ML18075A013

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Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Vol. 3, Chapter 21, Survey Area Release Record for Land Survey Area 08, Survey Units 09, 12 and 13, Rev. 1, J16698-2 Uds Level 2 Report Final Report
ML18075A013
Person / Time
Site: 07000036
Issue date: 04/22/2016
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TestAmerica Labs - St. Louis, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
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Download: ML18075A013 (15)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16698-2 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:

4/22/2016 4:37:05 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-16698-2 Page 2 of 15 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

6 Definitions/Glossary.......................................

7 Method Summary.........................................

8 Sample Summary.........................................

9 Client Sample Results......................................

10 QC Sample Results........................................

13 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16698-2 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-16698-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)

Report Number: 160-16698-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 3/28/2016 11:11 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 20.0º C.

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L08-13-13-T-E-B-00 (160-16698-1), L08-13-14-T-E-B-00 (160-16698-2), L08-13-15-T-E-B-00 (160-16698-3),

L08-13-16-T-E-B-00 (160-16698-4) and L08-13-17-T-E-B-00 (160-16698-5) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 03/28/2016, prepared on 03/31/2016 and analyzed on 04/21/2016.

Preparation Batch 160-243065:

The samples, analyzed by gamma spectroscopy, resulted in an RPD/RER (relative percent difference/replicate error ratio) outside of the acceptance criteria of 40%/1 for protactinium 231. Both the sample and sample duplicates activity are less than the MDC. The data have been qualified and reported. L08-13-13-T-E-B-00 (160-16698-1), L08-13-14-T-E-B-00 (160-16698-2), L08-13-15-T-E-B-00 (160-16698-3),

L08-13-16-T-E-B-00 (160-16698-4), L08-13-17-T-E-B-00 (160-16698-5), (LCS 160-243065/2-A), (MB 160-243065/1-A) and TestAmerica St. Louis Page 3 of 15 1

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16698-2 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-16698-2 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

(160-16698-A-1-I DU)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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10 11 Procedure HOP-PR-QA-006,. Chain ;;,/Custody Hematite Decommissioning Project !Revision: 4 I

Page 1 ofll Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY

.Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified I before the sample is released for use or analysis and send the completed CoC to HOP.

Chain of Cutody ID No. I F-032816-02 Pa2:e 1/1 Project Name:

Westinghouse Electric Company Contact PerSon:

Clark Evers Phone Number:

314-810-3336 Sampler Name Donte Love Sample ID LOS-13-13-T-E-B-OO L08-13-I4-T-E-B-OO L08-13-15-T*E-B-OO L08-l 3-l 6-T-E-B-OO L08-13-l 7-T~E-B-OO Company Name:

Received by:

Company Name:

Date Time 3/24/2016 10:20 3/24/2016 10:30 3/24/2016 10:25 3/24/2016 10:35 3/24/2016 15:00 wa-Date/Time

,- 2-'if. 1 v 0'11~

Date/Time Matrix s

s s

s s

Company Name:

Date/Time-~ ~,

1-l,s-t:

'I'. n

~ "

Laboratorv Name:

TA-MO Laboratory Address:

13715 Rider Trail North

  • § PhoneNo..

8 314-298-8566 1§ Laboratory Contact Person:

~ Ivan Vania Phone No.

708-870-8453 Tum Around Tim~

Rush (7 days)

Remarks 1 ILSA 08-13 Sidewall Bias 1 ILSA 08-13 Bias LSA 08-13 Bias LSA 08-13 Bias 1 ILSA 08-13 Bias 160-16698 Chain of Custody Total

'Cooler Temperature:

5 Ambient Cooler ID: I Shipper and Number:

0328-01 Date/Time I Comments: NIA Verified By:

Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16698-2 Login Number: 16698 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

N/A Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time (excluding tests with immediate HTs)

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Qualifiers Rad Qualifier Description U

Result is less than the sample detection limit.

