ML18075A011

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Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Vol. 3, Chapter 21, Survey Area Release Record for Land Survey Area 08, Survey Units 09, 12 and 13, Rev. 1, J16618-2 Uds Level 2 Report Final Report
ML18075A011
Person / Time
Site: 07000036
Issue date: 04/19/2016
From:
TestAmerica Labs - St. Louis, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18074A285 List:
References
HEM-18-6
Download: ML18075A011 (23)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16618-2 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:

4/19/2016 3:53:37 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-16618-2 Page 2 of 23 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

9 Definitions/Glossary.......................................

10 Method Summary.........................................

11 Sample Summary.........................................

12 Client Sample Results......................................

13 QC Sample Results........................................

20 QC Association Summary...................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16618-2 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-16618-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)

Report Number: 160-16618-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 3/22/2016 10:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 20.0º C and 20.0º C. The container label for sample 160-16618-13 did not match the information listed on the Chain-of-Custody (COC): F-031816-02 The container labels list L08-13-12-T-E-S-00 while the COC lists L08-13-11-T-E-S-00 @14:30. The client was contacted and a corrected CoC was forwarded to the lab. The correct sample ID of L08-13-12-T-E-S-00 was entered for reporting purposes.

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L08-13-01-T-E-S-00 (160-16618-1), L08-13-02-T-E-S-00 (160-16618-2), L08-13-03-T-E-S-00 (160-16618-3),

L08-13-04-T-E-S-00 (160-16618-4), L08-13-05-T-E-S-00 (160-16618-5), L08-13-06-T-E-S-00 (160-16618-6), L08-13-07-T-E-S-00 (160-16618-7), L08-13-08-T-E-S-00 (160-16618-8), L08-13-09-T-R-S-00 (160-16618-9), L08-13-10-T-E-S-00 (160-16618-10),

L08-13-11-T-E-S-00 (160-16618-11), L08-13-11-T-E-Q-00 (160-16618-12) and L08-13-12-T-E-S-00 (160-16618-13) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 03/22/2016, prepared on 03/25/2016 and analyzed on 04/15/2016.

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16618-2 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-16618-2 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

Preparation Batch 160-242278:

The samples, analyzed by gamma spectroscopy, resulted in an RPD/RER (relative percent difference/replicate error ratio) outside of the acceptance criteria of 40%/1 for protactinium-231. Both the sample and sample duplicates activity are less than the MDC. The data have been qualified and reported. L08-13-01-T-E-S-00 (160-16618-1), (160-16616-A-1-H) and (160-16616-A-1-I DU)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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10 11 Procedure HDP-PR-QA-006, Chain ofCustody Page 1 of!

Hematite Decommissioning Project JRevision: 4 L

J Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organi2ation, a person from each organi2ation should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-031816-0L_Page Project Name:

Westinghouse Electric Company Contact Person:

Clark Evers Phone Number:

314=810-3336 Sampler Name Kyle Weldon I of2

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13715 Rider Trail North

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I Rush Turn Around Time (7 days)

Remarks L08-13-0 l-T-E-S-00 3/18/2016 13:50 L08-I3-02-T-E-S-OO 3/18/2016 13:52 L08-l 3-03-T-E-S-OO 3/18/2016 13:55 L08-l 3-04-T-E-S-OO 3/18/2016 14:00 L08-I3-05-T-E-S-OO 3/18/2016 14:10 L08-l 3-06-T-E-S-OO 3/1 8/2016 14:15 L08-13-07-T-E-S-OO 3/18/2016 14:18 L08-l 3-08-T-E-S-OO 3/18/2016 14:25 L08-13-09-T-R-S-OO 3/18/2016 15:30 L08-l3-10-T-E-S-00 3/18/2016 15:32 L08-l 3-l 1-T-E-S-OO 3/18/2016 14:35 L08-13-1 l-T-E-Q-OO 3/18/2016 14;35 Relinquished bv: Cf~vtA et,..,._7~

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Date/Time 3 /d-d--[ t1.o o~3o Total 13 Cooler ID:

0318-02/03 Cooler Temperature:

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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision. 4 I

Page 1 of !

Westinghouse Non-Proprietary Class 3

, '--'" nur-r 1'.-\\,lA.*vvu - 1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed Coe to HDP.

Chain of Cutody ID No.

