ML17277A632: Difference between revisions

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| issue date = 06/21/1983
| issue date = 06/21/1983
| title = Rev 0 to Chemistry Procedure 12.10.7, Post-Accident Sampling & Analysis,Ph of Post-Accident Sample.
| title = Rev 0 to Chemistry Procedure 12.10.7, Post-Accident Sampling & Analysis,Ph of Post-Accident Sample.
| author name = MARTIN J
| author name = Martin J
| author affiliation = WASHINGTON PUBLIC POWER SUPPLY SYSTEM
| author affiliation = WASHINGTON PUBLIC POWER SUPPLY SYSTEM
| addressee name =  
| addressee name =  
Line 17: Line 17:


=Text=
=Text=
{{#Wiki_filter:0 WASHINGTON PUBLIC JJOONQQISBTIRBI 0LLEG PLAXT PRO(:El)t'RE ll:KiL:Itl.
{{#Wiki_filter:0 WASHINGTON PUBLIC JJOONQQISBTIRBI         0LLEG PLAXT PRO(:El) t'RE ll:KiL:Itl.
IVX P-PROCEDURE NUMBER<<12 m 10.7 VOLUME SAME APPRO D DATE 06/21/83 12 CHEMISTRY PROCEDURES SECTION 12.10 POST ACCIDENT SAMPLING AND ANALYSIS TITLE<<12.10.7 pH OF A POST ACCIDENT SAMPLE 12.1D.7.1 P~ur ose This procedure describes the analysis of an undiluted 1 ml sample obtained from the post accident sampling station.12.10.7.2 Precautions/Prere uisites A.Sample must be undiluted.
IVXP-PROCEDURE NUMBER             APPRO  D                    DATE
B.No analysis shall be performed unless conditions are ALARA.12.1D.7.S E~ui ment A.Micro pH probe B.pH probe holder (Attachment 1)C.Shielded storage area for pH,probe and holder D.Appropriate remote handling tools 12.1D.7.4 Reacaents pH 7 and pH 4 buffers 12.10.7 s 5 Procedure A.Buffer pH probe with pH 7 and pH 4 buf fers.CAUTION: Sample is highly radioactive.
                      <<12 10.7 m                                                            06/21/83 VOLUME SAME 12         CHEMISTRY PROCEDURES SECTION 12.10       POST ACCIDENT SAMPLING AND ANALYSIS TITLE
Dose rate instruments shall be in use to monitor the rest of the analysis.B.Remove cap from sample cask.C.With appropriate remote handling tools, insert pH probe holder through sample vial septum.8307050i73 830623 PDR ADOCK 05000397 E PDR PROCEDURE NUMBER REVISION NUMBER PAGE NUMBER WP.597 R]12.10.7 0 12.10.7-1 of 3 r 1 J t 0D.Pull to approximately 1/2 ml the syringe attached to the pH probe holder and measure the pH.E.Release the syringe, allowing sample to return to vial.F.Using approprate remote handling tools remove pH probe holder from the cask to the shielded storage area.G.Replace cap on the sample cask.H.Survey area for contamination.
                      <<12.10.7     pH OF A POST ACCIDENT SAMPLE 12.1D.7.1     P~ur ose This procedure describes the analysis of an undiluted             1 ml sample obtained from the post accident sampling station.
RQCKOURK NUMBKR 12.10.7 REVISION NUMBER 0!PAGE NUM BKR 12.10.7-2 of 3 SYRINGE I I TYGON TUBING HYPODERMIC NEEDLE 1" MICRO pH PROBE RUBBER STOPPER BIO RAD ION EXCHANGE COLUMN 3" HYPODERMIC NEEDLE W~9$pH Probe Holder Attachment 1 I"ROCKQURK NUM8KR (RKVISION NUM8KR)I'>0K NUMSKR 1 I l}}
12.10.7.2     Precautions/Prere     uisites A. Sample must be     undiluted.
B. No analysis shall be performed unless conditions are           ALARA.
12.1D.7.S     E~ui ment A. Micro   pH   probe B. pH probe holder (Attachment 1)
C. Shielded storage area for pH,probe and holder D. Appropriate remote handling tools 12.1D.7.4     Reacaents pH 7 and pH 4     buffers 12.10.7 s 5 Procedure A. Buffer   pH   probe with   pH 7 and pH 4 buf fers.
CAUTION:     Sample is highly radioactive. Dose rate instruments shall be in use   to monitor the rest of the analysis.
B. Remove cap     from sample cask.
C. With appropriate remote handling       tools, insert   pH probe holder through sample vial septum.
8307050i73 830623 PDR ADOCK     05000397 E                     PDR                   PROCEDURE NUMBER     REVISION NUMBER     PAGE NUMBER 12.10.7               0             12.10.7-1 of 3 WP.597 R ]
 
