Pu-238 05/21/14 u -3.98E-02 9.23E-02 2.73E-01 2.97E+OO 9.25E-02 pCi/g Pu-239/240 05/21/14 u -4.98E-02 9.43E-02 2.91E-01 2.67E+OO 9.45E-02 pCi/g Am-241 05/23/14 u lJOE-01 2.37E-Ol 2.92E-01 2.58E+OO 2.38E-01 pCi/g Cm-243/244 05/23/14 u 2.66E-01 3.0IE-01 2.88E-01 2.90E+OO 3.04E-01 pCi/g Cm-245/246 05/23/14 u -9.53E-03 1.58E-01 3.34E-01 1.78E+OO 1.58E-01 pCi/g Gamma Spec Be-7 05/14/14 2.53E-01 l.46E-01 2.13E-01 1.48E-01 pCi/g Na-22 05/14/14 u -1.54E-02 1.77E-02 2.68E-02 1.90E-02 pCi/g K-40 05/14/14 1.23E+Ol 6.81E-01 1.82E-01 l.24E+OO pCi/g Cr-51 05/14/14 u 1.75E-01 1.54E-01 2.81E-01 1.74E-01 pCi/g Mn-54 05/14/14 u 4.87E-03 l.35E-02 2.38E-02 l.37E-02 pCi/g Fe-59 05/14/14 u 4.52E-02 3.28E-02 6.23E-02 3.93E-02 pCi/g Co-56 05/14/14 u -5.16E-03 1.47E-02 2.43E-02 1.49E-02 pCi/g Co-57 05/14/14 u 7.48E-03 l.34E-02 2.31E-02 l.38E-02 pCi/g Co-58 05/14/14 u -1.lOE-02 l.57E-02 2.53E-02 l.65E-02 pCi/g Co-60 05/14/14 u -4.69E-03 l.35E-02 2.12E-02 3.82E-01 l.36E-02 pCi/g Ni-59 05/22/14 u -1.24E+Ol 1.45E+Ol 2.31E+ol 1.97E+02 1.56E+Ol pCi/g Zn-65 05/14/14 u -7.54E-03 3.91E-02 5.49E-02 3.92E-02 pCi/g Y-88 05/14/14 u -8.60E-03 9.44E-03 1.17E-02 1.02E-02 pCi/g Zr-95 05/14/14 u 4.70E-02 2.73E-02 5.17E-02 3.48E-02 pCi/g Nb-94 05/14/14 u -5.89E-04 l.26E-02 2.07E-02 7.13E-01 l.26E-02 pCi/g Nb-95 05/14/14 UI 3.llE-02 l.73E-02 3.l IE-02 2.48E-02 pCi/g Ru-106 05/14/14 u -3.68E-02 l.30E-01 2.1 IE-01 l.31E-Ol pCi/g Ag-llOm 05/14/14 u -1.92E-02 1.86E-02 2.87E-02 2.07E-02 pCi/g Sn-113 05/14/14 u 1.90E-02 1.82E-02 3.29E-02 2.0IE-02 pCi/g Sb-124 05/14/14 u 6.30E-03 2.32E-02 4.16E-02 2.34E-02 pCi/g Sb-125 05/14/14 u 3.44E-02 3.94E-02 6.30E-02 4.25E-02 pCi/g 1-129 05/27/14 u -6.99E-04 l.23E-01 2.00E-01 5.00E-01 1.23E-01 pCi/g Cs-134 05/14/14 u 2.IOE-02 l.75E-02 3.22E-02 2.00E-02 pCi/g Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units offt3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD. UI Uncertain identification for gamma spectroscopy. X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. M Reported result is less than the LLD and greater than the MDC. Page 41 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 398 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis GEL Sample ID: 348598004 Client: Pacific Gas and Electric Company Client Sample ID: FSS-0279 OOLl0-11-016-F-S Collect Date: April 29,2014 Client Matrix: Soil Receive Date: May 13,2014 Amount of Sample Received: Report Date: June 02,2014 2 Sigma 2 Sigma Isotope Run Date Qualifier Activity Uncertainty MDC LLD TPU Units Cs-136 05/14/14 u -1.79E-02 4.13E-02 6.67E-02 4.22E-02 pCi/g Cs-137 05/14/14 M 4.l IE-02 1.86E-02 2.65E-02 7.58E-01 l.88E-02 pCi/g Ba-133 05/14/14 u 6.63E-03 l.88E-02 2.89E-02 l.9IE-02 pCi/g Ba-140 05/14/14 u -l.87E-03 2.93E-02 4.63E-02 2.93E-02 pCi/g Ce-139 05/14/14 u -5.2IE-03 l.44E-02 2.37E-02 l.46E-02 pCi/g Ce-141 05/14/14 UI 4.85E-02 6.64E-02 4.85E-02 6.66E-02 pCi/g Ce-144 05/14/14 u -6.34E-03 I.16E-Ol l.7IE-Ol l.16E-01 pCi/g Nd-147 05/14/14 u 5.19E-02 2.09E-Ol 3.59E-Ol 2.l IE-01 pCi/g Pm-144 05/14/14 u 5.57E-03 l.27E-02 2.BE-02 l.30E-02 pCi/g Pm-146 05/14/14 u -2.3 lE-03 l.59E-02 2.66E-02 l.59E-02 pCi/g Eu-152 05/14/14 u l.77E-02 4.23E-02 6.82E-02 l.OIE+OO 4.3IE-02 pCi/g Eu-154 05/14/14 u -3.24E-02 4.9IE-02 7.62E-02 9.40E-Ol 5.13E-02 pCi/g Eu-155 05/14/14 u 8.54E-02 6.37E-02 9.52E-02 6.42E-02 pCi/g Ir-192 05/14114 u -4.75E-03 l.47E-02 2.49E-02 I.49E-02 pCi/g Hg-203 05/14/14 u 5.69E-03 l.81E-02 3.00E-02 I.83E-02 pCi/g Tl-208 05/14/14 l.82E-Ol 2.69E-02 2.22E-02 3.06E-02 pCi/g Pb-210 05/14/14 u l.82E+OO 2.67E+OO 4.73E+OO 2.80E+OO pCi/g Pb-212 05/14/14 4.9IE-01 4.6IE-02 4.6IE-02 6.17E-02 pCi/g Pb-214 05/14/14 5.57E-Ol 7.20E-02 5.lOE-02 8.50E-02 pCi/g Bi-212 05/14/14 4.56E-01 2.48E-Ol 2.87E-01 2.52E-Ol pCi/g Bi-214 05/14/14 4.67E-Ol 6.13E-02 4.45E-02 7.19E-02 pCi/g Ra-228 05/14/14 4.34E-Ol l.27E-01 8.29E-02 l.38E-01 pCi/g Ac-228 05/14/14 4.34E-01 l.27E-Ol 8.29E-02 l.38E-01 pCi/g Th-234 05/14/14 u l.6IE-Ol l.20E+OO l.43E+OO 1.20E+OO pCi/g U-235 05/14/14 UI l.75E-01 2.09E-Ol I.75E-01 2.lOE-01 pCi/g U-238 05/14/14 u l.6IE-Ol l.20E+OO l.43E+OO l.20E+OO pCi/g Np-237 05/14/14 u l.47E-03 2.67E-02 4.60E-02 l.llE-01 2.67E-02 pCi/g Np-239 05/14/14 u -l.94E-Ol 2.lOE-01 3.43E-Ol 2.28E-01 pCi/g Am-241 05/14/14 u l.38E-01 l.IOE-01 l.78E-01 l.27E-Ol pCi/g Notes: 1. LLDs are a-priori values.

2. MDCs are calculated a-posteriori values.

3. Gamma spectroscopy analysis results are calculated from a measurement using only one gamma energy line.

4. Air sample volumes are received in units offt3. GEL converts the units and reports them as m3.

Qualifiers: U Target isotope was analyzed for but not detected above the MDC and LLD. UI Uncertain identification for gamma spectroscopy. X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. M Reported result is less than the LLD and greater than the MDC. Page 42of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 399 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 Quality Control Data Page 43of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 400 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: June 2, 2014 Client: Pacific Gas and Electric, Humboldt Bay Power Plant Page 1 of 15 1000 King Salmon Avenue Eureka, California

Contact:

Ms. Dee Anderson Workorder: 348598 Parm name NOM Sam11Ie Qua! QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1387983 QC1203088581 348598001 DUP Arnericium-241 u 0.0943 u -0.0456 pCilg 0 NIA JXRI 05/23/1409:41 Uncert: +l-0.186 +l-0.193 TPU: +l-0.187 +l-0.194 Curium-2431244 u 0.0321 u 0.0713 pCilg 0 NIA Uncert: +l-0.258 +l-0.263 TPU: +l-0.258 +l-0.263 Curium-2451246 u 0.128 u -0.0261 pCilg 0 NIA Uncert: +l-0.185 +l-0.217 TPU: +l-0.186 +l-0.218 QC1203088582 LCS Americium-241 6.88 6.53 pCilg 94.9 (75%-125%) JXRl 0512111413:12 Uncert: +l-0.871 TPU: +l-1.16 Curium-2431244 13.9 12.3 pCi/g 88.9 (75%-125%) Un cert: +l-1.19 TPU: +l-1.87 Curium-2451246 M 0.377 pCi/g Uncert: +l-0.233 TPU: +l-0.237 QC1203088580 MB

Americium-241 u 0.112 pCi/g JXRI 05/2311409:41 Uncert: +l-0.218 TPU: +l-0.218 Curium-2431244 u -0.0376 pCi/g Uncert: +l-0.128 TPU: +l-0.129 Curium-2451246 u 0.0641 pCi/g Uncert: +l-0.203 TPU: +l-0.204 Batch 1387984 QC1203088588 348598001 DUP Plutonium-238 u -0.0233 u 0.0351 pCilg 0 NIA JXRl 0512111412:50 Uncert: +l-0.161 +l-0.132 TPU: +l-0.161 +l-0.132 Plutonium-2391240 u 0.148 u 0.116 pCilg 0 NIA Uncert: +l-0.240 +l-0.185 TPU: +l-0.241 +l-0.186 QC1203088589 LCS Plutonium-238 u 0.106 pCilg (75%-125%) JXRl 0512111412:50 Uncert: +l-0.169 TPU: +l-0.169 Page 44 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 401 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summan:: Workorder: 348598 Page 2 of 15 Parm name NOM Sam{!le Qua[ QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1387984 Plutonium-2391240 9.61 10.3 pCi/g 107 (75%-125%) Un cert: +l-1.30 TPU: +l-I.97 QC1203088587 MB Plutonium-238 u -0.0448 pCi/g JXRl 05121/1,412:51 Uncert: +l-0.104 TPU: +l-0.104 Plutonium-2391240 u -0.0336 pCi/g Uncert: +l-0.102 TPU: +l-0.102 Batch 1387985 QC!203088591 348598001 DUP Plutonium-241 u -17 u -21.4 pCi/g 0 NIA JXRl 0512711411:2: Uncert: +l-30.7 +l-28.5 TPU: +l-30.7 +l-28.5 QC1203088592 LCS Plutonium-241 417 345 pCi/g 82.8 (75%-125%) JXRl 0512711411 :3' Uncert: +l-40.l TPU: +l-85.2 QC!203088590 MB Plutonium-241 u -29.3 pCi/g JXRl 05127/1411:0 Uncert: +l-25.2 TPU: +l-25.2 Batch 1390686 QC1203095526 348598002 DUP Americium-241 u -0.0478 u 0.117 pCi/g 0 NIA JXRl 05129/1410:1* Un cert: +/-0.144 +l-0.266 TPU: +l-0.145 +l-0.267 Curium-2431244 u 0.0184 M 0.518 pCi/g 25.5 (0% - 100%) Uncert: +l-0.192 +l-0.405 TPU: +l-0.192 +l-0.410 Curium-2451246 u 0.0577 u -0.0179 pCi/g 0 NIA Un cert: +l-0.216 +l-0.154 TPU: +l-0.217 +l-0.155 QC1203095527 LCS Americium-241 12.5 12.8 pCi/g 103 (75%-125%) JXRl 05129/1410:1* Uncert: +l-I.63 TPU: +l-2.21 Curium-2431244 25.2 24.3 pCi/g 96.5 (75%-125%) Uncert: +l-2.21 TPU: +l-3.61 Curium-2451246 M 1.17 pCi/g Uncert: +l-0.548 TPU: +l-0.565 QC1203095525 MB Page 45of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 402 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 403 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com QC Summary Workorder: 348598 Page 4 of 15 Parm name NOM Sam~le Qnal QC Units RPD% REC% Range Anlst Date Timf Rad Gamma Spec Batch 1387698

                                         +l-0.139 Bismuth-212                             0.688                0.448     pCi/g    42.3        (0%-100%)