F-031816-02 Paee 2 of 2

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Laboratorv Name:

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Vania, Ivan From:

Swanson, Martin B. (SAIC) [swansomb@westinghouse.com]

Sent:

Tuesday, March 22, 2016 12:40 PM To:

Vania, Ivan Cc:

Gorski, Chad J

Subject:

RE: Samples Going Out This Morning Page 1 of 2 3/22/2016 The sample ID on page 2 of CoC F03181602 is incorrect. Please make the following correction: L081312TE S00. A corrected CoC will be sent along with the sample shipment on 3/23/16.

Regards, MartinSwanson Environmental Engineer Hematite Decommissioning Project Westinghouse Electric Company 3300 State Road P Festus, MO 63028 Phone: 3148103321 Fax: 3148103301 From: Vania, Ivan [1]

Sent: Tuesday, March 22, 2016 12:19 PM To: Swanson, Martin B. (SAIC)

Subject:

FW: Samples Going Out This Morning Good Afternoon Martin, The sample on page two of this CoC has a label ID of L08-13-12-T-E-S-00. Please advise if the label ID shouldbe used.

Regards, IvanHVania Project Manager II TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 13715 Rider Trail North Earth City, MO 63045 Tel 314.298.8566 l Fax 314.298.8757 www.testamericainc.com Weappreciateyourbusiness!

From: Swanson, Martin B. (SAIC) [2]

Sent: Tuesday, March 22, 2016 9:25 AM To: Vania, Ivan Cc: Dedner, Connie

Subject:

Samples Going Out This Morning Samples going out this morning from Westinghouse - Hematite are listed on the attached CoCs.

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Regards, MartinSwanson Environmental Engineer Hematite Decommissioning Project Westinghouse Electric Company 3300 State Road P Festus, MO 63028 Phone: 3148103321 Fax: 3148103301 This e-mail may contain proprietary information of the sending organization. Any unauthorized or improper disclosure, copying, distribution, or use of the contents of this e-mail and attached document(s) is prohibited. The information contained in this e-mail and attached document(s) is intended only for the personal and private use of the recipient(s) named above. If you have received this communication in error, please notify the sender immediately by email and delete the original e-mail and attached document(s).

This e-mail may contain proprietary information of the sending organization. Any unauthorized or improper disclosure, copying, distribution, or use of the contents of this e-mail and attached document(s) is prohibited. The information contained in this e-mail and attached document(s) is intended only for the personal and private use of the recipient(s) named above. If you have received this communication in error, please notify the sender immediately by email and delete the original e-mail and attached document(s).

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16618-2 Login Number: 16618 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

N/A Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time (excluding tests with immediate HTs)

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Qualifiers Rad Qualifier Description U

Result is less than the sample detection limit.

Qualifier F

Duplicate RPD exceeds the control limit Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 11 of 23 1

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Sample Summary TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-16618-1 L08-13-01-T-E-S-00 Solid 03/18/16 13:50 03/22/16 10:45 160-16618-2 L08-13-02-T-E-S-00 Solid 03/18/16 13:52 03/22/16 10:45 160-16618-3 L08-13-03-T-E-S-00 Solid 03/18/16 13:55 03/22/16 10:45 160-16618-4 L08-13-04-T-E-S-00 Solid 03/18/16 14:00 03/22/16 10:45 160-16618-5 L08-13-05-T-E-S-00 Solid 03/18/16 14:10 03/22/16 10:45 160-16618-6 L08-13-06-T-E-S-00 Solid 03/18/16 14:15 03/22/16 10:45 160-16618-7 L08-13-07-T-E-S-00 Solid 03/18/16 14:18 03/22/16 10:45 160-16618-8 L08-13-08-T-E-S-00 Solid 03/18/16 14:25 03/22/16 10:45 160-16618-9 L08-13-09-T-R-S-00 Solid 03/18/16 15:30 03/22/16 10:45 160-16618-10 L08-13-10-T-E-S-00 Solid 03/18/16 15:32 03/22/16 10:45 160-16618-11 L08-13-11-T-E-S-00 Solid 03/18/16 14:35 03/22/16 10:45 160-16618-12 L08-13-11-T-E-Q-00 Solid 03/18/16 14:35 03/22/16 10:45 160-16618-13 L08-13-12-T-E-S-00 Solid 03/18/16 14:30 03/22/16 10:45 TestAmerica St. Louis Page 12 of 23 1

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Client Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-1 Client Sample ID: L08-13-01-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:50 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.04 (2+/-)

0.155 (2+/-)