Qualifier F

Duplicate RPD exceeds the control limit Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 15 1

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Sample Summary TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-16698-1 L08-13-13-T-E-B-00 Solid 03/24/16 10:20 03/28/16 11:11 160-16698-2 L08-13-14-T-E-B-00 Solid 03/24/16 10:30 03/28/16 11:11 160-16698-3 L08-13-15-T-E-B-00 Solid 03/24/16 10:25 03/28/16 11:11 160-16698-4 L08-13-16-T-E-B-00 Solid 03/24/16 10:35 03/28/16 11:11 160-16698-5 L08-13-17-T-E-B-00 Solid 03/24/16 15:00 03/28/16 11:11 TestAmerica St. Louis Page 9 of 15 1

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Client Sample Results TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16698-1 Client Sample ID: L08-13-13-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:20 Date Received: 03/28/16 11:11 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.30 (2+/-)

0.186 (2+/-)

1 04/21/16 07:07 03/31/16 12:41 pCi/g 0.0772 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.336 0.409 0.383 1.39 Bismuth 212 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.0585 0.155 0.102 1.13 Bismuth 214 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.0818 0.178 0.0962 1.15 Lead 212 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.0846 0.166 0.0963 1.30 Lead 214 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.303 2.53 1.22 22.0 Potassium 40 pCi/g 03/31/16 12:41 04/21/16 07:07 1

1.30 0.800 0.796 U

-0.762 Protactinium 231 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.0585 1.00 0.155 0.102 1.13 Radium 226 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.0772 0.186 0.132 1.30 Thorium 232 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.871 0.558 0.544 1.16 Thorium 234 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.244 0.150 0.149 U

0.159 Uranium 235 pCi/g 03/31/16 12:41 04/21/16 07:07 1

0.0943 2.27 2.27 U

-0.0104 Americium 241 pCi/g 03/31/16 12:41 04/21/16 07:07 1

5.52 3.69 3.64 6.16 Protactinium 234m Tl-208 0.373 0.0454 0.0594 0.0317 pCi/g 03/31/16 12:41 04/21/16 07:07 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16698-2 Client Sample ID: L08-13-14-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:30 Date Received: 03/28/16 11:11 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.10 (2+/-)

0.169 (2+/-)

1 04/21/16 07:08 03/31/16 12:41 pCi/g 0.113 RL MDC 0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.330 0.396 0.373 1.29 Bismuth 212 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.0613 0.162 0.105 1.19 Bismuth 214 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.0647 0.153 0.0766 1.02 Lead 212 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.0775 0.158 0.0922 1.23 Lead 214 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.202 2.13 1.05 18.2 Potassium 40 pCi/g 03/31/16 12:41 04/21/16 07:08 1

1.17 0.221 0.217 U

0.377 Protactinium 231 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.0613 1.00 0.162 0.105 1.19 Radium 226 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.113 0.169 0.126 1.10 Thorium 232 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.830 0.571 0.539 1.81 Thorium 234 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.235 0.345 0.233 2.50 Uranium 235 pCi/g 03/31/16 12:41 04/21/16 07:08 1

0.105 0.0636 0.0635 U

0.0384 Americium 241 pCi/g 03/31/16 12:41 04/21/16 07:08 1

3.25 3.20 3.14 6.08 Protactinium 234m Tl-208 0.352 0.0447 0.0577 0.0325 pCi/g 03/31/16 12:41 04/21/16 07:08 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16698-3 Client Sample ID: L08-13-15-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:25 Date Received: 03/28/16 11:11 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.199 (2+/-)

1 04/21/16 07:09 03/31/16 12:41 pCi/g 0.156 RL MDC 0.160 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.372 0.401 0.384 1.11 Bismuth 212 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.0740 0.176 0.126 1.18 Bismuth 214 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.0739 0.163 0.0832 1.08 Lead 212 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.0776 0.183 0.118 1.34 Lead 214 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.242 2.19 1.29 17.2 Potassium 40 pCi/g 03/31/16 12:41 04/21/16 07:09 1