r 1
J t
 
D.
0 Pull to approximately 1/2 ml the syringe attached to the   pH probe holder and measure the pH.
E. Release the syringe, allowing sample to   return to vial.
F. Using approprate remote handling tools remove pH probe holder from the cask to the shielded storage area.
G. Replace cap on the sample cask.
H. Survey area for contamination.
RQCKOURK NUMBKR    REVISION NUMBER      PAGE NUMBKR 12.10.7               0       !   12.10.7-2 of 3
 
I I SYRINGE 1"
MICRO pH PROBE TYGON TUBING HYPODERMIC NEEDLE RUBBER STOPPER BIO RAD ION EXCHANGE COLUMN 3" HYPODERMIC   NEEDLE pH Probe Holder                                         )I'>0K NUMSKR I"ROCKQURK NUM8KR (RKVISION NUM8KR W~9$          Attachment 1          1       I                   l}}

Latest revision as of 14:56, 29 October 2019

Rev 0 to Chemistry Procedure 12.10.7, Post-Accident Sampling & Analysis,Ph of Post-Accident Sample.
ML17277A632
Person / Time
Site: Columbia Energy Northwest icon.png
Issue date: 06/21/1983
From: Martin J
WASHINGTON PUBLIC POWER SUPPLY SYSTEM
To:
Shared Package
ML17277A623 List:
References
12.10.7, NUDOCS 8307050173
Download: ML17277A632 (4)


Text

0 WASHINGTON PUBLIC JJOONQQISBTIRBI 0LLEG PLAXT PRO(:El) t'RE ll:KiL:Itl.

IVXP-PROCEDURE NUMBER APPRO D DATE

<<12 10.7 m 06/21/83 VOLUME SAME 12 CHEMISTRY PROCEDURES SECTION 12.10 POST ACCIDENT SAMPLING AND ANALYSIS TITLE

<<12.10.7 pH OF A POST ACCIDENT SAMPLE 12.1D.7.1 P~ur ose This procedure describes the analysis of an undiluted 1 ml sample obtained from the post accident sampling station.

12.10.7.2 Precautions/Prere uisites A. Sample must be undiluted.

B. No analysis shall be performed unless conditions are ALARA.

12.1D.7.S E~ui ment A. Micro pH probe B. pH probe holder (Attachment 1)

C. Shielded storage area for pH,probe and holder D. Appropriate remote handling tools 12.1D.7.4 Reacaents pH 7 and pH 4 buffers 12.10.7 s 5 Procedure A. Buffer pH probe with pH 7 and pH 4 buf fers.

CAUTION: Sample is highly radioactive. Dose rate instruments shall be in use to monitor the rest of the analysis.

B. Remove cap from sample cask.

C. With appropriate remote handling tools, insert pH probe holder through sample vial septum.

8307050i73 830623 PDR ADOCK 05000397 E PDR PROCEDURE NUMBER REVISION NUMBER PAGE NUMBER 12.10.7 0 12.10.7-1 of 3 WP.597 R ]

r 1

J t

D.

0 Pull to approximately 1/2 ml the syringe attached to the pH probe holder and measure the pH.

E. Release the syringe, allowing sample to return to vial.

F. Using approprate remote handling tools remove pH probe holder from the cask to the shielded storage area.

G. Replace cap on the sample cask.

H. Survey area for contamination.

RQCKOURK NUMBKR REVISION NUMBER PAGE NUMBKR 12.10.7 0  ! 12.10.7-2 of 3

I I SYRINGE 1"

MICRO pH PROBE TYGON TUBING HYPODERMIC NEEDLE RUBBER STOPPER BIO RAD ION EXCHANGE COLUMN 3" HYPODERMIC NEEDLE pH Probe Holder )I'>0K NUMSKR I"ROCKQURK NUM8KR (RKVISION NUM8KR W~9$ Attachment 1 1 I l