1 04/15/16 18:13 03/25/16 10:09 pCi/g 0.120 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.438 0.346 0.330 0.995 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.0605 0.159 0.104 1.17 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.0608 0.154 0.0756 1.04 Lead 212 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.0747 0.149 0.0838 1.19 Lead 214 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.289 2.38 1.15 20.3 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 18:13 1

1.10 0.171 0.169 U

0.246 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.0605 1.00 0.159 0.104 1.17 Radium 226 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.120 0.155 0.113 1.04 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.914 0.728 0.716 1.28 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.195 0.143 0.143 U

0.0981 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 18:13 1

0.108 0.0645 0.0644 U

-0.0203 Americium 241 pCi/g 03/25/16 10:09 04/15/16 18:13 1

4.66 3.09 3.09 U

1.37 Protactinium 234m Tl-208 0.325 0.0440 0.0555 0.0336 pCi/g 03/25/16 10:09 04/15/16 18:13 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-2 Client Sample ID: L08-13-02-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:52 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.184 (2+/-)

1 04/15/16 11:21 03/25/16 10:17 pCi/g 0.133 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.496 0.403 0.386 1.11 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.0729 0.167 0.120 1.12 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.0853 0.175 0.101 1.11 Lead 212 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.0816 0.178 0.115 1.31 Lead 214 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.380 2.19 1.29 17.3 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.823 0.481 0.481 U

0.169 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.0729 1.00 0.167 0.120 1.12 Radium 226 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.133 0.184 0.147 1.08 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.782 0.525 0.505 1.37 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.260 0.164 0.164 U

0.120 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 11:21 1

0.109 0.0652 0.0651 U

0.0220 Americium 241 pCi/g 03/25/16 10:17 04/15/16 11:21 1

6.63 2.45 2.42 U

3.91 Protactinium 234m Tl-208 0.386 0.0564 0.0692 0.0430 pCi/g 03/25/16 10:17 04/15/16 11:21 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-3 Client Sample ID: L08-13-03-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:55 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.938 (2+/-)

0.157 (2+/-)

1 04/15/16 11:52 03/25/16 10:17 pCi/g 0.128 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.413 0.502 0.479 1.44 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.0659 0.158 0.103 1.16 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.0794 0.163 0.0911 1.05 Lead 212 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.0820 0.168 0.0992 1.30 Lead 214 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.291 2.27 1.13 19.3 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 11:52 1

1.10 0.355 0.347 U

0.643 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.0659 1.00 0.158 0.103 1.16 Radium 226 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.128 0.157 0.124 0.938 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.877 0.579 0.559 1.46 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.259 0.152 0.151 U

0.130 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 11:52 1

0.0970 0.0581 0.0581 U

0.0238 Americium 241 pCi/g 03/25/16 10:17 04/15/16 11:52 1

5.38 3.04 3.04 U

0.449 Protactinium 234m Tl-208 0.363 0.0521 0.0643 0.0412 pCi/g 03/25/16 10:17 04/15/16 11:52 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-4 Client Sample ID: L08-13-04-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:00 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.06 (2+/-)

0.157 (2+/-)

1 04/15/16 11:54 03/25/16 10:17 pCi/g 0.105 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.409 0.469 0.450 1.29 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.0703 0.167 0.116 1.16 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.163 0.101 0.0995 U

0.116 Lead 212 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.0690 0.173 0.103 1.33 Lead 214 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.231 2.33 1.24 19.3 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 11:54 1

1.13 0.283 0.281 U

0.318 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.0703 1.00 0.167 0.116 1.16 Radium 226 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.105 0.157 0.113 1.06 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.907 0.724 0.706 1.54 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.251 0.122 0.122 U

0.0884 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 11:54 1

0.104 0.0614 0.0614 U

-0.00107 Americium 241 pCi/g 03/25/16 10:17 04/15/16 11:54 1

4.57 2.48 2.48 U

0.00210 Protactinium 234m Tl-208 0.382 0.0496 0.0635 0.0376 pCi/g 03/25/16 10:17 04/15/16 11:54 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-5 Client Sample ID: L08-13-05-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:10 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.935 (2+/-)

0.142 (2+/-)

1 04/15/16 11:57 03/25/16 10:17 pCi/g 0.0813 RL MDC 0.106 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.319 0.403 0.380 1.30 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.0615 0.136 0.0928 0.966 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.0560 0.127 0.0661 0.834 Lead 212 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.0587 0.133 0.0755 1.05 Lead 214 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.323 1.87 0.948 16.0 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.952 0.207 0.202 U