Un cert: +l-0.293 +l-0.271 TPU: +l-0.300 +l-0.274 Bismuth-214 0.473 0.450 pCi/g 5.01 (0%-20%) Un cert: +l-0.0626 +l-0.063 TPU: +l-0.0733 +l-0.0731 Cerium-139 u 0.00721 u 0.00293 pCi/g 0 NIA Uncert: +l-0.0163 +l-0.0134 TPU: +l-0.0167 +l-0.0134 Cerium-141 u 0.0123 u 0.00617 pCi/g 0 NIA Uncert: +l-0.0322 +l-0.0274 TPU: +l-0.0327 +/-0.0276 Cerium-144 u -0.00997 u 0.0137 pCi/g 0 NIA Uncert: +l-0.0984 +l-0.0991 TPU: +l-0.0986 +l-0.0993 Cesium-134 Ul 0.00 u 0.018 pCi/g 0 NIA Uncert: +l-0.0225 +l-0.0302 TPU: +l-0.0326 +/-0.0313 Cesium-136 Ul 0.00 u 0.0101 pCi/g 0 NIA Uncert: +l-0.0477 +l-0.0388 TPU: +l-0.0604 +l-0.0391 Cesium-137 M 0.111 M 0.140 pCi/g 23.2* (0%-20%) Un cert: +l-0.0308 +l-0.0311 TPU: +l-0.032 +l-0.0331 Chromium-SI u -0.123 u -0.106 pCi/g 0 NIA Un cert: +l-0.157 +l-0.154 TPU: +l-0.167 +l-0.161 Cobalt-56 u 0.000896 u -0.00779 pCi/g 0 NIA Un cert: +l-0.0146 +l-0.0159 TPU: +/-0.0146 +l-0.0163 Cobalt-57 u 0.00285 u 0.00688 pCi/g 0 NIA Uncert: +l-0.0129 +l-0.012 TPU: +l-0.0129 +l-0.0124 Cobalt-58 u 0.00964 u -0.00162 pCi/g 0 NIA Uncert: +l-0.0159 +l-0.0168 TPU: +l-0.0165 +l-0.0168 Cobalt-60 u 0.011 u 0.0104 pCi/g 0 NIA Uncert: +l-0.0156 +l-0.0168 TPU: +l-0.0163 +l-0.0175 Europium-152 u -0.0183 u -0.0477 pCi/g 0 NIA Uncert: +l-0.0496 +l-0.0424 TPU: +l-0.0503 +l-0.0477 Europium-154 u -0.0164 u 0.0559 pCi/g 0 NIA Uncert: +l-0.0475 +l-0.0792 TPU: +l-0.0481 +l-0.0832 Page 47of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 404 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 348598 Page 5 of 15 Parm name NOM Sam~le Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1387698 Europium-155 u 0.074 u 0.0261 pCi/g 0 NIA Uncert: +l-0.0561 +l-0.0504 TPU: +l-0.0656 -+l-0.0518 lridium-192 u -0.00463 u 0.00732 pCi/g 0 NIA Uncert: +l-0.015 +l-0.0144 TPU: +l-0.0151 +l-0.0148 Iron-59 u -0.00595 u -0.0149 pCi/g 0 NIA Uncert: +l-0.0353 +l-0.041 TPU: +l-0.0354 +l-0.0416 Lead-210 u 1.39 u 1.95 pCi/g 0 NIA Uncert: +l-2.77 +l-3.64 TPU: +l-2.85 +l-3.75 . Lead-212 0.594 0.582 pCilg 1.97 (0%-20%) Uncert: +l-0.0462 +l-0.0483 TPU: +l-0.0677 +l-0.0691 Lead-214 0.537 0.556 pCi/g 3.61 (0%-20%) Uncert: +l-0.0678 +l-0.0708 TPU: +l-0.0806 +l-0.0843 Manganese-54 u -0.00573 u -0.00582 pCilg 0 NIA Uncert: +l-0.0146 +l-0.015 TPU: +l-0.0149 +l-0.0152 Mercury-203 u 0.0157 u 0.00301 pCi/g 0 NIA Uncert: +l-0.0201 +l-0.0178 TPU: +l-0.0213 +l-0.0178 Neodymium-147 u 0.00497 u -0.0814 pCilg 0 NIA Uncert: +l-0.214 +l-0.222 TPU: +l-0.214 +l-0.225 Neptunium-237 u O.Dl5 u -0.00356 pCi/g 0 NIA Uncert: +l-0.0277 +l-0.0273 TPU: +l-0.0285 +l-0.0274 Neptunium-239 u -0.0392 u -0.0849 pCi/g 0 NIA Uncert: +l-0.212 +l-0.192 TPU: +l-0.213 +l-0.196 Niobium-94 u -0.00888 u -0.00143 pCi/g 0 NIA Uncert: +l-0.0142 +l-0.0138 TPU: +l-0.0148 +l-0.0138 Niobium-95 u 0.0212 u 0.0328 pCi/g 0 NIA Uncert: +l-0.0187 +l-0.0198 TPU: +l-0.0211 +l-0.0249 Potassium-40 12.4 12.7 pCilg 2.38 (0%-20%) Uncert: +l-0.703 +l-0.715 TPU: +l-1.26 +l-1.29 Promethium-144 u 0.00107 u -0.000129 pCilg 0 NIA Uncert: +l-0.0143 +l-0.0128 TPU: +l-0.0143 +l-0.0128 Promethium-146 u -0.00127 u -0.0012 pCilg 0 NIA Page 48 of 58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 405 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com QC Summan: Workorder: 348598 Page 6 of 15 Parm name NOM Sam[>le Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1387698 Uncert: +l-0.0163 +l-0.0183 TPU: +/-0.0163 +l-0.0183 Radium-228 0.605 0.603 pCi/g .397 (0%-20%) Un cert: +l-0.111 +l-0.112 TPU: +l-0.134 +l-0.134 Ruthenium-106 u -0.068 u 0.000686 pCi/g 0 NIA Uncert: +l-0.124 +l-0.130 TPU: +l-0.128 +l-0.130 Silver-1 lOm u -0.00917 u -0.0108 pCi/g 0 NIA Uncert: +l-0.0187 +l-0.0202 TPU: +l-0.0192 +l-0.0208 Sodium-22 u -0.00806 u 0.0204 pCi/g 0 NIA Uncert: +l-0.0169 +l-0.028 TPU: +l-0.0173 +l-0.0295 Thallium-208 0.179 0.155 pCi/g 14.7 (0%-20%) Un cert: +l-0.0238 +l-0.0305 TPU: +l-0.0279 +l-0.0331 Thorium-234 u 1.19 2.21 pCi/g 46.5 (0%- 100%) Un cert: +l-1.19 +l-1.49 TPU: +l-1.22 +l-1.57 Tin-113 u 0.010 u 0.0045 pCi/g 0 NIA Un cert: +l-0.0187 +l-0.0182 TPU: +l-0.0193 +l-0.0183 Uranium-235 u -0.033 u 0.0342 pCi/g 0 NIA Uncert: +l-0.108 +l-0.0917 TPU: +l-0.108 +l-0.0917 Uranium-238 u 1.19 2.21 pCi/g 46.5 (0%-100%) Un cert: +l-1.19 +l-1.49 TPU: +l-1.22 +l-1.57 Yttrium-88 u -0.00349 u -0.00204 pCi/g 0 NIA Uncert: +l-0.0104 +l-0.0101 TPU: +l-0.0105 +l-0.0101 Zinc-65 u -0.0259 u 0.0163 pCi/g 0 NIA Uncert: +l-0.0435 +l-O.D426 TPU: +l-0.0452 +l-0.0433 Zirconium-95 u 0.0249 u 0.00202 pCi/g 0 NIA Un cert: +l-0.0292 +/-0.0277 TPU: +l-0.0314 +l-0.0277 QC1203087899 LCS Actinium-228 u 0.324 pCi/g MXR.1 05114/1413:3~ Uncert: +/-0.822 TPU: +/-0.836 Americium-241 63.4 73.7 pCi/g 116 (75%-125%) Un cert: +l-2.78 TPU: +/-8.23 Antimony-124 u 0.0325 pCi/g Page 49 of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 406 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 348598 Page 7 of 15 Parm name NOM Sam11Ie Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1387698 Uncert: +/-0.136' TPU: +/-0.136 Antimony-125 u 0.133 pCi/g Un cert: +/-0.407 TPU: +/-0.412 Barium-133 u -0.057 pCi/g Uncert: +/-0.189 TPU: +/-0.191 Barium-140 u 0.0267 pCi/g Un cert: +/-0.0602 TPU: +/-0.0615 Beryllium-7 u -0.835 pCi/g Uncert: +/-1.21 TPU: +/-1.27 Bismuth-212 u 0.706 pCi/g Un cert: +/-1.89 TPU: +/-1.92 Bismuth-214 0.685 pCi/g Uncert: +/-0.417 TPU: +/-0.522 Cerium-139 u -0.0924 pCi/g Uncert: +/-0.104 TPU: +/-0.114 Cerium-141 u -0.11 pCi/g Un cert: +/-0. 188 TPU: +/-0.195 Cerium-144 u 0.0381 pCi/g Uncert: +/-0.832 TPU: +/-0.832 Cesium-134 u 0.0741 pCi/g Uncert: +/-0.162 TPU: +/-0.165 Cesium-136 u 0.0719 pCi/g Un cert: +/-0.257 TPU: +/-0.259 Cesium-137 23.1 24.1 pCi/g 104 (75%-125%) Un cert: +/-0.615 TPU: +/-2.16 Chromium-51 u -0.562 pCi/g Un cert: +/-1.06 TPU: +/-1.09 Cobalt-56 u -0.0348 pCi/g Un cert: +/-0.151 TPU: +/-0.152 Cobalt-57 0.407 pCi/g Uncert: +/-0.173 TPU: Page 50 of 58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 407 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Attachment 3: Lab Data for OOL 10-11 & OOL 10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summa1:y

       \Vorkorder:     348598                                                                        Page 8 of 15 Parmname                 NOM          Sam~le Qua)         QC     Units   RPD%     REC%       Range Anlst    Date Time Rad Gamma Spec Batch         1387698
                                                            +/-0.178 Cobalt-58                                       u      0.0368      pCi/g Uncert:                    +/-0.162 TPU:                     +/-0.163 Cobalt-60              22.9                               23.5     pCi/g            102   (75%-125%)