1.27 0.399 0.393 U

0.608 Protactinium 231 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.0740 1.00 0.176 0.126 1.18 Radium 226 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.156 0.199 0.160 1.15 Thorium 232 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.973 0.385 0.365 1.16 Thorium 234 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.263 0.226 0.223 0.360 Uranium 235 pCi/g 03/31/16 12:41 04/21/16 07:09 1

0.120 0.0719 0.0719 U

0.0192 Americium 241 pCi/g 03/31/16 12:41 04/21/16 07:09 1

5.86 3.99 3.97 U

3.06 Protactinium 234m Tl-208 0.363 0.0698 0.0793 0.0582 pCi/g 03/31/16 12:41 04/21/16 07:09 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16698-4 Client Sample ID: L08-13-16-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:35 Date Received: 03/28/16 11:11 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.169 (2+/-)

1 04/21/16 07:47 03/31/16 12:41 pCi/g 0.131 RL MDC 0.130 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.443 0.456 0.436 1.29 Bismuth 212 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.0742 0.181 0.123 1.27 Bismuth 214 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.0726 0.163 0.0864 1.06 Lead 212 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.0710 0.179 0.111 1.35 Lead 214 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.342 2.40 1.31 19.7 Potassium 40 pCi/g 03/31/16 12:41 04/21/16 07:47 1

1.16 0.195 0.195 U

0.179 Protactinium 231 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.0742 1.00 0.181 0.123 1.27 Radium 226 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.131 0.169 0.130 1.05 Thorium 232 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.946 0.334 0.320 U

0.915 Thorium 234 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.180 0.124 0.121 0.243 Uranium 235 pCi/g 03/31/16 12:41 04/21/16 07:47 1

0.107 0.0633 0.0633 U

-0.00114 Americium 241 pCi/g 03/31/16 12:41 04/21/16 07:47 1

4.97 2.84 2.84 U

0.000 Protactinium 234m Tl-208 0.387 0.0527 0.0663 0.0386 pCi/g 03/31/16 12:41 04/21/16 07:47 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16698-5 Client Sample ID: L08-13-17-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 15:00 Date Received: 03/28/16 11:11 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.27 (2+/-)

0.187 (2+/-)

1 04/21/16 07:48 03/31/16 12:41 pCi/g 0.0969 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.365 0.337 0.311 1.26 Bismuth 212 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.0730 0.170 0.109 1.26 Bismuth 214 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.0704 0.164 0.0805 1.10 Lead 212 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.0788 0.188 0.105 1.49 Lead 214 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.306 2.36 1.10 20.7 Potassium 40 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.786 0.467 0.466 U

0.201 Protactinium 231 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.0730 1.00 0.170 0.109 1.26 Radium 226 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.0969 0.187 0.138 1.27 Thorium 232 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.733 0.474 0.461 1.05 Thorium 234 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.239 0.143 0.143 U

-0.0621 Uranium 235 pCi/g 03/31/16 12:41 04/21/16 07:48 1

0.106 4.18 4.18 U

-0.00896 Americium 241 pCi/g 03/31/16 12:41 04/21/16 07:48 1

5.06 2.40 2.34 5.43 Protactinium 234m Pb-210 1.84 0.658 0.692 0.777 pCi/g 03/31/16 12:41 04/21/16 07:48 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.386 0.0579 0.0702 0.0452 pCi/g 03/31/16 12:41 04/21/16 07:48 1

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QC Sample Results TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-243065/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 247184 Prep Batch: 243065 Actinium 228 Analyte U

1 04/21/16 07:05 03/31/16 12:41 pCi/g 0.0723 MDC RL 0.00806 0.00806 (2+/-)

(2+/-)

MB 0.0008809 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.183 0.0987 0.0986 U

0.01923 Bismuth 212 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.0370 0.0406 0.0406 U

-0.004447 Bismuth 214 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.0178 0.0104 0.0104 U