0.408 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.0615 1.00 0.136 0.0928 0.966 Radium 226 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.0813 0.142 0.106 0.935 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.719 0.579 0.500 2.78 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.177 0.141 0.126 0.604 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 11:57 1

0.0907 0.0831 0.0830 U

-0.0403 Americium 241 pCi/g 03/25/16 10:17 04/15/16 11:57 1

2.68 2.63 2.58 5.36 Protactinium 234m Tl-208 0.296 0.0411 0.0511 0.0324 pCi/g 03/25/16 10:17 04/15/16 11:57 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-6 Client Sample ID: L08-13-06-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:15 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.33 (2+/-)

0.231 (2+/-)

1 04/15/16 11:59 03/25/16 10:17 pCi/g 0.137 RL MDC 0.188 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.796 0.529 0.521 0.842 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.0596 0.176 0.127 1.18 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.104 0.186 0.118 1.12 Lead 212 pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.0775 0.183 0.117 1.36 Lead 214 pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.461 2.43 1.50 18.7 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 11:59 1

1.11 0.392 0.385 U

0.657 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.0596 1.00 0.176 0.127 1.18 Radium 226 pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.137 0.231 0.188 1.33 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 11:59 1

1.00 0.647 0.632 1.35 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.289 0.155 0.155 U

0.113 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 11:59 1

0.125 0.0742 0.0742 U

-0.00396 Americium 241 pCi/g 03/25/16 10:17 04/15/16 11:59 1

6.56 3.42 3.41 U

1.79 Protactinium 234m Tl-208 0.392 0.0666 0.0781 0.0521 pCi/g 03/25/16 10:17 04/15/16 11:59 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 15 of 23 1

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Client Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-7 Client Sample ID: L08-13-07-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:18 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.10 (2+/-)

0.161 (2+/-)

1 04/15/16 12:24 03/25/16 10:17 pCi/g 0.0969 RL MDC 0.116 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.352 0.432 0.405 1.45 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.0591 0.160 0.101 1.19 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.0678 0.156 0.0791 1.04 Lead 212 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.0652 0.166 0.0939 1.32 Lead 214 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.397 2.21 1.11 18.7 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.997 0.230 0.226 U

0.371 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.0591 1.00 0.160 0.101 1.19 Radium 226 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.0969 0.161 0.116 1.10 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.864 0.303 0.290 U

0.823 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.251 0.138 0.138 U

0.111 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 12:24 1

0.107 0.0639 0.0638 U

-0.0168 Americium 241 pCi/g 03/25/16 10:17 04/15/16 12:24 1

5.08 2.92 2.92 U

0.962 Protactinium 234m Tl-208 0.354 0.0424 0.0561 0.0331 pCi/g 03/25/16 10:17 04/15/16 12:24 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-8 Client Sample ID: L08-13-08-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:25 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.01 (2+/-)

0.176 (2+/-)

1 04/15/16 12:28 03/25/16 10:17 pCi/g 0.101 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.393 0.406 0.391 1.05 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.141 0.117 0.103 0.536 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.0657 0.149 0.0765 0.985 Lead 212 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.0640 0.143 0.0913 1.06 Lead 214 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.274 2.14 1.12 17.8 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.951 0.235 0.232 U

0.332 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.141 1.00 0.117 0.103 0.536 Radium 226 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.101 0.176 0.143 1.01 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.736 0.289 0.274 0.865 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.210 0.0812 0.0812 U

0.0345 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 12:28 1

0.0958 0.0572 0.0572 U

-0.0146 Americium 241 pCi/g 03/25/16 10:17 04/15/16 12:28 1

4.37 2.44 2.44 U

0.325 Protactinium 234m Tl-208 0.351 0.0520 0.0635 0.0379 pCi/g 03/25/16 10:17 04/15/16 12:28 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-9 Client Sample ID: L08-13-09-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 15:30 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.03 (2+/-)

0.192 (2+/-)

1 04/15/16 12:31 03/25/16 10:17 pCi/g 0.122 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.395 0.469 0.448 1.33 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.0667 0.151 0.103 1.08 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.0773 0.159 0.0881 1.02 Lead 212 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.0662 0.165 0.0994 1.26 Lead 214 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.279 2.30 1.12 20.0 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 12:31 1