Uncert: +/-0.664 TPU: +/-1.94 Europimn-152 u -0.239 pCi/g Uncert: +/-0.416 TPU: +/-0.431 Europimn-154 u 0.197 pCi/g Uncert: +/-0.270 TPU: +/-0.285 Europimn-155 u -0.258 pCi/g Uncert: +/-0.447 TPU: +/-0.463 Iridimn-192 u -0.013 pCi/g Uncert: +/-0.126 TPU: +/-0.126 Iron-59 u 0.139 pCi/g Uncert: +/-0.323 TPU: +/-0.330 Lead-210 876 pCi/g Uncert: +/-97.6 TPU: +/-129 Lead-212 1.07 pCi/g Uncert: +/-0.345 TPU: +/-0.359 Lead-214 1.51 pCi/g Uncert: +/-0.489 TPU: +/-0.507 Manganese-54 u -0.065 pCi/g Uncert: +/-0.152 TPU: +/-0.155 Mercury-203 u 0.041 pCiig Uncert: +/-0.122 TPU: +/-0.124 Neodymimn-147 u 0.927 pCi/g Uncert: +/-0.899 TPU: +/-0.994 Neptunium-237 0.255 pCilg Uncert: +/-0.272 TPU: +/-0.296 Neptunimn-239 u -0.276 pCi/g Uncert: +/-1.97 TPU: +/-1.97 Page 51 of58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 408 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder:. 348598 Page 9 of 15 Parmname NOM Sam(!le Qnal QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1387698 Niobium-94 u 0.0142 pCi/g Uncert: +/-0.120 TPU: +/-0.120 Niobium-95 u -0.0196 pCi/g Uncert: +/-0.135 TPU: +/-0.135 Potassium-40 1.77 pCi/g Uncert: +/-0.577 TPU: +/-0.996 Promethium-144 u -0.00584 pCi/g Uncert: +/-0.114 TPU: +/-0.114 Promethium-146 u 0.0979 pCi/g Uncert: +/-0.203 TPU: +/-0.208 Radium-228 u 0.324 pCi/g Uncert: +/-0.822 TPU: +/-0.836 Ruthenium-106 u -0.873 pCi/g Uncert: +/-1.18 TPU: +/-1.25 Silver-l!Om u 0.124 pCi/g Uncert: +/-0.275 TPU: +/-0.281 Sodium-22 u 0.068 pCi/g Uncert: +/-0.0945 TPU: +/-0.0995 Thallium-208 0.253 pCi/g Uncert: +/-0.184 TPU: +/-0.185 Thorium-234 u -0.604 pCi/g Uncert: +/-8.06 TPU: +/-8.07 Tin-113 u 0.0161 pCi/g Uncert: +/-0.171 TPU: +/-0.172 Uranium-235 u 0.195 pCi/g Uncert: +/-0.819 TPU: +/-0.824 Uranium-238 u -0.604 pCi/g Uncert: +/-8.06 TPU: +/-8.07 Yttrium-88 u 0.0174 pCi/g Uncert: +/-0.0523 TPU: +/-0.0529 Zinc-65 u -0.139 pCi/g Page 52of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 409 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com QC Summary Workorder: 348598 Page 10 of 15 Parm name NOM Sam~le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1387698 Un cert: +/-0.417 TPU: +/-0.422 Zirconium-95 u 0.100 pCi/g Uncert: +/-0.238 TPU: +/-0.243 QC1203087897 ]\,ffi Actinium-228 u -0.00931 pCi/g MXRI 05/14/1413:3* Uncert: +/-0.0241 TPU: +/-0.0245 Americium-241 u 0.00265 pCi/g Uncert: +/-0.0353 TPU: +/-0.0354 Antimony-124 u 0.013 pCi/g Un cert: +/-0.0131 TPU: +/-0.0143 Antimony-125 u 0.014 pCi/g Uncert: +/-0.0142 TPU: +/-0.0156 Barium-133 u -0.00334 pCi/g Un cert: +/-0.00738 TPU: +/-0.00754 Barium-140 u 0.00351 pCi/g Un cert: +/-0.00722 TPU: +/-0.0074 Beryllium-7 u -0.00258 pCi/g Un cert: +/-0.0475 TPU: +/-0.0475 Bismuth-212 u -0.0287 pCi/g Un cert: +/-0.0735 TPU: +/-0.0747 Bismuth-214 u 0.00289 pCi/g Uncert: +/-0.0133 TPU: +/-0.0134 Cerium-139 u -0.0016 pCi/g Uncert: +/-0.00455 TPU: +/-0.00462 Cerium-141 u 0.00271 pCi/g Uncert: +/-0.00775 TPU: +/-0.00785 Cerium-144 u 0.0121 pCi/g Uncert: +/-0.0297 TPU: +/-0.0302 Cesium-134 u -0.00137 pCi/g Uncert: +/-0.00562 TPU: +/-0.00566 Cesium-136 u -0.00376 pCi/g Page 53of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 410 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 348598 Page 11 of 15 Parm name NOM SamJ:!le Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1387698 Uncert: +/-0.00533 TPU: +/-0.00563 Cesium-137 u 0.00255 pCi/g Un cert: +/-0.00646 TPU: +/-0.00657 Chromium-51 u -0.0015 pCi/g Uncert: +/-0.039 TPU: +/-0.039 Cobalt-56 u -0.00349 pCi/g Uncert: +/-0.0055 TPU: +/-0.00573 Cobalt-57 u 0.00225 pCi/g Un cert: +/-0.00463 TPU: +/-0.00474 Cobalt-58 u -0.00028 pCi/g Uncert: +/-0.00459 TPU: +/-0.00459 Cobalt-60 u -0.000913 pCi/g Uncert: +/-0.00377 TPU: +/-0.0038 Europium-152 u 0.00356 pCi/g Un cert: +/-0.0176 TPU: +/-0.0177 Europium-154 u 0.00459 pCi/g Un cert: +/-0.013 TPU: +/-0.0.132 Europium-155 u -0.00164 pCi/g Uncert: +/-0.0197 TPU: +/-0.0197 Iridium-192 u -0.00125 pCi/g Uncert: +/-0.00502 TPU: +/-0.00505 Iron-59 u 0.0023 pCi/g Un cert: +/-0.00775 TPU: +/-0.00782 Lead-210 u 1.02 pCi/g Un cert: +/-2.06 TPU: +/-2.06 Lead-212 u -0.0112 pCi/g Uncert: +/-0.0107 TPU: +/-0.0119 Lead-214 u 0.00363 pCi/g Uncert: +/-0.0135 TPU: +/-0.0136 Manganese-54 u 0.00293 pCi/g Uncert: +/-0.00484 TPU: Page 54of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 411 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QCSummaa Workorder: 348598 Page 12 of 15 Parm name NOM Sam~le Qua) QC. Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1387698

                                                        +/-0.00502 Mercury-203                                      u     -0.00111      pCi/g Uncert:                   +/-0.00516 TPU:                    +/-0.00518 Neodymium-147                                    u          0.026    pCi/g Un cert:                   +/-0.0331 TPU:                     +/-0.0352 Neptunium-23 7                                   u     -0.00536      pCi/g Uncert:                    +/-0.0107 TPU:                       +/-0.011 Neptunium-239                                    u       -0.0046     pCi/g Uncert:                    +/-0.0736 TPU:                     +/-0.0736 Niobium-94                                       u     -0.00198      pCi/g Un cert:                 +/-0.00533 TPU:                    +/-0.00541 Niobium-95                                       u       0.00151     pCi/g Uncert:                    +/-0.0055 TPU:                    +/-0.00555 Potassium-40                                     u        0.0136     pCi/g Uncert:                    +/-0.0643 TPU:                     +/-0.0646 Promethium-144                                   u        0.0015     pCi/g Uncert:                  +/-0.00499 TPU:                    +/-0.00504 Promethium-146                                   u       0.00206     pCi/g Un cert:                 +/-0.00635 TPU:                    +/-0.00643 Radium-228                                       u     -0.00931      pCi/g Un cert:                   +/-0.0241 TPU:                     +/-0.0245 Ruthenium-106                                    u       -0.0148     pCi/g Uncert:                    +/-0.0501 TPU:                     +/-0.0505 Silver-1 lOm                                     u       0.00354     pCi/g Uncert:                    +/-0.0073 TPU:                    +/-0.00749 Sodium-22                                        u       0.00161     pCi/g Uncert:                  +/-0.00456 TPU:                    +/-0.00462 Tballium-208                                     u     -0.00133      pCi/g Uncert:                  +/-0.00581 TPU:                    +/-0.00584 Thorium-234                                      u     -0.00135      pCi/g Uncert:                      +/-0.319 TPU:                       +/-0.319 Page 55 of 58 FSS Report                          HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12                                   Page 412 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summaa Workorder: 348598 Page 13 of 15 Parm name NOM SamQle Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1387698 Tin-113 u -0.0028 pCi/g Uncert: +/-0.00564 TPU: +/-0.00579 Uranium-235 u -0.0234 pCi/g Uncert: +/-0.036 TPU: +/-0.0375 Uranium-238 u -0.00135 pCi/g Uncert: +/-0.319 TPU: +/-0.319 Yttrium-88 u 0.00223 pCi/g Uncert: +/-0.00651 TPU: +/-0.00659 Zinc-65 u -0.00132 pCi/g Uncert: +/-0.0108 TPU: +/-0.0108 Zirconium-95 u -0.00348 pCi/g Uncert: +/-0.0086 TPU: +/-0.00875 Batch 1387906 QC1203088382 348598001 DUP Iodine-129 u 0.303 u -0.0211 pCi/g 0 N/ABSWl 05/27/1412:35 Uncert: +/-0.335 +/-0.160 TPU: +/-0.363 +/-0.160 QC1203088384 LCS Iodine-129 8.60 6.99 pCi/g 81.3 (75%-125%) BSWl 05/2711412:36 Un cert: +/-0.946 TPU: +/-1.18 QC1203088381 MB Iodine-129 u 0.133 pCi/g BSWl 05/27/1412:34 Uncert: +/-0.221 TPU: +/-0.229 QC1203088383 348598001 MS Iodine-129 9.13 u 0.303 7.31 pCi/g 80.1 (75%-125%) BSWl 05/28/1408: 19 Uncert: +/-0.335 +/-0.696 TPU: +/-0.363 +/-1.01 Rad Gas Flow Batch 1391080 QC1203096527 348598001 DUP Strontium-90 u 0.0167 u 0.000357 pCi/g 0 N/AKSDl 05/29/1416:16 Uncert: +/-0.0541 +/-0.0508 TPU: +/-0.0542 +/-0.0508 QC1203096528 LCS Strontium-90 3.70 4.35 pCi/g 118 (75%-125%) KSDl 05/2911416:16 Un cert: +/-0.251 TPU: +/-0.845 QC1203096526 MB Page 56 of 58 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 413 of 468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843)'556-8171 -www.gel.com QC Summary Workorder: 348598 Page 14 of 15 Parm name NOM SamEle Qual QC Units RPD% REC% Range Anlst Date Time Rad Gas Flow Batch 1391080 Strontium-90 u 0.0608 pCi/g KSDl 05/29/1416:1( Uncert: +/-0.0558 TPU: +/-0.0569 Rad Liquid Scintillation Batch 1387641 QCI203087734 348598003 DUP Nickel-63 u -2.49 u -26.2 pCi/g 0 NIA TYJI 05/22/1420:5t Uncert: +/-24.3 +/-22.9 TPU: +/-24.3 +/-22.9 QCI203087735 LCS Nickel-63 972 999 pCi/g 103 (75%-125%) TYJI 05/22/1421:21 Uncert: +/-39.7 TPU: +/-193 QC1203087733 MB Nickel-63 u -8.7 pCi/g TYJI 05/22/1420:2: Uncert: +/-20.0 TPU: +/-20.0 Batch 1387681 QCl203087838 348598001 DUP Technetium-99 u 0.000424 u 0.117 pCi/g 0 N/AMYMl 05/25/1412:4~ Uncert: +/-0.469 +/-0.479 TPU: +/-0.469 +/-0.480 QC1203087839 LCS Technetium-99 33.6 31.4 pCi/g 93.7 (75%-125%) MYMl 05/25/1413:2: Uncert: +/-0.997 TPU: +/-3.74 QCl203087837 MB Technetium-99 u -0.209 pCi/g MYMl 05/25/1412:0~ Uncert: +/-0.419 TPU: +/-0.419 Batch 1388352 QCl203089506 348598001 DUP Carbon-14 u -0.298 u 0.143 pCi/g 0 N/ABYSl 05/23/1402:5: Uncert: +/-0.340 +/-0.344 TPU: +/-0.340 +/-0.344 QC1203089508 LCS Carbon-14 36.9 38.2 pCi/g 104 (75%-125%) BYSl 05/22/1402:2: Uncert: +/-1.94 TPU: +/-3.39 QCl203089505 MB Carbon-14 u 0.365 pCi/g BYS! 05/2111422:0~ Uncert: +/-0.322 TPU: +/-0.323 QCl203089507 348598001 MS Carbon-14 37.5 u -0.298 39.9 pCi/g 106 (75%-125%) BYSl 05/22/1402:05 Page 57of58 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page414of468

Attachment 3 Lab Data for HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 GEL LABO RATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com QC Summary Workorder: 348598 Page 15 of 15 Parmname NOM Sample Qua! QC Units RPD% REC% Range Anlst Date Timf Rad Liquid Scintillation Batch 1388352 Uncert: +/-0.340 +/-1.99 TPU: +/-0.340 +/-3.52 Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). The Qualifiers in this report are defined as follows: M Result is <LLD and> MDC U Result is <LLD and< MDC UI Uncertain identification for gamma spectroscopy X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.

   **Indicates analyte is a surrogate/tracer compound.                               /

A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample i_s greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the RL is used to evaluate the DUP result. For PS, PSD, and SDIL T results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been perfoml.ed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 58of58 FSSReport HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 415 of 468

Attachment 4 Data Assessment HBPP-FSSP-OOLl0-11 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 416 of 468

Attachment 4 Data Assessment HBPP-FSSP-OOL 10-1 1 OOLl0-11 Frequency Plot 8 7 I/) r:: 6 0 ro Cll I/) 5

           .c 0
             ...0 Cll 4
           .c E

s z 3 2

1 0 0 .006 0 .033 0.060 0.087 0.115 0.142 Bin Upper End Value (pCi/gm) FSS Report HBPP-FSS P-OOL 10-11 & HBPP-FSSP-OOL 10-1 2 Page 417 of 468 L_

Attachmen t 4 Data Assessment HBPP-FSSP-OOL 10-1 1 OO L 10-11 Sample Res ults Quantile Plot 0.16 0.14 .. 0.12 E' 0) 0.1 0.08 I I I I I I I I I I I 0.079 0 s I I I

                                                                 *      *

I I

I I I I I

          *:;:    0.06                          I                                                             I

(.) I I

                                                ~ ------------ - ----------------------J I

I

<(

0.04 I I I I 0.02

0 0
10 20 30 40 50 60 70 80 90 100 Percentile
Direct Measurements - - median -
75th Percentile ----50th Percentile FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 418 of 468

Attachment 4 Data Assessment HBPP-FSSP-OOL 10-11 OOLl0-11 Sample Results Scatter Plot DCGLop = 7.58 pCifgm Cs-137 2.00E-01

0.179 1.50E-01 1.00E-01
0.077 5.00E-02 O.OOE+OO

                                                                                                          *   -0.026
          -5.00E-02

Activity - Average - "+3StDev" - "-3StDev" FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 419 of 468

Attachment 4 Data Assessment HBPP-FSSP-OOL 10-11 Retrospect ive Power Curve OOLl0-11 MARSSIM Power 2000 File Help Swvey Unit ID:

                             ~------         -    ---------
                                                               ~ Decision Alpha :