0.007254 Lead 212 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.0310 0.00555 0.00550 U

0.006710 Lead 214 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.164 2.28 2.28 U

-0.05688 Potassium 40 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.282 0.164 0.164 U

0.08744 Protactinium 231 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.0370 1.00 0.0406 0.0406 U

-0.004447 Radium 226 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.0723 0.00806 0.00806 U

0.0008809 Thorium 232 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.278 0.295 0.295 U

-0.06181 Thorium 234 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.0617 0.0339 0.0339 U

0.008807 Uranium 235 1

04/21/16 07:05 03/31/16 12:41 pCi/g 0.0257 0.0145 0.0145 U

-0.002268 Americium 241 1

04/21/16 07:05 03/31/16 12:41 pCi/g 2.29 0.0500 0.0500 U

0.005149 Protactinium 234m Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 03/31/16 12:41 04/21/16 07:05 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-243065/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 247187 Prep Batch: 243065 Americium 241 Analyte 116 87 98 98.42 101 10.2 0.507 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 34.0 32.64 3.42 0.150 pCi/g 96 87 - 120 Cobalt 60 31.5 30.45 3.08 0.118 pCi/g 97 87 - 115 Client Sample ID: L08-13-13-T-E-B-00 Lab Sample ID: 160-16698-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 247184 Prep Batch: 243065 Actinium 228 Analyte 1

0.33 1.177 1.30 0.201 0.0965 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.39 1.181 0.358 0.418 pCi/g 0.27 1

Bismuth 214 1.13 1.172 0.165 0.0651 pCi/g 0.14 1

Lead 212 1.15 1.030 0.156 0.0670 pCi/g 0.37 1

Lead 214 1.30 1.113 0.155 0.0804 pCi/g 0.58 1

Potassium 40 22.0 19.06 2.25 0.285 pCi/g 0.62 1

Protactinium 231

-0.762 U 0.5998 U F 0.265 1.07 pCi/g 1.28 1

Radium 226 1.13 1.172 0.165 1.00 0.0651 pCi/g 0.14 1

Thorium 232 1.30 1.177 0.201 0.0965 pCi/g 0.33 1

Thorium 234 1.16 1.233 0.543 0.835 pCi/g 0.07 1

Uranium 235 0.159 U

-0.04614 U 0.220 0.250 pCi/g 0.55 1

Americium 241

-0.0104 U 0.009895 U 0.0588 0.0989 pCi/g 0.01 1

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QC Sample Results TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: L08-13-13-T-E-B-00 Lab Sample ID: 160-16698-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 247184 Prep Batch: 243065 Protactinium 234m Analyte 1

0.50 U

2.810 6.16 2.96 4.84 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Tl-208 1

0.53 0.3134 0.373 0.0535 0.0318 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 14 of 15 1

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QC Association Summary TestAmerica Job ID: 160-16698-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Rad Leach Batch: 242446 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16698-1 L08-13-13-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-1 DU L08-13-13-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-2 L08-13-14-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-3 L08-13-15-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-4 L08-13-16-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-5 L08-13-17-T-E-B-00 Total/NA Prep Batch: 243065 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 242446 160-16698-1 L08-13-13-T-E-B-00 Total/NA Solid Fill_Geo-21 242446 160-16698-1 DU L08-13-13-T-E-B-00 Total/NA Solid Fill_Geo-21 242446 160-16698-2 L08-13-14-T-E-B-00 Total/NA Solid Fill_Geo-21 242446 160-16698-3 L08-13-15-T-E-B-00 Total/NA Solid Fill_Geo-21 242446 160-16698-4 L08-13-16-T-E-B-00 Total/NA Solid Fill_Geo-21 242446 160-16698-5 L08-13-17-T-E-B-00 Total/NA Solid Fill_Geo-21 LCS 160-243065/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-243065/1-A Method Blank Total/NA TestAmerica St. Louis Page 15 of 15 1

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