1.16 0.308 0.303 U

0.517 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.0667 1.00 0.151 0.103 1.08 Radium 226 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.122 0.192 0.162 1.03 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.877 0.325 0.304 1.10 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.174 0.140 0.134 0.382 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 12:31 1

0.105 0.0625 0.0624 U

0.00799 Americium 241 pCi/g 03/25/16 10:17 04/15/16 12:31 1

5.16 3.26 3.26 U

1.32 Protactinium 234m Tl-208 0.322 0.0463 0.0569 0.0363 pCi/g 03/25/16 10:17 04/15/16 12:31 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-10 Client Sample ID: L08-13-10-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 15:32 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.184 (2+/-)

1 04/15/16 12:37 03/25/16 10:17 pCi/g 0.0972 RL MDC 0.145 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.445 0.520 0.501 1.34 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.0639 0.150 0.100 1.08 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.0662 0.166 0.0823 1.12 Lead 212 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.0749 0.170 0.105 1.28 Lead 214 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.201 2.20 1.06 18.8 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 12:37 1

1.09 0.660 0.657 U

-0.497 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.0639 1.00 0.150 0.100 1.08 Radium 226 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.0972 0.184 0.145 1.12 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.795 0.603 0.592 1.08 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.181 0.143 0.142 U

0.155 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 12:37 1

0.0981 0.0582 0.0582 U

-0.00249 Americium 241 pCi/g 03/25/16 10:17 04/15/16 12:37 1

6.67 0.608 0.608 U

-0.0616 Protactinium 234m Tl-208 0.387 0.0495 0.0637 0.0349 pCi/g 03/25/16 10:17 04/15/16 12:37 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-11 Client Sample ID: L08-13-11-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:35 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.19 (2+/-)

0.207 (2+/-)

1 04/15/16 12:32 03/25/16 10:17 pCi/g 0.163 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.591 0.430 0.420 0.893 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.0788 0.207 0.143 1.44 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.0738 0.173 0.0926 1.13 Lead 212 pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.0875 0.188 0.116 1.42 Lead 214 pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.424 2.46 1.46 19.3 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 12:32 1

1.51 0.916 0.913 U

-0.675 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.0788 1.00 0.207 0.143 1.44 Radium 226 pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.163 0.207 0.167 1.19 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 12:32 1

1.00 0.412 0.392 1.22 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.253 0.211 0.209 0.308 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 12:32 1

0.113 0.0670 0.0670 U

-0.00432 Americium 241 pCi/g 03/25/16 10:17 04/15/16 12:32 1

7.02 4.17 4.16 U

2.43 Protactinium 234m Tl-208 0.393 0.0669 0.0783 0.0516 pCi/g 03/25/16 10:17 04/15/16 12:32 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-12 Client Sample ID: L08-13-11-T-E-Q-00 Matrix: Solid Date Collected: 03/18/16 14:35 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.27 (2+/-)

0.202 (2+/-)

1 04/15/16 13:30 03/25/16 10:17 pCi/g 0.119 RL MDC 0.155 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.386 0.437 0.417 1.25 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.0694 0.168 0.107 1.24 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.0783 0.166 0.0899 1.07 Lead 212 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.0676 0.173 0.0921 1.41 Lead 214 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.340 2.36 1.14 20.1 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 13:30 1

1.19 0.726 0.723 U

-0.566 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.0694 1.00 0.168 0.107 1.24 Radium 226 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.119 0.202 0.155 1.27 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.832 0.300 0.284 0.928 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.232 0.143 0.141 U

0.175 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 13:30 1

0.0768 0.0456 0.0456 U

-0.0114 Americium 241 pCi/g 03/25/16 10:17 04/15/16 13:30 1

4.83 2.84 2.83 U

1.69 Protactinium 234m Tl-208 0.354 0.0475 0.0601 0.0360 pCi/g 03/25/16 10:17 04/15/16 13:30 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

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Client Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-13 Client Sample ID: L08-13-12-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:30 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.167 (2+/-)

1 04/15/16 13:33 03/25/16 10:17 pCi/g 0.106 RL MDC 0.125 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.412 0.500 0.478 1.40 Bismuth 212 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.0692 0.164 0.112 1.15 Bismuth 214 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.0694 0.151 0.0815 0.980 Lead 212 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.0739 0.149 0.0900 1.15 Lead 214 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.406 2.40 1.30 19.7 Potassium 40 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.770 0.544 0.528 1.22 Protactinium 231 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.0692 1.00 0.164 0.112 1.15 Radium 226 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.106 0.167 0.125 1.08 Thorium 232 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.852 0.551 0.537 1.15 Thorium 234 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.166 0.112 0.111 0.170 Uranium 235 pCi/g 03/25/16 10:17 04/15/16 13:33 1