Errors

                                                                                .6_eta:

rR<q_ S_k S><l Swvey Unit 14 Radionuclide: JUnity Rule ~ Statistical Test 1 ~ ~

                                          <i Sign Test DCGL j7.58                  r WRS Test            o~I I                                  ~ I 7.58 Critical Value:
              .S.igma j.0343        ~                              LBGR J0.0766            Mcr= 218 .78 10
                                    ~                        I Probability that the Survey Unit Passes 1.0 Click anywhere on the graph to 0.8                                                                           update the power curve using newly 0.6                                                                           entered parameter values 0.4 0.2 0.0 11%      30%    5)%         70%        9 % 1 )0% 1 0%

True Survey Unit Concentration (percent of DCGL)

                                                                                    , 0%   1 J0%

Exit Program I FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 420 of 468

Posting Plot OOL10-11 9

                  !.17E41 ...

e

                                                                         -       OOL10-11 Survey Area X.XX E-XX =Result (pCi/g Cs-137) 9     =Sample Point Location FSS Re port                    HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-1 2                                   Pag e 421 of 468

Posting Plot OOL10-11 8

                 .7. . . .
                                                                     -       00110-11 Survey Area X.XX E-XX =Result (pCi/g Sr-90) 9     =Sample Point Location FSS Report                  HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12                                   Page 422 of 468

Attachment 4 Data Assessment HBPP-FSSP-OOL 10-11 RCP FSS-11 Attachment R 1 Rev.QC Page 1 of 1 Split Sample Assessment Form Survey Area No.: 001-10 lsurveyUnitNo.: 11 Survey Unit Name: Fisherman's Channel Sample Plan No.: HBPP-FSS-00110-11-00 Sample Measurement Location: #03 Sample

Description:

Comparison of split samples collected from sample measurement location #03 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The on-site result is the standard count and the off-site is the comparison. STANDARD COMPARISON Agreement Comparison Radio-nuclide Standard Comparison Comparison Ratio Acceptable Range Error Activity lcr chosen Resolution (e) Activity (g) (h)=(f)/(b) (YIN) (b) Uncertainty (a) (c) (d)=(b)/(c) (+/-} K-40 l.19E+ol 9.20E-01 13 0.6-1.66 1.22E+Ol 3.31E-Ol l.03E+OO y Pb-212 4.22E-01 4.65E-02 9 0.6-1.66 5.58E-Ol 2.12E-02 L32E+OO y Comments/Corrective Actions: None. Table 1 is provided to show acceptance-criteria to assess split samples. Resolution (d) Agreement Range (e)

                                                                                            <4                      No Comparison 4-7                           0.5-2.0 8-15                          0.6--1-66 16-50                         0.75-1.33 51-200                        0.80-1.25
                                                                                          >200                         0.85-1.18 Performed By:      /) f'_/ ~' /~                     jDate:   t /'-f. Concurrence: fly\~ -1:-    -r_:-- ;)     iDate: ct h ~¢:

0

                                                                                                         -    {

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 423 of 468

Attachment 4 Data Assessment HBPP-FSSP-OOL 10-11 RCP FSS-11 Attachment 8.1 Rev. DC Page 1 of 1 Split Sample Assessment Form Survey Area No.:* OOL-10 !surveyUnitNo.: 11 Survey Unit Name: Fisherman's Channel Sample Plan No.: HBPP-FSS-OOLI0-11-00 Sample Measurement Location: # 16 Sample

Description:

Comparison of split samples collected from sample measurement location #16 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The on-site result is the standard count and the off-site is the* comparison. STANDARD COMPARISON Agreement Comparison Radio-nuclide Standard Comparison Comparison Ratio Acceptable Range Error Activity lcr chosen Resolution (e) Activity (g) (h)=(f)/(b) (YIN) (b) Uncertainty (a) (c) (d)=(b)/(c) (f) K-40 9.33E+OO 8.60E-01 11 0.6-1.66 l.23F-T-Ol 3.41E-Ol l.32E+OO y Pb-212 3.82E-01 4.64E-02 8 0.6-1.66 4.91E-Ol 2.31E-02 l.29E+OO. y Comments/Corrective Actions: None. Table 1 is provided to show acceptance criteria to assess split samples. Resolution {d) Agreement Range {e)

                                                                                            <4                     No Comparison 4-7                            0.5-2.0 8-15                           0.6-1.66 16-50                         0.75-1.33 51-200                        0.80-1.25
                                                                                           >200                         0.85-1.18 Performed By:   /},,A /,A.           L/              !Date:  °I- (- /lf     Concurrence='yy\ _ ,_,_. 7 _  .... ,tJ    inate:

9~oh4.

                                                                                                         '    (

FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 424 of 468

Attachment 4 Data Assessment HBPP-FSSP-OOL 10-11 RCP FSS-11 Attachment 8.1 Rev.1 Page 1 of 1 Split Sample Assessment Form Survey Area No.: OOL-10 jsurvey Unit No.: 11 Survey Unit Name: Fisherman's Channel Sample Plan No.: HBPP-FSS-OOLl 0-11-00 Sample Measurement Location: 20 Sample

Description:

Comparison of a recounted sample collected from sample measurement location #20 and analyzed using gamma spectroscopy at the on-site laboratory. STANDARD COMPARISON Agreement Comparison Radio-nuclide Standard Comparison Comparison Ratio Acceptable Range Error Activity lcr chosen Resolution (e) Activity (g) (h)=(f)/(b) (YIN) (b) Uncertainty (a) (c) I d)=(b )/(C) (f) K-40 l.06E+Ol 8.90E-01 12 0.6-1.66 4.73E+OO 7.55E-01 0.446 N Pb-212 5.33E-01 5.lOE-02 10 0.6-1.66 1.41E-Ol 2.86E-02 0.265 N Comments/Corrective Actions: Placed into the corrective action Table 1 is provided to show acceptance criteria to assess split process by way of SAPN#l390520. samples. Resolution (d) Agreement Range (e)

                                                                                          <4                      No Comparison 4-7                          0.5-2.0 8-15                         0.6-1.66 16-50                       0.75 -1.33 51-200                      0.80-1.25
                                                                                         >200                        0.85-1.18 Performed By:    ()I!/ /C,.        L/(                 !Date:   ~ -/ -1~  Concun*ence:JYt,-:t.:=  h,. '-/,{__!Date: c;kl~
                                                                                                     '* I /                        /    '

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 425 of 468

Attachment 5 ALARA Statement FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 426 of 468

Attachment 5: ALARA Statement Pacific Gas and 0 f lectric Company Generic ALARA Review for Final Status Survey of Soil at HBPP July, 08, 2013 Martin C. Erickson Reviewed By:~~.Ll Date: *7 I IO/ 2.0\'3 Approved By: /,{~-'-/ Date: -~~/_t__,,/_t3_ __ Page I of~----Cj}_~------- FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 427 of 468

Attachment 5: ALARA Statement Table of Contents 1.0 Introduction ............................................................................................................2 2.0 Discussion ..............................................................................................................2 2.1 Cost of performing remediation work (CostR): .......................................... ,'.......... 2 2.2 Cost of waste disposal (Costw ): ........................................................................ 3 0 2.3 Cost of workplace accident (CostAcc): ................................................................ 3 2.4 Cost of traffic fatality (CostTF): .............................................................................3 2.5 Cost of worker dose (Cost ): ........................................................................3 WDose 2.6 Cost of Dose to the Public (Cost ): .............................................................. .4 PDose 2.7 Other costs associated with this situation (Cost 01 her) .......................................... .4 3.0 Calculation .............................................................................................................4 4.0 Conclusions ...........................................................................................................5 5.0 References .............................................................................................................5 ii FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 428 of 468

Attachment 5: ALARA Statement Executive Summary In addition to the requirement to limit the dose from residual, plant-related radioactivity in soil to members of the critical group to 25 mrem in any year, the License Termination Plan (LTP) requires an evaluation demonstrating that these levels are as low as reasonably achievable (ALARA). If compliance with the ALARA criterion cannot be demonstrated, remediation of the soil is required, even though this would further reduce the otherwise acceptable exposure to the critical group to levels below those required. This report is intended to provide a generic ALARA review to bound the conditions under which no further remediation is necessary for soils. Calculations were performed using LTP equations and conservative assumptions. The conclusion is that it is not cost-beneficial to remediate soil in which the levels of residual, plant-related radioactivity are below LTP release criteria. 1 HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 429 of 468 FSS Report

Attachment 5: ALARA Statement 1.0 Introduction Section 4.4 of the LTP [11 states that a generic ALARA evaluation for soils may be developed to determine if the clean up of soils beyond the DCGLs will be cost-beneficial for HBPP. Section 4.5 of the LTP provides equations and default values for this calculation. This process will be followed, assuming that the soil is at the DCGL and using conservative estimates of costs, distances and other inputs that the worksheet requires. The equation will calculate an action level (AL) that represents the ratio of concentration to the DCGL that would be cost-beneficial to remediate. If that ratio is greater than 1, remediation is not cost-beneficial. This calculation is meant to apply to areas of any MARSSIM class and any size. In a Class 1 area, where values of residual contamination may exceed the DCGL in limited w areas, the mean concentration may never exceed the DCGL . Since it is assumed that w the entire volume of soil removed is at DCGLw, the assumed mean will be at DCGLw. Therefore, the assumed case will be bounding. 2.0 Discussion The total cost (CostT) will be calculated using LTP equation in Section 4.4.1): Cost T

                 =CostR + CostWD + CostACC + CostTF + Costwoose+ Costpo se + Costother 0

These terms are defined and their values calculated as follqws: 2.1 Cost of performing remediation work (Cost ):

*R

Initially it will be assumed that the job is big enough to require earthmoving equipment. At a minimum, this would be either an excavator or a loader and truck. This turns out not to be a constraint, as explained later.

0 To come up with a conservative scenario, the cost of remediating one square meter from a larger project is calculated. Any smaller job by, itself, would have planning and administration costs that would be dominant. Factors contributing to Cost are identified in Attachment 1. The initial estimate for Cost is based R R on a job to remediate 2000 square meters of soil, but to make it comparable to the other costs, that value is adjusted to reflect the cost of 1 _square meter.

The adjusted value of Cost is $7 .32 to remediate 1 square meter of soil.

R

                 *Rounding down to the dollar, Cost R
                                                            = $7 Note: The value of CostR calculated above bounds the cost of a smaller excavation, e.g., one that doesn't require earthmoving equipment. For example, two workers who take an hour to dig up some soil and bring it back 2                       Page_+/-____~ of _______<j____ _

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 430 of 468

Attachment 5: ALARA Statement in wheelbarrow, with no work order or other formal planning, would cost the project about $100 in labor costs (assuming the cost to the project is $50/hr). So, the constraint that this only applies to jobs big enough to require earthmoving equipment can be removed. 2.2 Cost of waste disposal (Cost ): WD 0 As above, it will be assumed that one square meter of surface soil is to be remediated. Surface soil is considered to be the top 15 cm. The estimated 2 waste volume 3 will therefore be. 15 cm times the area of 1 m . This comes to 0.15 m. 0 The current cost of waste disposal for radiologically contaminated soil is $100 per cubic meter. This includes burial fees and shipping. 0 Rounding down to the dollar, Cost . WD

                                                           =$15 2.3         Cost of workplace accident (CostAcc):
          *Cost          = ($3,000,000)x(4.2E-8/h)x(Time to perform remediatfon).

ACC

          * $3,000,000 is the monetary value of a fatality equivalent to $2000 per person-rem.

4.2E-8 is the workplace fatality rate, in fatalities per hour worked.

          ~For a 1 square meter excavation, this would not be more than a few person-hours. (Assume Time =1.62 hr}

0 ($3,000,000) x (4.2E-8/h) x (1.62 h) = $0.20 *

Rounding down to the dollar, CostAcc =$0 2.4 Cost of traffic fatality (CostTF):
Cost TF

                         =($3,000,000)x(3.8E-8/km)x(Volume)x(Distance)/(Volume/shipment) .

Round trip distance from HBPP to Grand View, ID: 2292 km/shipment ... (from Google Maps) 3

            *Waste volume per shipment: 13.6 m /shpmt ... (default in LTP, Section 4.5.1.7.
                      .                                3                          3
            * ($3,000,000)x(3.8E-8/km)x(0.15 m )(2292 km/shpmt)/(13.6 m /shpmt)            =$2.88

Rounding down to the dollar, Cost = $2 TF 2.5 Cost of worker dose (Cost ):

WDose.

            ° Costwoose = ($2000/person-rem)x(Worker dose rate)x(Time) .

0 Dose rates would be insignificant. (Assume dose rate = 0.1 mrem/~ = 1E-4 rem/h) 3 Page __;5'_._,_of. _____CJ_ ..... . FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 431 of 468

Attachment 5: ALARA Statement 0 ($2000/person-rem) x (1 E-4 rem/h) x (1.62 h) =$0.32

Rounding down to the dollar, Costwoose = $0 2.6 Cost of Dose to the Public (Cost ):

                                                                  ,- PDose
                  ° Cost      is assumed to be no more than the Cost          .

DP WO

Assumed Cost :::: $0 PDose 2.7 Other costs associated with this situation {Costother)

There are no other costs associated with this remediation. 3.0 Calculation ALARA Action Level (AL): Cone

                                                ~~~~~~~~~~-x Costr                     r
                                                                                   ~~~-=
                                                                                        + /l AL= DCGLw             $2,000 X Pv  X 0.025  X F   X A    1-  e-(r+A)N where:
                 *Cost has been calculated above T
                 * $2000 is the monetary value of one person-rem (Table 4-1, LTP)

F =removable fraction= 1 ... (most conservative possible)
0.025 is the annual dose in rem to an average member of critical group from residual radioactivity.

0 r = monetary discount rate= 0.03/y ... (Table 4-1, LTP) 0 N = Number of years over which the collective dose is calculated = 1000 y ... (Table 4-1, LTP) 2

                 *PD= Population density for the critical group= 0.0001 people/m . (Table 4-1, LTP) 2

A = Area being evaluated = 1 m
Most conservative nuclide of concern is that with the longest half-life, Tc-99, with a half-life of 2.13E5 years (Table 6-1, LTP) and a decay constant (A) of

                                  -1 3.254E-6 y (Note: With the values for other variables used for this calculation, the t-e ... term equals 1 for any value of A. Therefore, the smallest AL, which is the most conservative, will occur when A, in the top of the equation, is smallest.)

Applying these values to the equation: 24 0.03 + 3.254E - 06 AL = 2000 x 0.0001 x 0.025 x 1 x 1 x 1 - e-Co.o3+3.254E-6)*1000 AL= 144 4 Page-* _(q___."_.of__ .ft____Cf_.~----**** FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 432 of 468

Attachment 5: ALARA Statement If Tc-99 were at DCGL: 0 Sum of DCGL Fractions =1 Since AL is greater than the Sum of DCGL Fractions, remediation is not cost-beneficial. In fact, remediation would not be cost-beneficial unless the concentration of any LTP nuclide in soil were at least 144 times the DCGL. 4.0 Conclusions Based upon the results of this ALARA evaluation, it is not cost-beneficial to remediate soil in which the levels of residual, plant-related radioactivity are below LTP release criteria.

5.0 References

1. HBPP License Termination Plan

2. U.S. Nuclear Regulatory Commission, NUREG-1530, "Reassessment of NRC's Dollar per Person-Rem Conversion Factor Policy," December 1995 5

Page _J______of_________ 9_~---* FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 433 of 468

Attachment 5: ALARA Statement Attachment 1 Cost estimate basis 6 Page _:]"__~_,,of*---- t/ ______ FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 434 of 468

Attachment 5: ALARA Statement Cost estimate for remediation work (CostR) Assume larger project, to dilute fixed costs: 2000 m2 , removing the top 15 cm of soil Time (hr) Rate ($/hr) Cost Const. Planner, Rad Engineer 50 $100 $5000 Supervision/management 1 $200 $200 Resurvey 50 $50 $2500 Additional off-site analysis $2400 Additional on-site analysis $1500 Equip + Operators 10 $250 $2500 RP Coverage 10 $50 $500 Total for 2000 mz $14,640 Cost per ni:.! $7.32. 7 Page _____9-_ ___of____ q___ _ FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 435 of 468

Attachment 6 Quality Verification Assessment Report FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 436 of 468

Attachment 6: QV Assessment 140830025 QV Assessment 140830025 FSS Survey No. HBPP-FSSP-OOL 10-11-00 Fisherman's Channel Quality Verification Short Form Assessment# 140830025 Fisherman's Channel Final Status Survey (FSS) Planning FSS Survey No: HBPP-FSSP-OOLl0-11-00 Date: April 29, 2014 To: Loren Sharp- Director Nuclear Plant Manager Organization Assessed: HBPP Site Closure DISTRIBUTION Via E-Mail E. Halpin A. Cordone J. Albers K.Rod R. Arroyo W. Barley M. Smith J. Kristofzski D. Evans M. Strehlow J. Hinds E. Nelson T. Irving S. Kirven J. Bourassa FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 437 of 468

Attachment 6: QV Assessment 140830025 QV Assessment 140830025 FSS Survey No. HBPP-FSSP-OOL 10-11-00 Fisherman's Channel DECOMMISSIONING NUCLEAR QUALITY VERIFICATION Humboldt Bay Power Plant Short Form Assessment# 140830025 Date: April 29, 2014 Organization Assessed: Sight Closure I FSS Assessment Scope: This assessment will verify adequacy of the Survey Plan for the FSS of the Fisherman's Channel. This particular survey intro-duces a number of variables that are atypical of a FSS of soils areas. This assessment will verify that these variables are appropriately addressed in the survey plan. Summary

Conclusions:

FFS plan number HBPP-FSSP-OOL 10-11-00 adequately addresses the unique challenges present by the FSS of the Fisherman's Channel. The plan provides sufficient detail to ensure trained, qualified and experienced technicians will be able to execute the survey as intended. When the survey plan was compared against the procedure for the preparation of FSS survey plans a number of minor discrepancies were identified. Many of th~ discrepancies were a result of using an uncontrolled copy of the form . Other inconsistencies were noted in the plan. For example at one place in the survey plan, the area was referred to as, the "Intake Canal" rather than the "Fisherman's Channel". Again, none of identified the discrepancies should affect the performance of a experienced technician. The Data quality is not compromised. These discrepancies could however affect the ql.Jality of records. The results of this assessment were reviewed with the responsible engineer and appropriate actions are being formulated. The discrepancies identified are addressed in Notification 1388478. Observations/Results:

Background:

Survey area OOL-1 O consists of the surface soils of the non-industrialized portion of the HBPP site. Survey Unit OOL-10-11 (Fisherman's Channel) is located at the west end of the site west of King Salmon Ave. The channel provided a flow path for water from Humboldt Bay to the Intake Canal. It also provides boat access for personnel docks in the community of King Salmon. The survey area is completely submerged at high tide. It will require a boat and sample dredge to acquire sediment samples for the FSS. It is anticipated that some of the preselected sample locations may be inaccessible due to safety reasons or other access constraints. Other challenges presented by this survey unit are as follows

The survey unit is under water and therefore the normal scan survey cannot be done.
The area is accessible to the public and normal control of access to the area cannot be achieved as per RCP FSS-4 "Isolation and Control of Areas for Final Status Survey"
This survey is intended to support partial release of this area prior to 2019. An early release may have consequences that were not accounted for in earlier planning.
Page 1of3 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 438 of 468

Attachment 6: QV Assessment 140830025 QV Assessment 140830025 FSS Survey No. HBPP-FSSP-OOL 10-11-00 Fisherman's Channel Observations: On April 28, 2014, Sample collection activities were observed at the Fisherman's channel. Observations were limited to what could be observed form the shore. It was noted during this observation that isolation and control measures prescribed by RCP FSS-4 were not apparent. This was discussed with the FSS engineer. He was aware that the normal Isolation and control measures could not be implemented for this survey area. This anomaly is to be addressed in the final report for this survey area. The survey plan was reviewed to determine how the plan addressed some of the unique challenges of this sur-Vey unit. The plan acknowledged that a scan survey could not be performed on submerged sediment. To compensate, a number of comp,ensatory measures were employed.

The investigation level was reduced from the required 50% of the DCGL to 25%.
Samples were collected in a triangular grid pattern with a random start point rather than all sample locations b~ing selected at random

        * - Five additional samples above the normal statistically determined number of fifteen samples were collected.

The plan addressed the early release of the survey area. Because of the planned early release of the survey area (Prior to 2019) Fe-55 screened in as a potentia( nuclide of concern. While not requijed by the License Termination Plan (LTP) or the procedure the sample will be analyzed for Fe-55. Pending development of a site specific Derived Concentration Guideline Level (DCGL) for Fe-55 the screening value for Fe-55 from NUREG 1757 Vol. 2 will be used. Based on the review of the survey plan and discussions with the responsible FSS engineer it is apparent that the unique challenges of this survey area are appropriately addressed. The survey plan was also reviewed against the guidance provided in RCP FSS-2 "Preparation of FSS Survey Plans and RCP FSS-2 Attachment 9.1 "Final Status Survey Planning (FSSP) Worksheet." A number of discrepancies were noted.

The form used to plan survey HBPP-FSSP-OOL 10-11-00 was not the controlled form provided in the plant manual. The header information was missing. That information identifies the form as attachment 9.1 to RCP FSS-2 revision OD. Using an uncontrolled copy of the form/procedure compromises document control measures designed to preclude the use of inappropriate of outdated documents. This can also create issues concerning the adequacy of .

records and determining what procedure/revision was used to generate the document in question. The use of an uncontrolled copy of the survey planning worksheet is inconsistent with guidance provided in the LTP section 5.8.1.6 Document Control.

In the general section of the plan for Survey HBPP-FSSP-OOL 10-11-00, fourth line it has.a header stating "Preparation for Fina.I Status Survey Activities." The approved controlled copy of the form refers to "Preparation for.Characterization Activities." QV recognizes that the preparation for either survey is about the same. The procedure should somehow acknowledge and accommodate this
On page 4 of the Survey Plan there is listed a value for an Adjusted "Lower Boundary of the Gray Region" (LBGR). The use of an Adjusted LBGR is not addressed in the procedure however it is consistent with guidance provided in the LTP.

Page 2 of 4 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 439 of 468

Attachment 6: QV Assessment 140830025 QV Assessment 140830025 FSS Survey No. HBPP-FSSP-OOL 10-11-00 Fisherman's Channel

On page 3 of 5 of attachment 9.1 to RCP FSS-2 under the heading MDC,s for HTD (Hard To Detect) Nuclide, PU-239 and PU-240 are listed separately. They are also listed separately in the LTP. In the survey plan for the Fisherman's Channel, they are listed together as Pu-239/240.
On page 4 of 5 of attachment 9.1 to RCP FSS-2 there are headings for MDCR and QC Checks and measurements. These heading s are not included in the plan. These should be retained in all survey plans and Checked N/A as appropriate.
On page 7 of the survey plan under section 7.0, the plan is missing three data fields.

The type of statistical test to be used Biased Sample information Biased Sample locations These data fields should be retained in all plans and marked N/A If appropriate

On page 8 of the survey plan, Table 1, "Sample Locations" is labeled as the Intake Canal rather than the Fisherman's Channel.

Many of the issues identified above are related to the first issue regarding the use of an uncontrolled document. Taken individually the items identified above are be considered minor with no significant impact on the quality of the survey. Taken together as a whole the problems may compromise the quality of the records of FSS activities. Recommendations: QV recommends that future FSS or Characterization survey plans be prepared using the approved form. QV also recommends the procedure and associated form be revised as appropriate. Page 3 of 4 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 440 of 468

Attachment 6: QV Assessment 140830025 QV Assessment 140830025 FSS Survey No. HBPP-FSSP-OOL 10-11-00 Fisherman's Channel Persons Contacted: M. Erickson FSS Consulting Engineer D. Randall FSS Engineer B. Endicott FSS Technical Specialist Documents Reviewed: o Final Status Survey Planning worksheet (RCP FSS-2 Attachment 9.1) for FSS Survey number HBPP-FSSP-OOL 1'0-t1-00

Generic ALARA Review for Final Status Survey of Soils at HBPP July 8, 2013
RCP FSS-2 revision OD "Preparation of FSS Survey Plans"
Humboldt Bay Power Plant License Termination Plan Chapter 5 "Final Status Survey Plan" Performed & Date:

Prepared by: /71~ 8. ,jo1if May 8, 14 ' C.C. Sokolsky, D (NSOC Secretary) Moore, B. (PSRC Secretary) Jones,S (RMS File) Schulz C (File Net) Page 4 of 4 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 441 of 468

Attachment 7 Survey Plan HBPP-FSSP-OOLl0-12 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-'12 Page 442 of 468

Attachment 7: Survey Plan OOL 10-12-00 Final Status Survey Planning Worksheet Page 1 of 13 GENERAL SECTION / ' Survey Area No: OOL 1O I Survey Unit No: 012 Survey Unit Name: Land Adjacent to Fisherman's Channel Final Status Survey Number; HBPP-FSSP-OOL 10-012-00 PREPARATION FOR FINAL STATUS SURVEY ACTIVITIES Check marks in the boxes below signify affirmative responses and completion of the action. 1.1 Files have been established for survey unit FSS records. Ye~ 0 No D N/A D 1.2 ALARA review has been completed for the survey unit. Yes 0 No D N/A D 1.3 The survey unit has been turned over for final status survey. Yes 0 No D N/A D 1.4 An initial walkdown has been performed 0 1.5 Activities conducted within area since turnover has been reviewed. 0

Based on reviewed information, subsequent walkdown: 0 not warranted D warranted If warranted, subsequent walkdown has been performed and documented OR The basis has been provided to and accepted for not performing a subsequent walkdown. D

     *1.6 A final classification has been performed. 0 Classification: CLASS 1 D CLASS 2 D CLASS30 DATA QUALITY OBJECTIVES (DQO)