0.102 0.0610 0.0610 U

0.0264 Americium 241 pCi/g 03/25/16 10:17 04/15/16 13:33 1

6.39 2.43 2.37 U

5.31 Protactinium 234m Tl-208 0.321 0.0487 0.0590 0.0380 pCi/g 03/25/16 10:17 04/15/16 13:33 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 19 of 23 1

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QC Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-242278/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246244 Prep Batch: 242278 Actinium 228 Analyte U

1 04/15/16 14:41 03/25/16 10:09 pCi/g 0.0870 MDC RL 0.0467 0.0467 (2+/-)

(2+/-)

MB

-0.01260 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.311 0.166 0.166 U

-0.02914 Bismuth 212 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.0181 0.0156 0.0156 U

0.0000 Bismuth 214 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.0274 0.0243 0.0242 U

-0.002973 Lead 212 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.0313 0.0139 0.0139 U

0.001726 Lead 214 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.237 2.33 2.33 U

-0.05829 Potassium 40 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.333 0.169 0.169 U

-0.008713 Protactinium 231 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.0181 1.00 0.0156 0.0156 U

0.0000 Radium 226 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.0870 0.0467 0.0467 U

-0.01260 Thorium 232 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.288 0.155 0.155 U

-0.01497 Thorium 234 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.0745 0.0346 0.0346 U

0.004824 Uranium 235 1

04/15/16 14:41 03/25/16 10:09 pCi/g 0.0225 0.0124 0.0124 U

-0.002749 Americium 241 1

04/15/16 14:41 03/25/16 10:09 pCi/g 3.73 0.600 0.600 U

0.0000 Protactinium 234m Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 03/25/16 10:09 04/15/16 14:41 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242278/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246245 Prep Batch: 242278 Americium 241 Analyte 116 87 98 98.78 101 10.3 0.503 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 34.0 32.70 3.42 0.145 pCi/g 96 87 - 120 Cobalt 60 31.6 29.63 2.99 0.119 pCi/g 94 87 - 115 Client Sample ID: Duplicate Lab Sample ID: 160-16616-A-1-I DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 246252 Prep Batch: 242278 Actinium 228 Analyte 1

0.55 1.086 1.28 0.165 0.110 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.71 1.219 0.334 0.243 pCi/g 0.64 1

Bismuth 214 1.35 1.187 0.162 0.0658 pCi/g 0.46 1

Lead 212 1.21 1.124 0.164 0.0599 pCi/g 0.24 1

Lead 214 1.55 1.389 0.174 0.0897 pCi/g 0.45 1

Potassium 40 23.6 20.70 2.43 0.363 pCi/g 0.57 1

Protactinium 231 0.638 U

-0.7669 U F 0.759 1.23 pCi/g 1.34 1

Radium 226 1.35 1.187 0.162 1.00 0.0658 pCi/g 0.46 1

Thorium 232 1.28 1.086 0.165 0.110 pCi/g 0.55 1

Thorium 234 1.75 1.356 0.344 0.860 pCi/g 0.42 1

Uranium 235 0.532 0.4079 0.157 0.197 pCi/g 0.36 1

Americium 241 0.0142 U 0.02613 U 0.0577 0.0961 pCi/g 0.1 1

TestAmerica St. Louis Page 20 of 23 1

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QC Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Duplicate Lab Sample ID: 160-16616-A-1-I DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 246252 Prep Batch: 242278 Protactinium 234m Analyte 1

0.01 U

1.429 1.49 U 2.91 4.99 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Tl-208 1

0.06 0.3800 0.388 0.0603 0.0334 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides Client Sample ID: Method Blank Lab Sample ID: MB 160-242279/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246251 Prep Batch: 242279 Actinium 228 Analyte U

1 04/15/16 11:19 03/25/16 10:17 pCi/g 0.0493 MDC RL 0.0270 0.0269 (2+/-)

(2+/-)

MB 0.01540 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.203 0.107 0.107 U

0.005256 Bismuth 212 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.0380 0.0173 0.0173 U

0.01019 Bismuth 214 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.0257 0.0194 0.0194 U

-0.002944 Lead 212 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.0296 0.0208 0.0208 U