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 443 of 468

Attachment 7: Survey Plan OOL 10-12-00 Final Status Survey Planning Worksheet Page 2of13 1.0 State the problem: Survey Area OOL-1 O consists of the surface area of the remainder of the HBPP land area. The open land area is comprised of soil. Survey Unit OOL10-12 is a sub unit of survey area OOL 10. It is bordered by Survey Unit OOL 10-11 over most of its boundary, in addition to off-site locations to plant south and King Salmon Avenue to plant east. It is approximately 46,364 square meters of surface area. The problem as defined by this survey plan is to demonstrate that the years of plant operation did not result in an accumulation of plant-related radioactivity that exceeds the release criteria. PG&E intends to submit a reques~ to the USN RC for an early site release for this and adjacent Survey Unit OOL 10-11 in accordance with the HBPP LTP. The early site release causes Fe-55 to screen in as a potential nuclide of concern. At present a site specific DCGL for FE-55 does not exist. The planning team for this effort consists of the Site Closure Manager, FSS Engineers, FSS Lead Technician and FSS Technicians. The FSS Engineers will make primary decisions with the concurrence of the Site Closure Manager. 2.0 Identify the decision: Does residual plant-related radioactivity, if present in the survey unit, exceed the release criteria? Alternative actions may include no action, investigation, resurv~y, remediation and reclassification. 3.0. Identify the inputs to the decision: Sample media: Sediment Types of measurements: Setjiment samples Radionucfides-of-concern: Cs-137 Applicable DCGL: The DCGLs applied under this survey plan correspond to the soil dose as determined in the LTP. For Fe-55 the screening level DCGLs ofNUREG 1757 Vol. 2 were applied for interim use until a site specific DCGL is determined. Nuclide DCGL Nuclide DCGL Nuclide DCGL (pCi/g) (pCi/g) (pCi/g) H-3 6.8E+02 1-129 4.8E+OO Pu-241 8.6E+02 C-14 6.3E+OO Cs-137 7.9E+OO Am-241 2.5E+01 Ni-59 1.9E+03 Eu-152 1.0E+01 Cm-243 2.9E+01 Co-60 3.8E+OO Eu-154 9.4E+OO Cm-244 4.8E+01 Ni-63 7.2E+02 Np-237 1.1E+OQ. Cm-245 1.7E+01 Sr-90 1.5E+OO Pu-238 2.9E+01 Cm-246 2.5E+01 Nb-94 7.1E+OO Pu-239 2.6E+01 Fe-55 1.0E+04 Tc-99 1.2E+01 Pu-240 2.6E+01 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 444 of 468

Attachment 7: Survey Plan OOL 10-12-00 Final Status Survey Planning Worksheet Page 3of13 Seventy one (71) samples from previous characterization data were used to provide the characterization data for survey area OOL 10. The data is sufficient to support the planning of Survey Unit OOL 10-12. Based on a review of the characterization data, Cs-137 was the only plant-related radionuclide that was identified consistently in the characterization samples analyzed. The results from the characterization data are summarized below:

o Cs-137 (51 detects) Cs-137 is present in 72 % of the characterization samples.

o Other HBPP ETD There were no other easy to detect nuclides identified >MDA. o HBPP HTO There were no hard to detect nuclides identified in the four samples analyzed. The presence of all radionuclides listed in this plan (gamma-emitters, HTD beta-emitters, and TRUs) in the soil (sediment) will be evaluated under this survey plan. Although no HTD nuclides are expected to be present, the contribution from HTD nuclides will be bounded by directly adding the dose contribution of a sample contaminated to approximately 3 times the DCGL (~22 pCi/g) for Cs-137. The resultant dose from HTD nuclides is presumed to be less than 1 mrem/y, which will be verified upon receipt of the sample result from General Engineering Laboratories (GEL), Savanah, SC prior to the implementation of this plan.

A consequence of the planned early site release for this area is that the earlier date (Prior to 2019) for site release causes Fe-55 to screen in as a potential nuclide of concern. Accordingly, although Fe-55 is not believed to be present, a DCGL must be developed to assess an appropriate MDC for its analysis.

In the interim, the sample will be counted for Fe-55 based on the screening level DCGLs of NUREG 1757 Vol. 2. The sample will be retained, per the requirements of the FSS program, in case it is later determined that a re-analysis for Fe-55 is necessary. The HBPP Site Closure Laboratory will analyze each soil sample for all listed gamma-emitting nuclides, Sr-90 and Tritium. In addition, 2 FSS soil samples will be sent to an independent laboratory for analyses of gamma-emitters and HTD radionuclides. FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 445 of 468

Attachment 7: Survey Plan OOL 10-12-00 Classification: Class 3 Average Cs-137 concentration: 0.38 pCi/g Standard deviation Cs- 137 (u): 0.18 pCi/g Surrogate DCGL: N/A (a surrogate DCGL will not be used) LBGR: Initial::: 0.5xDCGL = 3.79 pCi/g Cs-137 Adjusted LBGR( set 11/cr = 2.0) ::: 7.22 pCi/g Cs-137 Number of Samples: Calculated = 15 Survey Unit Area: 46,364 m 2 Grid Area (AIN): N/A Class 3 DCGLemc Cs-137: N/A Class 3 Investigation Level for soil samples: > 50% DCGL for Cs-137::: 3.79 pCi/g Cs-137 Gamma scanning Coverage: Approximately 10% of Survey Unit Investigation Level for SPA-3 Scans: Reproducible indication above background using 44-1 O and audible discrimination. The expected background range for 44-10 scans is between 3200 cpm and 5400 cpm. Radionuc!ides for analysis: All listed nuclides with the focus on Cs-137 MDCs for gamma analysis of soil samples: Nuclide 10% to %50 of the DCGL (pCi/g) Co-60 3.8E-01 to 1.9E+OO Nb-94 7.1E-01 to 3.55E+OO 1-129 4.8E-01 to 2.4E+OO Cs-137* 7.58E-01 to 3.79E+OO Eu-152 1.0E+OO to 5.0E+OO Eu-154 9.40E-01 to 4.70E+OO Np-237 1.1E-01 to 5.5E-01 The desired MDCs in the laboratory analyses of soil samples will be the 10% DCGL values. If it is impractical to achieve those, the 50% DCGL values mu~t be achieved in the laboratory analyses of the sediment samples.

The DCGL for Cs-137, the only nuclide expected to be present has been reduced to 24 mrem/y to account for any HTDs that might be present.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 446 of 468

Attachment 7: Survey Plan 001 10-12-00 Final Status Survey Planning Worksheet

Page5of13 MD C's for /-/TD nuclide:

Nuclide 10% to 50% of the DCGL (gCi/g) H-3 6.8E+01 3.4E+02 C-14 6.3E-01 3.15E+OO Fe-55 1.0E+03 5.0E+03 Ni-59 1.9E+02 9.5E+02 Ni-63 7.2E+01 3.6E+02 Sr-90 1.5E-01 7.5E-01 Tc-99 1.2E+OO 6.0E+OO Pu-238 2.9E+OO 1.45E+01 Pu-239/240 2.6E+OO 1.3E+01 Pu-241 8.6E+01 4.3E+02 Am-241 2.5E+OO 1.25E+01 Cm-243 2.9E+OO 1.45E+01 Cm-244 4.8E+OO 2.4E+01 Cm-245 1.7E+OO

8.5E+OO Cm-246 2.5E+OO 1.25E+01 The MDC values for difficult to detect nuclides will be conveyed to the outside laboratory via the sample Chain-Of-Custody form which wifl accompany the soil samples.

QC checks and measurements: QC checks for the 44-1 O will be performed in accordance with RCP-7U2 Two QC split samples will be collected One QC recount for soil samples will be performed by the HBPP Site Closure Lab FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 447 of 468

Attachment 7: Survey Plan OOL 10-12-00 Final Status Survey Planning Worksheet Page 6of13 4.0 Define the boundaries of the survey: o Boundaries of Survey Unit OOL 10-12 are as shown on the attached map. This area is bordered by the Survey Area OOL 10 and off-site locations on all sides. o The survey will be performed under appropriate weather

conditions (as defined by instrumentation limitations and human factors). Surveys will be performed during daylight hours.

5.0 Develop a decision rule: Upon review of the FSS data collected under this survey plan: (a) If all the sample data show that the soil concentrations of plant related nuclides are below the DCGLs and the sum of fractions of nu elides are below unity, then reject the null hypothesis (i.e., Survey Unit OOL 10-12 meets the release criteria). (b) If the investigation levels are exceeded, then perform an investigation survey. (c) If the average concentration of any listed nuclide exceeds its respective DCGL or the average sum of fractions for any listed nuclide exceeds one, then accept the null hypothesis (i.e., Survey Unit OOL 10-12 fails to meet the release criteria). Note: Alternate actions beyond investigations.include, remediation, reclassification and resurvey 6.0 Specify tolerable limits on decision errors: Null hypothesis: Residual plant-related radioactivity in Survey Unit OOL 10-12 exceeds the release criteria. Probability of type I error: 0.05 Probability of type II error: 0.05 LBGR: Adjusted to 7.22 pCifg Cs-137 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 448 of 468

Attachment 7: Survey Plan OOL 10-12-00 Final Status Survey Planning Worksheet Page 7of13 7.0 Optimize Design: Type of statistical test: WRS Test D Sign Test 0 (background will not be subtracted) Number and Loca. tion of Samples: *I Twenty (20) soil samples will be collected at locations I I based on a random selection IGENERAL INSTRUCTIONS .

1. Where possible, measurement locations will be identified using GPS. Each location will be marked to assist in identifying the location. Any locations that are not suitable for soil sampling will be relocated to the nearest suitable location and documented on the survey map.

2. Chain of Custody form/process will be used for all samples being shipped to the offsite laboratory.

3. All soil samples will be received and prepared as directed by the FSS Engineer.

Note: The split sample aliquot to be sent to an off-site lab for HTD analysis will not be dried prior to counting on site or shipping.

4. Survey instrument: Operation of the 2350-1 w/44-10 will be in accordance with RCP-7U3 with QC checks performed in accordance with *RCP-7U2. The instrument response checks shall be performed before issue and after use.

5. All 44-10 scans will be performed with the audible feature activated. FSS Technicians will listen for upscale readings to which they will respond by slowing down or stopping the probe to distinguish between random fluctuations in the background and greater than background readings.

6: The job hazards associated with the Survey described in this package will be addressed in the pre-job brief.

7. All personnel participating in this survey shall be trained in the operation of the instrumentation.

I SPECIFIC INSTRUCTIONS

1. All designated measurement locations will be identified by. GPS or by use of reference points and tape measure as necessary. If a designated sample location is obstructed for any reason, the FSS Engineer or the Lead FSS Technician will select an alternate location within one FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 449 of 468

Attachment 7: Survey Plan 00110-12-00 Final Status Survey Planning Worksheet Page 8of13 meter of the original location. A detailed description of the alternate location will be recorded on the survey form, the survey unit map will be annotated appropriately, and the alternate location will be conspicuously marked to facilitate re-visiting to identify and record the coordinates with GPS or by measurement from a known reference point when GPS is not available. \

2. Sample Requirements:

0 Collect twenty (20) random 1-liter soil samples in accordance with RCP FSS-8. Two (2) of the 20 random soil samples will be analyzed as QC split samples and one (1) will be a sample recount to fulfill the QC requirement. The QC split samples will also be analyzed for Hard-to-Detect nuclides. e Collect any biased 1-liter soil samples as per field direction from the FSS engineer assigned to this survey unit and/or the FSS Lead Technician. o If a sample location falls on an engineered surface, collect a sample of the engineered material and a sample of the soil below. The soil sample will* be used as the statistical sample and not the engineered material sample. The engineered material sample will have the designation OOL 10-12-xxx-EM where the "xxx" is the sample number corresponding to the soil sample location. o Soil samples will be collected as follows: o At the sample location, using a clean implement, dig a hole in the soil approximately 4 inches in diameter to a depth of 15 cm placing the soil in a plastic bag.

o Enlarge the hole as necessary radially until the desired amount of soils is collected.

Do not dig deeper than 15 cm. o Label the plastic bag with the sample location identifier. o Transfer the bag of soils to the sample preparation area.

3. Soil Sample Designation:

Statistical soil samples: OOL 10-12-001-F through OOL 10-12-020-F corresponding to sample locations 001 through 020. Biased soil samples: : OOL 10-:12-021-F-B through OOL 10-12-0xx-F-( B corresponding to the biased sample locations. QC split samples: OOL 10-12-011-F-S and OOL 10-12-019-F-S are to be designated as QC split samples. These samples will be sent to the off-site laboratorv.

Recount samples: OOL 10-12-007-F-RC is to be counted twice on site. The results will be compared as direCted ,

by the FSS Engineer. FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 450 of 468

                                                                          * . Attachment 7: Survey Plan OOL 10-12-00 Final Status Survey Planning Worksheet Page 9of13

4. Sample Analysis:

e Gamma analysis will be performed on all soil samples. If any of the gamma analyses show that an investigation level has been exceeded an investigation survey will be conducted at that sample location as directed in specific instruction # 6. e HBPP will analyze OOL 10-12-001-F through OOL 10-12-020-F and any biased samples for gamma-emitting nuclides, Tritium (H-3) and Sr-90. o HBPP will analyze OOL 10-12-007-F as a sample recount. The recounted sample will possess the naming convention OOL 10-12-007-F-RC. e HBPP will analyze OOL10~12-011-F-S and OOL10-12-019-F-S for gamma-emitting nuclides prior to being sent to the off-site laboratory.* These samples will be analyzed for gamma emitting nuclides and HTD at the off-site laboratory. o On-site gamma analysis of the samples shall achieve the MDC values stated in the DQO section of this plan. The MDC's fQr off-site analysis will be communicated to the laboratory using an attachment to the Chain-of-Custody form or previous direction that meets specified MDC's of this characterization survey plan.