-0.002353 Lead 214 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.312 0.254 0.254 U

-0.04821 Potassium 40 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.373 0.207 0.207 U

0.03123 Protactinium 231 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.0380 1.00 0.0173 0.0173 U

0.01019 Radium 226 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.0493 0.0270 0.0269 U

0.01540 Thorium 232 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.318 0.195 0.195 U

-0.01717 Thorium 234 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.0749 0.0452 0.0451 U

0.02434 Uranium 235 1

04/15/16 11:19 03/25/16 10:17 pCi/g 0.0295 0.0158 0.0158 U

0.0003897 Americium 241 1

04/15/16 11:19 03/25/16 10:17 pCi/g 1.88 1.08 1.08 U

0.5837 Protactinium 234m Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 03/25/16 10:17 04/15/16 11:19 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242279/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246252 Prep Batch: 242279 Americium 241 Analyte 116 87 94 94.13 101 9.79 0.462 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 34.0 32.09 3.36 0.154 pCi/g 94 87 - 120 Cobalt 60 31.6 29.25 2.95 0.0849 pCi/g 93 87 - 115 TestAmerica St. Louis Page 21 of 23 1

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QC Sample Results TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: L08-13-02-T-E-S-00 Lab Sample ID: 160-16618-2 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 246252 Prep Batch: 242279 Actinium 228 Analyte 1

0.40 0.9412 1.08 0.168 0.114 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.11 1.115 0.373 0.350 pCi/g 0

1 Bismuth 214 1.12 1.095 0.144 0.0488 pCi/g 0.07 1

Lead 212 1.11 0.9886 0.145 0.0555 pCi/g 0.37 1

Lead 214 1.31 1.224 0.154 0.0616 pCi/g 0.27 1

Potassium 40 17.3 17.44 2.04 0.241 pCi/g 0.04 1

Protactinium 231 0.169 U 0.6529 U 0.282 0.961 pCi/g 0.63 1

Radium 226 1.12 1.095 0.144 1.00 0.0488 pCi/g 0.07 1

Thorium 232 1.08 0.9412 0.168 0.114 pCi/g 0.40 1

Thorium 234 1.37 1.012 0.441 0.679 pCi/g 0.37 1

Uranium 235 0.120 U 0.1773 0.117 0.161 pCi/g 0.20 1

Americium 241 0.0220 U

-0.01967 U 0.0555 0.0926 pCi/g 0.35 1

Protactinium 234m 3.91 U 6.687 2.79 4.18 pCi/g 0.53 1

Tl-208 1

0.36 0.3410 0.386 0.0545 0.0309 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 22 of 23 1

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QC Association Summary TestAmerica Job ID: 160-16618-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Rad Leach Batch: 241584 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16616-A-1-I DU Duplicate Total/NA Solid Dry and Grind 160-16618-1 L08-13-01-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-2 L08-13-02-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-2 DU L08-13-02-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-3 L08-13-03-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-4 L08-13-04-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-5 L08-13-05-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-6 L08-13-06-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-7 L08-13-07-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-8 L08-13-08-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-9 L08-13-09-T-R-S-00 Total/NA Solid Dry and Grind 160-16618-10 L08-13-10-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-11 L08-13-11-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-12 L08-13-11-T-E-Q-00 Total/NA Solid Dry and Grind 160-16618-13 L08-13-12-T-E-S-00 Total/NA Prep Batch: 242278 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 241584 160-16616-A-1-I DU Duplicate Total/NA Solid Fill_Geo-21 241584 160-16618-1 L08-13-01-T-E-S-00 Total/NA Solid Fill_Geo-21 LCS 160-242278/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-242278/1-A Method Blank Total/NA Prep Batch: 242279 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 241584 160-16618-2 L08-13-02-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-2 DU L08-13-02-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-3 L08-13-03-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-4 L08-13-04-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-5 L08-13-05-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-6 L08-13-06-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-7 L08-13-07-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-8 L08-13-08-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-9 L08-13-09-T-R-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-10 L08-13-10-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-11 L08-13-11-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16618-12 L08-13-11-T-E-Q-00 Total/NA Solid Fill_Geo-21 241584 160-16618-13 L08-13-12-T-E-S-00 Total/NA Solid Fill_Geo-21 LCS 160-242279/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-242279/1-A Method Blank Total/NA TestAmerica St. Louis Page 23 of 23 1

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