5. Gamma scans:

e Scan 10% of the accessible survey area with a 44-10 in* rate-meter mode moving the detector at a speed of 0.2 m or less per second, keeping the probe at a distance of approximately 3" from the surface and following a serpentine path that includes at least 3 passes across each square meter. e Note the area scanned on the survey map e If an indication of greater-than background is discovered: o Rescan the area to determine if the indication was due to background fluctuation o If the indication was due to background fluctuation continue to scan the remainder of the area.* o If the indication was due to an elevated area then slowly scan the elevated area to determine the elevated activity boundaries and note on the map o Obtain a 1 liter biased soil sample at the point of the highest reading in the elevated area. Denote the sample using the naming methodology described in step 6.

6. If the results of any sample (statistical and/or biased points) analysis exceed an investigation level, perform a first level investigation as follows:

o Scan a 1 m radius footprint around the sample location with a 44-10 in rate-meter mode FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 451 of 468

Attachment 7: Survey Plan OOL 10-12-00 Final Status Survey Planning Worl<sheet Page 10of13 moving the detector at a speed of 0.2 m or less per second, keeping the probe at a distance of approximately 7-8 cm from the surface and following -a serpentine path that includes at least 3 passes across each square meter. The area of scan should be increased as necessary to bound any areas of elevated activity identified. o Mark the boundaries around any detected elevated areas in the soil and identify the boundaries on a survey map. Measure the total area of each outlined area in square centimeters. e Mark the location of the highest identified activity for each of the elevated areas in the soil and on the survey map. 0 At each of the highest identified activity area: o Perform and record a 1-minute scaler mode 44-10 measurement. Designate the reading as "OOL 10-12-xxx-F-SC-I" where "xxx" continues sequentially from t_he last number assigned to an investigation measurement. o Obtain a soil samP,le at the location. Designate the sample as "OOL 10-12 -xxx-F-1" where "xxx" continues sequentially from the last number assigned to an investigative sample. o Perform and record a post sample 1-minute 44-10 measurement. Designate the reading as described above. Prepared by: [}c,__L &v£vl{ Date: _if'-----'-1--=-t_-_,_/_'f_ FSS Engineer Reviewed by:~.,&;; C . t-,_.: L Date: ~btoI ht FSS gineer 7 Site Closure Manager Date: '/.h l/;f FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 452 of 468

Attachment 7: Survey Plan OOL 10~ 12-00 Final Status Survey Planning Worksheet Page 11 of 13 OOL 10-12 VSP Sample Locations Sample EastinQ* NorthinQ* 01 5947081.59 2159247.24 02 5947279.91 2159362.50 03 5947896.89 2159566.82 04 5947867.51 2159692.56 05 5947779.37 2159944.03 06 5948021.76 2159671.60 07 5947749.99 2160069.77 Recount 08 5947933.62 2159985.94 09 5948043.79 2159881.16 10 5948220.07 2159786.86 11 5947904.24 2160237.42 OCsnllt 12 5948014.41 2160132.64 13 5948198.04 2160048.81 14 5948102.55 2160258.37 15 5948168.66 2160174.55 16 5948374.32 2159954.51 17 5948278.83 2160164.07 18 5948433,08 2160331.72 19 5948455.11 2160352.68 QCSnlit 20 5948521.22 2160268.85 "CA Zone 1 NAD83/NAVD88 FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 453 of 468

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Final Status Survey Planning Worksheet Page 12of13 OOL10-12 Prospective Power Curve Fi~e Help

                                                                               ,-Decision Errors                  i r Required. S-aID.ple Size1 Sm:Yey Umt ID:                                                   j Alpha:                  Reta:    11 Sun:-ey    um: 15                !

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Attachment 7: Survey Plan 001 10-12-00 Final Status Smvey Planning Worksheet Page 13of13 44-10 Scan MDC/MDCR Values at Typically encountered count rates

                                     -IB MDCR = 1.38 c                                                           (RCP FSS 2)
                                   -VP xt Where, B  = background in the sampling interval (0.02 min) p = Surveyor Efficiency= 0.5 t =sampling time interval =0.02 min Ei=202 cpm/pCi/g for Cs-137 (LTP Table 5-13)

MDC BKG BKG/t MDCR (CPM) (pCi/g Cs-137) 2000 40 617 2.9 2500 50 690 3.1 3000 60 756 3.4 3500 70 816 3.7 4000 80 873 4.0 4500 90 926 4.3 5000 100 976 4.6 5500 110 1023 4.8 6000 120 1069 5.1 6500 130 1113 5.3 7000 140 1155 5.5 7500 150 1195 5.7 8000 160 1234 5.9 8500 170 1272 6.1 9000 180 1309 6.3 9500 190 1345 6.5 10000 200 1380 6.7 10500 210 1414 6.8 11000 220 1447 7.0 11500 230 1480 7.2 12000 240 1512 7.3 12500 250 1543 7.5 13000 260 1573 7.6

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FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 455 of 468

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HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 456 of 468 FSS Report

Attachment 8 Data Assessment HBPP-FSSP-OOLl0-12 FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL 10-12 Page 457 of 468

Atta chment 8 Data Assessment HBPP-FSSP-OOL 10-12 OOLl0-12 Frequency Plot 9 8 VI 7 c: 0 ca Q) 6 VI

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                     -0 .01 0 .14     0.29            0 .44        0 .59     0 .74            0.89            1.04         1.19 Bin Upper End Value {pCi/gm)

FSS Report HBPP-FSS P-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 458 of 468

Attachment 8 Data Assessment HBPP-FSSP-OOL 10-12 OOL 10-12 Sample Results Quantile Plot 1 . 4 ~------ 1.2 .._-----------------------------------------~* 0.8 E O'l 0.6 0 0..

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75th Percentile ----50th Percentile II.

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Pa ge 459 of 468

Attach ment 8 Data Assessmen t HBPP-FSSP-OOL 10-12 OOLl0-12 Sample Results Scatter Plot 1.40E+OO = DCGLop 7.58 pCi/gm Cs-137 1.20E+OO 1.00E+OO

1.024 8.00E-01 6.00E-01 4.00E-01 2.00E-01
0. 237 O.OOE+OO

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Activity - Average - "+3StDev" - "-3StDev" FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 460 of 468

Attachment 8 Data Assessment HBPP-FSSP-OOL 10-12 Retrospective Power Curve OOLl0-12 MARSSIM Power 2000 ---- ______--_ _' ______**---~~i:t.~..,..:. ~ ~ ---- --- File Help SUIVey Unit ID:

                                                                   - Decision Errors Alpha:         B.eta:

rRoqWred Srunp1' S~'J SUIVey Unit: 14 Radionuclide: junity Rule - Sta tis tical Test 1 loos ~ loos ~

r. Sign Test I WRS Test J2CGL 17.58 0 ~[ I ~ I 7.58 Critical Value:

                                    ....:J                              LBGR jo.237 Sigma 10.263          __:J    10 I                           Mcr= 27.93 Probabllity that the Survey Unit Passes                                                Click 1.0
                                                                       "                            anywhere on the graph to 0.8                                                                                update the power curve using newly 0.6                                                                                entered parameter values 0.4 0.2 0.0 10%       30%       50%          70%        91% 100% 1 0%      1 0%   150%

True Survey Unit Concentration (percent ofDCGL) Exit Program I FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 461 of 468

Posting Plot OOL10-12

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                                                                            - - 00110 -12 Survey Boundary X.XX E-XX =Result (pCi/g CS-137)

Q =Sample Point Location FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Pag e 462 of 468

Posting Plot OOL10-12

            \~
                                 -  OE--02 1.05E-01 -<:I>ti"
                                                                                - - 00110-12 Survey Boundary X.XX E-XX =Result (pCi/g Sr-90) 8    =Sample Point Location FSS Report                                  HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12                             Page 463 of 468

Attachment 8 Data Assessment HBPP-FSSP-OOL 10-12 RCP FSS-11 Attachment 8.1 Rev. OC Page 1 of 1 Split Sample Assessment Form Survey Area No.: OOL--10 jsurvey Unit No.: 12 Survey Unit Name: Land Adjacent to Fisherman's Channel Sample Plan No.: HBPP-FSS-OOLl 0-12-00 Sample Measurement Location: #07 Sample

Description:

Comparison of split samples collected from sample measurement location #07 and analyzed using gamma spec1roscopy in repeated counting at the on-site laboratory. The official on-site result 1s the standard count and the recount is the comparison. STANDARD COMPARISON Agreement Comparison Radio-nuclide Standard Comparison Comparison Ratio Acceptable Range Error Activity lcr chosen Resolution (e) Activity (g) (h)=(f)/(b) (YIN) (b) Uncertainty (a) (c) (d)=(b)/(c) (f) K-40 7.36E+OO 9.SOE-01 8 0.6-1.66 6.30E+OO 9.00E-01 8.56E-Ol y Comments/Corrective Actions: None. Table 1 is provided to show acceptance criteria to assess split samples. Resolution (d} Agreement Range (e}

                                                                                           <4                      _No Comparison 4-7                          0.5-2.0 8-15                          0.6-1.66 16-50                        0.75 -1.33 51-200                       0.80-1.25
                                                                                          >200                        0.85-1.18 Performed By:    /:)A/~               L              !Date:} -'SO'-/i./    Concurrence: )'y\_ ...t- 1      ..,~   JDate: c, /,_ /,..,.
                                                                                                          '-   t' FSS Report                                HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12                                                                               Page 464 of 468

Attachment 8 Data Assessment HBPP-FSSP-OOL 10-12 RCP FSS-11 Attachment 8.1 Rev. OC Page 1 of 1 Split Sample Assessment Form Survey Area No.: OOL-10 lsurveyUnitNo.: 12 Survey Unit Name: Land Adjacent to Fisherman's Channel Sample Plan No.: HBPP-FSS-OOLl0-12-00 Sample Measurement Location: #11 Sample

Description:

Comparison of split samples collected from sample measurement location# 11 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The on-site result is the standard count and the off-site is the comparison. STANDARD COMPARISON Agreement Comparison Radio-nuclide Standard Comparison Comparison Ratio Acceptable Range Error Activity 1cr chosen Resolution (e) Activity (g) (h )=(t)/(b) (YIN) (b) Uncertainty (a) (c) (d)=(b)/( c) (f) K-40 I .08E+ol 9.60£-01 II 0.6-1.66 l.24E+Ol 3.52E-01 1.15E+OO y Pb-212 3.99E-OI 5.00E-02 8 0.6-1.66 5.94E-OI 2.31E-i:l2 l.49E+OO y Comments/C01Tective Actions: None. Table I is provided to show acceptance criteria to assess split samples. Resolution (d} Agreement Range (e}

                                                                                                  <4                    No Comparison 4-7                        0.5-2.0 8-15                        0.6-1.66 16-50                     0.75-1.33 51-200                     0.80-1.25
                                                                                                 >200.                     Q.85 - 1.18 Performed By:   (,.c:'(:.'..,...11 / e~:....Ii f             lnate: cf- $ i;*-14 Concurrence:M.,...Z--.r... *
                                                                                                           \.  /

V lnate: 9k /,;-¢ FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 465 of 468

Attachment 8 Data Assessment HBPP-FSSP-OOL 10-12 RCP FSS-11 Attachment 8.1 Rev. QC Page 1of1 Split Sample Assessment Form Survey Area No.: OOL-10 Isurvey Unit No.: 12 Survey Unit Name: Land Adjacent to Fisherman's Channel Sample Plan No.: HBPP-FSS-OOLl0-12-00 Sample Measurement Location: #19 Sample

Description:

Comparison of split samples collected from sample measurement location #19 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The on-site result is the standard count and the off-site is the comparison. STANDARD COMPARISON Agreement Comparison Radio-nuclide Standard Comparison Comparison Ratio Acceptable Range Error Activity 1cr chosen Resolution (e) Activity (g) (h)=(f)/(b) (YIN) (b) Uncertainty (a) (c) (d)=(b)/(c) (f) K-40 l.08E+Ol 8.90E-Ol l.21E+Ol 0.6-1.66 1.33E+Ol 3.34E-01 1.23E+OO y Pb-212 4.94£.:01 4.86E-02 1.02E+Ol 0.6-1.66 6.22E-01 2.23E-02 1.26E+OO y Comments/Corrective Actions: None. Table I is provided to show acceptance criteria to assess split samples. Resolution (d} Agreement Range (e)

                                                                                              <4                   No Comparison 4-7                        0.5-2.0 8-15                       0.6-1.66 16-50                      0.75-1.33 51-200                     0.80-1.25
                                                                                            >200                      0.85-1.18 Performed By:     /711_/ A Lff                       !Date:   g. _3ti- ff- . Concurtence:m ...k:       ~.- ~       !Date: q /,,., ;,A
                                                                                                                                          /
                                                                                                          '-   {

FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL 10-12 Page 466 of 468

Attachment 8 Data Assessment HBPP-FSSP-OOL 10-12 Humboldt Bay Power Plant Area Survey Report FSS Survey#: ,io I **I ** o 0 FL Date: 'I* '?o--.wittfime* / 'fa o Location: ...!Lof!a!l!nd~A~d>iJiagic~ecun!ut!d..o..c.F~iswhewrml!.!.9Janu..:'sLC~hlliamnl!lne~11_-=S==c=a=n=A==r=e~a===='==-

Purpose:

OOL 10-12 scan survey 2190 sq.m.

                                                                                              -~~~~~~~~-

Previously scanned= '1 INSTRUMENT SURVEY PERFORMED BY TYPE SERIAL NO. r I FSS Report HBPP-FSSP-OOL10-11 & HBPP-FSSP-OOL10-12 Page 467 of 468

Attachment 8 Data Assessment HBPP-FSSP-OOL 10-12 Humboldt Bay Power Plant Area Survey Report FSS Survey#: ~'f- ()D[i'. Date: L/

3D, I 'Hime* i *-1 o o Location: ....!Lo.2a!.!..!!nd\.LA~dWciaillci!;<enwt...!!toLJFC.!is>!!.h~erwmMallln-"-'s_,,,,c11ha91nmn!!tel'---=S=c==a=n===A==r=e=a===='=====-

Purpose:

OOL 10-12 scan survey 4579 sq.m. Previously scanned= ~ INSTRUMENT SURVEY PERFORMED BY TYPE SERIAL No. CAL. DUE PRINT SIGN FSS Report HBPP-FSSP-OOL 10-11 & HBPP-FSSP-OOL10-12 Page 468 of 468

SUBMITIAL PROCESSING CHECKLIST Regulatory Services Engineer

SUBJECT:

PG&E LEITER: HBL- I (p ~ DO&' FIR~DATE: 11-9-/fe LOCATION: S:\LICENSE\LETIERS\ DOCUMENT VERIFICATION INITIALS/DATE

REFERENCES/BASES IDENTIFIED FOR FACTUAL INFORMATION ~ I 11/r:;fl'-
COMMITMENT(S} PROPERLY IDENTIFIED (Xl1.ID1}(HBAP E-10} tJ (fr 1~
MANAGER'S CONCURRENCE FOR RELEASE \V"f /~
RECORD OF REVIEW CHECKLIST (Xl1.ID1} COMPLETE AND SIGNED ~s 11*/9/
CLERICAL QUALITY/FORMAT REVIEW Draft #_I_* 4/M.J-1l)_:z Draft#_ /_ _

Draft#_ /_ _ FINAL CLERICAL REVIEW (Letterhead} Cl.Ak1__p_/:l

PEER REVIEW OF FINAL LETTER/ENCLOSURE(S} .

                                                                                               -~'--

PROVIDE TO SIGNATORY:
Final letter/enclosures, record of review, commitment memo -~'*
For FIRM submittals, was 2 days met? Yes D No D
COPY OF SUBMITTAL W/RECORD OF REVIEW, COMMITMENT DATA, AND COMPLETED CHECKLIST TO RMS (FIREPROOF} CABINET /_ _
INTERNAL -- provide this checklist, original of signed submittal, commitment data, and record of review to clerks I- -
NCRs, ARs, AND Q~R~~iWPf~f~;ppt (for LERs only) UPDATED FOR SUBMITIAL /_ _

COMPLETION TRACKING CLOSEOUT WITHIN 15 DAYS OF SUBMITIAL

                                                                                               -~'--

VERIFY COMMITMENT ENTRY ON NCR ACTs , AEs EDMS\RS-1

I -

                                       ~HIL-i~-cx::l?

DONE LETTERS SIGNED AT DCPP Prior to Signature HBPP Supervisor of Licensing (SOL) completes Rec~rd of Review Checklist ~5 Regulatory Services (RS) engineer is responsible for having the Peer Review Checklist completed ! ~3-RS clerical is responsible for having an editorial review completed C)iLJ RS engineer meets with signatory to have letter signed After Signature RS clerical handles hard copy distribution (external and internal) PERFORM PAGE CHECK - VERIFY ALL COPIES CONTAIN ALL PAGES & COMPARE PAGES TO TABLE OF CONTENTS RS clerical converts the letter WORD file to pdf file on s:\license\letters drive RS clerical handles electronic internal distribution of the pdf letter file via e-mail (HBPP Humboldt Distribution) RS clerical uploads the pdf letter file onto EDMS. RS clerical returns this Instruction sheet to SOL Front Office or Licensing sends pdf file (letter and enclosure) to Records Management to input the pdf file into RMS. s:\license\letters\instructions.doc

DCPP Form 69-20996 (06/25/12) X11.ID.1 Attachment 2 Page 1of1 Regulatory $ubmittai - Record of Review Checklist Submittal

Title:

._f._. -"--*G\...;=v'-***--"+'-"i---=~=* +.*.__. __.* __--'----_S___. (. . . . . . c..._~~B--*-c.~-* e.._'_*:;;.~.I_**ig_~--~-~--- _ .i_. Targeted Submittal Date: t d -- L.-:Z ~:. }-(,, Firm Submittal Date: NA ON/A Primary Reviewers Comments Resolved Yes No Yes No Lead Technical Reviewer:*1 iVL ~ D_ ~ D Lead Technical Mah~iger: 1 D 12( 0 D Direc::tor Review:

1 2 D !S1" D D Submittal Lead Mahagerr1ent: 1 l:L ~ 0 ~ []

~-

Independent T echnica! Reviewer: 1 0 ~ D Cross Discipline Reviewer(s): 0 D D D 0 Operations: D D D D 0 Maintenance: D D 0 D 0 Engineering: tJ o* D 0 D Site Services: D D D D D Quality: D 0 D D D LaW'. 0 D D D [j Cl1ernistry &. Env Ops: 0 0 D n 0 PSRC: D D D D 0 D D D D D D D D D d D D 0 0 Secondarv Reviewers Comments Resolved Yes No Yes No L -_** [;J7. ~** D ... °"°"' .ti D D D i;V* D [j D D D D 0 D D 0 D D D . ' D D D D D D D D D D D D D D I have reviewed and verified that all statements of fact in the submittal are correct. (Mark. NIA and. attach a copy of e-mail if documentation of !TR is electronic. )3 GVNIA Independent Technical Reviewer(s ): ------------~----____,,....-_,.,..,--~ Date: Date: _ _ _~_ Concurrence has been receiv.e.d from primary reviewers. Technical comm~nts have been re~olved. The independent tech. revieWr:lr h' ~view~ all technical (non-editorial) changes.* to the submittal. Lead Licensing Engineer: ~~~ . _. _ _ -. Date: I0- "'L (; - / (;, 1 These reviewers are considered to be the minimum required primary reviewers for submittals not containing an oath or affirmation or requiring PSRC review. Regulatory Sen/ices Manager approval is required to not obtain the review from any of these reviewers. 2 Director review is.satisfied if the submittal undergoes a review by the PSRC. 3 AHach a table of "statements requiring verification" and ITR approvals. 69-20996.D.OC *1222.0950

Skov, Jeffrey From: David Sokolsky <ddsokolsky@yahoo.com> Sent: Wednesday, November 09, 2016 10:30 AM To: Skov, .Jeffrey

Subject:

Fw: REVISED HBPP SUBMITTAL FOR YOUR REVIEW - PARTIAL SITE RELEASE This is an EXTERNAL EMAIL. Stop and think before clicking links or opening attachments. Jeff - Below is the email from the ITR Bill Parish. David On Monday, October 24, 2016 6:33 AM, "Parish, William C" <WCP?@pge.com> wrote: I have reviewed the letter HBL-16-008, the associated "HBPP Release Area Assessment" and found no technical issues that affect the validity of the submittal. William C. Parish WCP7@pqe.com W: 375-2641 (inside PG&E) W: 707-441-2641 (outside) parishwc@yahoo.com C: 979-557-9090 From: David Sokolsky [2] Sent: Sunday, October 23, 2016 6:48 PM To: Erickson, Martin; MCERICKSON2001@YAHOO.COM; Barley, Bill; Sharp, Loren; Hamzehee, Hossein; Parish, WilliamC Cc: Tyson R. Smith; Manheim, William (Law); Morris, James R; Rowberry, Kris; Halpin, Ed

Subject:

REVISED HBPP SUBMITTAL FOR YOUR REVIEW- PARTIAL SIT!; RELEASE This is an EXTERNAL EMAIL. Stop and think before clicking links or opening attachments. Attached is a significant revision to the partial site release (PSR) request draft submittal. A major change was due to the fact that the original draft was incorrectly identified as a License Amendment Request (LAR). This was based on the fact that LTP Section 1.2 states the PSR requires an LAR. However,* in a phone call with John Hickman on October 21, John mentioned that the statement in LTP Section 1.2 was incorrect and that the NRG should have caught it. Nevertheless, John clearly pointed out that the PSR does not affect the License nor the tech specs; therefore, an LAR is inappropriate .. Because this PSR request is no longer an LAR, the No Significant Hazards Consideration, previously contained in Enclosure 2. of the draft submittal, has been deleted from the PSR request. In addition, the letter does not have to be signed by an officer under penalty of perjury. Therefore, Loren Sharp 1

will sign the letter. Also, the Legal Department is now considered a Secondary Reviewer, not a Primary Reviewer. There were no technical changes made in the revised draft submittal. Please note that the original draft was based on a similar submittal by Yankee Rowe (YR) in 2005. The YR submittal was not an LAR, but used the terminology "release a portion of the YR site from its 10 CFR Part 50 License," which is a bit confusing. The previous HBPP draft included similar terminology. However, the revised HBPP draft uses the terminology "release a portion of the HBPP property from the Part 50 site," which is more appropriate. The attached draft incorporates comments received from the ITR and legal department. I am sending a separate email to the ITR and legal department describing resolution of their comments. The following are Primary Reviewers. Please respond with comments or concurrence by OCTOBER 25 so HBPP Plant Staff can submit the PSR by October 27. Marty _Erickson Bill Barley Loren Sharp Hossein Hamzehee Bill Parish The following are Secondary Reviewers. You do not have to respond, but if you have comments, please submit them to me by OCTOBER 25. Tyson Smith (legal) Jim Morris Kris Rowberry Thank you, David Sokolsky 415-961-3384 2

PEER REVIEW CHECKLIST LICENSING SUBMITTAL (To be performed on final draft only.) I PG&E Letter No. (e.g., HBL, HIL) ITEM QESCRIPTION INITIALS* Cover Letter Correct signatorv letterhead (Ref. Xl1.ID2 or HBAP E-12) JI"$~ Full names used for sianatorv & cc list; right people listed ~ Title correct l.rf Letter number verified against outgoina correspondence loa ~ Letter number appears on all pages ~ All pages numbered, except first page vS Date correct and appears on all pages (month, day, and year) .,\rj' Address and docket number(s) correct .:..\.-) Text reviewed for obvious errors, including editorial review ~l'-5'

TS and/or 10 CFR references correct . '.\~j' If affidavit required or NOV response, verify Law Department has reviewed ..Y-5 Enclosures Enclosures labeled cH

Text reviewed for obvious errors, including editorial review

~**

Revision bars included (if applicable) AJJA References to other documents correct (e.g., HBLs, DSAR, etc.) ~ Submittal addresses the specific regulation requirements w-s Each enclosure is correctly paginated d~\' '" Commitments Commitment implemented before or after LA receipt (LARs/RAls only) Commitment(s) quoted verbatim (&clarifications made if needed) Tracking Document - SAPN and task numbers tJI '" Assigned To - Name & Organization Code Commitment Type - Firm or Target & Due Date CTS Commitment - Y or. N indicator & Implementing Documents An individual from all departments assigned commitments was a Cross-Discipline Reviewer Ci?' LER Forms LER number correct" consistent with cover letter i-'tlt LER number & docket number(s) on first & remaining pages Title c0nsistent with cover letter & Outgoing Correspondence Screen Dates correct on first page header (month, day, & year) Dates & times consistent with 10 CFR 50. 72 ENS reports made Dates & times consistent with other source documents Dates & times consistent between abstract and narrative Paae numbers correct & all pages accounted for Abstract word count <1400 characters (including spaces) IEEE 803 codes entered and correct 0 Record of Review Checklist completed and signed ~\,._,R ROR Checklist t\ rL ,. Final Draft All discrepancies resolved with Lead Licensing Engineer .Y-3

Enter N/A where not applicable.

I have reviewed this submittal for the items initialed above. This submittal is ready for the signatory. t%9J/c Performed

       -~ A~~12.&~                    ~-,-z ~s hee.--i ~,,......,e ... /lt.J.
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HBL-16-008, Request for Partial Release of Humboldt Bay Power Plant Unit 3 Property from the Part 50 Site

Text

Dear Commissioners and Staff:

Background:

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Dear Ms. Anderson:

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